NCS000329_Monitoring Reports_20170823

August 23, 2017
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
*ATI
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: joe.hinkle(a,atimetals.com
Attached, please find stonnwate> inonitwing data foi Pennit No NCS000329. The wigiilals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitonng Period
Sample Number
I Start
End
Year 8 — Period 1
15
1 March 1, 2017
August 31, 2017
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Joe Hinkle
Environmental Manager

aLurmwacer
FM utfall #01 Co ie
—Ijisg. har e 0 1 ,
Drainage Area = 2,915,470sg. ft. = 69 acres
% Impervious = 345/o
Person Collecting Samples: -Pw.,,W Roe
Laboratory Performing Analysis:
Analytical Techniques and Methods: 40-CFR �P art 136
Results of Sample Ands
Parameter
Result I s (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
ND
0.001
Chromium, total recoverable
NP
I
Copper, total recoverable
D. o023
0.007
Nickel, total recoverable
AID
0.26
Zinc, total recoverable
Allp
0.067
Oil and Grease
20
Temp (receiving stream)
a 9, (deg C)
32
(deg C)
Total Residual Chlorine
-------------
0.017
pH
(st-d- units)
6-9 (std units)
Storm Date: -1;7 Storm Duration:-1 — Mrs.)
- /' -
Inches of Rainfall:
Duration of time preceding rain
event exceeding 0.1 11:
Estimated Flow Calculation:
Q = CIA
Q(Total) = Wervious Area) + MnPervious Area)
Q(tot., efs) = (.4 x inches rain/12 inches/ft. x 69 acres x.66) +.9 x inches
rain/12inches/ft. x 69 X'34)
Q(TotaL cfs) = 1.5180 x P (Inches of rain) + 1.7595 x (Inches of rain)
/.
q6 6.,5- — 'C -Ps

Sample Date: . 8
Allvac - Bakers Plant
Stonnwater Monit-pritg-lepo-g. Fn
Drainage Area = 212,952so. ft. = 4.9 acres
;Yo Impervious = 12%
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
01, -
30
COD
120
TSS
0
100
Cadmium
AID
0.001
Chromium, total recoverable
1
Copper, total recoverable
0.007
Nickel, total recoverable
DO
0.26
Zinc, total recoverable
0.067
pH
(std units)
. ,
6-9 (std units)
Storm Date: Storm Duration: - /. 5- (Hrs.) Inches of Rainfall: 0 - 6
Duration of time preceding rain event exceeding 0.1 ": _4u_ (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Wervious Area) + Q(finpervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x.88) +.9 x inches rain/121nches/ft. x 4.9 x.12)
Q(Total,cfS)=0.l437x_..D.60 -(Inches ofrain) + 0.0441 x &(o(D (Inches of rain)
= 0.113 cfs

Allvae - Bakers Plant
Storinwater Monitorin Re-ogy- Eia
Sample Date: ___jR-9:z7
Analytical Techniques and Methods:
Results of SanlDle Analvsis:
Sample Time: Aa? 4�%2,00,
mw­
Drainage Area = 336,580sci. ft. = 7.8- acres
% Impervious = 15%
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
7 'D
120
TSS
-$_ CIR
100
Cadmium
140
0.001
Chromium, total recoverable
I
Copper, total recoverable
0.007
Nickel, total recoverable
A92
0.26
Zinc, total recoverable
0.067
pH
(std units)
6-9 (std units)
Storm Date: Storm Duration: /. X' (Hrs.) Inches of Rainfall: 0. we
Duration of time preceding rain event exceeding 0.111: _'z9w__ "s.)
Q = CIA
WOW) = Wervious Area) + Q(Impervious Area)
Q(tot., cis) = (A x inches rain/1 2 inches/ft. x 7.8 acres x.85) +.9 x inches rain/12inches/ft. x 7.8 x. 15)
Q(Total,cf§)=0.22l0x__j!!Q.45;0 -(Inches of rain)+ 0.0878 x__,::�2. aa (Inches of rain)

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N

NCDENR
Stormwater Discharge ®utfall (SD®)
Qualitative Monitoring Report
h'orguidunce on filling out this form, please visit: htLp:/Ipol'Lai.ticderii-.orgZweb/wq/ws/su,Lnpdessw#tab-4
Permit No.: IV/C/ 3"/O/ o/Q/,�/�/�/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: Ail A114%.e, - A.xwx
County: hG+siin Phone No.
Inspector: Vo,0W &ooe Tie•
Dale of Inspection: 94 / 2
Time of Inspection: /a? : Y40,
Total Event Precipitation (inches): N- 64
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
[✓ryes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
........ .. ...._.. _ ---
By this signature, I certify that this report is accurate and complete to the best of my knowledge:

1. Outfall Description:
Outfall No. -5' ✓a! Structure (pipe, ditch, etc.) -;D,%/ 1!!/p-
Receiving Stream: r v �or,� �6'r eeeDescribe the industrial activiies that occuthin the outfall drainage area:
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /7 4OwZ
4. Clarity- Choose the number which best describes the clarity of the discharge, whet e 1 is
clear and 5 is very cloudy:
2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
10.
Q 2 3
Is there any foam in the stormwater discharge?
4 5
Yes
Is there an oil sheen in the stormwater discharge? Yes
Is there evidence of erosion or deposition at the outfall?
Other Obvious Indicators of Stormwater Pollution:
List and describe
Yes
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

