NCS000329_Monitoring Reports_20180618

fiATI
June 07, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
!"=
JUN 18 '1 018
C•;lit. _...
P.O. Box 5030
2020 Asheraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: joe.hinklena,atimetals.com
Attached,. please find stormwater monitoring data for Permit No NCS000329 The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
End
Year 9 — Period 1
17
March 1, 2018
1 August 31, 2018
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Scott an
Environmental Manager

Allvac - Bakers Plant ATI Alivavo
Storinwater MonitoringReport Fonn
Sample Date: 3--J5-l8 Sample Time: 3
1 00 f,
Drainage Area = 2,915,470sci. ft. 69 acres
% Impervious = 34%
Povid hope V, /4/,m e fz
lace 44 & lvb; c, t I
e
Parameter
Result-, (mg1l)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
NQ
0.001
Chromium, total recoverable
NV
I
Copper, total recoverable
A 0 /1
0.007
Nickel, total recoverable
Q. oQ
0.26
Zinc, total recoverable
0.067
Oil and Grease
N
20
Temp (receiving stream)
4B.1-1 (deg Q
32 (deg C)
'I'otal Residual Chlorine
Y-Y
0.017
pH
"'-'e (std units)
6-9 (std units)
Storm Date: Storm Duration: / - 05' (I-Irs.) Inches of Rainfall: Q
Duration of time preceding rain event exceeding 0.1 11:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., cis) = (A x inches rain/1 2 inches/ft. x 69 acres x .66) +.9 x inches rain/1 2inches/ft. x 69 x .34)
!f'(Total, cfs) = 1.5180 x V.o?:S- (Inches of rain)+ 1.7595 x_o.o?s- (Inches of rain"

ac`eAnalytical
—pacelabs.com
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
._-D
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Rlverslde Drive, Asheville, NC 28804
Florida/NI=LAP Certification #: E=81648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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leAnalX cal
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SAMPLE ANALYTE COUNT
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92385030001 SW OUTFALL #01(B) EPA 1664B
JMS
1
PASI-C
EPA200.7
SH1
5
PASI-A
SM 2540D
MVO
1
f ;ASI A
SM 4500-CI G
EWS
1
PASI-A
SM 5210B
RL O
1
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078
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[phone]
ANALYTICAL RESULTS
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Sample: SW OUTFALL #01(B) Lab ID: 92385030001 Collected: 05/15/18 15:54 Received: 05/16/18 08:18 Matrix: Water
Parameters
Field Data
Collected By
Collected Date
Collected Time
pH
fernperature
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
4500CL G Chlorine, Residual
Chlorine, Total Residual
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
Date: 05/29/2018 04:41 PM
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method
DPJ
1
0,5115/18 15-53
05/15/18
1
05/15/18 15:53
16:46
1
05/15/18 15:53
7.8
Std. Units
0.10
1
05/15/18 15.53
28.4
deg U
0.50
I
05/15/18 15:53
Analytical Method: EPA 1664B
ND
mg/L
5.0
1
05/24/18 05:02
Analytical Method: EPA 200.7 Preparation Method: EPA
200.7
ND
ug/L
1.0
1
05/2411815:10
05/2511815:04
7440-43-9
ND
ug/L
5.0
1
0512411815:10
05/25/1815:04
7440-47-3
10.9
ug/L
5.0
1
05/24/1815:10
05125/1815:04
7440-50-8
6.5
ug/L
5.0
1
05/24/1815:10
05/25/1815:04
7440-02-0
ND
ug/L
10.0
1
05/24/1815:10
05/25/1815:04
7440-66-6
Analytical Method: SM 2540D
6.3 mg/L
Analytical Method: SM 4500-CI G
0.044 mg/L
Analytical Method: SM 5210B
2.8 mg/L
Analytical Method: SM 5220D
31.0 mg/L
2.5 1 05/21/18 20:54
0.024 1 05/22/1810:40 7782-50-5 H6
2.0 1 05/17/18 07:38 05/22/18 02:55
25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
05/25/18 16:38
Page 4 of 15

aceAn*i cal
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 412124 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92385030001
METHOD BLANK: 2286233
Associated Lab Samples: 92385030001
Parameter Units
Uil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NU 5.0 Ob/24/18 04:56
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2286234
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5 36.9
96
78-114
MATRIX SPIKE SAMPLE:
2286235
92385786001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
39.5
103
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 412205 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92385030001
METHOD BLANK: 2286555
Matrix:
Water
Associated Lab Samples: 02386030001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
05125/1817:41
Chromium
ug/L
ND
5.0
05/25/1817:41
Copper
ug/L
ND
5.0
05/2511817:41
Nickel
ug/L
ND
5.0
05/25/1817:41
Zinc
ug/L
ND
10.0
05/25/1817:41
LABORATORY CONTROL SAMPLE:
2286556
Parameter
Units
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Nickel
ug/L
Zinc
ug/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
500
491
98
85-115
500
524
105
85-115
500
548
110
85-115
500
509
102
85-115
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286557
2286558
MS
MSD
92384986001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
515
523
103
104
70-130
2
Chromium
ug/L
ND
500
500
546
555
109
111
70-130
2
Copper
ug/L
2030
500
500
2580
2610
110
117
70-130
1
Nickel
ug/L
5.1
500
500
532
541
105
107
70-130
2
Zinc
ug/L
159
500
500
653
662
99
101
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
504
491
100
98
70-130
2
Chromium
ug/L
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg/L
Copper
ug/L
0.88
500
500
1390
1380
103
100
70-130
1
mg/L
Nickel
ug/L
0.13
500
500
650
630
104
100
70-130
3
mg/L
Zinc
ug/L
12.6
500
500
13400
13300
163
158
70-130
0 M6
mg/L
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, I.I.C.
Page 6 of 15

