WQ0000672_2018 Residual Annual Report_20190304

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0000672
SUBMITTAL DATED: 2/26/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address* Phone Number*
[e-mail] 4434899086
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0000672
Reviewer*
Troy Doby
Permittee * City of Lumberton
Facility Name * City of Lumberton
County* Robeson
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
City of Lumberton NC 2018 Annual Report.pdf 8.33MB
Application Form Engineering Rans, Specifications, Calculations, Etc.)

For nein and modification permit applications, the paper copy is required to be subrrutted to the
Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic
applications have been received_ The paper copy shall include the follo-kAmig:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineenng plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Service:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigb_ NC 27699-1613
By CourieriSpecial Delivery:
Division of Water Resources- Non -Discharge Branch
Ag Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Raleigh,NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or
Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/26/2019

435 Williams Court, Suite 100
Baltimore, MD 21220
www synagro. com
FEBRUARY 22, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2015 Annual Report for Permit No. WQ0000672
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Lumberton, NC.
If you have any questions or comments, please contact Harold Walters at [phone] or
Melvin Goad at [phone].
Sincerely,
Der,rick Shivar
Environmental Compliance Manager
Enclosures
cc: Harold Walters — City of Lumberton
Melvin Goad - Synagro
YOUR PARTNER FORA CLEANER,GREENERWORL.D

CITY OF LUMBERTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000672
2018 ANNUAL REPORT

City of Lumberton, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0000672 County Robeson Year 2018
Facility Name (as shown on permit) City of Lumberton W WTP NPDES No. NC0024571
Land Application Operator Svnaaro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Annlication Summary:
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 13
Total amount of dry tons applied during the year for all application sites: 476.32
Total number of acres utilized for land application during the year: 200.30
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application pemut (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1.
Part C —Cert
Only residuals approved for this permit were applied to the permitted sites.
2.
Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3.
Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4.
Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5.
All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6.
The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7.
All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8.
All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9.
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10.
No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediation.
it.
Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12.
No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13.
All buffer requirements as specified on the permit were maintained during each application of residuals.
ification:
"I cert
ify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Jim Walters, Director
of EUS Dept.
Permittee Name and Title (type or print)
ignature of Prepare? Date
(if different from Permittee)
�tgnature ofPermittee Date
(10
Signatt o re Date
(if different from Formittee and Pre 'er) .
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
LUMBERTON,NC
LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2018
2,046,000.00
G
269.61
D
244.54
July 2018
1,680,200.00
G
206.71
D
187.48
YEARLY TOTAL
377267200.00
G
476.32
D
432.02
1/25/2019

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000672 Laboratory
Facility Name: LUMBERTON, NC Waypoint Analytical Virginia Inc.
NPDES# : NCO024571
or WQ# (residual only)
WWiP Name: LUMBERTON WWTP
Residuals Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or
02/06/18
05/23/18
07/23/18
10/17/18
Date Composited
Percent Solids
3.16
2.40
2.95
3.59
PARAMETERS (mg/kg
dry weight)
Aluminum
33400
39100
41400
56000
Calcium
12800
12700
11800
14300
Magnesium
2170
1910
1420
1860
pH
7.20
6.70
6.70
5.90
Potassium
3960
3770
2730
2340
Sodium
12500
12900
11400
9160
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.'
Date ZI
NR -Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed saturdav - January 26 2ot9 at 172225 for 2101 of

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000672 Laboratory
Facility Name: LUMBERTON, NC Waypoint Analytical Virginia Inc.
NPDES# : NCO024571
or WQ# (residual only)
WWTP Name: LUMBERTON WWTP
Residuals Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or 02/08/18
05/23/18
07/23/18
10/17/18
Date Composited
Percent Solids
3.16
2.40
2.95
3.59
PARAMETERS (mg/kg dry weight)
Arsenic
3.06
<10
5.34
<9. 88
Cadmium
<2
<1
<1
<1. 98
Mercury
<0.4
<0.4
<0.4
0.235
Chromium
179
201
207
278
Copper
203
264
245
332
Lead
10.4
13.6
15.9
22.8
Molybdenum
<5
4.55
4.69
7.11
Nickel
15.6
12.7
24.2
38.1
Selenium
<5
<10
<5
<9.88
Zinc
418
499
587
887
Total Phosphorus
19900
21500
18500
26000
TKN
57700
315000
47300
37200
Ammonia -Nitrogen
5360
3320
3380
<100
Nitrate and Nitrite
134
146
<2.48
433
"I certify under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.'
DENR FORM RSSF (5/2003) Printed Saturday - January 26 2019 at 1T20 51 for 2101 01

Page: 1 of 2
Report Number: 18-040-0209
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number : 58554
Sample Id : Lumberton WWTP
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, M 23237
Main 804-743-94010 Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OFANALYSIS
Date Sampled: 2/8/2018 11:30:00
Date Received: 02/09/2018 00:00
Date Reported: 02/16/2018
Total Solids "
All values are on a dry
3.16
31600
100.0
R D
02/09/2018
14:40
SM -2540G
Moisture `
96.83
100.0
R D
02/09/2018
14:40
SM -2540G
Total Kjeldahl Nitrogen
5.77
57700
50.0
R D
02/12/2018
09:00
SM-4500-NH3C-TKN
Total Phosphorus
1.99
19900
100
MMT
02/14/2018
14:06
6010C
Total Potassium
0.40
3960
100
MMT
02/14/2018
14:06
6010C
Total Sulfur
0.91
9120
100
MMT
02/14/2018
14:06
601 OC
Total Calcium
1.28
12800
100
MMT
02/14/2018
14:06
6010C
Total Magnesium
0.22
2170
100
MMT
02/14/2018
14:06
6010C
Total Sodium
1.25
12500
1000
MMT
02/14/2018
14:41
6010C
Total Iron
9460
100
MMT
02/14/201814:06
6010C
Total Aluminum
33400
100
MOS
02/16/201813:34
6010C
Total Manganese
191
5.00
MMT
02/14/2018
14:06
6010C
Total Copper
203
5.00
MMT
02/14/2018
14:06
6010C
Total Zinc
418
5.00
MMT
02/14/2018
14:06
6010C
Ammonia Nitrogen
0.54
5360
50.0
R D
02/12/2018
09:00
SM-4500-NH3C
Organic N
5.23
52340
50.0
02/12/2018
09:00
CALCULATION
Nitrate+Nitrite-N
134
2.44
MMT
02/13/201811:30
4500NO3F-2011
weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our poor written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 18-040-0209
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sampled: 2/8/2018 11:30:00
Lab Number: 58554 Date Received: 02/09/2018 00:00
Sample Id : Lumberton WWTP Date Reported: 02/16/2018
Total Cadmium
<2.00
Total Chromium
179
Total Nickel
15.6
Total Lead
10.4
Total Arsenic
3.06
Total Mercury
<0.400
Total Selenium
<5.00
pry •
7.2
Total Molybdenum
<5.00
Comments:
CERT#257
5.00
SULFUR AND ORGANIC NITROGEN
NOT FOR COMPLIANCE PURPOSES.
2.UU
IVIIVII
ULr14/LV10
14:U0
vu iii.
5.00
MMT
02/14/201814:06
6010C
5.00
MMT
02/14/201814:06
6010C
5.00
MMT
02/14/201814:06
6010C
3.00
MMT
02/14/201814:06
6010C
0.400
MOS
02/13/201817:02
SW -7471B
5.00
MMT
02/14/201814:06
6010C
1.0
JM
02/12/201809:00
9045D
5.00
MMT
02/14/201814:06
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confiden(al use of aur clients, and may not be reprotluced in whole orpart
, nor may any reference be made
to the work, the results, or the company in any advertising, news release. or other public announcements without obtaining ourprior wnt[en authorization.
Pauric McGroary
Agronomist

SAMPLING LOG N ABS, INC. CHAIN OF CUSTODY
CUSTOMER: sYNaGRo SOUTHEAST II�IIINININIIIIIIIIIh�I�INlllll�lillllll�lll�llIII a�°8;83 RECORRECORD LYSIS
erlon 1324-26
LUTnWC] On W WTP
V�TSD 1 i�� WV « that the proper field sampling procedures
PROJECT MANAGER:
V�u/s�ed during the collection of these samples.
Phone: (33(x) 10�— 3Z� O/ WA�
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
S%SSL LAVVkWrMvoL WWF 5;LIn S��G'^^? Z/�jg
Relinquished b�mple�r: Date Time Recieved by: � REMARKS:
U ado Z /$ 9-po,, x
Relinquished by: batfe Time ' Recieved by:
Relinquished by: Date Time Recieved by:
SPECIAL INSTRUCTIONS: n 10 U01a)11 j e SDlids
For. monitoring purposes. PO#:
SLi: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zmc
White —A & L Canary— MANAGER COPY
ANALYSIS REQUEST
SAMPLE
I.D.
SL1
SL2
NH -N
a
NO -N
Organic
Cd
Cr
Ni
Pb
As
Hg
Se
PH
CaCO3
a
ds
Mo
CI
NOz N
wvJvT
PO
too
1#40
!/
14000"
!/
m
l/
k*
f/
to
to
14009
too
1,0
SLi: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zmc
White —A & L Canary— MANAGER COPY

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 218/2018 1/1/2018-3131/2018 4.7688
LIQUID
Na mg/I = (Na mg/kg x %Solids) + 100 = (12500 x 3.1600) :100 = 395
Ca mg/l = (Ca mg/kg x %Solids) + 100 = (12800 x 3.1600) + 100 = 404.48
Mg mg/I = (mg mg/kg x %Solids) + 100 = (2170 x 3.1600) + 100 = 68.572
Na meq = Na mg/I + Molec. Wgt. Na = 395 + 23 = 17.1739
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 404.48 + 20 = 20.224
Mg meq = Mg mg/I : Motec.Wgt.Mg = 68.572 + 12 = 5.71433
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 17.1739 - SgrRoot[0.5(20.224+5.71433)] = 4.76885
Printed: 1/29/2019
Page 1 16:22

Waypaint,.
ANALYTICAL
6/6/2018
Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Macksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-149-0206
Project Description: Lumberton WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 604-743.9401 °Fax [phone]
www.waypolnta n alyNcal.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 5!29/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were pertormed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E8710S7 North Carolina 257 South Carolina 93007
Page 1 of 6

WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
Waypoi
7621 Whitepine Road, Richmond, VA 23237
nt..
Main
804-743-9401 °Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample
Summary Table
Report Number: 18-149-0206
Client
Project Description: Lumberton WWTP
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method Lab ID
60902
Lumberton WWTP
Solids
05/23/201810:00
05/29/2018
60902
Lumberton WWTP
Solids
05/23/2018 10:00
05/29/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 18-149-0206
Account Number: 46525
Submitted By: Nate Roth
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville, NC 27028
Lab Number : 60902
Sample Id : Lumberton WWTP
WaypointGo
_
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS
Date Sampled: 5/23/2018 10:00:00
Date Received: 05/29/2018 00:00
Date Reported: 06/06/2018
Total Solids *
All values are on a dry
2.40
24000
100.0
JM
05/29/2018
15:15
SM -2540G
Moisture *
97.59
100.0
JM
05/29/2018
15:15
SM-254OG
Total Kjeldahl Nitrogen
31.50
315000
50.0
R D
06/01/2018
09:00
SM-4500-NH3C-TKN
Phosphorus
2.15
21500
50.0
KKM
06/05/201819:37
6010D
Potassium
0.38.
3770
50.0
KKM
06/05/201819:37
6010D
Sulfur
0.87
8660
50.0
KKM
06/05/201819:37
6010D
Calcium
1.27
12700
50.0
KKM
06/05/201819:37
6010D
Magnesium
0.19
1910
50.0
KKM
06/05/201819:37
6010D
Sodium
1.29
12900
250
KKM
06/05/2018
19:37
6010D
Iron
12200
50.0
KKM
06/05/201819:37
6010D
Aluminum
39100
50.0
KKM
06/05/201819:37
6010D
Manganese
266
5.00
KKM
06/05/201819:37
6010D
Copper
264
2.50
KKM
06/05/201819:37
6010D
Zinc
499
5.00
KKM
06/05/2018
19:37
6010D
Ammonia Nitrogen
0.33
3320
50.0
R D
05/31/2018
08:45
SM-4500-NH3C
Organic N
31.17
311680
50.0
05/31/2018
08:45
CALCULATION
Nitrate+Nitrite-N
146
2.33
MMT
05/31/2018
09:05
4500NO3F-2011
weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Pte e
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 18-149-0206
Account Number: 46525
Submitted By: Nate Roth
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville, NC 27028
Lab Number : 60902
Sample Id : Lumberton WWTP
WaypointIGO
m
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS
Cadmium
<1.00
Chromium
201
Nickel
12.7
Lead
13.6
Arsenic
<10.0
Mercury
<0.400
Selenium
<10.0
pH *
6.7
Molybdenum
4.55
Comments:
KKM
INC CERT#257
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES.
Date Sampled: 5/23/2018 10:00:00
Date Received: 05/29/2018 00:00
Date Reported: 06/06/2018
1.00
KKM
06/05/201819:37
6010D
2.50
KKM
06/05/201819:37
6010D
2.50
KKM
06/05/201819:37
6010D
3.00
KKM
06/05/201819:37
6010D
10.0
KKM
06/05/201819:37
6010D
0.400
SMC
06/04/201815:27
SW -74718
10.0
KKM
06/05/2018
19:37
6010D
1.0
R D
05/30/2018
08:50
9045D
2.50
KKM
06/05/201819:37
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports andletters are for the exclusive and confitlential use of our clients, and may not be reproducedin whole orpart. nor may any re
ference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourpdor written authorization.
Page 4 of 6
Pauric McGroary
Agronomist

Waypoint..®
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytical. com
Cooler Receipt Form
Customer Number: 46525
Customer Name: Synagro Central LLC/ Lumberton
Report Number: 18-149-0206
Shipping Method
Fed Ex O US Postal O Lab O Other
O UPS O Client O Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes O No
Number of coolers received � �
Custody seals intact on shipping container/cooler? O Yes O No � Not Required
Custody seals intact on sample bottles? O Yes O No � Not Required
Chain of Custody (COC) present? � Yes O No
COC agrees with sample label(s)? � Yes O No
COC properly completed � Yes O No
Samples in proper containers? � Yes O No
Sample containers intact? � Yes O No
Sufficient sample volume for indicated test(s)? � Yes O No
All samples received within holding time? � Yes O No
Cooler temperature in compliance? � Yes O No
Cooler/Samples arrived at the laboratory on ice. � Yes O No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes O No O N/A
Water -VOA vials free of headspace O Yes O No � N/A
Trip Blanks received with VOAs O Yes O No � N/A
Soil VOA method 5035 –compliance criteria met O Yes O No r♦ N/A
High concentration container (48 hr) O Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low concyre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? O Yes � No
Comments:
Signature: Brandi Watson —� Date &Time: 05/29/2018 12:50:47
Page 5 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2101-01-AEDLIQ-NC
LUMBERTON, NC WWTP AEROB. DIGESTED
5/23/2018
4/112018-6/30/2018
4.3604
LIQUID
Na mg/I = (Na mg/kg x %Solids) * 100 = (12900 x 2.4000) + 100 = 309.6
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (12700 x 2.4000) _ 100 = 304.8
Mg mg/I = (mg mg/kg x %Solids) + 100 = (1910 x 2.4000) :100 = 45.84
Na meq = Na mg/I _ Molec.Wgt.Na = 309.6 - 23 = 13.4609
Ca meq = Ca mg/I + Molec.Wgt.Ca = 304.8 - 20 = 15.24
Mg meq = Mg mg/I + Molec.Wgt.Mg = 45.84 + 12 = 3.82
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 13.4609 + SgrRoot[0.5(15.24+3.62)] = 4.3604
Printed: 1/29/2019
Page 7 16:22

Waypointry
ANALYTICAL
S/1 /2018
Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Macksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-205-0202
Project Description: Lumberton WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° FaK 804-271-6446
www.way pointanalytica Isom
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 7/24/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 138 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p ••. a=c.-C�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E873087 North Carolina 257 South Carolina 93007
rr�rr5
Page 1 of 7

WaypointM
ANALYTICAL
Client: Synagro Central LLC/ Lumberton
Project: Lumberton VVWTP
Lab Report Number: 18-205-0202
Date: 7/31/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointan alyti ca I. com
CASE NARRATIVE
Nitrate +Nitrite Nitrogen Method 4500NO3F-2011
Sample 61904 (Lumberton VVVVTP)
Analyte: NO3+NO2-N
OC Batch No: E65291/E65259
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Page 2 of 7

Waypoint.. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-205-0202
Client Project Description: Lumberton WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61904
Lumberton
WWTP
Solids
07/23/2018
12:55
07/24/2018
61904
Lumberton
WWTP
Solids
07/23/2018
12:55
07/24/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certifcation: #1354
Page 3 of 7