ALTT`�-TAA
NCDENR
Stormwater Discharge ®utfall (SD®)
Qualitative Monitoring Report
Yorguidance on filling out this form, please visit. http,//portal,ncdenr.org/web/-wiL/ws/sufnpdessw#tab-4
Permit No.: N/C/X/D/ O/a/,j/,d/-f/ or Certificate of Coverage No.:
Facility Name: 47',Z//t,�tc
County: &0166 17 Phone No. 1Dy-oTB9-y.T//
Inspector: ujp,,,V Yde 5%t .
Date of Inspection: _8 %%
Time of Inspection: AR I:3.31
Total Event Precipitation (inches): Z94 O
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
10/ Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
......... ......_.............._... _............._. .. .._... ...--
By this signature, I certify that this report is accurate and complete to the best of my knowledge:

1. Outfall Description:
Outfall No. Al Structure
Receiving Stream: 2
Describe the industrial activities that i
2. Color: Describe the color of the
(light, medium, dark) as descriptors: _
e, ditch, etc.) A
within the outfall drainage area:
colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /119/241P
4. Clarity: Choose the number which best describes the clarity of the discharge, whet e 1 is
clear and 5 is very cloudy:
2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ® 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
0 2 3 4 5
i. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes W
9. Is there evidence of erosion or deposition at the outfall? Yes ®°
10. Other Obvious Indicators of Stormwater Pollution:
List and describe /Y®/? e-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

A`Tt"�-YAA
NCDENR
St®rrnwater Discharge ®utfall (SD®)
Qualitative Monitoring Report
Por guidance on filling out this form, please visit; b-ttp://pQrtii,ncdenr,Qrg/web wq/ws/5u/nl2dessw#tatb-A
Permit No.: N/
Facility Name:
County: GG
Inspector: s
0/0-/Q/,q/a2/-9/ or Certificate of Coverage No.:
Date of Inspection: Y-g6 /7
Time of Inspection: A? -
J
Total Event Precipitation (inches): © - % 0
Phone No. Y-1-11
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
[O/Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
r '.

1. Outfall Description:
Outfall No. Structure (pipe,
Receiving Stream: ,/2r;/Ae�-
Describe the industrial activities that occur
etc.) �'`��� �� ��►
the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G Chi'
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 1VA12e
4. Clarity: Choose the number which hest describes the clarity of the discharge, whet e 1 is
clear and 5 is very cloudy:
® 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 6) 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
® 2 3 4 5
i. Is there any foam in the stormwater discharge? Yes
B. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 44o& e.,
Mote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

'Eswol
e
aceAnaIXical
www.paceJabs.com
1
I
August 18, 2017
Mr. Joe Hinkle
Allvac
RE: Project: Bakers Stormwater
Pace Project No.: 92350554
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

1-�-;a'cie Analj6cal
www.pacelabs.com
I
Project: Bakers Stormwater
Pace Project No.: 92350554
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water C:ertiflcatlon #. 31! 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
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I
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Bakers Stormwater
92350554
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92350664001
BSW01
SM 2540D
SLB
1
PASI-A
92350564002
BSW01
SM 5210B
ECH
1
PASI-A
92350554003
BSW01
SM 5220D
NAL
1
PASI-A
92350554004
BSW01
EPA 1664E
JMS
1
PASI-C
92350554005
BSW01
EPA200.7
SER, SH1
5
PASI-A
92360564006
BSW01
SM 4500-CI G
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
Sample: BSW01
Lab ID: 92350554001 Collected: 08/07/17 00:42
Received: 08/08/17 11:12 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
08/08/17 00:40
Field pH
8 Std. Units
0.10
1
08/08/17 00:40
Field Temperature
29.9 deg C
0.50
1
08/08/17 00:40
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solldb
32.4 rng/L
10.0
1
08/ 10/ 1`I 14:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20

aceAnaIXical
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7
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
Sample: BSW01 Lab ID: 92350554002 Collected: 08/08/17 00:43 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day
BOD, 5 day
Date: 08/18/2017 06:37 PM
Analytical Method: SM 5210B
7.2 mg/L 2.0 1 08/09/17 20:45 08/14/17 15:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Bakers Stormwater
Pace Project No.: 92350554
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSWO1 Lab ID: 92350554003 Collected: 08/08/17 00:45 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 82.0 mg/L 25.0 1 08/14/17 14:05
Date: 08/18/2017 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
Sample: BSW01 Lab ID: 92350564004 Collected: 08/08/17 00:46 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/16/17 05:30
Date: 08/18/2017 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
..pacelabs.com
i
I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
Sample: BSW01
Lab ID: 92350554005
Collected: 08/08/17 00:47
Received: 08/08/17 11:12 Matrix: Water
Parameters
Results
Units
Report Limit DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0 1
08/14/17 23:30
08/18/17 16:40
7440-43-9 M1
Chromium
ND
ug/L
5.0 1
08/14/17 23:30
08/17/17 20:26
7440-47-3
Copper
22.8
ug/t
5 0 1
08/14/17 23.30
08/17/17 20-26
7440-50-8
Nickel
ND
ug/L
5.0 1
08/14/17 23:30
08/18/17 16:40
7440-02-0 M1
Zinc
ND
ug/L
10.0 1
08/14/17 23:30
08/18/17 16:40
7440-66-6 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20