acdeAnalXical
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 411695 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92385030001
METHOD BLANK: 2284017 Matrix: Water
Associated I. ab Samples' 92385030001
Blank Reporting
Parameter Units Result I. imit Analyzed ' Qualifiers
Total Suspended Solids mg/L ND 2.5 05/21/18 20:49
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2284018
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 256 102 90-110
SAMPLE DUPLICATE: 2284019
92384724001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
SAMPLE DUPLICATE: 2284020
92384905001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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lacemnalX-Ncal
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL#01 (B)
Pace Project No.: 92385030
QC Batch: 411753
Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G
Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92385030001
METHOD BLANK: 2284194
Matrix:
Water
Associated l ab Samples, 92385030001
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Chlorine, Total Residual
mg/L
ND
0.024 05/22/18 10:40
SAMPLE DUPLICATE: 2284195
92384160004
Dup
Parameter
Units
Result
Result RPD Qualifiers
Chlorine, Total Residual
mg/L
0.41
0.45 8 H6
SAMPLE DUPLICATE: 2284196
92385030001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Chlorine, Total Residual
mg/L
0.044
0.046 4 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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lacoeAnalX-ical
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 411072 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92385030001
METHOD BLANK: 2280664
Associated Lab Samples: 92385030001
Parameter Units
BUD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2280665
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result L imit Analyzed Qualifiers
ND 2.0 05/22/18 02:12
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 169 85 84.6-115.4
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter Units Result Result
BOD, 5 day mg/L 10.5 11.5
RPD Qualifiers
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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7
acVI, AnaIX-kaI
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SWOUTFALL#01 (B)
Pace Project No.: 92385030
QC Batch: 412405
Analysis Method: SM
5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D
COD
Associated Lab Samples: 92385030001
METHOD BLANK: 2287604
Matrix: Water
Associated Lab Samples: 92385030001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
05/25/18 16:38
LABORATORY CONTROL SAMPLE: 2287605
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand mg/L
750
741
99
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606
2287607
MS
MSD
92384807001
Spike
Spike MS
MSD
MS MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result
% Rec % Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 272
100
100 360
363
88 91
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608
2287609
MS
MSD
92385152001
Spike
Spike MS
MSD
MS MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result
% Rec % Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 298
100
100 386
395
88 97
90-110
2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

laccuAnaIX"ical
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L1M1111914c�9
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting lirrdt.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL #01 (B)
92385030
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92386030001
SW OUTFALL #01 (B)
92385030001
SW OUTFALL #01(B)
EPA1664B
412124
92385030001
SW OUTFALL #01(B)
EPA 200.7
412205 EPA 200.7
412413
92385030001
SW OUTFALL #01(B)
SM 2540D
411695
92386030001
SW UU I FALL #01(b)
SM 4500-Cl G
4111W
92385030001
SW OUTFALL #01(B)
SM 5210B
411072 SM 5210B
411080
92385030001
SW OUTFALL #01(B)
SM 5220D
412405
Date: 05/29/2018 04:41 PM
REPORT OF LABORATORY ANALYSIS
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�aceftVkal
Document Name:
Sample Condition Upon Recei t SCUR
Document Revised: February 7, 2018
Page 1 of 2
A __
Document No.:
F•CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
• Client Name,
WO923s5o3o
.. • • • . Project #:
Courier: [Aed Ex EILIPS ❑USPS ❑Client
❑ Commercial ace ❑other: 112385030
Custody Seal Present? ❑Yes Seals Intact? ❑Yes Oo
Packing Material: ❑Bubble 1Vrap ubble Bags ❑None n Other
Date/initials Person Exam Ein, C
W-�* rl�
Thermo et
Gun ID:
92TO40 Type of Ice: Wet ❑glue []None
Cooler Temp ('C): —I./ . Correction Factor: Add/Subtract (°C) +0.4
Cooler Temp Corrected (°C):
USDA Regulated Soi j a N/A, water sample)
Did samples or nat4 in a quarantine zone within the United States: CA, NY, or SC (check maps)?
nYP4- m
Biological Tissue Frozen?
❑Ye — []N/A
Tempshould be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (ante tionaily,
including Hawaii and Puerto Rico)? []Yeso
Comments/Discrepancy:
Chain of Custody Present?
C Y
[]No
❑N/A
1.
Samples Arrived within Hold Time?
E&I
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
es
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
o
❑N/A
4.
Sufficient Volume?
es
[:]No
N/A
5.
Correct Containers Used?
-Pace Containers Used?
es
es
[]No
❑No
❑N/A
❑N/A
6.
Containers intact?
Wes
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
ka/A
g.
Sample Labels Match COC?
-Includes Datelrime/ID/Analysis Matrix:
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
[:]No
/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Des
Mo
❑No
N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
I J
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Dated me:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date: (- 1
( j
Project Manager SRF Review: `CJ J Date:i
�c
Page 13 of 16

Document Name:
Sample Condition Upon Recei�
-- — 88i?AnalOGal Document -No:
F-CAR-05-033-Rev.06
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
U
Z
Z
Z
Q
V
Z
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=
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Document Revised: February 7,2018
Page 1 of 2
Office
Project # W0 ; 92385030
PM: MWB Due Date: 05/25/18
CLIENT: 92—Allvac NC
m °
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Z N C z N Z
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N S N 61 = �. z Q ;!e N Z Z
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pH Adjustment Log for Preserved Samples
ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot it
adjusted i added
i i i _
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form viill be sent to the North Carolina OEHNR Certification Office Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 14 of 15