Report Number: 18-205-0202
Account Number: 46525
Submitted By: Nate Roth
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
WYa ointmG
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointa na lytica Isom
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sampled: 7/23/2018 12:55:00
Lab Number: 61904 Date Received: 07/24/2018 00:00
Sample Id : Lumberton WWTP Date Reported: 08/01/2018
Total Solids* 2.95 29500 100.0 JM U//Z4/LV"I6 lJ:bU arvr<o4w
Moisture * 97.04 100.0 JM 07/24/2018 13:50 SM -2540G
Total Kjeldahl Nitrogen 4.73 47300 50.0 R D 07/25/2018 09:00 SM-4500-NH3C-TKN
Phosphorus 1.85 18500 50.0 KKM 07/28/2018 03:09 6010D
Potassium 0.27 2730 50.0 KKM 07/28/2018 03:09 6010D
Sulfur 0.81 8110 50.0 BKN 07/30/2018 20:47 6010D
Calcium 1.18 11800 50.0 KKM 07/28/201803:09 6010D
Magnesium 0.14 1420 50.0 KKM 07/28/2018 03:09 6010D
Sodium 1.14 11400 250 KKM 07/28/201803:09 601 OD
Iron 12900 50.0 BKN 07/28/2018 03:09 6010D
Aiuminum 41400 50.0 KKM 07/28/2018 03:09 6010D
Manganese 292 5.00 KKM 07/28/2018 03:09 6010D
Copper 245 2.50 KKM 07/28/2018 03:09 6010D
Zinc 587 5.00 KKM 07/28/2018 03:09 6010D
Ammonia Nitrogen 0.34 3380 50.0 R D 07/25/2018 09:00 SM-4500-NH3C
Organic N 4.39 43920 50.0 07/25/2018 09:00 CALCULATION
Nitrate+Nitrite-N <2.48 2.48 MMT 07/26/201813:12 4500NO3F-2011
All values are on a dry
weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page 4 of 7

Report Number: 18-205-0202
Account Number: 46525
Submitted By: Nate Roth
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville . NC 27028
Waypoi nt..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sampled: 7/23/2018 12:55:00
Lab Number : 61904 Date Received: 07/24/2018 00:00
Sample Id : Lumberton WWTP Date Reported: 08/01/2018
Cadmium
`1.00
Chromium
207
Nickel
242
Lead
15.9
Arsenic
5.34
Mercury
<0.400
Selenium
<5.00
pH *
6.7
Molybdenum
4.69
Comments:
KKM
NC CERT#257
03:09
SULFUR AND ORGANIC NITROGEN
NOT FOR COMPLIANCE PURPOSES.
1.uu
rriw
vrr<or<u io
w.��
u���
2.50
KKM
07/28/2018
0109
6010D
2.50
KKM
07/28/2018
03:09
6010D
3.00
KKM
07/28/2018
03:09
601 OD
5.00
BKN
07/30/2018
20:47
6010D
0.400
MMT
07/27/201814:37
SW -74718
5.00
BKN
07/30/2018
20:47
601 OD
1.0
R D
07/25/2018
09:00
9045D
2.50
KKM
07/28/2018
03:09
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart
, nor may any reference be made
to the work, the results, orthe company in any advertising, news release, or ofherpublic announcements without obtaining ourpnor whtten authorization.
Page 5 of 7
Pauric McGroary
' Agronomist

Waypoint,.®
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalyNcal.co m
Cooler Receipt Form
Customer Number: 46525
Customer Name: Synagro Central LLCI Lumberton
Report Number: 18-205-0202
Shipping Method
O
Fed Ex
O
US Postal
O
Lab
UPS
O
Client
O
Courier
O Other: �—
Thermometer ID:
Shipping container/cooler uncompromised? � Yes O No
Number of coolers received r
Custody seals intact on shipping container/cooler? O Yes O No � Not Required
Custody seals intact on sample bottles? O Yes O No � Not Required
Chain of Custody (COC) present? � Yes O No
COC agrees with sample label(s)? � Yes O No
COC properly completed � Yes O No
Samples in proper containers? � Yes O No
Sample containers intact? � Yes O No
Sufficient sample volume for indicated test(s)? � Yes O No
All samples received within holding time? � Yes O No
Cooler temperature in compliance? � Yes O No
Cooler/Samples arrived at the laboratory on ice. � Yes O No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved O Yes O No � N/A
Water -VOA vials free of headspace O Yes O No � N/A
Trip Blanks received with VOAs O Yes O No � N/A
Soil VOA method 5035 –compliance criteria met O Yes O No � N/A
High concentration container (48 hr) O Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? O Yes � No
Comments:
Signature: �andi Watson � Date &Time: 07/24/2018 13:22:4
Page 6 of 7

u u �pN II p Iln�p r;, 7'S
II�piiiiiiiiii IIIIYNII lillilllllll�l illll r7245xols MAIN OF CUSTODY
SAMPLING LOG #� � SvneamCemmlLLOILumbeMn 10-.47:24 ECORD A ANALYSIS
Lumberton W W rP RECORD
CUSTOMER: SYNA+GRO
PROJECT MANAGER: (A Ra th
Phone: ) `103
Ag,L CUSTOMER SAMPLING SAMPLE
LAB # SAMPLE . LOCATION TYPE
1 ,,.,nkaller, W�'TP I 5ludga-
Relinquished by San�aie
Relinquished by:
Relinquished by:
SPECIAL I/N;STRUCTIONS:
For.
7/a3 a.3o
I attest that the proper field sampling procedures
were used during the collection of these samples,
,it 13uPs�
SAMPLER
# OF SAMPLING METHOD METHOD
CON
I.DTAINERS DATE TIME PRESERVED SHIPPED
OW v6,SYv
Date Time
Recieved by:
Dat Time
clave by:
Dat Time
Recieved by:
monitoring purposes.
IA:SS TGr '
REMARKS:
ANALYSIS REQUEST
SAMPLE a
I•®Ornic • SL1 SL2 NH4 N NO3 N Cd Cr Ni Pb As Hg Se pH
J""w 1,00F pow 1,00F 100or 1,00'r poo too 104*0 too Po"
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SI -1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 7/23/2018 7/1/2018-913012018 4.5236
LIQUID
Na mg/I = (Na mg/kg x %Solids) - 100 = (11400 x 2.9500) - 100 = 336.3
Ca mg/I = (Ca mg/kg x %Solids) - 100 = (11800 x 2.9500) _ 100 = 348.1
Mg mg/I = (mg mg/kg x %Solids) + 100 = (1420 x 2.9500) + 100 = 41.89
Na meq = Na mg/I + Molec.Wgt.Na = 336.3 : 23 = 14.6217
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 348.1 - 20 = 17.405
Mg meq = Mg mg/I + Molec.Wgt.Mg = 41.89 > 12 = 3.49083
SAR = Na meq : SgrRoot[0.5 x (Ca meq + Mg meq)] = 14.6217 + SgrRoot[0.5(17.405+3.49083)] = 4.5236
Printed: 1!29!2019
Page 1 16:22

Waypoint,.
ANALYTICAL
10/26/2018
Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-292-0206
Project Description: Lumberton WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalyNca I. com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 10/19/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E671087 North Carolina 257 South Carolina 93007
Page 1 of 6

Wa O' ■ ■�,.® 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
Y ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-292-0206
Client Project Description: Lumberton WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63240
Lumberton
WWTP
Solids
10/17/2018
14:00
6010D
10/19/2018
63240
Lumherton
WWTP
Solids
10/17/201814:00
WTN
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/2018
14:00
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/2018
14:00
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/2018
14:00
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/201814:00
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/2016
14:00
10/19/2018
63240
Lumberton
WWTP
Solids
10/17/201814:00
10/19/2018
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
SM-4500-NH3C
WTN
9045D
WTN
4600NO3F-2011
WTN
6010D
WTN
SW -7471B
WTN
SM-4500-NH3C-TKN
WTN
SM -2540G
WTN

Report Number: 18-292-0206
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
WaypointIGO
.
ANALYTICAL
7621 W hitepine Road, Richmond, VA 23237
Main 804.743-9401 0 Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sampled: 10/17/2018 14:00:00
Lab Number: 63240 Date Received: 10!19/2018 00:00
Sample Id : Lumberton WWTP Date Reported: 10/2612018
Total Solids' 3.59 35900 100.0 c.11t 1U%LJ/LU"IJ "IiS:GS JrvrLoffuu
Moisture ` 96.40 100.0 CJR 10/23/2018 18:23 SM -2540G
Total Kjeldahl Nitrogen 3.72 37200 250 CLP 10/23/2018 12:30 SM-4500-NH3C-TKN
Phosphorus 2.60 26000 98.8 KKM 10/25/201817:27 6010D
Potassium 0.23 2340 98.8 KKM 10/25/201817:27 6010D
Sulfur 0.97 9670 98.8 KKM 10/25/201817:27 6010D
Calcium 1.43 14300 198 KKM 10/25/201817:27 6010D
Magnesium 0.19 1860 98.8 KKM 10/25/201817:27 6010D
Sodium 0.92 9160 494 KKM 10/25/201817:27 6010D
Iron 18900 98.8 KKM 10/25/201817:27 6010D
Aluminum 56000 98.8 KKM 10/25/201817:27 6010D
Manganese 413 9.88 KKM 10/25!201817:27 6010D
Copper 332 4.94 KKM 10!25/201817:27 6010D
Zinc 887 9.88 KKM 10/25/201817:27 6010D
Ammonia Nitrogen <0.01 <100 100 ZBD 10/23!201809:30 SM -4500 -NI -13C
Organic N 3.72 37200 250 10/23/2018 09:30 CALCULATION
Nitrate+Nitrite-N 433 4.90 ZBD 10/23/201815:00 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. / ,,/
B -Analyte detected in blank H - Beyond Holding Time ?W« I"� 60w
Our reports and letters are forthe exclusive antl confidential use of our cBenfs, and may not be reproducetlin whole orpart
. normay any reference be made Pauric McGroary
to the work, the results, orthe company in any advertising, news release, or other public announcements without obtaining ourpdor wnften authohza4'on. AgrOnOmlSt
Page 3 of 6

Report Number: 18-292-0206
Account Number: 46525
Send To: Synagro Central LLC/ Lumberton
Mary Brewer
284 Boger Road
Mocksville , NC 27028
0
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
Project: Lumberton WWTP
REPORT OF ANALYSIS Date Sampled: 10/17/2018 14:00:00
Lab Number: 63240 Date Received: 10/19/2018 00:00
Sample Id : Lumberton WWTP Date Reported: 10/26/2018
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH'
Molybdenum
Comments:
All values are on a dry weight basis except as noted.by asterisk. Detection limit on all N series is on a wet basis.
B -Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whale orpaR, nor may any reference be made
to the work, the results, or the company in any ativertlsing news release, or otherpublic announcements without obtaining ourprior written authonza6on.
Page 4 of 6
Pauric McGroary
Agronomist
278
4.94
KKM
10/25/201817:27
6010D
38.1
4.94
KKM
10/25/201817:27
6010D
22.8
5.93
KKM
10/25/201817:27
6010D
<9.88
9.88
KKM
10/25/201817:27
6010D
0.235
0.0156
KKM
10/24/201812:31
SW -74716
<9.88
9.88
KKM
10/25/201817:27
6010D
5 g
JSL
10/25/2018
08:50
9045D
7.11
4.94
KKM
10/25/201817:27
6010D
All values are on a dry weight basis except as noted.by asterisk. Detection limit on all N series is on a wet basis.
B -Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whale orpaR, nor may any reference be made
to the work, the results, or the company in any ativertlsing news release, or otherpublic announcements without obtaining ourprior written authonza6on.
Page 4 of 6
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 10/17/2018 10/112016.12/31/2018 3.6180
LIQUID
Na mg/I = (Na mg/kg x %Solids) - 100 = (9160 x 3.5900) + 100 = 328.844
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (14300 x 3.5900) + 100 = 513.37
Mg mg/I = (mg mg/kg x %Solids) = 100 = (1860 x 3.5900) + 100 = 66.774
Na meq = Na mg/I - Molec.Wgt.Na = 328.844+23 = 14.2976
Ca meq = Ca mg/I + Molec.Wgt.Ca = 513.37 = 20 = 25.6685
Mg meq = Mg mg/I + Molec.Wgt.Mg = 66.774 = 12 = 5.5645
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 14.2976 = SgrRoot[0.5(25.6685+5.5645)] = 3.61801
Printed: 1/29/2019
Page 1 16:22

Waypoint..®
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa na lytics Isom
Cooler Receipt Form
Customer Number: 46525
Customer Name: Synagro Central LLC/ Lumberton
Report Number: 18-292-0206
Shipping Method
Fed Ex � US Postal � Lab � Other : �—
UPS � Client � Courier Thermometer ID: �—
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received r 'l
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? t♦ Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No � N/A
Water -VOA vials free of headspace � Yes � No � N/A
Trip Blanks received with VOAs 0 Yes 0 No � N/A
Soil VOA method 5035 –compliance criteria met � Yes � No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson � Date &Time: 10/19/2018 13:04:07
Page 5 of 6