aceAnalj cal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
Sample: BSW01 Lab ID: 92350554006 Collected: 08/08/17 00:49 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
4600CL G Chlorine, Residual
Chlorine, Total Residual
Date: 08/18/2017 06:37 PM
Analytical Method: SM 4500-CI G
0.071 mg/L 0.024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08115/1714:22 7782-50-5 H1
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I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Bakers Stormwater
Pace Project No.:
92350554
QC Batch:
373538 Analysis Method: EPA 1664E
QC Batch Method:
EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92350554004
METHOD BLANK: 2069811
Associated Lab Samples: 92350554004
Parameter Units
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/16/17 05:18
LABORATORY CONTROL SAMPLE:
2069812
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 37.1
93
78-114
MATRIX SPIKE SAMPLE:
2069813
35329509001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
54.5 40
92.9
96 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
QC Batch: 373202
Analysis Method: EPA200.7
QC Batch Method: EPA200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92350554005
METHOD BLANK: 2067775
Matrix: Water
Associated Lab Samples: 92350554005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Cadmium
ug/L
ND 1.0
08/17/17 20:10
Chromium
ug/L
ND 5.0
08/ 17/ 1 120.10
Copper
ug/L
NU b.0
08/1 //1 / 20:10
Nickel
ug/L
NU b.0
08/17/1 / 20:10
Zinc
ug/L
ND 10.0
08/17/17 20:10
LABORATORY CONTROL SAMPLE: 2067776
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
472
94
85-115
Chromium
ug/L
500
473
95
85-115
Copper
ug/L
500
492
98
85-115
Nickel
ug/L
500
463
93
85-115
Zinc
ug/L
500
484
97
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067777
2067778
MS
MSD
92350554005
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Cadmium ug/L
ND
500
500 307
306
61 61
70-130
0 M1
Chromium ug/L
ND
500
500 477
478
95 95
70-130
0
Copper ug/L
22.8
500
500 505
515
96 99
70-130
2
Nickel ug/L
ND
500
500 306
305
61 60
70-130
0 M1
Zinc ug/L
ND
500
500 323
323
64 64
70-130
0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350554
QC Batch: 372690
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92350554001
METHOD BLANK: 2064888
Matrix: Water
Associated Lab Samples: 92350554001
Blank Repurting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 08/10/17 14:24
LABORATORY CONTROL SAMPLE: 2064889
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 248
99 90-110
SAMPLE DUPLICATE: 2064890
92350492003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
SAMPLE DUPLICATE: 2064891
92350554001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
32.4
32.4 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350554
QC Batch: 373303
Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G
Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92350554006
METHOD BLANK: 2068370
Matrix: Water
Associated Lab Samples: 92350554006
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Chlorine, Total Residual
ma/t
ND 0 024 08/15/17 14-22
SAMPLE UUPLICA(E: 20683/1
92350405001 Dup
Parameter
Units
Result Result RPD Qualifiers
Chlorine, Total Residual
mg/L
ND ND H1
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersviile, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

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QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350554
QC Batch: 372626 Analysis Method: SM 5210B
QC Batch Method: SM 5210E Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92350554002
METHOD BLANK: 2064396
Associated Lab Samples: 92350554002
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2064397
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 08/14/1714:67
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 206 104 84.6-115.4
SAMPLE DUPLICATE: 2064398
92350649008 Dup
Parameter Units Result Result
BOD, 5 day mg/L 3.1 3.4
RPD Qualifiers
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350554
QC Batch: 373047 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92350554003
METHOD BLANK: 2067169 Matrix: Water
Associated Lab Samples: 92350554003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 08/14/17 14:05
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2067170
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 722 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172
MS MSD
92350458005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 115 750 750 879 867 102 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174
MS MSD
92350498001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 32.0 750 750 789 797 101 102 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: Bakers Stormwater
Pace Project No.: 92350554
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Di henylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (I CS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Bakers Stormwater
92350554
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92350554001
BSW01
92350554004
BSW01
EPA1664B
373538
92350564005
BSW01
EPA 200.7
373202 EPA 200.7
373510
92350554001
BSW01
SM 2540D
372690
92350554006
BSW01
SM 4500-CI G
373303
92350554002
13SWOI
8M 52101.3
3/2626 W 5210I3
W26/0
92350554003
BSW01
SM 5220D
373047
Date: 08/18/2017 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 20

Document Name:
Document Revised: August 4, 2017
_ - aceAnalXical'
Sample Condition Upon Receipt(SOUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.04
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersviko Raleigh❑ Mechanicsville❑
Client Name:
Project #: WO# ' 92350554
.. *��-,� � III
Courier: Fed Ex ❑UPS ❑Other: ❑Client 92
❑ Commercial ace 350554
Custody Seal Present? ❑]YYes to Seals Intact? ❑Yes \-Vo
Date/initials Person Examining Contel
Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ Other Biologic sue Frozen?
Thermometer: ` Iejt ❑Yes `� ❑N/A
WI Gun ID: _M�of
et ❑Blue ❑None
Type oflce.
Correction Factor: Cooler Temp Corrected (°C): Temp should be above freezing to 6°C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sol N/A, water sample)
Did sample or g Hate in q
r Ivoruarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {int n tiunally,
inrludina Hawaii and Puerto Ricol? FlYes o
Comments/Discrepancy:
Chain of Custody Present?
c(,Dxes
[]No
❑N/A
1.
Samples Arrived within Hold Time?
-s
[:]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
es
[]NO
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑N/A
4.
Sufficient Volume?
s
[:]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
es
[:]No
[]No
❑N/A
❑N/A
6.
Containers intact?
SQas
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Dyes
❑No
A
8.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
®$es
❑No
N/A
9.
Headspace in VOA Vials (>5.6mm)?
❑Yes
❑No
`
&/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
"'C
❑No
❑N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of split containers:
1
Project Manager SCURF Review:
Date/Time:
Field Data Required? UYes UNo
Date: e/ t,/ / 7
Project Manager SRF Review: �( Date:(rl
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 18 of 20

aceAna/ytica!'
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: August 4, 2017
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.04
Issuing Authority:
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Project #
Wp : 9235®554 PM: HWB Due Data• 08/17,17
CLIENT: 92-pllvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot ft
Page 19 of 20

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aceAnalytical
www.pacelabs.com
August 17, 2017
Mr. Joe Hinkle
Allvac
RE: r'roject: Dakers Stormwater
Pace Project No.: 92350557
,�?sJAI oaZ
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, -LC.
Page 1 of 16