Stormwater Monitoring
Chain of Custody Record
Project Number/Name: SW Outfall #01(B)
Project Location: ATI SM - Bakers
Sample 's Si nature:
8
Date: j-/g-CL
c
�
H
as a
Q
W
V
�..
>
u
Q. V
A
i
c
Requested Test Parameters
T
5- S-
G
G /®
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
s"
G
G 16
HNO3
Y
Cadmium
:$/
G
(9/ P
HCL
Y
Oil & Grease
G
G /&
H2SO4
Y
COD
G
G /6
None
Y
BOD j
G
G/(j
None
Y
TSS
G 16
None
Y
Residual Chlorine
Onsite Field H Analysis
Onsite Field Temperature Analysis
pH: _ %8 (sx.) Sample Time:
Temp: ,,Y_ (-C) Sample Time:
Analysis Time: .'s'
Analysis Time:
Meter Calibrated: Ye,
Thermometer Calibrated: & / N
Sampling and field analysis completed by:
Relinquished By:
Received By: +' .v, 'r
Date: J'=/
Time: �' • 5�..
Date: 5
Time (' j
Relinquished By:vw
Receive
y' -'
Date: �:; (v j
Time:
Date: �'
Time:
e: j
W-j
EHS-SW-Chain of Costody Outfall 01-Rev 001
Page 15 of 15

Allvac - Bakers Plant
7 W 1! -T-
Tr rT1"r-W.' "i
AnalyticalTechniques and Methods:
�-- i �11 I - �.' I �
�W,ample Time: S:.q
IF
fllriir 11
Drainage Area = 212,952so. ft. 4.9 acres
% Impervious = 12%
993��
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
0.001
Chromium, total recoverable
I
Copper, total recoverable
0.007
Nickel, total recoverable
LV - L9
0.26
Zinc, total recoverable
9Al
0.067
pH
(0.9 (std units)
6-9 (std units)
VWtorm Date: Storm Duration: / .05 "s.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": R
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., efs) = (A x inches rain/1 2 inches/ft. x 4.9 acres x .88) +.9 x inches rain/1 2inches/ft. x 4.9 x .12)
*(Total,cfs)=0.l437x-LQ-a-5- (Inches of rain)+ 1.0441 x 0. R6- (Inches of rain)

acmnalXical
www.p&celabs.com
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
A�,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

Pace Analytical Services, LLC
aceAnalytieaJ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NEL.AP Certification #: F87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification # 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

aceAnalj&al
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92385032001 SWOUTFALL#02 EPA200.7
SH1
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 5210B
RLO
1
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 13

Pace Analytical Services, LLC
aceMalXical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
( [phone]
I
ANALYTICAL RESULTS
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Sample: SW OUTFALL #02 Lab ID: 92385032001 Collected: 05/15/18 15:30 Received: 05/16/18 16:42 Matrix: Water
Parameters
Field Data
Collected By
Collected Date
Collected Time
p1-1
fernperature
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
Date: 05/29/2018 04:41 PM
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Analytical Method:
DPJ
1
05/15/18 15:30
05/15/18
1
05/15/18 15:30
15:24
1
05/15/18 15:30
6.9 Std. Units
0.10
1
05/ 15/18 15:30
26.1 deg C
0.50
1
05/15/18 15:30
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
ND ug/L
1.0
1
05/24/1815:10
05/25/1815:07
7440-43-9
44.6 ug/L
5.0
1
05/24/1815:10
05/25/1815:07
7440-47-3
170 ug/L
5.0
1
05/24/1815:10
05/25/1815:07
7440-50-8
41.0 ug/L
5.0
1
05/24/1815:10
05/2511815:07
7440-02-0
194 ug/L
10.0
1
05/24/1815:10
05/25/1815:07
7440-66-6
Analytical Method: SM 2540D
234 mg/L
25.0
1
05/21/18 20:54
Analytical Method: SM 5210B
4.6 mg/L
2.0
1
05/17/18 07:38
05/22/18 02:47
Analytical Method: SM 5220D
57.0 mg/L
25.0
1
05/25/1816:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
Page 4 of 13

lane'A.nalX'ical
pacelabs.com
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 412205
QC Batch Method: EPA 200.7
Associated Lab Samples: 92385032001
METHOD BLANK: 2286555
Associated Lab Samples: 92385032001
Parameter
Cadrniurn
Chrorniurn
Copper
Nickel
Zinc
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed
ug/L
NU
1.0
05/25/18 1 /:41
ug/L
ND
5.0
05/25/1817:41
ug/L
ND
5.0
05/25/1817:41
ug/L
ND
5.0
05/25/1817:41
ug/L
ND
10.0
05/25/1817:41
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2286556
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
491
98
85-115
Chromium
ug/L
500
524
105
85-115
Copper
ug/L
500
548
110
85-115
Nickel
ug/L
500
509
102
85-115
Zinc
ug/L
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286557
2286558
MS
MSD
92384986001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
515
523
103
104
70-130
2
Chromium
ug/L
ND
500
500
546
555
109
111
70-130
2
Copper
ug/L
2030
500
500
2580
2610
110
117
70-130
1
Nickel
ug/L
5.1
500
500
532
541
105
107
70-130
2
Zinc
ug/L
159
500
500
653
662
99
101
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
504
491
100
98
70-130
2
Chromium
ug/L
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg/L
Copper
ug/L
0.88
500
500
1390
1380
103
100
70-130
1
mg/L
Nickel
ug/L
0.13
500
500
650
630
104
100
70-130
3
mg/L
Zinc
ug/L
12.6
500
500
13400
13300
163
158
70-130
0 M6
mg/L
Results presented on this page are in
the units indicated by the
"Units" column except where an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

lmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 411695 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92385032001
METHOD BLANK: 2284017
Associated Lab Samples: 92385032001
Parameter
Units
total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 2284018
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 05/21/18 20:49
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 256 102 90-110
SAMPLE DUPLICATE: 2284019
92384724001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 2284020
92384905001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND ND
RPD Qualifiers
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

aceAnalytical
—pacelabs.com
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 411072
QC Batch Method: SM 5210B
Associated Lab Samples: 92385032001
METHOD BLANK: 2280664
Associated Lab Samples: 92385032001
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210E BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L NU 2.0 05/22/18 02:12
LABORATORY CONTROL SAMPLE:
2280665
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
BOD, 5 day
mg/L
198 169 85
84.6-115A
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg/L
10.5 11.5
9
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

aceAnalytical
www.p"labs.com
QUALITY CONTROL DATA
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 412405 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92385032001
METHOD BLANK: 2287604
Associated t ab Samples: 92385032001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2287605
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 05/25/1816:38 a
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 741 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606 2287607
MS MSD
92384807001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 272 100 100 360 363 88 91 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608 2287609
MS MSD
92385152001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 298 100 100 386 395 88 97 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

a'6Mnalyikal
www.pace)abs.corn
QUALIFIERS
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Llrnit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92385032001
SW OUTFALL #02
92385032001
SW OUTFALL #02
EPA 200.7
412205 EPA 200.7
412413
92385032001
SW OUTFAL L #0.2
SM 25401)
411605
92385032001
SW OUTFALL #02
SM 5210E
411072 SM 5210B
411089
92385032001
SW 011TFAL L #02
SM 5 20D
412405
Date: 05/29/2018 04:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

_ c7GeAf13 2 _ __ _
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
issuing Auihori —y-:-'
g ��
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvill4 Raleigh❑ Mechanicsville❑
MINE
Client Name: WO •923 03
Courier: Project #: Fed Ex UPS ❑USPS []Client III III I 11111111111111
❑ Commercial Pace ❑other. 92388032
Custody Seal Present? ❑Yes kP o Seals Intact? ❑Yes o �(Sr
1� Date/initials Person C Examin
Packing Material: []Bubble Wrap ❑Bubble Bags Cvone ❑ Other Biological sue Frozen?
❑Yes ❑N/A
Thermomet r: Type of Ice: q
t ❑Blue ❑Ncne
IR Gun ID: 92TO40
tooter f e np ('C): �—Currectiors Factor: Add/SublracL ('G) +0.4
Tempshould be above freezing to VC
Cooler Temp Corrected VC)- ❑ samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ([ N/A, water sample)
Did samples onQgiynate in I quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Ojm�e[jA�7tionally,
11v_-_ t7f.l_ u�,uan and auprtn RitnV nYes 7LP o
Comments/Discrepancy:
Chain of Custody Present?
Y
[:]No
❑N/A
1.
Samples Arrived within Hold Time?
l7lNo
N/A
2.
Short Hold Time Analysis (<72 hr.)?
es
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
<jja
❑N/A
4.
Sufficient Volume?
_s
.❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
[]No❑N/A
❑No
❑N/A
6.
Containers Intact?
QR9s
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
/A
8.
Sample Labels Match COC?
-Includes Dateitrime/ID/Analysis Matrix:
e' FI)es
T
[]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
[]Yes -
[]No
/A
10.
Trip Blank Present?
Trip Blank Custod Seals Present?
[]Yes
❑Yes
o
ONO
❑N/A
❑
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
f.
Project Manager SCURF Review:
Project Manager SRF Review:
1
s
Lot ID of split containers:
Date/Time:
Field Data Required? ❑Yes []No
Date: // (. / ? t
Date;
Page 11 of 13

JIMa
aCeAnafAGa1 — ___
Document Name:
Sample Condition Upon Receipt(SCUR)
-
Document Revised: February 7, 2018
Page 1 of 2
--Document No::--- _--
F-CAR-CS-033-Rev.06
— --- —Issuing-Authority:��` _
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or clechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # " W • 92385®32
PM: MWB
CLIENT:
Due Date: 05/25/18
92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
_
.._ __ ... �_ __ .. .r.o
ti-Mh rarnlina DFHNR Certification
Office (i.e.
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy or mu to m, will ue see .o
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 12 of 13

Stormwater Monitoring
Chain of Custody Record
Project Number/Name: SW Outfall #02(B)
Project Location: ATI SM - Bakers
Sam ler's Si nature:
Date: j"-
A
°'
a
.>
,
Requested Test Parameters
[
Cn �
ei
o
WE
4rO-218
3%3
G
G /0
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
G
G /d)
HNO3
Y
Cadmium C'(?
G
G / C)
H2SO4
Y
COD
G
G /C
None
Y
BOD
G
G /(D
No
Y
TSS
Onsite field H Analysis
Onsite Field Temperature Analysis
PH: �• 9 (s.u.) Sample Time: 3
Temp: d�. t (°C) Sample Time: ,3
Analysis Time:
Analysis Time:
Meter Calibrated: yes
Thermometer Calibrated: / N
Sam ling and field analysis completed b :
Relinquished B
Received
Date: S- 6- Time: •;S'.�.
Date:'
Relinquished By: ' ' yy�= -tc�t
Received
Iva
Date: }� � 4• �l
Time: "�,
Date:
(
Time:
EHS-SW-Chain of Costody Outfall 02-Rev 001
Page 13 of 13

