NCS000329_Monitoring Reports_20170316

I
March 16, 2017
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
MAR 2 1 2017
CENTRAL FILES
QWR SECTION
Aw
r+rATI
P.O. Box 5030
2020 Asheraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: joe.hinklena,atimetals.com
Attached, please find stormwater monitoring data foi Peiinit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoriig Period
Sample Number
Start
End
Year 7 — Period 2
14
1 September 1, 2016
February 28, 2017
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Since ely,
UC-
Joe inkle
Environmental Manager

A
Nickel, total recoverabAl
IN
A 1 100
®o 1) /,?A 1 0.067
Oil and Grease Alp 20
Temp (receiving stream) (deg f Q 32 :(deg Q
Total Residual Chlorine A A 1 0.017
M
. .0 (std units) 1 6-9 (std units)
Storm Date: - SY P Storm Duration: J. o?.5- (Hrs.) Inches of Rainf&H: -e9-6
lvraflon of time preceding rain event exceeding 0.1": S60 (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Perviotis Area) + Q(finpervious Area)
Q(tot., c1s) = (A x inches rain/1 2 inches/ft. x 69 acres x .66) +.9 x inches rain/12inches/it. x 69 x 34)
Q(Total, cfs) = 1.5180 x D-( P 0 (Inches ®f rain) + 1.7595 x (Inches of rain

c r
aceAnaljdical
www.pacefabs.com
February 15, 2017
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92329088
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
JQ pC
��g80RIC���
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

Pace Analytical Services, LLC
® 9800 Kincey Ave. Suite 100
aceAna1Xka1 Huntersville, NC 28078
wmpacelabs.com [phone]
s
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92329088
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAN Certification #: E8/648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification M 40
South Carolina Certification M 99030001
VirginiaNELAP Certification #: 460222
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

ace naljlti l
wwwparelabs.cam
r
•
Project: BAKERS STORMWATER
Pace Project No.: 92329088
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
Reported
Laboratory
92329088001 BSW01 EPA 1664B
JMS
1
PASI-C
Er'A 200.7
SCR
5
PA81-A
SM 2540D
ALC
1
PASI-A
SM 4600• Cl G
MDW
1
PASI-A
SM 5210B
C.I1-11
1
PASI-A
SM 5220D
MDW
1
PASI-A
• • •
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C. Page 3 of 15

ace rra1j cal
www.pacelab&com
I
Project: BAKERS STORMWATER
Pace Project No.: 92329088
Sample: BSW01
Parameters
Field Data
Collected By
Collected Date
Collected Time
Meld pH
Field Temperature
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
45000L G Chlorine, Residual
Chlorine, Total Residual
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
u
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92329088001 Collected: 02/08/17 02:40 Received: 02/08/17 11:15 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method:
DPJ
.1
02/09/17 11:38
02/08/17
1
02/09/17 11:38
02:55
1
02/09/17 11:38
1.0 Std. Units
0.10
1
02/09/1 / '11:38
13.8 deg C
0.50
1
02/09/17 11:38
Analytical Method: EPA 1664B
ND mg/L
5.0
1
02/15/17 07:35
Analytical Method: EPA200.7 Preparation Method: EPA200.7
ND ug/L
1.0
1
02/09/17 21:00 02/13/17 18:22
7440-43 0
ND ug/L
5.0
1
02/09/17 21:00 02/13/17 18:22
7440-47-3
18.4 ug/L
5.0
1
02/09/17 21:00 02/13/17 18:22
7440-50-8
ND ug/L
5.0
1
02/09/17 21:00 02/13/17 18:22
7440-02-0
12.8 ug/L
10.0
1
02/09/17 21:00 02/13/17 18:22
7440-66-6
Analytical Method: SM 2540D
7.2 mg/L
2.5
1
02/10/1714:36
Analytical Method: SM 4500-CI G
0.092 mg/L
0.024
1
02/09/17 20:45
7782-50-5
Analytical Method: SM 5210B
4.3 mg/L
Analytical Method: SM 5220D
38.0 mg/L
2.0 1 02/09/17 03:25 02/13/17 23:40
25.0 1
02/09/17 22:59
H1
Date: 02/15/2017 07:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 15

f`
ace nalj4 I
-f wwwpacelabs.cam
I
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 348256
QC Batch Method: EPA 1664E
Associated Lab Samples: 92329088001
METHOD BLANK: 1932211
Associated Lab Samples: 92329088001
Parameter t Inits
Oil and Grease mg/L
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result I irnit Analyzed CtualifiHl+;
ND 5.0 02/15/ 17 07:32
LABORATORY CONTROL SAMPLE: 1932212
Spike LCS LCS
Parameter Units Conc. Result % Rec
Oil and Grease mg/L 40 36.9 92
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
78-114
MATRIX SPIKE SAMPLE: 1932213
35293826002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 1.1 U 40 36.0 90 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15

Pace Analytical Services, LLC ,A
Analytical'
9800 Kincey Ave. Suite 100 -
Huntersville, NC 28078
w w.pacelabs.com
[phone]
QUALITY CONTROL
DATA
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 347561
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92329088001
METHOD BLANK: 1928155
Matrix: Water
Associated Lab Samples: 92329088001
Blank Reporting
Parameter
Units
Result L imit
Analyzed
Qualifiers
Cadmium
ug/L
ND
1.0 02/13/1717:01
Chromium
ug/L
ND
5.0 02/13/1717:01
Copper
ug/L
ND
5.0 02/13/1717:01
Nickel
ug/L
ND
5.0 02/13/1717:01
Zinc
ug/L
ND
10.0 02/13/1717:01
LABORATORY CONTROL SAMPLE: 1928156
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Cadmium
ug/L
500 556
111
85-115
Chromium
ug/L
500 554
111
85-115
Copper
ug/L
500 573
115
85-115
Nickel
ug/L
500 547
109
85-115
Zinc
ug/L
500 558
112
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1928157
1928158
MS
MSD
92329043019
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
537
540
107
108
70-130
1
Chromium
ug/L
NO
500
500
521
538
104
108
70-130
3
Copper
ug/L
NO
500
500
546
559
109
112
70-130
2
Nickel
ug/L
ND
500
500
518
528
104
106
70-130
2
Zinc
ug/L
ND
500
500
528
539
105
108
70-130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928159
MS
92328962003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1928160
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
561
559
112
112
70-130
0
Chromium
ug/L
0.013
500
500
552
544
108
106
70-130
2
mg/L
Copper
ug/L
0.011
500
500
593
589
116
116
70-130
1
mg/L
Nickel
ug/L
0.012
500
500
548
544
107
106
70-130
1
mg/L
Zinc
ug/L
0.085
500
500
634
621
110
107
70-130
2
mg/L
Results presented on this page are in
the units indicated by the "Units" column except where an alternate
unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15

�v
ace nalj6cal
wwwpacelabs.com
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 347724 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92329088001
METHOD BLANK: 1929058 Matrix: Water
Associated Lab Samples: 92329088001
Blank Reporting
Paramoter I.Inits Result I, imit Analysed Qualifiers
Total Suspended Solids mg/L ND 2.5 02/10/1 / 14:18
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1929059
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 240 96 90-11,10
SAMPLE DUPLICATE: 1929060
92328982003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
14.5
13.8 5
SAMPLE DUPLICATE: 1929061
92329112001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

ace nalj l
1 WM.pacelabs.cdm
i
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 347682 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92329088001
METHOD BLANK: 1928900 Matrix: Water
Associated Lab Samples: 92329088001
Blank Reporting
Pararnotor Wills Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 02/09/17 20:45
SAMPLE DUPLICATE: 1928901
92328999001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L NO ND H1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

tr=
ce nalj cal
wwwpacelabs.corn
R •, 11 . O; .
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 347491 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92329088001
METHOD BLANK: 1927949 Matrix: Water
Associated Lab Samples: 92329088001
Blank Reporting
Parameter Units Rosult Llrriit Arialyzc;d Qualifiera
BOD, 5 day mg/L ND 2.0 02/13/17 23:40
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1927950
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
BOD, 5 day
mg/L
198 170 86
84.6-115.4
SAMPLE DUPLICATE: 1027951
92329036001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

cenalyticl
www.pacelabs.com
1
LO I
Project: BAKERS STORMWATER
Pace Project No.: 92329088
QC Batch: 347683 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92329088001
METHOD BLANK: 1928918
Associated Lab Samples: 92329088001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 1928919
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Rrwiull Limit Analysed uualirlets
.a_
ND 25.0 02/09/17 22:59
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 754 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928920 1928921
MS MSD
92329195001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 2110 750 750 2600 2600 66 66 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928922 1928923
MS MSD
92329088001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Chemical Oxygen Demand mg/L 38.0 750 750 798 795 101 101 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

