NC0026051_Pretreatment Annual Report_20190226

Pretreatment Annual Report
Submission Requirements
PAR Year 2v � �.
Name Submitting: PM) fl 1a01'-b Date: 2IZ0 C11
Cover Letter
Certification Statement(s)
Narrative
Pretreatment Program Info Database Sheet
Pretreatment Performance Summary (PPS) o,
Significant Non-compliance Report (SNCR)
Historical SNC Report 0'
Public Notice(s) 12"
Allocation Table (AT)
SIU Semi-annual Data Sheets C'
Waste Reduction Information C�
Compliance Schedules D N1t
RECEI'VED/DENR/DWR
FEB 2 8 2019
Water Resources
Permitting Section

DURHAM
COUNTY Engineering and
1D1c
/ Environmental Services
`1881/ Utilities Division
February 26, 2019
Return Receipt Requested RECEtv��/C1F
Certified Mail# 7017 3380 0000 2143 9264 NR/D�/R
FEB282019
Ms. Vivien Zhong Water Resources
Division of Water Resources/PERCS Unit Water
ing Section
1617 Mail Service Center
Raleigh,NC 27699-1617
Re: 2018 Pretreatment Annual Report(PAR)
Dear Ms. Zhong:
Please find enclosed two copies of the Durham County Pretreatment Annual Report
(PAR) for the period of January 1, 2018 through December 31, 2018. If you have any
questions concerning the PAR please contact me at [phone].
Sincerely,
41A.Vej ,Lti)04/LL
Amy Moore
Laboratory& Compliance Manager
cc: Stephanie Brixey, Deputy Director of E&ES/POTW Director
End: Pretreatment Annual Report
(1) Copy
5926 NC Highway 55 East,Durham,North Carolina 27713
[phone] I Fax[phone] I dconc.gov
Equal Employment/Affirmative Action Employer

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2018 to December 31, 2018
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief,true, accurate and complete.
OA& CtN\Uti.' i•Qt4 9
St pZ a Brixey Date
Deputy Director of E&ES/POT Director

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2018 to December 31, 2018
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
)WuLWatL 2 z .1 (11
Amy M e Date
Laboratory& Compliance Manager

DURHAM COUNTY
PRETREATMENT ANNUAL REPORT
NARRATIVE
GENERAL PROGRAM INFORMATION:
Durham County submitted revisions to the Enforcement Response Plan(ERP)on January
17, 2013, that was approved April 3, 2013. Durham County submitted a revision of the
Long Term Monitoring Plan (LTMP) to the Division on September 5, 2013, that was
approved by the Division on October 8, 2013. Durham County submitted a revision of
the Sewer Use Ordinance (SUO) to the Division on December 18, 2012. A letter was
received from the Division on January 28, 2013, requesting additional information. The
March 21, 2013 and approved b
additional information was submittedpp y the Division on
April 3, 2013. The Industrial Waste Survey (IWS) was submitted to the Division on
March 9, 2016. The Division requested additional information that was submitted on
May 27, 2016. The IWS was approved by the Division on May 31, 2016. Durham
County submitted a revision of the Headwork's Analysis (HWA) on March 16, 2018, that
was approved by the Division on May 2, 2018. A copy of the "Pretreatment Program
Info Database"is included.
GENERAL PERMIT INFORMATION:
During the reporting period the following Industrial User Permits were issued, modified,
or renewed:
• AstraZeneca (formerly Pearl Therapeutics), IUP DC-078 was modified to update
a name change and became effective January 31, 2018. The permit was received
by the Division on January 24, 2018 and approved by email on August 6, 2018.
• Aurobindo USA, IUP DC-089 was issued with an effective date of October 9,
2017. The permit was received by the Division on October 13, 2017, and
additional information was received by the Division on November 7, 2017,
January 30, 2018, and February 15, 2018. The permit was approved by the
Division by email on February 16, 2018.
• Braebum, IUP DC-090 was issued with an effective date of January 1, 2018. The
permit was received by the Division on December 5, 2017. The permit was
approved by the Division on January 5, 2018. A letter from the POTW requesting
the permit be terminated was received by the Division on October 8, 2018. The
closeout inspection was conducted at the facility on September 26, 2018. The
permit was terminated on October 8, 2018. The approval letter from the Division
to terminate the permit was received by the POTW on October 10, 2018.
• Cree, IUP DC-076 was modified and became effective on May 14, 2018, to
update required detection levels for cyanide, molybdenum, selenium and total
nitrogen and Part III.6 was added to include the Toxic Organic Management Plan

requirements. The permit was received by the Division on May 8, 2018, and
approved by email on May 10, 2018. The permit was modified to remove the
wastewater reclamation system from the list of Building 6 IU treatment units and
the Pipe 008 discharge description was updated. The permit became effective
August 1, 2018. The Division received and approved the permit on July 25, 2018
by email.
• Cree RTP, IUP DC-040 was modified to update required detection levels for
cyanide, molybdenum, selenium and total nitrogen and Part III.6 was added to
include the Toxic Organic Management Plan requirements with an effective date
of May 14, 2018. The permit was received by the Division on May 8, 2018, and
approved by email on May 10,2018.
• DuPont, IUP DC-010 was terminated with an effective date of January 11, 2018.
The drop request letter was submitted to the Division on January 10, 2018. The
closeout inspection was conducted at the facility on December 27, 2017. The
request was approved in a letter dated January 24, 2018.
• GlaxoSmithKline, IUP DC-010 was terminated with an effective date of January
11, 2018. The termination request letter was submitted to the Division on January
10, 2018. The facility was purchased by Parmer RTP which was issued a local
permit DCL-093 and became effective January 12, 2018. The request to terminate
the permit was approved by the Division in a letter dated January 24, 2018.
• Novan, IUP DC-084 was renewed and became effective on September 14, 2018.
The permit was received and approved by the Division by email on August 10,
2018.
• Phononic, IUP DC-075 was renewed and became effective on March 7, 2018.
The permit was received by the Division on January 31, 2018, and approved by
email on February 6, 2018.
• PowerSecure, IUP DC-095 was modified with an effective date of January 31,
2018, to add requirements for a Sludge Management Plan, Toxic Organic
Management Plan and updated the monitoring location description. The permit
was received by the Division on November 16, 2017, with additional information
provided on January 30, 2018, and February 15, 2018. The Division approved the
permit by email on February 16, 2018.
• United Therapeutics, IUP DC-053 was modified to update the sampling location
for Pipe 002 and became effective on May 8, 2018. The permit was received and
approved by the Division by email on May 3, 2018.

SIU INFORMATION:
1. AstraZeneca (formerly Pearl Therapeutics) (IUP DC-078) — No permit
violations occurred at this facility.
2. Aurobindo USA(IUP DC-089)—Aurobindo was issued a Notice of Violation on
February 5, 2019, for late reporting of the December 2018 monthly average flow.
The report was received on February 4, 2019. The Notice of Violation was issued
in accordance with the ERP.
3. Biogen (IUP DC-080)—No permit violations occurred at this facility.
4. Braeburn (IUP DC-090)—Braeburn was issued a Notice of Violation on April 2,
2018, for late reporting of the January 2018 monthly average flow. The report was
received on April 10, 2018, which resulted in Significant Non-Compliance for
reporting. Braeburn was issued a Notice of Violation on July 11, 2018, for permit
exceedance of the monthly average of acetone which resulted in Significant Non-
Compliance. A resample was collected on July 12, 2018. Braeburn was issued a
Notice of Violation on August 16, 2018, for late reporting and failure to sample
for the first semi-annual period of 2018. A pH sample collected on September 25,
2018, was within the permit limit. A Notice of Violation was not issued due to no
production taking place. The low pH was due to boiler condensate. Braeburn did
not go into production and the permit was dropped. The Notices of Violation were
issued in accordance with the ERP.
5. Cintas (IUP DC-037)—Cintas was issued a Notice of Violation on July 25, 2018,
for failure to sample mercury during the first quarter of 2018. Cintas collected the
mercury sample within thirty (30) days as specified in the Notice. Cintas was
issued a Notice of Violation on August 6, 2018, for exceeding the daily maximum
for mercury on July 20, 2018. Cintas collected an additional mercury sample
within thirty (30) days as specified in the Notice. Cintas was issued a Notice of
Violation on December 18, 2018, for exceeding the daily maximum of Oil and
Grease (non-polar). The Notices of Violation were issued in accordance with the
ERP.
6. Cree, Inc. (IUP DC-076)—Cree was issued a Notice of Violation on January 23,
2018, for failure to submit the annual flow meter calibration report for Pipe 008.
The Notice of Violation was rescinded on February 5, 2018. The flow meter
calibration report was received April 12, 2017, with the Sewer Credit request and
not added to the pretreatment files in error. Cree was issued a Notice of Violation
on June 28, 2018 for failure to provide protection from accidental and slug
loading discharges of prohibited materials per Part II.1 of permit DC-076. Cree
discharged high pH to their equalization basin due to an operator emptying a tote
that was improperly labeled and stored. The tote was believed to be rainwater;
however, the tote contained caustic. Cree was required to revise the Toxic

Organic Management Plan/Accidental Discharge Slug Load Management Plan
(TOMP/ADSLM) to meet the Durham County Slug/Spill Plan Guidelines. The
revised TOMP/ADSLM and response to the Notice of Violation were received via
email on July 27, 2018. Cree was issued a Notice of Violation on November 29,
2018, for not monitoring mercury within the required timeline as detailed in the
permit. The permit requires Cree to sample mercury for the second semi-annual
period between the months of July through September. Cree monitored mercury
on October 9, 2018. The Notices of Violation were issued in accordance with the
ERP.
7. Cree RTP (IUP DC-040) — Cree was issued a Notice of Violation on November
29, 2018, for failure to sample mercury within the required timeline as detailed in
the permit. The permit requires Cree to sample mercury for the second semi-
annual period between the months of July through September. Cree collected a
sample for mercury on October 16, 2018. The Notice of Violation was issued in
accordance with the ERP.
8. JMC (IUP DC-023) — JMC was issued a Notice of Violation on April 2, 2018,
for exceeding the daily maximum and monthly average for chromium. JMC
collected additional samples on March 24-27, 2018. A report summarizing the
cause of the violation was received on April 5, 2018. The Notice of Violation was
issued in accordance with the ERP.
9. Micross (IUP DC-085)—Micross was issued a Notice of Violation on August 23,
2018, for late reporting of the monthly average flow rate for June 2018. The
report was received on August 3, 2018. Micross was issued a Notice of Violation
on December 18, 2018, for late reporting of Total Toxic Organics (TTO). TTO
certification for the second semi-annual period was due December 7, 2018.
Durham County collected TTO on December 19, 2018, as detailed in the permit.
The certification letter was received on December 17, 2018. The Notices of
Violation were issued in accordance with the ERP.
10. Novan (IUP DC-084) — Novan was issued a Notice of Violation on October 8,
2018, for the daily minimum of pH. An additional sample was collected for pH on
October 12, 2018. The Notice of Violation was issued in accordance with the
ERP.
11. Phononic (IUP DC-075)—Phononic was issued a Notice of Violation on July 11,
2018, for a nickel permit limit exceedance on June 18, 2018. Phononic was
issued a Notice of Violation on September 6, 2018, for a permit limit exceedance
of the maximum average flow for the month of July 2018 and for failure to notify
the Control Authority within 24 hours of becoming aware of the violation.
Phononic requested an increase in flow allocation on October 10, 2018, due to
increase in production. Phononic occupies a leased space from a locally permitted
property owner, ARE-100/800/801 Capitola, LLC IUP DCL-077. Durham County
requested the property owner pay additional system development fees to cover the

cost of treating the additional waste on October 12, 2018. A waiver was issued to
Phononic on October 11, 2018, for flow exceedances, to allow time to collect the
appropriate system development fees from the property owner. Phononic
exceeded the maximum average flow for the months of October and November
2018. In a letter dated December 11, 2018, Durham County gave Phononic
permission to report process flow minus RO water reject flow as the monthly
average flow. RO water reject flow is metered separately. Phononic was issued a
Notice of Violation for late reporting on December 18, 2018. The permit requires
the Total Toxic Organics (TTO) Certification to be submitted by December 7
annually. The TTO Certification was received on December 13, 2018. Phononic
was issued a Notice of Violation on January 14, 2019, for late reporting of pH,
molybdenum, and flow meter calibration record. Monitoring results are due no
later than the last day of the month following the month in which the samples
were collected. Flow meter calibration reports are due within 15 days of the
calibration. The pH and molybdenum samples were analyzed on September 24,
2018. The flow meter was calibrated on August 24, 2018. The report for pH,
molybdenum and flow meter calibration was received on December 14, 2018. The
Notices of Violation were issued in accordance with the ERP.
12. PowerSecure (IUP DC-095)—PowerSecure was issued a Notice of Violation on
November 29, 2018, for not monitoring mercury as required by the permit. The
permit requires PowerSecure to monitor mercury for the first semi-annual period
between the months of January through March and for the second semi-annual
period between the months of July through September. PowerSecure monitored
mercury on June 29, 2018, and October 12, 2018. PowerSecure was issued a
Notice of Violation on January 15, 2019, for the daily maximum of pH on a
sample collected on December 19, 2018. An additional pH sample was collected
on January 18, 2019. PowerSecure was issued a Notice of Violation for late
reporting on January 22, 2019. The monthly average flow for November 2018
was received on January 4, 2019. The Notices of Violation were issued in
accordance with the ERP.
13. SCM Metal (IUP DC-005) — SCM Metal was issued a Notice of Violation on
August 20, 2018, for exceedance of the daily maximum and monthly average of
copper on July 17, 2018. SCM Metal collected additional copper samples on
August 16, 2018, and September 7, 2018, as required in the Notice of Violation.
SCM Metal was issued a Notice of Violation on November 16, 2018, for not
monitoring mercury as required by the permit. The permit requires SCM Metal to
monitor mercury for the second semi-annual period between the months of July
through September. SCM Metal monitored mercury on October 9, 2018. The
Notices of Violation were issued in accordance with the ERP.
14. United Therapeutics (IUP DC-053) — No permit violations occurred at this
facility.

WASTE REDUCTION ACTIVITIES:
The Triangle Wastewater Treatment Plant participates in the following waste reduction
activities:
1. Recycling of plastic, glass, aluminum,newspaper and corrugated cardboard.
2. Recycling of used pens, markers, mechanical pencils, highlighters, scotch tape
dispensers and cores, and ink jet cartridges.
3. Recycling of used batteries.
4. Secondary containment for bulk storage of chemicals.
5. Recycling of used oil.
6. Reduction of paper generation.
7. Reduction of power consumption via automation. Logic controls are present that
operates the rotors used for aeration as well as the intensity of the Ultraviolet
Disinfection System.
Permit applications and inspection reports were reviewed for industrial waste reduction
activities information. The codes used in Part V, Waste Reduction Information of the
Industrial Waste Survey and Permit Application are used here. A copy of the code and
description is attached for reference.
Industry Name Code or description of waste reduction activity
AstraZeneca (formerly Pearl Therapeutics)
Aurobindo W19, W22,W34,W36,W62, W71
Biogen W13, W33,W34,W36,W39, W99
Braeburn
Cintas W13,W52
Cree W29, W31, W32, W33, W34, W36, W39, W51, W52,
W58, W99
Cree RTP W29, W39,W99
JMC W24, W52,W81
Micross W21, W23,W33,W34,W36
Novan W14,W55,W61,W62,W72

Phononic W34
PowerSecure
SCM W39
United Therapeutics W25, W52, W54, W55
WASTE REDUCTION CODES:
W 13 Improved maintenance scheduling recordkeeping, or procedures
W14 Changed production schedule to minimize equipment and feedstock
changeovers
W 19 Other changes in operating practices (explain briefly in comments)
W21 Instituted procedures to ensure that materials do not stay in inventory
beyond shelf-life
W22 Began to test outdated material-continue to use if still effective
W23 Eliminated shelf-life requirements for stable materials
W24 Instituted better labeling procedures
W25 Instituted clearinghouse to exchange materials that would otherwise
be discarded
W29 Other changes in Inventory control (explain briefly in comments)
W31 Improved storage or stacking procedures
W32 Improved procedures for loading,unloading and transfer operations
W33 Installed overflow alarms or automatic shutoff valves
W34 Installed secondary containment
W35 Installed vapor recovery systems
W36 Implemented inspection or monitoring program of potential spill or
leak sources
W39 Other spill and leak prevention (explain briefly in comments)
W41 Increased purity of raw materials
W42 Substituted raw materials
W49 Other raw material modifications (explain briefly in comments)
W51 Instituted recirculation within a process
W52 Modified equipment, layout, or piping
W53 Use of a different process catalyst

W54 Instituted better controls on operating bulk containers to minimize
discarding of empty containers
W55 Changed from small volume containers to bulk containers to
minimize discarding of empty containers
W58 Other process modifications (explain briefly in comments)
W59 Modified stripping/cleaning equipment
W60 Changed to mechanical stripping/cleaning devices (from solvents or
other materials)
W61 Changed to aqueous cleaners ( from solvents or other materials)
W62 Reduced the number of solvents used to make waste more amenable
to recycling
W63 Modified containment procedures for cleaning units
W64 Improved draining procedures
W65 Redesigned parts racks to reduce drag out
W66 Modified or installed rinse systems
W67 Improved rinse equipment design
W68 Improved rinse equipment operation
W71 Other cleaning and degreasing operation (explain briefly in
comments)
W72 Modified spray systems or equipment
W73 Substituted coating materials used
W74 Improved application techniques
W75 Changed from spray to other system
W78 Other surface preparation and finishing(explain briefly in comments)
W81 Changed product specifications
W82 Modified design or composition of product
W83 Modified packaging
W89 Other product modifications (explain briefly in comments)
W99 Other(specify in comments)
Additional Information:
During the first semi-annual period, Braeburn was in significant non-compliance (SNC)
for failure to provide self-monitoring data as required by the permit and for exceeding the
monthly permit limit for acetone. The permit was terminated after Durham County staff
verified that the facility did not discharge process waste.

PBM Graphics has a local permit and was in SNC during the first semi-annual period for
exceeding the mercury permit limit. Subsequent mercury sampling was conducted and
met permit limits.
Durham KTP Holdings has a local permit and was in SNC during the first semi-annual
period for mercury. Subsequent mercury sampling was conducted and met permit limits.
Republic Services has a local permit and was in SNC during the first semi-annual period
for mercury. Subsequent mercury sampling was conducted and met permit limits.
There were no SIU's in SNC for the second semi-annual period.
IBM has a local permit and was in SNC during the second semi-annual permit for
mercury. IBM is currently trying to determine the cause.
A historical Significant Non-Compliance (SNC) Report was not received by the Division
to include in this report. A copy of the previous SNC Report along with the 2017 and
2018 Pretreatment Annual Report Significant Non-Compliance Reports are attached as
requested in emails from the Division on December 13, 2018, and January 2, 2019.
Please update the pretreatment program info database with the following information:
Pretreatment Program Primary Contact: Ms. Amy Moore
Contact information for Ms. Amy Moore:
Ms. Amy Moore
919-560-9035 (phone)
919-544-8590 (fax)
Laboratory& Compliance Manager
5926 Highway 55 East
Durham,NC 27713

Pretreatment Program Info Database printed on: 12/12/2018
for Program Name Durham County
WVVTP Name Triangle Stream Information Iwc%at 7010 100.00
Program Approval Date 07/06/1995 7010 Flow cfs/mgd 0 / 0.00
Pretreatment Status 1Q10 Flow cfs/mgd 0.00 / 0.00
Full Stream Classification ws-iv
Region RRO Basin Number CPF05
County Durham \ Receiving Stream Name NORTHEAST CREEK J
NPDES Number NC0026051
NPDES Effective Date Last PAR Rec 02/19/2018 PAR Due Date 03/01/2018 mercury
12/01/2011 1631
NPDES Expire Date Current Fiscal required
P 04/30/2016 Year PCI Done
POT is Primary VW TP TRUE Last Audit on 07/27/2016 Audit Year Next yes
W
Design Flow mgd 12.0000 %Design mgd is SIU permitted 11.85 Permitted SIU flow(mgd)[Pt_SIU) 1.422
VWVTP SIU's 13 Program Sills 13
WWTP CIU's 12 Program CIUs 12 4.1111. LTMP IWS SUO ERP
date Inactive Date Next Due 04/01/2023 j 04/01/2021
Date Received by DWR 03/16/2018 09/05/2013 03/14/2016 12/20/2012 01/17/2013
Date Approved 05/02/2018 10/08/2013 05/31/2016 04/03/2013 04/03/2013
Adopt Date Required
Date Adopted 03/11/2013
Info in this Box from Pt contacts
Date Date Date
PT Pro Attended Attended Attended
Formal Name g.Prime Phonel ext Fax HWA Wksp IUP Wksp PAR Wksp
Ms.Stephanie Brixey (Prim 11919-560-9034 1919-544-8590 II 16/22/2011 11/23/2007 I
[e-mail] Deputy Director of E&ES/POTW 5926 NC Hwy 55 E 27713
Ms.Amy Moore I II l I II 2/9/2012 14/18/2012 11/19/2012
Ms.Laura Melton I 11919-560-9042 1 1919-544-8590 II I I I
[e-mail] Pretreatment Project Coordinator 5926 Highway 55 East 27713
i
JPretreatment Related NOVs from DWQ - , DWR Central Office Contact Vivien Zhong
3/24/2004 PAR-failure to enforce-nov/orders for SNC DWR Regional Contact Cheng Zhang
I

Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
1. Pretreatment Town Name: Durham County
2. "Primary" NPDES Number NCOO 26051 This Column
office
or Non Discharge Permit#if applicable=> use only
- EPA
WENDB
3. PAR begin Date, please enter 01/01/yy or 07/01/yy 3.=> 1/1/2018 PSSD
4. PAR end Date, please enter 06/30/yy or 12/31/yy 4.=> 12/31/2018 PSED
5. Total number of SIUs, includes CIUs 5.=> 13 slus
6. Number of CIUs 6.=> 12 clus
7. Enter the Higher Number, either (7a) or(7b)here=> 0 NOIN
7a. Number of SIUs not sampled by POTW 7a.=> 0
7b. Number of SIUs not inspected by POTW 7b.=> 0
8. Number of SIUs with no IUP, or with an expired IUP 8.=> 0 NOCM
9. Total Number of SIUs in SNC due to either IU Reporting violations or
IUP Limit violations. To avoid double counting some SIUs
Enter ( 9a+ 9b ) - 9c here=> 1 PSNC
Enter the Number of SIUs in SNC for :
9a. IU Reporting violations 9a.=> 1 MSNC
9b. IUP Limit violations 9b._> 1 SNPS
9c. Both IU Reporting& Limit violations 9c.=> 1
10. Number of SIUs in SNC due to IU Reporting violations
that were not sampled or inspected by POTW 10.=> 0 5NIN
11. Number of SIUs in SNC due to violation of 11.=> 0 SSNC
Compliance Schedule due dates
12. Number NOVs, NNCs, AOs, or similar assesed to SIUs 12.=> 24 FENF
13. Number Civil or Criminal Penalties assessed to SIUs 13.=> 0 JUDI
14. Number of SIUs included in public notice 14.=> 1 SVPU
15. Number of SIUs from which penalties collected 15.=> 0 IUPN
16. Total Amount of Civil Penalties Collected 16.=> $ 0
17. Total Number of SIUs on a compliance schedule 17.=> 0 socs
Foot Notes: AO Administrative Order NOV Notice of Violation
CIU Categorical Industrial User PAR Pretreatment Annual Report
CO Consent Order POTW Public Operated Treatment Works
IUP Industrial User Pretreatment Permit SIU Significant Industrial User
NNC Notice of Non-Compliance SNC Significant Non-Compliance,formerly RNC

Pretreatment Annual Report (PAR) PAR covers this calendar year=> 2018
Significant Non-Compliance Report (SNCR) Control Authority=Program=Town Name => Durham County
WWTP = Wastewater Treatment Plant, use separate form for each WWTP. WWTP Name => Triangle WWTP
SIU = Significant Industrial User NPDES # => NC0026051
SNC = Significant Non-Compliance
A SNCR Form must be submitted with every PAR, please write "None" if you had No SIUs in SNC during calendar year
SNC ? (Yes/No )
IUP Pipe Industry Name Parameter for each 6-month period.
# # or "Reporting" Jan. - June July- Dec.
DC-090 001 Braeburn Pharmaceuticals Late Reporting&Acetone YES NO
•
Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page .
Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
Form name: PAR,SNCR,2001
Date Revised: 1/4/2001

Pretreatment Annual Report (PAR) PAR covers this calendar year=> 2017
Significant Non-Compliance Report (SNCR) Control Authority=Program=Town Name => Durham County
WWTP = Wastewater Treatment Plant, use separate form for each WWTP. WWTP Name => Triangle WWTP
SIU = Significant Industrial User NPDES # => NC0026051
SNC = Significant Non-Compliance
A SNCR Form must be submitted with every PAR, please write "None" if you had No SIUs in SNC during calendar year
SNC ? (Yes /No )
IUP Pipe Industry Name Parameter for each 6-month period.
# # or "Reporting" Jan. - June July- Dec.
DC-023 001 JMC Chromium & failure to sample YES NO
DC-018 002 DuPont Copper NO YES
DC-084 001 Novan Mercury NO YES
Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page .
Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
Form name: PAR,SNCR,2001 in UU���M
Date Revised: 1/4/2001

'hi7.i.5 .:§r14
REPORT
Durham County ,
2010 2011 2012 2013 2014 2015 2016
1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half
Dupont/Dupont RTP Sites (E.I. du Pont de PreviousNames: Dupont(E.I.Nenemours)
IUP# DC-018 Pipe# 1 Dupont Electronics SIU Word Description:
metals-433-metal finisher
IUP Status:Active
TTO I I XI I
JMC (USA), Inc. PreviousNames:
IUP# DC-023 Pipe# 001 SIU Word Description:
metals-433-Cr metal production
IUP Status:Active
Chromium I I Ix
pH I I IX I I I I
Phononic PreviousNames:
IUP# DC-075 Pipe# 001 SIU Word Description:
Subpart A
IUP Status:Active
Reporting I I I I I XI I
An'X'in a semi-annual period indicates snc for the period for the respective parameter. f? (g Li \i7
PRINTED ON: 12/18/2017 This information is compiled from many sources,and has not been verified. PAGE 24
Contact the local pretreatment coordinator or state pretreatment staff if errors are noted.