Sample Date:
Laboratory Performing Analysis:
A' livac - Bakers Plant
Iffig
Drainage Area = 336,580so.7.8 acres
% Impervious = 15%
Ige- 'J_A C/o K-i-7-
_)0Q,Ce An9L1U7';r_zL1
ulzmwy�.
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
5D
120
TSS
100
Cadmium
XO
0.001
Chromium, total recoverable
I
/VP
Copper, total recoverable
0,066
0.007
Nickel, total recoverable
D. b66
0.26
Zinc, total recoverable
0.067
pH
7. 4? (std units)
6-9 (std units)
Storm Date: Storm Duration: / - 0 5- (Hrs.) Inches of Rainfall:5-
Duration of time preceding rain event exceeding 0.111:
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 7.8 acres x.85) +.9 x inches rain/121nches/ft. x 7.8 x.15)
Q(Tota1,cfs)=0.22l0x...D.Qs- -(Inches of rain)+ 0.0878 x__Q. c.2.1" (Inches of rain)

aceAnaly ical
..pacelabs.com
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

aceAnalj cal
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CERTIFICATIONS
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

r aceAnalj6cal
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92385033001 SW OUTFALL #03
EPA200.7
SH1
5
PASI-A
SM 2540D
WC
1
PASI-A
SM 5210B
RLO
1
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 13

lacie"A.nal�ical
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Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Sample: SW OUTFALL #03
Parameters
Field Data
Collected By
Collected Date
Collected Time
pH
Tomporature
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
Date: 05/29/2018 04:41 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92385033001 Collected: 05/15/18 15:42 Received: 05/16/18 16:42 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method:
DPJ 1 05/15/18 15:41
05/15/18 1 05/15/18 15:41
15:34 1 05/15/18 15:41
7.2 Std. Units 0.10 1 05/15/18 15:41
27.6 deg C 0.50 I 05/15/18 16:41
Analytical Method: EPA200.7 Preparation Method: EPA200.7
ND
ug/L
1.0
1
05/24/1815:10
05/25/1815:09
7440-43-9
ND
ug/L
5.0
1
05/24/1815:10
05/25/1815:09
7440-47-3
65.6
ug/L
&0
1
05/2411815:10
05/25/1815:09
7440-50-8
5.7
ug/L
5.0
1
05/24/1815:10
05/25/1815:09
7440-02-0
45.3
ug/L
10.0
1
05/24/1815:10
05/25/1815:09
7440-66-6
Analytical Method: SM 2540D
22.2 mg/L 5.0 1 05/21/18 20:55
Analytical Method: SM 5210B
6.5 mg/L 2.0 1 05/17/18 07:38 05/22/18 02:49
Analytical Method: SM 5220D
60.0 mg/L 25.0 1 05/25/1816:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

kmnalj6cal
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QUALITY CONTROL DATA
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
QC Batch: 412205 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92385033001
METHOD BLANK: 2286555
Matrix: Water
Associated Lab Samples: 92385033001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmlurn
ug/L
NU
1.0
06/25/ 18 11:41
Chromium
ug/L
ND
5.0
05/251,1817:41
Copper
ug/L
ND
5.0
05/25/1817:41
Nickel
ug/L
ND
5.0
05/25/1817:41
Zinc
ug/L
ND
10.0
05/25/1817:41
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2286556
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
Cadmium
ug/L
500
491
98
85-115
Chromium
ug/L
500
524
105
85-115
Copper
ug/L
500
548
110
85-115
Nickel
ug/L
500
509
102
85-115
Zinc
ug/L
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2286557
2286558
MS
MSD
92384986001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units Result
Cone.
Cone.
Result
Result
% Rec % Rec
Limits
RPD Qual
Cadmium
ug/L ND
500
500
515
523
103
104
70-130
2
Chromium
ug/L ND
500
500
546
555
109
111
70-130
2
Copper
ug/L 2030
500
500
2580
2610
110
117
70-130
1
Nickel
ug/L 5.1
500
500
532
541
105
107
70-130
2
Zinc
ug/L 159
500
500
653
662
99
101
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qua]
Cadmium
ug/L
ND
500
500
504
491
100
98
70-130
2
Chromium
ug/L
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg/L
Copper
ug/L
0.88
500
500
1390
1380
103
100
70-130
1
mg/L
Nickel
ug/L
0.13
500
500
650
630
104
100
70-130
3
mg/L
Zinc
ug/L
12.6
500
500
13400
13300
163
158
70-130
0 M6
mg/L
Results presented on this page are in
the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

lacmnalj6cal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1o0
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
QC Batch: 411695 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92385033001
METHOD BLANK: 2284017
Associated Lab Samples: 92385033001
Parameter Units
lutal Suspended 5ullds ing/L
LABORATORY CONTROL SAMPLE: 2284018
Parameter Units
Total Suspended Solids mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NU 2.5 05/21/18 20:49
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 256 102 90-110
SAMPLE DUPLICATE: 2284019
92384724001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 2284020
92384905001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND ND
RPD Qualifiers
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

lac
eAnalytical
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Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
QC Batch: 411072
QC Batch Method: SM 5210B
Associated Lab Samples: 92385033001
METHOD BLANK: 2280664
Associated t ab Samples* 92385033001
Parameter Units
BOD, 5 day mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NU 2.0 05/22/18 02:12
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2280665
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 169 85 84.6-115.4
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L 10.5 11.5 9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

acmnalj6cal
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Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
QC Batch: 412405
QC Batch Method: SM 52201]l
Associated Lab Samples: 92385033001
METHOD BLANK: 2287604
Associated Lab Samples: 92385033001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2287605
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NU 25.0 05/25/1816:38
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 741 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606 2287607
MS MSD
92384807001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 272 100 100 360 363 88 91 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608 2287609
MS MSD
92385152001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 298 100 100 386 395 88 97 90-110 2 M1
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

lacmnalXical
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QUALIFIERS
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Analytical
Batch
92385033001
SW OUTFALL #03
92385033001
SW OUTFALL #03
EPA 200.7
412205 EPA 200.7
412413
92385033001
SW OUTFALL #03
SM 2540D
411695
92385033001
SW OUTFALL #03
SM 5210B
411072 SM 5210B
411089
92385033001
SW OUTFAL L #03
SM 52201)
412405
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13

