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HomeMy WebLinkAboutWQ0037637_Annual Report_20190301t� n Engineers and Sal Scientists Agri -Waste Technology, Inc. 501 North Salem Street Suite 203 Apex, NC 27502 919-859-0669 www.agriwaste.com January 25, 2019 Billy Dunham, President Craven Ag Services, Inc. 2115 Highway 55 New Bern, NC 28562 Subject: Annual Report for Residuals Permit WQ0037637- Calendar Year 2018 Craven Ag Services, Inc. Craven County, NC Mr. Dunham: Please find attached the required annual report for this facility. This permit allows for several residuals sources. These are the Town of Bridgeton, Town of Maysville, Ocean Bay Villas, and Pruitt Health Care. Of these, only Town of Bridgeton and Town of Maysville was land applied during 2018. All are small domestic wastewater plants with annual sampling requirements. All are liquid residuals with very low (less than 2%) solids contents. Included with this report, as required, are soil test reports and residuals sampling analyses for the two wastewater plants with residuals removal for land application. Also included are the bench sheets supporting that PSRP was met. Also included are the operator daily log field sheets and a copy of Permit WQ0037637 Attachment B. This is the fourth year of land application for this permit. Cumulative loadings are shown as required. For each residuals source, residuals are lime stabilized using hydrated lime to meet PSRP. Vector attraction is met by either, or both, alkaline stabilization and/or incorporation within 6 hours after application. No occasions of permit non-cornpliance are noted. Land Application Events: Four fields received residuals in 2018 and these occurred in six differing application events. The fields and application events are shown in the table below. Residuals application events for 2018- Craven Ag Services, Inc. Field No. 2018 application events Volume Acres Source 3-1 7/11/18 38,200 gal 3.0 Town of Maysville 6-1 1/25/18 40,000 gpq 6.4 Town of Maysville 6-1 3/8/18 19,000 gal 6.4 Town of Bridgeton 6-3 1/24/18 21,000 gal 4.6 Town of Bridgeton 6-3 6/20/18 21,000 gal 4.6 Town of Bridgeton 6-4 8/24/18 20,000 gal 6.2 Town of Bridgeton Summary comments about the residuals sources The residuals sources under this permit are low solids and handled as liquids. All are domestic with no pretreatment program or industrial inputs. Volumes are very low and field application rates are very low, and the resulting constituent loading rates of nutrients and metals are correspondingly low. No annual or lifetime limits are approached. Residuals are lime stabilized as per EPA 503 and DWR 2T requirements. Bench sheets attached to this report substantiate the data collection to support PSRP. Please note that the SAR for the Town of Bridgeton was recalculated based on sludge sample raw data. The lab report with the SAR (calculated) of 0.9 is incorrect. The true SAR as calculated by the raw Na, Ca, and Mg data is 29.2. Note that while this SAR would be considered a high value if this were an irrigation water source, that a 1-time event with the low_volume-does ----- pose any concern to soils or crops. The key parameter to watch with any product with a high sodium concentration is the exchangeable sodium percentage (ESP) in the soil. This relates the sodium percentage as a function of the soil cation exchange capacity. Bridgeton residuals went to fields 6-1, 6-3, and 6-4. The ESP for each of these soils is as follows: Field ESP 6-1 1.09 6-3 1.25 6-4 3.33 In all cases, ESP is well below threshold recommended values for action of 15. Our recommendation is to monitor sodium continually, and reduce or eliminate sodium sources to any field when ESP exceeds 10. 2__. The order of this annual report is as follows: COVER LETTER FORM ACF FORMS RSSF AND RSSF(B) FORMS MFLSF (one for each field: 3-1, 6-1, 6-3, 6-4) FORMS FSF (one for each field: 3-1, 6-1, 6-3, 6-4) LABORATORY SHEETS Includes: Residuals Sample Data Residuals TCLP Operators Alkaline Stabilization Data Log Sheets FORMS PVRF 2T SOIL TEST RESULTS FIELD SOILS TESTS SUPPLEMENTAL `lam 1) COPIES OF PERMIT FIELD MAPS FOR FIELDS 3-1, 6-3,1. 6-1 2) PERMIT WQ0037637 ATTACHMENT B ------------------------------------------------------------------------------------------------------------------ The permittee and contact information: Craven Ag Services, Inc. John W. (Billy) Dunham, President and ORC 2115 Highway 55 New Bern, NC 28562 252-670-8530 cra_venaservices ii mail.com This annual report was prepared by: Karl Shaffer, L.S.S. Agri Waste Technology, Inc. 501 N. Salem St.- Suite 203 Apex, NC 27502 919-244-1984 kshaffer@agriwaste.com Please contact me for any questions or concerns about this report. Thank you for allowing us to provide this service. Sincerely, .' � 4 /0//' Karl Shaffer, LSS 3 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: 0 030707 County: A iL64 Year: Facility Name (as shown on permit): 11 (-'raven 1rg Land Application Operator: B; t t 2019 Phone: 2,5°2 - 6 70 - $F 3Q Land application of residuals as allowed by the permit occurred during the past calendar year? XYes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Anplication Summarv: Total number of application fields in the ermit: ' Total number of fields utilized for land application during the year: Total amount of dry tons applied during the year for all application sites: �• 6 Total number of acres utilizes for land application during the year: awe 0, Part B - Annual Comuiance Statement: �} Facility was compliant during calendar year with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. A Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." <La",Wc, U% o`caF1'— Permittee Name and Title (type or print) ignature of Permittee Date —fI -/ Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) v ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: VJQ 00376 31 Laboratory: 1) tnylrolwed 1 Facility Name: C OeRW r ._ r i S 2) Residual Source WQ # or /� 3) NPDES #: / e- 00 74 4) WWTP Name: 5) Residual Analvsis Data Conc. Sample or Composite Date Parameter Limit !-F (mg/kg) m k a Z.. Percent Solids (%) NA or surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. certify, under penalty of law, that this document wos p�epared under my direction or supervision in accordance with a system designed assure tiat qualifted personnel properly gathered and valuated the information submitted. I am aware that there are significant nalties for submitting false information, including the; ossibility of fines and imprisonment for knowing violations." 5rignature of Preparer 'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 a -1.? /p' Date DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: D Od 37 6 3' Facility Name: MILD V -Servlsea Residual Source NPDES # or WQ#: oej 74 0,3-7 WWTP Name: -rOW OIC rr ual Analvsis Data Parameter (mg/kg) '/Z 5// A 7/17 7.0 3490 =mom . ,� -® A as 10. ,SZ * PPA, Laboratory: 1) L�Y1V rYl1'1'1Q17f �. 2) itn rirvn 3) 4) 5) or Composite Date e alty of law, that this document was pi tpared under my direction or supervision in accordance with a system that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are for submitting false information, including the possibility of fines and imprisonment for knowing violations." reparer!