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SECTION 3

FACIIdTYNAME: LUMBERTON,NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: RAINS
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 33.56
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90
Page:
Lime Applied **"
Date Lbs/Ac
Total Gallons/Ac: 16,142.01
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
Annual lbs/acre59
0.021 0.004 0.822 0.973 0.063 0.002 0.019 0.096 0.020 2.331 73.47
Cumulative Ibs/acre 0.078 0.028 2.809 3.845 0.241 0.004 0.079 0.383 0.080 6.741 IMMMEN
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations."
N/A=Not Applicable NR —Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019
allons (G) or Cubic Yards ICY)
Dry,
Site
Inches
Apph-
V01a-
Miner -
or Wet Tons (WT) (specify)
Tons
Cord.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
7/16/18
2295400.00 (G)
13573.9641
2.95
1.670
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
3,380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
7/17/18
435400.00 (G)
2568.0471
2.95
0.316
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300. p
3,380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
272,800.00 (G)
16,142.011
Total Gallons/Ac: 16,142.01
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
Annual lbs/acre59
0.021 0.004 0.822 0.973 0.063 0.002 0.019 0.096 0.020 2.331 73.47
Cumulative Ibs/acre 0.078 0.028 2.809 3.845 0.241 0.004 0.079 0.383 0.080 6.741 IMMMEN
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations."
N/A=Not Applicable NR —Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: LUMBERTON, NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0002
RFSiDJIAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 12.97
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60
Page
Lime Applied'**
Date L6s�Ac
Total Gallons/Ac: 299
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
Total Wet Tons/Ac:
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
As
Cd
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TIIN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
107
Annual lbs/acre
7/17/18
62,000.00 (G)
17222.222
2.95
2.119
LUAEDL
DRY
0-<I/2"
SUR
0.5
0.30
47,300. p
3,3807p2.48
p
14868
I BERMUDAGRASS PASTURE
7/18/18
43,400.00 (G)
12055.556
2.95
1.483
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
3,380.48
p
14868
BERMUDAGRASS PASTURE
Jul -18
105,400.00 (G)
29,277.778
277.78
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Pb
Hg
Mo
Ni
To
Zn P PAN
TOTALS:
107
Annual lbs/acre
0.038
0.007
1.491
1.765
0.115
0.003
0.034
0.174
0.036
4.228 133.26
Cumulative lbs/acm
0.113
0.039
4.598
6.447
0.370
0.008
0.122
0.625
0.116
11.232
LUAEDL = LUMBERTON, NC W WTP AEROH. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there we significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %—percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: LUMBERTON, NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 4.58
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40
Page: 1
Lime Applied ***
Date Lbs/Ac
Total Gallons/Ac: 10,941.15
oilers (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
Total Wet Tons/Ac:
or Wet Tons (VTT) (specify)Tons
Cond.
Precip.
cation
till-
all-
Ammonia
Nitrate
PAN
DATE or
As
Per
Residual
Dry, Wet,
Pact 24
Method
zafion
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
per Acre
Solids
40
7/17/18
37,200.00 (G)
10941.176
2.95
1.346
LUAEDL
DRY
0-<I/2"
SUR
0.5
0.30
47,300.p
3,380.00 p
2.48 p
14868
BERMUDAGRASSPASTURE
Jul -18
37,200.00 (G)
10,941.176
0.109
0.537
0.102
9.092
Total Gallons/Ac: 10,941.15
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Pb
Hg
Mo
Ni
Se
Zn P PAN
TOTALS:
40
Annual lbs/acre
0.014
0.003
0.557
0.660
0.043
0.001
0.013
0.065
0.013
1.580 49.80
Cumulative lbs/acre
0.092
0.038
3.707
5.764
0.312
0.005
0.109
0.537
0.102
9.092
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
J certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0004
RFCmii AT. CrliiRf A/CI * See list at bottom of reoort
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: RAINS
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 7.63
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60
Page:
Lime Applied ***
Daie Lls
Total Gallons/Ac: 17,222.22
Total Wet Tons/Aa
Total Cubic Yds/Ac: 0.00
TOTALS:
Annual lbs/acre
I Cumulative Ibs/acre
0.023
allons (G) or Cubic Yards (CY)
0.877
Dry
0.067
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/17/18
62,000.00 -(G)
17222.222
2.95
2.119
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
3,380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
62 M0,00 (G)
17,222.222
Total Gallons/Ac: 17,222.22
Total Wet Tons/Aa
Total Cubic Yds/Ac: 0.00
TOTALS:
Annual lbs/acre
I Cumulative Ibs/acre
0.023
0.004
0.877
1.036
0.067
0.097
1 0.037
1 3.918
1 5.701
1 0.321
Hg Mo Ni
0.002 0.020 0.103
0.006 0.109 0.548
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=plan or mg/kg ** Volatilization Rate: Surface 0.5, injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACBdTYNAME: LUMBERTON,NC
OWNER. OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0005
DUQMTTAT gnTTTarFigl * qPP ligt at hnnnm of rennrt
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: RAINS
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 15.25
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70
Page: 1
Lime Applied ***
Date Lbe/Ac
Total Gallons/Ac: 14,252.87
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
Annual lbs/acre
Cumulative Ibs/acre
As � Cd � Cr I Cu I Pb
0.019
allons (G) or Cubic Yards (CY)
0.726
Dry,
0.056
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
A
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/19/18
99,200.00 (G)
11402.299
2.951.403
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
3,380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
7/20/18
249800.00 (G)
2850.575
2.95
0.351
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
3,380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
1244000.00 (G)
14,252.874
Total Gallons/Ac: 14,252.87
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
Annual lbs/acre
Cumulative Ibs/acre
As � Cd � Cr I Cu I Pb
0.019
0.004
0.726
0.859
0.056
0.092
0.035
3.540
r5.019
0.296
Hg Mo Ni
0.001 0.01.6 0.085
0.006 0.099 0.492
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
T --
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A= Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACT ITY NAME: LUMBERTON, NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0006
RESIDUAL SOURCE(S):* See list at bottom of report
ANN UAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 38.14
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80
Page: 1
Lime Applied ***
Date LbatAc
alIons (G) or Cubic Yards (CY)
Total Gallons/Ac: 20,945.95
Dry
site
Inches
Apph-
Vola-
Miner -
Total Wet Tons/Ac:
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
As
Cd
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
77
Annual lbs/acre
7/18/18
223,200.00 (G)
15081.081
2.95
1.855
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
33380.00 p
2.48 p
14868
I BERMUDAGRASS PASTURE
7/19/18
865800.00 (G)
5864.865
2.95
0.721
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
47,300.p
35380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
310,000.00 (G)
20,945.946
Total Gallons/Ac: 20,945.95
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se Zn P PAN
TOTALS
77
Annual lbs/acre
0.028
0.005
1.067
1.263
0.082
0.002
0.024
0.125
0.026
3.025 95.34
Cumulative lbs/acre
0.107
0.040
4.629
6.848
0.368
0.008
0.126
0.648
0.113
11.250
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0007
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 45.76
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 17.50 ACRES PERMITTED: 17.50
Page: 1
Lime Applied ***
Date Lbs/Ac
Total Gall
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
Total Wet Tons/Ac:
or Wet Tons (WT) (specify)Tons
Cond.
Precip.
cation
tili-
alr
Ammonia
Nitrate
PAN
DATE or
As
Cd
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
78
7/20/18
99,200.00 (G)
5668.571
2.95
0.697
LUAEDL
DRY
OQ/2"
SUR
0.5
0.30
47,300.p
35380.00 p
2.48 p
14868
I BERMUDAGRASS PASTURE
7/26/18
2722800.00 (G)
15588.571
2.95
1.918
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
47,300.p
31380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
372,000.00 (G)
21,257.142
0.075
7.495
ons/Ac: 21,257.14
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Pb
Hg
Mo
Ni
Se
Zn P PAN
TOTALS:
78
Annual lbs/acre
0.028
0.005
1.083
1.281
0.083
0.002
0.025
0.127
0.026
3.070
96.75
Cumulative lbs/acre
0.060
0.025
3.190
4.850
0.238
0.006
0.079
0.422
0.075
7.495
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INI - Injection, SURIN -Incorporation **' See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: OZZELL BAKER
SITE #: NC RO 00016 FIELD# : RO 00016 0008
RPq MTTAT.SCITTRCECSI* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 18.31
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
Page: 1
Lime Ap lied ***
Date Lbs/Ac
Total Gallons/Ac: 19,578.95
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
/:R,4f1[O�ES�
1 Cumulative ]bs/acre
0.026
allons (G) or Cubic Yards (CY)
0.997
Dry
0.077
Site
Inches
Appli-
Vola-
Miner -
0.005
0.123
0.578
0.124
10.134
or Wet Tons (WT) (specify)
Tons
Card.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/26/18
435400.00 (G)
5710.526
2.95
0.702
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
473300.p
32380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
7/27/18
105,400.00 (G)
13868.421
2.95
1.706
LUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
47,300.p
37380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
148,800.00 (G)
199578.947
Total Gallons/Ac: 19,578.95
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
/:R,4f1[O�ES�
1 Cumulative ]bs/acre
0.026
0.005
0.997
1.180
0.077
0.116
1 0.045
1 4.086
1 6.044
1 0.362
Hg
Mo
Ni
Se
Zn P PAN
0.002
0.023
0.117
0.024
72
2.828 89.11
0.005
0.123
0.578
0.124
10.134
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %—percent p=plan or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INT - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: J T CAMPEN
SITE #: NC RO 00016 FIELD# : RO 00016 0018
RRSTDI TAL SOURCE(Sl:* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 28.22
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 12.30 ACRES PERMITTED: 12.30
Page: 1
Lime Applied xxx
Date Lbs�Ac
Tota] Gallons/Ac: 189
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
Total Wet Tons/Ac:
or Wet Tons (WT) (specify)
/
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATEor
As
Cd
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
68
Annual ]bs/acre
7/27/18
2292400.00 (G)
18650.407
2.95
2.294
LUAEDL
MOIST
0-4/2"
SUR
0.5
0.30
47,300.p
31380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
2291400.00 (G)
18,650.407
3.110
0.257
34.242
650.41
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Pb
Hg
Mo
Ni
Se
Zn P PAN
TOTALS:
68
Annual ]bs/acre
0.025
0.005
0.950
1.124
0.073
0.002
0.022
0.111
0.023
2.693 84.89
Cumulative lbs/acre
0.282
0.127
11.835
41.689
3.704
0.047
0.777
3.110
0.257
34.242
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: 7T CAMPEN
SITE #: NC RO 00016 FIELD# : RO 00016 0019
RFCR)I iAi. qOT TRCF(S) * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WAGRAM
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 2.29
OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60
Page: I
Lime Applied ***
Date Lbs/Ac
Total Gallons/Ac: 119
allons (G) or Cubic Yards (CY)
0.592
Dry
0.045
Site
Inches
Appli-
Vola-
Miner -
0.014
1.679
52.91
43
0.021
0.388
or Wet Tons (WT) (specify)
0.164
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/27/18
18,600.00 (G)
11625.000
2.95
1.430
LUAEDL
MOIST
N<1/2"
SUR
0.5
0.30
475300.p
39380.00 p
2.48 p
14868
BERMUDAGRASS PASTURE
Jul -18
18,600.00 (G)
115625.000
625.00
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
Annual lbs/acre
� Cumulative ]bs/acre
0.015
0.003
0.592
0.701
0.045
0.149
0.119
7.609
36.436
2.433
Hg
Mo
Ni
Se
Zn
P
PAN
0.001
0.013
0.069
0.014
1.679
52.91
43
0.021
0.388
2.323
0.164
24.457
LUAEDL = LUMBERTON, NC W WTP AEAOB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR—Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN3 - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: LUMBERTON, NC
OWNER. CITY OF LUMBERTON (AIRPOR
SITE #: NC RO 00017 FIELD# : RO 00017 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 83.33
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 25.40 ACRES PERMITTED: 25.40
Page: I
Lime Applied
Date Lba�Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
all-
zation
THIN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
As
Cd
Cr
Cu Pb
Hg
3/17/18
1671400.00 (G)
6590.551
3.16
0.868
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
I SOYBEANS
3/18/18
933000.00 (G)
3661.417
3.16
0.482
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
SOYBEANS
3/19/18
148,800.00 (G)
5858.268
3.16
0.772
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
SOYBEANS
3/23/18
1485800.00 (G)
5858.268
3.16
0.772
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
(SOYBEANS
3/24/18
74,400.00 (G)
2929.134
3.16
0.386
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
SOYBEANS
Mar -18
6329400.00 (G)
249897.638
Total Gallons/Ac: 24,897.64
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Pb
Hg
Mo
Ni
Se Zn P PAN
TOTALS:
121
Annual lbs/acre
0.020
0.013
1.175
1.332
0.068
0.003
0.033
0.102
0.033
2.743 130.58
Cumulative lbs/acre
0.160
0.087
9.086
20.128
1.667
0.035
0.419
1.969
0.193
20.616
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INS - Injection, SURIN -Incorporation *'* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME'. LUMBERTON,NC
OWNER: CITY OF LUMBERTON (AIRPOR
SITE #: NC RO 00017 FIELD# : RO 00017 0003
RRgiDT TAI. SOI TRCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 66.18
OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 28.00 ACRES PERMITTED: 28.00
Page: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
nation
Miner -
ali-
nation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
As
Cd
3/19/18
186,000.00 (G)
6642.857
3.16
0.875
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
SOYBEANS
3/23/18
204,600.00 (G)
7307.143
3.16
0.963
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
575700.p
5,360.00 p
134.00 p
18516
SOYBEANS
3/24/18
111,600.00 (G)
3985.714
3.16
0.525
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
SOYBEANS
Mar -18
5024200.00 (G)
17,935.714
12.426
IMMI
Total Gallons/Ac: 17,935.71
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu Ph
Hg
Mo
Ni
Se
Zn ==
TOTALS:
88
Annual lbs/acre
0.014
0.009
0.846
0.960
0.049
0.002
0.024
0.074
0.024
1976. 94.06
Cumulative lbs/acre
0.098
0.060
5.703
8.175
0.386
0.012
0.153
0.739
0.138
12.426
IMMI
LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there me significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg "* Volatilization Rate: Surface 0.5, injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITYNAME: LUMBERTON,NC
OWNER: ROBERT BASKERVILLE, JR
SITE #: NC RO 00028 FIELD# : RO 00028 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: RAINS
PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 120.10
OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON -503):
ACRES UTILIZED: 56.90 ACRES PERMITTED: 56.90
Page: I
Lime Applied *"
Date Lbs/Ac
DATE or
Total Gallons/Ac: 169
at Ions (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ah-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
As
Cd
3/14/16
297,600.00 (G)
5230.228
3.16
0.689
LUAEDL
DRY
0- 1/2"
SUR
0.5
0.30
57,700.p
5,360.00 p
134.00 p
18516
I CORN
3/15/18
279,000.00 (G)
4903.339
3,16
0.646
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700.p
57360.00 p
134.00 p
18516
I CORN
3/16/18
285,200.00 (G)
5012.302
3.16
0.660
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
57,700. p
5,360.00 p
134.00 p
18516
I CORN
3/17/18
49,600.00 (G)
87L7051
3.16
0.115
LUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
573700.p
5,360.00 p
134.00 p
18516
CORN
Mar -18
911,400.00 (G)
16,017574
01757
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
As
Cd
Cr
Cu PbHg
Mo
Ni
Se
Zn P PAN
TOTALS:
76
Annual lbs/acre
0.013
0.008
0.756
0.857
0.044
0.002
0.021
0.066
0.021
1.765 84.00
Cumulative lbs/acre
0.082
0.039
4.338
5.426
0.306
0.007
0.105
0.653
0.083
6.998 MMEM
LUAEDL = LUMBERTON, NC W WTP AEAOB. DIGESTED LIQUID -
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A= Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg *` Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

SECTION 4

SUMMIT Summil Enhironmenta7 Technologies,TInc.
33/0 Win St.
rWIROMldENTALTEOHNOWMES, INN Cuyahoga Falls, Ohio 44223
Anafytica/ Laboraforlaa TEL: [phone] FAX [phone]
Website: Mtn Aviviv.seltekeom
March O5, 2018
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Lumberton WWTP
Dear Nate Roth:
Order No.: 18020512
Summit Environmental Technologies, Inc. received 1 samples) on 2/9/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely, �� //
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88
-0735, Cali£omia 07256CA, Colondq ConnecticutPH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Dlinois
200061, Indiana C -OH -13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 040fi1, Maryland 339, Minnesota
409711, New Hmnpslilre 2996, New Iersey OH006, New York 11777, North Caroliva 39705 and 631, North Dakota R-201, Oklahoma 9940, Orcgon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah 0H0092320114, Virginia VELAP 9456, Washington
C891
Page 1 of 27

SUMMIT SummitEm�ironmenta7Technol10 es,Win
Ina Case Narrative
ffJ
3310 Win St.
FHVIRONMENTAL TECHNOLOGIES, INC- Cuyahoga Falls, Ohio 44223 WO#: 18020512
Art tytiral;abora?orJes TEL: [phone] FAX: [phone]
Website: hao llw3viv.seltekcon¢ Date: 3/5/2018
CLIENT: Synagro
Project: Lumberton WWTP
WorkOrder Narrative:
18020512: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc, holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report, State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples
are reported
on an
"as received" or
"wet weight" basis unless indicated as
"dry weight" using the "-dry"
designation
on the
reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
18020512-OOlA SVOC-BNA_TCLP(8270): Sample exhibited outlying surrogate recovery due to
sample matrix.
Analytical Sequence QC Notes:
ccv 40ng S8- svoc-mstr_s(8270): The BNA 8270 CCV (Batch R60867) exhibited high recovery for
Pyridine; Associated samples are ND for Pyridine.
les -30915 tclp-svoc-cpest_tclp(8081): The TCLP Pesticide LCS (Batch 30915) exhibited high recovery
for Surrogate: DCB; TCMX exhibited control; All other analytes of interest exhibited recoveries within
the acceptance limits.
Original
Page 2 of 27

SUMMIT samn,uE„v;ronn,enlalTechaorogies, t Qualifiers and Acronyms
M33/o wia s
CWHOMM ENTAL TECHHQ WV I€5, INC Cuyahoga Falls, Ohio 4422 WO#: 18020512
Artaly6rar Laboraiarfes TEL: [phone] FAY: (330) 253-446
Webs;le: haallaivw.serrekco Date: 3/5/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
This list of Qualifiers and Acronyms refl
The compound was analyzed for but was not detected.
S
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m
Manual integration was used to determine the area response.
d
Manual integration in which peak was deleted
N
The result is presumptive based on aMass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GUMS.
X
The result was not confirmed when GUMS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimum Compound Limit
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
ects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 27

Sunmlit Environmental TechnaloWin St. WOTkOrdeT
Not33100 Win St.
UNVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Sample Summary
Analytical LaOarseories TEL: [phone] FLY: [phone] WO#: 18020512
Website: Into //wwwseaek.eom 05-Mar-18
CLIENT: Synagro
Project: Lumberton WWTP
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
18020512-001 Lumberton W WTP 2/8/2018 11.30:00 AM 2/9/2018 10'.30.00 AM Sludge
Page 4 of 27

SUMmT Summit Environmental Technologies, Inc.
3310 Win St.
�VIFIONPAFNTALTSCHNOLOO1'SS, IMC. Cuyahoga Falls, Ohio 44223
Analytieaf Laborafcrnes TEL: [phone] FAX. [phone]
Website: hito llwww.settek.com
DATESREPORT
WO#: 18020512
OS -Mar -l8
Client: Synago
Project: Lumberton WWTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
18020512-001A Lumberton W WTP 2/8/2018 1130:00 AM Sludge Ignitability of Solids (SW -846:1030) 2/16/2018 2:00:00 PM
pH
(SW9045D)
Reactive Cyanide (9014/7.3.32) -Solid
Reactive Sulfide (9034)/7.3.4.2
2/16/2018 1:51:00 PM
2/15/2018 12:11:00 PM
2/15/2018 12:11:00 PM
TCLP Herbicides Analysis (SWI311/8
2/19/2018 11:30:00 A
2/24/2018 7:46:00
AM
TCLP Mercury Analysis (SW1311/74'12/12/2018 6:00:00
PM
2/13/2018 5:45:00
PM
2/14/2018 11:46:00
AM
TCLP Metals Analysis (SW1311/6010:2/12/2018 6:00:00
PM
2/13/2018 5:15.23
PM
2/14/2018 9:12:24
PM
TCLP Pesticides Analysis (SW1311/8(2/12/2018 6:00.00
PM
2/14/2018 7:00:00
AM
2/17/2018 6:57:00
AM
TCLP Semi -Volatiles Analysis 2/12/2018 600.00
PM
2/14/2018 9
00:00
AM
2/15/2018 629:00
PM
(SW 1311/8270)
TCLP Volatiles Analysis
2/12/2018 6:00:00
PM
2/14/2018 238.00
PM
Original
Page 5 of 27