Document Name:
Document Revised: February 7, 2018
CCAnalyl]Cdl b
Sample Condition Upon Recei t SCUR)
Page 1 of 2
Document No..
Issuin Author(
g ty:
i
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville� Raleigh❑ Mechanicsville❑
•P,' ' i Client Name: Project #• •
WO • 92385Q33
• • �' � (�
El Commercial ace �UP5 E]USPS❑Other: []Client III III I 111111111111111
92385033
Custody Seal Present? []Yes %, Me Seals Intact? ❑Yes QE�Wo
Date/initials Person Examining Con nts:L�i Vi `(
Packing Material: ❑Bubble Wrap ❑Bubble Bags ne ❑ Other Biological Tissue Frozen? �1
Thermomet . r' ❑Ye:pNo ❑N/A
Gun ID:
92TO40 Type of Ice: Vet ❑Blue ❑None _`
Cooler Temp (•C): Correction factor: Add/Subtract (•C) 10.4 Temp should be above freezing to VC
Cooler Temp Corrected (•C): LA- tV (]Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil N/A, water sample)
Did samples on inatel'Iiarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
(—Ives . rm. Inclodina Hawaii and Puerto Rico)? ❑Yes (E
Comments/Discrepancy:
Chain of Custody Present?
es
❑No
❑N/A
1.
Samples Arrived within Hold Time?
i5es
ONo
N/A
2.
Short Hold Time Analysis (<72 hr.)?
QS6
❑No
❑N/A
3.
Rush Turn Around Time Requested?
)]Yes
%ao,
❑N/A
4.
Sufficient Volume?
es
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
k
❑No
❑No
❑N/A
❑N/A
6.
Containers Intact?
Yes
[]No
N/A
7.
Dissolved analysis: Samples Field Filtered?
Yes
[]No
N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
011
[]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
QYes .
BNo
N/A
10.
Trip Blank Present?
Trip Blank Custody SealsPresent7
[]Yes
[(Yes
Eyo
ON,
A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes []NO
Person contacted: Date/Time:
Project Manager SCURF Review: �— Date: �i (� ✓I l U
Project Manager 5Rf Review: � — Date:
Page 11 of 13

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
___
—Documert No—:
wissuing Acrthorityt--- --
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # W® ; 238533 -�
PM: MWB Due Date: 05/25/18
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 12 of 13

Stormwater Monitoring
Chain of Custody Record
Project Number/Name:
SW Outfall #03(B)
Project Location: ATI SM - Bakers
Sample 's Si nature:
Date: LA - 8
Ow
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Ey
W
Requested Test Parameters
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23 3
T
- S=
G
G /®
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
$:
G
G/ O
HNO3
Y
Cadmium f
:
G
G /O
H2SO4
Y
COD
G
G /®
None
Y
BOD
G
G /
LEL
Y
TSS
Onsite fieI5 pH Analysis
Onsite Field Temperature Analysis
PH: ��_(sx.)
Sample Time:
;,3
Temp: (°C) Sample Time:
Analysis Time:
Analysis Time: 3•'33
Meter Calibrated: Ye
Thermometer Calibrated: (9 / N
Sampling and field analysis completed b :
IReceiveaI;y:\—,-Yt-A\,vj3—
Relin wished By:
Date: 5-'-/6
Time:
Date: ( — . �,�
i �.
Relinquished B
c� -
Receive B
,`
Date: U
ITime:' `�'
Date:
ime:
EHS-SW-Chain of Costody Outfall 03-Rev 001
Page 13 of 13

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i�
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit htt sp ://deg.ne.gov/about/divisions/energy-mineral-land-
resources/energy-mineral-1 and-permits/stormwater-permits/npdes-industrial-sw#tab-4
Permit No.: NlCI,�IQ/Q/Qll�l�l or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: 4 js A//YaC nga.,kw-s-
County: an I0A Phone No. 'jD'Y' a89—'A/S//
Inspector: Dowlw ` C 3A
Date of Inspection:
Time of Inspection: .3 : sa
Total Event Precipitation (inches): D • o?Jf
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
........... ..... ................ .. .............
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. Raw I Structure (pipe, ditch, etc.): Sp//l Nl6w
Receiving Stream: If
Describe the industrial activities that occur within the outfall drainage area:
MElk 1 S'4ofVe-
rage I of 2
S WU-242, Last modified 07/28/2017