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AFFIDAVIT OF PUBLICATION
Account# Ad Number Identification PO Cols Lines
155525 0003841711 Public Notice Jan-Jun 2018 1 63
Attention: STATE OF NORTH CAROLINA
DURHAM COUNTY ENGINEERING- UTILITY DIVISION COUNTY OF WAKE
5926 HVVY 55 EAST Before the undersigned,a Notary Public of j
DURHAM, NC 27713 Johnston County,North Carolina,duly
commissioned and authorized to administerII
oaths,affirmations,etc.,personally appeared
Public Notice BETSY WOMBLE,who being duly sworn or
Durham County in accordance with Fed-
eral and State Regulations, is hereby affirmed,according to law,doth depose and
giving public notice. Listed below are
users in significant noncompliance with say that he or she is Accounts Receivable
national pretreatment regulations (40
CFR Part 403),state pretreatment regu- Specialist of the News&Observer Publishing
lotions(15 NCAC 2H.0900),or local pre-
treatment regulations during January Company,a corporation organized and doing
2018 through June 2018.
Braeburn Pharmaceuticals, Inc.located business under the Laws of the State of
at 627 Davis Drive, Suite 100 and regu- North Carolina,and publishinga newspaper
laced by significant industrial User Per-
mit No.DC-090 was in a status of signifi-
cant noncomplionce for failure to pro- known as Durham Herald-Sun,Durham
vide self-monitoring data within thirty
days from the due date and exceeding County and State aforesaid,the said
the permit limitation for acetone. A
written notification titled"Notice of Vio- newspaper in which such notice,paper,
lotion"was sent to the user's authorized
representative requiring them to notify document,or legal advertisement was
the County of the cause of the violation.
Subsequent acetone sampling completed published was,at the time of each and every
in July 2018 met the permit limit.
PBM Graphics located at 3700 S.Miami such publication,a newspaper meeting all of
Boulevard and regulated by local indus- the requirements and qualifications of Section
trial User Permit No. DCL-060 was in
status of significant noncompliance for 1-597 of the General Statutes of North
exceeding the permit limitation for mer-
cury. A written notification titled "No- Carolina and was a qualified newspaper
Lice of Violation"was sent to the user's
authorized representative requiring within the meaning of Section 1-597 of the
them to notify the County of the cause of
the violation. Subsequent mercury sam- General Statutes of North Carolina,and that
Piing completed in August 2018 met the
permit limit. as such he or she makes this affidavit;and is
Durham KTP Holdings, LLC located at
523 Davis Drive,and regulated by local familiar with the books,files and business of
industrial User Permit No.DCL-066 was
in status of significant noncomplionce said corporation and by reference to the files
for exceeding the permit limitation for
mercury. A written notification titled of said publication the attached advertisement
"Notice of Violation" was sent to the
user's authorized representative requir-
ing them to notify the County of the .1
cause of the violation. Subsequent mer- Insertion(s)
curt, sampling completed in June 2018
met the permit Iimit.
Republic Services of North Carolina, Published On:
LLC located at 5111 Chin Page Road, September 11,2018
and regulated by local industrial User
Permit No.DCL-092 was in status of sig-
nificant noncompliance for exceeding
the permit limitation for mercury. A
written notification titled"Notice of Vio-
lation"was sent to the user's authorized
representative requiring them to notify
the County of the cause of the violation.
Subsequent mercury sampling complet-
ed in July 2018 met the permit limit.
H-S:September 11,2018
',. rp, i-c- ri V11(7 FE; -- 17611,4,1 (A)\---11/14,‘AL,
BETSY WOMBLE,Accounts Receivable
I
L) Specialist
.on 1
-. SEE 13 2018 .z-i
. .-. . COUNTY 1�(titlN O( t-u a cn X _
DURHAM 1r�tU Sworn to and subbed before me this
1 CNNINttRING GLPARTMEN1 11th day of September,2018
UTILITY OIVISI My Commission Expires:7/10/2023
�.- .,. WENDY DAWSON
;.• Notary Public
i "r` North Carolina
' ' Johnston County

IN
TUESDAY SEPTEMBER 112018
4B Classified HERALDSUN.COM
•
Class± s
2800 pet services&supplies 5300
DOG TRAININGI OBEDIENCE, PROB-
legals annou to LEM Triangfedagtrotnercom
9194119.0554
legals/public notices 301 announcemi farm &
Public Notice AMERICA% equipment
Durham County in accordance with Fed-
eraliviandp State tice. Listed
a hereby farm products/supplies 5550
giving public notice. Listed below are
users in significant noncompliance with Every Thuf;
national pretreatment regulations (40 FI ELDOF B GREENSIWri.Sat.Sam
CFR Part 403),state pretreatment regu- Re Hours Tu &Thurs.
lotions(15 NCAC 2H.0900),or local pre- 3pm For Sole:Okra&Purple hull peas i
treatment regulations during January 406 E.Trinit Si/Ib.Tomatoes$1 per lb.or$25 for a 5-gal.
2018 through June 2018. bucket.Other vegetables if available
Braeburn Pharmaceuticals, Inc.located $2 You pick!Brown Farms-3910 Breeze Rd,
at 627 Davis Drive, Suite 100 and regu- CLEAN ANDIb Rougenant.919-819-5008.
Iated by significant industrial User Per-
mit No.DC-090 was in a status of signifi
v noncompliance for failure to pro-
vide real estate
self-monitoring data within thirty
days from the due date and exceeding em t-
the permit limitation for acetone. A
written notification titled"Notice of Vio- !
lotion"was sent to the user's authorized -
representative requiring them to notify help want 6 homes for rent 6325
the County of the cause of the violation.
Subsequent acetone sampling completed ,
in July 2018 met the permit limit. ROOM&BOAR 313 CLAY ST.3 large bedroom/1 Bath.Cen-
tral
PBM Graphics located at 3700.5.Miami strong,healthy 1 LR,air and heat.porch.Wh h9okup.1 Large
Boulevard and regulated C local Indus-
Chores!No airlift.. LR,Indoor front 919-471-0518
trial User Permit No. DCL-060 was In SERVICE PI 3307 NORTH Duke St.2br/1.5ba,hardwood
status of significant noncompliance for DRAIN CU floors, new kitchen, deck, fenced back
exceeding the permit limitation for mer- EXPERT- yard,cental Heat/ac,1 yr.lease,$1395/mo
cury. A.written notification titled "No- Driver's L. +sec.dep.919-471-2007
tice of Violation"was sent to the user's Mandatory Dr apartments for rent 6400
authorized representative requiring Application
them to notify the County of the cause of 2200 Do
the violation. Subsequent mercury sam- D 807 N. Buchanan Blvd, 1Br apt.$600/mo.
piing completed in August 2018 met the Call 919-688-0448 for details.
permit limit.
Durham KTP Holdings, LLC located at 5004
G townhomes for rent 6425
523 Davis Drive,and regulated by local S�
industrial User Permit No.DCL-066 was 3ba/2.5ba Completely furnished w/1 car ga-
in status of significant noncompliance hair,1st rage. quiet neigborhood- minutes from
for exceeding the permit limitation for mercury. A written notification titled Duke University.$1600/mo,landscaping&"Notice of Violation" was sent to the autDmDtr. util.incl.References required.please call
5006
Ms.Jones at 907-341-9959 for application.
user's authorized representative requir-
ing them to notify the County of the
cause of the violation. Subsequent mer- BU ., i rooms for rent 6450
cury sampling completed in June 2018 •574
met the permit limit. A COZY ROOM
Republic Services of North Carolina, In Quiet neighborhood!
LLC located at 5111 Chin Page.Road, NKC Micro,fridge,AC,cable privileges.
and regulated by local industrial User 'puppies WORKING MALE ONLY.$124(wk.
Permit No.DCL-092 was in status of sig- wormed 919-237-1357
nificant noncompliance for exceeding show and
the permit limitation for mercury. A -nomenal Area:East Durham,Hwy 98&70,furnish-
written notification titled"Notice of Vio- ,7-636-6699 ed wifi,all utlfli.near busline,starting at
lotion"was sent to the user's authorized $550&up.www.alimani.com&919-231-1704
representative requiring them to notify FAYETTEVILLE ST. AREA rooms for
the County of the cause of the violation. rent.No drugs.$135/wk&dep.919-622-3170
Subsequent mercury sampling complet-
ed July 2018 met the
11,2018 permit limit. farms&acreage 6546
notice to creditors 302 AUCTION
10.28 AC VACANT SITE
ALL PERSONS, firms and corporations WEDS SEPT 26TH
having claims against PHYLLIS MOSS Or 12:00 NOON ON SITE
MCGHEE,deceased, of Durham Coun- 15165MINERALSPRINGSRD
ty,N.C.,are notified to exhibit the same
to the undersigned on or before Decem- n� WWW.DAVISREALTYNC.COM
her 13,2018,or this notice will be plead- I1tF11.1 [phone]
ed in bar of recovery. Debtors of the de- NC LIC 21005/2354 i
cedent are asked to make Immediate dy to the15th
payment. This llth day of September, lemon and
2018. Gregory Wayne McGhee, Admin- s before they
istrator,2000 Hayes Rd,Creedmoor, NC 919-414-2258
27522. H-S:9-11,18,25,10-2,2018 trans ortation
9`nes,Paps&
pALL PERSONS,firms and corporations (91
having claims against SENORA R. ��p�;y������� trucks&vans 8600
DECOSTA,deceased,of Orange County, F T PS,
N.C.,are notified to exhibit the same to 9
1964 FORD F100 Truck For Sale! New
the undersigned on or before November condition,54,000 mi. V-8 power steering
30,2018,or this notice will be pleaded in HOUSE
bar of recovery. Debtors of the decedent RATES!Pik labrador &brakes,new tires.f19,000.336-364-8525
Dew claws
are asked toh makey immediate payment. childleld armed near LEGAL AD DEADLINES Ads to run
This 28th day of August,2018. ,3 500 00 434_ Wed-Sat are due by noon two days prior.
Alan F. Karr, Executor, 112 WoodcresT
Dr.,Chapel Hill,NC 27516. Ads to run Sun•Tues are due by noon Fri.

NAN
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AFFIDAVIT OF PUBLICATION
Account# Ad Number Identification PO Cols Lines
155525 0004088635 Public Notice Jul-Dec 2018 1 21
Attention: Corinna Somers STATE OF NORTH CAROLINA
DURHAM COUNTY ENGINEERING- UTILITY DIVISION COUNTY OF WAKE
5926 HVVY 55 EAST Before the undersigned,a Notary Public of
DURHAM, NC 27713 Johnston County,North Carolina,duly
commissioned and authorized to administer
oaths,affirmations,etc.,personally appeared
Public Notice BETSY WOMBLE,who being duly sworn or
Durhurn County accordance with Fed-
eral and State Regulations, is hereby affirmed,according to law,doth depose and
giving public notice. Listed below are
users in significant noncompliance with say that he or she is Accounts Receivable
national pretreatment regulations (40
CFR Port 403),state pretreatment regu- Specialist of the News&Observer Publishing
lotions(15 NCAC 2H.0900),or local pre-
treatment regulations during July 2018 Company,a corporation organized and doing
through December 2018.
International Business Machines Corpo- business under the Laws of the State of
ration located at 3039 Cornwallis Road
and regulated by local industrial user North Carolina,and publishing a newspaper
Permit No.DCL-006 was in status of sig-
nificant noncompliance for exceeding known as Durham Herald-Sun,Durham
the permit limitation for mercury. A
written notification titled"Notice of Vio- County and State aforesaid,the said
lotion"was sent to the user's authorized
representative requiring them to notify newspaper in which such notice,paper,
the County of the cause of the violation.
H-S:February 19,2019 document,or legal advertisement was
published was,at the time of each and every
such publication,a newspaper meeting all of
the requirements and qualifications of Section
1-597 of the General Statutes of North
Carolina and was a qualified newspaper
within the meaning of Section 1-597 of the
General Statutes of North Carolina,and that
as such he or she makes this affidavit;and is
familiar with the books,files and business of
said corporation and by reference to the files
of said publication the attached advertisement
1 Insertion(s)
Published On:
February 19,2019
fQiA1
(A)\--11/1,111yCL
BETSY WOMBLE,Accounts Receivable
Specialist
Received Llw Da.�,u.d�x
Electronic Notary RiA lic
FEB 21 2019 State of North Carolina
Sworn to and subscribed before me this
Durham County 19th day of February,2019
Utilities Division
My Commission Expires: 7/10/2023
WENDY DAWSON
AV*, Notary Public
North Carolina
'�' Johnston County

6B Classified TUESDAY FEBRUARY 19 2019
HERALDSUN.COM
01 1
, assi srn.com/c'assipp
10 • Email: [e-mail]
foreclosure iment2300 lawn/garden/ service misc. 2800
IegaIs North Carolina,to wit: landscaping/trees 2400 CONCRETE Being all of Lot 11 of Cambri
WYndcross Townhomes, Phase III,
shown on plat recorded in Plat Bop A
Page 81 of the Durham County Regi: R E E WO R MWJ Concrete
legals/public notices 301 Save and except any releases, d
Sod propertyse or rr sncommonlyances f rec
knoy *Garage and Room
FAMILY COURT OF THE STATE OF 6525 Clarksdale Lane, Durhamj=s in giving
NEW YORK COUNTY OF QUEENS: 27713. UNTS on Foundations
SUMMONS Docket No. B-12480/18 A cash deposit (no personal checf
CITY OF NEW YORK In the Matter of five percent(5%)of the purchase iaterials and Complete tree *Patio, Driveway and
the Application of CATHOLIC GUARDI- or Seven Hundred Fifty Dir Cost!
AN SERVICES for the Custody and (5750.00), whichever is greater, w Sidewalks
Guardianship of the person BISHOP required at the time of the sale. F(II BUY
LA'BRAUN SMALLS A Minor under the ing the expiration of the statutory work. Grind •Basement,Storage
age of 18 years of age bid period, all the remaining anrerial &
Pursuant to Section 384-b of the Social are immediately due and owing. T( Building and
Services Law of the State of New York. PARTY PURCHASERS MUST ;TALL.
In the Name of the People of the State of THE EXCISE TAX AND THE stumps. Also Monolithic Slabs
New York:TO:ASHANT ISHARISSA CORDING COSTS FOR THEIR DE�+J Nr.pity 7 •
ROBINSON Whereabouts Unknown A Said property to be offered pursuC *Repair Damage Slab
Petition having been filed in the Court, this Notice of Sale is being,offere,e job is
alleging that the above-named child in sale, transfer and conveyance /, �7 1 C�
the care of Catholic Guardian Services, WHERE IS." There are no reprelNEf remove e limbs.. Free Estimate
should be committed to the guardian- floss of warranty relating to the tf
ship and custody of Catholic Guardian any physical, environmental, heal
ateS Insured Any Size Job
Services,an authorized agency; a COPY safety conditions existing in, on,Lrranty
of said Petition being annexed hereto; relating to the property being offer
YOU ARE HEREBY SUMMONED to sale. This sale is made subject to a;enC@ 596-6766
appear before this Court at 151-20 Ja- or liens, unpaid taxes, any unpaid W E Ferrell maica Avenue, Jamaica, New York, transfer taxes, special assessm1B5,
County of Queens,on the 9th day of April easements, rights of way, deeds 1 or
2019, at 12:00 o'clock in the afternoon of lease, and any other encumbranciUrf
said day,at Part 4,before the Honorable exceptions of record. To the best citing 606-2204
Curt Ruben to show Garde why the knowledgeigned,theandr belief of the 6 g 2 90 67
Court should not enter an Order commit- signed, current owner(s)of the A$
tins the guardianship and custody of erty is/are Franklin P.Wright, IV
said child to the Petitioner, as provided Linda B.Johnson,unmarried. 000-3369
by law. PLEASE TAKE NOTICE that An Order for possession of the prof
upon your failure to appear, All of your may be issued pursuant to G.S.4 garage sales 4100
parental rights in the child may be ter- in favor of the purchaser and again
minuted. PLEASE TAKE FURTHER party or Parties in possession b 2400 travel services 2450
NOTICE that your failure to appear clerk of superior court of the cou yard/garage sales 27705 4100
shall constitute a denial of your interest which the property Is sold. Any •
in the child, which denial may result, who occupies the property pursuan MOVE OUT SALEI Thur.2/14 through 2/28.
without further notice,in the transfer or rental agreement entered into • - 1233 Berkeley Street, Apt. B. Like new
commitment of the child's care,custody newed on or after October 1,2007, lawnmower 485,storage containers,door
ti . PLEASE or in the child'sTHEadop-O after receiving the noticem of sale,pr h Harrat buster stopper, gallon of Glidden blue
Tian. PLEASE TAKE FURTHER NO- note the rental agreement by vrov paint, tv's, like new space heaters, &
TICE that you have the right to be rep- written notice of termination to the much more!Ca11984-500-8460 to buy.
resented by a lawyer and, if the Court lord,to be effective on a date statiiee
finds that you are unable to pay for a the notice that is at least 10 days,b
lawyer,you have the right Court. have a t contained
more than 90 days notice after the sale arson •
CII
E R 0 KE E®
yer rigaed by the , the event tht In the oof sale,pro rsI •
pets
of your failure to attend,the Court will that the mortgagor has not cured t�
hear and determine the petition as pro- fault at the time the tenant provide
vided by law. BY ORDER OF THE notice of termination [NCGS 4 animals
COURT/s/Robert Patanski Clerk of 21.16A(b)(2)1. Upon termination a CASINO&RESORT a
the Family Court Dated: County of rental agreement,the tenant is liabi_g March 3,4,5th.Queens rent due under the rental agree •
H-S:February 19,2019 • dogs 5006
mprorated to the effective date of Thmoval g
If the on. 4� 2 Nights,3 Days,If the trustee Is unable to convey Ti AUSTRALIAN SHEPHERDS
Public Notice this property for any reason, the. • 1
Durham County in accordance with Fed- remedy of the purchaser is the retu61Et8E - _
oral and State Regulations, is hereby the deposit. Reasons of such inabill BUS TRIP a .,tt A'
giving public notice. Listed below are convey include, but are not limite4hr. •
users in significant noncompliance with the filing of a bankruptcy petition
national pretreatment regulations (40 to the confirmation of the sale and+1�6', $75
7G 5 free play -.4
CFR Part 403),state pretreatment regu- statement of the loan without the kRYlee tapara Seers Aolomel;eflorlhiple,0ir6om
15 NCAC 2H.0900), or local pre- edge of the trustee. If the validity o
lotions (
treatment regulations during July 2018 sale is challenged by any-partY,nSed
through December2018. trustee, in their sole discretion, if' I Call for Details�+
International Business Machines Corpo- believe the challenge to have merit,tired 1 g�g-383—�Yoe 1
-
ration located at 3039 Cornwallis Road request the court to declare the sa
and regulated by local industrial User be void and return the deposit. The.
Permit No.DCL-006 was in status of sig- chaser will have no further remedy. °f [e-mail]
nificant noncompliance for exceeding Trustee Services of Carolina,LLC 139 AKC Aus - .. • -••'•les,M/F,
the permit limitation for mercury. A Substitute Trustee r 'tinny®. Blue Merles&Block Tri with Blue Eyes,
written notification titled"Notice of Vio- Brock&Scott,PLLC unt I asn www.kingfieldfarm.com, 51,250 757-805-
lation"was sent to the user's authorized Attorneys for Trustee Services of C. 0287
representative requiring them to notify na,LLC , . " Join us every month.
the County of the cause of the violation. 5431 Oleander Drive Suite 200 =` Dobermans AKC!Top Euro Lines,Pups&
H-S:February 19,2019 Wilmington,NC 28403 www.triangledog4
PHONE:[phone] service misc. 2800 www.tr,19-81 dogtrainer.tom
FAX:(910)392,5587iii
REQUEST FOR PROPOSALS File No.:15-00820-FCO2
The University of North Carolina at H-S:February 19,16,2019 pet services&supplies 5300
it:
Chapel Hill DRAINAGE LF.M 80�LVlNG.ITr�a B dE alner.Rc
School of Medicine Institute for Global
Health&Infectious Disease
om
The University of North eCarolinayat T GENERAL COURT OT I• s WORK 919-819-0554
Chapel Hill wishes to acquire by lease JUSTICE SUPERIOR COURT
approximately 1,800 - 2,000 rentable DIVISION BEFORE THE CLERK,
square feet of office/medical space in 17SP63 T V '
the Raleigh, NC area,more specifically NOTICE OF LIEN HOLDER'S SALE real estate
within a two-mile radius of UNC Rex REAL PROPERTY
Hospital on Lake Boone Trail. Lease In the Matter of Foreclosure of a cer & French Drains
term desired is six (6) years and ten Claim of Lien claimed against M1
(10) months with three(3)one(1)Year Emanuel Harris dated August 5, 2 •
renewal options. Possession date by or and Recorded in the Office of the Cash Installed homes for sale 6125
before August 1,2019. The deadline for of Superior Court of Durham Cou
receiving proposals is 4:00 PM, Febru- North Carolina as 16 M 943,
ary 26,2019.For specifications,proposal Hope Derby Carmichael,Trustee,
forms and additional information con- Under and by virtue of the power • Grates for Carports I AUCTION
tact: University Property Office, 103 authority contained in that certain I
Airport Drive,Suite 128,CB#1060,The laration of Covenants, Conditions POSTPONED
University of North Carolina at Chanel Restrictions for Horton Hills Home •„ .,, �.

TWWTP Allocation Table Printed: 2/22/2019, 12:04 PM
Allocation Table Page 1 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/08/18
Permits last modified: 10/08/18
POTw=> Triangle WWTP
NPDES#=> NC0026051
FLOW
Industry Type Renewal Modification Date Permit Limits
IUP INDUSTRY NAMES Permit Pipe of Effective Effective Permit
Count (please list alphabeticly) number _ number Industry Date Date Expires MGD gal/day
1 AstraZeneca Pharmaceuticals DC-078 001 439 D&E Pharmaceutical 01/01/17 01/31/18 12/31/21 0.0020 2,000
2 Aurobindo USA DC-089 001 439 D&E Pharmaceutical 10/09/17 10/08/19 0.0390 39,000
3 Biogen DC-080 001 439 D&E Pharmaceutical-no CN 08/24/15 03/24/17 08/23/20 0.2500 250,000
4 Cintas DC-037 - 001 Full Service Laundry Facility 11/05/17 11/01/22 0.1200 120,000
5 Cree(008,009) DC-076 469 Semi Conductor Mfg. 08/01/14 08/01/18 07/31/19 0.4510 451,000
Cree 008 008 (Combined Discharge) monitor
Cree 009 009 (Combined Discharge) monitor
6 Cree RTP DC-040 012 469 Semi Conductor Mfg. 10/01/16 05/14/18 07/31/19 0.3290 329,000
7 JMC(USA)Inc DC-023 001 433 Cr Metal Production 07/02/17 ' 07/01/22 0.0100 10,000
8 Micross Advanced DC-085 001 469 E R&D Semiconductor 10/21/16 10/20/19 0.0750 75,000
9 Novan,Inc DC-084 001 439 E R&D Pharmaceutical 09/14/18 09/13/23 0.0200 20,000
10 Phononic DC-075 001 469 A Semi Conductor Mfg. 03/08/18 03/06/23 0.0200 20,000
11 PowerSecure DC-095 001 433 Metal Finisher 11/13/17 01/31/18 11/12/19 0.0060 6,000
12 SCM Metals DC-005 001 471.104A Powder Former 07/01/16 06/30/21 0.0500 50,000
13 United Therapeutics DC-053 , 001 (Combined Discharge) 05/25/15 _ 05/08/18 05/24/20 0.0500 50,000
002 Pharmaceutical
Column Totals=> 1.4220 1,422,000
Basis=> NPDES
MAHL from HWA(lbs/day)=> NPDES Permitted Flow=> 12.0000
Uncontrollable Loading(lbs/day)=> 5.3100
Total Allowable for Industry(MAIL)(lbs/day)=> 6.6900
Total Permitted to Industry(lbs/day)=> 1.4220
MAIL left(lbs/day)_> 5.2680
Percent Allow. Ind. (MAIL)still available(%)=> 78.7%
Percent MAHL still available(%)=> 43.9%
5 Percent MARL(lbs/day)=> 0.6000

TWVVTP Allocation Table Printed: 2/22/2019, 12:04 PM
Allocation Table Page 2 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/08/18
Permits last modified: 10/08/18
POTw=> Triangle WWTP
NPDES#=> NC0026051
BOD TSS Ammonia Arsenic Cadmium
Industry Permit Limits Permit Limits Permit Limits Permit Limits _ Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alpbabeticly) number J number mg/I lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day
1 AstraZeneca Pharmaceuticals DC-078 001 _
2 Aurobindo USA DC-089 001 monitor _ monitor monitor monitor
3 Biogen DC-080 001 monitor monitor monitor monitor
4 Cintas DC-037 001 monitor monitor monitor monitor
5 Cree(008,009) DC-076 _
Cree 008 008 monitor monitor
1
Cree 009 009
6 Cree RTP DC-040 012 monitor monitor monitor
7 JMC (USA)Inc DC-023 001 monitor 0.0250 0.0021
8 Micross Advanced DC-085 001 monitor monitor
9 Novan,Inc DC-084 001 monitor
10 Phononic DC-075 001
11 PowerSecure DC-095 001 1 0.0700 0.0035
12 SCM Metals DC-005 001 _ monitor
13 United Therapeutics DC-053 001 monitor monitor monitor monitor
002
Column Totals=> 0 0 0 0.00001 0.0056
Stream Stream
Basis=> Design Design Design Std Std
MAHL from HWA(lbs/day)=> 20016 25020 2502.00 0.8962 0.2987
Uncontrollable Loading(lbs/day)=> 8281 9964 1306.42 0.1329 0.0133
Total Allowable for Industry(MAIL)(lbs/day)=> 11735 15056, 1195.58 0.7633 0.2854
Total Permitted to Industry(lbs/day)=> 0 0 0.00 0.0000 0.0056
MAIL left(lbs/day)_> 11735 15056 1195.58 0.7633 0.2799
Percent Allow. Ind. (MAIL)still available(%)=> 100.0% 100.0% 100.0% 100.0% 98.0%
Percent MAHL still available(%)=> 58.6% 60.2 % 47.8 % 85.2% 93.7%
5 Percent MAHL(lbs/day)_> 1001 1251 125.10 0.0448 0.0149

TWVVTP Allocation Table Printed: 2/22/2019, 12:04 PM
Allocation Table 4/12/2018 REVISED Page 3 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/08/18
Permits last modified: 10/08/18
POTw=> Triangle WWTP
NPDES#=> NC0026051
Chromium Copper Cyanide Lead Mercury
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day
1 AstraZeneca Pharmaceuticals DC-078 001 0.000142 0.000002
I
2 Aurobindo USA DC-089 001 monitor monitor 0.000142 0.000046
3 Biogen DC-080 001 0.000142 0.000296
4 Cintas DC-037 001 monitor monitor monitor 0.000142 0.000142
5 Cree(008,009) DC-076 0.000142 0.000534
Cree 008 008 monitor 1 ...... monitor monitor monitor monitor
Cree 009 009 monitor monitor
6 Cree RTP DC-040 012 monitor monitor 0.0500 monitor 0.000142 0.000390
7 JMC(USA)Inc DC-023 001 0.6500 0.0542 0.7000 0.0584 0.03001, 0.0025 0.1600 0.0133 0.000142 0.000012
8 Micross Advanced DC-085 001 monitor_ monitor monitor 0.000142 0.000089
~�9 Novan,Inc DC-084 001 monitor 0.000142 0.000024
10 Phononic DC-075 001 0.000142 0.000024
11 PowerSecure DC-095 001 1.7100 0.0856 2.0700 0.1036 0.5000 0.0250 0.4300 0.0215 0.000142 0.000007
12 SCM Metals DC-005 001 0.5000 0.2085 0.0300 0.0125 0.1000 0.0417 0.000142 0.000059
13 United Therapeutics DC-053 001 monitor_ 0.000142 0.000059
002 r
Column Totals=> 1 0.1398 0.3705, 0.09001 0.0766 0.001684
Stream AS/Nit/TF Stream Stream
Basis=> Std inhibition Std Std NPDES
MARL from HWA(lbs/day)=> 4.8465 23.6589 0.7950 3.1596 0.025829
Uncontrollable Loading(lbs/day)=> 0.1771 1.9308 0.0221 0.1949 0.003543
Total Allowable for Industry(MAIL)(lbs/day)=> 4.6694 21.7281 0.7728 2.9647 0.022286
Total Permitted to Industry(lbs/day)=> 0.1398 0.3705 0.0900 0.0766 0.001684
MAIL left(lbs/day)=> 4.5296 21.3576 0.6828 2.8882 0.020602
Percent Allow.Ind. (MAIL)still available(%)=> 97.0% 98.3 % 88.4% 97.4% 92.4%
Percent MARL still available(%)=> 93.5 % 90.3 % 85.9% 91.4% 79.8%
5 Percent MAHL(lbs/day)=> 0.2423 1.1829_ 0.0397 0.1580 0.001291