Pace Analytical Services, LLC
aceAnalytical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
1
f
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92329088
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting I imit
S - Surrogate
1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
t •
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

/- Ice nalj l
nnasvpacalabs.can
r'
i
Project: BAKERS STORMWATER
Pace Project No.: 92329088
Pace Analytical Services, LLC a
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Analytical
Batch
92329088001
BSW01
92329088001
BSW01
EPA1664B
348256
92329088001
BSW01
EPA 200.7
347561 EPA 200.7
347718
92329088001
BSW01
SM 2540D
347724
92329088001
88W01
SM 4500-Cl V
347682
92329088001
BSW01
SM 5210B
347491 SM 5210B
347499
92329088001
BSW01
SM 5220D
347683
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15

d I aceAnaljdlol•
vucument rvame: uocument Revised: Sept. 21, 2016
Condition Upon Recelpt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Qualitv Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersviile Raleigh[] Mechanicsville[)
slowClient Nameq:, WVOW• 92329088
Courier. QFed Ex QUPS ❑USPs Pent
❑ Commercial FlPace QOther: ttt
9232 088
Custody Seal Present? ❑Yes No Seals Intact? OYes ENo
Date/initials Person Examining Contentst.. - S' %
Packing Material: ❑Bubble Wrap E5Bubble Bags ❑None ❑Other: y
Thermometer,
IR fun ll)r ( Wet ❑Blue ❑None. ampies on Ice, cooling process has begun
Type of Ice-
Col. rectlan Factor: Cooler f einp Corrected (.�I: 1 Biological. Tissue Frozen? ()Yes WN5 ❑N/A
Temp should be above �f.r,e� zing to 6°C
L1
USDA Regulate •Soil ( N/A, water sample)
Did samples qdginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (tntenw(lonaily,
Elves o including Hawaii and Puerto Rico)? ❑Yes Mo
Chain of Custody Present? es ON. ON/A 1.
Samples Arrived within Hold Time? es ❑No ON/A 2.
Short Hold Time Analysis (472 hr.)? es ❑No QN/a 13.
Rush Turn Around Time Requested? OYes Offo ON/A 4.
Sufficient Volume? es ON, ❑N/A S.
-orrect Containers Used? es ON. ❑NIA 1 6.
samples Field Filtered?
;ample Labels Match COC?
feadspace in VOA Vials (>5-6mm)?
"rip Blank Present?
'rip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
7.
8. Note if
27es ONO ❑N/A 19.
OYes ❑No
1Q.
11.
Date/Time:
In the dissolved container .=:
Field Data Required? ❑Yes ❑No
Date: a�
T
Date:
ote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be.sriit to the Nur th Carolina DEHNH Certification Office (i.e,
ut of hold, incorrec3 preservative, out of temp, Incorrect containers)
Page 13 of 15

Document Name:
Document Revised: Sept. 21, 2016
a?clg alj/f/C7/
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
Project WO#42329088
is
verified and within the acceptance range for
preservation samples.
�
PN'MWB
Oue Date: 02/17/17
**Bottom half of box is to list
number
of bottles
i/
!j '�
CLIENT: B2—A1
lilac NC
Z Z Z \ V
o
M
N
E
`y
1
Z
Z
.G
A
^
Z N
N
ei
=
•Z••
d
;
V
U
Z
Q
Z
z
=
1
v1
\
.�
iyy9
U
x
a
i.
a\
,77
M
Q
1 s
ina
m
3
V
?
u
a
NC
�
SOc
O
> > n=
QQ
Z
Z
.D
O
E
ZO
,Z
M
a<
=
nr
dN
ZxN
i
a a n JR
a
V
1Ln
O
.6
E E
a
E
Ln
�b
�L
Q
O
C
.i y
•-
d
„
yy
R1
a
a
J
@
Q Q
J
Q
<
J
J
N
�.
In
J
J
N
E E E `w E
v1 0 0 != o
1N-I N V) rl N
E
0
N
E
0
ry
E
0
�
'
3
a
=
c
N
`w
E
o
ern
(J
E
E
E
s
S
E
N
E
N
E
o d
N C
E
N
E
W
sf M N A M
a a a n. a
M
T
M
a
a
O t9
t7
t7
U'
C7
011
C7
i7
C? O
Li
a
pM ®
(�J1 Z
}
Q >
}
N
N
m
7 C7
1
N
\N\,
N\
I'N
1 3
N
I
N%\N
NNI
I
7
N
INNNN
N,
I
s
N
N
NNN
N
NN
7
\N\N
N
8
9
N
NNNN
\d
10
,
NNN\
N
—
it
12
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Page 14 of 15

w
(N UJ
�
lnelul saldweg
J
N
0
U
Z
w
u
o
(N!A)
<-)
Z
itF
o
Z
tOi
I61000 paleaS
c -Y
0 0
a
J
dpolsn0
l _ L
\ w
y
a
N
(NIA) ON
IL
�
uo panl030a
`
(N/A) auuolyO lenplsaa
�-
z
O
0. ul dwel
a
LU
w
�.
Q
U
rJ
3
0
/®
l;
w
u'.
Q
O f-
;,
q
v
�f"2tt�4 1, Q
d
7
tl n
)n
m
a
LL
/
pNU
i;sal sIslgeudj
m
°
y
)ay10
y
w
louey)aW
U
¢
VS7UN
HOeN
Qd
L.,
2
h
v
c ONH
€
E
a
.
°OSZH
U
Q
_
paniasa)duN
_
u "�
ti
n
H 8
O
"g 8 2
o
a`
$
,X
Sa3NIV1N0030#
'^
w
w
w
N0110311001V dW313ldWVS
A
r
I
O
S
Z
fJ
W
zw
z
a f
w
w
Z
O
W
LL
N
c
dJ
U
W
~
LL
LL
a
a
t
1
v
¢
G
a
W
14)
j
(&100=0 9V80=9) 3dA13ldVJVS
r •
U
1
c
Z
`)
(llal s) sapw p;en ass) 3000 XINIVW
'y
y '
„ `�'
0 1�
�'
E
a
o f
o
O`LU
H
z
Z
«O
1
7 a
�..
v m u
oP
e
c��
a
NK a:U
a
a`
a
V c`
is `m
_
tit
C)
g< g'�d�o
o33a`Ul)0 4-6
z
w
0
W
0
�1
�3
y
T
J
® z
ti
ui ? W
ZO
CL N g
�
•�
o
a�=a
o
��
��
�s
�
rJ
5a
o e
�1
`�cl
°� a d
bi
n&
ti0
ge15of15
# W311
N
M
v
m
r
w
a
;V
v� ci a
w Lo
car
a
CL