RISUMMIT Summit Enviromnenral Technologies, Inc. 3310 Win S!. Analytical Report
FNVIRONMENTALTECHNOLOWEs; INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Lyboraiories; TEL: [phone] FAX: [phone] WO#: 18020512
Website: http Avwrv.settek.c°m Date Reported: 3/5/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 2/8/2018 11:30:00 AM
Lab ID: 18020512-OOIA
Project: Lumberton WWTP
Client Sample ID Lumberton WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SWl31117470)
TCLP Mercury ND 0.00500 mg/L 1 2/14/2018 11:46:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010 SW301OA Analyst: KMS
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND 0.500 mg/L 1 2/14/2018 9:12:24 PM
TCLP Barium(Ba) ND 5.00 mglL 1 2/14/2018 9:12:24 PM
TCLP Cadmium(Cd) ND 0.100 mglL 1 2/14/2018 9:12:24 PM
TCLP Chromium(Cr) ND 0.200 mglL 1 2/14/2018 9:12:24 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 2/14/2018 9:12:24 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 2/14/2018 9:12:24 PM
TCLP Silver(Ag) ND 0.500 mglL 1 2/14/2018 9:12:24 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW351OC Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270)
1,4 -Dichlorobenzene ND 0.0800 mg/L 2 2/15/20186:29:00 PM
2,4,5 -Trichlorophenol ND 0.200 mglL 2 2/15/2018 6:29:00 PM
2,4,6 -Trichlorophenol ND 0.200 mg/L 2 2/15/2018 6:29:00 PM
2,4-Dinitrotoluene ND 0.100 mglL 2 2/15/20186:29:00 PM
Cresols, Total ND 4.00 mg/L 2 2/15/2018 6:29:00 PM
Hexachloro-1,3-butadiene ND 0.100 mg/L 2 2/15/20186:29:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 2/15/2018 6:29:00 PM
Hexachloroethane ND 0.0800 mg/L 2 2/15/2018 6:29:00 PM
Nitrobenzene ND 0.0800 mg/L 2 2/15/20186:29:00 PM
Pentachlorophenol ND 0.200 mg/L 2 2/15/2018 6:29:00 PM
Pyridine ND 0.200 QC+ mg/L 2 2/15/20186:29:00 PM
Surr. 2-Fluorophenol 8.40 10-109 S %Rec 2 2/15/2018 6:29:00 PM
Surr: Phenol -d6 3.04 10-109 S % Rec 2 2/15/2018 6:29:00 PM
Surr: Nitrobenzene -d5 85.4 19-120 % Rec 2 2/15/201B 6:29:00 PM
Surr: 2,4,6-Tribromophenol 8.48 10 - 120 S % Rec 2 2/15/2018 6:29:00 PM
Surr: 2-Fluorobiphenyl 73.0 22-117 % Rec 2 2/15/2018 6:29:00 PM
Surr: p-Terpheny1-d14 81.6 34-116 % Rec 2 2/1512018 6:29:00 PM
Qualifiers: '
Value exceeds Maximwn Contaminant Level.
H
Holding times for preparation or analysis exoeeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identiEed compounds
O RSD is greater han RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 6 of 27

SUMMIT
9an,mil Environmental Technor1Win t. Analytical Report
33100 Win St.
RI
fNVIRQNMENTAL TECHNQLpGIe5,1NC Cuyahoga Falls, Ohio 44223 (base report)
Analytical l_abpraiories TEL: [phone] FAX: [phone] WO#: 18020512
Website: Into d/iuww sertek com Date Report
ed: 3/5/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 2/8/2018 11:30:00 AM
Lab ID: 18020512-OOIA
Project: Lumberton WWTP
Client Sample ID Lumberton W WTP
Analyses
} Value exceeds Maximum Conta
Qualifiers:
Result
RL Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8270C
SW3510C Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
NOTES:
Sample exhibited outlying surrogate recovery due to sample
matrix.
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8081A
SW3510C Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
0.0200
mg/L
2
2/17/2018 6:57:00 AM
Toxaphene
ND
0.0400
mg/L
2
2/17/2018 6:57:00 AM
Endrin
ND
0.00200
mg1L
2
2/17/2018 6:57:00 AM
gamma -BHC -
ND
0.00200
mg/L
2
2/17/20186:57:00 AM
Heptachlor
ND
0.00200
mg/L
2
2/17/2018 6:57:00 AM
Heptachlor epoxide
ND
0.00200
mg/L
2
2/17/2018 6:57:00 AM
Methoxychlor
NO
0.00200
mg/L
2
2/17/2018 6:57:00 AM
Surr: TCMX
39.6
10-119
%Rec
2
2/17/2018 6:57:00 AM
Sun, DCB
33.5
10-119
% Rec
2
2/17/2018 6:57:00 AM
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8151A
SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW131118151)
2j4 -D
ND
1.00
mg/L
1
2/24/2018 7:46:00 AM
21415 -TP
NO
0.500 d
mg/L
1
2/24/20187:46:00 AM
Surr: DCAA
84.2
20-140
% Rec
1
2/24/2018 7:46:00 AM
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8260B
SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
111-Dichloroethene
ND
0.125
mg/L
25
2/14/20182:38:00 PM
1,2-Dichloroethane
ND -
0.125
mg/L
25
2/14/2018 2:38:00 PM
MEK
ND
0.625
mg/L
25
2/14/2018 2:38:00 PM
Benzene
ND
0.125
mg/L
25
2/14/2018 2:38:00 PM
Carbon tetrachloride
ND
0.125
mg/L
25
2/14/2018 2:38:00 PM
Chlorobenzene
ND
0.125
mg/L
25
2/14/2018 2:38:00 PM
Chloroform
ND
0.125
mg/L
25
2114/20182:38:00 PM
Tetrachlomethene
ND
0,125
mg1L
25
2114/20182:38:00 PM
Trichloroethene
ND
0.125
mglL
25
2/14/2018 2:38:00 PM
E Value above quantitation mage
Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDfimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 27
minant Level.
H
E Value above quantitation mage
Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDfimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 27

SUMMIT
Summit Environmental Techno/WSt. Analytical Report
331010 Win S[.
"I
f-NVIRONMENTALTECHNOLOCIES, INC Cuyahoga Falls, Ohio 49223 (base report)
Analytical Lahoraiodes TEL: [phone] FAX: [phone] WO#: 18020512
Website: brm.11uni v.senek.com Date Reported: 3/5/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 2/8/2018 11:30:00 AM
Lab ID: 18020512-OOIA
Project: Lumberton WWTP
Client Sample ID Lumberton W WTP
Analyses
Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Vinyl chloride ND
Sun, 4-Bromofluorobenzene 101
Surr: Dibromofluoromethane 101
Surr: Toluene -d8 99.8
RCI -SOLID -W/ IGNITABILITY1030
REACTIVE CYANIDE (901417.3.3.2) -SOLID
Cyanide, Reactive ND
SW8260B SW7311M Analyst: MES
0.0500
mglL
25
2/14/2018 2:38:00
PM
70 -130
%Rec
25
2/14/2018 2:38:00
PM
70 -130
% Rec
25
2/14/2018 2:38:00
PM
70 - 130
% Rec
25
2/14/2018 2:38:00
PM
SW9014
Analyst:
MS
0.500 mg/Kg 1 2/15/2018 12:11:00 PM
RCI-SOLID-W/IGNITABILITY7030 SW
7030 Analyst: AJT
IGNITABILITY OF SOLIDS 15W-646: 1030)
Ignitability non-flammable 1 2/16/2018 2:00:00 PM
RCI -SOLID -W/ IGNITABILITY1030 SW9045D Analyst: DHC
PH (SW9045D)
pry 7.1 s.u.@19.7C 1 2/16/20181:51:00 PM
RCI -SOLID -W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 2/15/2018 12:11:00 PM
QualiLers: * Value exceeds Maximum Contaminant Level.
H Holding times fnr preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to deteanine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 27

Summit Envirorsmental TechnologiesinSt. QC SUMMARY REPORT
SUMMIT Jf1'' 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, 1NC Cuyahoga Falls, Ohio 44223 WO#: 18020512
rj
Rrtelyllcaf Laburelarw TEL: [phone] FAX.. [phone]
Website: kttp.11w"v.settek.com 05 -Mar -18
Client: Synagro
Proiect: Lumberton WWTP BatchED: 30838
Sample ID mb-30838 SampType: M13LK TestCode: tclp-voc-MST Units: mg/L Prep Date: 211212018 RunNo: 80629
Client ID: PBS Batch ID: 30838 TestNo: SW8260B SW1311M Analysis Date: 2/14/2018 SegNo: 1418440
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDL]mit Qua[
1,1-Dichloroethene ND 0.125
1,2-Dichloroethane ND 0.125
MEK ND 0.625
Benzene ND 0.125
Carbon tetrachloride ND 0.125
Chlorobenzene ND 0.125
Chloroform ND 0.125
Tetrachloroethene ND 0.125
Trichloroethene ND 0.125
Vinyl chloride ND 0.0500
Surr: 4-Bromofluorobenzene 1150 1250 91.7 70 130
Surr: Dibromofluoromethane 1170 1250 93.6 70 130
Surr: Toluene -d8 1270 1250 102 70 130
Sample ID Ica 20ug/L 6876/ SampType: LCS TestCode: tclp-voc-MST Units: ri Prep Date: RunNo: 80629
Client ID: LCSS Batch ID: 30838 TestNo: SW8260B SW1311M Analysis Date: 2/14/2018 SegNo: 1418443
Analyte Result PQL SPK value SPK Ref Val % REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qua]
1,1-Dichloroethene 0.0215 0.00500 0.0200 0 108 79.4 131
1,2-Dichloroethane 0.0204 0.00500 0.0200 0 102 73.6 137
MEK 0.0944 0.0250 0.100 0 94.4 55.1 163
Benzene 0.0200 0.00500 0.0200 0 99.8 73.1 132
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded I Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimmn Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 9 of 27

U'EF Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONME14TAL TECRNO LOOIES, INC Cuyahoga Falls, Ohio 44223
WO#: 18020512
An91ytical Laborsicrhe TEL: [phone] FAX. [phone]
Website.: htty://www.settekcom 05 -Mar -18
Client: Synagro
Project: Lumberton WWTP BatchED: 30838
Sample ID
Ics 20ug/L 6676/
Samp Type:
LCS
TestCode:
tclp-voc-MST Units: mglL
Prep Date:
RunNo: 80629
Client ID:
LCSS
Batch ID:
30838
TestNo:
SW8260B SW1311M
Analysis Date: 2114/2018
SegNm 1418443
Analyte
0.0191
0.00500
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.0190
0.00500
0.0200
0
94.9
63.7
139
Chlorobenzene
0.0198
0.00500
0.0200
0
98.8
72.3
139
Chloroform
0.0191
0.00500
0.0200
0
95.5
79.3
129
Tetrachloroethene
0.0203
0.00500
0.0200
0
102
56.2
187
Trichloroethene
0.0202
0.00500
0.0200
0
101
64.1
138
Vinyl chloride
0.0172
0.00200
0.0200
0
86.0
22.1
147
Surr: 4-Bromofluorobenzene
53.4
50.00
107
80.4
126
Surr: Dibromofluoromethane
47.4
50.00
94.8
70.3
125
Burr: Toluene -d8
51.3
50.00
103
82
117
QualiSers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Hlank
E
Value above quantitation range
H
Holding times far preparation or analysis exceeded
I
Analyte detected below quantitation limits
M
Manual Integrntion used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 10 of 27

.umm'l Summit Environmental Technologies,Inc. QC SUMMARY RE mns01 1
3310 Win St.
tNVIRON416NTAL TECHNOLOG7=_S1 INC Cuyahoga Falls, Ohio 44223 WO#: 18020512
ArralyL'cal Labaratar{es TEL: [phone] FAX: [phone]
Website: http //wmv.settek.eom 05 Mar48
Client: Synagro
Project: Lumberton WWTP BatchID: 30851
Sample ID MB -30851 Samp Type: MBLK TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 2/13/2016 RunNo: 80585
Client ID: PBS Batch ID: 30851 TestNo: SW6010 SW3010A Analysis Date: 2/14/2018 SegNo: 1418801
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As) ND 0.500
TCLP Barium(Ba) ND 5.00
TCLP Cadmium(Cd) ND 0.100
TCLP Chromium(Cr) ND 0.200
TCLP Lead(Pb) ND 0.500
TCLP Selenium(Se) ND 0.0500
TCLP Silver(Ag) ND 0.500
Sample ID LCS-30851 SampType: LCS TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 2113/2018 RunNo: 80585
Client ID: LCSS Batch ID: 30851 TestNo: SW6010 SW3010A Analysis Date: 2/14/2018 SegNo: 1418802
Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Rbf Val %RPD RPDUmit Qual
TCLP Arsenic(As) 2.12 0.500 2.000 0 106 80 120
TCLP Barium(Ba) ND 5.00 2.000 0 110 80 120
TCLP Cadmium(Cd) 2.07 0.100 2.000 0 103 80 120
TCLP Chromium(Cr) 2.18 0.200 2.000 0 109 80 120
TCLP Lead(Pb) 2.21 0.500 2.000 0 110 80 120
TCLP Selenium(Se) 2.19 0.0500 2.000 0 110 80 120
TCLP Silver(Ag) 2.17 0.500 2.000 0 109 80 120
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 11 of 27

UIT Summit SummitEnvironmental Technologies, � e. QC SUMMARY REPORT
"IS3310 Win St.
EmVIHONMEHTALnCHNOLOGI£S, NC Cuyahoga Falls, Ohio 44223 WO#: 16620512
Anafytic:a1 Laboratories TEL: [phone] FAX. [phone]
Website: htto://www settekeom 05-Mar48
Client: Synagro
Project: Lumberton WWTP BatchED: 30851
Sample ID 18020537-001AMS SampType: MS TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 2/13/2018 RunNo: 80585
Client ID: BatchQC Batch ID: 30851 TestNo: SW6010 SW3010A Analysis Date: 211412018 SegNo: 1418822
Analyte Result PQL SPK value SPK Ref Val % REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qua]
TCLP Arsenic(As) 2.28 0.500 2.000 0 114 70 130
TCLP Barium(Ba) ND 5.00 2.000 0.009314 104 70 130
TCLP Cadmium(Cd) 2.11 0.100 2.000 0.001106 105 70 130
TCLP Chromium(Cr) 2.09 0.200 2.000 0.004313 104 70 130
TCLP Lead(Pb) 2.05 0.500 2.000 0 102 70 130
TCLP Selenium(Se) 2.30 0.0500 2.000 0 115 70 130
TCLP Silver(Ag) 2.24 0.500 2.000 0 112 70 130
TCLP
Arsenic(As)
2.31
0.500
2.000
0
116
70
130
2.276
1.55
Sample ID
Client ID:
Analyte
18020537.001AMSD
BatchQC
SampType:
Batch ID:
MSD
30851
Result
TestCode:
TestNo:
PQL
Mtl-TCLP-7(6
SW6010
SPK value
Units: mg lL
SW3010A
SPK Ref Val
Prep Date: 2/13/2018
Analysis Date: 2/14/2018
% REC LowLimit HighLimit RPD Ref Val
RunNo: 60585
SegNo: 1418823
%RPD RPDLimit Qua]
TCLP
Arsenic(As)
2.31
0.500
2.000
0
116
70
130
2.276
1.55
2u
TCLP
Barium(Ba)
ND
5.00
2.000 0.009314
105
70
130
0
0
20
TCLP
Cadmium(Cd)
2.13
0.100
2.000 0.001106
106
70
130
2.110
0.826
20
TCLP
Chromium(Cr)
2.10
0.200
2.000 0.004313
105
70
130
2.088
0.743
20
TCLP
Lead(Pb)
2.07
0.500
2.000
0
104
70
130
2.045
1.40
20
TCLP
Selenium(Se)
2.34
0.0500
2.000
0
117
70
130
2.304
1.46
20
TCLP
Silver(Ag)
2.25
0.500
2.000
0
113
70
130
2.240
0.510
20
Qualifiers: '
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
H
Holding times for prepazation or analysis exceeded
I
Analyte detected below quantitation limits
MO
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 27