* defined to 40 CFR Part 503.9(r) and 15A NCAC 2T J�1102 (26) Date DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Laboratory: Facility Name: �' Se s en Residual Source WQ # or NPDES #: 2D 0 r 4 9 2- WWTP Name: o&vn c' , Residual Analysis Data 1) ie�✓irc9wPr7�cd CI>ernInc 2) 3) 4) 5) I Parameter Conc. .� �. Percent Solids (%)I��ff Cadmium Chromium Molybdenum 'For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "T certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name:_ Residual Source NPDES # or WQ#: A/C 0r, 2 j 4. g 2- WWTP Name: e4 Residual Analysis Data Laboratory: C/-* ,,; s6- /'M C 2) 3) 4) 5) Parameter (mg/kg) �- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* f Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C f`we n A`, r� I Gas Total Dry Tons Applied (Annual): ,o2a i a Permit #: W 0 PO a Cation Exchange Capacity (non 503 only): n; A Operator: )nhn W put, �,�y�.� Owner:yGU All W, 201- h2�M Predominant Soil Series: j&I 6 rook, Acres Used: 3, Q Acres Permitted: 3.0 Site #: j ail G h Field #: 3- Residual Analvsis Data (Heave Metals and Total Phosphorus use mgtkg, % Solids use Raw Percent #): Com- posite Date Total P • •.•ENNEEMENEEN. E Annual Heaw Metal Field Loadings (Calculated in lbs/acre): MEN Total Phos- phorus ®. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including -the possibility of fines and imprisonment for knowing violations". gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Prayer.wJ Sir V1,CQ j Total Dry Tons Applied (Annual): 3 45 Permit #: UJ co 3 Cation Exchange Capacity (non 503 only): NA _ Operator: ab �, (/� yn e, yr, Owner: jL.N Nn W Durham Predominant Soil Series: '�grbom Acres Used: 6, Acres Permitted: 6 A _ Site #: 6 Field #: 6-1 Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent #): k ' .10 posite Daten-i rAm Wa_�--_-_____ Annual Heavy Metal Field Loadings (Ualculated in lbs/acre): Total 1/ 2 3 4 5 6 7 S 9 10 11 12 DT/Ac./ f/���i j �' �/ �f vc • i of�/ 0 7�� App. / Event a 48 01%3 r r rc s CLzais Arsenic ;.rdpQ9 043� J.Lbi2. CadmiumcW65'31 001 fG Copper . 01 LZ O-q Lead 601 Total e� t phonis "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that -qualified -personnel properly gathered -and -evaluated the -$formation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". gnature of Land Applier //-� Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* V Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report FacilityName: Crewe r1 Total Dry Tons Applied (Annual): 6. Permit #: W!2 00 3-76 3'7 Cation Exchange Capacity (non 503 only): AJ Operator: _jOAA (Al 'p,,p( rr Owner: Jd�sr �+� �n �m Predominant Soil Series: Lg p Acres Used: 4 , Acres Permitted: 4.6 Site #: �pU G h �_ Field #: 6,- 3 Residual Annlvsis Data (Heavy Metals and Total Phosphorus use mom. % Solids use Raw Percent #): Com- Date positeMENOMONEE TotalAN Phos- . • j ra Annual Heavy Metal Held Loadings (Ualculated in ibs/acre): Total DT/Ac./ Event _1J )� o J/B 9.0 33.6. 2 J �I �,3 3 /� % c. _±j 5 L 6 7 8 9 10 11 12 y m_ Arsenic 4 ObQ , ppp 5 . dt6 Cadmium .0007 r OOZ ► bCk� Copper a 0 3 ,• 0 ... • 1 46 hromi l�J� ;33 , ; 3,3 . !1 Fo b Lead Mercury aZ- ]AR COW?- Molyb- denum Nickel Selenium Q ., n y zing Total hors- - 4 3 , 4 -1 . "I certify, under penalty of law, that this document was prepared under my direction or supervision .in -accordance with a system4esigned° to assure sm"L talified °personnel- properly gathered•°and evaluated1l1q.. illfloi�atioa submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment -for knowing violations". C!% ignature of Land Applier -1 Date DENR FORM MFLSF (12/2006) w ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: CrAveyti Seril ke, S Total Dry Tons Applied (Annual): .4-1 Permit #: ,3 7 Cation Exchange Capacity (non 503 only): N A Operator: J6 hm W Dan hn ry, Owner: 'r W 7l1 r,, k6km Predominant Soil Series: I.e_e y± Acres Used: _I! , Z Acres Permitted: %, , � Site #: Field #: Residual Analvsis Data (Heavy Metals and Total Phosphorus use mgft, % Solids use Raw Percent #): MEN'@o o n oa•.•D. Total0 Phos- Phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): M _ Total P• I ■.• "I certify, under penalty of -law, that this document was prepared under my direction or supervision in accordance with a -system designed to assure that -qualified 1 personnel properly gathered and -evaluated. the -information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier Date DENR FORM MFLSF (12/2006) 6_1 _ V, ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Crtry n-9-%r'i/icec-• Land Owner: Operator: John (Aifir -i . Crop 1 Name: tIfer PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: (/j jo � .j 3 � -7 Field #: 3 % Acres Utilized: Annual Dry Tons Applied: �� Site #: r Acres Permitted: Predominant Soil Series:Cation Exchange Capacity (non 503): Crop 1 Max. PAN:. Crop 2 Name: w,j er- ale Crop 2 Max. PAN: 3.0 30 1U Q ° Q Volume applied (enter one) Solids% Liquid Cu. Yds Gallons i 0 /o Solids Volume Applied per PP p Acre (Dry Tons/AC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. Wei' Moist) Precip. Past 24 Hrs. inches Y c'2 0 * 0 o 7d w m p '`� ` * *, THIN mglkg z o o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 7 i-t 1 0 &C 140 ©, V ZetiZ 121711,317 0, 4T millei i Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS: As Cr Pb H Mo Ni Se Zn P Lime A lied Annual lbs/acre [ 1 .001 i . Mit . fJb . /. .CJD ,. Z: , 0d . :.:...::..... .... - Date lbs/ac Prior Years Cumulative i s/a c71w XCd yJ/6 e 2F , „0 068 �i........ Current Cumulative lbs/ac , �pZ .-5 r fil,s' 4.. �1. e �l , d....:.:.:::... Permitted C. P. L. R.**** A ?fib N t Permit PAN Limit lst/2nd Crop! "I certify, under penalty of law, that this document was prepared Mader my direction or supervision in accordance with a system designed to assure that qualified personnel properly' gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment fot knowing violations." A - *A lication Method: S - Surface IN - Injection INC - Incorporation Signature of Land Applier Pp f 9 9 _ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BY,ANK OR BOX WHEN NOT APPLICABLE. Facility Name: (y rmer A ,�Cryi< <5 WQ Permit #: VJ D6 Field #: �p " 1 Acres Utilized: Land Owner: p r Annual Dry Tons Applied: ` , 5 Site #: Acres Permitted: 6. Operator: , Jj0&n w dun &IQT Predominant Soil Series: �x.�� r� Cation Exchange Capacity (non 503): Crop 1 Name: i-Ue 41 m ;� Crop 1 Max. PAN: 60 Crop 2 Name: LC r m lg M _,7 Crop 2 Max. PAN: 1 o N A Volume applied ' (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#,Past Fert., Animal Waste, etc) Cond.itPrecip. (Dry' Moist) 24 His. inches �. oWet� c 0 m * N * w TKN mg/kg mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 I q0 &K /. 2l G 0.4 1015 a's-11 L,D 0,wo rge erm 3 0.d -3 NC007Vf 3- mop 0 � . � n. , Si8� 11.7/ r. 5 3, r � ,�xr . 4 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: As Cd Cu Cr Pb H Mo Ni Se Zn P , Sip, Lime A lied Annual lbs/acre 0011Z, ; r. ".0602".0027 . t33 d E. W& oOI46 . 