Pace Analytical Services, LLC
aceAnalytical o 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
078—pacelabs.com [phone]
CERTIFICATIONS
Project: Bakers Stormwater
Pace Project No.: 92350557
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2226 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #- M-NC030
Virginia/VFI AP Certification #- 460222
North Carolina Drhilking Water Corlinc:allon hi. 37712
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Pace Analytical Services, LLC
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Huntersville, NC 28078078
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[phone]
SAMPLE ANALYTE COUNT
Project: Bakers Stormwater
Pace Project No.: 92350557
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92350557001 BSW02
SM 2540D
MVC
1 PASI-A
92350557002 BSW02
SM 5210B
ECH
1 PASI-A
92350557003 BSW02
SM 5220D
NAL
1 PASI-A
92350557004 BSW02
EPA200.7
SER
5 PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalX cal"
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350557
Sample: BSW02
Lab ID: 92350557001 Collected:
08/08/17 00:32
Received: 08/08/17 11:12 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
08/08/17 12:30
Field pH
6.8 Std. Units
0.10
1
08/08/17 12:30
Field Temperature
26.5 deg C
0.50
1
08/08/17 12:30
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
T0.0 rrng/L
12.6
1
08/ 10/ l7 23:158
REPORT OF LABORATORY ANALYSIS
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Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 16

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350557
Sample: BSW02 Lab ID: 92350557002 Collected: 08/08/17 00:34 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day
BOD, 5 day
Date: 08/17/2017 10:09 AM
Analytical Method: SM 5210B
6.6 mg/L 2.0 1 08/09/17 20:45 08/14/17 15:09
REPORT OF LABORATORY ANALYSIS
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t
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ANALYTICAL RESULTS
Project: Bakers Stormwater
Pace Project No.: 92350557
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW02 Lab ID: 92350557003 Collected: 08/08/17 00:35 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 52.0 mg/L 25.0 1 08/14/17 14:05
Date: 08/17/2017 10:09 AM
REPORT OF LABORATORY ANALYSIS
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1
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350557
Sample: BSW02 Lab ID: 92350557004 Collected: 08/08/17 00:37 Received: 08/08/17 11:12 Matrix: Water
Parameters
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
Date: 08/17/2017 10:09 AM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
ND
ug/L
1.0
1
08/14/1714:10
08/15/1715:54
7440-43-9
7.3
ug/L
5.0
1
08/14/1714:10
08/15/1715:54
7440-47-3
140
ug/L
5.0
1
08/14/1714-10
08/15/1715.54
7440-50-8
6.4
ug/L
5.0
1
08/14/1714:10
08/15/1715:54
7440-02-0
35.4
ug/L
10.0
1
08/14/1714:10
08/15/1715:54
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 7 of 16

Pace Analytical Services, LLC
ate
ceAnalytical @
loo
9800Hunte
Kincey Ave. 128078
svi le, NC
www.pacelabs.com
I
[phone]
QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350557
QC Batch: 372824
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92350557004
METHOD BLANK: 2065686
Matrix: Water
Associated Lab Samples: 92350557004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug/L
ND 1.0
08/15/1714:26
(;I Irorniurn
ug/L
NU 5.0
08/15/1 / 14:26
Copper
ug/L
ND 5.0
08/15/1714:26
Nickel
ug/L
ND 5.0
08/1511714:26
Zinc
ug/L
ND 10.0
08/15/1714:26
LABORATORY CONTROL SAMPLE: 2065687
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Cadmium
ug/L
500 478
96 85-115
Chromium
ug/L
500 482
96 85-115
Copper
ug/L
500 507
101 85-115
Nickel
ug/L
500 481
96 85-115
Zinc
ug/L
500 499
100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2065688 2065689
MS MSD
92350542001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Cone. Cone. Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium ug/L
ND
500 500 473
464 95 93
70-130
2
Chromium ug/L
ND
500 500 480
473 96 95
70-130
1
Copper ug/L
0.017
500 500 521
515 101 100
70-130
1
mg/L
Nickel ug/L
ND
500 500 476
469 95 94
70-130
1
Zinc ug/L
ND
500 500 496
489 98 96
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2065690
2065691
MS
MSD
92350498001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Cadmium
ug/L
ND
500
500
460
453
92
91
70-130
2
Chromium
ug/L
ND
500
500
469
462
94
92
70-130
2
Copper
ug/L
ND
500
500
513
505
102
101
70-130
2
Nickel
ug/L
ND
500
500
467
461
93
92
70-130
1
Zinc
ug/L
ND
500
500
491
485
97
96
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC.
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1
I
QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350557
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 372821
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92350557001
METHOD BLANK: 2065670
Matrix: Water
Associated Lab Samples: 92350557001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 08/10/17 23:50
LABORATORY CONTROL SAMPLE. 2065671
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 258 103 90-110
SAMPLE DUPLICATE: 2065672
92350737001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
18.7 D6
SAMPLE DUPLICATE: 2065673
92350675001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
34.7 37.3 7 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Bakers Stormwater
Pace Project No.: 92350557
QC Batch: 372626
QC Batch Method: SM 5210B
Associated Lab Samples: 92350557002
METHOD BLANK: 2064396
Associated Lab Samples: 92350557002
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 2.0 08/14/1714:57
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CON I ROL SAMPLE: 2064391
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 206 104 84.6-115.4
SAMPLE DUPLICATE: 2064398
92350649008 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L 3.1 3.4 9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalj cal e
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t
Project: Bakers Stormwater
Pace Project No.: 92350557
QC Batch: 373047
QC Batch Method: SM 5220D
Associated Lab Samples: 92350557003
METHOD BLANK: 2067169
Associated Lab Samples: 92350557003
Parameter
Chemical Oxygen Demand
QUALITY CONTROL DATA
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 25.0 08/14/1714:05
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2067170
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 722 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172
MS MSD
92350458005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 115 750 750 879 867 102 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174
MS MSD
92350498001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 32.0 750 750 789 797 101 102 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

aceAnalj cal
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7
I
QUALIFIERS
Project: Bakers Stormwater
Pace Project No.: 92350557
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Llmlt.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chioroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

