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Home My WebLink AboutNCG020354_2015 Annual Summary DMR StormwaterANNUAL SUMMARY DISCHARGE MONITORING REPORT (DMR) — STORMWATER SUBMIT TO CENTRAL OFFICE* General Permit No. NCG020000 Calendar Year _Did A d03 371j `Report ALL STORMWATER monitoring data on this form (include "No Flov 7"No Discharge" and Benchmark Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year. Certificate of Coverage No. NCG02 ®F3100 sL►(k�►r�l %�t� 1 /Y�� + rFacility Name: County:I Phone Number: ( } Total no. of SDOs monitored Certified Laboratory Lab#� Lab # Stormwater Discharge Outfall (SDO) No. _ I VMA Outfall? Yes ❑ No 2 Is this outfall currently in Tier 2 for any parameter? Yes ❑ No [:�' Was this outfall ever in Tier 2 during the past year? Yes ❑ No Eg- If (his uulfall was in Tier 2 last year, was rnurithly rnuidtolling discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring Other ❑ Outfall No. 1 Total Rainfall, inches TSS, mg/I SS, mill Turbidity,Non-polar NTU Upstream (U) Turbidity, NTU Downstream (D ) Turbidity, NTU O&G, mg/1 (VMA) New Motor Oil Usage allmo. Stormwater Date Sample Collected, mo/dd/ r Indicate NO F applicable Circle gemqrnark 0050 0.1 Circle chmark N/A 26/10s°l ► N/A Quality is >55 galfmo. average requires TSS and Non-polar OSG monitoring Permit Date 10/1/2015 — 9/30/2020 Last Revised 10-2-2015 MT Certificate of Coverage No. NCG02 ® 7 ®L7J Additional Outfall Attachment (make copies as needed for additional outfalls) Stormwater Discharge Outfall (SDO) No. ?_ VMA Outfall? Yes ❑ No a Is this outfall currently in Tier 2 for any parameter? Yes ❑ No [� Was this outfall ever in Tier 2 during the past year? Yes ❑ No [� If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring E]-� Other ❑ Outfall No. Total Rainfall, inches TSS, mgll SS, ml/I Turbidity, NTU Upstream (U) Turbidity, NTU Downstream (D) Turbidity, NTU Non -polar O&G, mg/l (VMA) New Motor Oil Usage al/mo. Stormwater Benchmarks Indicate NO aFLO;� c"� :� 00 0 0.1 C' mart 5 25/10 N/A Water applies N/A Standarrd ApplIes `� >65 averagearequires TSS and O&G monitoringlar Date Sample Collected, mo/ddl r :. `f Permit Date 10/1 /2015 — 9/30/2020 Last Revised 10-2-2015 Certificate of Coverage No, NCG02]L Additional Outfall Attachment (make copies as needed for additional outfalls) Stormwater Discharge Outfall (SDO) No. 19_ VMA Outfall? Yes ❑ No 21 Is this outfall currently in Tier 2 for any parameter? Yes ❑ No Was this outfall ever in Tier 2 during the past year? Yes ❑ No If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring [� Other ❑ • Total - Turbidity, Upstream•.New T i MM Motor Oil Wall/Usage Stormwater Benchmarks!jN/A . { iii 0� . , .. , . avenge mquim • _ .A.;I • . • $?go-._ ! !' K s5_' .�]�:;.da _mod .�^s1,..{-: Permit Date 10/1/2015 — 9/30/2020 Last Revised 10-2-2015 Certificate of Coverage No, NCG02 [0 ; C51 Additional Outfall Attachment (make copies as needed for additional outfalls) Stormwater Discharge Outfall (SDO) No. VMA Outfall? Yes ❑ No Q Is this outfall currently in Tier 2 for any parameter? Yes ❑ No Was this outfall ever in Tier 2 during the past year? Yes ❑ No Q' If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency Ll Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring 9-11 Other ❑ Outfall No. Total Rainfall, inches TSS, mg/l SS, ml/I Turbidity, NTU Upstream (U) Turbidity, NTU Downstream (D) Turbidity, NTU Non -polar O&G, mgll (VMA) New Motor Oil Usage Stormwater Benchmarks Ccrcl ark 10 50 0.1 Cary,ark 50 25/10 N/A s�;e;°;`,.s N/A �„„15 average req�;ns TSS and 03G moNnoltnhn'e`Date Sample Collected, mold / r jIndkAftN° Permit Date 10/112015 — 9130/2020 Last Revised 10-2-2015 Certificate of Coverage No Additional Outfall Attachment (make copies as needed for additional outfalls) Stormwater Discharge Outfall (SDO) No. VMA Outfall? Yes ❑ Is this outfall currently in Tier 2 for any parameter? Yes ❑ Was this outfall ever in