001Z,d.' >; Date lbs/ac Prior Years Cumulative lbs/.ac , 0 60`" 17 , p e ^ 03 Current Cumulative lbs/ c .00 OAST , dpdo,^ ,;00 , lyd,IZ ' 7� Permitted C. P. L. R.**** 3 3 133 "A 1..267 1 5 NA Permit PAN Limit lst/2nd Crop . i� "I certify, under penalty% of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including �he,possibility of fines and imprisonment for "owing violations." Signature df. Land Applier 'al'-e-r-e Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ""C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: crave ,Surf u.5- WQ Permit #: kip a53'7( —7 Field #: �— j Acres Utilized: ¢, Land Owner: i n�r Annual Dry Tons Applied:' ^ �, $ Site #: Acres Permitted: Operator: J A W PVAfAft, Predominant Soil Series: te6V7 Cation Exchange Capacity (non 503): /M Crop 1 Name: e,rryl adex Crop 1 Max. PAN: 13 Z Crop 2 Name: ,,j n4,ar rije Crop 2 Max. PAN: 57b °enter ° -Sr c� o O Volume applied one Solids/ ( ) Liquid ' Cu. Yds Gallons o /o Solids Volume A lied er PP p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Pert,, Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches Y l;,° o a o w _. , N * � 0 -� * * w TKN mglkg Z w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Cro/p�2 Crop I Crop 2 i 6 C , 19,073 .3 A1e,607Vff3Jmo1W 65I o V- 7/ � . L 612.0 i oat> , 3. NC OC7 83 �' r 4 5 ,5 6546 W, 7/ s 85 9� Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTS- :: As Cd Cu Cr Pb H Mo Ni Se Zn P , Lime Applied Annual bs/acre Q O j. _ `:. a 00/ / p Z ; . 36 Gbo. , � , ow 34 , /' . R _. P 13,E . w . Q ; ' t 66g, . Ql.? Z4 . �060 26 IS . �aZ7 .006 ,. . AIA 4 i2G 0677.0. 374 . ! .. 69Z a � ..5 2 9 :•:•:::: ::::::::: :::::::::::::::::: ...................... Date lbs/ac Prior Years Cumulative lbs/ac Current. Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop P ' "I certify, under pe4alty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier - «-e Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C' n P r S t'v( Q Permit #: W w no37( 3 Field #: �j— 4 Acres Utilized: 6,2 Land Owner: Annual Dry Tons Applied/ Site #: 3 Acres Permitted: , Z Operator: Predominant Soil Series: L Oh Cation Exchange Capacity (non 503): NA Crop 1 Name: YYI; N& Crop 1 Max. PAN: la 3 Crop 2 Name: VZ�S'" Crop 2 Max. PAN: S0 ° Volume applied (enter one) Shcids/ % Volume Applied PP Residual Sources Soil Cond. Precip. Past 24 c w Z i* Nitrate PAN Applied Name of Crop Type a� a ° Liquid Solids per P Acre (NPDES #, WQ#, Fert., Animal (Dry, Hrs. 5 � .» � `� �' �" � - TKN o vo ° ° and (lbs/acre) Receiving Residual Ca Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, inches o w a * ° , * ° w o ° �• Nitrite Application Moist) o 0 mgtkg mg/kg mglkg Crop 1 Crop 2 Crop 1 I Crop 2 1 n lVC_d07Y - r i C / D 0, 15/8® �!•'7/ 5; gS ,1-1,3 Ih:/pf Residuals Applications totals on FORM FSF supp ( attach FORM FSF suZZn91P this form): TOTALs: , As Cd Cu Cr Pb H Mo Ni Se 3• �f3 Lime Alied Annualabs/acre ve ® lfi S ;¢a?� a�a2 % .D�ld11DP . l�Ob va�'I .:.fedDate lbs/ac Prior Years Cumulatii+elbs/ac ®Q 35" ; ,Q��f3 ,DOOaa ,-xV,3g W&501 .66a .dPWA -A >: PermittedC. P. L. R. *** 313 4 113392(:�-7 1 !S . N 3-Z4 9 4a Permit PAN Limit lst/2nd Crop S0 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified, personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) v Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, N& nteo, NC 27954 s 252.473MM Lab/Fax 255-A Wilmington I•Iighway, Jacksonville, NC 28540 • 910.347-%43 Lab/Pax info@envirotmicn taichemists.coni Town of Maysville Date of Report, Nov 21, 2018 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Schumata Brown Report#: 2018-17388 Project ID: Sludge Lab ID Sample 1D: Collect DatelTime Matrix Sampled by 18-43923 Site: sludge 10/23/2018 10:40 AM Water Robert A. Boomer Test Method Results Date Analyzed Total Solids N SM 2540 s 1.83 % 10/25/2018 Ammonia nitrogen SM 4500 NH3 C 703 mg/L 11/05/2018 Chlordane SW 848 Method 8081 W3510 <0.02 mg/L 10/30/2018 Endrin sw W Method 8081813510 <0.0005 mg/L 10/30/2018 Heptachlor SW 845 Method 5081SM10 <0.0005 mg/L 10/30/2018 Heptachlor epoxide SW 848 Method W81EV3510 <0.0005 mg/L 10/30/2018 Undane SW 848 Method 8081et3510 <0.0005 mg/L 10/30/2018 Methoxychlor SW 848 Method ao818rs510 <0.0005 mg/L 10/30/2018 Toxaphene SW 848 M81 hod 80811W510 <0.05 mg/L 10/30/2018 1,4-Dichiorobenzene (TCLP) SW 848 method 8270/3510 <0.050 mg/L 10/30/2018 2,4,5-Tdchiorophenol (TCLP) SW 84e method 8270/3510 <0.050 mg/L 10/3012018 2,4,6-Trichlorophenol (TCLP) SW 84e method 827=510 <0.050 mg/L 10/30/2018 2,4-01nitrotoluene (TCLP) SW 848 method 827OM510 <0.050 mg/L 10/30/2018 Cresol (TCLP) SW 848 method 8270M510 <0.050 mg/L 10/30/2018 Hexachloro-1, 3-butadiene (TCLP) SW 848 method 8270/3510 <0.050 mg/L 10/30/2018 Hexachlorobenzene(TCLP) sWU8method8270rd510 <0.050 mg/L 10/30/2018 Hexachloroethane (TCLP) SW B48 method 8270/3510 <0,050 mg/L 10/30/2018 m-Cresol (TCLP) SW 84e method 8270010 <0.050 mg/L 10/30/2018 Nitrobenzene (TCLP) SW 848 method 827of3510 <0.050 mg/L 10/30/2018 o-Cresol (TCLP) SW 848 method awo/3510 <0.050 mg/L 10/30/2018 p-Cresol (TCLP) SW 848 method 827t113510 <0.050 mg/L 10/3012018 Pentachlorophenol (TCLP) SW 848 method 827013510 <0.250 mg/L 10/30/2018 Pyridine (TCLP) SW 848 method 8270/3510 <0.050 mg/L 10/30/2018 2,4,5-TP SW846 Method 8151A <0.003 mg/L 10/31/2018 2,4-C SW848 Method 8151A <0.003 mg/L 10/31/2018 1,1-Dichloroethylene SW048Method 82MSM <0.01 mg/L 11/8/2018 Report S:: 2018-17388 Page 1 of 8 v Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 0 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702I,ab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax uifo@environmentalchemistscom Town of Maysville Date of Report: Nov 21, 2018 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Schumata Brown Report #: 2018-17388 Project ID: Sludge 1,2-Dichloroethane SW846Method 82B01 M < 0.01 mg/L 11/8/2018 Benzene SW848 Method82SOM30 < 0.01 mg/L 11/8/2018 Carbon Tetrachloride SW848 Method 6260030 < 0.01 mg/L 11/812018 Chlorobenzene SW846 Method 8260roM < 0.01 mg/L 11/8/2018 Chloroform SW848Method 8280 O30 <0.01mg/L 11/8/2018 Methyl ethyl ketone SW846 Method 828018030 < 0.05 mg/L 11/8/2018 Tetrachloroethylene SW846 Method BZsW= < 0.01 mg/L 11/8/2018 Trichloroethylene swe4eMedwde29GM= <0.01 mg/L 11/8/2018 Vinyl Chloride SW848 Method 8MOM030 < 0.01 mg/L 11/8/2018 RCI Cyanide EPA 336.4 <0.05 mg/L 11/07/2018 Reporting limit elevated du to matrix Interference. Sulfide SM 4M S D 0.82 mg/L 11/07/2018 Analyzed outside of holding time. Ignitability SW 848 method 1010 >21511F 10/30/2018 Sludge Residuals Aluminum' EPA 200.7 5090mg/L 10/30/2018 Arsenic EPA 200.7 49.1 mg/L 10/31/2018 Cadmium EPA 200.7 <29.9 mg/L 10/30/2018 Calcium EPA 200.7 32200 mg/L 11/01/2018 Chromium EPA 200.7 <29.9 mg/L 10/30/2018 Copper EPA 200.7 639 mg/L 10/3012018 Lead EPA 200.7 <29.9 mg/L 10/30/2018 Magnesium EPA 200.7 2600 mg/L 11/01/2018 Molybdenum EPA 200.7 <29.9 mg/L 11/02/2018 Nickel EPA 200.7 <29.9 mg/L 10/30/2018 Potassium EPA 200.7 3900 mg/L 11/01/2018 Selenium EPA 200.7 <29.9 mg/L 10/30/2018 Sodium EPA 200.7 3190 mg/L 11/01/2018 Zino EPA 200.7 3480 mg/L 10/30/2018 Report k 2018A7388 Page 2 013 Town of Maysville Post Office Box 265 Maysville NC 28655 