Alivae - Bakers Plant
Stormwater Monitoring Revort Fonn
Sample Date: 9-/;l Sample Time:
Sample Location:
Laboratory Performing Anatysis:
Results of
IM
Chromium, total recoverable
M1W
Stormwater Discharge Outfall #02 (Non -Commingled)
Drainage Area = 212 952s 4.9 acres
% Impervious = 12%
40 CFR Part 136
(std uni
Benchmark -Values (mg/1)
30
120
100
0.001
1
0.007
0.26
0.067
6-9 (std units)
Storm Date: A -9 �17 Storm Duration: (Hrs.) Inches of Rainfall:
lip Fpii�11!111�ppq� pppqi g
Estimated Flow Calculation:
Q = CIA
Q(TOW) = Q(Pervious Area) + Wnpervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x.88) +.9 x inches rain/12inches/ft. x 4.9 x.12)
Q(Total, cfs) = 0.1437 x 0-60 (Inches o of rain) + 0.0441 x (Inches of rain)
cfs

Pace Analytical Services, LLC
aceAnalytical ® 9800 KinceyAve. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
February 15, 2017
Mr. Joe Hinkle
Allvac
RE: Project: Bakers Stormwater
Pace Project No.: 92329090
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

aceAnalytical
f www.peo0abs.com
t
Project: Bakers Stormwater
Pace Project No.: 92329090
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NFL AP C'ortifictation # F87648
Massachusetts Certification #: M NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Cortificfatinn # 4ttt030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13

a&
y ` acemaoeal
www.pacelabScan
Project: Bakers Stormwater
Pace Project No.: 92329090
Lab ID Sample ID
92329090001 BSW02
SAMPLE ANALYTE COUNT
Method
EPA 200.7
SM 2540D
SM 5210B
SM 5220D
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts
Reported
Laboratory
SER
5
PASI-A
ALC
1
PASI-A
CJH1
1
PASI-A
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

Z�l
;aceAna1j&ca1@
f www.pacetabs.corn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100 '
Huntersville; NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92329090
Sample: BSW02
Lab ID: 92329090001 Collected: 02/08/17 02:15 Received: 02/08/17 11:15 Matrix: Water
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ 1
02/09/17 12:11
Collected Date
02/08/17 1
02/09/17 12:11
Collected Time
02:29 1
02/09/17 12:11
Field pH
7.2 Std. Units 0.10 1
02/09/17 12:11
Field Temperature
14.3 deg C 0.50 1
02/09/17 12:11
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND ug/L 1.0 1 02/09/17 21:00
02/13/17 18:25
7440-43-9
Chromium
13.9 ug/L 5.0 1 02/09/17 21:00
02/13/17 18:25
7440-47-3
Copper
422 ug/L 5.0 1 02/09/17 21:00
02/13/17 18:25
7440-50-8
Nickel
14.2 ug/L 5.0 1 02/09/17 21:00
02/13/17 18:25
7440-02-0
Zinc
131 ug/L 10.0 1 02/09/17 21:00
02/13/17 18:25
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
48.9 mg/L 3.5 1
02/10/17 14:36
5210E BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
14.8 mg/L 2.0 1 02/09/17 03:25
02/13/17 23:40
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
66.0 mg/L 25.0 1
02/09/17 22:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

acMnalj cal
www.pacetabs.com
t
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92329090
QC Batch: 347561
Analysis Method: EPA
200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92329090001
METHOD BLANK: 1928155
Matrix: Water
Associated Lab Samples: 92329090001
Dlank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug/L
ND 1.0
02/13/1717:01
Chromium
ug/L
ND 5.0
02/13/1717:01
Copper
ug/L
ND 5.0
02/13/1717:01
Nickel
ug/L
ND 5.0
02/13/1717:01
Zinc
ug/L
ND 10.0
02/13/1717:01
LABORATORY CONTROL SAMPLE: 1928156
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result % Rec Limits Qualifiers
Cadmium
ug/L
500 556
111 85-115
Chromium
ug/L
500 554
111 85-115
Copper
ug/L
500 573
115 85-115
Nickel
ug/L
500 547
109 85-115
Zinc
ug/L
500 558
112 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928157 1928158
MS MSD
92329043019
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Conc. Cone. Result
Result % Rec % Rec
Limits
RPD Qua[
Cadmium ug/L
ND
500 500 537
540 107 108
70430
1
Chromium ug/L
ND
500 500 521
538 104 108
70-130
3
Copper ug/L
ND
500 500 546
559 109 112
70-130
2
Nickel ug/L
ND
500 500 518
528 104 106
70-130
2
Zinc ug/L
ND
500 500 528
539 105 108
70-130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928159
MS
92328962003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1928160
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
561
559
112
112
70-130
0
Chromium
ug/L
0.013
500
500
552
544
108
106
70-130
2
mg/L
Copper
ug/L
0.011
500
500
593
589
116
116
70-130
1
mg/L
Nickel
ug/L
0.012
500
500
548
544
107
106
70-130
1
mg/L
Zinc
ug/L
0.085
500
500
634
621
110
107
70-130
2
mg/L
Results presented on this page are in
the units indicated by the
"Units" column except where an alternate
unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13

IneAnaly�ical®
www.pacalabs.com
s
QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92329090
QC Batch: 347724 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92329090001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100 '
Huntersville, NC 28078
[phone]
METHOD BLANK: 1929058
Matrix:
Water
Associated Lab Samples: 92329090001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5
02/10/17 14:18
LABORATORY CONTROL SAMPLE: 1929059
Spike
LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
240
96 90-110
SAMPLE DUPLICATE: 1929060
92328982003
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
14.5
13.8
5
SAMPLE DUPLICATE: 1929061
92329112001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

6 �
aceAnal(tical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92329090
QC Batch: 347491 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92329090001
METHOD BLANK: 1927949 Matrix: Water
Associated Lab Samples: 92329090001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifierc
BOD, 5 day mg/L ND 2.0 02/13/17 23:40
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1927950
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result %Rec
Limits Qualifiers
BOD, 5 day
mg/L
198 170 86
84.6-115.4
SAMPLE DUPLICATE: 1927951
92329036001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

IOeAnalytica!®
wwpacetabs.cortt
3
QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92329090
QC Batch: 347683 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92329090001
METHOD BLANK: 1928918 Matrix: Water
Associated Lab Samples: 92329090001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/t: ND 25.0 02/09/17 22:59
4
E
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1928919
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
750
754
101
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928920
1928921
MS
MSD
92329195001
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec % Rec Limits RPD Qual
Chemical Oxygen Demand
mg/L 2110
750
750
2600
2600
66 66 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928922 1928923
MS MSD
92329088001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 38.0 750 750 798 795 101 101 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

aceAnalytical
www.pacetabscom
QUALIFIERS
Project: Bakers Stormwater
Pace Project No.: 92329090
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - AdjuMod Method Detection Limit.
PQL - Practical Quantitation Limit
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAMIX cal
www.pacete6tccom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Bakers Stormwater
Pace Project No.: 92329090
g
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92329090001
BSW02
92329090001
BSW02
EPA 200.7
347561 EPA 200.7 347718
92329090001
BSW02
SM 2540D
341/24
92329090001
BSW02
SM 5210B
347491 SM 5210B 347499
92329090001
BSW02
SM 5GGOD
34/683
Date: 02/15/2017 07:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 13

