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Home My WebLink AboutNCG020854_2016 Analytical Results Wastewater_20160630�alc eAnalytica wwwpecela6s carp June 30, 2016 Glenn Amey Charrah 330 S Tryon St Suite 510 Charlotte, NC 28202 RE: Project: Stormwater 6/28 Pace Project No.: 92303136 Dear Glenn Amey: Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, ,; Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Collin Mummerl, Charah Inc REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Page 1 of 16 aceAnalyt'%cal " pacs1ebs.can Project: Stormwater 6128 Pace Project No.: 92303136 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification* 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 Page 2 of 16 GtVt-i/ naly cal' wwwpacalab&wn SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 2225 Riverside Or Asheville, NC 28804 (828)254-7176 Project: Pace Project No. Stormwater 6128 92303136 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92303136001 BASIN 2 SM 2540D CHM 1 PASI-E SM 254OF CHM 1 PASI-E EPA 180.1 MLS 1 PASI-A 92303136002 BASIN 4 SM 2540D CHM 1 PASI-E SM 2540F CHM 1 PASI-E EPA 180.1 MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page 3 of 16 �,;ace Analytical www.peselab&=n Project: Stormwater 6/28 Pace Project No.: 92303136 Lab Sample ID Client Sample ID Method Parameters 92303136001 BASIN 2 SM 2540D Total Suspended Solids EPA 180.1 Turbidity 92303136002 BASIN 4 EPA 180.1 Turbidity Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 15.3 mg/L 3.3 06/29/1614:08 13.4 NTU 1.0 06/30/1610:42 5.4 NTU 1.0 06/3011610:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page 4 of 16 accAnalytical o waw.pacelabscam PROJECT NARRATIVE Project: Stormwater 6/28 Pace Project No.: 92303136 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Charah Date: June 30, 2016 Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 General Information: 2 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below, Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, Inc. Page 5 of 16 1'!;a'ceAna1ytica10 www.pacelabscom PROJECT NARRATIVE Project: Stormwater 6/28 Pace Project No: 92303136 Method: SM 254OF Description: 2540F Total Settleable Solids Client: Charah Date: June 30, 2016 Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 General Information: 2 samples were analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below Matrix Spikes: Ail percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page 6 of 16 aceAnalytical " maw.pecelabs.cam Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 PROJECT NARRATIVE Project: Stormwater 6/28 Pace Project No., 92303136 Method: EPA 180.1 Description: 180.1 Turbidity Client: Charah Date: June 30, 2016 General Information: 2 samples were analyzed for EPA 180.1 All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spilka: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Page 7 of 16 Pace Analytical Services, Inc. aceA+� fe+j� 2225 Riverside Dr. Ir�Ct1Xtt a Asheville, NC 28804 bs.corn (828)254-7176 ANALYTICAL RESULTS Project: Stormwater 6/28 Pace Project No.: 92303136 Sample: BASIN 2 Parameters lab ID: 92303136001 Collected: 06/28/16 12:00 Results Units Report Limit DF Received: 06/2811614:15 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 15.3 mg/L 3.3 1 06/29/1614:08 264OF Total Settleable Solids Analytical Method: SM 254OF Total Settleable Solids ND mL/tJhr 0.10 1 06/29/16 12:35 180.1 Turbidity Analytical Method: EPA 180.1 Turbidity 13.4 NTU 1.0 1 06/3011610:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 16 Pace Analytical Services, Inc. 2225 Riverside Dr 1!2ceAnalytical' Asheville, NC 28804 w4w.pa abs.com (828)254-7176 ANALYTICAL RESULTS Project: Stormwater 6/28 Pace Project No. 92303136 Sample: BASIN 4 Lab ID: 92303136002 Collected: 06/28/16 12:20 Received: 06/28/16 14:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 06/29/16 14:08 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids ND mUL/hr 0.10 1 06/29/16 12:35 180.1 Turbidity Analytical Method: EPA 180.1 Turbidity 5.4 NTU 1.0 1 06130/1610:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc. Page 9 of 16 11�;a7ceAnalyticals` wwwpacslabs com QUALITY CONTROL DATA Project: Stormwater 6/28 Pace Project No.: 92303136 QC Batch: EDEN/23295 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description 2540D Total Suspended Solids Associated Lab Samples: 92303136001, 92303136002 Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 METHOD BLANK: 1768700 Matrix: Water Associated Lab Samples: 92303136001, 92303136002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 06/29/16 13:59 LABORATORY CONTROL SAMPLE: 1768701 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250� 258� 103 90-110 SAMPLE DUPLICATE: 1769669 92302994002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1769670 92303054001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids _.. .._._ . _ mg/L 53.3 52.6 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc Page 10 of 16 ceAnalj4icala .. cart i QUALITY CONTROL DATA Project: Stormwater 6/28 Pace Project No 92303136 QC Batch: EDEN/23292 Analysis Method: SM 2540F QC Batch Method: SM 2540F Analysis Description' 2540F Total Settable Solids Associated Lab Samples: 92303136001, 92303136002 METHOD BLANK: 1768594 Matrix: Water Associated Lab Samples 92303136001, 92303136002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Settleable Solids mUUhr ND 0.10 06/29/16 12:35 SAMPLE DUPLICATE: 1768595 92303136001 Dup Parameter Units Result Result RPD Qualifiers Total Settleable Solids mL/Uhr ND ND Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc Page 11 of 16 aceAnalyllcal www.pacwabs.com QUALITY CONTROL DATA Project: Stormwater 6128 Pace Project No.: 92303136 QC Batch: WET/45945 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description 180.1 Turbidity Associated Lab Samples: 92303136001, 92303136002 METHOD BLANK: 1769908 Matrix: Water Associated Lab Samples: 92303136001. 