2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: d ar
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /VdA e
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
® 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
(Rj' 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
(D 2 3 4 5
Is there any foam in the stormwater discharge? O Yes OeNo.
Is there an oil sheen in the stormwater discharge? oYes 12)No.
Is there evidence of erosion or deposition at the outfall? O Yes � No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe " tad n Q
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07Y28/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit ht s:Hde .nc. ov/about/divisions/ener -mineral-land-
resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4
Permit No.: N/C/ S/ O / O/ D /SI,IQI or Certificate of Coverage No.: N/C/G/_/_/_/ /_/ /
Facility Name: ,4r� z4//iret G -J&Ai Pr r
County: &hiDii Phone No. 70 y-a q
Inspector: 190WId Age ag
Bate of Inspection- z
Time of Inspection: 3
Total Event Precipitation (inches): e9 . a S
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. SW Structure (pipe, ditch, etc.): 10 pQ
Receiving Stream: _
Describe the industrial activities that occur within the outfall drainage area:
me a 1 rc9
Page 1 of 2
SWU-242, Last modified 07/28/2017

, 2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 64a G
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 © 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 ® 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 ® 3 4 5
7. Is there any foam in the stormwater discharge? O Yes No.
8. Is there an oil sheen in the stormwater discharge? OYes (DNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes ONO.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe A e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

6 #H
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https:Hdeg.nc.gov/about/divisions/energy-mineral-land-
resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4
Permit No.: N/C/�/ D /D / O l,�l�lyQ/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: --A7,r-
County: ZZ4/,2/7
Inspector: 2?6W"W Pppd /
Date; of hispection.
Tiine of hlspmtioit:
Total Event Precipitation (inches): t9. a S
Phone No. 7tPAl -O?Sq
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of
1. Outfall Description:
Outfall No. 85WcQj Structure (pipe, ditch, etc.):
Receiving Stream:
Dl�D2 ��iTcit
Describe the industrial activities That occur withinthe outfall drainage area:
Page 1 of 2
SWU-242, Last modified 07/28/2017

. 2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G7le6.'`
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 0/1 PG
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
('D 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
® 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes No.
8. Is there an oil sheen in the stormwater discharge? OYes (SNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes '*"No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Mi e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

lacoAnalyfical"
w"..pamlabs.cwn
May 24, 2018
Mr. Joe Hinkle
Allvac
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
A^
REPOR I OF LABORAI ORY ANALYSIS
This report shall not be reproduced, except in full,
f
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

Pace Analytical Services, LLC
leac
Analyt.�eal 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pamiabs.com [phone]
CERTIFICATIONS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Maaaaahusotts Cortificition # M N0030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky LIST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/M AP Certification #: 460222
REPORT OF t_ABORATORY ANALYSIS
`Phis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceMalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92385034001
NONCONTACT #1
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034002
NONCONTACT #2
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92386034003
NONCONTACT #3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92386034004
NUNCON [AC 1 #4
EPA 1664B
JMS
.1
PASIA;
SM 4500-CI G
EWS
1
PASI-A
92385034005
NONCONTACT #5
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034006
NONCONTACT #6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034007
NONCONTACT #7
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034008
NONCONTACT #8
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 20

laconalj6cal"
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #1 Lab ID: 92385034001 Collected: 05/15/18 10:40 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05/24/18 05:02
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, total Residual 0.035 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #2 Lab ID: 92385034002 Collected: 05/15/18 11:00 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease 14.9 mg/L 5.0 1 05/24/18 05:03
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.039 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

lacieAnalyficafo
www.pacelabs.can
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #3 Lab ID: 92386034003 Collected: 05/15/18 11:23 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05/24/18 05:06
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.053 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

aGeAnalj&al
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #4 Lab ID: 92385034004 Collected: 05/15/18 11:45 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.40 mg/L 0.048 2 05/22/18 10:40 7782-50-5 H6
REPORT OF LABORATORY ANALYSIS
l his report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20

lacmnalWical"
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #7 Lab ID: 92385034007 Collected: 05/15/18 12:52 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05/24/18 05:08
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.097 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
I his report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 20

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #8 Lab ID: 92385034008 Collected: 05/15/18 13:15 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05/24/18 05:08
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.051 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

lrV3Analytical
W—pacelabs.com
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 412124 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
METHOD BLANK: 2286233 Matrix: Water
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease ing/L ND 5.0 05/24/ 18 04:56
LABORATORY CONTROL SAMPLE:
2286234
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5 36.9
96
78-114
MATRIX SPIKE SAMPLE:
2286235
92385786001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
39.5
103
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 20

1,'%,Analy4ical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 411753 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
METHOD BLANK: 2284194 Matrix: Water
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, lotal Residual mg/L NU 0.024 Ob/22/18 10:40
SAMPLE DUPLICATE: 2284195
92384160004 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0.41 0.45 8 H6
SAMPLE DUPLICATE: 2284196
92385030001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0.044 0.046 4 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

(�IacieAnalj6calo
www.pacelabs.com
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDt -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S Surrogato
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

aceAnaljtical
wwwpacelabs.rom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92385034001
NONCONTACT #1
EPA 1664B
412124
92385034002
NONCONTACT #2
EPA 1664B
412124
92385034003
NONCONTACT #3
EPA 1664E
412124
92385034004
NONCONTACT #4
EPA 1664E
412124
92385034005
NONCONTACT #5
EPA 1664B
412124
92385034006
NONCONTACT #6
EPA 1004B
412124
92385034007
NONCONTACT #7
EPA 1664B
412124
92386034008
NONCONTACT #8
EPA 1664E
412124
92385034001
NONCONTACT #1
SM 4500-CI G
411753
92385034002
NONCONTACT #2
SM 4500-CI G
411753
92385034003
NONCONTACT #3
SM 4500-CI G
411753
92385034004
NONCONTACT #4
SM 4500-CI G
411753
92385034005
NONCONTACT #5
SM 4500-CI G
411753
92385034006
NONCONTACT #6
SM 4500-CI G
411753
92385034007
NONCONTACT #7
SM 4500-CI G
411753
92385034008
NONCONTACT #8
SM 4500-CI O
411753
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 20

laneAnalXjcal.
www.pacelabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #5 Lab ID: 92385034005 Collected: 05/15/18 12:10 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.22 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
I his report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

aceAna1j4ica1
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #6 Lab ID: 92385034006 Collected: 05/15/18 12:30 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.044 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20