aceAn,7Yica/6
uucumenr ivame.
:ondition UponRecei
Document No.:
F-CAR-CS-033-Rev.01
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood
uocument Revised: Sept. 21, 2016
Page 1 of 2
Issuing Authority:
Pace Quality Office
Huntersville R Raleigh[! MechanksvilleQ
MEMO Project
Client Name: WO# ° v'/ �j.�`�' -�{� .
� 1 1 1-
Courier: FIFed Ex UPS ❑USPS 20lent
commercial ❑Pace ❑Other: 11 111 11 11 1 111
,_.,/ 92329090
Custody Seal Present? QYes l�o Seals intact? ❑Yes
Date/initials Person Examining Contents:.
Packing Material: ❑Bubble Wrap r�Rfubble Bags ❑None -❑Other:
Thermometer- ,,--,�i
. RGun i0: et �NOe 05amples on lce, coolingprocess has begun
0 )-- Type of ice: �6tue
Correction Factor: Cooler Tamp Corrected (°C)i _LA Biological Tissue Frozen? [ Yes ! No nN/A
Tamp should be above
�,f.�r,e,e�• !fig to VC
USDA !Regulated Soil( G� 6/A, water sample)
oDid samples orl 'hate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
yes
including Hawaii and Puerto Rica)? Oyes Elko
Chain o#Custod Present?
es
ONO
QNJA
1.
Samples Arrived within Hold Time?
/A
2.
Short Hold Time Ma sis (<72 hr. ?
/A
3.
Rush Turn Around Time Requested?
4U.
A
4.
Sufficient Volume?'
A
S.
:orrect Containers Used?
A
6.-Pac�ontainers
Used?
.
;ample Labels Match CoC?
teadspace In VOA vials (>5.6mm?
'rlp Blank Present?
r Ip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample '
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Qfe� ONO ONIA-1 7.
OYes, ONO /A S. Note if sediment is visible in
CRY/es ON. ON/A 9.
Oyes ONO
12.
Date/Time,
Field Data Required? []Yes ❑No
Date:
ote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certificatler,.Offlce (i.e.
ut of hold, incorrect preservative, out of temp, incorrect cont Rlers)
Page 11 of 13

Document Name:
Document Revised: Sept, 21, 2016
Sample Condition Upon ReceiptiSCURi
Page 2 of 2
Document No..,
Issuing Authority:
aceAna1Xica><
I -'
F-CAR-CS-033-Rev.01
Pace Quality Office
" (necK marK Lop nail oT pox it pti and/or aecniorination Froject fif
� ® '
90
is verified and within the acceptance range for
PM: MWB Due Date: 02/17/17
preservation samples.
"Bottom half of box is to list number of bottles i �.� �
CLIENT; 92-R1 ivac NC
z
z
z
z
a
a
v
z
z
z
a
dot
.2
N
Z
°
N
C
D
Z
.a
°�
N
N
v
,- I
z
Z
Z
N
2
1 2
aa+
2
m
N
a2i
S
M
z
\
Z 'Q�. z O
a
n
a
m
O
M
u
x
m
a
n
V
O
4
Z
O
a
�i `
Lt
sa
i+
u
u_
x
IW
Z
L
'0°
u
ro
:c
c
a
V
x
a5
1
2
y
E
X
2
1
y j c z
i 2 a !3
to
to
U
v{
tl
f
G
[
L
tGN�1
4
e�
Qyy
p
E
aN-t
E
to
{A
u
rti
E
t7
E
N
E
111
E
N
v
rl
a
si
E
N
a
ry
E
N
m
LS
'
�'
'3 E £ L
�' v v �q N A C N
E
Z
N
u
u
x
M
J�
H
M
Q
M
x
O1
r
Ot
41
a At x != H eq .9 3
iT Q
;;
O
a
M
a
N
a
ri
a
M
a
M
a
M
a
M
a
Ve
ai
t7
rl
!9
r9
t7
c9
l7
t9
t9
t7
Ur ttf N M
O �. a a a 2
_
m
m
m
ea
tom
go3
.¢
a
a
> > h �
1
N
I
i
\N\\�
I
z
N
---
\N\\
N
\\N
N
N
\�\N
N,'\
N
NN\
S
\NN\
N
NN\
N
\
\�
N
\\\\d
N
\\\J
I
8
N
N
\\\d
I
I
-\\d
'Td
9
N
N\N\
N
\�\\�
\\J
10
N
N\NN
N
\N\
I
li
\NN--
12
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Page 12 of 13

0
z
0
0
z
s
in
X
0
z
z z >
z M
M
Xt
> 0
r Z
V
M In C
M
M
0
V
M-
:j,j Tempin'C
9
Received on
CD Ice (Y�
CD
Custody
r
rn
0
Sealed Cooler
0
(YIN)
z
0
4
0
z
c:.
CD
rA
Samples Intact
(Y/N)
ITEM#
V)
rn M
C:
O
M
02
T
MATRIX CODE tsEs va.,jd miss to Ian)
SAMPLE TYPE (G=GRAB C=COMP)
............ .... ... ...
1> 4 n
m
0
0
m r-
M
m
SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
f—L
HNO,
HCl
NaOH
Na2S20z
Test
M
r
0
2
C z
0 T
--4 0
C
9 (D
M
0
z
CL
>
X M
0 z
0 0
z
Residual Chlorine (YIN)
M
;U
ft
0 0
(D Y)
x z
M
:0 Zi
Z
P
z
0
M
;0
3 of 13

Aflvae ® Bakers Plant
St® water Monifor ing-Reiport Fonn
Sample Date: Sample Time: ep?
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Parameter
BOO
COD
TSS
Cadmium
Chromium, total recoverable
Copper, total recoverable
Nickel, total recoverable
ME
Benchmark Values (mg/1)
30
120
100
0.001
1
0.007
0.26
0.067
6-9 td units)
St® Date: QL: St® Duration: S..2d- fts.) lynches of Rainfall: C9 . 6 0
Duration of time preceding rain event exceeding 0.111: S66 fts.)
Estimated Flow Calculation:
Q = CIA
WOW) = Q(Pervious Area) + Q(finpervious Area)
Q(tot., cfs) = (A x inches rain/1 2 inches/ft. x 7.8 acres x.85) +.9 x inches raWl 2inches/ft. x 7.8 x .15)
Q(Total, cfs) = 0.2210 x 0. (00 (Inches of fain) + 0.0878 x (Inches of rain)
= - 19 - /9-f cfs
� =14 R,
N
IN
(std units)

6 „
aceAnalj4kal
..r
**w.pacelabs.=n
r
1
February 15, 2017
Mr. Joe Hinkle
Allvac
RE: Project: Bakers Stormwater
Pace Project No.: 92329091
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

Pace Analytical Services, LLC
aceAnalj6cal o 9800 Kincey Ave. Suite100
Huntersvilie, NC 28078078
www.pacelabs.com
[phone]
l
CERTIFICATIONS
Project: Bakers Stormwater
Pace Project No.: 92329091
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
1=lorida/Nf=LAll Certification #: E81648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification M 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification M 460221
North Carolina Wastewater Certification M 40
South Carolina Certification #: 99030001
Virginia/VEIAP Certification #: 460222
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

Pace Analytical Services, LLC
'
acenlytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wmpacalabs.com
I
[phone]
SAMPLE ANALYTE COUNT
Project: Bakers Stormwater
Pace Project No.: 92329091
Analysts
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92329091001 BSW03
SM 2540D
ALC
1 PASI-A
92329091002 BSW03
SM 5210B
WH1
1 PASI-A
92329091003 BSW03
SM 5220D
MDW
1 PASI-A
92329091004 BSW03
EPA200.7
SER
5 PASI-A
I zIA;IQ t1l ]&] iy A z: Iil71l ti7..�'l_\ c I\71'�
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 16

aceAnalj cal
t www.pacelabs.com
1
ANALYTICAL RESULTS
Project: Bakers Stormwater
Pace Project No.: 92329091
® r
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab lD: 92329091001 Collected: 02/08/17 02:38 Received: 02/08/17 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 17.2 mg/t 2.5 1 02/10/17 14:37
Date: 02/15/2017 07:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 16

aceAnalytical
MW..pacelabs.com
ANALYTICAL RESULTS
Project: Bakers Stormwater
Pace Project No.: 92329091
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab ID: 92329091002 Collected: 02/08/17 02:40 Received: 02/08/17 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day 4.7 mg/L 2.0 1 02/09/17 03:25 02/13/17 23:40
Date: 02/15/2017 07:45 PM
REPORT" OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