Tier 2 during the past year? Yes ❑ If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring Q� Other u NCG02 [6] 61L No No f� No [� Outfall No. Total Rainfall, inches TSS, mg/I SS, mill Turbidity, NTU Upstream (U) Turbidity, NTU Downstream (D) Turbidity, NTU Non -polar O&G, mg/I (VMA)(gal/Mo.) New Motor Oil Usage Stormwater Benchmarks In&wft NO FLOappilC c mark 160 0.1 C1mle NIA bmark 5 26110 skaantla, Quality Wat10 liies NIA ality Standard ; es 15 >55 galiMo. average requires lar T03G mormoSS and ring Date Sample_:" Collected, mold / r 121 Z D '' , q2)' t Permit Date 10/1/2015 — 9/30/2020 Last Revised 10-2-2015 Certificate of Coverage No. NCG02 ®0MY] Additional Outfall Attachment (make copies as needed for additional outfalls) Stormwater Discharge Outfall (SDO) No. VMA Outfall? Yes ❑ No []� �I Is this outfall currently in Tier 2 for any parameter? Yes ❑ No [� Was this outfall ever in Tier 2 during the past year? Yes ❑ No If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ No, turbidity benchmark exceedances did not require monthly monitoring Other ❑ Out-7 No. Total Rainfall, inches TSS, mg/I SS, mill Turbidity, NTU Upstream (U) Turbidity, NTU Downstream (D) Turbidity, NTU Non -polar O&G, mg/I (VMA) New Motor Oil Usage al/mo.) Stormwater Benchmarks Indicate NO apPowae g Circle Benchmark 100/50 0.1 Circle nchmark 125110 N/A Standard apppli s N/A Standard appWater lies s 1 `� >55 galimo. average requires TSS and 03G monitoringlar Date Sample Collected, molddf r x Permit Date 10/1/2015 — 9/30/2020 Last Revised 10-2-2015 Certificate of Coverage No. NCG02 ❑nnF] CERTIFICATION "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Required by 40 CFR §122 221 Signature Date Mail Annual Summary Stormwater DMR to the NCDEQ Central Office: Note the address is correct — Central Files is housed in DWR (not DEMLR) N.C. Department of Environmental Quality (DEQ) Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files Telephone (919) 807-6300 Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at: (919) 707-9220 Permit Date 10/1/2015 — 9/30/2020 Last Revised 10-2-2015 .Green Meadow, LLC February 25, 2016 North Carolina Department of Environmental Quality Division of Water Resources ATTN: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Stormwater Monitoring Results Brickhaven Mine No. 2 Tract "A" Permit No. NCG020354 Chatham County To whom it may Concern: Attached, please find the results for the stormwater monitoring required at the Brickhaven Mine No. 2, Tract "A" site. The stormwater basins were under construction during 2015 and did not discharge in the first half of the year. Construction of Basins 2, 3, 4, and 6 was completed in the second half of 2015 and Basin 1 was completed in early 2016. Due to the timing of the construction of the site and the stormwater basins, the seeding and subsequent growth of the grass was sporadic; therefore, did not provide an effective measure for filtering the stormwater. Thus, we exceeded the TSS and Turbidity limits. This exceedance put the site into Tier One Response for Turbidity and Tier One for benchmarks except turbidity. Our response is as follows: 1. Within one week of receipt of the results, we conducted a stormwater management inspection to identify causes and potential action items to improve our discharge. 2. The identified action items include: i. Sample each basin to determine which flocculent to use at each basin. ii. Establish the use of a floc block (or similar) in the swales leading to each basin. iii. Establish vegetative cover as soon as seasonally possible. 3. Establish monthly sampling of stormwater discharge. 4. Record this exceedance in our SWPPP. 