TVVVVTP Allocation Table Printed: 2/22/2019, 12:04 PM
Allocation Table Page 4 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/08/18
Permits last modified: 10/08/18
POTw=> Triangle WWTP
NPDES#=> NC0026051
Molybdenum Nickel Selenium Silver Zinc
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list aipnabeticly) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day
1 AstraZeneca Pharmaceuticals DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor
pi
3 Biogen DC-080 001 monitor monitor
4 Cintas DC-037 001 monitor monitor monitor monitor
11 III 111111
5 Cree(008,009) DC-076
I
Cree 008 008 0.4570 monitor monitor monitor monitor
IIMINIIIIIIIIMP i
Cree 009 009 4 monitor
6 Cree RTP DC-040 012 monitor monitor monitor monitor monitor
7 JMC(USA)Inc DC-023 001 monitor 0.01670.0900 0.0075 0.5600 0.0467
11.
8 Micross Advanced DC-085 001 monitorL.. monitor monitoii monitor
9 Novan,Inc DC-084 001 monitor monitor monitor
10 Phononic DC-075 001 monitor
11 PowerSecure DC-095 001 monitor�0 0.0500 _ 0.0120 1.48001 0.0741
12 SCM Metals DC-005 001 monitor_ monitor monitor monitor
13 United Therapeutics DC-053 001 monitor monitor
I
i
002
Column Totals=> I L 0.4570 0.0867 0.00001 i 0.0195 0.1208
Sludge
Sludge Stream Ceiling AS/Nit/TF AS/Nit/TF
Basis=> Ceiling HASL Std HASL inhibition inhibition
MAHL from HWA(lbs/day)=> 22.9553 2.4843 0.4219 12.3224 49.2894
Uncontrollable Loading(lbs/day)=> 0.3366 0.3321 0.0930 0.0443 18.1304
Total Allowable for Industry(MAIL)(lbs/day)=> 22.6188 2.1522 0.3289 12.2781, 31.1590
Total Permitted to Industry(lbs/day)=> 0.4570 0.0867 0.0000 0.0195 0.1208
MAIL left(lbs/day)=> 22.1618 2.0655 0.3289 12.2585 31.0382
Percent Allow. Ind. (MAIL)still available(%)=> 98.0% 96.0% 100.0% 99.8% 99.6%
Percent MARL still available(%)=> 96.5 % 83.1 % 78.0% 99.5 % 63.0%
5 Percent MAHL(lbs/day)=> 1.1478 0.1242 0.0211 0.6161 2.4645

TVVVVTP Allocation Table Printed: 2/22/2019, 12:04 PM
Allocation Table Page 5 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 10/08/18
Permits last modified: 10/08/18
POTW=> Triangle WWTP
NPDES#=> NC0026051
Total Nitrogen Total Phos. Chloride Fluoride
Industry Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number 1 mg/I lbs/day mg/1 lbs/day mg/1 lbs/day mg/I lbs/day
1 AstraZeneca Pharmaceuticals DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor monitor monitor
_
3 Biogen DC-080 001 monitor monitor monitor monitor
4 Cintas DC-037 001 monitor monitor monitor' monitor
5 Cree(008,009) DC-076 7.0000 26.3294
Cree 008 008 monitor monitor monitor monitor
Cree 009 009 monitor monitor
6 Cree RTP DC-040 012 monitor monitor monitor 7.0000 19.2070
7 JMC(USA)Inc DC-023 001 monito , monitor_ monitor monitor
di•8 Micross Advanced DC-085 001 monitor monitor monitor 6.0000 3.7530
9 Novan,Inc DC-084 001 monitor
10 Phononic DC-075 001
-~11 PowerSecure DC-095 001
12 SCM Metals DC-005 001 monitor monitor monitor monitor
13 United Therapeutics DC-053 001 monitor monitor monitor N.. monitor
002
Column Totals=> 0.001 0.00 1 0.00001 49.2894
Basis=> Design Design Stream Std NPDES
MAHL from HWA(lbs/day)=> 4003.2000 650.00 16179.5562 100.3290
Uncontrollable Loading(lbs/day)=> 1988.6492 238.92 3844.2251 31.7881
Total Allowable for Industry(MAIL)(lbs/day)=> 2014.55 411.08 12335.3311 68.5409
Total Permitted to Industry(lbs/day)=> 0.00 0.00 0.0000 49.2894
MAIL left(lbs/day)=> 2014.55 411.08 12335.3311 19.2515
Percent Allow.Ind. (MAIL)still available(%)=> 100.0% 100.0% 100.0% 28.1 %
Percent MAHL still available(%)=> 50.3 % 63.2% 76.2 % 19.2%
5 Percent MAHL(lbs/day)=> 200.16, 32.5000 808.9778 5.0164

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Ouija'l: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/12/2018 S AstraZeneca021218Se1 < 0.003 /20.7 mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 0.05 /20.7 mg/L < /
TW
Feb 2018 Week 2 < 0.003 / mg/L < /
Apr 2018 Week 4 < 0.05 / mg/L < /
Feb 2018 Average < 0.003 /8.2 mg/L < /
Apr 2018 Average < 0.05 /8.2 mg/L < /
2018 Quarter 1 < 0.003 / mg/L < /
2018 Quarter 2 < 0.05 / mg/L < /
2018 1st 6 Months(Avg) < 0.026 / mg/L < /
2018 1st 6...(Max) < 0.05 / mg/L /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Pear10118Flow 0.001519 / MGD /
02/28/2018 S AstraZeneca0218F1ow 0.001442 / MGD /
03/31/2018 S AstraZeneca0318F1ow 0.001502 / MGD /
04/30/2018 S AstraZeneca0418F1ow 0.001295 / MGD /
06/01/2018 S AstraZeneca0518F1ow 0.00116 / MGD /
06/30/2018 S AstraZeneca0618F1ow 0.001081 / MGD /
Jan 2018 Week 4 0.001519 / MGD /
Feb 2018 Week 4 0.001442 / MGD /
Mar 2018 Week 4 0.001502 / MGD /
Apr 2018 Week 4 0.001295 / MGD /
Jun 2018 Week 1 0.00116 / MGD /
Jun 2018 Week 4 0.001081 / MGD /
Jan 2018 Average 0.001519 /0.002000 MGD /
Feb 2018 Average 0.001442 /0.002000 MGD /
Mar 2018 Average 0.001502 /0.002000 MGD /
Apr 2018 Average 0.001295 /0.002000 MGD /
Jun 2018 Average 0.001121 /0.002000 MGD /
2018 Quarter 1 0.001488 / MGD /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2018 Quarter 2 0.001179 / MGD /
2018 1st 6 Months(Avg) 0.001333 / MGD /
2018 1st 6...(Max) 0.001519 / MGD /
2018 1st 6...(Min) 0.001081 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 5 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/12/2018 S AstraZeneca021218Sel < 7.5 / mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 7.5 / mg/L < /
TW
Feb 2018 Week 2 < 7.5 / mg/L < /
Apr 2018 Week 4 < 7.5 / mg/L < /
Feb 2018 Average < 7.5 / mg/L < /
Apr 2018 Average < 7.5 / mg/L < /
2018 Quarter 1 < 7.5 / mg/L < /
2018 Quarter 2 < 7.5 / mg/L < /
2018 1st 6 Months(Avg) < 7.5 / mg/L < /
2018 1st 6...(Max) < 7.5 / mg/L < /
2018 1st 6...(Min) < 7.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/12/2018 S AstraZeneca021218Sel < 0.0003 /20.7 mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 0.0005 /20.7 mg/L < /
TW
Feb 2018 Week 2 < 0.0003 / mg/L < /
Apr 2018 Week 4 < 0.0005 / mg/L < /
Feb 2018 Average < 0.0003 /8.2 mg/L < /
Apr < <
8 Average 0.0005 /8.2 mg/L /
P
2018 Quarter 1 < 0.0003 / mg/L < /
2018 Quarter 2 < 0.0005 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2018 1st 6 Months(Avg) < 0.0004 / mg/L < /
2018 1st 6...(Max) < 0.0005 / mg/L < /
2018 1st 6...(Min) < 0.0003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/12/2018 S AstraZeneca021218Sel < 0.0003 /20.7 mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 0.0005 /20.7 mg/L < /
TW
Feb 2018 Week 2 < 0.0003 / mg/L < /
Apr 2018 Week 4 < 0.0005 / mg/L < /
Feb 2018 Average < 0.0003 /8.2 mg/L < /
Apr 2018 Average < 0.0005 /8.2 mg/L < /
2018 Quarter 1 < 0.0003 / mg/L < /
2018 Quarter 2 < 0.0005 / mg/L < /
2018 1st 6 Months(Avg) < 0.0004 / mg/L < /
2018 1st 6...(Max) < 0.0005 / mg/L < /
2018 1st 6...(Min) < 0.0003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/12/2018 S AstraZeneca021218Sel 0.000002 /0.000142 mg/L /
f
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
' 04/30/2018 P AstraZeneca043018PO 0.000001 /0.000142 mg/L /
TW
Feb 2018 Week 2 0.000002 / mg/L /
Apr 2018 Week 4 0.000001 / mg/L /
Feb 2018 Average 0.000002 / mg/L /
Apr 2018 Average 0.000001 / mg/L /
2018 Quarter 1 0.000002 / mg/L /
2018 Quarter 2 0.000001 / mg/L /
2018 1st 6 Months(Avg) 0.000002 / mg/L /
2018 1st 6...(Max) 0.000002 / mg/L /
2018 1st 6...(Min) 0.000001 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/12/2018 S AstraZeneca021218Se1 < 0.003 /3 mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 0.001 /3 mg/L < /
TW
Feb 2018 Week 2 < 0.003 / mg/L < /
Apr 2018 Week 4 < 0.001 / mg/L < /
Feb 2018 Average < 0.003 /0.7 mg/L < /
Apr 2018 Average < 0.001 /0.7 mg/L < /
2018 Quarter 1 < 0.003 / mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) < 0.003 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/12/2018 S AstraZeneca021218Se1 < 0.025 /20.7 mg/L < /
f
04/30/2018 P AstraZeneca043018PO < 0.001 /20.7 mg/L < /
TW
Feb 2018 Week 2 < 0.025 / mg/L < /
Apr 2018 Week 4 < 0.001 / mg/L < /
Feb 2018 Average < 0.025 /8.2 mg/L < /
Apr 2018 Average < 0.001 /8.2 mg/L < /
2018 Quarter 1 < 0.025 / mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.013 / mg/L < /
2018 1st 6...(Max) < 0.025 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/12/2018 S AstraZeneca021218Se1 6.6 /6- 10 SU /
f
04/30/2018 P AstraZeneca043018PO 7.3 /6- 10 SU /
TW
Feb 2018 Week 2 6.6 / SU /
Apr 2018 Week 4 7.3 / SU /
Feb 2018 Average 6.6 / SU /
Apr 2018 Average 7.3 / SU /
2018 Quarter 1 6.6 / SU /
2018 Quarter 2 7.3 / SU /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2018 1st 6 Months(Avg) 6.95 / SU /
2018 1st 6...(Max) 7.3 / SU /
2018 1st 6...(Min) 6.6 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 6

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/06/2018 S Aurobindo020618Self 0.304 / 10.35 mg/L /
04/27/2018 P Aurobindo042718POT 0.146 / 10.35 mg/L /
W
Feb 2018 Week 1 0.304 / mg/L /
Apr 2018 Week 4 0.146 / mg/L /
Feb 2018 Average 0.304 /4.1 mg/L /
Apr 2018 Average 0.146 /4.1 mg/L /
2018 Quarter 1 0.304 / mg/L /
2018 Quarter 2 0.146 / mg/L /
2018 1st 6 Months(Avg) 0.225 / mg/L /
2018 1st 6...(Max) 0.304 / mg/L /
2018 1st 6...(Min) 0.146 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/06/2018 S Aurobindo020618Self 62 / mg/L /
04/27/2018 P Aurobindo042718POT 45 / mg/L /
W
Feb 2018 Week 1 62 / mg/L /
Apr 2018 Week 4 45 / mg/L /
Feb 2018 Average 62 / mg/L /
Apr 2018 Average 45 / mg/L /
2018 Quarter 1 62 / mg/L /
2018 Quarter 2 45 / mg/L /
2018 1st 6 Months(Avg) 53.5 / mg/L /
2018 1st 6...(Max) 62 / mg/L /
2018 1st 6...(Min) 45 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/23/2018 S Aurobindo0118Flow 0.000968 / MGD /
02/21/2018 S Aurobindo0218Flow 0.000835 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/19/2018 S Aurobindo0318Flow 0.000961 / MGD /
04/30/2018 S Aurobindo0418F1ow 0.00102 / MGD /
05/21/2018 S Aurobindo0518F1ow 0.001042 / MGD /
06/20/2018 S Aurobindo0618F1ow 0.00107 / MGD /
Jan 2018 Week 4 0.000968 / MGD /
Feb 2018 Week 3 0.000835 / MGD /
Mar 2018 Week 3 0.000961 / MGD /
Apr 2018 Week 4 0.00102 / MGD /
May 2018 Week 3 0.001042 / MGD /
Jun 2018 Week 3 0.00107 / MGD /
Jan 2018 Average 0.000968 /0.039 MGD /
Feb 2018 Average 0.000835 /0.039 MGD /
Mar 2018 Average 0.000961 /0.039 MGD /
Apr 2018 Average 0.00102 /0.039 MGD /
May 2018 Average 0.001042 /0.039 MGD /
Jun 2018 Average 0.00107 /0.039 MGD /
2018 Quarter 1 0.000921 / MGD /
2018 Quarter 2 0.001044 / MGD /
2018 1st 6 Months(Avg) 0.000983 / MGD /
2018 1st 6...(Max) 0.00107 / MGD /
2018 1st 6...(Min) 0.000835 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/06/2018 S Aurobindo020618Se1f 139 / mg/L /
04/27/2018 P Aurobindo042718POT 307 / mg/L /
W
Feb 2018 Week 1 139 / mg/L /
Apr 2018 Week 4 307 / mg/L /
Feb 2018 Average 139 / mg/L /
Apr 2018 Average 307 / mg/L /
2018 Quarter 1 139 / mg/L /
2018 Quarter 2 307 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
2018 1st 6 Months(Avg) 223 / mg/L /
2018 1st 6...(Max) 307 / mg/L /
2018 1st 6...(Min) 139 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/06/2018 S Aurobindo020618Se1f < 0.00008 / mg/L < /
04/27/2018 P Aurobindo042718POT < 0.00008 / mg/L < /
W
Feb 2018 Week 1 < 0.00008 / mg/L < /
Apr 2018 Week 4 < 0.00008 / mg/L < /
Feb 2018 Average < 0.00008 / mg/L < /
Apr 2018 Average < 0.00008 / mg/L < /
2018 Quarter 1 < 0.00008 / mg/L < /
2018 Quarter 2 < 0.00008 / mg/L < /
2018 1st 6 Months(Avg) < 0.00008 / mg/L < /
2018 1st 6...(Max) < 0.00008 / mg/L < /
2018 1st 6...(Min) < 0.00008 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/06/2018 S Aurobindo020618Self 65 / mg/L /
04/27/2018 P Aurobindo042718POT 51 / mg/L /
W
Feb 2018 Week 1 65 / mg/L /
Apr 2018 Week 4 51 / mg/L /
Feb 2018 Average 65 / mg/L /
Apr 2018 Average 51 / mg/L /
2018 Quarter 1 65 / mg/L /
2018 Quarter 2 51 / mg/L /
2018 1st 6 Months(Avg) 58 / mg/L /
2018 1st 6...(Max) 65 / mg/L /
2018 1st 6...(Min) 51 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/06/2018 S Aurobindo020618Se1f 391 / mg/L /
04/27/2018 P Aurobindo042718POT 640 / mg/L /
W
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
Feb 2018 Week 1 391 / mg/L /
Apr 2018 Week 4 640 / mg/L /
Feb 2018 Average 391 / mg/L /
Apr 2018 Average 640 / mg/L /
2018 Quarter 1 391 / mg/L /
2018 Quarter 2 640 / mg/L /
2018 1st 6 Months(Avg) 515.5 / mg/L /
2018 1st 6...(Max) 640 / mg/L /
2018 1st 6...(Min) 391 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/06/2018 S Aurobindo020618Se1f 0.063 / mg/L /
04/27/2018 P Aurobindo042718POT 0.057 / mg/L /
W
Feb 2018 Week 1 0.063 / mg/L /
Apr 2018 Week 4 0.057 / mg/L /
Feb 2018 Average 0.063 / mg/L /
Apr 2018 Average 0.057 / mg/L /
2018 Quarter 1 0.063 / mg/L /
2018 Quarter 2 0.057 / mg/L /
2018 1st 6 Months(Avg) 0.060 / mg/L /
2018 1st 6...(Max) 0.063 / mg/L /
2018 1st 6...(Min) 0.057 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/06/2018 S Aurobindo020618Se!f 0.014 / mg/L /
04/27/2018 P Aurobindo042718POT < 0.003 / mg/L < /
W
Feb 2018 Week 1 0.014 / mg/L /
Apr 2018 Week 4 < 0.003 / mg/L < /
Feb 2018 Average 0.014 / mg/L /
Apr 2018 Average < 0.003 / mg/L < /
2018 Quarter 1 0.014 / mg/L /
2018 Quarter 2 < 0.003 / mg/L < /
2018 1st 6 Months(Avg) < 0.008 / mg/L < /
2018 1st 6...(Max) 0.014 / mg/L /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/06/2018 S Aurobindo020618Se1f < 0.005 / 10.35 mg/L < /
04/27/2018 P Aurobindo042718POT < 0.005 / 10.35 mg/L < /
W
Feb 2018 Week 1 < 0.005 / mg/L < /
Apr 2018 Week 4 < 0.005 / mg/L < /
Feb 2018 Average < 0.005 /4.1 mg/L < /
Apr 2018 Average < 0.005 /4.1 mg/L < /
2018 Quarter 1 < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/06/2018 S Aurobindo020618Se1f 0.7 / mg/L /
04/27/2018 P Aurobindo042718POT 0.1 / mg/L /
W
Feb 2018 Week 1 0.7 / mg/L /
Apr 2018 Week 4 0.1 / mg/L /
Feb 2018 Average 0.7 / mg/L /
Apr 2018 Average 0.1 / mg/L /
2018 Quarter 1 0.7 / mg/L /
2018 Quarter 2 0.1 / mg/L /
2018 1st 6 Months(Avg) 0.4 / mg/L /
2018 1st 6...(Max) 0.7 / mg/L /
2018 1st 6...(Min) 0.1 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/06/2018 S Aurobindo020618Self < 0.005 / 10.35 mg/L < /
04/27/2018 P Aurobindo042718POT < 0.005 / 10.35 mg/L < /
W
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
Feb 2018 Week 1 < 0.005 / mg/L < /
Apr 2018 Week 4 < 0.005 / mg/L < /
Feb 2018 Average < 0.005 /4.1 mg/L < /
Apr 2018 Average < 0.005 /4.1 mg/L < /
2018 Quarter 1 < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 l st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
02/05/2018 S Aurobindo020518Se1f 0.000004 /0.00142 mg/L /
Hg
04/26/2018 P Aurobindo042618POT 0.000028 /0.00142 mg/L /
WHg
Feb 2018 Week 1 0.000004 / mg/L /
Apr 2018 Week 4 0.000028 / mg/L /
Feb 2018 Average 0.000004 / mg/L /
Apr 2018 Average 0.000028 / mg/L /
2018 Quarter 1 0.000004 / mg/L /
2018 Quarter 2 0.000028 / mg/L /
2018 1st 6 Months(Avg) 0.0000157 / mg/L /
2018 1st 6...(Max) 0.0000275 / mg/L /
2018 1st 6...(Min) 0.0000039 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30%2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/06/2018 S Aurobindo020618Se1f < 0.003 / 1.5 mg/L < /
04/27/2018 P Aurobindo042718POT < 0.005 / 1.5 mg/L < /
W
Feb 2018 Week 1 < 0.003 / mg/L < /
Apr 2018 Week 4 < 0.005 / mg/L < /
Feb 2018 Average < 0.003 /0.35 mg/L < /
g F�
Apr 2018 Average < 0.005 /0.35 mg/L < /
' 2018 Quarter 1 < 0.003 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.004 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/06/2018 S Aurobindo020618Self < 0.001 / mg/L < /
04/27/2018 P Aurobindo042718POT < 0.001 / mg/L < /
W
Feb 2018 Week 1 < 0.001 / mg/L < /
Apr 2018 Week 4 < 0.001 / mg/L < /
Feb 2018 Average < 0.001 / mg/L < /
Apr 2018 Average < 0.001 / mg/L < /
2018 Quarter 1 < 0.001 / mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/06/2018 S Aurobindo020618Self < 0.005 / 10.35 mg/L < /
04/27/2018 P Aurobindo042718POT < 0.005 / 10.35 mg/L < /
W
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Feb 2018 Week 1 < 0.005 / mg/L < /
Apr 2018 Week 4 < 0.005 / mg/L < /
Feb 2018 Average < 0.005 /4.1 mg/L < /
Apr 2018 Average < 0.005 /4.1 mg/L < /
2018 Quarter 1 < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/06/2018 S Aurobindo020618SeIf 0.6 / mg/L /
04/27/2018 P Aurobindo042718POT 0.5 / mg/L /
W
Feb 2018 Week 1 0.6 / mg/L /
Apr 2018 Week 4 0.5 / mg/L /
Feb 2018 Average 0.6 / mg/L /
Apr 2018 Average 0.5 / mg/L /
2018 Quarter 1 0.6 / mg/L /
2018 Quarter 2 0.5 / mg/L /
2018 1st 6 Months(Avg) 0.6 / mg/L /
2018 1st 6...(Max) 0.6 / mg/L /
2018 1st 6...(Min) 0.5 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/06/2018 S Aurobindo020618Self 64.3 / mg/L /
04/27/2018 P Aurobindo042718POT 75.6 / mg/L /
W
Feb 2018 Week 1 64.3 / mg/L /
Apr 2018 Week 4 75.6 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
Feb 2018 Average 64.3 / mg/L /
1 Apr 2018 Average 75.6 / mg/L /
2018 Quarter 1 64.3 / mg/L /
2018 Quarter 2 75.6 / mg/L /
2018 1st 6 Months(Avg) 69.95 / mg/L /
2018 1st 6...(Max) 75.6 / mg/L /
2018 1st 6...(Min) 64.3 / mg/L / 1
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/06/2018 S Aurobindo020618Setf < 2.5 /200 mg/L < /
04/27/2018 P Aurobindo042718POT < 2.5 /200 mg/L < /
W
Feb 2018 Week 1 < 2.5 / mg/L < /
Apr 2018 Week 4 < 2.5 / mg/L < / 1
Feb 2018 Average < 2.5 / mg/L < /
Apr 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
2018 Quarter 2 < 2.5 / mg/L < /
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/06/2018 S Aurobindo020618Se1f 8.9 /6.0- 10.0 SU /
04/27/2018 P Aurobindo042718POT 7.6 /6.0- 10.0 SU /
W
Feb 2018 Week 1 8.9 / SU /
Apr 2018 Week 4 7.6 / SU /
Feb 2018 Average 8.9 / SU /
Apr 2018 Average 7.6 / SU /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2018 Quarter 1 8.9 / SU /
2018 Quarter 2 7.6 / SU /
2018 1st 6 Months(Avg) 8.25 / SU /
2018 1st 6...(Max) 8.9 / SU /
2018 1st 6...(Min) 7.6 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: • 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/06/2018 S Aurobindo020618Se1f 16 /66 °C /
04/27/2018 P Aurobindo042718POT 20 /66 °C /
W
Feb 2018 Week 1 16 / °C /
Apr 2018 Week 4 20 / °C /
Feb 2018 Average 16 / °C /
Apr 2018 Average 20 / °C /
2018 Quarter 1 16 / °C /
2018 Quarter 2 20 / °C /
2018 1st 6 Months(Avg) 18 / °C /
2018 1st 6...(Max) 20 / °C /
2018 1st 6...(Min) 16 / °C /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/06/2018 S Aurobindo020618Se1f 63.7 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
04/27/2018 P Aurobindo042718POT 75.1 / mg/L /
W
Feb 2018 Week 1 63.7 / mg/L /
Apr 2018 Week 4 75.1 / mg/L /
Feb 2018 Average 63.7 / mg/L /
Apr 2018 Average 75.1 / mg/L /
2018 Quarter 1 63.7 / mg/L /
2018 Quarter 2 75.1 / mg/L /
2018 1st 6 Months(Avg) 69.4 / mg/L /
11 2018 1st 6...(Max) 75.1 / mg/L /
2018 1st 6...(Min) 63.7 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/06/2018 S Aurobindo020618Self 2.73 / mg/L /
04/27/2018 P Aurobindo042718POT 5.54 / mg/L /
W
Feb 2018 Week 1 2.73 / mg/L /
Apr 2018 Week 4 5.54 / mg/L /
Feb 2018 Average 2.73 / mg/L /
Apr 2018 Average 5.54 / mg/L /
2018 Quarter 1 2.73 / mg/L /
2018 Quarter 2 5.54 / mg/L /
2018 1st 6 Months(Avg) 4.135 / mg/L /
2018 1st 6...(Max) 5.54 / mg/L /
2018 1st 6...(Min) 2.73 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/06/2018 S Aurobindo020618Se1f 55 / mg/L /
04/27/2018 P Aurobindo042718POT 80 / mg/L /
W
Feb 2018 Week 1 55 / mg/L /
Apr 2018 Week 4 80 / mg/L /
Feb 2018 Average 55 / mg/L /
Apr 2018 Average 80 / mg/L /
2018 Quarter 1 55 / mg/L /
2018 Quarter 2 80 / mg/L /
2018 1st 6 Months(Avg) 67.5 / mg/L /
2018 1st 6...(Max) 80 / mg/L /
2018 1st 6...(Min) 55 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 12

Aurobindo USA
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/06/2018 S Aurobindo020618Se1f 0.3196 / mg/L /
Feb 2018 Week 1 0.3196 / mg/L /
Feb 2018 Average 0.3196 / mg/L /
2018 Quarter 1 0.3196 / mg/L /
2018 1st 6 Months(Avg) 0.3196 / mg/L /
2018 1st 6...(Max) 0.3196 / mg/L /
2018 1st 6...(Min) 0.3196 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/06/2018 S Aurobindo020618Se1f 0.212 / mg/L /
04/27/2018 P Aurobindo042718POT 0.129 / mg/L /
W
Feb 2018 Week 1 0.212 / mg/L /
Apr 2018 Week 4 0.129 / mg/L /
Feb 2018 Average 0.212 / mg/L /
Apr 2018 Average 0.129 / mg/L /
2018 Quarter 1 0.212 / mg/L /
2018 Quarter 2 0.129 / mg/L /
2018 1st 6 Months(Avg) 0.171 / mg/L /
2018 1st 6...(Max) 0.212 / mg/L /
2018 1st 6...(Min) 0.129 / mg/L /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 12 of 12