Suinmit Environmental Technologies, Inc. QC SUMMARY REPORT
ffISUMMINt 3310 Wm S[.
UCVIBON MENTAL TE.CMMO LOG'IES, IMC Cuyahoga Falls, Ohio 44223 WO#: 18020512
A+talyllcaf Laboratories TEL: [phone] FAX. [phone]
Website: him 1Avww.settekcom 05-Mar-18
Client: Synagro
Project: Lumberton WWTP BatchlD: 30856
iCLP Mercury
associated Method Blank
H
Holding times for preparation or analysis
RunNo: 80594
mple ID
MB -30856
SampType:
MBLK
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 2/13/2018
RunNo: 80594
ant ID:
PBS
Batch ID:
30856
TestNo:
SW7470A SW7470A
Analysis Date: 2/14/2018
SegNo: 1417316
ialyte
30856
TestNo:
Result
PQL
SPK value SPK Ref Val
% REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
ND 0.00200
iCLP Mercury
associated Method Blank
H
Holding times for preparation or analysis
RunNo: 80594
imple ID
18020537-001AMSD
SampType:
imple ID
LCS-30856
SampType:
LCS
TestCode:
HG_TCLP(74
Batch ID:
Units: PPM
Prep
Date: 2/13/2018
RunNo: 80594
ent ID:
LCSS
Batch ID:
30856
TestNo:
SW7470A
SW7470A
Analysis
Date: 2/14/2018
SegNo: 1417318
ialyte
Result
PQL
SPK
value SPK Ref Val
% REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
0.00403 0.00200 0.00400 0 101 80 120
TCLP Mercury
associated Method Blank
H
Holding times for preparation or analysis
RunNo: 80594
imple ID
18020537-001AMSD
SampType:
imple ID
18020537-001AMS
SampType:
MS
TestCotle:
HG_TCLP(74
Batch ID:
Units: PPM
Prep
Date: 2113/2018
RunNo: 80594
Lent ID:
BatchQC
Batch ID:
30856
TestNo:
SW7470A
SW7470A
Analysis
Date: 2/14/2018
SegNo: 1417336
ialyte
Result
PQL
SPK
value SPK Ref Val
% REC LowLimit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
0.00440 0.00200 0.00400 0 110 75 125
3LP Mercury 0.00465 0.00200 0.00400 0 11ti lb
associated Method Blank
H
Holding times for preparation or analysis
RunNo: 80594
imple ID
18020537-001AMSD
SampType:
MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 211 312 01 8
Lent ID:
BatchQC
Batch ID:
30856
TestNo:
SW7470A SW7470A
Analysis Date: 2/1412018
SegNo: 1417337
talyte
Result
PQL
SPK value SPK Ref Val
% REC Lowl-iiit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
¢o u.uua4u oar ae
Qualifiers: * Value exceeds Maximum Contazninant Level. B Analyte detected in the
E Value above quantitation range
exceeded S Analyte detected below quantitation limits M Manual Integrntion used to determine
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 27
associated Method Blank
H
Holding times for preparation or analysis
¢o u.uua4u oar ae
Qualifiers: * Value exceeds Maximum Contazninant Level. B Analyte detected in the
E Value above quantitation range
exceeded S Analyte detected below quantitation limits M Manual Integrntion used to determine
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 27

u'.'L Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
�VIRONRIEBJTALTFCHt10L001FS,]KC Cuyahoga Falls, Ohio 44223 WO#: 18020512
A+talyticaf Labaralorie TEL: [phone] FAX. [phone]
Website: htto11wivw.seaekcom11wivw.settekcom 05 -Mar -18
Client: Synagro
Project: Lumberton WWTP BatchID: 30856
Qua]ifiers: ' Value exceeds Maximum Conturrinant Level. B Analyte detected m the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 27
Sample ID
18020537-001AMSD
SampType:
MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 211 312 01 8
RunNo: 80594
Client ID:
BatchQC
Batch ID:
30856
TestNo:
SW7470A SW7470A
Analysis Date: 2 /1 412 01 8
SegNo: 1417337
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Qua]ifiers: ' Value exceeds Maximum Conturrinant Level. B Analyte detected m the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 27

summly Summit Environmental Tech no
3310 Win St.
Inc.ff1t. QC SUMMARY REPORT
3310
ENVIRONIMNTALTECHN4LOG4ES, MC Cuyahoga Falls, Ohio 44223
WO#: 18020512
Arrslytfcal Laboralorms TEL: [phone] FAX. [phone]
Website: htta://www.settek.com 05-Mar-18
Client: Synagro
Project: Lumberton WWTP BatchID: 30562
Chlortlane, total
ND
0.0100
Toxaphene
ND
0.0200
Endrin
ND
RunNo: 80750
Sample ID
mb-30862
SampType:
mblk
TestCode:
tclp-svoc-cpe
Units: mg/L
Prep Date: 2/14/2018
Client ID:
PBS
Batch ID:
30862
TestNo:
SW8081A
SW3510C
Analysis Date: 2/17/2018
SegNo: 1422483
Analyte
0.0100
0
Result
PQL
SPK value
SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
Chlortlane, total
ND
0.0100
Toxaphene
ND
0.0200
Endrin
ND
0.00100
gamma -BHC
ND
0.00100
Heptachlor
ND
0.00100
Heptachlor epoxide
ND
0.00100
Methoxychlor
ND
0.00100
Surr: TCMX
20.4
SW3510C
Surr. DCB
21.1
4nalyte
20.00
0.00759
102
10
119
20.00
20
106
10
119
Endrin
0.00759
0.00100
0.0100
0
75.9
20
157
RunNo: 80750
'>ample ID
Ics-30862
SampType:
Ics
TestCoda
tclp-svoc-cpe
Units: mg/L
Prep Date: 2/14/2018
Client ID:
LCSS
Batch ID:
30862
TestNo:
SW8081A
SW3510C
Analysis Date: 2/17/2018
SegNo: 1422484
4nalyte
0.0100
0
Result
PQL
SPK value
SPK Ref Val
% REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qual
Endrin
0.00759
0.00100
0.0100
0
75.9
20
157
gBHC
amma-
0.00654
000100
.
0.0100
0
65.4
22
137
Heptachlor
0.00691
0.00100
0.0100
0
69.1
24
121
Heptachlor epoxide
0.00734
0.00100
0.0100
0
73.4
27
152
Methoxychlor
0.00890
0.00100
0.0100
0
89.0
10
199
Surr: TCMX
14.3
20.00
71.3
10
119
Surr: DCB
12.5
20.00
62.4
10
119
Qualifiers: ' Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater thanRSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 27

U '.T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffIS3310 Win St.
ENVIRONMENTAL TECHUOLOOIES, INC Cuyahoga Falls, Ohio 44223 WO#: 18020512
Anelyllcal 4. bofstorles TEL: [phone] FAX [phone]
Website: httv://www.settekcom 05-Mar-18
Client: Synagro
Project: Lumberton WWTP BatchID: 30862
Sample ID 18020406-001ams SampType: ms TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 2/14/2018 RunNo: 80750
Tient ID: BatchQC Batch ID: 30862 TestNo: SW8081A SW3510C Analysis Date: 211 712 01 8 SegNo: 1422485
4nalyte Result PQL SPK value SPK Ref Val % REC LowUrnit HighLimit RPD Ref Val % RPD RPDLimit Qual
Endrin 0.0115 0.00200 0.0100 0 115 zu ur
gamma -BHC 0.0105 0.00200 0.0100 0 105 22 137
Heptachlor 0.00984 0.00200 a0100 0 98.4 24 121
Heptachlor epoxide 0.0113 0.00200 0.0100 0 113 27 152 QMR
Methoxychlor 0.0118 0.00200 0.0100 0 118 10 199 m
Surr: TCMX 20.1 20.00 100 10 119
Surr: DCB 16.2 20.00 81.2 10 119
Sample ID 18020406-001amsd SampType: msd TestCode: tclpsvcc-cpe Units: mg/L Prep Date: 211 412 01 8 RunNo: 80750
Client ID: BatchQC Batch ID: 30862 TestNo: SW8081A SW3510C Analysis Date: 211 712 01 8 SegNo: 1422486
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDLimit Qual
Endrin 0.00911 0.00200 0.0100 0 91.1 20 157 0.0115 22.9 30
gamma -BHC 0.00805 0.00200 0.0100 0 80.5 22 137 0.0105 26.0 30
Heptachlor 0.00741 0.00200 0.0100 0 74.1 24 121 0.00984 28.1 30
Heptachlor epoxide 0.00828 0.00200 0.0100 0 82.8 27 152 0.0113 31.2 30 Rm
Methoxychlor 0.00910 0.00200 0.0100 0 91.0 10 199 0.0118 26.2 30 m
Sur: TCMX 15.4 20.00 77.1 10 119 0
Surr: DCB 12.1 20.00 60.5 10 119 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 16 of 27

U' •r Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffIS33/0 Win St.
ENVIRON WNTAL TECHtAO LO04ES, 1KC Cuyahoga Falls, Ohio 44223
WO#: 18020512
Anelyrfcal LxbWalciiew TEL: [phone] FAX. [phone]
Website: hap 11www.settekcom 05-Mar-18
Client: Synagro
Project: Lumberton WWTP BatchID: 30863
1,4 -Dichlorobenzene
ND
0.0400
2,4,5 -Trichlorophenol
ND
0.100
2,4,6 -Trichlorophenol
RunNm 80687
Sample ID
MB40863
SampType:
MBLK
TestCode:
SVOC-BNA_T Units: mg/L
Prep Date: 211 412 01 8
Client ID:
PBS
Batch ID:
30863
TestNo:
SW8270C SW3510C
Analysis Date: 211 512 01 8
SegNo: 1420135
Analyte
Hexachlorobenzene
ND
Result
PQL
SPK value SPK Ref Val
% REC LowUmit Highl-imit RPD Ref Val
% RPD RPDUmit Qual
1,4 -Dichlorobenzene
ND
0.0400
2,4,5 -Trichlorophenol
ND
0.100
2,4,6 -Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
o -Cresol
ND
0.100
m/p-Cresol(s)
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Sum: 2-Fluorophenol
0.478
Surr Phenol -d6
0.232
Sum: Nitrobenzene -d5
0.853
Sum: 2,4,6 -Tri brom ophenol
0.550
Sum: 2 -Fluoro biphenyl
0.815
Sum: p-Terphenyl-d14
1.01
1.000
Value exceeds Maximum Contaminant Level
47.8
10
109
1.000
H
23.2
10
109
1.000
Manual Integration used to determine
85.3
19
120
1.000
O
55.0
10
120
1.000
Permit Limit
81.5
22
117
1.000
101
34
116
Qualifiers: *
Value exceeds Maximum Contaminant Level
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDImut
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
QC+
Original
Page 17 of 27

'� Summit Environmental Technolo0WiInc.nSt. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 18020512
Analybiwf Laboratories TEL: [phone] FAX [phone]
OS -Mar -18
Website: htty llwww settekeom
Client: Synagro
Pra;ert Lumberton WWTP BatehlD: 30863
Sample ID LCS-30863 SampType: LCS TeSLCode: SVOC-BNA_T Units: mg/L Prep Date: 2114/2018 RunNo: 80687
Client ID: LCSS Batch ID: 30863 TestNo: SW8270C SW3510C Analysis Date: 211 512 01 8 SegNo: 1420136
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDLimit Qua[
1,4 -Dichlorobenzene 0.480 0.0400 0.8000 u ou.0 La. 1 ;Z
u
2,4,5 -Trichlorophenol 0.549 0.100 0.8000 0 68.6 11.7 151
2,4,6 -Trichlorophenol 0.547 0.100 0.8000 0 68.3 12.4 150
2,4-Dinitrotoluene 0.545 0.0200 0.8000 0 68.2 20.6 140
o -Cresol 0.517 0.100 0.8000 0 64.6 13.8 137
m/p-Cresol(s) 0.518 0.100 0.8000 0 64.7 10 134
Cresols, Total ND 2.00 1.600 0 64.7 10 129
Hexachloro-1,3-butadiene 0.451 0.00800 0.8000 0 56.4 14.7 137
Hexachlorobenzene 0.506 0.0200 0.8000 0 63.3 12 139
Hexachloroethane 0.480 0.0400 0.8000 0 60.1 14.8 132
Nitrobenzene 0.558 0.0400 0.8000 0 69.8 15.6 138
Pentachlorophenol 0.476 0.100 0.8000 0 59.5 10 156
Pyridine 0.265 0.100 0.8000 0 33.1 1 130 QC+
Surr: 2-Fluorophenol 0.411 1.000 41.1 10 147
Surr: Phenol -d6 0.192 1.000 19.2 10 140
Surr: Nitrobenzene -d5 0.696 1.000 69.6 10 169
Surr 2,4,6-Tribromophenol 0.456 1.000 45.6 10 185
Surr: 2-Fluorobiphenyl 0.621 1.000 62.1 10 169
Surr: p-Terphenyl-d14 0.769 1.000 76.9 10 179
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 27

Vi t•r Summit Environmental Technologies, Inc. QC SUMMARY REPORT
PF s33/0 Win St.
LIVIRONMENTALTECHIJOLOGIES7114C Cuyahoga Falls, Ohio 44223 WO#: 18020512
Arralytica! ra47rarorles TEL: [phone] FAX [phone]-Mar-18
Website http://www.settekcom
Client: Synagro
V.. I'o,.r- T.nmherfon WWTP BatchID: 30956
Sample ID mb-30956 SampType: mblk TestCode: tclp-svoc-her Units: mg/L Prep Date: 211 912 01 8 RunNo: 80937
:tient ID: PBS Batch ID: 30956 TestNo: SW8151A SW8151A Analysis Date: 2/21/2018 SegNo: 1428106
4nalyte Result PQL SPK value SPK Ref Val %REC LOWUrnit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 1.00 u
214,5 -TP ND 0.500 0 0 d
Surr: DCAA 440 500.0 88.0 20 140
Sample ID Ics-30956 SampType: lcs TestCode: tclp-svoc-her Units: mg/L Prep Date: 211 912 01 8 RunNo: 80937
Client ID: LCSS Batch ID: 30956 TestNo: SW8151A SW8151A Analysis Date: 2/21/2018 SegNo: 1428107
Analyte Result - PQL SPK value SPK Ref Val %REC LoWLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
24-D ND 1.00 0.500 0 88.7 62.6 125
2,4,5 -TP ND 0.500 0.500 0 85.2 52.5 128
Surr: DCAA 444 500.0 88.9 20 140
Qualifiers: * Value exceeds Maximmn Contaminant Level. H Analyte detected in the associated Method Blank
H Holding times for Prepazation or analysis exceeded I Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 27

MISUMMIEF
Summit Environmental Technologies, lnc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TSCHNOLOGIES,AC Cuyahoga Falls, Ohio 44223 WO#: 18020512
Analyllcdl Laba+Blarnw TEL: [phone] FAX [phone]
Website: htW hivww settek Com OS -Mar -l8
Client: Synagro
PrniPvr, Lumberton WWTP BatchID: 30956
sample ID 18020408-001ams SampType: ms TestCode: tc-svoc-her Units: mglL Prep Date: 2/19/2018 SegNo: 81049
Tient ID: BatchQC Batch ID: 30956 TestNo: SW8151A SW8151A Analysis Date: 212 412 01 8 SegNo: 1433337
analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDLimit Qua[
214-D ND 11.3 u.ouu u a».7 31 j
��
2,475 -TP ND 11.3 0.500 0 90.8 38 100
Surr: 2,4-Dichlorophenylacetic acid 459 500.0 91.7 20 140
Sample ID 18020408-001amsd SampType: mad TestCode: tclp-svoc-her Units: mg/L Prep Date: 211 912 01 8 RunNo: 81049
;lient ID: BatchQC Batch ID: 30956 TestNo: SW8151A SW8151A Analysis Date: 212 412 01 8 SegNo: 1433338
analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
n in
2,4-D ND 11.3 u.ouu u ;.,.i �L
-- -
ND 11.3 0.500 0 87.9 38 106 0 0 30
2,4,5 -TP
Surr: 2,4-Dich[orophenylacetic acid 444 500.0 85.7 20 140 0 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 20 of 27

V 1 Summit EnviraameataiTeehnal10WSt. QC SUMMARY REPORT
MMOU 3310 Win St.
ENVIRONM04TALT6CHN4LQalESrMC Cuyahoga Falls, Ohio 44223 WO#: 18020512
Anuryllcal Lvboralorie TEL. [phone] FAX. [phone]
OS -Mar -l8
Website: htta 11www settekcom
Client: Synagro
n...;o,.♦• T,nmhertnn WWTP BatchID: R80692
Sample ID MB -R80692 SampType: MBLK TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 80692
:Tient ID:PBS Batch ID: R80692 TestNo: SW9014 Analysis Date: 211 512 01 8 SegNo: 1420299
analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
iample ID LCS-R80692 SampType: LCS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 80692
Nent ID: LCSS Batch ID: R80692 TestNo: SW9014 Analysis Date: 2/15/2018 SegNo: 1420301
analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
AAn
Cyanide, Reactive 10.4 0.500 1u.uu u ;6+ W
�
iample ID 18020660.001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 80692
;lient ID: Batch= Batch ID: R80692 TestNo: SW9014 Analysis Date: 211 512 01 8 SegNo: 1420309
\nalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qua[
Cyanide, Reactive
9.86 0.500 lu.ull u uu.0 W L.�
Sample ID 18020660-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: /K Prep
Prep Date: RunNo: 80692
Client ID: Batch= Batch ID: R80692 TestNo: SW9014 Analysis Date: 211512018 SegNo: 1420311
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qua[
Cyanide, Reactive 9.96 0.500 10.00 0 99.6 81.6 122 9.860 0.979 5
Qualifiers:
* Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDIimit
P Second colmnn continuation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 21 of 27

U 1 1� Summit Environmental Technologies.Inc. QC SUMMARY l�EPQA1
MIS3310 Win St.
ENVIRON 1d ENTAL T6.CHN0 LOnIES, INC Cuyahoga Falls, Ohio 44223 WOO: 18020512
ArWlytroal LaborafrarAW TEL: [phone] FAX. [phone]
Website: htta://wwwsettekcom 05 -Mar -18
Client: Synagro
Project: Lumberton WWTP BatchID: R80692
Qual�ers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Hlank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Malyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 27
RunNo: 80692
Sample ID 18020660-001AMSD
SampType:
MSD
TestCode:
Cyanide,Rea Units: mg/Kg
Prep Date:
Client ID: BatchQC
Batch ID:
R80692
TestNo:
SW9014
Analysis Date: 2/15/2018
SegNo: 1420311
Analyte
Result
PQL
SPK value SPK Ref Val
%REG LowUmit HighUrr it RPD Ref Val
% RPD RPDLimit Qua]
Qual�ers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Hlank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Malyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 27