Document Name: Document Revised: February 7, 2018
_ __ Sample Condition Upon _ etei A(SCUI;)e Page 1 of 2
aceAnalyiwoI Document No.: Issuing Authority:
r F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
o
n
Client Name:
Project
Courier: []Fed Ex ❑UPS I EJUSPS ❑Client
I illlll
❑ Commercial t OPace ❑Other: 82385034
Custody Seal Present? ❑Yes (�No Seals Intact? ❑Yes o ��1 .
TT Date/initials Person Examining Lten
Packing Material: []Bubble Wrap r�i8 bble Bags ❑None ❑ Other
Thermo; / C�,
R Gun ID: 42T040 Type of ice: ''`�"t ❑Blue
Cooler Temp ('C): Ll I Correction Factor: Add/Subtract (°C) -i•0.4
Cooler Temp Corr6ctrid (°C): !
USDA Regulated Soil in N/A, water sample)
Did samples orjgipate in I quarantine zone within the United States: CA, NY, or SC (check maps)?
MYec t1ilbin
Biological ue Frozen?
❑Yes N/A
[]None
Tamp should he above freezing to 6°C
[]Sarnples out of tamp criteria. Sampler on ire, cooling process
has begun
Did samples originate from a foreign source (InterDAlonally,
including Hawaii and Puerto Rico)? Dyes
Comments/discrepancy:
Chain of Custody Present?
es
[]No❑N/A
1.
Samples Arrived within Hold Time?
es
❑No
[-]N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes llZo
❑N/A
4.
Sufficient Volume?
es
[:]No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
k.12Ves
[]No
[]No
[-]N/A
❑N/A
6.
Containers Intact?
es
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Yes
❑No
NIA
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Q(�es
�4\�
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
PV.
IG/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
o
❑No
❑t{/A
�v((N//A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes ❑No
Person contacted: Date/Time:
Project Manager SCURF Review:) Date:f
Project Manager SRF Review: Date:
Page 16 of 20

GeAflalyhCal—�
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
issaing Authority
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # O : 923034
PM: MWB Due Date: 05/25/18
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot It
neu nm l'...NC�eHnn
llfFle•u ri a
Note: Wheneverthereisadiscrepancy attecnngrNormLarounacompnancesampleo,aL.Ny-1„> Y„1,,<-11.�.. ••-••••--•--- ---
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 20

(NON CONTACT)
Bakers North
Chain of Custody Record
ATI
Specially Materials
page k1
Project Number/Name: NonContact oling Water
Project Location: Allvac Bakers
Sampler's Signature:
IDate:
V!
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Requested Test
Parameters
G
Ge
None
Y
.,�"
,3f�.
Residual Chlorine
N
:QQa,,
G
GO
None
Y
Residual Chlorine
G
GAD
None
Y
ia?3.8
Residual Chlorine
hn p
;,,,
G
G,D
None
Y
Residual Chlorine
G
G/0
None
Y
Residual Chlorine
JAA
G
G&
None
Y
Residual Chlorine
G
G/,b
None
Y
Residual Chlorine
AM
G
G
None
Y
7.3
Residual Chlorine
Meter Calibrated:
J N
IThermometer
Calibrated
®/ N
Sampling and Field analysis completed by:
Relinquished By:
lReceived
BY:
Date: S 6-Ae
Date:
Relinquished By:
Received
Date: » r
Time:
a
Date:
Time:
EHS Baker South SW REV # 2 5/10/2016
Page 18 of 20

— -- ceAri�a ical--
!
Document Name:
Sample Condition Upon Recei t(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
--
Docum-
ent No.:
F-CAR-CS-033-Rev.06
ssuingAuthordy:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
Projectit
WO#:92385034
verified and within the acceptance range for preservation
PM: MWB
Due Date: 05/25/18
samples.
CLIENT:
92-Allvae NC
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
E
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=
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot g
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certrfrcation Office %he.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 19 of 20

Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
AT
Specialty Materials
page #2
Project Number/Name: NonContact Cooling Water
Project Location: Allvac Bakers
Sampler's Signature:
Date:
6
in
o
i=
CL
0
L.
Q.
d
=
0
a
Z
a
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Requested Test
Parameters
`'� Z:36"So
g"- ✓�-
/0
G
G
HCL
Y
30. y
Oil & Grease
Aff4mid'e-00?
G
G
HCL
Y
, 7
Oil & Grease
Con a cf#S
G
G
HCL
Y
Oil & Grease
G
G
HCL
Y
Oil & Grease
en 5�
D
G
G
I HCL
Y
Oil & Grease
G
G
HCL
Y
Oil & Grease
p f%7
G
G
HCL
Y
Oil & Grease
VOW
G
G
HCL
Y
,,3
Oil & Grease
Meter Calibrated: / N
Thermometer Calibrated: / N
Sampling and Field analysis completed by:
Relinquished By:
IRelinquished By:;�
Date :� =/(_
Time: ty�a•-.
Date ITi
e:
Relinquished By:
�: � `v �'� . ,
R wished B
Date: 5 � I ( ' J
Time:
EHS Baker South SW REV # 2 5/10/2016
I,
Page 20 of 20