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
01/16/2018 P Biogen011618POTW < 0.025 / 12.19 mg/L < 0.0114 / lbs/day
Jan 2018 Week 3 < 0.025 / mg/L < 0.0114 / lbs/day
Jan 2018 Average < 0.025 /4.83 mg/L < 0.0114 / lbs/day
2018 Quarter 1 < 0.025 / mg/L < 0.0114 / lbs/day
2018 1st 6 Months(Avg) < 0.025 / mg/L < 0.0114 / lbs/day
1 2018 1st 6...(Max) < 0.025 / mg/L < 0.0114 / lbs/day
2018 1st 6...(Min) < 0.025 / mg/L < 0.0114 / lbs/day
2018 1st 6...(Count) 1 / l /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/25/2018 P Biogen012518POTW 2.2 / mg/L 1.6403 / lbs/day
02/07/2018 S Biogen020718Self 2 / mg/L 0.8559 / lbs/day
Jan 2018 Week 4 2.2 / mg/L 1.6403 / lbs/day
Feb 2018 Week 1 2 / mg/L 0.8559 / lbs/day
Jan 2018 Average 2.2 / mg/L 1.6403 / lbs/day
Feb 2018 Average 2 / mg/L 0.8559 / lbs/day
2018 Quarter 1 2.1 / mg/L 1.2481 / lbs/day
2018 1st 6 Months(Avg) 2.1 / mg/L 1.2481 / lbs/day
2018 1st 6...(Max) 2.2 / mg/L 1.6403 / lbs/day
2018 1st 6...(Min) 2 / mg/L 0.8559 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Biogen0118Flow 0.072306 /0.375 MGD /
02/28/2018 S Biogen0218Flow 0.049254 /0.375 MGD /
03/31/2018 S Biogen0318Flow 0.053557 /0.375 MGD /
04/30/2018 S Biogen0418Flow 0.062309 /0.375 MGD /
05/31/2018 S Biogen0518Flow 0.069327 /0.375 MGD /
06/30/2018 S Biogen0618Flow 0.073605 /0.375 MGD /
Jan 2018 Week 4 0.072306 / MGD /
Feb 2018 Week 4 0.049254 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 10

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Mar 2018 Week 4 0.053557 / MGD /
Apr 2018 Week 4 0.062309 / MGD /
May 2018 Week 4 0.069327 / MGD /
Jun 2018 Week 4 0.073605 / MGD /
Jan 2018 Average 0.072306 /0.250 MGD /
' Feb 2018 Average 0.049254 /0.250 MGD /
Mar 2018 Average 0.053557 /0.250 MGD /
Apr 2018 Average 0.062309 /0.250 MGD /
May 2018 Average 0.069327 /0.250 MGD /
Jun 2018 Average 0.073605 /0.250 MGD /
2018 Quarter 1 0.058372 / MGD /
2018 Quarter 2 0.068414 / MGD /
2018 1st 6 Months(Avg) 0.063393 / MGD /
2018 1st 6...(Max) 0.073605 / MGD /
2018 1st 6...(Min) 0.049254 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
01/25/2018 P Biogen012518POTW 125 / mg/L 93.2 / lbs/day
02/07/2018 S Biogen020718Self 38.2 / mg/L 16.348 / lbs/day
Jan 2018 Week 4 125 / mg/L 93.2 / lbs/day
Feb 2018 Week 1 38.2 / mg/L 16.348 / lbs/day
Jan 2018 Average 125 / mg/L 93.2 / lbs/day
Feb 2018 Average 38.2 / mg/L 16.348 / lbs/day
2018 Quarter 1 81.6 / mg/L 54.774 / lbs/day
2018 1st 6 Months(Avg) 81.6 / mg/L 54.774 / lbs/day
2018 1st 6...(Max) 125 / mg/L 93.200 / lbs/day
2018 1st 6...(Min) 38.2 / mg/L 16.348 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 10

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/25/2018 P Biogen012518POTW < 0.00008 / mg/L < 0.000056 / lbs/day
02/07/2018 S Biogen020718Self < 0.0005 / mg/L < 0.000214 / lbs/day
Jan 2018 Week 4 < 0.00008 / mg/L < 0.000056 / lbs/day
Feb 2018 Week 1 < 0.0005 / mg/L < 0.000214 / lbs/day
Jan 2018 Average < 0.00008 / mg/L < 0.000056 / lbs/day
Feb 2018 Average < 0.0005 / mg/L < 0.000214 / lbs/day
2018 Quarter 1 < 0.00029 / mg/L < 0.000135 / lbs/day
2018 1st 6 Months(Avg) < 0.00029 / mg/L < 0.000135 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000214 / lbs/day
2018 1st 6...(Min) < 0.00008 / mg/L < 0.000056 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/25/2018 P Biogen012518POTW 47 / mg/L 35.043 / lbs/day
02/07/2018 S Biogen020718Se1f 269 / mg/L 115.1231 / lbs/day
Jan 2018 Week 4 47 / mg/L 35.043 / lbs/day
Feb 2018 Week 1 269 / mg/L 115.1231 / lbs/day
Jan 2018 Average 47 / mg/L 35.043 / lbs/day
Feb 2018 Average 269 / mg/L 115.1231 / lbs/day
2018 Quarter 1 158 / mg/L 75.0831 / lbs/day
2018 1st 6 Months(Avg) 158 / mg/L 75.0831 / lbs/day
2018 1st 6...(Max) 269 / mg/L 115.1231 / lbs/day
2018 1st 6...(Min) 47 / mg/L 35.0430 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
01/25/2018 P Biogen012518POTW 199 / mg/L 148.37 / lbs/day
02/07/2018 S Biogen020718Self 88 / mg/L 37.66 / lbs/day
Jan 2018 Week 4 199 / mg/L 148.37 / lbs/day
Feb 2018 Week 1 88 / mg/L 37.66 / lbs/day
Jan 2018 Average 199 / mg/L 148.37 / lbs/day
Feb 2018 Average 88 / mg/L 37.66 / lbs/day
2018 Quarter 1 143.5 / mg/L 93.02 / lbs/day
2018 1st 6 Months(Avg) 143.5 / mg/L 93.02 / lbs/day
2018 1st 6...(Max) 199 / mg/L 148.37 / lbs/day
2018 1st 6...(Min) 88 / mg/L 37.66 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

Bioeen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
01/16/2018 P Biogen011618POTW < 0.005 / 12.19 mg/L < 0.0023 / lbs/day
Jan 2018 Week 3 < 0.005 / mg/L < 0.0023 / lbs/day
Jan 2018 Average < 0.005 /4.83 mg/L < 0.0023 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/25/2018 P Biogen012518POTW 0.97 / mg/L 0.7232 / lbs/day
02/07/2018 S Biogen020718Self 0.7 / mg/L 0.2996 / lbs/day
Jan 2018 Week 4 0.97 / mg/L 0.7232 / lbs/day
Feb 2018 Week 1 0.7 / mg/L 0.2996 / lbs/day
Jan 2018 Average 0.97 / mg/L 0.7232 / lbs/day
Feb 2018 Average 0.7 / mg/L 0.2996 / lbs/day
2018 Quarter 1 0.84 / mg/L 0.5114 / lbs/day
2018 1st 6 Months(Avg) 0.84 / mg/L 0.5114 / lbs/day
2018 1st 6...(Max) 0.97 / mg/L 0.7232 / lbs/day
2018 1st 6...(Min) 0.7 / mg/L 0.2996 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
01/16/2018 P Biogen011618POTW < 0.005 / 12.19 mg/L < 0.0023 / lbs/day
Jan 2018 Week 3 < 0.005 / mg/L < 0.0023 / lbs/day
Jan 2018 Average < 0.005 /4.83 mg/L < 0.0023 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Count) I / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10
t

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/16/2018 P Biogen011618POTWH 0.000026 /0.000142 mg/L /
g
03/24/2018 S Biogen032418SelfHg 0.000005 /0.000142 mg/L /
05/11/2018 P Biogen051118POTWH 0.000022 /0.000142 mg/L /
g
Jan 2018 Week 3 0.000026 / mg/L /
Mar 2018 Week 4 0.000005 / mg/L /
May 2018 Week 2 0.000022 / mg/L /
Jan 2018 Average 0.000026 / mg/L /
Mar 2018 Average 0.000005 / mg/L /
May 2018 Average 0.000022 / mg/L /
2018 • Quarter 1 0.000016 / mg/L /
2018 Quarter 2 0.000022 / mg/L /
2018 1st 6 Months(Avg) 0.0000177 / mg/L /
2018 1st 6...(Max) 0.0000263 / mg/L /
2018 1st 6...(Min) 0.0000047 / mg/L /
2018 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Masts/Limit
Methylene Chloride
01/16/2018 P Biogen011618POTW < 0.005 / 1.77 mg/L < 0.002271 / lbs/day
Jan 2018 Week 3 < 0.005 / mg/L < 0.002271 / lbs/day
Jan 2018 Average < 0.005 /0.41 mg/L < 0.002271 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.002271 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.002271 / lbs/day
2018 1st 6•...(Max) < 0.005 / mg/L < 0.002271 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.002271 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample!!) Result/Limit Mass/Limit
Methylene Chloride
2018 1st 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/25/2018 P Biogen012518POTW < 0.001 / mg/L < 0.0007 / lbs/day
Jan 2018 Week 4 < 0.001 / mg/L < 0.0007 / lbs/day
Jan 2018 Average < 0.001 / mg/L < 0.0007 / lbs/day
2018 Quarter 1 < 0.001 / mg/L < 0.0007 / lbs/day
2018 1st 6 Months(Avg) < 0.001 / mg/L < 0.0007 / lbs/day
2018 1st 6...(Max) < 0.001 / mg/L < 0.0007 / lbs/day
2018 1st 6...(Min) < 0.001 / mg/L < 0.0007 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date Sample!D Result/Limit Mass/Limit
n-Amyl acetate
01/16/2018 P Biogen011618POTW < 0.005 / 12.19 mg/L < 0.0023 / lbs/day
Jan 2018 Week 3 < 0.005 / mg/L < 0.0023 / lbs/day
Jan 2018 Average < 0.005 /4.83 mg/L < 0.0023 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.0023 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10
i

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001 1
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite •
01/25/2018 P Biogen012518POTW 0.7 / mg/L 0.5 / lbs/day
02/07/2018 S Biogen020718Se1f 0.6 / mg/L 0.24 / lbs/day
Jan 2018 Week 4 0.7 / mg/L 0.5 / lbs/day
Feb 2018 Week 1 0.6 / mg/L 0.24 / lbs/day
Jan 2018 Average 0.7 / mg/L 0.5 / lbs/day
Feb 2018 Average 0.6 / mg/L 0.24 / lbs/day
2018 Quarter 1 0.6 / mg/L 0.37 / lbs/day
2018 1st 6 Months(Avg) 0.6 / mg/L 0.370 / lbs/day
2018 1st 6...(Max) 0.7 / mg/L 0.500 / lbs/day
2018 1st 6...(Min) 0.6 / mg/L 0.240 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/25/2018 P Biogen012518POTW 11.3 / mg/L 8.425 / lbs/day
02/07/2018 S Biogen020718Self 9.5 / mg/L 4.066 / lbs/day
Jan 2018 Week 4 11.3 / mg/L 8.425 / lbs/day
Feb 2018 Week 1 9.5 / mg/L 4.066 / lbs/day
Jan 2018 Average 11.3 / mg/L 8.425 / lbs/day
Feb 2018 Average 9.5 / mg/L 4.066 / lbs/day
2018 Quarter 1 10.4 / mg/L 6.245 / lbs/day
2018 1st 6 Months(Avg) 10.4 / mg/L 6.245 / lbs/day
2018 1st 6...(Max) 11.3 / mg/L 8.425 / lbs/day
2018 l st 6...(Min) 9.5 / mg/L 4.066 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/16/2018 P Biogen011618POTW < 2.5 /200 mg/L < /
Jan 2018 Week 3 < 2.5 / mg/L < /
Jan 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 1 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

Biogeq
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/16/2018 P Biogen011618POTW 7.6 /5.5- 10.5 SU /
02/07/2018 S Biogen020718Se1f 7.48 /5.5- 10.5 SU /
Jan 2018 Week 3 7.6 / SU /
Feb 2018 Week 1 7.48 / SU /
Jan 2018 Average 7.6 / SU /
Feb 2018 Average 7.48 / SU /
2018 Quarter 1 7.54 / SU /
2018 1st 6 Months(Avg) 7.54 / SU /
2018 1st 6...(Max) 7.6 / SU /
2018 1st 6...(Min) 7.48 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
•
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/16/2018 P Biogen011618POTW 13 /66 °C /
Jan 2018 Week 3 13 / °C /
Jan 2018 Average 13 / °C /
2018 Quarter 1 13 / °C /
2018 1st 6 Months(Avg) 13 / °C /
2018 1st 6...(Max) 13 / °C /
2018 1st 6...(Min) 13 / °C /
2018 1st 6...(Count) 1 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10

Biogen
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/25/2018 P Biogen012518POTW 10.6 / mg/L 7.903 / lbs/day
02/07/2018 S Biogen020718Se1f 8.9 / mg/L 3.809 / lbs/day
Jan 2018 Week 4 10.6 / mg/L 7.903 / lbs/day
Feb 2018 Week 1 8.9 / mg/L 3.809 / lbs/day
Jan 2018 Average 10.6 / mg/L 7.903 / lbs/day
Feb 2018 Average 8.9 / mg/L 3.809 / lbs/day
2018 Quarter 1 9.75 / mg/L 5.856 / lbs/day
2018 1st 6 Months(Avg) 9.75 / mg/L 5.856 / lbs/day
2018 1st 6...(Max) 10.6 / mg/L 7.903 / lbs/day
2018 1st 6...(Min) 8.9 / mg/L 3.809 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/25/2018 P Biogen012518POTW 1.7 / mg/L 1.2675 / lbs/day
02/07/2018 S Biogen020718Self 1.4 / mg/L 0.5992 / lbs/day
Jan 2018 Week 4 1.7 / mg/L 1.2675 / lbs/day
Feb 2018 Week 1 1.4 / mg/L 0.5992 / lbs/day
Jan 2018 Average 1.7 / mg/L 1.2675 / lbs/day
Feb 2018 Average 1.4 / mg/L 0.5992 / lbs/day
2018 Quarter 1 1.55 / mg/L 0.9333 / lbs/day
2018 1st 6 Months(Avg) 1.55 / mg/L 0.9333 / lbs/day
2018 1st 6...(Max) 1.7 / mg/L 1.2675 / lbs/day
2018 1st 6...(Min) 1.4 / mg/L 0.5992 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
01/25/2018 P Biogen012518POTW 336 / mg/L 250.520256 / lbs/day
02/07/2018 S Biogen020718Self 22.2 / mg/L 9.50087 / lbs/day
Jan 2018 Week 4 336 / mg/L 250.520256 / lbs/day
Feb 2018 Week 1 22.2 / mg/L 9.50087 / lbs/day
Jan 2018 Average 336 / mg/L 250.520256 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

Bio2en
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Effluent Sam le T e: Wastewater Out all: 001
P YP f
Sample Date SamplelD Result/Limit Mass/Limit
TSS
Feb 2018 Average 22.2 / mg/L 9.50087 / lbs/day
2018 Quarter 1 179.1 / mg/L 130.010563 / lbs/day
2018 1st 6 Months(Avg) 179.1 / mg/L 130.011 / lbs/day
2018 1st 6...(Max) 336 / mg/L 250.520256 / lbs/day
2018 1st 6...(Min) 22.2 / mg/L 9.500870 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/07/2018 S Biogen020718Self < 0.001 / mg/L < /
Feb 2018 Week 1 < 0.001 / mg/L < /
Feb 2018 Average < 0.001 / mg/L < /
2018 Quarter 1 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/25/2018 P Biogen012518POTW 0.67 / mg/L 0.499549 / lbs/day
02/07/2018 S Biogen020718Self 0.796 / mg/L 0.340662 / lbs/day
Jan 2018 Week 4 0.67 / mg/L 0.499549 / lbs/day
Feb 2018 Week 1 0.796 / mg/L 0.340662 / lbs/day
Jan 2018 Average 0.67 / mg/L 0.499549 / lbs/day
Feb 2018 Average 0.796 / mg/L 0.340662 / lbs/day
2018 Quarter 1 0.733 / mg/L 0.420106 / lbs/day
2018 1st 6 Months(Avg) 0.733 / mg/L 0.420106 / lbs/day
2018 1st 6...(Max) 0.796 / mg/L 0.499549 / lbs/day
2018 1st 6...(Min) 0.67 / mg/L 0.340662 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10
I-

r
Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
05/25/2018 P Braeburn052518POT 12.3 / 13.1 mg/L /
W
May 2018 Week 4 12.3 / mg/L /
May 2018 Average 12.3 /5.1 mg/L * * /
2018 Quarter 2 12.3 / mg/L /
2018 1st 6 Months(Avg) 12.3 / mg/L /
2018 1st 6...(Max) 12.3 / mg/L /
2018 1st 6...(Min) 12.3 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: I 100.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 1 100.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/24/2018 S Braeburn0118Flow 0.000349 / MGD /
02/22/2018 S Braeburn0218Flow 0.000291 / MGD /
03/20/2018 S Braeburn0318Flow 0.000252 / MGD /
04/18/2018 S Braeburn0418Flow 0.000283 / MGD /
05/21/2018 S Braeburn0518Flow 0.000253 / MGD /
06/20/2018 S Braeburn0618Flow 0.000253 / MGD /
Jan 2018 Week 4 0.000349 / MGD /
Feb 2018 Week 4 0.000291 / MGD /
Mar 2018 Week 3 0.000252 / MGD /
Apr 2018 Week 3 0.000283 / MGD /
May 2018 Week 3 0.000253 / MGD /
Jun 2018 Week 3 0.000253 / MGD /
Jan 2018 Average 0.000349 /0.010 MGD /
Feb 2018 Average 0.000291 /0.010 MGD /
Mar 2018 Average 0.000252 /0.010 MGD /
Apr 2018 Average 0.000283 /0.010 MGD /
May 2018 Average 0.000253 /0.010 MGD /
Jun 2018 Average 0.000253 /0.010 MGD /
2018 Quarter 1 0.000297 / MGD /
2018 Quarter 2 0.000263 / MGD /
2018 1st 6 Months(Avg) 0.000280 / MGD /
2018 1st 6...(Max) 0.000349 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 6

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Ouifall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2018 lst6...(Min) 0.000252 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
05/25/2018 P Braeburn052518POT < 0.00008 / mg/L < /
W
May 2018 Week 4 < 0.00008 / mg/L < /
May 2018 Average < 0.00008 / mg/L < /
2018 Quarter 2 < 0.00008 / mg/L < /
2018 1st 6 Months(Avg) < 0.00008 / mg/L < /
2018 1st 6...(Max) < 0.00008 / mg/L < /
2018 1st 6...(Min) < 0.00008 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
05/25/2018 P Braeburn052518POT 68 / mg/L /
W
May 2018 Week 4 68 / mg/L /
May 2018 Average 68 / mg/L /
2018 Quarter 2 68 / mg/L /
2018 1st 6 Months(Avg) 68 / mg/L /
2018 1st 6...(Max) 68 / mg/L /
2018 1st 6...(Min) 68 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
05/25/2018 P Braebutn052518POT < 0.001 / 13.1 mg/L < /
W
May 2018 Week 4 < 0.001 / mg/L < /
May 2018 Average < 0.001 /5.1 mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 6
I•

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over DailyC TRC: #Over Mo AvgC TRC: 0 0.00 #Over Wk AvgC TRC: 0 0.00 #Over Qt AvgC TRC: 0 0.00
0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
05/25/2018 P Braeburn052518POT < 0.001 / 13.1 mg/L < /
W
May 2018 Week 4 < 0.001 / mg/L < /
May 2018 Average < 0.001 /5.1 mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
05/24/2018 P Braeburn052418Hg 0.000003 /0.000142 mg/L /
May 2018 Week 4 0.000003 / mg/L /
May 2018 Average 0.000003 / mg/L /
2018 Quarter 2 0.000003 / mg/L /
2018 1st 6 Months(Avg) 0.0000034 / mg/L /
2018 1st 6...(Max) 0.0000034 / mg/L /
2018 1st 6...(Min) 0.0000034 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 6
4

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
05/25/2018 P Braeburn052518POT < 0.001 / 1.8 mg/L < /
W
May 2018 Week 4 < 0.001 / mg/L < /
May 2018 Average < 0.001 /0.4 mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
05/25/2018 P Braebum052518POT < 0.001 / 13.1 mg/L < /
W
May 2018 Week 4 < 0.001 / mg/L < /
May 2018 Average < 0.001 /5.1 mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.001 / mg/L < /
2018 1st 6...(Max) < 0.001 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 1 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 6

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
05/25/2018 P Braebum052518POT 6.2 /6- 10 SU /
W
May 2018 Week 4 6.2 / SU /
May 2018 Average 6.2 / SU /
2018 Quarter 2 6.2 / SU /
2018 1st 6 Months(Avg) 6.2 / SU /
2018 1st 6...(Max) 6.2 / SU /
2018 1st 6...(Min) 6.2 / SU /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
05/25/2018 P Braeburn052518POT 27 /66 °C /
W
May 2018 Week 4 27 / °C /
May 2018 Average 27 / °C /
2018 , Quarter 2 27 / °C /
2018 1st 6 Months(Avg) 27 / °C /
2018 1st 6...(Max) 27 / °C /
2018 1st 6...(Min) 27 / °C /
2018 1st 6...(Count) 1 / /
**
Monday,February25,2019 Indicates Violation Indicates TRC Violation Page 5 of 6
g

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
VOC
05/25/2018 P Braeburn052518POT 12.3 / mg/L /
W
May 2018 Week 4 12.3 / mg/L /
May 2018 Average 12.3 / mg/L /
2018 Quarter 2 12.3 / mg/L /
2018 1st 6 Months(Avg) 12.3 / mg/L /
2018 1st 6...(Max) 12.3 / mg/L /
2018 1st 6...(Min) 12.3 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
05/25/2018 P Braeburn052518POT 0.014 / mg/L /
W
May 2018 Week 4 0.014 / mg/L /
May 2018 Average 0.014 / mg/L /
2018 Quarter 2 0.014 / mg/L /
2018 1st 6 Months(Avg) 0.014 / mg/L /
2018 1st6...(Max) 0.014 / mg/L /
2018 1st 6...(Min) 0.014 / mg/L /
2018 1st 6...(Count) 1 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 6