Pace Analytical Services, LLC
aceAnalytical ®
9800Suite
Hunte sville, NC28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA CROSS REFERENCE
TABLE
Project: Bakers Stormwater
Pace Project No.: 92350557
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92350557001 BSW02
92350557004 BSW02
EPA 200.7
372824 EPA 200.7
373300
92350557001 BSW02
SM 2540D
372821
92350557002 RSW02
SM 5210B
372626 SM 6210B
372670
92350567003 BSW02
SM 5220D
373047
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 16

1 . aceAnal !cal'
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: August 4, 2017
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.04
Issuing Authority:
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
Client Name: Project W® ' 235055 "
Courier: ``��ed Ex ❑UPS ❑USPS ❑Client 11111111111111111111111
❑ Commercial C,l_(IPace ❑Other:
TT 92350357
Custody Seal Present?
Dyes IPA Seats Intact? ❑Yes
41
T
Date/Initials Person Examining [on is Q
Packing Material:
Thermometelr
\tit tK Gun ID:
❑Bubble Wrap ❑Bubble Bags ,. one
-�—�� \
(,
Type Pfie 9t
;
❑ Other Biological Tissue Frozen?
❑Yes to ❑N/A
❑Blue ❑None
Correction Factor:
Cooler Temp Corrected (`C):
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
`,�'
Regulated Soil . /A, water sample)
lia3 begun
Did samples or' mate in
myes (o
T
a quarantine zone within the United States: CA, NY, or SC (check
maps)?
Did samples originate from a foreign source (internationally,
indudine Hawaii and Puerto Rico)? nYes . 171`No
Comments/Discrepancy:
Chain of Custody Present?
s
[:]No
❑N/A
1.
Samples Arrived within Hold Time?
QZTAs
(:]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
❑No
❑N/A
3.
Time
Rush Turn Around me Requested?
❑Yes
c
two
❑N/A
4.
Sufficient Volume?
s
❑No
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
K bes
[]No
[]No
❑N/A
❑N/A
6.
Containers Intact?
KP s
[]No
[-]N/A
7.
Dissolved analysis: Samples Field Filtered?
Yes
No
/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
{(71 es
[]No
N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑N
/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[--]Yes
❑Yes
❑No
❑N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of split containers:
Project Manager SCURF Review: '
u
Field Data Required? ❑Yes ❑No
Date/Time:
Date: of c` t
Project Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 14 of 16

Document Name:
Document Revised: August 4, 2017
-
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
aceAnalytical
Document No.:
Issuing Authority:
r _'
F-CAR-CS-033-Rev.04
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Project # WO :92350557
PM: MWB Due Date: 08/17/17
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
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pH upon receipt
Date preservation adjusted
Time preservation
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Lot H
Page 15 of 16

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e16of16

R;;Vos
acmnalytical
www.p&celabs.com
August 16, 2017
Mr. Joe Hinkle
Allvac
RE: Project: Bakers Stormwater
Pace Project No.: 92350558
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnaIXical
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CERTIFICATIONS
Project: Bakers Stormwater
Pace Project No.: 92350558
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia/VFL.AP Certification M 460222
North Carolina Drinking Water Cerlificalion #: 37712
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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4
17;aceAna1yficq1'
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350558
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92350558001
BSW03
SM 2540D
SLB
1
PASI-A
92350558002
BSW03
SM 5210B
ECH
1
PASI-A
92350558003
BSW03
SM 5220D
NAL
1
PASI-A
92350558004
BSW03
EPA 200.7
SER
5
PASI-A
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aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1o0
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350558
Sample: BSW03
Lab ID: 92350558001 Collected: 08/08/17 00:55
Received: 08/08/17 11:12 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
08/08/17 12:52
Field pH
6.9 Std. Units
0.10
1
08/08/17 12:52
Field Temperature
27.6 deg C
0.50
1
08/08/11 12:b2
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total ('3U,%pondod Solids
6.2 m0/L
50
1
08/13/17 10.44
Date: 08/16/2017 06:44 PM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLG
9800 Kincey Ave. Suite lo0
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350558
Sample: BSW03 Lab ID: 92350558002 Collected: 08/08/17 00:57 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day
BOD, 5 day
Date: 08/16/2017 06:44 PM
Analytical Method: SM 5210B
2.5 mg/L 2.0 1 08/09/17 20:45 08/14/17 15:16
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bakers Stormwater
Pace Project No.: 92350558
Sample: BSW03 Lab ID: 92350558003 Collected: 08/08/17 00:58 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD
Chemical Oxygen Demand
Date: 08/16/2017 06:44 PM
Analytical Method: SM 5220D
25.0 mg/L 25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/14/17 14:05
Page 6 of 16