Attention: Schumata Brown Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 91039Z O223 Lab • 910392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.3473843 Lab/Fax i n fo@onvironmentalchemi smcom Date of Report: Nov 21, 2018 Customer PO #: Customer ID: 17020023 Report #: 2018-17388 Project ID: Sludge Nitrate+Nitrite-Nitrogen EPA353.2 71.0mg/L 11/06/2018 pH SM 4500 H 8 6.98 units 10/31/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 Ora a 55500 mg/L 11/05=18 Total Phosphorus SM 46W P F 266 mg/L 11/07/2018 Mercury Swe4s 74718 <0.984 mg/L 11/04/2018 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 11/0412018 Barium EPA 200.7 <1.0 mg/L 11/05/2018 Cadmium EPA200.7 <1.0 mg/L 11/0412018 Chromium EPA 200.7 <1.0 mg/L 11/04/2018 Lead EPA 200.7 <1.0 mg/L 11/04/2018 Selenium EPA 200.7 <1.0 mg/L 11/05/2018 Silver EPA 200.7 <1.0 mg/L 11/05/2018 Mercury EPA 245.1 <0.0002 mg/L 11 /04/2018 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: .. . Report#% 2018-17386 TY_ � Page 3 of 3 ROOD Analytical & Consuiting Chemists Client: Town of Maysville WWTP ADDRESS: •64 'B6 a( 9L16 g' /vEAI S fl.LL#- Al -C, .1 Sample identifioation ENVIRONMENTAL CHEMISTS, INC ��g;" 'F,�9;��05 NCDENR: DWO CERTIFICATION # 94 NCDHHS: DI.S CERTIFICATION # 37720 lnfb@environmentatchemiste.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME: Annual Sludge REPORT_ NO: - CONTACT NAME: PO N0, REPORT TO: PHONIIFAX: COPY TO: Date I Time �C NINE NINON NINE 1. 2. Temperature when Received: cepted: Delivered By:-_ - .-- _ _ _ � _ Received Comments: ---.-.-- A 3,11, SL ISfudge, 2thei ANALYSIS RE$uEs-rEU 0- 23- (V TURNAROUND: -7"0, BOX 7i,85, 114 OAKivON!-. GREENVILLE, N.C. 27835-7085 TOWN OF BRIDGETON HYDRO SERVICES & CONSULTING MR. KEVIN MULLINEAUX P.O. BOX 317 HAVELOCK ,NC 28532 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH (not to be used for reporting) 7.0 01/25/18 JTH 4500HB-11 Aluminum, (dry wt. basis), mg/kg 3490 02/20/18 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 02/21/18 MTM 311313-04 Calcium (dry wt. basis), mg/kg 35446 02/20/18 LFJ EPA200.7 Cadmium (dry wt, basis), mg/kg 1.1 02/20/18 MTM 3113E-04 ::opper (dry wt. basis), .mg/kg 392 02/20/18 LFJ EPA200.7 Chromium, T.(dry wt. basis),mglkg 17 02/20/18 LFJ EPA200.7 Lead (dry weight basis), mg/kg 22 02/19/18 MTM 3113E-04 Magnesium (dry wt. basis), mg/kg 3717 02/20/18 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.12 02/12/18 LFJ EPA7471B Nickel (dry wt. basis), mg/kg 16 02/20/18 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 7694 02/20/18 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 02/22/18 MTM 3113B-04 Sodium (dry wt. basis), mg/kg 21480 02/20/18 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 1854 02/20/18 LFJ EPA200.7 Sodium Adsorption Ratio (calc) 0.9 Total Solids, % 0.49 01/25/18 MAR 2540G11 TKN (dry wt.), mg/kg c 65180 02/20/18 MF 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 91.71 02/20/18 CML 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 18180 02/20/18 DTL 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 5.85 02/21/18 CLO 353.2 R2-93 Molybdenum (dry wt. basis), mg/kg 6 02/20/18 LFJ EPA200.7 Drinking Water In, 37715 West awater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 440 A DATE COLLECTED: 01/25/18 DATE REPORTED : 02/2.8/18 REVIEWED BY: � SGS �1 Orlando, FL The results set: forth herein are provided by SOS North America Inc. e?-H(liYlr4;Ojly Z. Autemated Report Technical Report for Environment 1, Inc Town of Bridgeton Hydro Services & Consulting; Havelock, NC 440C SGS Job Number: FA56037 Sampling Date: 07/17/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentlinc.com ATTN: Deedee Woolard Total number of pages in report: 14 m Test results contained within this data package meet the requirements Caitlin Brlce, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC.(86038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except In its entirety, without the written approval of SGS. Test results relate only to samples analyzed. I SGS North America Inc. - 4405 Vineland Road - Suite C-15 - Orlando, FL 32811 - tel: 407-425.6700 - fax: 407-425-0707 1 of 74 SOS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about UnauthoPized:rnodification of this report is strictly prohibited. how we can serve you better at: SG9, Review standard terms at: http://www.sgs.com/eii/terms-acid-conditions EHS.US.CustomerCam@sgs.com FAse037 Seciions Table of Contents Section1: Sample Summary................................................................................................... I Section2.: Summary of Hits.................................................................................................... 4 Section 3: Sample Results........................................................................................................ 5 3.1: FA56037-1: SLUDGE SAMPLE.................................................................................. 6 Section4: Misc. Forms............................................................................................................ 12 4.1: Chain of Custody........................................................................................................... 13 2of14 PASO437 _I N SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA56037 Town of Bridgeton Hydro Services & Consulting; Havelock, NC Project. No: 44OC Sample Collected Matrix Client ! Number Date Time By Received Code Type Sample ID FA56037-1 07/17/18 10:55 KM 07/21/18 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. 3of14 FAB0037 Summary of Hits Job Number: FA56037 Amount: Environment 1, Inc Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Collected: 07/17/18 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA56037-1 SLUDGE SAMPLE Corrosivity as pH 7.4 Ignitability (Flashpoint) a > 200 (a) Not ignitable. su SW846 CHAF7 Deg. F SW846 1010 Page 1 of 1 ��� 4 of 14 FA68037 -SGtt- Orlando, FL Sample Results Report of Analysis Section 3 _SG5of14 S, . PASS037 t SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE :Lab Sample ID: FA56037-1 Date Sampled: 07/17/18 Matrix: SO - Sludge Date Received; 07/21/18 Method: SW846 8260B SW846 1311 Percent Solids: 0.3 Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 M0104294.1) 10 07/26/18 17:21 TD 07/24/18 11:00 OP71005 VM4510 Run #2 YPurge Volume #1 5.0 MI. F#2 VOA TCLP List TCLP Leachate method SW8461311 CAS No. Compound Result HW# MCL RL MDL Units Q 71-43-2 Benzene ND D018 0.50 0.010 0.0031 mg/1 78-93-3 2-Butanone (MEK) ND D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ND D021 100 0.010 0.0020 mg/1 67-66-3 Chloroform ND D022 6.0 0,010 0.0030 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 0.0026 mg/1 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 0.0031 mg/1 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 0.0032 mg/1 127-18-4 Tetrachloroethylene a ND D039 0.70 0.010 0,0022 mg/I 79-01-6 Trichloroethylene ND D040 0.50 0.010 0.0035 mg/1 75-01-4 Vinyl Chloride ND D043 0.20 0.010 0.0041 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 83-118% 17060-07-0 1, 2-Dichloroethane-D4 103% 79-125% 2037-26-5 Toluene-D8 100% 85-112% 460-00-4 4-Bromofluorobenzene 100% 83-118% (a) Associated ICV outside control limits high, however sample ND. ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a, compound _..SG9 6of14 FAB0037 SGS North America Inc. Report -of Analysis Pagea-of l Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA56037-1 Date Sampled: 07/17/18 Matrix: SO - Sludge Date Received: 07/21/18 +Method: SW846 8270D SW846 3510C Percent Solids: 0.3 Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X061593.1) 1 07/25/18 20:12 MV 07/24/18 10:45 OP71031 SX2560 Run #2 Initial Volume Final Volume Run #1 100 ml 1.0 ml Run #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND D023 200 0.050 0.0056 mg/1 3&4-Methylphenol ND D024 200 0.050 0.0098 mg/1 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/l 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/l 88-06-2 2,4,6-Trichlorophenol ND D042 2.0 0,050 0.0075 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.050 0.0050 mgA 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.0081 mg/I 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/1 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/I 67-72-1 Hexachloroethane ND D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/I 110-86-1 Pyridine ND D038 5.0 0.10 0.020 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 18% 14-67% 4165-62-2 Phenol-d5 10% 10-50% 118-79-6 2,4,6-Tribromophenol 60% 33-118% 4165-60-0 Nitrobenzene-d5 59% 42-108% 321-60-8 2-Fluorobiphenyl 57% 40-106% 1718-51-0 Terphenyl-dl4 70% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of14 _ aw- FASS037 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE iLab Sample ID: FA56037-1 Date Sampled: 07/17/18 !Matrix: SO - Sludge Date Received: 07/21/18 'Method: SW846 8151A SW846 3510C Percent Solids: 0.3 ;Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page-1 of 1 "7 1 Run #1 Run #2 File ID DF CC058945.D 1 Analyzed 07/26/18 13:12 By NJ Prep Date 07/24/18 14:00 Prep Batch Analytical Batch OP71039 GCC1324 Initial Volume Final Volume [Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2,4-D ND D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 84% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/i/11) B = Indicates analyte found in associated method blank E — Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SG Sof14 FA66037 SGS North America Inc. Report of Analysis Page I Of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA56037-1 Date Sampled: 07/17/18 -Matrix: SO - Sludge Date Received: 07/21/18 'Method: SW846 8081B SW846 3510C Percent Solids: 0.3 Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 TT388749.D 1 07/24/18 17:45 KL 07/24/18 10:00 OP71032 GTT2161 Run #2 Initial Volume Final Volume Run #1 100 ml 5.0 ml Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) ND D013 0.40 0.00010 0.000022 mg/I 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/l 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychior ND D014 10 0.00020 0.000050 mg/l 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 92% 42-127% 2051-24-3 Decachlorobiphenyl 94% 27-127% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _SG9of14 S.- FA66037 0 SGS North America Inc. Report of Analysis Iieat Sample ID: SLUDGE SAMPLE ab Sample ID: FA56037-1 Date Sampled: 07/17/18 Satrix. SO - Sludge Date Received: 07/21/18 Percent Solids: 0.3 rojeot: Town of Bridgeton Hydro Services & Consulting, Havelock, NC Pagel of 1 Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/l 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Barium < 2.0 D005 100 2.0 mg/1 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/l 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/I 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Lead < 0.050 D008 5.0 0.050 mg/l 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/l 1 07/26/18 07/26/18 Ic SW846 7470A 1 SW846 7470A 4 Selenium < 0.10 D010 1.0 0.10 mg/l 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 Silver < 0.10 D011 5.0 0.10 mg/l 1 07/24/18 07/26/18 LM SW846 6010D 2 SW846 3010A 3 (1) Instrument QC Batch: MA15072 (2) Instrument QC Batch: NIA15074 (3) Prep QC Batch: MP34065 (4) Prep QC Batch: MP34078 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) _..SG 70of14 FAbs037 e� SGS North America Inc. Report of Analysis Page•l.of 1 Client Sample ID: SLUDGE SAMPLE Date Sampled: O7/17/18 Lab Sample ID: FA56037-1 Matrix: SO -Sludge Data Received: 07/21/18 Percemt Solids: 0.3 project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC General Chemistry Analyte Result RL Units DF Analyzed By Method Corrosivity as pH 7.4 su 1 07/25/18 13:50 BW SW846 CHAP7 Cyanide Reactivity < 480 480 mg/kg 1 08/02/18 14:54 JK SW846 CHAP? Ignitability (Flashpoint) a > 200 Deg. F 1 07/26/18 11:24 BW SW8461010 Solids, Percent 0.3 % 1 07/24/18 11:39 jC SM19 2540G Sulfide Reactivity b < 16000 16000 mg/kg 1 07/31/18 13:16 BW SW846 CHAP? (a) Not ignitable. (b) Associated BS recovery outside control limits. RL = Reporting Limit 11 of 14 ._SU0 FASS037 SG5 Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 I 0 12 of.14 _ PA6603Z Rpvh+mment 1, Inc. CHAIN OF CUMDY PO.Box.7065,114Oakmont Dr. Orcenvllle, IVG 27558 entilrovotrn ulnexam DISWPBCT1oN Phone (252) 756-M • Fox (252) 756-0633 ❑ CHIAttINB CLIRrit 440C Week:I i❑ W TOWN OF.ggIDGMN i� NONE p pp G G G G WjoR08SRVIMS & CONSULTING ❑ MR. ICBM KMLUMUX P.O. Box 317 A A A A A A. A SAVSLOCIC NC 26532 a (252) 723-0101 k rc .9phplEtpC4ii0F, IM TM b Fvf -V ------ - PLEASE READ InstnmcUons forcompletina this form on the reverse side. Fnp 1 sa Page L of I CfiLOfiINEF�UIRAl1�AiCOl1ECIIDN PHA ODNTAUIEATYPE,Pdi CHEAYCIU.PfiE5E51VAilON A -NONE 0-NAM i S-FWD, E-HCL i O-H,W, T-ZING ACETATFJNAOH o-rmn+loeut�E --' q,A53�1CATI0N ❑ WASTEWATER(N M ❑ pRSW6N0YflDER ❑ OWUMW ❑ SOUDWASTESECM CHAIN OF CUSTODY (SEAL) MAINTAINED OURINS 8 ENUOELIVERY N BAIELESOOLLECTEDR. d WA ESRMWWIASATJ_I---C 1. Ex e r al lace a C r posas sem or e v for drab a ale In the blocks above for each parameler requested. tl 337512 FA56037: Chain of Custody Page I of 2 13of14 FAS6037 'I SGS Sample Receipt Summary Job Number; FASS037 Client, ENVA Project: TOWN OF BRIDGETON Date I Time Received; 7/21/2018 9:15:00 AM Delivery Method: FED EX A)rbilt We,. 