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
06/12/2018 S Cintas061218Self 0.344 / mg/L 0.2386 / lbs/day
Jun 2018 Week 2 0.344 / mg/L 0.2386 / lbs/day
Jun 2018 Average 0.344 / mg/L 0.2386 / lbs/day
2018 Quarter 2 0.344 / mg/L 0.2386 / lbs/day
2018 1st 6 Months(Avg) 0.344 / mg/L 0.2386 / lbs/day
2018 1st 6...(Max) 0.344 / mg/L 0.238600 / lbs/day
2018 1st 6...(Min) 0.344 / mg/L 0.238600 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/16/2018 P Cintas011618POTW 1.1 / mg/L 0.6508 / lbs/day
01/17/2018 S Cintas011718Self 11.1 / mg/L 5.045 / lbs/day
02/20/2018 S Cintas022018Self 12.6 / mg/L 7.328 / lbs/day
03/28/2018 S Cintas032818Se1f 12.3 / mg/L 6.9766 / lbs/day
04/17/2018 S Cintas041718Se1f 17.6 / mg/L 7.7005 / lbs/day
05/02/2018 S Cintas050218Self 33 / mg/L 19.4812 / lbs/day
06/12/2018 S Cintas061218Self 29 / mg/L 20.1145 / lbs/day
Jan 2018 Week 3 6.1 / mg/L 2.8479 / lbs/day
Feb 2018 Week 3 12.6 / mg/L 7.328 / lbs/day
Mar 2018 Week 4 12.3 / mg/L 6.9766 / lbs/day
May 2018 Week 1 33 / mg/L 19.4812 / lbs/day
Apr 2018 Week 3 17.6 / mg/L 7.7005 / lbs/day
Jun 2018 Week 2 29 / mg/L 20.1145 / lbs/day
Jan 2018 Average 6.1 / mg/L 2.8479 / lbs/day
Feb 2018 Average 12.6 / mg/L 7.328 / lbs/day
Mar 2018 Average 12.3 / mg/L 6.9766 / lbs/day
Apr 2018 Average 17.6 / mg/L 7.7005 / lbs/day
May 2018 Average 33 / mg/L 19.4812 / lbs/day
Jun 2018 Average 29 / mg/L 20.1145 / lbs/day
2018 Quarter 1 9.28 / mg/L 5.0001 / lbs/day
2018 Quarter 2 26.53 / mg/L 15.7654 / lbs/day
2018 1st 6 Months(Avg) 16.67 / mg/L 9.6138 / lbs/day
2018 1st 6...(Max) 33 / mg/L 20.1145 / lbs/day
2018 1st 6...(Min) 1.1 / mg/L 0.6508 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Cintas0118Flow 0.061623 /0.180 MGD /
02/28/2018 S Cintas0218F1ow 0.05441 /0.180 MGD /
03/31/2018 S Cintas0318Flow 0.061825 /0.180 MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
04/30/2018 Cintas0418F1ow 0.053518 /0.180 MGD /
05/31/2018 S Cintas0518F1ow 0.058507 /0.180 MGD /
06/30/2018 S Cintas0618F1ow 0.065313 /0.180 MGD /
Jan 2018 Week 4 0.061623 / MGD /
Feb 2018 Week 4 0.05441 / MGD /
Mar 2018 Week 4 0.061825 / MGD /
Apr 2018 Week 4 0.053518 / MGD /
May 2018 Week 4 0.058507 / MGD /
Jun 2018 Week 4 0.065313 / MGD /
Jan 2018 Average 0.061623 /0.120 MGD /
Feb 2018 Average 0.05441 /0.120 MGD /
Mar 2018 Average 0.061825 /0.120 MGD /
Apr 2018 Average 0.053518 /0.120 MGD /
May 2018 Average 0.058507 /0.120 MGD /
Jun 2018 Average 0.065313 /0.120 MGD /
2018 Quarter 1 0.059286 / MGD /
2018 Quarter 2 0.059113 / MGD /
2018 1st 6 Months(Avg) 0.059199 / MGD /
2018 1st 6...(Max) 0.065313 / MGD /
2018 1st 6...(Min) 0.053518 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
01/16/2018 P Cintas011618POTW 725 / mg/L 428.933 / lbs/day
01/17/2018 S Cintas011718Self 697 / mg/L 316.79 / lbs/day
02/20/2018 P Cintas022018POTW 478 / mg/L /
02/20/2018 S Cintas022018Se1f 304 / mg/L 176.803 / lbs/day
03/23/2018 P Cintas032318POTW 178 / mg/L /
03/28/2018 S Cintas032818Se1f 1930 / mg/L 1094.703 / lbs/day
04/17/2018 S Cintas041718Self 1120 / mg/L 490.032 / lbs/day
04/19/2018 P Cintas041918POTW 690 / mg/L /
05/02/2018 S Cintas050218SeIf 515 / mg/L 304.024 / lbs/day
05/18/2018 P Cintas051818POTW 325 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
06/12/2018 S Cintas061218Se1f 272 / mg/L 188.66 / lbs/day
06/12/2018 P Cintas061218POTW 1197 / mg/L /
Jan 2018 Week 3 711 / mg/L 372.861 / lbs/day
Feb 2018 Week 3 391 / mg/L 176.803 / lbs/day
Mar 2018 Week 4 1054 / mg/L 1094.703 / lbs/day
Apr 2018 Week 3 905 / mg/L 490.032 / lbs/day
May 2018 Week 1 515 / mg/L 304.024 / lbs/day
May 2018 Week 3 325 / mg/L /
Jun 2018 Week 2 734.5 / mg/L 188.66 / lbs/day
Jan 2018 Average 711 / mg/L 372.861 / lbs/day
Feb 2018 Average 391 / mg/L 176.803 / lbs/day
Mar 2018 Average 1054 / mg/L 1094.703 / lbs/day
Apr 2018 Average 905 / mg/L 490.032 / lbs/day
May 2018 Average 420 / mg/L 304.024 / lbs/day
Jun 2018 Average 734.5 / mg/L 188.66 / lbs/day
2018 Quarter 1 718.7 / mg/L 504.307 / lbs/day
2018 Quarter 2 686.5 / mg/L 327.572 / lbs/day
2018 1st 6 Months(Avg) 702.6 / mg/L 428.564 / lbs/day
2018 1st 6...(Max) 1930 / mg/L 1094.703 / lbs/day
2018 1st 6...(Min) 178 / mg/L /
2018 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
06/12/2018 S Cintas061218Self < 0.0005 / mg/L < 0.000347 / lbs/day
Jun 2018 Week 2 < 0.0005 / mg/L < 0.000347 / lbs/day
Jun 2018 Average < 0.0005 / mg/L < 0.000347 / lbs/day
2018 Quarter 2 < 0.0005 / mg/L < 0.000347 / lbs/day
2018 1st 6 Months(Avg) < 0.0005 / mg/L < 0.000347 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000347 / lbs/day
2018 1st 6...(Min) < 0.0005 / mg/L < 0.000347 / lbs/day
2018 1st 6...(Count) 1 / I /
Sample Date SampleID Result/Limit Mass/Limit
Chloride
01/16/2018 P Cintas011618POTW 246 / mg/L 145.5413 / lbs/day
06/12/2018 S Cintas061218Se1f 99.6 / mg/L 69.083 / lbs/day
Jan 2018 Week 3 246 / mg/L 145.5413 / lbs/day
Jun 2018 Week 2 99.6 / mg/L 69.083 / lbs/day
Jan 2018 Average 246 / mg/L 145.5413 / lbs/day
Jun 2018 Average 99.6 / mg/L 69.083 / lbs/day
2018 Quarter 1 246 / mg/L 145.5413 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2018 Quarter 2 99.6 / mg/L 69.083 / lbs/day
2018 1st 6 Months(Avg) 172.8 / mg/L 107.312 / lbs/day
2018 1st 6...(Max) 246 / mg/L 145.5413 / lbs/day
2018 1st 6...(Min) 99.6 / mg/L 69.0830 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
01/17/2018 S Cintas011718Self 0.037 / mg/L 0.016817 / lbs/day
02/20/2018 S Cintas022018Self 0.011 / mg/L 0.006456 / lbs/day
03/28/2018 S Cintas032818Self 0.106 / mg/L 0.060124 / lbs/day
04/17/2018 S Cintas041718Self 0.048 / mg/L 0.021133 / lbs/day
05/02/2018 S Cintas050218Se1f 0.026 / mg/L 0.015113 / lbs/day
06/12/2018 S Cintas061218Se1f < 0.003 / mg/L < 0.001734 / lbs/day
Jan 2018 Week 3 0.037 / mg/L 0.016817 / lbs/day
Feb 2018 Week 3 0.011 / mg/L 0.006456 / lbs/day
Mar 2018 Week 4 0.106 / mg/L 0.060124 / lbs/day
Apr 2018 Week 3 0.048 / mg/L 0.021133 / lbs/day
May 2018 Week 1 0.026 / mg/L 0.015113 / lbs/day
Jun 2018 Week 2 < 0.003 / mg/L < 0.001734 / lbs/day
Jan 2018 Average 0.037 / mg/L 0.016817 / lbs/day
Feb 2018 Average 0.011 / mg/L 0.006456 / lbs/day
Mar 2018 Average 0.106 / mg/L 0.060124 / lbs/day
Apr 2018 Average 0.048 / mg/L 0.021133 / lbs/day
May 2018 Average 0.026 / mg/L 0.015113 / lbs/day
Jun 2018 Average < 0.003 / mg/L < 0.001734 / lbs/day
2018 Quarter 1 0.051 / mg/L 0.027799 / lbs/day
2018 Quarter 2 < 0.025 / mg/L < 0.01266 / lbs/day
2018 1st 6 Months(Avg) < 0.038 / mg/L < 0.020229 / lbs/day
2018 1st 6...(Max) 0.106 / mg/L 0.060124 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.001,734 / lbs/day
2018 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/17/2018 S Cintas011718Self 0.193 / mg/L 0.087719 / lbs/day
02/20/2018 S Cintas022018Self 0.091 / mg/L 0.052634 / lbs/day
03/28/2018 S Cintas032818Self 0.563 / mg/L 0.319336 / lbs/day
04/17/2018 S Cintas041718Self 0.215 / mg/L 0.094069 / lbs/day
05/02/2018 S Cintas050218Self 0.152 / mg/L 0.089731 / lbs/day
06/12/2018 S Cintas061218Self 0.036 / mg/L 0.025039 / lbs/day
Jan 2018 Week 3 0.193 / mg/L 0.087719 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Feb 2018 Week 3 0.091 / mg/L 0.052634 / lbs/day
Mar 2018 Week 4 0.563 / ' mg/L 0.319336 / lbs/day
Apr 2018 Week 3 0.215 / mg/L 0.094069 / lbs/day
May 2018 Week 1 0.152 / mg/L 0.089731 / lbs/day
Jun 2018 Week 2 0.036 / mg/L 0.025039 / lbs/day
Jan 2018 Average 0.193 / mg/L 0.087719 / lbs/day
Feb 2018 Average 0.091 / mg/L 0.052634 / lbs/day
Mar 2018 Average 0.563 / mg/L 0.319336 / lbs/day
Apr 2018 Average 0.215 / mg/L 0.094069 / lbs/day
May 2018 Average 0.152 / mg/L 0.089731 / lbs/day
Jun 2018 Average 0.036 / mg/L 0.025039 / lbs/day
2018 Quarter 1 0.282 / mg/L 0.15323 / lbs/day
2018 Quarter 2 0.134 / mg/L 0.069613 / lbs/day
2018 1st 6 Months(Avg) 0.208 / mg/L 0.111421 / lbs/day
2018 1st 6...(Max) 0.563 / mg/L 0.319336 / lbs/day
2018 1st 6...(Min) 0.036 / mg/L 0.025039 / lbs/day
2018 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Flow
04/17/2018 S Cintas041718Self ).052461500 /0.180 MGD /
Apr 2018 Week 3 0.052462 / MGD /
Apr 2018 Average 0.0524615 /0.120 MGD /
2018 Quarter 2 0.052462 / MGD /
2018 1st 6 Months(Avg) 0.052462 / MGD /
2018 1st 6...(Max) 0.052462 / MGD /
2018 1st 6...(Min) 0.052462 / MGD /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/16/2018 P Cintas011618POTW 0.4 / mg/L 0.2367 / lbs/day
01/17/2018 S Cintas011718Self 0.28 / mg/L 0.1273 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/20/2018 S Cintas022018SeIf < 0.05 / mg/L < 0.0291 / lbs/day
03/28/2018 S Cintas032818Self 0.29 / mg/L 0.1645 / lbs/day
04/17/2018 S Cintas041718Se1f < 0.05 / mg/L < 0.0219 / lbs/day
05/02/2018 S Cintas050218Se1f < 0.05 / mg/L < 0.0295 / lbs/day
06/12/2018 S Cintas061218Self < 0.05 / mg/L < 0.0347 / lbs/day
Jan 2018 Week 3 0.34 / mg/L 0.182 / lbs/day
Feb 2018 Week 3 < 0.05 / mg/L < 0.0291 / lbs/day
Y
Mar 2018 Week 4 0.29 / mg/L 0.1645 / lbs/day
Apr 2018 Week 3 < 0.05 / mg/L < 0.0219 / lbs/day
May 2018 Week 1 < 0.05 / mg/L < 0.0295 / lbs/day
Jun 2018 Week 2 < 0.05 / mg/L < 0.0347 / lbs/day
Jan 2018 Average 0.34 / mg/L 0.182 / lbs/day
Feb 2018 Average < 0.05 / mg/L < 0.0291 / lbs/day
Mar 2018 Average 0.29 / mg/L 0.1645 / lbs/day
Apr 2018 Average < 0.05 / mg/L < 0.0219 / lbs/day
May 2018 Average < 0.05 / mg/L < 0.0295 / lbs/day
Jun 2018 Average < 0.05 / mg/L < 0.0347 / lbs/day
2018 Quarter 1 < 0.26 / mg/L < 0.1394 I lbs/day
2018 Quarter 2 < 0.05 / mg/L < 0.0287 / lbs/day
2018 1st 6 Months(Avg) < 0.17 / mg/L < 0.0919 / lbs/day
2018 1st 6...(Max) 0.4 / mg/L 0.2367 / lbs/day
2018 1st 6...(Min) < 0.05 / mg/L < 0.0219 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
01/17/2018 S Cintas011718Se1f 0.028 / mg/L 0.012726 / lbs/day
02/20/2018 S Cintas022018Self 0.0204 / mg/L 0.011864 / lbs/day
03/28/2018 S Cintas032818Self 0.0887 / mg/L 0.050311 / lbs/day
04/17/2018 S Cintas041718Self 0.0326 / mg/L 0.014263 / lbs/day
05/02/2018 S Cintas050218Self 0.0203 / mg/L 0.011984 / lbs/day
06/12/2018 S Cintas061218Self < 0.0025 / mg/L < 0.001734 / lbs/day
Jan 2018 Week 3 0.028 / mg/L 0.012726 / lbs/day
Feb 2018 Week 3 0.0204 / mg/L 0.011864 / lbs/day
Mar 2018 Week 4 0.0887 / mg/L 0.050311 / lbs/day
Apr 2018 Week 3 0.0326 / mg/L 0.014263 / lbs/day
May 2018 Week 1 0.0203 / mg/L 0.011984 / lbs/day
Jun 2018 Week 2 < 0.0025 / mg/L < 0.001734 / lbs/day
Jan 2018 Average 0.028 / mg/L 0.012726 / lbs/day
Feb 2018 Average 0.0204 / mg/L 0.011864 / lbs/day
Mar 2018 Average 0.0887 / mg/L 0.050311 / lbs/day
Apr 2018 Average 0.0326 / mg/L 0.014263 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 16

F
Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Lead
May 2018 Average 0.0203 / mg/L 0.011984 / lbs/day
Jun 2018 Average < 0.0025 / mg/L < 0.001734 / lbs/day
2018 Quarter 1 0.0457 / mg/L 0.024967 / lbs/day
2018 Quarter 2 < 0.0185 / mg/L < 0.009327 / lbs/day
2018 1st 6 Months(Avg) < 0.0321 / mg/L < 0.017147 / lbs/day
2018 1st 6...(Max) 0.0887 / mg/L 0.050311 / lbs/day
' 2018 1st 6...(Min) < 0.0025 / mg/L < 0.001734 / lbs/day
2018 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/15/2018 P Cintas011518POTWH 0.00006 /0.000142 mg/L /
g
Jan 2018 Week 3 0.00006 / mg/L /
Jan 2018 Average 0.00006 / mg/L /
2018 Quarter 1 0.00006 / mg/L /
2018 1st 6 Months(Avg) 0.0000599 / mg/L /
2018 1st 6...(Max) 0.0000599 / mg/L /
2018 1st 6...(Min) 0.0000599 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
06/12/2018 S Cintas061218Self 0 / mg/L 0.0069 / lbs/day
Jun 2018 Week 2 0 / mg/L 0.0069 / lbs/day
Jun 2018 Average 0 / mg/L 0.0069 / lbs/day
2018 Quarter 2 0 / mg/L 0.0069 / lbs/day
2018 1st 6 Months(Avg) 0.010 / mg/L 0.0069 / lbs/day
2018 1st 6...(Max) 0.010 / mg/L 0.0069 / lbs/day
2018 1st 6...(Min) 0.010 / mg/L 0.0069 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/17/2018 S Cintas011718Self 0.0402 / mg/L 0.018271 / lbs/day
02/20/2018 S Cintas022018Self 0.029 / mg/L 0.016866 / lbs/day
03/28/2018 S Cintas032818Se1f 0.0744 / mg/L 0.0422 / lbs/day
04/17/2018 S Cintas041718Self 0.0475 / mg/L 0.020783 / lbs/day
05/02/2018 S Cintas050218Self 0.0306 / mg/L 0.018064 / lbs/day
06/12/2018 S Cintas061218Self 0.0146 / mg/L 0.010127 / lbs/day
Jan 2018 Week 3 0.0402 / mg/L 0.018271 / lbs/day
Feb 2018 Week 3 0.029 / mg/L 0.016866 / lbs/day
Mar 2018 Week 4 0.0744 / mg/L 0.0422 / lbs/day
Apr 2018 Week 3 0.0475 / mg/L 0.020783 / lbs/day
May 2018 Week 1 0.0306 / mg/L 0.018064 / lbs/day
Jun 2018 Week 2 0.0146 / mg/L 0.010127 / lbs/day
Jan 2018 Average 0.0402 / mg/L 0.018271 / lbs/day
Feb 2018 Average 0.029 / mg/L 0.016866 / lbs/day
Mar 2018 Average 0.0744 / mg/L 0.0422 / lbs/day
Apr 2018 Average 0.0475 / mg/L 0.020783 / lbs/day
May 2018 Average 0.0306 / mg/L 0.018064 / lbs/day
Jun 2018 Average 0.0146 / mg/L 0.010127 / lbs/day
2018 Quarter 1 0.0479 / mg/L 0.025779 / lbs/day
2018 Quarter 2 0.0309 / mg/L 0.016325 / lbs/day
2018 1st 6 Months(Avg) 0.0394 / mg/L 0.021052 / lbs/day
2018 1st 6...(Max) 0.0744 / mg/L 0.042200 / lbs/day
2018 1st 6...(Min) 0.0146 / mg/L 0.010127 / lbs/day
2018 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/16/2018 P Cintas011618POTW 0.2 / mg/L 0.089 / lbs/day
01/17/2018 S Cintas011718Self 0.1 / mg/L 0.031 / lbs/day
02/20/2018 S Cintas022018Self 0 / mg/L 0.021 / lbs/day
03/28/2018 S Cintas032818Self 0.1 / mg/L 0.055 / lbs/day
04/17/2018 S Cintas041718Self 0.1 / mg/L 0.044 / lbs/day
05/02/2018 S Cintas050218Self 0.1 / mg/L 0.035 / lbs/day
06/12/2018 S Cintas061218Self < 0.1 / mg/L < 0.035 / lbs/day
Jan 2018 Week 3 0.1 / mg/L 0.06 / lbs/day
Feb 2018 Week 3 0 / mg/L 0.021 / lbs/day
Mar 2018 Week 4 0.1 / mg/L 0.055 / lbs/day
Apr 2018 Week 3 0.1 / mg/L 0.044 / lbs/day
May 2018 Week 1 0.1 / mg/L 0.035 / lbs/day
Jun 2018 Week 2 < 0.1 / mg/L < 0.035 / lbs/day
Jan 2018 Average 0.1 / mg/L 0.06 / lbs/day
Feb 2018 Average 0 / mg/L 0.021 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
Mar 2018 Average 0.1 / mg/L 0.055 / lbs/day
Apr 2018 Average 0.1 / mg/L 0.044 / lbs/day
May 2018 Average 0.1 / mg/L 0.035 / lbs/day
Jun 2018 Average < 0.1 / mg/L < 0.035 / lbs/day
2018 Quarter 1 0.1 / mg/L 0.049 / lbs/day
2018 Quarter 2 < 0.1 / mg/L < 0.038 / lbs/day
2018 1st 6 Months(Avg) < 0.1 / mg/L < 0.044 / lbs/day
2018 1st 6...(Max) 0.2 / mg/L 0.089 / lbs/day
2018 1st 6...(Min) 0.0 / mg/L 0.021 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/16/2018 P Cintas011618POTW 29.6 / mg/L 17.512 / lbs/day
01/17/2018 S Cintas011718Self 85.2 / mg/L 38.724 / lbs/day
02/20/2018 S Cintas022018Se1f 42.1 / mg/L 24.485 / lbs/day
03/28/2018 S Cintas032818Se1f 76.4 / mg/L 43.334 / lbs/day
04/17/2018 S Cintas041718Se1f 80 / mg/L 35.002 / lbs/day
05/02/2018 S Cintas050218Se1f 95.6 / mg/L 56.436 / lbs/day
06/12/2018 S Cintas061218Self 78.5 / mg/L 54.448 / lbs/day
Jan 2018 Week 3 57.4 / mg/L 28.118 / lbs/day
Feb 2018 Week 3 42.1 / mg/L 24.485 / lbs/day
1 Apr 2018 Week 3 80 / mg/L 35.002 / lbs/day
Mar 2018 Week 4 76.4 / mg/L 43.334 / lbs/day
May 2018 Week 1 95.6 / mg/L 56.436 / lbs/day
Jun 2018 Week 2 78.5 / mg/L 54.448 / lbs/day
Jan 2018 Average 57.4 / mg/L 28.118 / lbs/day
Feb 2018 Average 42.1 / mg/L 24.485 / lbs/day
Mar 2018 Average 76.4 / mg/L 43.334 / lbs/day
Apr 2018 Average 80 / mg/L 35.002 / lbs/day
May 2018 Average 95.6 / mg/L 56.436 / lbs/day
Jun 2018 Average 78.5 / mg/L 54.448 / lbs/day
2018 Quarter 1 58.33 / mg/L 31.014 / lbs/day
2018 Quarter 2 84.7 / mg/L 48.629 / lbs/day
2018 1st 6 Months(Avg) 69.63 / mg/L 38.563 / lbs/day
2018 1st 6...(Max) 95.6 / mg/L 56.436 / lbs/day
2018 1st 6...(Min) 29.6 / mg/L 17.512 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM (Polar)
01/16/2018 P Cintas011618POTW < 2.5 / 100 mg/L < 1.479078 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil& Grease,HEM(Polar)
01/17/2018 S Cintas011718Se1f 75.8 / 100 mg/L 34.451477 / lbs/day
02/20/2018 S Cintas022018Self 35.9 / 100 mg/L 20.879077 / lbs/day
03/28/2018 S Cintas032818Self 34.3 / 100 mg/L 19.455077 / lbs/day
04/17/2018 S Cintas041718Self 21.7 / 100 mg/L 9.494377 / lbs/day
05/02/2018 S Cintas050218Self 74.5 / 100 mg/L 43.980223 / lbs/day
06/12/2018 S Cintas061218Self 50.7 / 100 mg/L 35.165745 / lbs/day
Jan 2018 Week 3 < 39.2 / mg/L < 17.965278 / lbs/day
Feb 2018 Week 3 35.9 / mg/L 20.879077 / lbs/day
Mar 2018 Week 4 34.3 / mg/L 19.455077 / lbs/day
Apr 2018 Week 3 21.7 / mg/L 9.494377 / lbs/day
May 2018 Week 1 74.5 / mg/L 43.980223 / lbs/day
Jun 2018 Week 2 50.7 / mg/L 35.165745 / lbs/day
Jan 2018 Average < 39.2 / mg/L < 17.965278 / lbs/day
Feb 2018 Average 35.9 / mg/L 20.879077 / lbs/day
Mar 2018 Average 34.3 / mg/L 19.455077 / lbs/day
Apr 2018 Average 21.7 / mg/L 9.494377 / lbs/day
May 2018 Average 74.5 / mg/L 43.980223 / lbs/day
Jun 2018 Average 50.7 / mg/L 35.165745 / lbs/day
2018 Quarter 1 < 37.1 / mg/L < 19.066177 / lbs/day
2018 Quarter 2 49 / mg/L 29.546782 / lbs/day
2018 1st 6 Months(Avg) < 42.2 / mg/L < 23.5579 / lbs/day
2018 1st 6...(Max) 75.8 / mg/L 43.980223 / lbs/day
2018 1st 6...(Min) < 2.5 / mg/L < 1.479078 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM (Non-Polar)
01/16/2018 P Cintas011618POTW 7 / 100 mg/L 4.1414 / lbs/day
01/17/2018 S Cintas011718Se1f 32.5 / 100 mg/L 14.7714 / lbs/day
02/20/2018 S Cintas022018Self 10.1 / 100 mg/L 5.8741 / lbs/day
03/28/2018 S Cintas032818Self 28.2 / 100 mg/L 15.9951 / lbs/day
04/17/2018 S Cintas041718Self < 2.5 / 100 mg/L < 1.0938 / lbs/day
05/02/2018 S Cintas050218Self 27.9 / 100 mg/L 16.4704 / lbs/day
06/12/2018 S Cintas061218Self 14.2 / 100 mg/L 9.8492 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM (Non-Polar)
Jan 2018 Week 3 19.8 / mg/L 9.4564 / lbs/day
Feb 2018 Week 3 10.1 / mg/L 5.8741 / lbs/day
Mar 2018 Week 4 28.2 / mg/L 15.9951 / lbs/day
Apr 2018 Week 3 < 2.5 / mg/L < 1.0938 / lbs/day
May 2018 Week 1 27.9 / mg/L 16.4704 / lbs/day
Jun 2018 Week 2 14.2 / mg/L 9.8492 / lbs/day
Jan 2018 Average 19.8 / mg/L 9.4564 / lbs/day
Feb 2018 Average 10.1 / mg/L 5.8741 / lbs/day
Mar 2018 Average 28.2 / mg/L 15.9951 / lbs/day
Apr 2018 Average < 2.5 / mg/L < 1.0938 / lbs/day
May 2018 Average 27.9 / mg/L 16.4704 / lbs/day
Jun 2018 Average 14.2 / mg/L 9.8492 / lbs/day
2018 Quarter 1 19.5 / mg/L 10.1955 / lbs/day
2018 Quarter 2 < 14.9 / mg/L < 9.1378 / lbs/day
2018 1st 6 Months(Avg) < 17.5 / mg/L < 9.7422 / lbs/day
2018 1st 6...(Max) 32.5 / mg/L 16.4704 / lbs/day
2018 1st 6...(Min) < 2.5 / mg/L < 1.0938 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/16/2018 P Cintas011618POTW 7.6 /6.0- 10.5 SU /
01/17/2018 S Cintas011718Self 6.9 /6.0- 10.5 SU /
02/20/2018 S Cintas022018Se1f 7 /6.0- 10.5 SU /
03/28/2018 S Cintas032818Self 7.3 /6.0- 10.5 SU /
04/17/2018 S Cintas041718Self 7.5 /6.0- 10.5 SU /
05/02/2018 S Cintas050218Self 7.6 /6.0- 10.5 SU /
06/12/2018 S Cintas061218Self 6.8 /6.0- 10.5 SU /
Jan 2018 Week 3 7.25 / SU /
Feb 2018 Week 3 7 / SU /
Mar 2018 Week 4 7.3 / SU /
Apr 2018 Week 3 7.5 / SU /
May 2018 Week 1 7.6 / SU /
Jun 2018 Week 2 6.8 / SU /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
Jan 2018 Average 7.25 / SU /
Feb 2018 Average 7 / SU /
Mar 2018 Average 7.3 / SU /
Apr 2018 Average 7.5 / SU /
May 2018 Average 7.6 / SU /
Jun 2018 Average 6.8 / SU /
2018 Quarter 1 7.2 / SU /
2018 Quarter 2 7.3 / SU /
2018 1st 6 Months(Avg) 7.24 / SU /
2018 1st 6...(Max) 7.6 / SU /
2018 1st 6...(Min) 6.8 / SU /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
06/12/2018 S Cintas061218Self 0.573 / mg/L 0.397435 / lbs/day
Jun 2018 Week 2 0.573 / mg/L 0.397435 / lbs/day
Jun 2018 Average 0.573 / mg/L 0.397435 / lbs/day
2018 Quarter 2 0.573 / mg/L 0.397435 / lbs/day
2018 1st 6 Months(Avg) 0.573 / mg/L 0.397435 / lbs/day
2018 1st 6...(Max) 0.573 / mg/L 0.397435 / lbs/day
2018 1st 6...(Min) 0.573 / mg/L 0.397435 / lbs/day
2018 1st 6...(Count) 1 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/16/2018 P Cintas011618POTW 16 /66 °C /
01/17/2018 S Cintas011718Self 22 /66 °C /
02/20/2018 S Cintas022018Self 29.5 /66 °C /
03/28/2018 S Cintas032818Self 31.8 /66 °C /
04/17/2018 S Cintas041718Self 22.9 /66 °C /
05/02/2018 S Cintas050218Self 34.5 /66 °C /
06/12/2018 S Cintas061218Self 33.8 /66 °C /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 12 of 16
l

r
Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Jan 2018 Week 3 19 / °C /
Feb 2018 Week 3 29.5 / °C /
Mar 2018 Week 4 31.8 / °C /
Apr 2018 Week 3 22.9 / °C /
May 2018 Week 1 34.5 / °C /
Jun 2018 Week 2 33.8 / °C /
Jan 2018 Average 19 / °C /
Feb 2018 Average 29.5 / °C /
Mar 2018 Average 31.8 / °C /
Apr 2018 Average 22.9 / °C /
May 2018 Average 34.5 / °C /
Jun 2018 Average 33.8 / °C /
2018 Quarter 1 24.8 / °C /
2018 Quarter 2 30.4 / °C /
2018 1st 6 Months(Avg) 27.2 / °C /
2018 1st 6...(Max) 34.5 / °C /
2018 1st 6...(Min) 16 / °C /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # 0/0
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/16/2018 P Cintas011618POTW 29.4 / mg/L 17.394 / lbs/day
01/17/2018 S Cintas011718Self 85.2 / mg/L 38.724 / lbs/day
02/20/2018 P Cintas022018POTW 39.3 / mg/L /
02/20/2018 S Cintas022018Self 42 / mg/L 24.427 / lbs/day
03/23/2018 P Cintas032318POTW 45.5 / mg/L /
03/28/2018 S Cintas032818Self 76.3 / mg/L 43.278 / lbs/day
04/17/2018 S Cintas041718Self 79.9 / mg/L 34.959 / lbs/day
04/19/2018 P Cintas041918POTW 21 / mg/L /
05/02/2018 S Cintas050218Se1f 95.6 / mg/L 56.436 / lbs/day
05/18/2018 P Cintas051818POTW 50.1 / mg/L /
06/12/2018 S Cintas061218Self 78.5 / mg/L 54.448 / lbs/day
06/12/2018 P Cintas061218POTW 47.2 / mg/L /
Jan 2018 Week 3 57.3 / mg/L 28.059 / lbs/day 1
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 13 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Feb 2018 Week 3 40.65 / mg/L 24.427 / lbs/day
Mar 2018 Week 4 60.9 / mg/L 43.278 / lbs/day
Apr 2018 Week 3 50.45 / mg/L 34.959 / lbs/day
May 2018 Week 1 95.6 / mg/L 56.436 / lbs/day
May 2018 Week 3 50.1 / mg/L /
Jun 2018 Week 2 62.85 / mg/L 54.448 / lbs/day
Jan 2018 Average 57.3 / mg/L 28.059 / lbs/day
Feb 2018 Average 40.65 / mg/L 24.427 / lbs/day
Mar 2018 Average 60.9 / mg/L 43.278 / lbs/day
Apr 2018 Average 50.45 / mg/L 34.959 / lbs/day
May 2018 Average 72.85 / mg/L 56.436 / lbs/day
Jun 2018 Average 62.85 / mg/L 54.448 / lbs/day
2018 Quarter 1 52.95 / mg/L 30.956 / lbs/day
2018 Quarter 2 62.05 / mg/L 48.614 / lbs/day
2018 1st 6 Months(Avg) 57.5 / mg/L 38.524 / lbs/day
2018 1st 6...(Max) 95.6 / mg/L 56.436 / lbs/day
2018 1st 6...(Min) 21 / mg/L /
2018 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/16/2018 P Cintas011618POTW 3.53 / mg/L 2.0885 / lbs/day
01/17/2018 S Cintas011718Self 9.6 / mg/L 4.3632 / lbs/day
02/20/2018 P Cintas022018POTW 3.86 / mg/L /
02/20/2018 S Cintas022018Self 4.2 / mg/L 2.4427 / lbs/day
03/23/2018 P Cintas032318POTW 4.74 / mg/L /
03/28/2018 S Cintas032818Self 8.1 / mg/L 4.5943 / lbs/day
1 04/17/2018 S Cintas041718Self 9.6 / mg/L 4.2003 / lbs/day
04/19/2018 P Cintas041918POTW 2.66 / mg/L /
05/02/2018 S Cintas050218Self 8.4 / mg/L 4.9588 / lbs/day
05/18/2018 P Cintas051818POTW 6.56 / mg/L /
06/12/2018 S Cintas061218Self 8.2 / mg/L 5.6876 / lbs/day
06/12/2018 P Cintas061218POTW 6.72 / mg/L /
Jan 2018 Week 3 6.565 / mg/L 3.2259 / lbs/day
Feb 2018 Week 3 4.03 / mg/L 2.4427 / lbs/day
Mar 2018 Week 4 6.42 / mg/L 4.5943 / lbs/day
Apr 2018 Week 3 6.13 / mg/L 4.2003 / lbs/day
May 2018 Week 1 8.4 / mg/L 4.9588 / lbs/day
May 2018 Week 3 6.56 / mg/L /
Jun 2018 Week 2 7.46 / mg/L 5.6876 / lbs/day
Jan 2018 Average 6.565 / mg/L 3.2259 / lbs/day
Feb 2018 Average 4.03 / mg/L 2.4427 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 14 of 16
l