Pace Analytical Services, LLC
Kincey Ave.
ate 100
ceAnalytical e 9800Hunte sv lle, NC128078
www.pacelabs.com
[phone]
ANALYTICAL RESULTS
Project: Bakers Stormwater
Pace Project No.: 92350558
Sample: BSW03 Lab ID: 92350558004 Collected: 08/08/17 01:00 Received: 08/08/17 11:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0
1
08/14/1714:10
08115/1716:10
7440-43-9
Chromium
ND
ug/L
5.0
1
08/14/1714:10
08/15/1716:10
7440-47-3
Copper
23.5
ug/L
5.0
1
08/1411714:10
08/15/1716:10
7440-50-8
Nickel
ND
ug/L
5.0
1
08/14/1714:10
08/15/1716:10
7440-02-0
Zinc
14.7
ug/L
10.0
1
08/14/1714:10
08/15/1716:10
7440-66-6
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350558
QC Batch: 372824
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92350558004
METHOD BLANK: 2065686
Matrix: Water
Associated Lab Samples: 92350558004
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Cadmium
ug/L
ND
1.0
08/15/1714:26
Chromium
1.10/1
NI)
5 0
08/15/17 14-26
Copper
ug/L
ND
5.0
08/15/1714:26
Nickel
ug/L
ND
6.0
08/15/1714:26
Zinc
ug/L
ND
10.0
08/15/1714:26
Qualifiers
LABORATORY CONTROL SAMPLE:
2065687
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Cadmium
ug/L
500
478
96
85-115
Chromium
ug/L
500
482
96
85-115
Copper
ug/L
500
507
101
85-115
Nickel
ug/L
500
481
96
85-115
Zinc
ug/L
500
499
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2065688
MS
92350542001
Spike
Parameter
Units
Result
Cone.
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Copper
ug/L
0.017
500
mg/L
Nickel
ug/L
ND
500
Zinc
ug/L
ND
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2065690
MS
92350498001
Spike
Parameter
Units
Result
Cone.
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Copper
ug/L
ND
500
Nickel
ug/L
ND
500
Zinc
ug/L
ND
500
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Qualifiers
2065689
MSD
Spike MS MSD MS MSD % Rec
Cone. Result Result % Rec % Rec Limits RPD
500 473 464 95 93 70-130 2
500 480 473 96 95 70-130 1
500 521 515 101 100 70-130 1
500 476 469 95 94 70-130 1
500 496 489 98 96 70-130 1
2065691
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
500 460 453 92 91 70-130 2
500 469 462 94 92 70-130 2
500 513 505 102 101 70-130 2
500 467 461 93 92 70-130 1
500 491 485 97 96 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC.
Qua]
Qual
Page 8 of 16

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Project: Bakers Stormwater
Pace Project No.: 92350558
QC Batch: 372880
QC Batch Method: SM 2540D
Associated Lab Samples: 92350558001
METHOD BLANK: 2066136
Associated Lab Samples: 92350558001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 2066137
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2066138
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2066139
Parameter
Total Suspended Solids
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 08/13/1710:44
Spike LCS
Conc. Result
250 240
92350558001 Dup
Result Result
5.2 ND
92350698002 Dup
Units Result Result
mg/L 30.6 27.2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
96 90-110
RPD Qualifiers
RPD Qualifiers
12 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

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Project: Bakers Stormwater
Pace Project No.: 92350558
QC Batch: 372626
QC Batch Method: SM 5210B
Associated Lab Samples: 92350558002
METHOD BLANK: 2064396
Associated Lab Samples: 92350558002
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 2.0 08/14/1714:57
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2064397
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
BOD, 5 day
mg/L
198 206 104
84.6-115.4
SAMPLE DUPLICATE: 2064398
92350649008 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
13.1 3.4
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Bakers Stormwater
Pace Project No.: 92350558
QC Batch: 373047 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92350558003
METHOD BLANK: 2067169
Associated Lab Samples: 92350558003
Parameter Units
Chemical Oxygen Demand _ mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 08/14/1714:05
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2067170
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 722 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172
MS MSD
92350458005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 115 750 750 879 867 102 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174
MS MSD
92350498001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Chemical Oxygen Demand mg/L 32.0 750 750 789 797 101 102 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: Bakers Stormwater
Pace Project No.: 92350558
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
S Surrogate
1,2-Dlphenylhydrazlne decomposes to and cannot be separated from Azobenzene using Method 8210. 'fhe result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Bakers Stormwater
Pace Project No.:
92350558
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92350558001
BSW03
92350558004
BSW03
EPA 200.7
372824 EPA 200.7
373300
92350558001
BSW03
SM 2540D
372880
92350558002
BSW03
SM 52,10B
372626 SM 5210B
372670
92350558003
BSW03
SM 5220D
373047
Date: 08/16/2017 06:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Document Name:
Document Revised: August 4, 2017
°
� _ . aC6Ana1jftal
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.04
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Courier:
❑ Commercial
Custody Seal Present?
Huntersville Q�) Raleigh❑ Mechanicsville❑
Client Name:
Pro
❑Fed Ex ❑UPS ❑USPS ❑Client
iz—aace ❑Other:
❑Yes 'Q�flo Seals Intact? ❑Yes cL�'
Packing Material: ❑Bubble Wrap ❑Bubble Bags ne
Thermome : t
Gun ID: `�-i—�—�' �:;
n ace
Type of I
Correctiotor: tooter Temp Corrected (°C): ��
,�,. WWi _ 92350558
11111111111111111111111
92350558
Date/Initials Person Examining Con"":3 _�)
❑ Other Biological 'ssue Frozen?
❑Blue ❑None
❑Yes o [:]N/A
Temp should be above freezing to 6°C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sol( (i N/A, water sample)
Did samples orjtQ nate'inn quarantine zone within the united States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inte�nationaily,
.ri-i ,.,�i„d:.,a uo,.,o,� n 4 a,iartn Rirnl7 nyec �I•(j 0
u
-
Comments/Discrepancy:
Chain of Custody Present?
es
[]No
N/A
1.
Samples Arrived within Hold Time?
Qqes
[]NO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
es
❑No
❑N/A
3.
Rush Turn Around Time Requested?
Yes
o
[]N/A
4.
Sufficient Volume?
Yes
[:]No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
'es
s
[]No
[-]No
[]N/A
❑N/A
6.
Containers Intact?
s
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
6Yes
❑No
YA
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
l
s
❑No
' N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑Na
A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
(fit U
❑No
N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Date/Time:
fieia uata rtegwrear Ljres Lpvo
Lot ID of split containers:
Project Manager SCURF Review: Li Date:
Project Manager SRF Review: Date:
G�uit�
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sentto the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 14 of 16