Summit SummitEnvironmerstalTechnologies,Inc. QC SUMMARY 1\L'POR1
3310 Win St.
ENVIRONIAENTAL TECHNOLOGIES, NC Cuyahoga Falls, Ohio 44223 WO#: 18020512
ArtalyUW1 Laboratories TEL: [phone] FAX [phone]
Website: hUv.11www.serekcom//www.seUekcom 05 -Mar -18
Client: Synagro
Project: Lumberton WWTP BatchID: R80694
Sulfide, Reactive
ND 25.0
e associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
mple ID
MB -R80694
SampType:
MBLK
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 80694
ent ID:
PBS
Batch ID:
R80694
TestNo:
SW9034
Analysis Date: 2/15/2018
SegNo: 1420454
alyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qual
Sulfide, Reactive
ND 25.0
Sulfide, Reactive
4620 25.0 4800 0 96.2 85 115
Sulfide, React
e associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
mple ID
LCS-RB0694
SampType:
LCS
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 80694
ent ID:
LCSS
Batch ID:
R80694
TestNo:
SW9034
Analysis Date: 2/1 512 01 8
SegNo: 1420455
alyte
Result
PQL
SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4620 25.0 4800 0 96.2 85 115
Sulfide, React
e associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
mple ID
18020660-001AMS
SampType:
MS
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 80694
ent ID:
BatchQC
Batch ID:
R80694
TestNo:
SW9034
Analysis Date: 2/15/2018
SegNo: 1420463
alyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
% RPD RPDLimit Qua[
ive
4720 25.0 4800 30.00 97.7 8U 12u
mple ID 18020660.001AMSD SampType: MSD TestCode: Sulfide
Sulfide, Reactive 4560 25.0 4800 30.00 94.4 8u ¢u wl<u 0.40 33
e associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Units: mg/Kg
Prep Date:
RunNo: 80694
ent ID:
BatchQC
Batch ID:
R80694
TestNo:
SW9034
Analysis Date: 211 512 01 8
SegNo: 1420464
alyte
Result
PQL
SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
% RPD RPDLimit Qual
E Value above quantitation range
M Manual Sategrntion used to determine
e associated Method Blank
H
Holding times for preparation or analysis exceeded
I
Analyte detected below quantitation limits
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column omfr ation exceeds
PL
Permit Limit
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in th
'
O RSD is greater than RSDhmit Original
R RPD outside accepted recovery limits
Page 23 of 27

u'!ll Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Wm St.
ENVIRON 1dENTAL TECHHO LOG U81 ,INC Cuyahoga Falls, Ohio 44223 WO#: 15020512
An®iyllcal L�bnrslerie TEL [phone] FAX [phone]
Website: htta //w w settekcom OS -Mar -18
Client: Synagro
Project: Lumberton WWTP BatchID: R80694
Sample ID
18020660.001AMSD
SampType:
MSD
TestCode:
Sulfide,React
Units:
mg/Kg
Client ID:
BatchQC
Batch ID:
R80694
TestNo:
SW9034
Result PQL SPK value SPK Ref Val
Prep Date: RunNo: 80694
Analysis Date: 211 512 01 8 SegNo: 1420464
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[
Qual�ers: � Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integrntion used to determine
MC Value is below Minimum Compound limit ND Not Detected O RSD is greater thanRSDImut
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 24 of 27

� '� Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ff 3310 Win St.
ENVIRONMENTALTECHNOL00l£$; INC Cuyahoga Falls, Ohio 44223 WO#: 18020512
Analytical;aborstoni TEL: [phone] FAX [phone]
OS-Mar-18
Website: htto//www settekcom
Client: Synagro
Prniert Lumberton WWTP BatchID: R80715
Sample ID LCS-R80715 SampType: LCS TestCode: Ignitability_S Units: Prep Date: RunNo: 80715
Client ID: LCSS Batch ID: R80715 TestNo: SW1030 Analysis Date: 2/16/2018 SegNo: 1420935
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDL]mit Qua]
Ignitability 7.51 7.240 u Iun to
Sample ID 18020512-001ADUP SampType: DLP TestCode: Ignitability_S Units: Prep Date: RunNo: 80715
;lient ID: Lumberton WWTP Batch ID: R80715 TestNo: SW1030 Analysis Date: 211 612 01 8 SegNo: 1420937
lnalyte Result PQL SPK value SPK Ref Val % REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qual
Ignitability non-flammable
R
iample ID 18020513-001ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: un on 60715
Tient ID: BatchQC Batch ID: R80715 TestNo: SW1030 Analysis Date: 211 612 01 8 SegNo: 1420940
Malyte Result PQL SPK value SPK Ref Val % REC LowLimit HighLimit RPD Ref Val % RPD RPDLimit Qual
Ignitability non-fl
ammable
Qualifiers: * Value exceeds Maximum Contaminant Level. H Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integation used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 25 of 27

SUMMIT Summit Environmental Technolo0 WinInc.
St. QC SUMMARY REPORT
ELMOU 3310 Win St. `G
ENVIRONMENTAL TECHNOLOGIES, ]INC Cuyahoga Falls, Ohio 44223 WO#: 18020512
A4a1ydcal Laboraierie TEL. [phone] FAX. [phone]
Website.: http://www.settek com OS -Mar -18
Client: SynagrO
n...:onr- T.nmhertnn WWTP BatchID: R80717
sample ID LCS-RB0717 SampType: LCS TestCode: pH_Oil(9045 Units: s.u.@20.8C Prep Date: RunNo: 80717
:tient ID: LCSW Batch ID: R80717 TestNo: SW9045D Analysis Date: 211 612 01 8 SegNo: 1420941
lnalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[
pH
7.0 t.0 u iw ..,, ,,,,
lample ID 18020645-001ADUP SampType: DUP TestCode: pH_011(9045 Units: s.u.@19.7C Prep Date: RunNo: 80717
:lient ID: Batch= Batch ID: R30717 TestNo: SW9045D Analysis Date: 211 612 01 8 SegNo: 1420943
>na[yte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[
<a n to
H
5.5 u u
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding tunes for preparation or analysis exceeded 7 Analyte deterred below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confmnation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 26 of 27

Summit Environmental Technologies, Inc. Analysts RequestlChBin of Custody
331-0 Win Stnet For Summit Environmental Technologies. Inc uw only
Cuyahaga Falk, Ohio 44223 Tch 330 253.8211- Fax: [phone] Yage_of� SET Nta
npnny N+rme (PICy a PnoO
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Page 27 of 27

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number: W00000672
W WTP Name: City of Lumberton W WTP NPDES Number: NCO024571
Monitoring Period: From 01/01/18 To 03/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Option/AIt.4 -
(vS reduction)
(40 -day bench)
Excee-
of
Type
Technique
Option/Alt. 7
Option/Alt. 8
Minimum Geo. Mean Maximum Units
dences
Analysis
(Drying—Unstable)
Option/Alt. 9
Fecal
2x10 to the 61"
NTN
(hijection)
(Incorporation)
No vector attraction reduction
MPN/g
Coliform
power per gram
of total solids
35100
47980
71900
CFU/g
0
quarterly
grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction
(40 CFR 503.33/15A NCAC 02T.1107)
-Please indicate option/alternative
performed:
0fron/Alt. I
Option/Alt.2
Option/Alt. 3
Option/AIt.4 -
(vS reduction)
(40 -day bench)
(30 -day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying—Stable)
(Drying—Unstable)
Option/Alt. 9
Option/Alt. 10
(hijection)
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T. ] 106 an
d the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met "
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T. 1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have not been met" (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that thepathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Walton W WTP Operator
Preparer Name and Title (type or print)
�
Land Applier Name and Title (if applicable) (type or print)
%4�ie�61 4
Signature of Preparer* Date
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T.1102 (26)
d Applier (if applicable)
Signature of Lan
Date

Cameron Testing Services, Inc, Laboratory Report NC VENR*054
Na PHHS #377%
US EPA ANCO191
Oio tr, .t Synagro ��GT 6PJjf 180240
fit" Lumberton t#rJ Yes
Sample Information
suhlPieu N. Rath Rt a"` 02/08/18 '= J. Zubeek o�te';I 02/08118
�'
Analyses and Results
180240 -1 ;ua� Gr Fea.Colifartn-S 37240 CYure 37299 OF108f76 S8 szzzp-MF
-2 <35800 CFaie 35809
-3 35100 MOO 35100
4 71900 Crura 36000
-5 70200 CFUm 35100
=6 35300 Crm 35344
4• 69900 enure 35000
Geomean .47984
`180240 -1 >AWN Gr TS N 2,69% out p?109118 56 2540 G "T5
-2 2.70% oat
-3 2.85% aot
4 2.780A e.a1
-5 2:85% 0,61
2.83% a.ai
7
2,86% 0 a1
Report
Review�7%p
Project Manager Date
'S19 S: Stale Sit. 4141ti6-d?a6
'$a;�fnd.NC 77330 ehrisr cnmcmnlesting.cnm-

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City Of Lumberton
Environmental Laboratory
Speciric Oxygen Uptake Rate I Worksheet
Date &Analyst: 419!98 9 57;am KCL Dige.%r r, AI, DLly
Total Solids
Sample volume used for to solids Is 25 mL
Weight of dish: 1-8 1 A: g
Weight of dish + dried solids: 1'125x7g
Weight of dried solids: 0.47 g
Total Solids: 18.638 g/L
SOUR
Time
Temperature
Dissolved
(Minutes)
Oxygen (mg/L)
°C
1
A 9+Ilk94D
'L3iA9',
kms"� 9 .;QOM`
r. V F
9f9 a4=;
2
31�s
5
6
7
8
x�f40Q aKy a3f d;
Qq Ilk
Ilk, 9 T r
ti4 -r,� ;i Q S`§�iS
rIlk I
14WWO Rk
I-r`s x 94.-O.Q r'ra ...34;.= a,' ,.,d* '8-.�bBM -
n;t'QQSX �8e60
g
113
12
13
14r.,4eA,0
15,140,0
h
r -n j
.se§D
is �r $,A.3 r
Oxygen Consumption Rate
SOUR Temperature Correction
0.07 mg/
SOURLlminute
0.23 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
13.625
Fsewage sludge is> 20°C, SOUR= (mglg)/hr
If sewage sludge is <20°C, SOUR = (mg/g)/hr
SOUR passes if result is _< 1
.5 (mglg)hr
Version 1111!11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rata (SOURI Worksheet
Date &Analyst: 41,10/1 B :$ $4afn r 'ISGL e ,,,419
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
mL
9
9
g/L
Oxygen Consumption Rate 0.09
SOUR
SOUR Temperature Correction
mg/L/minute
(mglg)/hr
Average Sewage Sludge
Temperature During Test
°C
14
If sewage sludge is > 20°C, SOUR =MQ
(mg/g)lhr
If sewage sludge is < 20°C, SOUR =(mglg)/hr
SPUR passes if result is <_ 1.5 (mgig)hr
Version 91/1/11

City of Lumberton
Environmental Laboratory
Specific Oxyoen Uptake Rate (SOURI Worksheet
Dake &Analyst:41;11198 8 54.am. :KCL Qigester#
Total Solids
Sample volume used for total solids test: 40 mL
Welght of dish: ` 1 9
Weight of dish + dried solids: ;95;112 9
Weight of dried solids:0.18 g
Total Solids: 18,08 g/L
SOUR
Time
Temperature
Dissolved
(Minutes)
oC
Oxygen (mMg
p
14 04>F rn B 26;
s 14 UO rra 8x21
7/l�
Pi r
�u1S'Q0 ?a r7k3.8fl.
15 00.' 7 85
%1,5
X 15:44 i 6.87 t
3
5
7�t4,90k
10L.
11
12
13
14
15
Oxygen Consumption Rate
0.10 mg
SOUR
SOUR Temperature Correction
/L/minute
0.33 (mg(g)/hr
Average Sewage Sludge
Temperature During Test
°C
14.5
If sewage sludge is > 20°C, SOUR = Q(mg/g)/hr
If sewage sludge is < 201 SOUR 01 (mg/g)/hr
SOUR passes if result is <_'f.5 (mglg)hr
Version 11/1/11

City of Lumberton
n~vironmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4/.12/78;°t08am .'KCL Il.geskarlkh-,R1Y�'.
Total Solids
Sample volume used for total solids test:
Weight of dish:lm6, g
Weight of dish + dried solids: W, .. g -z 1i5'; g
Weight of dried Solids: 0.19 g
Total Solids: 19.09 g/L
SOUR
Time
Temperature Dissolved
(Minutes)
oC Oxygen (mg/L)
0
18 OQ,ti mss: x 8 27sl
2
I's{
y 314 D4.�7 a
3u:r74:Q9,�a
4
590.
6
LL
3�7
LOQ,tn Y,()7ur�'
(5A0, G 94
10
11
12'75004
13
14
15
-1c5,;qc5,; r im
Oxygen Consumption Rate
0.09 mg
SOUR
SOUR Temperature Correction
/L/minute
0..28 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
14.25
=— -
If sewage sludge is > 20°C, SOUR = % _(mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 11/1('11

City of Lumberton
Environmental Laboratory
Speciric Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:h13/16 $`d2am ICS ' R.ges$r 2:. ,!]ay 5 •. c
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
mL
9
9
g/L
Oxygen Consumption Rate 0.09
SOUR
SOUR Temperature Correction
0.29
mg/L/minute
(mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
15.3125
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 1111/11

City OT Lumberton
environmental Laboratory
Specific Oxygen Uptake Rate (SOURI Worksheet
Date & Analyst: 4/16118 ; 817am .cISCI "; pigesteri# 2 DaY s'=
Total solids
Sample volume used for total solids test: 70 mL
Weight of dish: 925.75; g
Weight of dish + dried solids: ;125.,-`95 g
Weight of dried solids: 0,19 g
Tota! Solids: 19.5 g/L
SOUR
Oxygen Consumption Rate 0.07
SOUR
SOUR Temperature Correction
mg/L/minute
(mglg)/hr
Average Sewage Sludge
Temperature During Test
°C
19
If sewage sludge is> 20°C, SOUR = &z2 0I(mglg)/hr
If sewage Sludge is < 20°C, SOUR = " (mg/g)lhr
SOUR passes if result is <_ 1.5 (mglg)hr
Verion
41/1/1 I

City Of Lumberton
Environmental Laboratory
Specific Oxvaen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4197118 BMam >KCL Digester.# 2 'l]ay 7.
Total Solids
Sample volume used Far total solids test: 10 mL
Weight of dish: 121.96, g
Weight of dish + dried solids: "t22:95 9
Weight of dried solids: 0.19 g
Total Solids: I 19,51g/(-
SOUR
9.5 g/L
SOUR 0.15 (mg/g)!hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15.075
If sewage sludge is > 20°C, SOUR
F sewage sludge is < 20°C, SOUR = bo2q (mg/g)!hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 'I Ill/ I'I

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number: W00000672
WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571
Monitoring Period: From 04/01/18 To 06/30/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
u n ucau.e w aue...a...o �...,....�.. .,.a00 �
Vector Att
Sludge
,...,....... .. ....... .........._ _.._._....-
Pathogen Density
No. of
Frequency
Sample
Analytical
Pazameter
Allowable Leve] in
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10 to the 611
WN
MPN/g
Coliform
power per gram
of total solids
41800
47100
84000
CFU/g
0
quarterly
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MEN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
Please indicate option/alternative performed:
n/Alt. 4
Option/Alt 1 Option/Alt 2
(VS reduction) (40 -day bench)
Option/Alt. 5 Option/Alt. 6
(14 -Day Aerobic) (Alk Stabilization)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation)
Option/Alt. 3 OP
(30 -day bench) (Spec. 02 uptake) X
Option/Alt. 7 Option/Alt. 8
(Drying—Stable) (Drying—Unstable)
No vector att
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in
raction reduction alternatives were performed
40 CFR 503.33/I SA NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Walton WWTP Operator
Prepazer Name and Title (type or print) Land Applier Name an
d Title (if applicable) (type or print)
/ ��
Signature ofPreparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
s
Synagro
, EA
Lumberton WWTP
Sample Information
IME� 05/23118 ' w
e _.
Analyses and Results
NC DENR#654
NC PHHS #37799
115 EPA#NC01916
780862
Yes
J. Zubeck <<� 05/23/18
180862 -1 suwee Gr Fec. Coflform-S 8400D cPufg 42000 05123!16 SB 9222D -MF
-2 <42200 cFurg 42200
-3 43500 cruig 43500
-4 <41800 cFurg 41800
-5 43900 GFwO 43900
-6 <42600 cFUlo 42600
4 <42600 cFwg 42600
Geomean 47100
180862 -1 =mag( Gr TS (%) 2.38% 0101 05123116 SB 2540 G -TS
.2 2.37% 0.01
-3 2.30% 0.01
4 2.39% 0.01
-5 2.28% 0.01
-6 2.35% 0.01
_7 2.35% 0.01
Report D�/ 9Li�l
ReviewProject Manager - - Date
X14 S. Steele Str.
Sanford NC 27330
919-208340
ohris(rl�came[ontesting.0om