5. Record our response in the SWPPP. Action items i and ii have been put in place. We are preparing to vegetate the site as soon as seasonally possible. Please contact me with any questions you may have regarding this information. Green Meadow, LLC • 12601 Plantside Drive • Louisville, Kentucky 40299 0: 502-245-1353 • F: 502-245-7398 Sincerely, n q Glenn Amey, PG Engineering Manager Green Meadow, LLC • 12601 Plantside Drive • Louisville, Kentucky 40299 0: 502-245-1353 • F: 502-245-7398 aceAnalytical —pacelabs.com December 30, 2015 Glenn Amey Charrah 330 S Tryon St Suite 510 Charlotte, NC 28202 RE: Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Dear Glenn Amey: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on December 28, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 19 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 19 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: NPDES Basin Monitoring 12/28 92281239 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92281239001 SED 1 SM 2130B KCE 1 PASI-E SM 2540D DWJ 1 PASI-E SM 2540F KCE 1 PASI-E 92281239002 SED 2 SM 2130B KCE 1 PASI-E SM 2540D DWJ 1 PASI-E SM 2540F KCE 1 PASI-E 92281239003 SED 3 SM 2130B KCE 1 PASI-E SM 2540D DWJ 1 PASI-E SM 2540F KCE 1 PASI-E 92281239004 SED 4 SM 2130E KCE 1 PASI-E SM 2540D DWJ 1 PASI-E SM 2540F KCE 1 PASI-E 92281239005 SED 6 SM 2130E KCE 1 PASI-E SM 2540D DWJ 1 PASI-E SM 2540F KCE 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 19 �WeAnalytical@ www.pacelabs.com Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Lab Sample ID Client Sample ID Method Parameters 92281239001 SED 1 SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids 92281239002 SED 2 SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids 92281239003 SED 3 SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids 92281239004 SED 4 SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids 92281239005 SED 6 SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SUMMARY OF DETECTION Result Units Report Limit Analyzed 13200 NTU 500 12/29/1514:20 8900 mg/L 100 12/30/15 08:45 920 mUUhr 0.10 12/29/1514:10 4980 NTU 250 12/29/1514:20 680 mg/L 31.2 12/30/15 08:47 0.10 mUUhr 0.10 12/29/1514:11 4260 NTU 250 12/29/1514:20 186 mg/L 12.5 12/30/15 08:47 0.20 mUUhr 0.10 12129/1514:11 3100 NTU 250 12/29/1514:20 492 mg/L 20.0 12/30/15 08:48 0.10 mUUhr 0.10 12/29/1514:12 2000 NTU 250 12/29/1514:20 431 mg/L 20.0 12/30/15 08:48 0.20 mL/Uhr 0.10 12/29/1514:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 4 of 19 aceAnalytical www.pacelabs.com PROJECT NARRATIVE Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Method: SM 2130B Description: 2130B Turbidity EDN Client: Charah Date: December 30, 2015 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 General Information: 5 samples were analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 19 aceAnalj6cal —pacelabs.com PROJECT NARRATIVE Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Charah Date: December 30, 2015 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 General Information: 5 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: Ail surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 19 aceAnalytical www.pacelabs.com I PROJEW NARRA'IIVI_ Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Method: SM 2540F Description: 2540F Total Settleable Solids Client: Charah Date: December 30, 2015 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 General Information: 5 samples were analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 19 P aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Sample: SED 1 Lab ID: 92281239001 Collected: 12/28/15 12:00 Received: 12/28/15 16:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2130E Turbidity EDN Analytical Method: SM 2130B Turbidity 13200 NTU 500 1000 12/29/1514:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8900 mg/L 100 1 12/30/15 08:45 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids 920 mL/L/hr 0.10 1 12/29/15 14:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Sample: SED 2 Lab ID: 92281239002 Collected: 12/28/15 12:00 Received: 12/28/15 16:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2130B