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Mar 2018 Average 6.42 / mg/L 4.5943 / lbs/day
Apr 2018 Average 6.13 / mg/L 4.2003 / lbs/day
May 2018 Average 7.48 / mg/L 4.9588 / lbs/day
Jun 2018 Average 7.46 / mg/L 5.6876 / lbs/day
2018 Quarter 1 5.672 / mg/L 3.3722 / lbs/day
2018 Quarter 2 7.023 / mg/L 4.9489 / lbs/day
2018 1st 6 Months(Avg) 6.348 / mg/L 4.0479 / lbs/day
2018 1st 6...(Max) 9.6 / mg/L 5.6876 / lbs/day
2018 1st 6...(Min) 2.66 / mg/L /
2018 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
01/16/2018 P Cintas011618POTW 600 / mg/L 354.978756 / lbs/day
01/17/2018 S Cintas011718Self 374 / mg/L 169.984863 / lbs/day
02/20/2018 P Cintas022018POTW 500 / mg/L /
02/20/2018 S Cintas022018Self 566 / mg/L 329.179883 / lbs/day
03/23/2018 P Cintas032318POTW 892 / mg/L /
03/28/2018 S Cintas032818Self 892 / mg/L 505.945433 / lbs/day
04/17/2018 S Cintas041718Se1f 839 / mg/L 367.086755 / lbs/day
04/19/2018 P Cintas041918POTW 1700 / mg/L /
05/02/2018 S Cintas050218Se1f 304 / mg/L 179.462922 / lbs/day
05/18/2018 P Cintas051818POTW 207 / mg/L /
06/12/2018 S Cintas061218Self 93.3 / mg/L 64.713294 / lbs/day
06/12/2018 P Cintas061218POTW 974 / mg/L /
Jan 2018 Week 3 487 / mg/L 262.481809 / lbs/day
Feb 2018 Week 3 533 / mg/L 329.179883 / lbs/day
Mar 2018 Week 4 892 / mg/L 505.945433 / lbs/day
Apr 2018 Week 3 1269.5 / mg/L 367.086755 / lbs/day
May 2018 Week 1 304 / mg/L 179.462922 / lbs/day
May 2018 Week 3 207 / mg/L /
Jun 2018 Week 2 533.7 / mg/L 64.713294 / lbs/day
Jan 2018 Average 487 / mg/L 262.481809 / lbs/day
Feb 2018 Average 533 / mg/L 329.179883 / lbs/day
Mar 2018 Average 892 / mg/L 505.945433 / lbs/day
Apr 2018 Average 1269.5 / mg/L 367.086755 / lbs/day
May 2018 Average 255.5 / mg/L 179.462922 / lbs/day
Jun 2018 Average 533.7 / mg/L 64.713294 / lbs/day
2018 Quarter 1 637.3 / mg/L 340.022234 / lbs/day
2018 Quarter 2 686.2 / mg/L 203.754324 / lbs/day
2018 1st 6 Months(Avg) 661.8 / mg/L 281.622 / lbs/day
2018 1st 6...(Max) 1700 / mg/L 505.945433 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 15 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2018 1st 6...(Min) 93.3 / mg/L /
2018 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/17/2018 S Cintas011718Self 1.18 / mg/L 0.536316 / lbs/day
02/20/2018 S Cintas022018Se1f 1.1 / mg/L 0.639749 / lbs/day
03/28/2018 S Cintas032818Se1f 1.79 / mg/L 1.015294 / lbs/day
04/17/2018 S Cintas041718Self 1.12 / mg/L 0.490032 / lbs/day
05/02/2018 S Cintas050218Self 0.772 / mg/L 0.455741 / lbs/day
06/12/2018 S Cintas061218Self 0.573 / mg/L 0.397435 / lbs/day
Jan 2018 Week 3 1.18 / mg/L 0.536316 / lbs/day
Feb 2018 Week 3 1.1 / mg/L 0.639749 / lbs/day
Mar 2018 Week 4 1.79 / mg/L 1.015294 / lbs/day
Apr 2018 Week 3 1.12 / mg/L 0.490032 / lbs/day
May 2018 Week 1 0.772 / mg/L 0.455741 / lbs/day
Jun 2018 Week 2 0.573 / mg/L 0.397435 / lbs/day
Jan 2018 Average 1.18 / mg/L 0.536316 / lbs/day
Feb 2018 Average 1.1 / mg/L 0.639749 / lbs/day
Mar 2018 Average 1.79 / mg/L 1.015294 / lbs/day
Apr 2018 Average 1.12 / mg/L 0.490032 / lbs/day
May 2018 Average 0.772 / mg/L 0.455741 / lbs/day
Jun 2018 Average 0.573 / mg/L 0.397435 / lbs/day
2018 Quarter 1 1.357 / mg/L 0.730453 / lbs/day
2018 Quarter 2 0.822 / mg/L 0.447736 / lbs/day
2018 1st 6 Months(Avg) 1.089 / mg/L 0.589095 / lbs/day
2018 1st 6...(Max) 1.79 / mg/L 1.015294 / lbs/day
2018 l st 6...(Min) 0.573 / mg/L 0.397435 / lbs/day
2018 1st 6...(Count) 6 / 6 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 16 of 16

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
02/21/2018 S CreeP8022118Self 0.188 / mg/L 0.426474 / lbs/day
Feb 2018 Week 3 0.188 / mg/L 0.426474 / lbs/day
Feb 2018 Average 0.188 / mg/L 0.426474 / lbs/day
2018 Quarter 1 0.188 / mg/L 0.426474 / lbs/day
2018 1st 6 Months(Avg) 0.188 / mg/L 0.426474 / lbs/day
2018 1st 6...(Max) 0.188 / mg/L 0.426474 / lbs/day
2018 1st 6...(Min) 0.188 / mg/L 0.426474 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/09/2018 P CreeP8020918POTW 24.5 / mg/L 49.8404 / lbs/day
02/21/2018 S CreeP8022118Se1f 18.8 / mg/L 42.6474 / lbs/day
Feb 2018 Week 2 24.5 / mg/L 49.8404 / lbs/day
Feb 2018 Week 3 18.8 / mg/L 42.6474 / lbs/day
Feb 2018 Average 21.65 / mg/L 46.2439 / lbs/day
2018 Quarter 1 21.65 / mg/L 46.2439 / lbs/day
2018 1st 6 Months(Avg) 21.65 / mg/L 46.2439 / lbs/day
2018 1st 6...(Max) 24.5 / mg/L 49.8404 / lbs/day
2018 1st 6...(Min) 18.8 / mg/L 42.6474 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S CreeP80118Flow 0.238808 / MGD /
02/28/2018 S CreeP80218F1ow 0.243921 / MGD /
03/31/2018 S CreeP80318F1ow 0.277734 / MGD /
04/30/2018 S CreeP80418flow 0.250209 / MGD /
05/31/2018 S CreeP800518Flow 0.407715 / MGD /
06/30/2018 S CreeP80618F1ow 0.389228 / MGD /
Jan 2018 Week 4 0.238808 / MGD /
Feb 2018 Week 4 0.243921 / MGD /
Mar 2018 Week 4 0.277734 / MGD /
Apr 2018 Week 4 0.250209 / MGD /
May 2018 Week 4 0.407715 / MGD /
Jun 2018 Week 4 0.389228 / MGD /
Jan 2018 Average 0.238808 / MGD /
Feb 2018 Average 0.243921 / MGD /
Mar 2018 Average 0.277734 / MGD /
Apr 2018 Average 0.250209 / MGD /
May 2018 Average 0.407715 / MGD /
Jun 2018 Average 0.389228 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 9
L

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 008
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2018 Quarter 1 0.253488 / MGD /
2018 Quarter 2 0.349051 / MGD /
2018 1st 6 Months(Avg) 0.301269 / MGD /
2018 1st 6...(Max) 0.407715 / MGD /
2018 1st 6...(Min) 0.238808 / MGD /
2018 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/21/2018 S CreeP8022118Se1f < 0.0005 / mg/L < 0.001134 / lbs/day
Feb 2018 Week 3 < 0.0005 / mg/L < 0.001134 / lbs/day
Feb 2018 Average < 0.0005 / mg/L < 0.001134 / lbs/day
2018 Quarter 1 < 0.0005 / mg/L < 0.001134 / lbs/day
2018 1st 6 Months(Avg) < 0.0005 / mg/L < 0.001134 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.001134 / lbs/day
2018 1st 6...(Min) < 0.0005 / mg/L < 0.001134 / lbs/day
2018 1st 6...(Count) 1 / 1 /
1 Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/09/2018 P CreeP8020918POTW 199 / mg/L 404.8259 / lbs/day
02/21/2018 S CreeP8022118Self 198 / mg/L 449.159 / lbs/day
Feb 2018 Week 2 199 / mg/L 404.8259 / lbs/day
Feb 2018 Week 3 198 / mg/L 449.159 / lbs/day
Feb 2018 Average 198.5 / mg/L 426.9925 / lbs/day
2018 Quarter 1 198.5 / mg/L 426.9925 / lbs/day
2018 1st 6 Months(Avg) 198.5 / mg/L 426.992 / lbs/day
2018 1st 6...(Max) 199 / mg/L 449.1590 / lbs/day
2018 1st 6...(Min) 198 / mg/L 404.8259 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
02/21/2018 S CreeP8022118Self < 0.003 / mg/L < 0.005671 / lbs/day
Feb 2018 Week 3 < 0.003 / mg/L < 0.005671 / lbs/day
Feb 2018 Average < 0.003 / mg/L < 0.005671 / lbs/day
2018 Quarter 1 < 0.003 / mg/L < 0.005671 / lbs/day
2018 1st 6 Months(Avg) < 0.003 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 9

Cree. Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/21/2018 S CreeP8022118Se1f 0.067 / mg/L 0.151988 / lbs/day
Feb 2018 Week 3 0.067 / mg/L 0.151988 / lbs/day
m 0.151988 lbs/day
2018 Average 0.067 / mg/L /
2018 Quarter 1 0.067 / mg/L 0.151988 / lbs/day
2018 1st 6 Months(Avg) 0.067 / mg/L 0.151988 / lbs/day
2018 1st 6...(Max) 0.067 / mg/L 0.151988 / lbs/day
2018 1st 6...(Min) 0.067 / mg/L 0.151988 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/09/2018 P CreeP8020918POTW 0.025 / mg/L 0.050858 / lbs/day
02/21/2018 S CreeP8022118Self 0.012 / mg/L 0.027222 / lbs/day
Feb 2018 Week 2 0.025 / mg/L 0.050858 / lbs/day
Feb 2018 Week 3 0.012 / mg/L 0.027222 / lbs/day
Feb 2018 Average 0.019 / mg/L 0.03904 / lbs/day
2018 Quarter 1 0.019 / mg/L 0.03904 / lbs/day
2018 1st 6 Months(Avg) 0.019 / mg/L 0.039040 / lbs/day
2018 1st 6...(Max) 0.025 / mg/L 0.050858 / lbs/day
2018 1st 6...(Min) 0.012 / mg/L 0.027222 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/09/2018 P CreeP8020918POTW 2.66 / mg/L 5.4112 / lbs/day
02/21/2018 S CreeP8022118Self 2.1 / mg/L 4.7638 / lbs/day
Feb 2018 Week 2 2.66 / mg/L 5.4112 / lbs/day
Feb 2018 Week 3 2.1 / mg/L 4.7638 / lbs/day
Feb 2018 Average 2.38 / mg/L 5.0875 / lbs/day
2018 Quarter 1 2.38 / mg/L 5.0875 / lbs/day
2018 1st 6 Months(Avg) 2.38 / mg/L 5.0875 / lbs/day
2018 1st 6...(Max) 2.66 / mg/L 5.4112 / lbs/day
2018 1st 6...(Min) 2.1 / mg/L 4.7638 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/21/2018 S CreeP8022118Self < 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Week 3 < 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.005671 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.005671 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 9

1 Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Lead
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/21/2018 S CreeP8022118Self 0.00001 / mg/L /
05/14/2018 P CreeP8051418POTW 0.000075 / mg/L /
Hg
Feb 2018 Week 3 0.00001 / mg/L /
May 2018 Week 2 0.000075 / mg/L /
Feb 2018 Average 0.00001 / mg/L /
May 2018 Average 0.000075 / mg/L /
2018 Quarter 1 0.00001 / mg/L /
2018 Quarter 2 0.000075 / mg/L /
2018 1st 6 Months(Avg) 0.0000421 / mg/L /
2018 1st 6...(Max) 0.0000745 / mg/L /
2018 1st 6...(Min) 0.0000096 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/09/2018 P CreeP8020918POTW < 0.003 / mg/L < 0.0051 / 0.457 lbs/day
02/21/2018 S CreeP8022118Self < 0.003 / mg/L < 0.0057 / 0.457 lbs/day
Feb 2018 Week 2 < 0.003 / mg/L < 0.0051 / lbs/day
Feb 2018 Week 3 < 0.003 / mg/L < 0.0057 / lbs/day
Feb 2018 Average < 0.003 / mg/L < 0.0054 / lbs/day
2018 Quarter 1 < 0.003 / mg/L < 0.0054 / lbs/day
2018 1st 6 Months(Avg) < 0.003 / mg/L < 0.0054 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.0057 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.0051 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 9

r
Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/21/2018 S CreeP8022118Self < 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Week 3 <t 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.005671 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/09/2018 P CreeP8020918POTW 1.9 / mg/L 3.845 / lbs/day
02/21/2018 S CreeP8022118Self 1.8 / mg/L 4.083 / lbs/day
Feb 2018 Week 2 1.9 / mg/L 3.845 / lbs/day
Feb 2018 Week 3 1.8 / mg/L 4.083 / lbs/day
Feb 2018 Average 1.8 / mg/L 3.964 / lbs/day
2018 Quarter 1 1.8 / mg/L 3.964 / lbs/day
1 2018 1st 6 Months(Avg) 1.8 / mg/L 3.964 / lbs/day
2018 1st 6...(Max) 1.9 / mg/L 4.083 / lbs/day
2018 1st 6...(Min) 1.8 / mg/L 3.845 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/09/2018 P CreeP8020918POTW 38.3 / mg/L 77.914 / lbs/day
02/21/2018 S CreeP8022118Self 26.2 / mg/L 59.434 / lbs/day
Feb 2018 Week 2 38.3 / mg/L 77.914 / lbs/day
Feb 2018 Week 3 26.2 / mg/L 59.434 / lbs/day
Feb 2018 Average 32.25 / mg/L 68.674 / lbs/day
2018 Quarter 1 32.25 / mg/L 68.674 / lbs/day
2018 1st 6 Months(Avg) 32.25 / mg/L 68.674 / lbs/day
2018 1st 6...(Max) 38.3 / mg/L 77.914 / lbs/day
2018 1st 6...(Min) 26.2 / mg/L 59.434 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/09/2018 P CreeP8020918POTW < 2.5 / mg/L < /
02/21/2018 S CreeP8022118Self < 2.5 / mg/L < /
Feb 2018 Week 2 < 2.5 / mg/L < /
Feb 2018 Week 3 < 2.5 / mg/L < /
I
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
Feb 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD mp p Result/Limit Mass/Limit
pH
02/09/2018 P CreeP8020918POTW 8.8 /5.0-10.5 SU /
02/21/2018 S CreeP8022118Se1f 8.7 /5.0-10.5 SU /
Feb 2018 Week 2 8.8 / SU /
Feb 2018 Week 3 8.7 / SU /
Feb 2018 Average 8.75 / SU /
2018 Quarter 1 8.75 / SU /
2018 1st 6 Months(Avg) 8.75 / SU /
2018 1st 6...(Max) 8.8 / SU /
2018 1st 6...(Min) 8.7 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
02/21/2018 S CreeP8022118Se1f < 0.005 / mg/L < 0.011342 / lbs/day
Feb 2018 Week 3 < 0.005 / mg/L < 0.011342 / lbs/day
Feb 2018 Average < 0.005 / mg/L < 0.011342 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.011342 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.011342 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.011342 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.011342 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Cree, Inc.(AI1)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/21/2018 S CreeP8022118Self < 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Week 3 < 0.0025 / mg/L < 0.005671 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.005671 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.005671 / lbs/day
2018 1st 6...(Count) I / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Sulfate
02/21/2018 S CreeP8022118Self 213 / mg/L 483.1862 / lbs/day
Feb 2018 Week 3 213 / mg/L 483.1862 / lbs/day
Feb 2018 Average 213 / mg/L 483.1862 / lbs/day
2018 Quarter 1 213 / mg/L 483.1862 / lbs/day
2018 1st 6 Months(Avg) 213 / mg/L 483.186 / lbs/day
2018 1st 6...(Max) 213 / mg/L 483.1862 / lbs/day
2018 1st 6...(Min) 213 / mg/L 483.1862 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/09/2018 P CreeP8020918POTW 17 /66 °C /
02/21/2018 S CreeP8022118Self 23 /66 °C /
Feb 2018 Week 2 17 / °C /
Feb 2018 Week 3 23 / °C /
Feb 2018 Average 20 / °C /
2018 Quarter 1 20 / °C /
2018 1st 6 Months(Avg) 20 / °C /
2018 1st 6...(Max) 23 / °C /
2018 1st 6...(Min) 17 / °C /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/25/2018 P CreeP8012518POTW 24.3 / mg/L 58.975 / lbs/day
02/09/2018 P CreeP8020918POTW 36.4 / mg/L 74.049 / lbs/day
02/21/2018 S CreeP8022118Self 24.3 / mg/L 55.124 / lbs/day
03/27/2018 P CreeP8032718POTW 24.2 / mg/L 53.484 / lbs/day
04/18/2018 P CreeP8041818POTW 34.5 / mg/L 65.027 / lbs/day
05/15/2018 P CreeP051518POTW 14.5 / mg/L 46.558 / lbs/day
06/15/2018 P CreeP8061518POTW 16.2 / mg/L 60.663 / lbs/day
Jan 2018 Week 4 24.3 / mg/L 58.975 / lbs/day
Feb 2018 Week 2 36.4 / mg/L 74.049 / lbs/day
Feb 2018 Week 3 24.3 / mg/L 55.124 / lbs/day
Mar 2018 Week 4 24.2 / mg/L 53.484 / lbs/day
Apr 2018 Week 3 34.5 / mg/L 65.027 / lbs/day
May 2018 Week 3 14.5 / mg/L 46.558 / lbs/day
Jun 2018 Week 3 16.2 / mg/L 60.663 / lbs/day
11 Jan 2018 Average 24.3 / mg/L 58.975 / lbs/day
Feb 2018 Average 30.35 / mg/L 64.586 / lbs/day
Mar 2018 Average 24.2 / mg/L 53.484 / lbs/day
Apr 2018 Average 34.5 / mg/L 65.027 / lbs/day
May 2018 Average 14.5 / mg/L 46.558 / lbs/day
Jun 2018 Average 16.2 / mg/L 60.663 / lbs/day
2018 Quarter 1 27.3 / mg/L 60.408 / lbs/day
2018 Quarter 2 21.73 / mg/L 57.416 / lbs/day
2018 1st 6 Months(Avg) 24.91 / mg/L 59.126 / lbs/day
2018 1st 6...(Max) 36.4 / mg/L 74.049 / lbs/day
2018 1st 6...(Min) 14.5 / mg/L 46.558 / lbs/day
2018 1st6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/25/2018 P CreeP8012518POTW 1.95 / mg/L 4.7325 / lbs/day
02/09/2018 P CreeP8020918POTW 1.79 / mg/L 3.6414 / lbs/day
02/21/2018 S CreeP8022118Self 2.6 / mg/L 5.898 / lbs/day
03/27/2018 P CreeP8032718POTW 1.92 / mg/L 4.2434 / lbs/day
04/18/2018 P CreeP8041818POTW 3.05 / mg/L 5.7488 / lbs/day
05/15/2018 P CreeP051518POTW 1.39 / mg/L 4.4632 / lbs/day
06/15/2018 P CreeP8061518POTW 1.86 / mg/L 6.9651 / lbs/day
Jan 2018 Week 4 1.95 / mg/L 4.7325 / lbs/day
Feb 2018 Week 2 1.79 / mg/L 3.6414 / lbs/day
Feb 2018 Week 3 2.6 / mg/L 5.898 / lbs/day
Mar 2018 Week 4 1.92 / mg/L 4.2434 / lbs/day
Apr 2018 Week 3 3.05 / mg/L 5.7488 / lbs/day
May 2018 Week 3 1.39 / mg/L 4.4632 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 9
i

r
Cree, Inc.(AI1)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Oufall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Jun 2018 Week 3 1.86 / mg/L 6.9651 / lbs/day
Jan 2018 Average 1.95 / mg/L 4.7325 / lbs/day
Feb 2018 Average 2.195 / mg/L 4.7697 / lbs/day
Mar 2018 Average 1.92 / mg/L 4.2434 / lbs/day
Apr 2018 Average 3.05 / mg/L 5.7488 / lbs/day
May 2018 Average 1.39 / mg/L 4.4632 / lbs/day
Jun 2018 Average 1.86 / mg/L 6.9651 / lbs/day
2018 Quarter 1 2.065 / mg/L 4.6288 / lbs/day
2018 Quarter 2 2.1 / mg/L 5.7257 / lbs/day
2018 1st 6 Months(Avg) 2.08 / mg/L 5.0989 / lbs/day
2018 1st 6...(Max) 3.05 / mg/L 6.9651 / lbs/day
2018 1st 6...(Min) 1.39 / mg/L 3.6414 / lbs/day
2018 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/21/2018 S CreeP8022118Se1f 2.5541 / mg/L /
Feb 2018 Week 3 2.5541 / mg/L /
Feb 2018 Average 2.5541 / mg/L /
2018 Quarter 1 2.5541 / mg/L /
2018 1st 6 Months(Avg) 2.5541 / mg/L /
2018 1st 6...(Max) 2.5541 / mg/L /
2018 1st 6...(Min) 2.5541 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/21/2018 S CreeP8022118Se1f 0.437 / mg/L 0.991326 / lbs/day
Feb 2018 Week 3 0.437 / mg/L 0.991326 / lbs/day
Feb 2018 Average 0.437 / mg/L 0.991326 / lbs/day
2018 Quarter 1 0.437 / mg/L 0.991326 / lbs/day
2018 1st 6 Months(Avg) 0.437 / mg/L 0.991326 / lbs/day
2018 1st 6...(Max) 0.437 / mg/L 0.991326 / lbs/day
2018 1st 6...(Min) 0.437 / mg/L 0.991326 / lbs/day
2018 1st 6...(Count) 1 / 1 /
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S CreeP90I18Flow 0.011667 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
02/28/2018 S CreeP90218F1ow 0.015007 / MGD /
03/31/2018 S CreeP90318F1ow 0.016105 / MGD /
04/30/2018 S CreeP90418F1ow 0.016692 / MGD /
05/31/2018 S CreeP90518Flow 0.02168 / MGD /
06/30/2018 S CreeP90618Flow 0.021795 / MGD /
Jan 2018 Week 4 0.011667 / MGD /
Feb 2018 Week 4 0.015007 / MGD /
Mar 2018 Week 4 0.016105 / MGD /
Apr 2018 Week 4 0.016692 / MGD /
May 2018 Week 4 0.02168 / MGD /
Jun 2018 Week 4 0.021795 / MGD /
Jan 2018 Average 0.011667 / MGD /
Feb 2018 Average 0.015007 / MGD /
Mar 2018 Average 0.016105 / MGD /
Apr 2018 Average 0.016692 / MGD /
May 2018 Average 0.02168 / MGD /
Jun 2018 Average 0.021795 / MGD /
2018 Quarter 1 0.01426 / MGD /
2018 Quarter 2 0.020056 / MGD /
2018 1st 6 Months(Avg) 0.017158 / MGD /
2018 l st 6...(Max) 0.021795 / MGD /
2018 1st 6...(Min) 0.011667 / MGD /
2018 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/09/2018 P CreeP9020918POTW 60 / mg/L /
02/21/2018 S CreeP9022118Se1f 75.5 / mg/L /
Feb 2018 Week 2 60 / mg/L /
Feb 2018 Week 3 75.5 / mg/L /
Feb 2018 Average 67.75 / mg/L /
2018 Quarter 1 67.75 / mg/L /
2018 1st 6 Months(Avg) 67.75 / mg/L /
2018 1st 6...(Max) 75.5 / mg/L /
2018 1st 6...(Min) 60 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/21/2018 S CreeP9022118Se1f 0.07 / mg/L /
Feb 2018 Week 3 0.07 / mg/L /
Feb 2018 Average 0.07 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 5