1002829223D10DD3281100439402212380 Therm ID: I 1; Therm CF: 0.1; # of coolers: 1 Cooler Temps (Raw Measured) IC: Cooler 1: (3.0); Cooler Temps (Corrected) °C: Coder 1: (4.0); Cooler Information Y or N Sample Information Y or N NIA 1. Custody Seals Present ® ❑ 1. Semple labels present on bottles ® ❑ 2. Custody Seals Intact ® ❑ 2. Samples preserved properly ® ❑ 3. Temp criteria achieved ® ❑ 3. Sufficient volumelconlainers recvd for analysis: ® ❑ 4. Cooler lamp verification IB &n 4. Condition of sample Intact 5. Cooler media iu rB o1 5. Sample recvd within HT ® ❑ 6, Dales/TlmesllDs on COC match Sample Label ® ❑ Trio Blank information Y or N N/A 7. VOCs have headspace ❑ ❑ 1. Tdp Blank present / cooler ❑ ❑ ® 8. Bottles received for unspecified tests ❑ 2. Tdp Blank fisted on CDC ❑ ❑ to 9. Composllinp Instructions dear ❑ ❑ 10. Voa Sall 10trJJers received post 48hrs? ❑ ❑ W or S NIA 11. % Solids Jar received? ❑ ❑ 3. Type Of TS Received ❑ ❑ ® 12. Residual Chlorine Present? Cl ❑ Misc. information Number of Encores: 2&Gram 5•Grem Test Strip lot #s: pH 43 230315 Residual Chlorine Test Skip Lot#; Comments Number of 5035 Field tots: PH 10.12 _ __ 219813A "001 Technician: SHAYlJ1P Date: 7121/2018 9:15:00 AM 11w. Dal, =07 . Number of Lob Filtered Metals: _ Other. (Specify) , _ Reviewer. Date: FA56037: Chain of Custody Page 2 of 2 14 of 14 FA56037 .J Environment 1, Inc. P.O. Box 7085,114 Oakmont Dr. Omonville. NC 2785E environmentliac.com DTSDVFB=0N Phone (252) 756.6200 - Fax (252) 7560633 CHLOWNE CLIENT. aae C Week:1 r-y vv TOWN OF MaDMON NONE HYDRO MRVICSB dt GONOMTiNG m1CMN pmpLLflVB uX P.O. BOX 311 $A,VXWCK NC 2= M 723-0i0I 4,, F 17117 1 la46 s I4 ' CHAYN OF CUSTODY RECORD 4mmmmmmm PLEASE RF11D insbutdlom for comosti no this forth on the m=w: a side. FORS: as Page 1 of I OURNEWiVd1 DATaxLEanON pHO MA CONfmPERTYmm A•NONE D•NAOH B-HN% a-MM 0-Hp, F-MCAOETATE44ADH G-NAVIOSULI'm aAGSFCOM DRNIONBWA ER DWOM SOUDNWBTESECiION CHAIN OF CUMDY (SEAL) MAIMAINED DURING Shi�EhTMEI.IVERY N SAiI SCM1.80 EOW. (Pleeeel�9 .p MLES RECEIuEI)wtaBAT-0 0OMMENM Sampler must place a V for compositetxwe �b or a V for p 3 7 emb sample In the Wode afor each r requested . CRAVEN AG SERVICES INC. Alkaline Stabilization Of Solids Analysis Bench Sheet Facility Name: �iu� %y — - ����_ P.O. # Batch Size (gallons) : D lbs. or Gallons Used: 1. 7a G Material used for Stabilization: A1v,-h4 L,, ( DATE Initial ph H jTemp C JCorr Fa + ,Corr. pH ITime jpH 16 7 *.(4 3 ej 17.01 PJLa,,f-41 1 2 Hour pH 24 Hour pH Temp C Corr Fa + Corr pH Time pH Temp C Carr Fa + Intial JJ-7 -•34 11-31 f!'Ap is yea-0 -•.3G tCorrpHTime RAW,3 !-2•Y -39 FAA 3 43 13. t r 31 ?il4 vT IA►r.; O .... .r. d! OIO QdOp ooN O CI O 'OoC o O N OO O�� Oo as� U pO pp {Y c! Off! iN 9 � W as 9 .M N e o 0 0 g Nv cV e-- aTE Iftuc1C - m 1DYE,(Alq�4 3 26) lat�ic5►as� -�_ - -- — - GAL'LD/iS //� {.f(' PUI.oED 7tRiE =ANTU � f ®/d - - — ------------- ---------------------- C CRAVEN AG SERVICES INC. Alkaline Stabilization Of Solids Analysis Bench Sheet Facility Marine : i6c (we-e-i &rA%dea,. z/ x/ P.O. # - - -- — Batch Size ( gallons) : J-/De4 lbs. or Gallons Used: !!N Material used for StabilizationAr�Iar —�- Initial ph 2 Hour pH 24 Hour pH DATE pH Temp C Corr FaT+Corr- pH Time pH Temp C Corr Fa + Corr pH Time pH Temp C Corr Fa + Corr pH Time Intial OPERATM. l � 0 CRAVEN AG SERVICES INC. ` Alkaline StabilizationOf • e . Lbs. or Gallons Used: I Material for Stabilization: 1�Initial phI ®wmMR � m'rw�-������� =gym --__- 1 ." W. 9 N N N � � W:t-1 ��VV o o TT c s5 a pp o v d s d N Cf IrT Q CQ N T p� N m N C�11 N [ram CD ti LL7 M N r. O DAILY GkMT =.LoG. F Aar W wa1� P7 St Q W W Q V7 lY� It if a lost io it _ LV ^y ll' _ CRAVEN AG SERVICES, INC. 2115 Hwy 55 W -New Bern NC 28562 _ (252) 633-5334 DAILY OPERATING LOG Delivery Order # TRUCK # TIME Event # Toda Date "�4 - Weather SITE # GALLONS DRIVER SUPERVISOR COMMENTS - � l D G - 3 aoo I j I i r comments BD BILLY DUNHAM �MD—MAC DUNHAM JD JOHN DUNHAM MH—MIKE HARDISON ----DAVID EMMON fYE SW---STEVE WETHERINGTON PM----PABLO MARTINEZ _ CS---CHARLES STOCKS _ __t✓� �T- CRAVED AG SERVICES INC. 46 Alkaline Stabilization Of Solids Analysis Bench Sheet Facility Name : Batch Size ( gallons) : J-D .0 Lbs, or Gallons Used: 04 (r Material used for Stabilization: /..e Initial ph 2 Hour pH 24 Hour pH DATE pH I Temp C Corr Fa + Corr. pH Time pH Temp C Corr Fa + Corr pH Time pH ITe—Mip—ClICorr Fa + ICorr pH Time Intial ?9-r8 .. ' 3 O .3s 3 ! .?Y �, .06 / !t Sr 34 -Lt, ! .qjL (47+ f-13 -rg .ar .25'.6 V-rl © ( _A3 1.1eli .d ! i.T/ •3v i G r ,qo D:lY 3 Y .71 A,16 401 1 3 3o 11,31 , 3 . / ! /.TIG 2 .0lr I I 07 36 12 , Y � et7 r d ..r tr, .7y gd.1. ,o .91 /311- 33 1f.2 1 a ! ri31 3 r jr.3v T &B O Q d too a O OLa CD a a t$ O a d d a C;o Fo,' d o pq� cc d dF e H +F- M co C4 co n N Q' CV N Cv N r CM pp W r OO a- iti r .(pr. �- r e- r e- r' CI -r- s - iWLYgPERATM.tOG• - r- hl� +i IMI o7l i I I 17M d r a I a in a i kfoltra 4 r c � aD 4,- � 40 V I co N +r- m r t^ � r r r� Y �— "Ly OPERATDX,- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: 11 R�V� V lG� ,, WQ Permit Number: JAI _ 6200379 S -7 WWTP Name: a sU, ( NPDES Number: Monitoring Period: From To 2 3l l g Pathogen Reduction (15A NCAC 02 .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Allc Treatment) El Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo 'lie ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization A Air Drying ❑ CompostinE ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number ot Frequency Sample Analytical Parameter in Sludge MinimumGeo. Mean axim Units Excee- of Analysis Type Tech- nicue 2 x 10 to the MPN 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry weir;ht) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform] weight) Vprtnr At+ractinn Reduction (1 _SA NCAC 02T .1107)- Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) IM No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction rea uirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." o6 Vi' �vn JDrr' Dun Aam Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ei�ture of Preparer* Date i tore of Land Applier (if applicable) Date �l *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) or Facility Name: Craven oervices WQ Permit Number:LkIQ 003 76 3 WWTP Name: Towr: ey" rid NPDES Number:MG 60 74? 7 Monitoring Period: From I Z, to g To l 2 r Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ ❑........... Alt. C (Prior Testing) A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ElJ. Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ 1 Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying ❑ Composting ❑ JAerobic Digestion ❑ naero is Digestion ........ . .......... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Nurn r o Eence- Frequency of Analysis y Sample Type Analytical Tech - Minimum Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gam of total solids MPN CFU 1000 mpn per gam of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 gams total solid (dry weight) vector Ar[ractron xeuuction (15A NC:AC 02T .1107) -Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) N No vector attraction reduction alternatives were erformed ❑ l:r:K111+1UA110N STATL+NffiNT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." JO�n (Al. DvAam JOhrt W . DunkoLwl Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ti ignature of Preparer* Date , ?ignatZure of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) r Waypointw ANALYTICAL Client: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem NC 28562 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 "Every acre... Every year® www.waypointanalytical.com Grower: Craven Ag Services, Inc. Report No: Cust No: Date Printed: Date Received; PO: Page Lab Number: 33733 Field Id: Sample Id : R3-1 SOIL ANALYSIS 18-311-0804 24170 11/12/2018 11 /07/2018 1 of 6 Tdst Method Results T SOIL TER; RATIOS"' -• U utarBd Cagen .: Ex6hainga_Capgaty' LOW Madill um Soil pH 1:1 7.6 8.2 me 100g Buffer pH %Saturabon Phosphorus P) M3 412 ppm %sat meq K 1.3 0.1 Ca 92.9 7.6 Mg 4.5 OA H 0.0 0.0 Na 1.7 0.1 Potassium K M3 42 ppm Calcium (ca) M3 1523 ppm Magnesium M M3 44 ppm Sulfur S