ceAnaljltical
www.pacelabacom
3'
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92329091
Sample: SSW03 Lab ID: 92329091003 Collected: 02/08/17 02:41 Received: 02/08/17 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
5220D COD
Chemical Oxygen Demand
Date: 02/15/2017 07:45 PM
Analytical Method: SM 5220D
36.0 mg/L 25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,
without the written consent of Pace Analytical Services, LLC.
02/09/17 22:59
Page 6 of 16

aceftlj&al
www.pacelabs.com
I_\► Is1�►'��ra_1
Project: Bakers Stormwater
Pace Project No.: 92329091
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03
Lab ID: 92329091004
Collected: 02/08/17 02:43
Received: 02/08/17 11:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
02/09/17 12:01
Collected Date
02/08/17
1
02/09/17 12:01
Collected Time
02:55
1
02/09/17 12:01
Hold pl 1
1.3 51d. Units
0.10
1
02/09/ 11 12:0 I
1 ield temperature
14.1 deg C
0.50
1
02/09/17 12:01
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND ug/L
1.0
1
02/09/17 21:00 02/13/17 18:28
7440-43-9
Chromium
18.6 ug/L
5.0
1
02/09/17 21:00 02/13/17 18:28
7440-47-3
Copper
76.7 ug/L
5.0
1
02/09/17 21:00 02/13/17 18:28
7440-50-8
Nickel
ND ug/L
5.0
1
02/09/17 21:00 02/13/17 18:28
7440-02-0
Zinc
66.4 ug/L
10.0
1
02/09/17 21:00 02/13/17 18:28
7440-66-6
Date: 02/15/2017 07:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

aCeAnalj6cal OD
www.parelabs.com
Project: Bakers Stormwater
Pace Project No.: 92329091
QC Batch: 347561 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92329091004
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1928155
Matrix:
Water
Associated Lab Samples: 92329091004
Blank
Reporting
Parameter
Units
Result
t imit
Analyzed
Qualifiers
Cadmium
ug/L
ND
1.0
02/13/1111:01
Chromium
ug/L
ND
5.0
02/13/1717:01
Copper
ug/L
ND
5.0
02/13/1717:01
Nickel
ug/L
ND
5.0
02/13/1717:01
Zinc
ug/L
ND
10.0
02/13/1717:01
LABORATORY CONTROL SAMPLE:
1928156
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
556
111
85-115
Chromium
ug/L
500
554
111
85-115
Copper
ug/L
500
573
115
85-115
Nickel
ug/L
500
547
109
85-115
Zinc
ug/L
500
558
112
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1928157
1928158
MS
MSD
92329043019
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
537
540
107
108
70-130
1
Chromium
ug/L
ND
500
500
521
538
104
108
70-130
3
Copper
ug/L
ND
500
500
546
559
'109
'112
70-130
2
Nickel
ug/L
ND
500
500
518
528
104
106
70-130
2
Zinc
ug/L
NO
500
500
528
539
105
108
70-130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928159
MS
92328962003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1928160
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
561
559
112
112
70-130
0
Chromium
ug/L
0.013
500
500
552
544
108
106
70-130
2
mg/L
Copper
ug/L
0.011
500
500
593
589
116
116
70-130
1
mg/L
Nickel
ug/L
0.012
500
500
548
544
107
106
70-130
1
mg/L
Zinc
ug/L
0.085
500
500
634
621
110
107
70-130
2
mg/L
Results presented on this page are in
the units indicated by the "Units" column except where an alternate
unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

ace naljftal
www.pacelabs.com
Project: Bakers Stormwater
Pace Project No.: 92329091
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
QC Batch: 347724
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92329091001
METHOD BLANK: 1929058
Matrix: Water
Associated Lab Samples: 92329091001
Blank Reporting
Paramotor
Units
Result t imit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 02/10/17 14:18
LABORATORY CONTROL SAMPLE: 1929059
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 240
96 90-110
SAMPLE DUPLICATE: 1929060
92328982003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
14.5
13.8 5
SAMPLE DUPLICATE: 1929061
92329112001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Ftesuits presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

aceAnalyiical
www.pacelabs.cam
r
Project: Bakers Stormwater
Pace Project No.: 92329091
QC Batch: 347491 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92329091002
METHOD BLANK: 1927949
Associated Lab Samples: 92329091002
Parameter units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result t imit Analyied QualifiOlt;
ND 2.0 02/13/17 23:40
LABORATORY CONTROL SAMPLE:
1927950
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
BOD, 5 day
mg/L
198 '170 86
84.6-115.4
SAMPLE DUPLICATE: 1927951
92329036001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
ND ND
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16

afilm
An liltical
www.paWabs.com
1
Project: Bakers Stormwater
Pace Project No.: 92329091
QC Batch: 347683
QC Batch Method: SM 5220D
Associated Lab Samples: 92329091003
METHOD BLANK: 1928918
Associated Lab Samples: 92329091003
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 1928919
Parameter Units
Cheirflwl Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyeed Qualifiers
ND 25.0 02/09/17 22:59
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 754 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928920 1928921
MS MSD
92329195001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 2110 750 750 2600 2600 66 66 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928922 1928923
MS MSD
92329088001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 38.0 750 750 798 795 101 101 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Pace Analytical Services, LLC
aCftla ytical ® 9800 KinceyAve. Suite 100
Huntersville, NC 28078
wmpacelabs.com
[phone]
i
QUALIFIERS
Project: Bakers Stormwater
Pace Project No.: 92329091
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitatiun Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
W-TETOTITTOOTITM
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
I_10I_\5i1140 p\111WI:
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
This report shall not be reproduced, except in full,
Date: 02/15/2017 07:45 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

0
ace nalj4ical
_.r
/ w pacWabs.com
1
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Bakers Stormwater
Pace Project No.: 92329091
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92329091004
BSW03
92329091004
BSW03
EPA 200.7
347561 EPA 200.7
92329091001
BSW03
SM 2540D
347724
9232909,1002
BSW03
SM 52,10B
347491 SM 52,10B
92329091003
BSW03
SM 5220D
347683
9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
347718
347499
Date: 02/15/2017 07:45 PM
Page 13 of 16

uucument ivame: Document Revised: Sept. 21, 2016
aceARa/ytica/® Sample Condition Upon Recelpt(SCUR) Page 1 of 2
—LL
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden(Q Greenwood ❑ Huntersville Raleigh(Q Mechanicsvillen
som
Client Name:
Project g WO#°
92329091
'Courier: QFed Ex ❑UPS ❑USPS
❑ C'ommercial ❑Pace nOther: 11 1111
92329091
Custody Seal Present? FlYes Leo Seals intact? ❑Yes 2/No
Date/initials Person ExaminingContents"]�-
Packing Material: (_]Bubble Wrap bble Sags None ❑Other:
ThennomeLer•
IR Gun ID: TWO 9 Type of ices et ❑Blue ❑ Non e amples on ice, cooling process has begun
Correction Factor: Cooler Temp Corrattad (°C); blolugital. llssue Frozen? (Dyes ZN' o (JN/A
Temp should be above frej6ig to 6®C T—
USDA Regulated Soil ( UNIA, water sample)
Did samples 9 ginate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter i
E]Yes jV[� o including Hawaii and Puerto Rico)? DYes PlNo onaily,
Chain of Custody Present?
es
ON.
QN/A
1.
Sam las Arrived within Hold Tirne?
❑No
❑N/A
2.
Short Hold Time Anai sis {<72 hr.)?
es
❑No
ONIA
3.
Rush Turn Around Time Requested?
QYes
o
❑N/A
4.
Sufficient Volume?'
04's
ON.
❑N/A
S.
=orrect Containers Used?
s
[]No
❑N/A
6.
-Pat ontainers Used?
Ls�res
No
[]N/A
:Ontainers Intact?
es
[:]No
❑N/A
7.
Pam les Field Filtered?
By
(]No
/A
S.
Note if sediment is visible in the dissolved container.: .
ample Labels Match COC?
/ es
[]No
EIN/A
9.
-includes Date/Time/ID/Analysis Matrix: W
leads ace in VOA Vials (>S-6mm)?
DYes
❑No
/A
10.
'rip Blank Present?
Oyes
[]No
rip Blank Custody Seals Present?
]]Yes
❑No
/A
CLIENT NOTIFICATION/RESOLUTION
Held Data Required? QYes []No
Person Contacted:
Date/Time:
Comments/Sample
Discrepancy:
. . ...
Project Manager SCURF Review:
Date: ,� i�,1►'1
Protect Manager SRF Review: 1—K-)Date:
ote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
ut of hulC; icorrect preservative, out of temp, incorrect containers)
Page 14 of 16