Turbidity EDN Analytical Method: SM 2130B Turbidity 4980 NTU 250 500 12/29/1514:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 680 mg/L 31.2 1 12/30/15 08:47 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids 0.10 mUUhr 0.10 1 12/29/15 14:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 19 . aceAnalytical wmpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Sample: SED 3 Lab ID: 92281239003 Collected: 12/28/15 12:00 Received: 12/28/15 16:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 2130E Turbidity EDN Analytical Method: SM 2130B Turbidity 4260 NTU 250 500 12/29/1514:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 186 mg/L 12.5 1 12/30/15 08:47 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids 0.20 mL/L/hr 0.10 1 12/29/15 14:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Sample: SED 4 Lab ID: 92281239004 Collected: 12/28/15 12:00 Received: 12/28/15 16:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 2130E Turbidity EDN Analytical Method: SM 2130B Turbidity 3100 NTU 250 500 12/29/1514:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 492 mg/L 20.0 1 12/30/15 08:48 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids 0.10 mL/L/hr 0.10 1 12/29/15 14:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Sample: SED 6 Lab ID: 92281239005 Collected: 12/28/15 12:00 Received: 12/28/15 16:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2130B Turbidity EDN Analytical Method: SM 2130B Turbidity 2000 NTU 250 500 12/29/1514:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 431 mg/L 20.0 1 12/30/15 08:48 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids 0.20 mL/L/hr 0.10 1 12/29/15 14:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 QC Batch: EDEN/21242 Analysis Method: SM 2130B QC Batch Method: SM 2130B Analysis Description: 2130B Turbidity EDN Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 METHOD BLANK: 1638714 Matrix: Water Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Turbidity NTU ND 0.50 12/29/1514:20 SAMPLE DUPLICATE: 1638715 Turbidity Parameter 92281249001 Dup Units Result Result NTU 1.5 RPD Qualifiers 1.4 7 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 QC Batch: EDEN/21246 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 METHOD BLANK: 1639021 Matrix: Water Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/30/15 08:44 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 1639022 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 260 104 90-110 SAMPLE DUPLICATE: 1639023 92281239001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 8900 8890 0 SAMPLE DUPLICATE: 1639024 92281296001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 337 320 5 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 QC Batch: EDEN/21237 Analysis Method: SM 2540F QC Batch Method: SM 2540F Analysis Description: 254OF Total Settable Solids Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 METHOD BLANK: 1638626 Matrix: Water Associated Lab Samples: 92281239001, 92281239002, 92281239003, 92281239004, 92281239005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Settleable Solids mL/L/hr ND 0.10 12/29/15 14:10 SAMPLE DUPLICATE: 1638627 92281239001 Dup Parameter Units Result Result RPD Qualifiers Total Settleable Solids mL/L/hr 920 920 0 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 19 aceAnalytical www.pacelabs.com I QUALIFIERS Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST-E Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:30 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NPDES Basin Monitoring 12/28 Pace Project No.: 92281239 Lab ID Sample ID QC Batch Method QC Batch 92281239001 SED 1 SM 2130B EDEN/21242 92281239002 SED 2 SM 2130B EDEN/21242 92281239003 SED 3 SM 2130E EDEN/21242 92281239004 SED 4 SM 2130E EDEN/21242 92281239005 SED 6 SM 2130E EDEN/21242 92281239001 SED 1 SM 2540D EDEN/21246 92281239002 SED 2 SM 2540D EDEN/21246 92281239003 SED 