Cree. Inc.(All)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample DateSamplelD Result/Limit Mass/Limit ct
Copper
2018 Quarter 1 0.07 / mg/L /
2018 1st 6 Months(Avg) 0.070 / mg/L /
2018 1st 6...(Max) 0.070 / mg/L /
2018 1st 6...(Min) 0.070 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/09/2018 P CreeP9020918POTW 1.03 / mg/L /
02/21/2018 S CreeP9022118Self 1.6 / mg/L /
Feb 2018 Week 2 1.03 / mg/L /
Feb 2018 Week 3 1.6 / mg/L /
Feb 2018 Average 1.32 / mg/L /
2018 Quarter 1 1.32 / mg/L /
2018 1st 6 Months(Avg) 1.32 / mg/L /
2018 1st 6...(Max) 1.6 / mg/L /
2018 1st 6...(Min) 1.03 / mg/L /
2018 1st 6...(Count) 2 / / 1
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/21/2018 S CreeP9022118Se1f 0.00005 / mg/L /
05/14/2018 P CreeP9051418POTW 0.000177 / mg/L /
Hg
Feb 2018 Week 3 0.00005 / mg/L /
May 2018 Week 2 0.000177 / mg/L /
Feb 2018 Average 0.00005 / mg/L /
May 2018 Average 0.000177 / mg/L /
2018 Quarter 1 0.00005 / mg/L /
2018 Quarter 2 0.000177 / mg/L /
2018 1st 6 Months(Avg) 0.0001133 / mg/L /
2018 1st 6...(Max) 0.000177 / mg/L /
2018 1st 6...(Min) 0.0000495 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/09/2018 P CreeP9020918POTW < 0.003 / mg/L < /
02/21/2018 S CreeP9022118Self < 0.003 / mg/L < /
Feb 2018 Week 2 < 0.003 / mg/L < /
Feb 2018 Week 3 < 0.003 / mg/L < /
Feb 2018 Average < 0.003 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
2018 Quarter 1 < 0.003 / mg/L < /
2018 1st 6 Months(Avg) < 0.003 / mg/L < /
2018 1st 6...(Max) < 0.003 / mg/L < /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/09/2018 P CreeP9020918POTW 20 / mg/L /
02/21/2018 S CreeP9022118Self 154 / mg/L /
Feb 2018 Week 2 20 / mg/L /
Feb 2018 Week 3 154 / mg/L /
Feb 2018 Average 87 / mg/L /
2018 Quarter 1 87 / mg/L /
2018 1st 6 Months(Avg) 87 / mg/L /
2018 1st 6...(Max) 154 / mg/L /
2018 1st 6...(Min) 20 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/09/2018 P CreeP9020918POTW 7.8 /5.0- 10.5 SU /
02/21/2018 S CreeP9022118Self 7.9 /5.0- 10.5 SU /
Feb 2018 Week 2 7.8 / SU /
Feb 2018 Week 3 7.9 / SU /
Feb 2018 Average 7.85 / SU /
2018 Quarter 1 7.85 / SU /
2018 1st 6 Months(Avg) 7.85 / SU /
2018 1st 6...(Max) 7.9 / SU /
2018 1st 6...(Min) 7.8 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 5

i
Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Sulfate
02/21/2018 S CreeP9022118Self 51.9 / mg/L /
Feb 2018 Week 3 51.9 / mg/L /
Feb 2018 Average 51.9 / mg/L /
2018 Quarter 1 51.9 / mg/L /
2018 1st 6 Months(Avg) 51.9 / mg/L /
2018 1st 6...(Max) 51.9 / mg/L /
2018 1st 6...(Min) 51.9 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/21/2018 S CreeP9022118Se1f 22.5 / °C /
Feb 2018 Week 3 22.5 / °C /
Feb 2018 Average 22.5 / °C /
2018 Quarter 1 22.5 / °C /
2018 1st 6 Months(Avg) 22.5 / °C /
2018 1st 6...(Max) 22.5 / °C /
2018 1st 6...(Min) 22.5 / °C /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/25/2018 P CreeP9012518POTW 46 / mg/L /
03/27/2018 P CreeP9032718POTW 69.3 / mg/L /
04/18/2018 P CreeP9041818POTW 62.3 / mg/L /
05/15/2018 P CreeP9051518POTW 25.8 / mg/L /
06/15/2018 P CreeP9061518POTW 37.6 / mg/L /
Jan 2018 Week 4 46 / mg/L /
Mar 2018 Week 4 69.3 / mg/L /
Apr 2018 Week 3 62.3 / mg/L /
May 2018 Week 3 25.8 / mg/L /
Jun 2018 Week 3 37.6 / mg/L /
Jan 2018 Average 46 / mg/L /
Mar 2018 Average 69.3 / mg/L /
Apr 2018 Average 62.3 / mg/L /
May 2018 Average 25.8 / mg/L /
Jun 2018 Average 37.6 / mg/L /
2018 Quarter 1 57.65 / mg/L /
2018 Quarter 2 41.9 / mg/L /
2018 1st 6 Months(Avg) 48.2 / mg/L /
2018 1st 6...(Max) 69.3 / mg/L /
2018 1st 6...(Min) 25.8 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2018 1st 6...(Count) 5 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/25/2018 P CreeP9012518POTW 5.16 / mg/L /
03/27/2018 P CreeP9032718POTW 7.13 / mg/L /
04/18/2018 P CreeP9041818POTW 6.2 / mg/L /
05/15/2018 P CreeP9051518POTW 3.45 / mg/L /
06/15/2018 P CreeP9061518POTW 5.77 / mg/L /
Jan 2018 Week 4 5.16 / mg/L /
Mar 2018 Week 4 7.13 / mg/L /
Apr 2018 Week 3 6.2 / mg/L /
May 2018 Week 3 3.45 / mg/L /
Jun 2018 Week 3 5.77 / mg/L /
Jan 2018 Average 5.16 / mg/L /
Mar 2018 Average 7.13 / mg/L /
Apr 2018 Average 6.2 / mg/L /
May 2018 Average 3.45 / mg/L /
Jun 2018 Average 5.77 / mg/L /
2018 Quarter 1 6.145 / mg/L /
2018 Quarter 2 5.14 / mg/L /
2018 1st 6 Months(Avg) 5.542 / mg/L /
2018 1st 6...(Max) 7.13 / mg/L /
2018 1st 6...(Min) 3.45 / mg/L /
2018 1st 6...(Count) 5 / /
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Cree0118Flow 0.250475 /0.600 MGD /
02/28/2018 S Cree0218F1ow 0.258928 /0.600 MGD /
03/31/2018 S Cree0318F1ow 0.293839 /0.600 MGD /
04/30/2018 S Cree0418Flow 0.266901 /0.600 MGD /
05/31/2018 S Cree0518F1ow 0.429395 /0.600 MGD /
06/30/2018 S Cree0618F1ow 0.411024 /0.600 MGD /
Jan 2018 Week 4 0.250475 / MGD /
Feb 2018 Week 4 0.258928 / MGD /
Mar 2018 Week 4 0.293839 / MGD /
Apr 2018 Week 4 0.266901 / MGD /
May 2018 Week 4 0.429395 / MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 5

P
Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jun 2018 Week 4 0.411024 / MGD /
Jan 2018 Average 0.250475 /0.451 MGD /
Feb 2018 Average 0.258928 /0.451 MGD /
Mar 2018 Average 0.293839 /0.451 MGD /
Apr 2018 Average 0.266901 /0.451 MGD /
May 2018 Average 0.429395 /0.451 MGD /
' Jun 2018 Average 0.411024 /0.451 MGD /
2018 Quarter 1 0.267747 / MGD /
2018 Quarter 2 0.369107 / MGD /
2018 1st 6 Months(Avg) 0.318427 / MGD /
2018 1st 6...(Max) 0.429395 / MGD /
2018 1st 6...(Min) 0.250475 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/09/2018 P Cree020918POTW 1.41 /8 mg/L /
02/21/2018 S Cree022118Self 2.07 /8 mg/L /
Feb 2018 Week 2 1.41 / mg/L /
Feb 2018 Week 3 2.07 / mg/L /
Feb 2018 Average 1.74 /7 mg/L /
2018 Quarter 1 1.74 / mg/L /
2018 1st 6 Months(Avg) 1.74 / mg/L /
2018 1st 6...(Max) 2.07 / mg/L /
2018 1st 6...(Min) 1.41 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: l Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 2

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
1 Mercury-LL
02/21/2018 S Cree022118Se1f 0.000012 /0.000142 mg/L /
05/14/2018 P Cree051418POTW1-Ig 0.000076 /0.000142 mg/L /
Feb 2018 Week 3 0.000012 / mg/L /
May 2018 Week 2 0.000076 / mg/L /
Feb 2018 Average 0.000012 / mg/L /
May 2018 Average 0.000076 / mg/L /
2018 Quarter 1 0.000012 / mg/L /
2018 Quarter 2 0.000076 / mg/L /
2018 1st 6 Months(Avg) 0.0000436 / mg/L /
2018 lst6...(Max) 0.0000755 / mg/L /
2018 1st 6...(Min) 0.0000117 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/09/2018 P Cree020918POTW < 2.5 /200 mg/L < /
02/21/2018 S Cree022118Self 10.4 /200 mg
/L /
Feb 2018 Week 2 < 2.5 / mg/L < /
Feb 2018 Week 3 10.4 / mg/L /
Feb 2018 Average < 6.45 / mg/L < /
2018 Quarter 1 < 6.45 / mg/L < /
2018 1st 6 Months(Avg) < 6.45 / mg/L < /
2018 1st 6...(Max) 10.4 / mg/L /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 2

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
02/21/2018 S CreeRTPP12022118Se < 0.05 / mg/L < 0.034621 / lbs/day
1 If
Feb 2018 Week 3 < 0.05 / mg/L < 0.034621 / lbs/day
Feb 2018 Average < 0.05 / mg/L < 0.034621 / lbs/day
2018 Quarter 1 < 0.05 / mg/L < 0.034621 / lbs/day
2018 1st 6 Months(Avg) < 0.05 / mg/L < 0.034621 / lbs/day
2018 1st 6...(Max) < 0.05 / mg/L < 0.034621 / lbs/day
2018 1st 6...(Min) < 0.05 / mg/L < 0.034621 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/09/2018 P CreeRTPP12020918P 3.3 / mg/L 2.285 / lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se 6.5 / mg/L 4.5007 / lbs/day 1
if
Feb 2018 Week 2 3.3 / mg/L 2.285 / lbs/day
Feb 2018 Week 3 6.5 / mg/L 4.5007 / lbs/day
Feb 2018 Average 4.9 / mg/L 3.3928 / lbs/day
2018 Quarter 1 4.9 / mg/L 3.3928 / lbs/day
2018 1st 6 Months(Avg) 4.9 / mg/L 3.3928 / lbs/day
2018 1st 6...(Max) 6.5 / mg/L 4.5007 / lbs/day
2018 1st 6...(Min) 3.3 / mg/L 2.2850 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
02/09/2018 S CreeRTPP12020918Se < 0.005 / mg/L < 0.003462 / lbs/day
If
02/21/2018 S CreeRTPP12022118Se < 0.005 / mg/L < 0.003462 / lbs/day
If
05/15/2018 S CreeRTPP12051518Se < 0.005 / mg/L < 0.004659 / lbs/day
If
Feb 2018 Week 2 < 0.005 / mg/L < 0.003462 / lbs/day
Feb 2018 Week 3 < 0.005 / mg/L < 0.003462 / lbs/day
May 2018 Week 3 < 0.005 / mg/L < 0.004659 / lbs/day
Feb 2018 Average < 0.005 / mg/L < 0.003462 / lbs/day
May 2018 Average < 0.005 / mg/L < 0.004659 / lbs/day
2018 Quarter 1 < 0.005 / mg/L < 0.003462 / lbs/day
2018 Quarter 2 < 0.005 / mg/L < 0.004659 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.003861 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.004659 / lbs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.003462 / lbs/day
2018 1st 6...(Count) 3 / 3 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample 7j/pe: Effluent Wastewater nut full: 012
Sample Date SamplelD Result/Limit Masts/Limit
Average Flow for Month
01/22/2018 S CreeRTPP120118F1ow 0.090105 /0.469 MGD /
02/28/2018 S CreeRTPP120218F1ow 0.083023 /0.469 MGD /
03/19/2018 S CreeRTPP120318Flow 0.090515 /0.469 MGD /
04/30/2018 S CreeRTPP120418F1ow 0.096864 /0.469 MGD /
05/21/2018 S CreeRTPP120518F1ow 0.111718 /0.469 MGD /
06/20/2018 S CreeRTPP120618F1ow 0.127903 /0.469 MGD /
Jan 2018 Week 4 0.090105 / MGD /
Feb 2018 Week 4 0.083023 / MGD /
Mar 2018 Week 3 0.090515 / MGD /
Apr 2018 Week 4 0.096864 / MGD /
May 2018 Week 3 0.111718 / MGD /
Jun 2018 Week 3 0.127903 / MGD /
Jan 2018 Average 0.090105 /0.329 ' MGD /
Feb 2018 Average 0.083023 /0.329 MGD /
Mar 2018 Average 0.090515 /0.329 MGD /
Apr 2018 Average 0.096864 /0.329 MGD /
May 2018 Average 0.111718 /0.329 MGD /
Jun 2018 Average 0.127903 /0.329 MGD /
2018 Quarter 1 0.087881 / MGD /
2018 Quarter 2 0.112162 / MGD /
2018 1st 6 Months(Avg) 0.100021 / MGD /
2018 1st 6...(Max) 0.127903 / MGD /
2018 1st 6...(Min) 0.083023 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Barium
02/21/2018 S CreeRTPP12022118Se 0.0366 / mg/L 0.025342 / lbs/day
If
Feb 2018 Week 3 0.0366 / mg/L 0.025342 / lbs/day
Feb 2018 Average 0.0366 / mg/L 0.025342 / lbs/day
2018 Quarter 1 0.0366 / mg/L 0.025342 / lbs/day
2018 1st 6 Months(Avg) 0.0366 / mg/L 0.025342 / lbs/day
2018 1st 6...(Max) 0.0366 / mg/L 0.025342 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Barium
2018 1st 6...(Min) 0.0366 / mg/L 0.025342 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/21/2018 S CreeRTPP12022118Se < 0.0005 / mg/L < 0.000346 / lbs/day
If
Feb 2018 Week 3 < 0.0005 / mg/L < 0.000346 / lbs/day
Feb 2018 Average < 0.0005 / mg/L < 0.000346 / lbs/day
2018 Quarter 1 < 0.0005 / mg/L < 0.000346 / lbs/day
2018 1st 6 Months(Avg) < 0.0005 / mg/L < 0.000346 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000346 / lbs/day
2018 1st 6...(Min) < 0.0005 / mg/L < 0.000346 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/09/2018 P CreeRTPP12020918P 60 / mg/L 41.5447 / lbs/day
OTW
02/21/2018 S CreeRTPPI2022118Se 95.9 / mg/L 66.4023 / lbs/day
if
Feb 2018 Week 2 60 / mg/L 41.5447 / lbs/day
Feb 2018 Week 3 95.9 / mg/L 66.4023 / lbs/day
Feb 2018 Average 77.95 / mg/L 53.9735 / lbs/day
2018 Quarter 1 77.95 / mg/L 53.9735 / lbs/day
2018 1st 6 Months(Avg) 77.95 / mg/L 53.9735 / lbs/day
2018 1st 6...(Max) 95.9 / mg/L 66.4023 / lbs/day
2018 1st 6...(Min) 60 / mg/L 41.5447 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
02/21/2018 S CreeRTPP12022118Se < 0.003 / mg/L < 0.001731 / lbs/day
If
Feb 2018 Week 3 < 0.003 / mg/L < 0.001731 / lbs/day
Feb 2018 Average < 0.003 / mg/L < 0.001731 / lbs/day
2018 Quarter 1 < 0.003 / mg/L < 0.001731 / lbs/day
2018 1st 6 Months(Avg) < 0.003 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Out all: 012
.f
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/21/2018 S CreeRTPP12022118Se 0.035 / mg/L 0.024096 / lbs/day
If
Feb 2018 Week 3 0.035 / mg/L 0.024096 / lbs/day
Feb 2018 Average 0.035 / mg/L 0.024096 / lbs/day
2018 Quarter 1 0.035 / mg/L 0.024096 / lbs/day
2018 1st 6 Months(Avg) 0.035 / mg/L 0.024096 / lbs/day
2018 1st 6...(Max) 0.035 / mg/L 0.024096 / lbs/day
2018 1st 6...(Min) 0.035 / mg/L 0.024096 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/12/2018 S CreeRTPP12011218Se 0.015 / mg/L 0.011 / 0.05 lbs/day
If
01/23/2018 S CreeRTPP12012318Se 0.043 / mg/L 0.032 / 0.05 lbs/day
If
02/09/2018 S CreeRTPP12020918Se 0.009 / mg/L 0.006 / 0.05 lbs/day
if
02/09/2018 P CreeRTPP12020918P 0.008 / mg/L 0.006 /0.05 lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se 0.01 / mg/L 0.007 /0.05 lbs/day
If
03/09/2018 S CreeRTPP12030918Se < 0.004 / mg/L < 0.003 /0.05 lbs/day
If
03/23/2018 S CreeRTPP12032318Se < 0.004 / mg/L < 0.003 / 0.05 lbs/day
if
04/13/2018 S CreeRTPP12041318Se 0.01 / mg/L 0.008 / 0.05 lbs/day
If
04/26/2018 S CreeRTPP12042618Se < 0.004 / mg/L < 0.003 / 0.05 lbs/day
If
05/15/2018 S CreeRTPP12051518Se 0.01 / mg/L 0.009 /0.05 lbs/day
if
05/25/2018 S CreeRTPP12052518Se < 0.004 / mg/L < 0.004 /0.05 lbs/day
If
06/13/2018 S CreeRTPP12061318Se 0.016 / mg/L 0.017 /0.05 lbs/day
if
06/29/2018 S CreeRTPP12062918Se 0.015 / mg/L 0.016 / 0.05 lbs/day
If
Jan 2018 Week 2 0.015 / mg/L 0.011 / lbs/day
Jan 2018 Week 4 0.043 / mg/L 0.032 / lbs/day
Feb 2018 Week 2 0.008 / mg/L 0.006 / lbs/day
Feb 2018 Week 3 0.01 / mg/L 0.007 / lbs/day
Mar 2018 Week 2 < 0.004 / mg/L < 0.003 / lbs/day
Mar 2018 Week 4 < 0.004 / mg/L < 0.003 / lbs/day
Apr 2018 Week 2 0.01 / mg/L 0.008 / lbs/day
Apr 2018 Week 4 < 0.004 / mg/L < 0.003 / lbs/day
May 2018 Week 3 0.01 / mg/L 0.009 / lbs/day
May 2018 Week 4 < 0.004 / mg/L < 0.004 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 12
L

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Jun 2018 Week 2 0.016 / mg/L 0.017 / lbs/day
Jun 2018 Week 4 0.015 / mg/L 0.016 / lbs/day
Jan 2018 Average 0.029 / mg/L 0.022 / lbs/day
Feb 2018 Average 0.009 / mg/L 0.006 / lbs/day
Mar 2018 Average < 0.004 / mg/L < 0.003 / lbs/day
Apr2018 Average < 0.007 / mg/L < 0.006 / lbs/day
May 2018 Average < 0.007 / mg/L < 0.007 / lbs/day
Jun 2018 Average 0.016 / mg/L 0.017 / lbs/day
2018 Quarter 1 < 0.013 / mg/L < 0.01 / lbs/day
2018 Quarter 2 < 0.01 / mg/L < 0.01 / lbs/day
2018 1st 6 Months(Avg) < 0.012 / mg/L < 0.010 / lbs/day
2018 1st 6...(Max) 0.043 / mg/L 0.032 / lbs/day
2018 1st 6...(Min) 0.004 / mg/L < 0.003 / lbs/day
2018 1st 6...(Count) 13 / 13 /
Sample Count: 13 Months Sampled: 6 Weeks Sampled : 12 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/09/2018 S CreeRTPPl2020918Se 1.3 /8 mg/L 0.9001 / lbs/day
If
02/09/2018 P CreeRTPP12020918P 1.43 /8 mg/L 0.9901 / lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se 1.9 /8 mg/L 1.3156 / lbs/day
If
Feb 2018 Week 2 1.37 / mg/L 0.9451 / lbs/day
Feb 2018 Week 3 1.9 / mg/L 1.3156 / lbs/day
Feb 2018 Average 1.54 /7 mg/L 1.0686 / lbs/day
2018 Quarter 1 1.54 / mg/L 1.0686 / lbs/day
2018 1st 6 Months(Avg) 1.54 / mg/L 1.0686 / lbs/day
2018 1st 6...(Max) 1.9 / mg/L 1.3156 / lbs/day
2018 1st 6...(Min) 1.3 / mg/L 0.9001 / lbs/day
2018 1st 6...(Count) 3 / 3 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 12

Cree, Inc RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type. Effluent Wastewater Outfall: 012
Sample Count: 3 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/21/2018 S CreeRTPP12022118Se < 0.0025 / mg/L < 0.001731 / lbs/day
if
Feb 2018 Week 3 < 0.0025 / mg/L < 0.001731 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.001731 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/09/2018 S CreeRTPP12020918Se 0.000018 /0.000142 mg/L /
If
02/21/2018 S CreeRTPP12022118Se 0.000003 /0.000142 mg/L /
If
05/14/2018 P CreeRTPP12051418P 0.000017 /0.000142 mg/L /
OTWHg
Feb 2018 Week 2 0.000018 / mg/L /
Feb 2018 Week 3 0.000003 / mg/L /
May 2018 Week 2 0.000017 / mg/L /
Feb 2018 Average 0.00001 / mg/L /
May 2018 Average 0.000017 / mg/L /
2018 Quarter 1 0.00001 / mg/L /
2018 Quarter 2 0.000017 / mg/L /
2018 1st 6 Months(Avg) 0.000012 / mg/L /
2018 1st 6...(Max) 0.000018 / mg/L /
2018 1st 6...(Min) 0.000003 / mg/L /
2018 1st 6...(Count) 3 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Count: 3 Months Sampled : 2 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/09/2018 P CreeRTPP12020918P < 0.003 / mg/L < 0.0017 / lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se < 0.003 / mg/L < 0.0017 / lbs/day
If
Feb 2018 Week 2 < 0.003 / mg/L < 0.0017 / lbs/day
Feb 2018 Week 3 < 0.003 / mg/L < 0.0017 / lbs/day
Feb 2018 Average < 0.003 / mg/L < 0.0017 / lbs/day
2018 Quarter 1 < 0.003 / mg/L < 0.0017 / lbs/day
2018 1st 6 Months(Avg) < 0.003 / mg/L < 0.0017 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.0017 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.0017 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/21/2018 S CreeRTPP12022118Se < 0.0025 / mg/L < 0.001731 / lbs/day
If
Feb 2018 Week 3 < 0.0025 / mg/L < 0.001731 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.001731 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/09/2018 P CreeRTPP12020918P 2.2 / mg/L 1.496 / lbs/day
1 OTW
11 02/21/2018 S CreeRTPP12022118Se 7.5 / mg/L 5.193 / lbs/day
If
Feb 2018 Week 2 2.2 / mg/L 1.496 / lbs/day
Feb 2018 Week 3 7.5 / mg/L 5.193 / lbs/day
Feb 2018 Average 4.8 / mg/L 3.344 / lbs/day
2018 Quarter I 4.8 / mg/L 3.344 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2018 1st 6 Months(Avg) 4.8 / mg/L 3.344 / lbs/day
2018 1st 6...(Max) 7.5 / mg/L 5.193 / lbs/day
2018 1st 6...(Min) 2.2 / mg/L 1.496 / lbs/day
2018 1st6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/09/2018 P CreeRTPP12020918P 14.7 / mg/L 10.178 / lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se 24.4 / mg/L 16.895 / lbs/day
If
Feb 2018 Week 2 14.7 / mg/L 10.178 / lbs/day
Feb 2018 Week 3 24.4 / mg/L 16.895 / lbs/day
Feb 2018 Average 19.55 / mg/L 13.537 / lbs/day
2018 Quarter 1 19.55 / mg/L 13.537 / lbs/day
2018 1st 6 Months(Avg) 19.55 / mg/L 13.537 / lbs/day
2018 1st 6...(Max) 24.4 / . mg/L 16.895 / lbs/day
2018 1st 6...(Min) 14.7 / mg/L 10.178 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/09/2018 P CreeRTPP12020918P < 2.5 /200 mg/L < /
OTW
02/21/2018 S CreeRTPP12022118Se < 2.5 /200 mg/L < /
If
Feb 2018 Week 2 < 2.5 / mg/L < /
Feb 2018 Week 3 < 2.5 / mg/L < /
Feb 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 12
I

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/23/2018 S CreeRTPP12012318Se 7.5 /5.0- 10.5 SU /
If
02/09/2018 S CreeRTPP12020918Se 7.5 /5.0- 10.5 SU /
If
02/09/2018 P CreeRTPP12020918P 7.1 /5.0- 10.5 SU /
OTW
02/21/2018 S CreeRTPP12022118Se 7.6 /5.0- 10.5 SU /
If
04/26/2018 S CreeRTPP12042618Se 8.5 /5.0- 10.5 SU /
If
05/15/2018 S CreeRTPP12051518Se 7.2 /5.0- 10.5 SU /
if
05/25/2018 S CreeRTPP12052518Se 8.1 /5.0- 10.5 SU /
If
Jan 2018 Week 4 7.5 / SU /
Feb 2018 Week 2 7.3 / SU /
Feb 2018 Week 3 7.6 / SU /
Apr 2018 Week 4 8.5 / SU /
May 2018 Week 3 7.2 / SU /
May 2018 Week 4 8.1 / SU /
Jan 2018 Average 7.5 / SU /
Feb 2018 Average 7.4 / SU /
Apr 2018 Average 8.5 / SU /
May 2018 Average 7.65 / SU /
2018 Quarter 1 7.43 / SU /
2018 Quarter 2 7.93 / SU /
2018 1st 6 Months(Avg) 7.64 / SU /
2018 1st 6...(Max) 8.5 / SU /
2018 1st 6...(Min) 7.1 / SU /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 4 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
02/21/2018 S CreeRTPP12022118Se < 0.005 / mg/L < 0.003462 / lbs/day
If
Feb 2018 Week 3 < 0.005 / mg/L < 0.003462 / lbs/day
Feb 2018 Average < 0.005 / mg/L < 0.003462 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
2018 Quarter 1 < 0.005 / mg/L < 0.003462 / lbs/day
2018 1st 6 Months(Avg) < 0.005 / mg/L < 0.003462 / lbs/day
2018 1st 6...(Max) < 0.005 / mg/L < 0.003462 / Ibs/day
2018 1st 6...(Min) < 0.005 / mg/L < 0.003462 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/21/2018 S CreeRTPP12022118Se < 0.0025 / mg/L < 0.001731 / lbs/day
If
Feb 2018 Week 3 < 0.0025 / mg/L < 0.001731 / lbs/day
Feb 2018 Average < 0.0025 / mg/L < 0.001731 / lbs/day
2018 Quarter 1 < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6 Months(Avg) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.001731 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Sulfate
02/21/2018 S CreeRTPP12022118Se 133 / mg/L 92.0908 / lbs/day
If
Feb 2018 Week 3 133 / mg/L 92.0908 / lbs/day
Feb 2018 Average 133 / mg/L 92.0908 / lbs/day
2018 Quarter 1 133 / mg/L 92.0908 / lbs/day
2018 1st 6 Months(Avg) 133 / mg/L 92.0908 / lbs/day
2018 1st 6...(Max) 133 / mg/L 92.0908 / lbs/day
2018 1st 6...(Min) 133 / mg/L 92.0908 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/23/2018 S CreeRTPP12012318Se 20.3 /66 °C /
If
02/09/2018 S CreeRTPPI2020918Se 17.3 /66 °C /
If
02/09/2018 P CreeRTPP12020918P 14 /66 °C /
OTW
02/21/2018 S CreeRTPP12022118Se 21.6 /66 °C /
If
04/26/2018 S CreeRTPP12042618Se 22.4 /66 °C /
if
05/15/2018 S CreeRTPP12051518Se 24.1 /66 °C /
If
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 12
i