Document Name:
Document Revised: Sept. 21, 2016
r
r aceAIIalXical
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
Project #
°
92`32909
is verified and within the acceptance range for
--
preservation samples.
PH:
M6dB
Due Date:
021
i7/ i7
**Bottom half of box is to list number of bottles
CLIENT:
92®A1 Ivac NC
v
u
O
Z
m
¢
Z
(0
S
N
onS
4
2 Z N i
Y
Oif
A
.Q
N
W
v
Y
Y
IT
_
\
\
Z
Q
d
a
EVE. $ CL
pQ
U
0.
O
�.
A
Z
V
x
O
._¢.
O
'
u
w
Lq
�o
L C ¢ oZ
?
x
�
V
W
C
"
Jam•
OL
.M U
�
a a
�'
yr
a
u
r
Fti
a
.CC
m
E
a
E
a
a
¢
J
vv
Q
EfA
`r
O
O
M
O
d
9r
S!
J J J d J
J
J
J
C
Q
Q
J
Q
J
>
!
'/
N
N
J
-J
J
E E E iv E
in o o _= o
�Ln
N-1 N Ln e.f N
E
tf0�
N
E
0
N
E
0
v
3
iu
=
e-1
w
�-/
E
o
N
°`i
_
�y
E
o
N
m
(�
G
E
E
�'
y
""
'°
>
.M..
E
vi
M
E
10�
N
E
o
N
w
L
E
N
# > > > = a
E Q M fV r# M
a a a M a a
Z
to
M
N
M
a
U
M
a
u.
O
�
N
t7
S
l9
7
M
t9
of
N
l7
N
M
L7
Q
M
l7
S
O1
r
Qt
t7
�
Qf
O
O.
M
'�
Q
O
Y
(�J
�.
fL
M
a
FL
N
a
M
n
a
3
�
m CO m m CO
m
m
m
.S
eC
st
s(
4
4
>
>
>
>
vt
in
m
U
t7
1
\
i
3
t r/
t
4
{
5
6
7
8
9
10
11
12
N\N
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot ##
Page 15 of 16

w
4
L7
Z
`z
�
Z
W
O
O
ul
W
F-
3
}"
Z
z
Z�
jr
W
(7
2
}
a,
a�
Q
03
w
Q tL
a_
w
W
�-
X
om
V
1
T
a
€ C
0
ma �� 0`
c
c r c
U C' a a
u� a ti a'
,m
o
U
c
E
(A ( U Q
w
G
_ a
J
O
zm
A
(NIA) euuo140 lenplseN
sz
F
O
O
U
J
2
N
w
g
w
0
LL
Q
m
do
I
;se.L slsA)euV
'm
Ja410
O
}
JOue4laW
w
a
`OZS�eN
HOeN
IOH
h
4
'ONH
"OSZH
w
r
peAjasaidun
MONIV1N00 d0 #
-
NO110311001V dVJ313ldWVSui
a
l
1
(gam
w
N
n
n
n
p
°9
2 i
V W
U
z
W
O
C
0
W
C
V
u
r
LL
i
Sa
o�LU
�
O
V
Q
p
W
w
v1
J
w
(dW00=0 9V)JJ=J) 3dA131dNVS
(Ual O)SaPOOP:IeA.Oa4) 3000XINIVW
o aE003«o
N O
8
_
U °
x
I
ga g' dam° v
Hs
O'S'>'ain0sai=O
F
a
LU
® z
O
€ tag m
Z
O
t
��
2-1
C] 9 CO n
M
c
° E
c N
V
9
# W3il
(NIA)
Ioelul saldweS
10
0
- (NIA)
181000 paleas
Apopn0 r
0
(NIA) aoi o
uo paAlaoaa o
d
J
—1
o. uI dwal C
LL
a
c�72
a
C
i s
J J E
IL a
(n U)
i
z E
A
z C
r a
z 2
a to o
16 of 16

r
M
N
N
H
a
-�+
A
r
ert
0
O
m
(
n
A
r+
0
�
N
a•
3
�
�
O
CL
�
g
D
A
Z
O
i
0
3
W
X
0
a)
A
N
O
M
G
0
O
I
h
•
Oq
IN
f"1
r+
TI
O
W
a)
-1
e
m
f+
m
4
�D

o
`° rA a
c
p
a
M
fb
e� Fr1* a
o aro a
m
x ^*
d b
a wa
.m a
a°a a m d
� W
ob
g o`v
-R
th If
y
a a m a
"� p 2
a
all.
M �Og tltl® � a
R FA b
o mm�
F i .r
� ffi tD
tD �m
IL
d
gL
G Qe
M A
ea>� V
a
oz��pg.Oy��.•
ME
CD
10
° .04
b O
mb.
� O

aceAnalXical
www.pscelabacom
i
February 21, 2017
Mr. Joe Hinkle
Allvac
1
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 14, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aceAnalwical
t www.paoelabs.com
t
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NFL AP Certification # F87648
Massachusetts Certification #: M NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
Smith Carolina Cortifcation #: 00030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100 t
Huntersville, NC 28078
[phone]
Page 2 of 19

1�;axAnalj&cal
www.pamlabacom
SAMPLE ANALYTE COUNT
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92329851001
BAKERS NON CONTACT #1
EPA 1664B
JMS
1
PAST-C
SM 4500-CI G
MDW
1
PASI-A
92329851002
BAKERS NON CONTACT #2
EPA 1664B
JMS
.1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92329851003
BAKERS NON CONTACT #3
EPA 1664B
JMS
I
17ASI C
SM 4500-CI G
MDW
1
PASI-A
92329851004
BAKERS NON CONTACT #4
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92329851005
BAKERS NON CONTACT #5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92329851006
BAKERS NON CONTACT #6
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92329851007
BAKERS NON CONTACT #7
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92329851008
BAKERS NON CONTACT #8
EPA 1664B
JMS
1
PASI-C
SM 4500-Cl G
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 19

