NCG020354_2016 Analytical Results Wastewater_20160114

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1_,A11(ac6Ana1j4ica1
www.pacelabs.com
i
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
January 14, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Sed Basin 7 1/7
Pace Project No.: 92282272
PcCr6-Q 3S�-/
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Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
%4 pCCRFO��
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 19

[ F
aceAna1j caf
www.pacelabs.com
I
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Lab ID Sample ID
92282272001 SED 7
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
SM 2130B
DWJ
1
PASI-E
SM 2540D
CHM
1
PASI-E
SM 2540F
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 9222D
RC
1
PASI-R
REPORT OF LABORATORY ANALYSIS
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aceAnalytical o
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY OF DETECTION
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Lab Sample ID
Method
Client Sample ID
Parameters
Result
Units
92282272001
SED 7
SM 2130B
Turbidity
9.6
NTU
SM 2540D
Total Suspended Solids
7.9
mg/L
EPA 9040
pH
4.2
Std. Units
SM 9222D
Fecal Coliforms
4.0
CFU/100 mL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Report Limit
Analyzed Qualifiers
0.50
01/08/1611:10
2.5
01/08/1611:27
0.10
01/08/1611:47 H6
1.0
01/07/1616:20 1g
Page 4 of 19

,�aceAnalyfical'
www.pacelabs.com
I
PROJECT NARRATIVE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Method: SM 2130B
Description: 2130E Turbidity EDN
Client: Charah
Date: January 14, 2016
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 19

t s
aCoe Analytical
- www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN/21359
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1643609)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 6 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Method: SM 2540F
Description: 2540F Total Settleable Solids
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 7 of 19

0
aceAna1j cal ®
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Method: EPA 9040
Description: 9040 pH
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SED 7 (Lab ID: 92282272001)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 19

a
aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Method: SM 9222D
Description: MBIO 9222D Fecal Coliform RAL
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 9222D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: RB10/5848
1g: This is a less than value
• SED 7 (Lab ID: 92282272001)
• Fecal Coliforms
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 9 of 19

Pace Analytical Services, Inc.
aceAnalytical
2225 Riverside Dr.
J
Asheville, NC 28804
www.pacelabs.com
I
[phone]
ANALYTICAL RESULTS
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Sample: SED 7
Lab ID: 92282272001 Collected:
01/07/16
12:00
Received: 01/07/16 16:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qua[
2130E Turbidity EDN
Analytical Method: SM 2130B
Turbidity
9.6 NTU
0.50
1
01/08/1611:10
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7.9 mg/L
2.5
1
01/08/16 11:27
254OF Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mL/L/hr
0.10
1
01/08/16 11:10
9040 pH
Analytical Method: EPA 9040
pH
4.2 Std. Units
0.10
1
01/08/16 11:47 H6
MBIO 9222D Fecal Coliform RAL
Analytical Method: SM 9222D
Fecal Coliforms
4.0 CFU/100 mL
1.0
1
01/07/16 16:20 1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
QC Batch: EDEN/21357 Analysis Method: SM 2130B
QC Batch Method: SM 2130B Analysis Description: 2130E Turbidity EDN
Associated Lab Samples: 92282272001
METHOD BLANK: 1643578 Matrix: Water
Associated Lab Samples: 92282272001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 0.50 01/08/1611:10
SAMPLE DUPLICATE: 1643579
92282272001 Dup
Parameter Units Result Result
Turbidity NTU 9.6 9.6
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 19

aceAnalj6cal
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
QC Batch: EDEN/21359
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92282272001
METHOD BLANK: 1643607
Matrix: Water
Associated Lab Samples: 92282272001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 01/08/16 11:26
LABORATORY CONTROL SAMPLE: 1643608
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 242
97 90-110
SAMPLE DUPLICATE: 1643609
92282233001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
72.0 67.2 7 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 19

aceAnalytical @
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
QC Batch: EDEN/21356 Analysis Method: SM 254OF
QC Batch Method: SM 2540F Analysis Description: 2540F Total Settable Solids
Associated Lab Samples: 92282272001
METHOD BLANK: 1643576
Associated Lab Samples: 92282272001
Parameter Units
Total Settleable Solids mL/L/hr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 01/08/1611:10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc..
Page 13 of 19

ar
_ aceAnalyticai
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I
QUALITY CONTROL DATA
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
QC Batch: EDEN/21361 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92282272001
SAMPLE DUPLICATE: 1643679
Parameter
pH
92282272001 Dup
Units Result Result RPD Qualifiers
Std. Units 4.2 4.2 0 H6
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
QC Batch: R1310/5848
QC Batch Method: SM 9222D
Associated Lab Samples: 92282272001
METHOD BLANK: 1643328
Associated Lab Samples: 92282272001
Parameter
Fecal Coliforms
SAMPLE DUPLICATE: 1643329
Parameter
Fecal Coliforms
QUALITY CONTROL DATA
Analysis Method: SM 9222D
Analysis Description: 9222D MBIO Fecal Coliform - RAL
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
CFU/100 mL ND 1.0 01/07/16 15:35
92282231001 Dup
Units Result Result RPD Qualifiers
CFU/100 mL 6.0 17.0 96
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc..
Page 15 of 19