Document Name:
Document Revised: August 4, 2017
aceAnalyiicalSample
Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.04
Issuing Authority:
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Project # WO# : g2350558
PM: MWB Due Date: 08/17/17
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
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Lot #
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age 16 of 16

11�;a'ceAnalyfical'
www.p"iabs.com
I
August 04, 2017
Mr. Joe Hinkle
Allvac
1*17 - Go^ hit 0,6o11ncJ
RE: Project: NonContact Cooling Water
Pace Project No.: 92349614
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 01, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
pCC/%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

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Project: NonContact Cooling Water
Pace Project No.: 92349614
Charlotte Certification iDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M NC030
North Carolina Drinking Water Certification #. 31112
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 400222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
NonContact Cooling Water
92349614
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92349614001
Non Contact Cooling #1
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614002
Non Contact Cooling #2
EPA 1664B
JMS
1
PASI-C
SM 4500-0I G,
MDW
1
PASI-A
92349614003
Non Contact Cooling #3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614004
Non Contact Cooling #4
EPA 1004D
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614005
Non Contact Cooling #5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614006
Non Contact Cooling #6
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614007
Non Contact Cooling #7
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92349614008
Non Contact Cooling #8
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

aceAnalytical
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l
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #1 Lab ID: 92349614001 Collected: 07/31/17 07:00 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/04/17 05:59
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.12 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 21

Pace Analytical Services, LLC
® 9800 KinceyAve. Suite too
aceAnalytical Huntersville, NC 28078
www.pacelabs.com
[phone]
1
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #2 Lab ID: 92349614002 Collected: 07/31/17 07:10 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/04/17 05:59
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.17 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

aceAnalytical
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I
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92349614
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Non Contact Cooling #3 Lab ID: 92349614003 Collected: 07/31/17 07:25 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/04/17 06:00
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.15 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 6 of 21

aceAnalytical
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t
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #4 Lab ID: 92349614004 Collected: 07/31/17 07:43 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/04/17 06:00
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.085 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 21

aceAna p cal
www.pacelabs.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92349614
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Non Contact Cooling #5 Lab ID: 92349614005 Collected: 07/31/17 08:08 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units IReport Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/04/17 06:00
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.027 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 21

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #6 Lab ID: 92349614006 Collected: 07/31/17 08:27 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/04/17 06:04
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.031 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #7 Lab ID: 92349614007 Collected: 07/31/17 08:45 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/04/17 06:04
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.027 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
Sample: Non Contact Cooling #8 Lab ID: 92349614008 Collected: 07/31/17 09:05 Received: 08/01/17 11:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/04/17 06:04
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.095 mg/L 0.024 1 08/02/17 17:49 7782-50-5 H3
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 21

aceAnalytical e
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4
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92349614
QC Batch: 371874 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007,
92349614008
METHOD BLANK: 2060348 Matrix: Water
Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007,
92349614008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Clrease frig/L ND 5.0 08/04/ 17 05:57
LABORATORY CONTROL SAMPLE: 2060349
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 38.8 97 78-114
MATRIX SPIKE SAMPLE: 2060350
92349575001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits
t
Oil and Grease mg/L ND 40 38.0 93 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 12 of 21

aceAnalytical e
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i
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92349614
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 371637 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007,
92349614008
METHOD BLANK: 2059096 Matrix: Water
Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007,
92349614008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
CI Ilofirfe, Total Residual ing/L ND U.U24 08/02/ I / 11:49
SAMPLE DUPLICATE: 2059097
92348807001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L ND ND H1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 21

Pace Analytical Services, LLC
aceAnalytical ® 9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
www.pacelabs.com
[phone]
E
QUALIFIERS
Project: NonContact Cooling Water
Pace Project No.: 92349614
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
8 Surrogate
1,2-Dlphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. 1 he result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
`4 -- Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

aceAnalytical
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t
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NonContact Cooling Water
Pace Project No.: 92349614
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92349614001
Non Contact Cooling #1
EPA 1664B
371874
92349614002
Non Contact Cooling #2
EPA 1664E
371874
92349614003
Non Contact Cooling #3
EPA 1664B
371874
92349614004
Non Contact Cooling #4
EPA 1664E
371874
9234961400.5
Non Contact Cooling #5
EPA 1664B
371874
92349614006
Non Contact Cooling #6
EPA 1664E
371874
92349614007
Non Contact Cooling #7
EPA 1664B
371874
92349614008
Non Contact Cooling #8
EPA '1664B
371874
92349014001
Non Contact Cooling #1
SM 4500-CI G
371637
92349614002
Non Contact Cooling #2
SM 4500-CI G
371637
92349614003
Non Contact Cooling #3
SM 4500-CI G
371637
92349614004
Non Contact Cooling #4
SM 4500-CI G
371637
92349614005
Non Contact Cooling #5
SM 4500-CI G
371637
92349614006
Non Contact Cooling #6
SM 4500-CI G
371637
92349614007
Non Contact Cooling #7
SM 4500-CI G
371637
92349614008
Non Contact Cooling #8
SM 4b00-CI G
371637
Date: 08/04/2017 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