92303136002 Blank Reporting Parameter Units Result Limit Analyzed Turbidity NTU _ ND 1.0 06130/1610:42 LABORATORY CONTROL SAMPLE: 1769909 Qualifiers Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10 100 90-110 SAMPLE DUPLICATE: 1769910 92303136001 Dup Parameter Units Result Result RPD Qualifiers Turbidity NTU 13.4 13.2 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc. Page 12 of 16 aceAnalyticale wwwpacelabs.com QUALIFIERS Project: Stormwater 6128 Pace Project No.. 92303136 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit PQL- Practical Quantitation Limit. RL - Reporting Limit S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270- The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethyivinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SVV846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PASI-E Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc Page 13 of 16 1�;a7ceAnalytical' www.pacsfabs.mm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 6/28 Pace Project No.: 92303136 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92303136001 BASIN 2 SM 2540D EDEN/23295 92303136002 BASIN 4 SM 2540D EDEN/23295 92303136001 BASIN 2 SM 254OF EDEN/23292 92303136002 BASIN 4 SM 2540F EDEN/23292 92303136001 BASIN 2 EPA 180.1 WET/45945 92303136002 BASIN 4 EPA 180.1 WET/45945 Date: 06/30/2016 11:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Analytical Batch Page 14 of 16 Document Name: r Sample Condition Upon Rout t(SCt1R) Document No.: F-RAt-CS-001-Rev.04 • �I' Client Name: z' Project st: Courier: M Fed Ex ❑uP ❑uses _ Client ❑ Commercial []Pace ❑Other: Document Revised: May 24, 2016 _ Page 1 of 2 Issuing Authority: Pace Ralelah Quality Office W 'Oft • 92303136 1111111111111111111111 92303136 Custody Seal Present? ❑Yes VNo Seals Intact? []Yes [XNo Date/Initlais Person Examining Contents, � Z� AP Packing Material: ❑Bubble Wrap ❑Bubble Bags Non ❑Other: ! Thermometer: T1505 Type f! [ Wet []Blue []None ❑Samples on ice, cooling process h s begun Correction Factor: OA'C Cooler Temp Corrected ('C): Biological Tissue Frozen? El ONO X/A Temp should be above Ffezing to 6'CiUSDA Regulated Sall (N/A, water sample) Did samples riginate In uarantine zone within the United States: CA, NY, orSC (check maps)? old samples originate from a foreign source (interpationally, f�ivacMn Inrludin¢ Hawaii and Puerto Rlcol? rlYes NO Comments/DIscrepency. Chain of Custody Present? Yes ❑No 1]N/A 1. Samples Arrived within Hold Time? Yes ❑No N/A 2. Short Hold Time Anal sls <02 hr.)? Yes ON. QNJA 3. � Rush Turn Around Time Requested? Elyes 156NO ❑NJA 4. Sufficient Volume? Yes []No[]WA S. Correct Containers Used? [7Yes ❑No []NJA 6. -Pace Containers Used? (Yes C]No LJNJA Containers Intact? tYes No EINIA 7. Samples Field Filtered? ❑Yes ❑No Q4 S. Note If sediment is visible In the dissolved container Sample labels Match COC? (Yes []NO ❑N/A 9, -Includes Date/Time/ID/Analysis Matrlx: A7 ACI containers needing acid/base preservation have been 10.1 "04a checked? [Yes ❑No ❑N/A All containers needing preservation are found to be In / HOPHQ compliance with EPA recommendation? MOsa+a«: (HNOs, H2504, HCk2; NaOH >9 Sulfide, NaOH>12 Cyanide) ( Yes ❑No ❑N/A wn+Obu Exceptions: VOA, Conform, TOC, On and Grease, ff 0R0/8015 (water) DOC LLH Yes No EINIA NaW1L'& `a"'0 Samples checked for dechlorinatlon? Yas []No N A 11. Heads aca In VOA Vials >"mm ? ljy.r, ON. N/A ' 12, Trip Blank Present? ❑Yes []NO N/A 13. Trip Blank Custody Seals Present? Dyes ❑No eN/A Pace Trip Blank lot # (if purchased): CUENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Datefnme: Field Data Required? []Yes []No Project Manager SCURF Review: �`" Date: I/ A?/ I <. Project Manager SRF Review: Date: ! r Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Ca Tina qHNR Certification Office (Le. Out of hold, incorrect preservative, out of tamp, incorrect containers) Page 15 of 16 t clei t' matt ol " .picslabs,toal j 6701 Confewoe Drive, Raleigh, NC 27607 ph: (919) 634.4984, Esc: (919) 8348497 NCWW Cartd67, NCDW CerW7731 Report Results To: Company: Chain of Custody • AddressAlit MDAL,rc —i'fr 1 • Attn:,..�r1dJ•t'1t" Phone: Fax: Sampled by (signature): Bill To: Project Reffe*re♦nce� , WA Z—�Y Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rusts profwa are su 30d to Pry+ approval by OW laboratory Requested Due Date: Fieceipt t gwociits ( L.! Vniy) 0 4t2°C I Tend: °G Res. Chlorine: ❑ Absent ❑ Present ❑ rda Acid prasKv. <27 ❑ Yes ❑ NO ❑ nla Base prasaw. -127 ❑ Yes ❑ No ❑ rda Page 16 of 16