Pace Analytical Services, Inc.
® 2225 Riverside Dr.
aceAna1j&a1Asheville, NC 28804
www.pacelabs.com [phone]
QUALIFIERS
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Lab ID
Sample ID
QC
Batch Method
QC Batch
92282272001
SED 7
SM
2130B
EDEN/21357
92282272001
SED 7
SM
2540D
EDEN/21359
92282272001
SED 7
SM
2540F
EDEN/21356
92282272001
SED 7
EPA 9040
EDEN/21361
92282272001
SED 7
SM
9222D
RB10/5848
Date: 01 /14/2016 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical Method
Analytical
Batch
Page 17 of 19

-_ aceAnalytical
wwrw.pscelsbs.cam
6701 Conference Drive, Raleigh, NC 27607
ph: [phone], fax: [phone]
NCWW CerM7, NCDW Cert#37731
Chain oCustody
Report Results To:
Company:
Address: M fit
Attn: _M:rt�e.t-+''
Fax: �'�i (VKcI't`C C, )tnk • �y�
Sampled by (signature):
Bill To:
Project Reference: :!�c- s; n -'
12 i'�_1t p_rctT_
Project Number:
Purchase Order #:
• Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
`Rush projects are subject to prior approval by
the laboratory
Requested Due Date:
Page 18 of 19

Document Name:
Document No.:
Document Revised: 260CT2015
Page 1 of 2
Issuing Authority.
Pace Huntersville Quality Office
Client Name:
Nra,�mrey; Project #; : `�
M 1�11�
Courier: ❑Fed Ex []UPS ❑LISPS [Cllent II II 'III I I iII II
nCommerclal ❑Pace Other: 1
92282272
Custody Seal on Cooler/Box Present? ❑Yes Qdo Seats intact? Dyes PKo
Packing Material: ❑Bubble Wrap []Hubble Bags [/None ❑Other:
Thermometer AIR Gun SN: 122065387
Used: ❑ IR Gun SN:122065371 Type of ice: [ Yet []Blue []None []Samples on Ice, cooling process has begun
Cooler Temp Corrected (`C): r Biological Tissue Frozen? []Yes ❑No N/A
Temp should be above fre zing to 61C Correction Factor: 010 °C Date and Initials of Person Examining Contents
USDA Regulated Soil ( (?N/A, water sample)
Did samples o_r,l8Inate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
[]Yes (,QN0 Including Hawaii and Puerto Rico)? ❑Yes "No
if Yes to either question, fill out a Regulated Soil Checklist and Include with 5CURICOC oaverwork. /
COMMENTS:
Chain of Custody Present?
Yes
ONO
❑N/A
1,
Chain of Custody Filled Out?
Yes
ONO
N/A
2.
Chalri of Custody Relinquished?
iAYes
ONO
❑N/A
3.
Sampler Name and/or Signature on COC?
Yes
ONO
❑N/A
4.
Samples Arrived within Hold Time?
Yes
ONO
N/A
S.
Short Hold time Anal sis <72 fir)?
Yes
LINO
CINJA
6qI
Rush Turn Around Time Requested?
Oyes
dNo
N/A
7.
Sufficient Volume?
MYes
ONO
N/A
8.
Correct Containers Used?
-Pace Containers Used?
es
ges
ONO
ONO
❑N/A
❑N/A
9.
Containers Intact?
Yes
ONO
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
OYes
ONO
AN/A
11. Note if Sediment Is vlsible In the dissolved container
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
yes
ONO
❑N/A
12.
All containers needing acid/base preservation have been
checked?
All containers needing preservation are found to be in
compliance with EPA recommendation?
(HNO3, HzSO4, HCI<2; NaOH >9 Sulfide, NaOH>32 Cyanide)
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC, LLHg
(Yes
T
Yes
Yes
[]NO
[:]No
ONO
❑N/A
❑NIA
ONIA
13.
Samples checked for dechlorization
16yes
ONO
[]N/A
14.
Headspace in VOA Vials (>5-6mm)?
[]Yes ,
ONO
N/A
15.
Trip Blank Present?
Trip Blank Custody Seals Present?
Pace TripBlank lot # (if purchased):
❑Yes
©Yes
❑No
ONO
N/A
(fN/A
!!!!!
16.
CLIENT NOTIFICATION/RESOLUTION Field Data Required? []Yes []No
Person Contacted: Date/Time;
Comments/Resolution:
Project Manager SCURF Review: _ Date: f
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the / rth roltna DEHNR Certification Office (i.e. out of
hold, Incorrect preservative, out of temp, Incorrect containers).