Pace Analytical Services, LLC
acemalyfieal� 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pawabscom
[phone]
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT Lab ID: 92329851001 Collected: 02/13/17 09:20 Received: 02/14/17 10:36 Matrix: Water
#1
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 02/21/17 08:01
4500CL G Chlorine, Residual Analytical Method- SM 4500-0I G
Chlorine., Total Residual 0.22 mg/L 0.024 1 02/15/17 00-36 7782-50-5 1)6,H3
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 19

ac6Ana1j ca!
www.abs.rwm
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT Lab ID: 92329851002 Collected: 02/13/17 09:41 Received: 02/14/17 10:36 Matrix: Water
#2
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 02/21/17 08:02
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Cldorino, Total Residual ND rng/L 0.024 I 02/15/I 100.3(i 1182-5O-5 113
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab ID: 92329851003 Collected: 02/13/17 09:55 Received: 02/14/17 10:36 Matrix: Water
#3
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16646
Oil and Grease ND mg/L 5.0 1 02/21/17 08:02
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, fetal Residual 1.3 mg/L 0.24 10 02/,15P1/ 00:36 /182-50-5 H3
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aVuAnaljftal
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab ID: 92329851004 Collected: 02/13/17 10:12 Received: 02/14/17 10:36 Matrix: Water
#4
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND ing/L 5.0 1 02/21/17 08:02
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, fetal Residual 0.83 mg/L 0,096 4 02/15/17 00:36 7782-50-5 H3
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

ae6Analytical
www.pacelabs.co»
ANALYTICAL RESULTS
4
4
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT Lab ID: 92329851005 Collected: 02/13/17 10:27 Received: 02/14/17 10:36 Matrix: Water
#5
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 02/21/17 08:04
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 4.0 mg/L 0.48 20 02/15/17 00:36 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21/2017 06:19 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

Ar
aeMnalj&al
( www.paWebs.com
I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT Lab ID: 92329851006 Collected: 02/13/17 10:45 Received: 02/14/17 10:36 Matrix: Water
#6
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease Analytical Method: EPA 16646
Oil and Grease ND mg/L 5.0 1 02/21/17 08:04
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Tatal Residual 2.3 rrig/L 0.24 10 02/15/11 00.36 1182-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21/2017 06:19 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19

aceAnaljitical
www.pacalebs=rn
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT
#7
Parameters
HEM, Oil and Grease
Oil and Grease
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 02/21/2017 06:19 PM
Pace Analytical Services, LLC a
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92329851007 Collected: 02/13/17 10:57 Received: 02/14/17 10:36 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 1664E
ND mg/L 5.0 1 02/21/17 08:04
Analytical Method: SM 4500-Cl G
2.4 mg/L 0.48 20 02/15/1 / 00:36 / /82-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAna1j&al
www.pacalsbacom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Sample: BAKERS NON CONTACT Lab ID: 92329851008 Collected: 02/13/17 11:15 Received: 02/14/17 10:36 Matrix: Water
#8
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 02/21/17 08:05
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Ibtal Residual 0.31 mg/L 0.024 1 02/15/17 00:36 7782-50-5 1-11
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

aceAnalyteel
www.pacelab8.corn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
QC Batch: 349110 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92329851001, 92329851002, 92329851003, 92329851004, 9232985100,5, 92329851006, 92329851007,
92329851008
METHOD BLANK: 1936691 Matrix: Water
Associated Lab Samples: 92329851001, 92329851002, 92329851003, 92329851004, 92329851005, 92329851006, 92329851007,
92329851008
Blink Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 02/21/17 07:51
LABORATORY CONTROL SAMPLE: 1936692
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 37.4 94 78-114
MATRIX SPIKE SAMPLE: 1936693
92330121001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L ND 40 35.7 89 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21/2017 06:19 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 19

m Y
ace Analytical
( www.PaMlabs.com
f
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
QC Batch: 348230 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92329851001, 92329851002, 92329851003, 92329851004, 92329851005, 92329851006, 92329851007,
92329851008
METHOD BLANK: 1932083 Matrix: Water
Associated Lab Samples: 92329851001, 92329851002, 92329851003, 92329851004, 92329851005, 92329851006, 92329851007,
92329851008
Blank Reporting
Parameter Units Result t imit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 02/15/17 00:36
SAMPLE DUPLICATE: 1932084
92329851001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0.22 0.30 29 D6,H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21/2017 06:19 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 19

aceAnalytkal
www.pecelebssom
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
c
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Metl led Detection Limit.
POL - Practical Quantitation Limit.
RI - Reporting t imit
S Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration_
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
III Analysis conducted outside the EPArnethod Bolding tlrrie.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21/2017 06:19 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

aceAnalytical
J www.pacelabs.com
1
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NONCONTACT COOLING WATER
Pace Project No.: 92329851
Lab ID
92329851001
92329851002
92329851003
92329851004
92329851005
92329851006
923298511001
92329851008
92329851001
92329851002
92329851003
92329851004
92329851005
92329851006
92329851007
92329851008
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample ID QC Batch Method QC Batch Analytical Method
BAKERS NON CONTACT #1
EPA 1664B
349110
BAKERS NON CONTACT #2
EPA 1664B
349110
BAKERS NON CONTACT#3
EPA 1664E
349110
BAKERS NON CONTACT #4
EPA 1664E
349110
BAKERS NON CONTACT #5
EPA1664B
349110
BAKERS NON CONTACT #6
EPA 1664E
340110
BAKERS NUN CON (AC 1 #1
LPA I664B
349110
BAKERS NON CONTACT #8
EPA 1664B
349110
BAKERS NON CONTACT #1
SM 4500-CI G
348230
BAKERS NON CONTACT'#2
SM 4500-CI G
348230
BAKERS NON CONTACT #3
SM 4500-Cl G
348230
BAKERS NON CONTACT #4
SM 4500-0 G
348230
BAKERS NON CONTACT #5
SM 4500-CI G
348230
BAKERS NON CONTACT#6
SM 4500-Cl G
348230
BAKERS NON CONTACT #7
SM 4500-CI G
348230
BAKERS NON CONTACT #8
SM 4500-CI G
348230
Date: 02/21/2017 06:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 15 of 19

IaceAnalytical
Laboratory receiving samples:
Asheville ❑ Eden[J
uocument Name:
Sample Condition Upon Receipt(SCUR)
Document No.:
F-CAR-CS-033-Rev.01
Greenwood ❑ Huntersvilie
Document Revised: Sept. 21, 2016 F
Page 1 of 2
Issuing Authority:
Pace Quality Office
Raleigh[] Mechanicsville[_)
If • MU • • • • Client N me: W4 1
Project
Courier: ElFed Ex UPS USPS []Client III III I IN 1111111111111
❑ Commercial tpPace []Other: 92329851_
Custody Seal Present? Elyes qNo Seals intact? ElYes jNo ( E ( `)
Date/tn)tialsPersan Examining Contents- j� i�i {
Packing Material: []Bubble Wrap \[jiubble Bags ❑None [Other:
Thermometer:
h Gun ID: Type of Ice' t ❑Blue ❑None �Sarmpies on ice, cooling process has begun
Correction Factor, Cooler Tern Corrected °C : , a Biological Tissue Frozen? nYes
p ( } � _`1 '&o ...INfA
Iernp should be above freezing to 6°C
USDA Regulated Soil � fth/A, water sample)
Did samples prriginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Int m tionally,
❑Yes including Hawaii and Puerto Rico)? []Yes EL46
Comments/Discrepancy.-
--Chain of Custody Present? ldies i]No ©NIA 1.
i Rush Turn Around Time Requested? QYes 4JN0 NIA 4:
Sufficient Volume? es ONO ON/A 5,
Correct Containers Used? (.O!s ❑No [jN/A 6.
Sample Labels Match COC?
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample
Discrepancy:
Lames ONo ❑N/A 19,
UYes LINO W! /A 10.
Oyes bt o` ❑N/A 11.
Note if
Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: F'
Date: Lr ! t
Project Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 16 of 19