M3 13 apm Boron BI M3 0.4 pprn Copper Cu M3 2.9 ppm Iron Fe M3 199 pprn K/Mg,Ragq:- 0219� Gwm Ratio: Manganese (Mn) M3 8 ppm Zinc Zn M3 9.4 o m Sodium Na M3 32 ppm Soluble Salts Organic Matter LOI 1.4% ENR 72 Nitrate Nitrogen Crop: Rye SOIL FERTILITY GUIDELINES Yield Goal : 60 bu/acre Rec Units: LB/ACRE IhaY _„ LEME`-' (tans) N = 5. IC=p IB 0 0 86 0 89 18 13 0.5 0 4 0 Crop : Millet Pasture Yield Goal : 3 tons/acre Rec Units: LB/ACRE 0 0 90 0 80 18 10 1 0.5 0 1 4 0 Comments: Rye For small grains apply 20-40 lbs N/acre in the fall and the remainder as a top dressing before jointing. For high yields of small grains or for small grains on wet soils, a split application of spring N may be beneficial. When small grain is grazed, increase the N fertilization rate by 60 lbs N/Acre. Apply 1/2 in the fall and the rest in mid or late winter. • On small grains apply recommended P and K before or at planting. Millet Pasture • When millet or sorghum sudans are harvested for silage or hay apply 40 lbs N/Acre at seeding and 60 lbs. N/Acre after establishment. Then apply 60 lbs. N/Acre after each harvest except the last. • When millets or sorghum sudans are used for grazing apply 40 to 60 lbs N/Acre at seeding and 60 lbs N/Acre per month during the growing season. M3 - Mehlich 3 BPH - Lime Index LOI - Loss On Ignition 1:1 -Water pH Analysis prepared by. WaypointAnalytical Tennessee. Inc. Waypoint. ANALYTICAL j Client I Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbern NC 28562 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 "Every acre ... Every year, www.waypolntanalytical.com Grower: Report No: Craven Ag Services, Inc. Cust No: Date Printed: Date Received PO: Page SOIL ANALYSIS 18-311-0804 24170 11/12/2018 11 /07/2018 2 of 6 Lab Number: 33734 Field Id : Sample Id : R6-1 Test Method -.77777 Results I �y Mediu" , 1;�1a� ated.Ca� adarige Civil* Soil pH 1:1 6.9 9.2 megl100g Buffer pH %saturation Phosphorus P) M3 172 ppm %sat meq K 2.1 0.2 Ca 84.6 7.8 Mg 11.0 1.0H 1.1 0.1 Na 1.6 0.1 -, --_-.. -_� Potassium X M3 76 p m Calcium (ca) Magnesium (M ) M3 M3 1556 JPPM 121 ppm Sulfur S M3 12 ppm _ _ _- F Boron iB M3 0.4 pprn Copper Cu M3 1.8 ppm Iron Fe M3 157 porn K/Mg "co: 0'A9 CalMg.Ratio: 7.69 Man anese (Mn) M3 11 ppm Zinc (Znl M3 7.6 pprn Sodium tNa) M3 33 ppm or4anlcmatter I LOI i 3.4% ENR 112 1 Nitrate 1 I SOIL FERTILITY GUIDELINES Crop : Bermudagrass Pasture Yield Goal: 3 tonslacre Rec Units: LB/ACRE ;.' !�1`-.,' `LIIVIF- . {toe,). H , :. ..pa=,g6 ,, K,O tVEg•.. .. ; 0 0 135 0 106 0 10 0.5 0 1 4 0 Crop: Rye Yield Goal : 60 bu/acre Rec Units: LB/ACRE 0 0 86 0 74 1 0 14 1 0.5 0 1 4 0 Comments: Bermudagrass Pasture • For perennial warm season grass pasture other than hybrid bermuda, apply 75 to 130 Ibs N/Acre per season. If under intensive grazing system apply 125 to 175 Ibs N/Acre in 2 or 3 applications. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. For grass hay or pasture needing high rates split the P and K application. Apply 112 in the spring and 1/2 in late summer. Rye For small grains apply 20-40 Ibs N/acre in the fall and the remainder as a top dressing before jointing. For high yields of small grains or for small grains on wet soils, a split application of spring N may be beneficial. When small grain is grazed, increase the N fertilization rate by 60 Ibs N/Acre. Apply 1/2 in the fall and the rest in mid or late winter. • On small grains apply recommended P and K before or at planting. M3 - Mehlich 3 BPH - Lime Index LOI - Loss On Ignition 1:1 - Water pH Analysis prepared by: WaypointAnslytioal Tennessee, Inc. Waypoi t ANALYTICAL Client; Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem NC 28562 Lab Number: 33736 Test Metho Soil PH 1:1 Buffer pH Phosphorus P M3 Potassium K M3 Calcium Ca M3 Magnesium (Mg) M3 Sulfur 3 M3 Boron IS) M3 Iron F Man a Zinc i2 So�diur 31 clubl i 0 and Nitrate M3 M3 M3 M3 Results 7.4 139 Dom 1341 120 10 0.6 1.9 185 19 8.9 33 LOI 1 1.8% ENR 80 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 "Every acre ... Every year® www.waypointanalytical.com Field Id : Grower: Craven Ag Services, Inc. Report No: Cust No: Date Printed: Date Received P0: Page: Sample Id : R6-3 SOIL ANALYSIS 18-311-0804 24170 11/12/2018 11 /07/2018 3of6 8.0 meg1100g %sat meq K 2.3 0.2 ca 83.6 6.7 Mg 12.5 1.0 H 0.0 0.0 fiYl f Na 1.8 0.1 I CalMg Ratio- 6.77 EI SOIL FERTILITY GUIDELINES Crop : Bermudagrass Pasture Yield Goal: 3 tons/acre Rec Units: LB/ACRE - 0 0 135 0 109 0 11 1 0 0 1 3 0 Crop: Rye Yield Goal : 60 bu/acre Rec Units: LB/ACRE ` 0 0 86 0 77 0 15 1 0 0 1 3 0 Comments : Bermudagrass Pasture • For perennial warm season grass pasture other than hybrid bermuda, apply 75 to 130 Ibs N/Acre per season. If under intensive grazing system apply 125 to 175 Ibs N/Acre in 2 or 3 applications. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. Rye For small grains apply 20-40 Ibs N/acre in the fall and the remainder as a top dressing before jointing. For high yields of small grains or for small grains on wet soils, a split application of spring N may be beneficial. When small grain is grazed, increase the N fertilization rate 1by 60 Ibs N/Acre. Apply 1/2 in the fall and the rest in mid or late winter. • On small grains apply recommended P and K before or at planting. M3 - Mehlich 3 BPH - Lime Index LOI - Loss On Ignition 1:1 -Water pH Analysis prepared by. WaypointAnaly0cal Tennessee, Inc. Waypointw ANALYTICAL Client: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbern NC 28562 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 "Every acre ... Every year® www.waypointanalytical.com Grower: Craven Ag Services, Inc. Report No: Cust No: Date Printed: Date Received P0: Page: Lab Number: 33737 Field Id : Sample Id : R64 SOIL ANALYSIS_ 18-311-0804 24170 11/12/2018 11/07/2018 4of6 Tast Method Results . me Ito - .. - 6ciian9h't Pa�Y 6.0 meg11009 Soli pH 1:1 6.3 Buffer pH BPH 7.87 %Saturation Phosphorus (P) M3 430 ppm %sat meq K 2.6 0.2 Ca 66.4 4.0 Mg 18.5 1.1 H 10.0 0.6 Na 2.8 0.2 .' -':'' : •, '°' m` V" ,; Potassium K M3 60 Calcium Ca M3 797 m Magnesium (Mg) M3 133 ppm Sulfur S) M3 12 ppm Boron B] M3 0.3 ppm Copper Cu M3 12.6 ppm 9 Ratio; D.14• Iron Fe M3 169 pm Manganese (Mn M3 12 ppm "'' CVMg Rana::.3.58 Zinc n) M3 72.5 ppm Sodium Na M3 38 ppm Soluble Salts Organic Matter LOI 1.7% ENR 78 Nitrate Nitrogen Crop: Rye SOIL FERTILITY GUIDELINES Yield Goal: 60 bu/acre Rec Units: LB/ACRE 71 Mg p 0 0 86 0 82 0 14 1.0 0 4 0 Crop : Soybeans Yield Goal : 50 bu/acre Rec Units: LB/ACRE 11 0 0 0 0 106 1 0 14 1 1.0 0 1 5 0 Comments Rye For small grains apply 20-40 Ibs N/acre in the fall and the remainder as a top dressing before jointing. For high yields of small grains or for small grains on wet soils, a split application of spring N may be beneficial. When small grain is grazed, increase the N fertilization rate by 60 lbs N/Acre. Apply 1/2 in the fall and the rest in mid or late winter. • On small grains apply recommended P and K before or at planting. Soybeans • For soybeans on soils with a pH of 6.2 or less, apply limestone as recommended and plant seed treated with molybdenum. Apply 1-2 oz of sodium molybdate (0.4-0.8 oz of elemental