aceAnalXical
Laboratory receiving samples:
Asheville ❑ Eden❑
VuLV"'C'R
Sample Condition Upon Receipt(SCUR Ppr �l `ulo
Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
SIMME11 Client Name:
❑ _ Projectp 'WI'OII #I I ' : I 9II2I'3I I4I'9II
L- ---�
61
Courier: ❑ - ❑UPS ❑USPS ❑Client
Commercial ace ❑Other: 92349614
Custody Seal Present? ❑Yes �_ Seals Intact? ❑Yes EfNo /
Date/Initials Person Examining Contents: AIC /
Packing Material: ❑Bubble Wrap Bubble Bags ❑None ❑Other:
Thermometer: El —
T�
IR Gun ID: t 0O�)— Type f Ice: et ❑Blue ❑None Samples on ice, cooling process has begun
Correction Factor: Cooler Temp Corrected (°C): r Biological Tissue Frozen? ❑Yes []No l ]WX
Temp should be above free/AEwater
to 6°C
USDA Regulated soil { sample)
Did samples on rd{e in a yuaranthle 10ue witldn the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (interna ' ally,
❑Yes _ including Hawaii and Puerto Rico)? Dyes No
Chain of Custody Present? L+l /
❑No
[I N/A
1.
Samples Arrived within Hold Time? 5*es
[]NO,
❑N/A
2.
Short Hold Time Analysis (<72 hr.)? ❑Yes
No
❑N/A
3.
4.
S.
6.
Rush Turn Around Time Requested? ❑Yes OK10 ❑N/A
Sufficient Volume? es ❑No ❑N/A
Correct Containers Used? es []No ❑N/A
-Pace Containers Used? es
❑No
❑N/A
Containers Intact? es
❑No
❑N/A
7.
Samples Field Filtered? ❑Ye
No
❑N/A
S.
Note if sediment is visible in the dissolved container
Sample Labels Match COC? Yes
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
-
Headspace in VOA Vials (>5-6mm)? ❑Yes
❑No
N/
10.
11.
Trip Blank Present? ❑Yes No N/A
Trip Blank Custody Seals Present? ❑Yes
[IN.
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes ❑No
Person Contacted:
Date/Time:
Commen,a/Sample
Discrepancy:
Project Manager SCURF Review:
Date: ,
Project Manager SRF Review:
_
Date: NtI f r
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 16 of 21

Document Name:
Document Revised: Sept. 21, 2016
aCeAnalidica/
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination Project #
®# : 92349614
is verified and within the acceptance range for
preservation samples.
PM: MWB Due Date: 08/10/17
**Bottom half of box is to list number of bottles
CLIENT: 92-A1lvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot#
Page 17 of 21

aceAnalytical
Laboratory receiving samples:
Asheville ❑ Eden❑
luiricm ivarne: vocument rcevisea: Sept, u, tine
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Greenwood ❑ HuntersvilleRaleigh❑ Mechanicsville❑
flm• Client Name Project #: W® 3 961
Courier: ❑Fed Ex ❑UPS ❑LISPS ❑Client
❑ Commercial ace ❑Other:
Custody Seal Present? ❑Yes � Seals Intact? ❑Yes No
Date/Initials Person Examining Contents:
Packing Material: "Bubble Wrap ubble Bags ❑None ❑Other:
Thermometer: ❑ IR Gun ID: 4AW-'e❑Blue ❑None
Typ of Ic
Correction Factor: Cooler Temp Corrected (•C): o
Temp should be above freezing to 6°C
USDA Regulated Soil (2 N/A, water sample)
Did samp�les, �01 Inate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
[]YesImo
PM: MWB Due Date: 08/10/17
CLIENT: 92—Allvae NC
Samples on ice, cooling process has begury
Biological Tissue Frozen? ❑Yes ❑No 011 A
Did samples originate from a foreign source (interns 'onaily,
including Hawaii and Pi artn Rirn19 MVae ni.,
Comments/Discrepancy:
Chain of Custody Present?
Yes
[]No
❑N/A
1.
Samples Arrived within Hold Time?
L�jYes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
LIN.
❑N/A
3.
Rush Turn Around Time Requested?
❑Ye
o
❑N/A
4.
Sufficient Volume?'
Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
es
❑No
[]No
❑N/A
❑N/A
6.
Containers Intact?
[3 es
❑No
❑N/A
7.
Samples Field Filtered?
❑Yes
eNo
❑N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date�me/ID/Analysis Matrix: 1^ F {
Headspace in VOA Vials (>5-6mm)?
Yes
❑Yes
No
[:]No"
❑No
❑N/A
N/A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
[]Yes
❑No
[:]No
-N A
❑ NAk-
11,
aa�a�., �•a+� irl\ i JUitl/ nC3ULU i IUN
Person Contacted:
Comment:•/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? []Yes ❑No
Date/Time:
Date:
Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 18 of 21

Document Name:
Document Revised: Sept. 21, 2016
aceAnalXical a
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
's verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Project #
Due Date: 08/10/17
CLIENT: 92-Ailvae NC
PM: MWB
u
v
0.
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Page 19 of 21

it ATI
Spcciatly Materials
Storm Water Monitorinja
(NON CONTACT)
Bakers North
Chain of Custody Record
Project Number/Name: NonContact Cooling Water
Project Location: Allvac Bakers
Sampler's Signature:
Date: 21- 9
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Meter Calibrated:
/ N
IThermorneter Calibrated
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Sampling and Field analysis completed by:
Relinquished By:
Received By:
,_st
t
Date: •/- 7
Time.
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Date: '� l " 1
Time:
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Date: , i —
Time:
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Date:
Time:
EHS Baker South SW REV N 2 5/10/2016
13 9
Page 21 of 21

AI
Specialty Materials
(NON CONTACT)
Bakers North
Chain of Custody Record
Project Number/Name: NonContact Cooling Water
Project Location: Alivac Bakers
Sampler's Signature:
Date: 7-SI-/
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Sampling and Field analysis completed by:
Relinquished By:
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Date :8-/-- 7
Time: QQo.,
Date :
Time: j
Relinquished By:
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Date: - j -
Time:
Date :
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EH5 Baker South SW REV # 2 5/10/2016 1
114 PC,( ,3-23
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002
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Page 20 of 21