219 S. Steelestr. Cameron Testing Services, Inc. Chain of Custofly
Sanford, NC 27330 Nc Wwrr;W Cert. #854 NC PHHS Cert# 37799 US EPA NC01918 Page ../.. Of
Rush work will require prior approval. Additional charges will apply

City of Lumberton
Environmental Laboratory
Specific Oxynen Uptake Rate (SOUR) Worksheet
bate
&
Analyst
3 F i l �?8i
81 -ga 1:-
v;
0
wsWCa gl(OQ,_$
' d8�m(
sf's
22`
;(N�
3
4
70a Ilal
r1S8
do-, ppq _0 a0zj
dLLLL I- dol rrrrrr
qaar�4
-q
111'
rdo
&
I mo. k .. QO M 1 dt58 f z u's;
r,:'`I
13
Total Solids
Sample volume used for total solids test
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
V• .
`may(-51ur.a .i .
D.17
17.31
mL
9
9
g!L
Time
Temperature
Dissolved
(Minutes)
00
Oxygen (mg/L)
0
wsWCa gl(OQ,_$
ied519 Ty�yi
1
22`
3
4
70a Ilal
r1S8
do-, ppq _0 a0zj
dLLLL I- dol rrrrrr
7
8
10
111'
D a3'
PFF
011, do..
I mo. k .. QO M 1 dt58 f z u's;
12
13
OWNS=
14hPj?42Q^,;
133
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Avorage Sewage Sludge
Temperature During Test
oD
20.875
0.12 mg/L/minute
0.42 (mglg)/hr
I
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxyaen Uptake Rate (SOUR) Worksheet
Date & Analyst
Total Solids
Sample volume used for total solids test
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
OUR
9
9
Time
Temperature Dissolved
(Minutes)
aC Oxygen (mg/L)
0,;q=
�_22�OD� aa�a.rnm52dti!
24'
4
0Ss03I FIs
& '- tLO©
6
Au
';H 0xa7-''x4766 r
7
a>Ilk �?s.4u6.
8
Fit
"'0�c1?4r45 z
904°k4.,
10_
',.aor-&2 IIFF:u.
11
a�00�.1a,1�ll w
RA OQ N l i -'.RA Blr r +
kr—M i' i ,�q� 5,:: .r `n: = ?88 a.s t�7s'
12Y
13
3 63M a
Oxygen Consumption Rate
0.11 mg/
SOUR
*Be
L/minute
0.34 (mg,g)/hr
SOUR Temperature
Temperature ,•uring I BSE,
sewage sludge is > 200C, SOUR =sewage sludge is < 20'C, SOUR = =
SOUR passes if result is <_ 1.5 (mglg)hr
Version 1111/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst: nvGy .:`. ,A #`7 ti�'`, '1
Total Solids
Sample volume used for total solids test.
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
mL
9
9
g/L
Oxygen Consumption Rate 0.08
SOUR
SOUR Temperature Correction
mgNrninute
(mg(g)!hr
sludgeTemperature During I est
sewage • sewage sludge is < 2WC, SOUR = MM(mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxvgen Uptake Rate (SOUR) Worksheet
Date & Analyst:ke i A .1 t/,18if3$ar�i' r;a7�Sti;<, s,AB#1; r 1�pYn4 j
Total Solids
Sample volume used for total solids test
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
N, 341j hd��§i;ia
0.19
18.91
mL
9
9
g/L
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
u0
0
L' i
� a
3
1r11IF p._
°....
4
2{101om ,,
11784
5
vfil
g
w k.-'
�9_IRS
7
8
PFF
10
d10
'�� F ` '9
11-b0�
F
122�..�z�7gt60.t:,
1v I
14:}
;. qQ/Occcc�
firN .. NIVO � Ja fii c
t� COQ.«Ya i
15
Oxygen Consumption Rate
SOUR Temperature Correction
0.05 mg/
SOURL/minute
0.16 (mg/g)/hr
Temperature ■
IS
sewage sludge is >
1 ' • L' i SIM.
sewage sludge is � 2 SOUP, =r� �.�_ � � Vit,
SOUR passes if result is:5
1.5 (mglg)hr
Version 11/1/11

City Of Lumberton
Environmental Laboratory
Specific Oxvoen Uptake Rate (SOUR) Worksheet
Date & Analyst: "W1,24iR ORLY
Total Solids
Sample volume used for total solids test
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
r,'auv. �L12'�v
0.19
19.45
mL
9
9
9
g/L
Time
Temperature
Dissolved
(Minutes)
Oxygen (mg/L)
oC
0
1
6�2 '-arm
30ns-
4
5
?7
6
7
8
10
Gua
6Y475
11
_
airy
� , p,. ^s,00 `�.
��5� a
12
":fx53�5i
13
Vii:_.. 0 iF
5f45 `w`.1•'.'
14
0.0
sia5,4e` ri
15.2
Oxygen Consumption Rate
0.06 mg
SOUR
SOUR Temperature Correction
lLlminute
D.19 (mglg)!hr
Temperature During
sewage sludge is > 200C, SOURnit %
sewage sludge is < 200C, jffl,Mj(mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific OxIii Uptake Rate BOURI Worksheet
Date & Analyst s'+ 5/15;1.18' 7i58arri KCL A6#1.` gay,6'ir
Total Solids
Sample volume used for total solids test. Mg/l.
Weight of dish: g
eight of dish + dried solids: g
eight of dried solids: g
otal Solids:
SOUR
Time
(Minutes)0C
Temperature
Dissolved
oxygen¢¢(mg/L)
�2Mix' 0ti�122
vt6 51{' I t 1 ',
2
3
(.>t<i."vl. ..2x44 au:. •}`
m „'18 tl . "'+ ';
4
6
10ITKa
12
44 ' S
'5 j' ,
13
22AQr
5@6
14
15
Oxygen Consumption Rate
0.00 mg/
SOUR
SOUR Temperature Correction
L/minute
0.01 irngrgyhr
Average Sewage Sludge
Temperature During Test
°C
22
v'. .
If sewage sludge is > 20°C, SOUR = R (mg/g)/hr
If sewage sludge is < 20°C, SOUR =oe A _ .,. (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/1 t

City of Lumberton
environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst , I ,'5J)6I;18 ,g 1$af�i , ,KCt /�B7 Day 7
Total Solids
Sample volume used for total solids test.
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
OUR
Time
(Minutes)
Temperature
oC
Dissolved
Oxygen (mg/L)
oI
t"a,
,. r ,. TI
125!75
72r300�a,aC'.`:
0.19
4;„"06, at
III
18.98
Time
(Minutes)
Temperature
oC
Dissolved
Oxygen (mg/L)
oI
t"a,
,. r ,. TI
6,48 y
72r300�a,aC'.`:
5r11s
4;„"06, at
III
IN
9
IW,`.; i
I WI
IITI.
13
X300 nr
5 ¢1 F
47 ,
Oxygen Consumption Rate
SO
0,06 mg/Llminute
OUR
SOUR Temperature Correction
mL
0
9
9
g/L
0.20 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
23
i
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = oN74 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 91M/11

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQ Permit Number
WWTP Name: City of Lumberton WWTP NPDES Number: _
Monitoring Period: From 07/01/18 To 09/30/18
W00000672
NC0024571
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
m
BetaRay GamaRay Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
33400
40800
66800
CFU/g
0
quarterly
grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
0pfion/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake) X
Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14 -Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying—Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/ISA NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/l5A NCAC v2i. i iuu and the vector attraction
reduction requirement in 40 CPR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Walton WWTP Operator
Prepazer Name and Title (type or
print)
Signature ofPreparer* Date
a7Z R
Land Applier Name and Title (if applicable) (Type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T.1102 (26)
Date

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
US EPA#NC01918
Si
- Synagro s s P 181259
7
R,1 Ja Lumberton WWTP �_[ a ary Yes
Sample Information
ed J. Busse u �; 07/23/18 Rec��d C. Cameron pate's 07123118
Analyses and Results
181259
-1 3wdgE Gr
Fec. Coliform -S 66000
CFUlg
33000
07/24/18 ERP 9222D • MF
-2
33400
Uuig
33400
-3
33400
Mig
33400
-4
66800
CFUIg
33400
-5
<33900
Mig
33900
-6
<33800
twig
33800
4
<33600
Mig
33800
Geomean 40800
181259
-1 3wdge Gr
TS (%) 3.03%
0.01
07/24/18 ERP 2540 G -TS
-2
2.99%
001
-3
2.99%
0.01
-4
2.99%
0.01
-5
2.95%
0.01
-6
2.96%
0.01
-7
2.98%
0.01
Report
Review
Project Manager
Date
219 5, Steele Slr. 919-208-4240
Sanford NC 27330 chrisQQ Qcemeron[esling.c0m

.219 S. Steele Str- Chain of Custody
Cameron Testing Services, Inc.
Sanl0rd, NC 27330 NC WW/GW Cert. #654 NC PHHS Cert# 37799 US EPA NC01918 Page I Of
Rush work will require prior approval. Additional charges will apply
Company:.
�'
Entail:lIez
d,,,.�
CTS
lab use
Contact•..
Phone:
3 3
-
y d3 y.c
2 `�
Sample Temp
- (C) Z.Z
Lab ID I
$ 12s q
-
-..
- -- --
-
-----
—
Address(City,
-
Fax:
-
-
Ice (Y/N)
-
f
- -
State, 2p)
Iay_��a-
M ocic,s J A I Ie�NG
a 7o ag
Notes_
'.Permit (Y/N)
�
�.
Project
LtA„t, 9e c ioh IL)(,JT P
Rush(YM) '
Due:
Collected!, Name: J 6 t," 9
L/ 5s i
Signature:
Sample
Information
Number of bottles
Requested
Analysis
I
a
Prese"atives:.(U)npresewed, H(C)I,
CTS Lab
Sample ID
E
m
}
O
m
o
o
H2(s)O4, H(N)O3, (Na)Thiosulfate, Na(0)H,ID
"
F -`o
0
Other (X),
Indicate
Lum/a-rfa .
I
7/;5 lass
GR S L
j
I U
..
-S
Y,
S
\V
Relin' uished:
vedi
Daterrime
Jo(ti�_13L-sfcz�-
-
b7/z3/r8
12_
- __
_
Rush work will require prior approval. Additional charges will apply

City of Lumberton
Environmental Laboratory
Specific Oxvoen Uptake Rate (SOUR) Worksheet
Date
& Analyst:
Dissolved
Oxygen (mg/L)
1
Are
`�2fi pfinalMOW
2L6
3
-b d8f0
4'IMAW_
Total
Solids
5
N = AA S,-
7
UMARAW
Sample volume used for total solids test.
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
Time
(Minutes)
Temperature
oC
Dissolved
Oxygen (mg/L)
1
`�2fi pfinalMOW
2L6
3
-b d8f0
4'IMAW_
dl
5
N = AA S,-
7
UMARAW
9
*01 00
vii' - -
10
118'0Q
-9
12'
Oxygen Consumption Rate
0.02 mg
SOUR
SOUR Temperature Correction
mL
9
9
g!L
/Llminute
0.06 (mglg)!hr
SOUR passes if result is _< 1.5 (mg/g)hr
Version 11!1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOURI Worksheet
Date & Analyst: E IERIff $" UMMMM .
Total Solids
volumeample - . for total. •
eight• '
eight of . dried • •'
eight of ed
Solids:otal ims '
SOUR
Oxygen Consumption Rate 0.01
SOUR
SOUR Temperature Correction
mg/L(minute
(mg/g)/hr
SOUR passes if result is <_ 1.5 (mglg)ftr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Upiake Rate (SOUR) Worksheet
Date & Analyst:��8/$�� .:._
Total Solids
ample voll"�Ilzqp
eight of dish: NAME I
eight of . solids: , W ' .
eight of dried solids:
• Solids:
SOUR
Oxygen Consumption Rate 0.02
SOUR
SOUR Temperature Correction
0.06
mg/Llminute
(mg/g)/hr
SOUR passes if result is 5 1:5 (mglg)hr
Version 11/1/1 t

City of Lumberton
Environmental Laboratory
Specific OxVgen Uptake Rate {SOUR) Worksheet
Date & Analyst 111 OORYINTMINJNJ
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
0,18
18A
Oxygen Consumption Rate 0.01
SOUR
SOUR Temperature Correction
rid
9
g!L
mg/L/minute
(mglg)/hr
SOUR passes if result is S 1.5 (mglg)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOURI Worksheet
Date & Analyst B/,S/18t1i ICCLvDi,jU ty15°
Total Solids
Sample volume used for total solids test: u - , mL
W eight of dish;MEN*g
Weight of dish + dried solids: &r i 1 ` ` g
Weight of dried solids: 0.23 g
Total Soiids: 22.95 g/L
SOUR
Oxygen Consumption Rate 0.01
OUR
SOUR Temperature Correction
0.03
mg/Llminute
(mg/g)/hr
SOUR passes if result is _< 7.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
899It(_;S 7 04a (. � r RIM b �
Date & Analyst ., J,=
Total Solids
Sample volume used for total solids test: mL
Weight of dish: g
Weight of dish + dried solids: g
Weight of dried solids: P 0.21 g
Total Solids: 21.17 g/L
SOUR
Oxygen Consumption Rate 0.01
SOUR
SOUR Temperature Correction
mg/Llminute
(mg/g)/hr
SOUR passes if result is 5 1.5 (mglg)hr
Version 11/1!11

City of Lumberton
Environmental Laboratory
Specific Oxvgen Uptake Rate (SOUR1 Worksheet
Date &Analysts $j1;Q11$ >6Y2jn KCL}� ppig#r;rR� s7a ;.
Total Solids
Sample volume used for Total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
OUR
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0,02 mg/Llminute
0.04 (mg/g)/hr
SOUR passes if result is 5 1.5 (mg/g)hr
Version 11/1111
epi
o.22
22.43
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0,02 mg/Llminute
0.04 (mg/g)/hr
SOUR passes if result is 5 1.5 (mg/g)hr
Version 11/1111

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton WQPermit Number: W00000672
WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571
Monitoring Period: From 10/01/18 To 12/31/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If an"urahin rn aitarnnfivr nrrfnrmeni !(`I nee A nr ('Ince Rl rnrnnlntr thr fnllnwina monitnrina data,
Parameter
Vector Attraction Reduction (40 CFR503.33/15A
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
"I certify,
under of law, that the requirements in 40
Excee-
of
Type
Technique
not been
met" (Please note if you check this statement attach an
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
230700
<32800
<47600
CFU/g
0
quarterly
grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
NCAC 02T.1107)
Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt. 2
(VS reduction) (40 -day bench)
Option/Alt. 5 Option/Alt. 6
(14 -Day Aerobic) (Alk Stabilization)
Option/Alt. 9 Option/Mt. 10
(Injection) (Incorporation)
Option/Alt. 3 Option/Alt. 4
(30 -day bench) (Spec. 02 uptake) X
Option/Alt. 7 Option/Alt. 8
(Drying—Stable) (Drying—Unstable)
No vector attraction reduction altern
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in
atives were performed
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requir
40 CFR 503.33/15ANCAC 02T.1107 have
been met:'
"I certify,
under of law, that the requirements in 40
CFR 503.32/15A
NCAC 02T.1106 and the vector attraction
reduction
penalty pathogen
requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have
not been
met" (Please note if you check this statement attach an
explanation
why you have not met one or both of the requirements.)
ements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Walton, WWTP Operator
Pr//e//parer Name and Title (type or print) Lend Applier Name and Title (if applicable) (type or print)
4121 � Iii /A
Signature ofPreparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc.,
:PP NCDENR #554
NC PHHS 037799
Synagm 181787: US EPASNCUlgla
_Lumberton WWTPInl x,.14 `I': 'r -
Sample Information
.1-11 if�:lRothIFS=I., 10/10118 Mj, Zubeck 10110118
Analyse.e.and Results
181767 1 9Vasr or FeC, Col ForM 5 [30800 CFU4 30800 10h1116 ERP 92220' -MF
2 <30700 Onwo 30700
3 <30900 =10 30900
4 <30800 Awa 3a60o
6 <30900 CFUg 30900
6 431100 CFufp 31100
7 <47600 cpu19 4-1600
Geomean <32800
18178'7 1 aiuuae o T3(%) 3;2$e!o u,ut 7Ni1It8 ERP 25406 -TS
2 3.26% ao1
3 3:24% o,ar
4 125% o.ot
5 3.24% a.at
6 3,U% 001
7 2.10% 0.01
Report
Review.
Rrojec! Manager
1] A 3. Slgclo STr: A14' -20H-0140
SaefirJ iVC 17)39 chefs rQcameronksliltgepfi