molybdenum) per acre as a seed treatment. M3 - Mehlich 3 BPH - Lime Index LOI - Loss On Ignition 1:1 -Water pH Analysis prepared by: WaypointAnalydcal Tennessee, Inc. Report Number ' 18-311-0316 Account Number Waypoint 24170 ANALYTICAL Send To: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem, NC 28562 Project: Craven Ag Services Lab Number: 97053 Sample ID: R3-1 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Page: 1 of 6 Purchase Order: Report Date: 11/12/2018 Date Received: 11/07/2018 Date Sampled: Quantitation Analysis Result Limit Method Arsenic , mg/Kg 1.46 0.500 6010D Cadmium, mg/Kg <0.100 0.100 6010D Copper, mg/Kg 4.78 0.250 601 OD Lead, mg/Kg 6.10 0.300 6010D Nickel, mg/Kg 1.92 0.250 601 OD Selenium, mg/Kg <0.500 0.500 6010D Zinc, mg/Kg 17.9 0.500 6010D Method Reference: USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision Comments: Date and Time Test Started Analyst 11/0912018 23:00 KKM 11/09/2018 23:00 KKM 11/09/2018 23:00 KKM 11/09/2018 23:00 KKM 11/09/2018 23:00 KKM 11/09/2018 23:00 KKM 11/09/2018 23:00 KKM Jimmy R. Ferguson Report Number 18-311-0316 (D Account Number Waypoint 24170 ANALYTICAL Send To: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem, NC 28562 Project: Craven Ag Services Lab Number: 97054 Sample ID: R6-1 2790 Whitten Road, Memphis, TN 38233 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OF ANALYSIS Page: 2 of 6 Purchase Order: Report Date: 11/12/2018 Date Received: 11/07/2018 Date Sampled: Quantitation Analysis _ Result Limit Method Arsenic, mg/Kg 3.99 0.500 6010D Cadmium, mg/Kg <0.100 0.100 6010D Copper, mg/Kg _ 5.92 0,250 6010D Lead, mg/Kg 4.32 0.300 6010D Nickel, mg/Kg 2.38 0.250 6010D Selenium, mg/Kg <0.500 0.500 6010D Zinc, mg/Kg 20.3 0.500 6010D Method Reference: USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision Comments: Date and Time Test Started Analyst 11/09/2018 23:05 KKM 11/0912018 23:05 KKM 11/09/2018 23:05 KKM 11/09/2018 23:05 KKM 11/09/2018 23:05 KKM 11/09/2018 23:05 KKM 11/09/2018 23:05 KKM Jimmy R. Ferguson Report Number 1 Waypoint-(D Acccoucountt NNumber u 24170 ANALYTICAL Send To: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem, NC 28562 Project: Craven Ag Services Lab Number: 97055 Sample ID: R6-3 Analysis 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OF ANALYSIS Page: 3 of 6 Purchase Order: Report Date: 11/12/2018 Date Received: 11/07/2018 Date Sampled: Quantitation Result Limit Method Arsenic, mg/Kg 4.53 0.500 6010D Cadmium, mg/Kg <0.100 0.100 6010D Copper, mg/Kg 4.96 0.250 6010D Lead , mg/Kg 6.08 0.300 6010D Nickel, mg/Kg 2.37 0.250 6010D Selenium, mg/Kg <0.500 0.500 6010D Zinc, mg/Kg 17.9 0.500 6010D Method Reference: USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision Comments: Date and Time Test Started Analyst 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM 11/09/2018 23:11 KKM Jimmy R. Ferguson Report Number ' 1 Waypoint. Accouccou ntt Nu Number 24170 ANALYTICAL Send To: Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbem, NC 28562 Project: Craven Ag Services Lab Number: 97056 Sample ID: R6-4 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OF ANALYSIS Page: 4 of 6 Purchase Order: Report Date: 11/12/2018 Date Received: 11/07/2018 Date Sampled: Quantitation Analysis Result Limit Method Arsenic, mg/Kg 0.971 0.500 6010D Cadmium, mg/Kg <0.100 0.100 6010D Copper, mg/Kg 19.9 0.250 6010D Lead, mg/Kg 4.15 0.300 6010D Nickel, mg/Kg 1.64 0.250 601 OD Selenium, mg/Kg <0.500 0.500 6010D Zinc, mg/Kg 92.0 0.500 6010D Method Reference: USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision Comments: Date and Time Test Started Analyst 11 /0912018 23:16 KKM 11/0912018 23:16 KKM 11/09/2018 23:16 KKM 11 /0912018 23:16 KKM 11/09/2018 23:16 KKM 11 /09/2018 23:16 KKM 11/09/2018 23:16 KKM Jimmy R. Ferguson 1 It -.4sir �4 A EVA., 0 1- r1l MONOV/0%,", 7�3 Y AppI ication Area (acres) F e d Surface Subsurface \- 6-I 6.4 11.7 I 6-2 17.5 17.5 6-3 4.6 4.6 5- 0 8 6.2 y�, (jar'. ;y�:,t. ...'i• :� .... �M S •jn�• ..,� A�._ Buffers Property Line (SO-) Perennial Stream (100') Surface Water (100') Ditch (25') _ - House (200') House (400') Legend Propery Line - Surface Water Field ® Unused Area f Boundary Perennial Stream Well Ditch ® House Roach r M. x Soil Bore Parcel: 1-068-017 0 375 750 35.3159,-77.2671 1,500 Feet ` North CaroFne Statepiane, W a3 Jan. 2015 Craven k . Services, Inc. / Appr icat-on Area (acres) e d Surface Subsurface '1 � •� r h•� 17.5 17.5 --- 5-3 4.6 4.6 _ � • �:1F ;tip _ •g" r .A A® f L: i / 4, Buffers Property Line (50' Perennial Stream (1001) ` Surface Water (100') 15. Ditch (25') House (200') r House (400') t mom Legend -,. Surface Water Propery Line Field Boundary ® Unused Area Perennial Stream Well <<� Ditch ® House x Soil Bare Roach Parcel: 1-068-017 0 375 750 1,500 Feet .�. 35.3159, -77.2671 J North Carolina Stateplane, NAD83 Jan. 2015 Craven A . Serviced Inc. LC 4. soa � s� .. - a 40L /` ATTA� ,l\TT B - Approved Land Application Sites Craven Ag Services, Inc. Certification Date: April 17, 2015 Permit Number: WQ0037637 Version:1.0 Field Owner Lessee County Craven Latitude 35.329r Longitude 77.26960 Net Acrea a Surface Subsurface 1.3 1.7 Dominant Soil Series Ba-Bayboro Figures 1 2-1 Roach, Winfred Allen & Gloria - 2-2 Roach, Winfred Allen & Gloria Craven 35.330r 77.26910 3.1 4.0 Se -Seabrook 1 2-3 Roach, Winfred Allen & Gloria Craven 35.33100 77.2719° 19.2 1 19.5 Ba Bayboro 1 24 Roach, Winfred Allen & Gloria Craven 35.33330 77.27010 27.6 32.4 Ap-Arapahoe 1 2-5 Roach, Winfred Allen & Gloria Craven 35.3320° 77.27420 3.8 5.0 Se -Seabrook 1 3-1 Roach, W Allen & Gloria Arrington Craven 35.3214 77.2695 5.6 6.6 Se -Seabrook 2 3-2 Roach, W Allen & Gloria Arrington Y Craven 35.3236 77.2694 14.6 14.6 To-Torhunta 2 3-3 Roach, W Allen & Gloria Arrington Craven 35.3244 77.2716 6.1 6.1 To-Torhunta 2 4-1 McKeel, Linda B et al Roach; Winfred Allen Craven 35.3277 77.2840 8.0 8.0 Ba-Bayboro 3 4-2 McKeel, Linda B et al Roach, Winfred Allen Craven 35.3267 77.2862 10.5 10.5 To-Torhunta 3 4-3 McKeel, Linda B et al I Roach, Winfred Allen Craven 35.3258 77.2894 5.8 5.8 StA-State 3 4-4 McKeel, Linda B et al Roach, Winfred Allen Craven 35.3252 77.2893 3.1 3.1 To-Torhunta 3 4-5 McKeel, Linda B et at Roach, Winfred Allen Craven Craven 35.3243 35.3166 77.2916 77.2671 5.4 12.4 15.2 12.4 CnB-Conctoe TaB Tarboro 3 5 6-1 Roach, Disclaimer Trust -Winfred 6-2 Roach, Disclaimer Trust -Winfred Craven 35.3165 77.2639 17.5 17.5 Portsmouth 4 6-3 Roach, Disclaimer Trust -Winfred Craven 353171 77.2598 4.6 4.6 Ln-Leon 4 6-4 Roach, Disclaimer Trust -Winfred Craven 35.3151 77.2697 7.1 7.1 Ln-Lean 4 7-1 Roach, Disclaimer Trust -Winfred Craven 35.3449 77.2940 5.5 5.9 Tm-Tomodey 5 7-2 Roach, Disclaimer Trust W-infred Craven 35.3499 77.2969 10.6 10.7 Pa-Pantego 5 7-3 Roach, Disclaimer Trust -Winfred Craven 35.3447 77.2921 11.3 11.3 TM-Tomotley 5 7-4 Roach, Disclaimer Trust -Winfred Craven 35.3414 77.2962 20.8 25A Tm-Tomotley 5 8-1 Roach, Disclaimer Trust -Winfred Craven Craven 35.3287 35.3409 77.2729 77.2911 13.9 2.6 13.9 2.6 Ba-Bayboro Se -Seabrook 6 7 10-1 Roach, Disclaimer Trust -Winfred Total 220.4 243.9 WQ0037637 Version 1.0 Attachment B Page 1 of 1