Document Name: Document Revised: Sept. 21, 2016
Sampie Condition Upon Receipt(SCUR) Page 2 of 2
E aceAnalytica/� Document No.: IssuinLrr Ai&hnr1t,,
*Check mark top half of box if pH and/or dechlorination
Is verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Pi
PM: MWB Due Date: 02/23/17
CLIENT: 92-Allvae NC
2
GL
M
u
a.
J
to
e�•t
en
m
Z
i f:t 41 Vti U
D Z C N z
U D U
J J a J J
n. 4EEE�EEFE
O O & O O
N h tt N N
D z
a a a a a
m m m m m
z
Q
Z
J
O
N
N
a
m
N Q. z
M C? � ^'
x a
QT '�' t in
i° C Cl O S
d 7 x r.
,� `m d s Q
J -
O M � O r
N .�i H N ,.{ N
U D '
{� ••� •+ m .�• m
a t� C7 tR C7 U'
m S� Q d R C d
Z
Z
a
Q `�.
-+ V
E x
rn
qQ
d 2
m m
t? U'
d O
(�L±1
CJ
N
z
E
O
h
m
t7
>
4
?
c
O
m
L>
>
s�
O
m
x
E
v
'd
rn
L7
._.
.Y
of
�
:x
}
Y
d
O
z
ML
"�,,
}
M�
O
rc
'y�r
m
a
v
E
N
ut
a
f0
r
z
a4,
O
1r1
iN-�•
ev
a
f+'t
m
O
z
u
O
a
W
C
a
D
E
N
1
N
�5
\N\N
\i
I
I
\N
z
/
.\N
3
N�
N
I
k\
\N\�
N
I
I
NN
I
I
I
-\N
\N
s
/
I
I
�\
NNN
I
6
\t�
N\N
NN
7
\
11
1
NNNN
N
NNN
II-
NN
8
\'I
I
N
NN
N
I
N\�
N
I
I
NNNN
N
NNN
I
10
I
NNNN
N
NNN
I
11
12
\N
pH Adjustment
Log for Preserved Samples
Sample ID Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Page 17 of 19

(NON CONTACT)
Baker north
Chain of Custody Record
Speclaity Materials
oaae #2
Project Number/Name: NonContact Cooling Water
Project Location: Ailvac Raker
Sampler's Signature:
;.y, f Ss�
ttc,.,.,...
Date: :� - �-
M
a
Q.
GJ
0
C
O
CL
>
tdCIO
v
O
tJ
0
i
a
C
Requested Test
Parameters
Z1
K3 JvnLin�r��-13-
7
%o�c.
G
G
HCL
Y
Oil &Grease
G
G
HCL
Y
j' . °`
Oil & Grease
.':Fyn,
G
G
HCL
Y
3a
Oil & Grease
G
G
HCL
Y
Oil & Grease
G
G
HCL
Y
Oil & Grease U
G
G
HCL
Y
3``
Oil & Grease
,:5"7,
G
G
HCL
Y
j`4
Oil & Grease y
Kj(e,jfvtaiIm 4#Zk'
G
G
HCL
Y
`
Oil & Grease
Meter Calibrated: `/ N IThermorneter
Calibrated: / N
Sampling and Field analysis completed by: x , s, `
Relinquished By:
IRelinquished
By:.
1
Date ;:,? /y-
Time: -' 7' 1,>
Date:) -IT- j-7-ITime:
t)
Relinquished By:
`yam , , _ L ;
Relinquished
Date : ,,? -1
Time:
Date : "Z C
Time:
EHS Baker South SW REV # 2 5/10/2016
X.1L
7Y
3�
V
Page 18 of 19

Storm Water Monitoring
(NON CONTACT)
Baker North
Chain of Custody Record
reV ATI
Spedany Matelots
n..e #1
Project Number/Name: NonContact Cooling Water
Project Location: Allvac Baker
Sampler's Signature:
.,
%� G,sti�e�
Dater-/=
m
°•
IV
®
i=
O
a,
°
O
y
!
.*'-,
is
a
-
®
s
CL
a
d
LLCL
a
0
v
+�+
d
r
C!
C
Requested Test
Parameters
t
G
Gj$
None
Y
3s,3"`'
Residual Chlorine .
, % L,
G
GjIP
None
Y
J 9, °�=
Residual Chlorine
G
G/T
None
Y
13. J °`
Residual Chlorine
G
G/P
None
Y
36,61
Residual Chlorine 1
sik �f
G'
G
G/O
None
Y
y
> , ``
Residual Chlorin
;%rs`v,rf
g
G
G&
None
Y
*7,
,,I`�
Residual Chlorine
G
G/T
None
Y
°�
Residual Chlorine Zh
,' ;5v,,
G
G
None
Y
• C
Residual Chlorine
Meter Calibrated:
/ N
IThermometer
Calibrated
i/ N
Sampling and field analysis completed by:
Relinquished By: .a.4
Received BY:� ,,
Date: R - y -
Time:
> .`v;>�'
Date: —i
Time: t'�
Relinquished By:
Received By . . r
(t
,
Date: ]
Time: I'; f
IDate:
Time:
EHS Baker South SW REV # 2 5/10/2016
Page 19 of 19

�,*.
NCDENR
Stormwater Discharge ®utfall (SDD)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit. http://Vortal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
Permit No.: N/C/S/D/Q/O/3/,eZ/Q/ or Certificate of Coverage No.:
Facility Name: 41)52r e-,694,Kenr
County: Z47APA Phone No. 7d0' 0289
Inspector:
Date of Inspection:
Time of Inspection: 4-/94*--
Total Event Precipitation (inches): ®. L®
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
�es ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
I
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the j
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
"100 -/)

tom„
{ h
e °
1. Outfall Description:
Outfall No..5� Structure (pipe, ditch, etc.)
Receiving Stream: - P-Z rk
Describe the industrial activities that occur within the outfall drainage area:
IWR 6
V
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: cld
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): A199wel
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
® 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
® 2 3 4 5
f. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
® 2 3 4 5
i. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
18. Other Obvious Indicators of Stormwater Pollution:
List and describe &ege
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
StA7ii_249 i.acr mn.i;fim.; � n nv�n� o
Page 2 of 2

IVA
Ll
`4
RC-DENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit. http://portal.ncdenr.org/web/wq/ws/su,/npdessw#tab-4
Permit No.: IV/C/S/D/Q/o%�,�/�/ or Certificate of Coverage No.:
Facility Name: _Ali &/omc -Bo-kgrr
County: on Phone No. ?®-Y aB9-Y.//
Inspector: 21&W, Ado*
Date of Inspection:
Time of Inspection:
Total Event Event Precipitation (inches): 0. (vD
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
�es ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitothig to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
A 1 /I .

1: Outfall Description:
Outfall No. SWda Structure (pipe, ditch, etc.) ire
Receiving Stream: k/ Fri' Cree,+e
Describe the industrial activities that occur within the outfall drainage area:
Gf
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Zi 4y` Az;I��g/ _Awl-A-
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy.
1 2 b 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 (2) 3 4 5
f. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
® 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes (n
R. Is there an oil sheen in the stormwater discharge? Yes 49
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 1612 2
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWI]-242. Last mndifinri I n /9S /7m

A 7--A
ifC&DEEWR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Deport
Forguidance on filling out this form, please visit: http://12ortal.ncdenr.org/web/wg/wslsu/npdessw#tab-4
Permit No.: N/C/S/ o/o/O/,�/�/_f/ or Certificate of Coverage No.: IV/C/G/_/ /_/_/_/_/
Facility Name: _ _ /�T.� //ibe - XVX&-r
County:
Phone No. __X-Y-v189Ty5'1/
Inspector: _Z401W Pwe
=.TR
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): 6.6D
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Ea<yes ® No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable stone event" (requirements vary, depending on the permit).
..........
QuAltative moijituring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event` is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office_—_— --- _�
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
n /) /I

1. Outfall Description:
Outfall No. -5W0.3 S
Receiving Stream:
Describe the industrial activit
ditch, etc.)
is
i that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: C14
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): Alkwe
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
® 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
® 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
10.
1 ® 3
Is there any foam in the stormwater discharge?
4 5
Yes
Is there an oil sheen in the stormwater discharge? Yes
Is there evidence of erosion or deposition at the outfall?
Other Obvious Indicators of Stormwater Pollution:
List and describe lVOA e-
6
Yes V
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2