3 SM 2540D EDEN/21246 92281239004 SED 4 SM 2540D EDEN/21246 92281239005 SED 6 SM 2540D EDEN/21246 92281239001 SED 1 SM 2540F EDEN/21237 92281239002 SED 2 SM 2540F EDEN/21237 92281239003 SED 3 SM 2540F EDEN/21237 92281239004 SED 4 SM 2540F EDEN/21237 92281239006 SGD 6 SM 2540F EDEN/21237 Date: 12/30/2015 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Analytical Method Analytical Batch Page 17 of 19 E aceAnalytical www.pacclabs.com 6701 Conference Drtva, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 834.6497 NOW W Ce067, NCDW Cert#37731 Report Results To: Company: Address: I71 Mon c urf - r I c>_f wov�l RJ., � • vi y tJG� Zi 5'3�I Phone: Fax: GMv{e,-ICCarc.k.at Sampled by (signature): Bain 0f Custody W.O.# Bill To: Project Reference: t1JFD,6:S 15 -5 iA' pn i i�ri ic� Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: �t'Hc.cc.Ltc. �'j'olicic�� 'T55, %YYbi.l; � Z 1 ©o Z jz i; `„'C1f i4ELbi< �OIJ�Sr Sr J✓Y�iictt ,z It,' vv K 1 L't �u-J tGs+LtG �OI it S, I�Sr ✓b+di ego M� 5 Relinqui by (signature) Fir by Dag ( Time AltrgG"shed by (signature) ved by (signature) Da Time Relinquished by (signature) Received by (signature) Date Tme Receipt Conditions (La4) Only) ❑ 4±VC ❑Temp: r°C Res. Chlorine: ❑ Absent ❑ Present ❑ rda Acid preserv. <2? 0Yes ❑No ❑Na Base preserv. >12? ❑ Yes ❑ No ❑ n/a Page 18 of 19 T Oocument Name: A Sample Condition Upon Receipt(SC 1 aceAnalytieal Document No.: j F-RAL-CS-001-rev.03 Oocurnent Revised: 260CT2015 Page 1 of 2 issuing Authority: Pace Huntersville Quality Office Client Name: Project If: WO#:92281239 um, AV,, Courier: ❑fed Ex ❑UPS ❑USPS oIlent ❑Commercial ❑Pace ❑Other: 92281239 iii Custody Seal on Cooler/Box Present? ❑Yes P,0 Seals intact? ❑Yes C oN-o Packing Material: []Bubble Wrap []Bubble Bags ANone ❑Other: Thermometer X-i IRGunSN:122065387 Used: IR Gun SN:122065371 Type of tee: ,&Wet (]Blue []None []Samples on ice, cooling process has begun Cooler Temp Corrected (`C): Biological Tissue Frozen? [Yes ❑No N/A Temp should be above freezing to 6°C Correction Factor: 0.0 "C Date and Initials of Person Examining Contents 2 Z USDA Regulated Soil ( ON/A, water sample) ID'Id samples or mate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes ( No Including Hawaii and Puerto Rico)? ❑Yes [;lo If Yes to either question, fill out a Regulated Soil Checklist and include with SCUR/COC paperwork. COMMENTS: Chain of Custody Present? Yes ❑No ❑N/A 1. Chain of Custody Filled Out? Yes ONO N/A 2- Chaln of Custody Relinquished? 96X9s QNo N/A 3. Sampler Name and/or Signature on COC? e$ JJNO N/A 4. Samples Arrived within Hold Time? 16yes ONO ❑N/A S. Short Hold Time Analysis (<72 hr)? Yes ON, ❑N/A 6. S0V�- t Rush Turn Around Time Requested? Yes No N/A 7. Sufficient Volume? Yes No N/A B. Correct Containers Used? ( Yes ONo [jN/A 9. -Pace Containers Used? ( Yes No N/A Containers Intact? Yes CJND ❑N/A 10. filtered Volume Received for Dissolved Tests? No N/A 11. Note if sedlmdnt Is visible in the dissolved container Sample Labels Match COC? ,-,]Yes tLl Yes ❑No ❑N/A 12. -Includes Date/Time ID Ana) sis Matrix - All All containers needing acid/base preservation have been 13. checked? Yes ❑No ❑N/A Ail containers needing preservation are found to be in (( compliance with EPA recommendation? (HNO3, H2SO4, HCI<2; NaOH >9 Sulfide, NaOH>32 Cyanide) F4Yes ©No [3N/A Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC,LLH es []No N A Samples checked for dechlorization EiYes No N A 14. Heads ace in VOA Vlals (>5-6mm)? []Yes . C3No /A 15. Trip Blan-, Present? DYes QNo PN/A 16. Trip Blank Custody Seals Present? []Yes ❑No • VN/A Pace Trip Blank tot N (if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Resolution: Date/Time: Field Data Required? []Yes ❑No Project Manager SCURF Review: 4 — irate: 1�- �y Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the orth hold, Incorrect preservative, out of temp, incorrect containers). Office (Le. out of Page 19 of 19