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst:$
Total Solids
ample volume :d E "S�-,
eight of dish: IMF IRA
- dried . eight of dried solids:
®.
SOUR
Oxygen Consumption Rate 0.14
SOUR
0.39
SOUR Temperature Correcklon
Average Sewage Sludge
Temperature During Test
oC
24
mg/L/minute
(mg/gJ/hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Speclfic Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst �"s Mvid o, _ .
Total Solids
. .- IV,
solids:eight of dish:
eight of dish + dried '
eight of dried solids: �'
Solids:otal X7 �'
SOUR
Oxygen Consumption Rate 0.12
SOUR
0.3£3
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
23
mglLlminute
(mglg)/hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOl1Rl Worksheet
Date & Analyst:4��Qc�
Total Solids
eight of dish: �M, Rfilmig
Vaight of dish + dried solids:-•
VeIght of dried solids:
. ,Solids:'
SOUR
Oxygen Consumption Rate 0.14
SOUR
0.42
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
23
mglL/minute
(mgrg)Ihr
Version 11/1111

City of Lumberton
Environmental Laboratory
specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst s X10/ �'(! 1:87�r9` ItKx
Total Solids
Sample volume used for total solids test: „ mL
Weight of dish: ' g
Weight of dish+ dried solids rY- g
Weight of dried solids: 0.21 g
Total Solids: 20.0 g/L
SOUR
Oxygen Consumption Rate fl•13
SOUR
Correction 0.38
SOUR Temperature
Temperature During
sewage k
SOUR passes if result is:5 115 (mg/g)hr
Version 11/1
/11
mg/Llminute
(mglg)Ihr

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst: " Olf2�Irm 8d isti P
Total Solids
Sample volume used for total solids test:Mg/l, mL
Weight of dish: g
Veight of dish + dried solids: 9
Weight of dried solids: g
Total Solids:
SOUR
Oxygen Consumption Rate 0.10
SOUR
Correction 0.26
SOUR Temperature
Average Sewage Sludge
Temperature During Test
°C
22
mglLlminute
(mg/g)!hr
Version 11/7/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 70(1�"118'h07atn, idD�911:a!
Total Solids
Sample Volume used for total solids test: tl`(1 mL
Weight of dish:- k ° g
Weight of dish + dried solids: .' g
Weight of dried solids: 0.19 g
Total Solids: 19.42 g/L
SOUR
Oxygen Consumption Rate u.ue
SOUR 0'19
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
mg/Llminute
(mglg)(hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxvaen Uptake Rate (SOUR) Worksheet
Date & Analyst 'IQ(I a7ta�p0?4U�gitPYa._
Total Solids
Sample volume used for total solids test: ? mL
Weight of dish:
m g
Weight of dish + dried solids: 9
Weight of dried solids: 0.18 g
Total Solids: 17.75 g/L
SOUR
Oxygen Consumption Rate 0.07
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
21.875
mglL/minute
(mg/g)/hr
Version 11/1!11

Agricultural Lime Application Log
Year: 2018
Project: Lumberton
Field
(state -county -site -Heid)
Soil
pH
(from
Lime Requirement
soil analysis)
Tons/Acre
Applied
Date Applied
NC-RO-16-1
6.4
O.OT/Ac.
NC-RO-16-2
5.7
0.7T/Ac.
Ordered*
NC-RO-16-3
6.1
O.OT/Ac
NC-RO-16-4
5.5
1.2T/Ac
Ordered*
NC-RO-16-5
5.9
0.3T/Ac
Ordered*
NC-RO-16-6
6.1
O.OT/Ac.
NC-RO-16-7
7.0
0.0 VAG
NC-RO-16-8
6.6
0.0 T/Ac
NC-RO-16-18
6.7
0 OT/Ac.
NC-RO-16-19
6.6
O.OT/Ac.
NC-RO-17-02
5.5
0.8T/Ac.
Ordered*
NC-RO-17-03
5.5
0.8T/Ac.
Ordered*
NC-RO-28-02
5.5
1.1 T/Ac
1.OT/Ac.
05/01/18
Ag lime will be applied once field and crop conditions are suitable

SECTION 7

NCDA&CS Agronomic Division Phone: (919)
733-2655
Website: w ,ncagr.govlagronomil
being funded
through a grant from the North
Report No. FY19-SL004993
LFQe
Commission.
Client:
Ozzell/Arrin Baker
Advisor:
E Bruce
%,r'"
s
Predictive
2996 Evergreen Church
Rd
Synagro
Pembroke, NC 28372
284 Boger Rd
_
Soil Report
Mehlich-3
Extraction
Mocksville, NC 27028
Sampled County: Robeson
,ts
Links to Helpful Information
Client ID: 156712
Advisor
ID: 475821
Sampled: 07/15/2018
Received: 09/18/2018 completed: 09/25/2018
Farm: NC-RO-16
Sample ID: 16-01Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
110
0 0
0
0
0
0
Note: 12
2-
0.0
Test Results [units -
WN in g]cm3; CEC and Na in meq/100 crrr3; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P -I K -I
Ca% Mg%
SMI
Mn -I
Mn -All Mn -A[2
Zn -I
Zn -AI
Cu -1
Na ESP SS -I NO3-N
1.49 1.17 11.6
89 1.3 6.4
88 53
73 14
49
35
32
100
100
59
0.2 2
Sample ID: 16-02
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M
0.7
180-220 0
90
0 0
0
0
0
0
Note: 12
2-
0.0
Test Results [units -
WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N
in mg/da]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P4 K-1
Ca% Mg%
S4
Mn -1
Mn -All Mn -AQ
Zn -I
Zn -AI
Cu -I
Na ESP SS -I NO3-N
1.25 1.17 7.8
74 2.0 5.7
92 60
56 14
46
29
34
75
75
58
0.2 3
Sample ID: 16-03Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
160
0 0
0
0
0
0
Note: 12
2-
0.0
Test Results [units -
WN in g/cm3; CEC and Na in meq/100 crrr3; NO3-N
in mg/da]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P=I K -I
Ca% Mg%
SMI
Mn -I
Mn -All Mn-Al2
Zn -I
Zn -AI
Cu -I
Na ESP SS -I NO3-N
0.81 1.24 7.5
84 1.2 6.1
196 32
70 11
46
50
45
134
134
94
0.2 3
Nort�t Carolina
Totino Trust Pu:ad Cwilllsskm
Reprogramming of the laboratory -information -management system that
makes this report
possible is
being funded
through a grant from the North
Carolina Tobacco
Trust Fund
Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner ofAgriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No, FY19-SL004993
Ozzell/Arvin Baker Page 2 of 3
Sample ID: 16-04 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past., M 1.2 180-220 0 160 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq]100 cm3; NO3-N in mg/dal: Soil Class: Mineral
HM% WN CEC BS% Ac pH P=I K-1 Ca% Mg% SMI Mn -I Mn-AI1 Mn-Al2 Zn -I Zn -AI Cu -I Na ESP SS -I NO3-N
2.08 1.17 8.4 68 2.7 5.5 81 31 54 13 68 27 33 77 77 64 0.2 2
Sample ID: 16-05 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N PzOS K20 Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past., M 0.3 180-220 0 80 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 crap; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P -I K -I Ca% Mg% SMI Mn -I Mn-AI1 Mn-Al2 Zn -I Zn -AI Cu -1 Na ESP SS -I NO3-N
2.29 1.09 10.6 80 2.1 5.9 116 63 65 12 53 29 34 99 99 71 02 2
Sample ID: 16-07 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 160 0 0 pH$ 0 0 0 Note: 12 Note:
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P -I K4 Ca% Mg% SMI Mn -I Mn -All Mn-AI2 Zn4 Zn -AI Cu -1 Na ESP SS -I NO3-N
0.56 1.39 7.4 96 0.3 7.0 256 29 81 13 44 88 55 129 129 129 0.2 3
Sample ID: 16-08 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 200 0 0 pH$ 0 0 0 Note: 12 Note:
2- 0.0
Test Results [units - WN in g/cd; CEC and Na in meq/100 carp; NO3-N in mg/d0]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K4 Ca% Mg% SMI Mn -I Mn -All Mn-Al2 Zn -I Zn -AI Cu -I Na ESP SS4 NO3-N
0.56 1.35 6.7 90 0.6 6.6 113 16 79 10 35 66 48 74 74 76 0.2 3

NCDA&CS Agronomic Division Phone: [phone] Website: www,ncagr.gov/agronomi/ Report No. FY19-SL004993
Ozzell/Arrin Baker Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
Cumlcopper index
is applied. If MG is recommended and lime is needed, use dolomitric lime. ESP
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K -I potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies MO potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
MIN mineral soil class
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
Mn manganese
an excellent source; 175 to 250 Ib per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -1 levels appear Mn-Al1 Mn -availability index for crop 1
only on reports for greenhouse soil or problem samples. Mn -A]2 Mn -availability index for crop 2
Mn -I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M -O mineral -organic soil class
notations appear on the soil report, refer to $Notem Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various,crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www ncagr gov/agronomi/oboart4 htmY89ind information that P-1 phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5 phosphate
S -I sulfur index
SS -I soluble salt index
Test Results Wtv weight per volume
Zn -AI zinc availability index
The first seven values [soil class, HM%, WN, CEC, BS % , Ac and pH] describe the soil and its degree of acidity. The Zn -I zinc index
remaining 16 [P -I, K -I, Ca%, Mg%, Mn -1, Mn -All, Mn-AI2, Zn -1, Zn -AI, Cu -I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www ncagr go vlagronomi/uvrst htm

Page 1 of 1
ReportNo: 18-361-0643
Account No: 46431
Advisor: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Way0
point.
-ANALYTICAL
client: Ozzie Baker
2996 Evergreen Ch Rd
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa na lyticel.com
Farm: NC-RO-16
Date Received: 12/27/2018
Date of Report: 12/31/2018
Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K4 S-1 Mn4 Zn -I Zn -AI Cu4 CEC BS% Ca% Mg% ESP Na SS -I NOS N
12454 6 NC RO 16 6 MIN 1.0 6.1 0.6 69 48 33 19 45 45 35 4.6 87 64 16 1.8 0.1
ICrop Recommendations: Rec Uom Lime (Uacre) N P205 K20 S Mn Mn -AI Zn Cu B Mg Last Crop
1- Adjust .pH to 6.0 Ib/acre 0.0 4 27 0
Comment:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommentlations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 18-361-0642
Account No: 46431
Advisor: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Waypoint.
ANALYTICAL
Client: Oaie Baker
2996 Evergreen Ch Rd
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointa na lytica I.com
Farm:
NC -RU -16
Date Received: 12/27/2018
Date of Report: 12/31/2018
Lab No Field ID
Sample ID
Soil Class HM%
WN pH
Ac
P-1
K-1
S -I
Mn -I
Zn -I
Zn -AI
Cu -1
CEC
BS%
Ca%
Mg%
ESP Na SS -I NOS N
12452
NC-RO-16-18
MIN 1.0
6.7
0.3
182
14
50
113
250
250
215
5.7
94
78
13
1.5 0.1
Crop Recommendations:
1 -Adjust pH to 6.0
Rec Uom
Ib/acre
Lime (Nacre)
0.0
N
PZ 05
KZO
S
Mn
2
Mn -Al
74
Zn
Cu
B
Mg
0
Last Crop
12453
NC-RO-16-19
MIN 0.6
6.6
0.2
95
7
27
19
83
83
115
3.1
92
74
15
2.0 0.1
ICrop Recommendations:
1 -Adjust pH to 6.0
Rae Uom
Ib/acre
Lime (Nacre)
0.0
N
PZ 05.
K20
S
Mn
4
Mn -Al
19
Zn
Cu
B
Mg
10
Last Crop
Comment:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
Inc.
North Carolina Division of Water Quality Cert'rficaticn #257, Analysis and fertility recommendations shown on
this report are pertormed in accordance within NCDA guidelines, Analysis
prepared
by: Waypoint Analytical Virginia,

NCDA&CS Agronomic Division Phone: [phone]
Website: www,ncagr.gov/agronomi/
Report No.
FY18-SL033004
pOLT°"''..�, Predictive
Client:
Delois/Pete Allen
Advisor:
Nate Roth
o°
6N
688 Deep Branch Rd.
Synagro- PALS Account
Soil
Report
Mehlich-3
Extraction
Lumberton, NC 28360
284 Boger Rd
Mocksville, NC 27028
Sampled County : Robeson
Links to Helpful Information
Sampled:
03/01/2018
Received:
04/18/2018
Farm: RO-17
Completed:
04/30/2018
Client ID: 434958
Advisor ID: 425354
Sample ID: RO172
Recommendations:
Lime
Nutrients (Ib/acre)
—IB
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
6-u
Information
Lime History:
1 -Soybean
1.1
0 0
90 0 0
0
0
0 0
Note: 3
2 -
Test Results [units - WN in
g/cm3; CEC and Na in
meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
PMI K -I
Ca% Mg%
SMI Mn -I Mn -All Mn-Al2
Zn -I
Zn -AI
Cu -1 Na ESP
SS -I NO3-N
2.76 1.42 8.4
70 2.5 5.5
67 25
61 7
34 31 29
107
107
52 0.3 4
Sample ID: RO173Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Soybean
0.8
0 90
130 25 0
10
0
0 0
Note: 3
2-
0
Test Results [units - WN in
g/cm3; CEC and Na in
meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
PMI K -I
Ca% Mg%
S4 Mn -I Mn -All Mn=AI2
Zn -I
Zn -AI
Cum] Na ESP
SS -I NO3-N
1.37 1.38 5.5
67 1.8 5.5
19 9
61 4
38 12 17
40
40
28 0.3 5
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner ofAgricu/ture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No, FY18-SL033004
Delois/Pete Allen I Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. Bs % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
CU4copper index
is applied. If MG is recommended and lime is needed, use dolomitric lime. ESP
ESP exchangeable sodium percent
HM % percent humic matter
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K -I potassium index
Ib/acre unless otherwise specifibd). Recommendations for N (and sometimes for B) are based on research/field studies K2O potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg % % CEC occupied by magnesium
MIN mineral soil class
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is Mn manganese
an excellent source; 175 to 250PIb per acre aldne or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn -All Mn -availability index for crop 1
only on reports for greenhouse soil or problem samples. Mn-Al2 Mn -availability index for crop 2
Mn -I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M -O mineral -organic soil class
notations appear on the soil report, refer to Noted Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. -L NO3-N nitrate nitrogen
ORG organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of loll 000 sq ft. If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www ncagr oov/aoronomi/obnart4 htmtnd information that PMI phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5 phosphate
S -I sulfur index
SS -I soluble salt index
Test Results Will weight per volume
Zn -AI zinc availability index
The first seven values [soil class, HM%, WN, CEC; BS%, Ac and pH] describe the soil and its degree of acidity. The Zn -I zinc index
remaining 16 [P -I, K-1, Ca%, Mg%, Mn -1, Mn -All, Mn-Al2, Zn -I, Zn -Al, Cu -I, S-1, SS -1, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www ncaor gov/agronomi/uyrst htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY18-SL033003
pll6T . Predictive Client: Carnell Locklear Advisor: Synagro
�G 3009 Daniel McLeod Rd. 284 Boger Rd
s o Mehlich-3 Extraction Red Springs, NC 28377 Mocksville, NC 27028
Soil Report
J"b Links to Helpful Information Sampled: 03/01/2018 Sampled County : Robeson
Received: 04/18/2018
Farm: RO-28 Completed: 04/30/2018 Client ID: 275468 Advisor ID: 404711
Sample ID: RO262 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 1.1 120 - 160 0 0 0 0 0 0 0 0 Note: 3
2 -
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3): Soil Class: Mineral
HM% WN CEC BS% Ac pH P=I K -I Ca% Mg% SMI Mn -I Mn -All Mn=AI2 Zn -I Zn -AI Cu -1 Na ESP SS -I NO3-N
2.37 1.21 8.1 69 2.5 5.5 244 122 50 11 55 82 66 281 281 247 0.2 2
®North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Trox/er, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY18-SL033003
Carnell Locklear
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS %
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
Ca/
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
CU4
copper index
ESP
exchangeable sodium percent
Fertilizer
HM %
percent humic matter
Recommendations for field crops or otherlarge areas are listed separately for each nutrient to be added (in units of
K -I
potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg %
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -1 levels appear
Mn
manganese
Mn -All
Mn -availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2
Mn -availability index for crop 2
Mn -I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M -O
mineral -organic soil class
notations appear on the soil report, refer to $Note: SecondaNutrients and Micronutrients. In general, homeowners do not
ry
N
nitrogen
us crop notes also address lime fertilizer needs; visit
need to be concerned about micronutrients. Various
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit `l www.ncaar.00v/aoronomi/obpart4.htmYtafind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
SMI
sulfur index
Test Results
SS -I
soluble salt index
WN
weight per volume
Zn -AI
zinc availability index
The first seven values [soil class, HM%, WN, CEC, BS %, Ac and pH] describe the soil and its degree of acidity. The
Zn
index
remaining 16 [P -I, K -I, Ca%, Mg%, Mn -1, Mn -All, Mn-Al2, Zn -I, Zn -AI, Cu -1, 3-1, SS -I, Na, ESP, SS -1, NO3-N (not routine)
-I
zinc
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaorcov/aaronoml/uvrst.htm