Cree. Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
05/25/2018 S CreeRTPP12052518Se 23.5 /66 °C /
If
Jan 2018 Week 4 20.3 / °C /
Feb 2018 Week 2 15.7 / °C /
Feb 2018 Week 3 21.6 / °C /
Apr 2018 Week 4 22.4 / °C /
May 2018 Week 3 24.1 / °C /
May 2018 Week 4 23.5 / °C /
Jan 2018 Average 20.3 / °C /
Feb 2018 Average 17.6 / °C /
Apr 2018 Average 22.4 / °C /
May 2018 Average 23.8 / °C /
2018 Quarter 1 18.3 / °C /
2018 Quarter 2 23.3 / °C /
2018 1st 6 Months(Avg) 20.5 / °C /
2018 1st 6...(Max) 24.1 / °C /
2018 1st 6...(Min) 14 / °C /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 4 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/09/2018 P CreeRTPP12020918P 12.5 / mg/L 8.655 / lbs/day
OTW
02/21/2018 S CreeRTPP12022118Se 16.9 / mg/L 11.702 / lbs/day
If
Feb 2018 Week 2 12.5 / mg/L 8.655 / lbs/day
Feb 2018 Week 3 16.9 / mg/L 11.702 / lbs/day
Feb 2018 Average 14.7 / mg/L 10.178 / lbs/day
2018 Quarter 1 14.7 / mg/L 10.178 / lbs/day
2018 1st 6 Months(Avg) 14.7 / mg/L 10.179 / lbs/day
2018 1st 6...(Max) 16.9 / mg/L 11.702 / lbs/day
2018 1st 6...(Min) 12.5 / mg/L 8.655 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/09/2018 P CreeRTPP12020918P 1.24 / mg/L 0.8586 / lbs/day
OTW
Feb 2018 Week 2 1.24 / mg/L 0.8586 / lbs/day
Feb 2018 Average 1.24 / mg/L 0.8586 / lbs/day
2018 Quarter 1 1.24 / mg/L 0.8586 / lbs/day
2018 1st 6 Months(Avg) 1.24 / mg/L 0.8586 / lbs/day
2018 1st 6...(Max) 1.24 / mg/L 0.8586 / lbs/day
2018 l st 6...(Min) 1.24 / mg/L 0.8586 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/21/2018 S CreeRTPP12022118Se 0.2502 / mg/L /
If
Feb 2018 Week 3 0.2502 / mg/L /
Feb 2018 Average 0.2502 / mg/L /
2018 Quarter 1 0.2502 / mg/L /
2018 1st 6 Months(Avg) 0.2502 / mg/L /
2018 1st 6...(Max) 0.2502 / mg/L /
2018 1st 6...(Min) 0.2502 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/21/2018 S CreeRTPP12022118Se 0.595 / mg/L 0.411985 / lbs/day
If
Feb 2018 Week 3 0.595 / mg/L 0.411985 / lbs/day
Feb 2018 Average 0.595 / mg/L 0.411985 / lbs/day
2018 Quarter 1 0.595 / mg/L 0.411985 / lbs/day
2018 1st 6 Months(Avg) 0.595 / mg/L 0.411985 / lbs/day
2018 1st 6...(Max) 0.595 / mg/L 0.411985 / lbs/day
2018 1st 6...(Min) 0.595 / mg/L 0.411985 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 12 of 12

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Ouijall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
01/31/2018 P JMC013118POTW 0.04 / mg/L 0.000311 / lbs/day
03/05/2018 S JMC030518Self < 0.025 / mg/L < 0.000195 / lbs/day
Jan 2018 Week 4 0.04 / mg/L 0.000311 / lbs/day
Mar 2018 Week 1 < 0.025 / mg/L < 0.000195 / lbs/day
Jan 2018 Average 0.04 / mg/L 0.000311 / lbs/day
Mar 2018 Average < 0.025 / mg/L < 0.000195 / lbs/day
2018 Quarter 1 < 0.032 / mg/L < 0.000253 / lbs/day
2018 1st 6 Months(Avg) < 0.032 / mg/L < 0.000253 / lbs/day
2018 1st 6...(Max) 0.040 / mg/L 0.000311 / lbs/day
2018 1st 6...(Min) < 0.025 / mg/L < 0.000195 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/31/2018 P JMC013118POTW 1.2 / mg/L 0.0094 / lbs/day
03/05/2018 S JMC030518Self 4.1 / mg/L 0.0319 / lbs/day
Jan 2018 Week 4 1.2 / mg/L 0.0094 / lbs/day
Mar 2018 Week 1 4.1 / mg/L 0.0319 / lbs/day
Jan 2018 Average 1.2 / mg/L 0.0094 / lbs/day
Mar 2018 Average 4.1 / mg/L 0.0319 / lbs/day
2018 Quarter 1 2.65 / mg/L 0.0207 / lbs/day
2018 1st 6 Months(Avg) 2.65 / mg/L 0.0207 / lbs/day
2018 1st 6...(Max) 4.1 / mg/L 0.0319 / lbs/day
2018 1st 6...(Min) 1.2 / mg/L 0.0094 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S JMC0118F1ow 0.000284 / MGD /
02/28/2018 S JMCO218F1ow 0.000331 / MGD /
03/31/2018 S JMC0318Flow 0.000285 / MGD /
04/30/2018 S JMC0418F1ow 0.000274 / MGD /
05/31/2018 S JMC0518Flow 0.000287 / MGD /
06/30/2018 S JMC0618F1ow 0.000304 / MGD /
Jan 2018 Week 4 0.000284 / MGD /
Feb 2018 Week 4 0.000331 / MGD /
Mar 2018 Week 4 0.000285 / MGD /
Apr 2018 Week 4 0.000274 / MGD /
May 2018 Week 4 0.000287 / MGD /
Jun 2018 Week 4 0.000304 / MGD /
Jan 2018 Average 0.000284 /0.01 MGD /
Feb 2018 Average 0.000331 /0.01 MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Mar 2018 Average 0.000285 /0.01 MGD /
Apr 2018 Average 0.000274 /0.01 MGD /
May 2018 Average 0.000287 /0.01 MGD /
Jun 2018 Average 0.000304 /0.01 MGD /
2018 Quarter 1 0.0003 / MGD /
2018 Quarter 2 0.000288 / MGD /
2018 1st 6 Months(Avg) 0.000294 / MGD /
2018 1st 6...(Max) 0.000331 / MGD /
2018 1st 6...(Min) 0.000274 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
' Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/31/2018 P JMC013118POTW < 0.00008 /0.04 mg/L < 0.000001 / lbs/day
03/05/2018 S JMC030518Self < 0.0005 /0.04 mg/L < 0.000004 / lbs/day
Jan 2018 Week 4 < 0.00008 / mg/L < 0.000001 / lbs/day
Mar 2018 Week I < 0.0005 / mg/L < 0.000004 / lbs/day
Jan 2018 Average < 0.00008 /0.025 mg/L < 0.000001 / lbs/day
Mar 2018 Average < 0.0005 /0.025 mg/L < 0.000004 / lbs/day
2018 Quarter 1 < 0.00029 / mg/L < 0.000002 / lbs/day
2018 1st 6 Months(Avg) < 0.00029 / mg/L < 0.000002 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000004 / lbs/day
2018 1st 6...(Min) < 0.00008 / mg/L < 0.000001 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
I #Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 11
i

r
JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/31/2018 P JMC013118POTW 750 / mg/L 5.9047 / lbs/day
03/05/2018 S JMC030518Self 3100 / mg/L 24.1476 / lbs/day
Jan 2018 Week 4 750 / mg/L 5.9047 / lbs/day
Mar 2018 Week 1 3100 / mg/L 24.1476 / lbs/day
Jan 2018 Average 750 / mg/L 5.9047 / lbs/day
Mar 2018 Average 3100 / mg/L 24.1476 / lbs/day
2018 Quarter 1 1925 / mg/L 15.0262 / lbs/day
2018 1st 6 Months(Avg) 1925 / mg/L 15.0262 / lbs/day
2018 1st 6...(Max) 3100 / mg/L 24.1476 / lbs/day
2018 1st 6...(Min) 750 / mg/L 5.9047 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
01/31/2018 P JMC013118POTW 0.079 / 1 mg/L 0.000624 / lbs/day
03/05/2018 S JMC030518Self 1.9 / 1 mg/L * * 0.0148 / lbs/day
03/24/2018 S JMC032418Self 0.14 / 1 mg/L /
03/25/2018 S JMC032518Se1f 0.12 / 1 mg/L /
03/26/2018 S JMC032618Se1f 0.1 / 1 mg/L /
03/27/2018 S JMC032718Se1f 0.092 / 1 mg/L /
Jan 2018 Week 4 0.079 / mg/L 0.000624 / lbs/day
Mar 2018 Week 1 1.9 / mg/L 0.0148 / lbs/day
Mar 2018 Week 4 0.113 / mg/L /
Jan 2018 Average 0.079 /0.650 mg/L 0.000624 / lbs/day
Mar 2018 Average 0.47 /0.650 mg/L 0.0148 / lbs/day
2018 Quarter 1 0.405 / mg/L 0.007712 / lbs/day
2018 1st 6 Months(Avg) 0.405 / mg/L 0.007712 / lbs/day
2018 1st 6...(Max) 1.9 / mg/L 0.014800 / lbs/day
2018 1st 6...(Min) 0.079 / mg/L /
2018 1st 6...(Count) 6 / 2 /
Sample Count: 6 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: I 16.67 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 1 16.67 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/31/2018 P JMC013118POTW 0.086 / 1 mg/L 0.000673 / lbs/day
03/05/2018 S JMC030518Self 0.027 / 1 mg/L 0.00021 / lbs/day
Jan 2018 Week 4 0.086 / mg/L 0.000673 / lbs/day
Mar 2018 Week 1 0.027 / mg/L 0.00021 / lbs/day
Jan 2018 Average 0.086 /0.7 mg/L 0.000673 / lbs/day
Mar 2018 Average 0.027 /0.7 mg/L 0.00021 / lbs/day
2018 Quarter 1 0.056 / mg/L 0.000442 / lbs/day
2018 1st 6 Months(Avg) 0.056 / mg/L 0.000442 / lbs/day
2018 1st 6...(Max) 0.086 / mg/L 0.000673 / lbs/day
2018 1st 6...(Min) 0.027 / mg/L 0.000210 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/31/2018 P JMC013118POTW < 0.003 /0.04 mg/L < 0.00002 / lbs/day
03/05/2018 S JMC030518Se1f < 0.003 /0.04 mg/L < 0.000019 / lbs/day
Jan 2018 Week 4 < 0.003 / mg/L < 0.00002 / lbs/day
Mar 2018 Week 1 < 0.003 / mg/L < 0.000019 / lbs/day
Jan 2018 Average < 0.003 /0.03 mg/L < 0.00002 / lbs/day
Mar 2018 Average < 0.003 /0.03 mg/L < 0.000019 / lbs/day
2018 Quarter 1 < 0.003 / mg/L < 0.00002 / lbs/day
2018 1st 6 Months(Avg) < 0.003 / mg/L < 0.000020 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.000020 / lbs/day
2018 1st 6...(Min) < 0.003 / mg/L < 0.000019 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 1 I

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/31/2018 P JMC013118POTW 0.18 / mg/L 0.0014 / lbs/day
03/05/2018 S JMC030518Se1f 0.27 / mg/L 0.0021 / lbs/day
Jan 2018 Week 4 0.18 / mg/L 0.0014 / lbs/day
Mar 2018 Week 1 0.27 / mg/L 0.0021 / lbs/day
Jan 2018 Average 0.18 / mg/L 0.0014 / lbs/day
Mar 2018 Average 0.27 / mg/L 0.0021 / lbs/day
2018 Quarter 1 0.23 / mg/L 0.0018 / lbs/day
2018 1st 6 Months(Avg) 0.23 / mg/L 0.0018 / lbs/day
2018 1st 6...(Max) 0.27 / mg/L 0.0021 / lbs/day
2018 1st 6...(Min) 0.18 / mg/L 0.0014 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
01/31/2018 P JMC013118POTW 0.0064 /0.260 mg/L 0.00005 / lbs/day
03/05/2018 S JMC030518Self 0.002 /0.260 mg/L 0.000016 / lbs/day
Jan 2018 Week 4 0.0064 / mg/L 0.00005 / lbs/day
Mar 2018 Week 1 0.002 / mg/L 0.000016 / lbs/day
Jan 2018 Average 0.0064 /0.160 mg/L 0.00005 / lbs/day
Mar 2018 Average 0.002 /0.160 mg/L 0.000016 / lbs/day
2018 Quarter 1 0.0042 / mg/L 0.000033 / lbs/day
2018 1st 6 Months(Avg) 0.0042 / mg/L 0.000033 / lbs/day
2018 1st 6...(Max) 0.0064 / mg/L 0.000050 / lbs/day
2018 1st 6...(Min) 0.002 / mg/L 0.000016 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/05/2018 S JMC030518Self}Ig 0.00001 /0.000142 mg/L /
04/10/2018 P JMC041018POTW 0.000003 /0.000142 mg/L /
Mar 2018 Week 1 0.00001 / mg/L /
Apr 2018 Week 2 0.000003 / mg/L /
Mar 2018 Average 0.00001 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sam lelD Result/Limit Mass/Limit
P P
Mercury-LL
Apr 2018 Average 0.000003 / mg/L /
2018 Quarter 1 0.00001 / mg/L /
2018 Quarter 2 0.000003 / mg/L /
2018 1st 6 Months(Avg) 0.0000065 / mg/L /
2018 1st 6...(Max) 0.00001 / mg/L /
2018 1st 6...(Min) 0.0000029 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/31/2018 P JMC013118POTW < 0.1 / mg/L < 0.0004 / lbs/day
Jan 2018 Week 4 < 0.1 / mg/L < 0.0004 / lbs/day
Jan 2018 Average < 0.1 / mg/L < 0.0004 / lbs/day
2018 Quarter 1 < 0.1 / mg/L < 0.0004 / lbs/day
2018 1st 6 Months(Avg) < 0.05 / mg/L < 0.0004 / lbs/day
2018 1st 6...(Max) < 0.05 / mg/L < 0.0004 / lbs/day
2018 1st 6...(Min) < 0.05 / mg/L < 0.0004 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/31/2018 P JMC013118POTW 0.0046 /0.3 mg/L 0.000036 / lbs/day
03/05/2018 S JMC030518Self 0.0052 /0.3 mg/L 0.000041 / lbs/day
Jan 2018 Week 4 0.0046 / mg/L 0.000036 / lbs/day
Mar 2018 Week 1 0.0052 / mg/L 0.000041 / lbs/day
Jan 2018 Average 0.0046 /0.2 mg/L 0.000036 / lbs/day
Mar 2018 Average 0.0052 /0.2 mg/L 0.000041 / lbs/day
2018 Quarter 1 0.0049 / mg/L 0.000038 / lbs/day
2018 1st 6 Months(Avg) 0.0049 / mg/L 0.000038 / lbs/day
2018 1st 6...(Max) 0.0052 / mg/L 0.000041 / lbs/day
2018 1st 6...(Min) 0.0046 / mg/L 0.000036 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 1 I

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/31/2018 P JMC013118POTW 31.1 / mg/L 0.245 / lbs/day
03/05/2018 S JMC030518Self 86 / mg/L 0.67 / lbs/day
Jan 2018 Week 4 31.1 / mg/L 0.245 / lbs/day
Mar 2018 Week 1 86 / mg/L 0.67 / lbs/day
Jan 2018 Average 31.1 / mg/L 0.245 / lbs/day
Mar 2018 Average 86 / mg/L 0.67 / lbs/day
2018 Quarter 1 58.6 / mg/L 0.457 / lbs/day
2018 1st 6 Months(Avg) 58.6 / mg/L 0.457 / lbs/day
2018 1st 6...(Max) 86 / mg/L 0.670 / lbs/day
2018 1st 6...(Min) 31.1 / mg/L 0.245 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/31/2018 P JMC013118POTW 33.2 / mg/L 0.261 / lbs/day
03/05/2018 S JMC030518Self 90.6 / mg/L 0.706 / lbs/day
Jan 2018 Week 4 33.2 / mg/L 0.261 / lbs/day
Mar 2018 Week 1 90.6 / mg/L 0.706 / lbs/day
Jan 2018 Average 33.2 / mg/L 0.261 / lbs/day
Mar 2018 Average 90.6 / mg/L 0.706 / lbs/day
2018 Quarter 1 61.9 / mg/L 0.484 / lbs/day
2018 1st 6 Months(Avg) 61.9 / mg/L 0.484 / lbs/day
2018 1st 6...(Max) 90.6 / mg/L 0.706 / lbs/day
2018 1st 6...(Min) 33.2 / mg/L 0.261 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/31/2018 P JMC013118POTW < 2.5 /200 mg/L < /
03/05/2018 S JMC030518Self < 2.5 /200 mg/L < /
Jan 2018 Week 4 < 2.5 / mg/L < /
Mar 2018 Week 1 < 2.5 / mg/L < /
Jan 2018 Average < 2.5 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date Sam lelD Result/Limit p p Mass/Limit
Oil&Grease,Total
Mar 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/31/2018 P JMC013118POTW 7 /6- 10.5 SU /
03/05/2018 S JMC030518Se1f 7.5 /6- 10.5 SU /
Jan 2018 Week 4 7 / SU /
Mar 2018 Week 1 7.5 / SU /
Jan 2018 Average 7 / SU /
Mar 2018 Average 7.5 / SU /
2018 Quarter 1 7.25 / SU /
2018 1st 6 Months(Avg) 7.25 / SU /
2018 1st 6...(Max) 7.5 / SU /
2018 1st 6...(Min) 7 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/31/2018 P JMC013118POTW < 0.0003 /0.160 mg/L < 0.000002 / lbs/day
03/05/2018 S JMC030518Self < 0.0005 /0.160 mg/L < 0.000004 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 11

JMC (USA),Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
Jan 2018 Week 4 < 0.0003 / mg/L < 0.000002 / lbs/day
Mar 2018 Week 1 < 0.0005 / mg/L < 0.000004 / lbs/day
Jan 2018 Average < 0.0003 /0.090 mg/L < 0.000002 / lbs/day
Mar 2018 Average < 0.0005 /0.090 mg/L < 0.000004 / lbs/day
2018 Quarter 1 < 0.0004 / mg/L < 0.000003 / lbs/day
2018 1st 6 Months(Avg) < 0.0004 / mg/L < 0.000003 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000004 / lbs/day
2018 1st 6...(Min) < 0.0003 / mg/L < 0.000002 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/31/2018 P JMC013118POTW 15 /66 °C /
Jan 2018 Week 4 15 / °C /
Jan 2018 Average 15 / °C /
2018 Quarter 1 15 / °C /
2018 1st 6 Months(Avg) 15 / °C /
2018 1st 6...(Max) 15 / °C /
2018 1st 6...(Min) 15 / °C /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/31/2018 P JMC013118POTW 2.07 / mg/L 0.016 / lbs/day
03/05/2018 S JMC030518Self 4.6 / mg/L 0.036 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Jan 2018 Week 4 2.07 / mg/L 0.016 / lbs/day
Mar 2018 Week 1 4.6 / mg/L 0.036 / lbs/day
Jan 2018 Average 2.07 / mg/L 0.016 / lbs/day
Mar 2018 Average 4.6 / mg/L 0.036 / lbs/day
2018 Quarter 1 3.34 / mg/L 0.026 / lbs/day
2018 1st 6 Months(Avg) 3.34 / mg/L 0.026 / lbs/day
2018 1st 6...(Max) 4.6 / mg/L 0.036 / lbs/day
2018 1st 6...(Min) 2.07 / mg/L 0.016 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/31/2018 P JMC013118POTW 0.117 / mg/L 0.0009 / lbs/day
03/05/2018 S JMC030518Self 0.12 / mg/L 0.0009 / lbs/day
Jan 2018 Week 4 0.117 / mg/L 0.0009 / lbs/day
Mar 2018 Week 1 0.12 / mg/L 0.0009 / lbs/day
Jan 2018 Average 0.117 / mg/L 0.0009 / lbs/day
Mar 2018 Average 0.12 / mg/L 0.0009 / lbs/day
i 2018 Quarter 1 0.119 / mg/L 0.0009 / lbs/day
2018 1st 6 Months(Avg) 0.119 / mg/L 0.0009 / lbs/day
2018 1st 6...(Max) 0.12 / mg/L 0.0009 / lbs/day
2018 1st 6...(Min) 0.117 / mg/L 0.0009 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/31/2018 P JMC013118POTW 0.176 /0.9 mg/L 0.001386 / lbs/day
03/05/2018 S JMC030518Self 0.054 /0.9 mg/L 0.000421 / lbs/day
Jan 2018 Week 4 0.176 / mg/L 0.001386 / lbs/day
Mar 2018 Week 1 0.054 / mg/L 0.000421 / lbs/day
Jan 2018 Average 0.176 /0.56 mg/L 0.001386 / lbs/day
Mar 2018 Average 0.054 /0.56 mg/L 0.000421 / lbs/day
2018 Quarter 1 0.115 / mg/L 0.000903 / lbs/day
2018 1st 6 Months(Avg) 0.115 / mg/L 0.000903 / lbs/day
2018 1st 6...(Max) 0.176 / mg/L 0.001386 / lbs/day
2018 1st 6...(Min) 0.054 / mg/L 0.000421 / lbs/day
2018 l st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall. 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 11 of I

i
Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/26/2018 S Micross012618Self 3.2 / mg/L 0.5024 / lbs/day
02/01/2018 P Micross020118POTW 2.7 / mg/L 0.6468 / lbs/day
Jan 2018 Week 4 3.2 / mg/L 0.5024 / lbs/day
Feb 2018 Week 1 2.7 / mg/L 0.6468 / lbs/day
Jan 2018 Average 3.2 / mg/L 0.5024 / lbs/day
Feb 2018 Average 2.7 / mg/L 0.6468 / lbs/day
2018 Quarter 1 2.95 / mg/L 0.5746 / lbs/day
2018 1st 6 Months(Avg) 2.95 / mg/L 0.5746 / lbs/day
2018 1st 6...(Max) 3.2 / mg/L 0.6468 / lbs/day
2018 1st 6...(Min) 2.7 / mg/L 0.5024 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
01/26/2018 S Micross012618Self < 0.0034 / mg/L < 0.000534 / lbs/day
Jan 2018 Week 4 < 0.0034 / mg/L < 0.000534 / lbs/day
Jan 2018 Average < 0.0034 / mg/L < 0.000534 / lbs/day
2018 Quarter 1 < 0.0034 / mg/L < 0.000534 / lbs/day
2018 1st 6 Months(Avg) < 0.0034 / mg/L < 0.000534 / lbs/day
2018 1st 6...(Max) < 0.0034 / mg/L < 0.000534 / lbs/day
2018 1st 6...(Min) < 0.0034 / mg/L < 0.000534 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Micross0118Flow 0.022042 /0.100 MGD /
02/28/2018 S Micross0218Flow 0.022925 /0.100 MGD /
03/31/2018 S Micross0318Flow 0.02325 /0.100 MGD /
04/30/2018 S Micross0418F1ow 0.030023 /0.100 MGD /
05/31/2018 S Micross05l8Flow 0.038755 /0.100 MGD /
06/30/2018 S Micross06l8Flow 0.045409 /0.100 MGD /
Jan 2018 Week 4 0.022042 / MGD /
Feb 2018 Week 4 0.022925 / MGD /
Mar 2018 Week 4 0.02325 / MGD /
Apr 2018 Week 4 0.030023 / MGD /
May 2018 Week 4 0.038755 / MGD /
Jun 2018 Week 4 0.045409 / MGD /
Jan 2018 Average 0.022042 /0.075 MGD /
Feb 2018 Average 0.022925 /0.075 MGD /
Mar 2018 Average 0.02325 /0.075 MGD /
Apr 2018 Average 0.030023 /0.075 MGD /
May 2018 Average 0.038755 /0.075 MGD /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jun 2018 Average 0.045409 /0.075 MGD /
2018 Quarter 1 0.022739 / MGD /
2018 Quarter 2 0.038062 / MGD /
2018 1st 6 Months(Avg) 0.030401 / MGD /
2018 1st 6...(Max) 0.045409 / MGD /
2018 1st 6...(Min) 0.022042 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/26/2018 S Micross012618Self < 0.00018 / mg/L < 0.000028 / lbs/day
02/01/2018 P Micross020118POTW < 0.00008 / mg/L < 0.000018 / lbs/day
Jan 2018 Week 4 < 0.00018 / mg/L < 0.000028 / lbs/day
Feb 2018 Week 1 < 0.00008 / mg/L < 0.000018 / lbs/day
Jan 2018 Average < 0.00018 / mg/L < 0.000028 / lbs/day
Feb 2018 Average < 0.00008 / mg/L < 0.000018 / lbs/day
2018 Quarter 1 < 0.00013 / mg/L < 0.000023 / lbs/day
2018 1st 6 Months(Avg) < 0.00013 / mg/L < 0.000023 / lbs/day
2018 1st 6...(Max) < 0.00018 / mg/L < 0.000028 / lbs/day
2018 1st 6...(Min) < 0.00008 / mg/L < 0.000018 / lbs/day
2018 1st6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/26/2018 S Micross012618Self 23 / mg/L 3.6112 / lbs/day
02/01/2018 P Micross020118POTW 51 / mg/L 12.2166 / lbs/day
Jan 2018 Week 4 23 / mg/L 3.6112 / lbs/day
Feb 2018 Week 1 51 / mg/L 12.2166 / lbs/day
Jan 2018 Average 23 / mg/L 3.6112 / lbs/day
Feb 2018 Average 51 / mg/L 12.2166 / lbs/day
2018 Quarter 1 37 / mg/L 7.9139 / lbs/day
2018 1st 6 Months(Avg) 37 / mg/L 7.9139 / lbs/day
2018 1st 6...(Max) 51 / mg/L 12.2166 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2018 1st 6...(Min) 23 / mg/L 3.6112 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
01/26/2018 S Micross012618Self 0.003 / mg/L 0.000429 / lbs/day
Jan 2018 Week 4 0.003 / mg/L 0.000429 / lbs/day
Jan 2018 Average 0.003 / mg/L 0.000429 / lbs/day 1
2018 Quarter 1 0.003 / mg/L 0.000429 / lbs/day
2018 1st 6 Months(Avg) 0.003 / mg/L 0.000429 / lbs/day
2018 1st 6...(Max) 0.003 / mg/L 0.000429 / lbs/day
2018 1st 6...(Min) 0.003 / mg/L 0.000429 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/26/2018 S Micross012618Self 0.105 / mg/L 0.016486 / lbs/day
02/01/2018 P Micross020118POTW 0.078 / mg/L 0.018588 / lbs/day
Jan 2018 Week 4 0.105 / mg/L 0.016486 / lbs/day
Feb 2018 Week 1 0.078 / mg/L 0.018588 / lbs/day
Jan 2018 Average 0.105 / mg/L 0.016486 / lbs/day
Feb 2018 Average 0.078 / mg/L 0.018588 / lbs/day
2018 Quarter 1 0.091 / mg/L 0.017537 / lbs/day
2018 1st 6 Months(Avg) 0.091 / mg/L 0.017537 / lbs/day
2018 1st 6...(Max) 0.105 / mg/L 0.018588 / lbs/day
2018 1st 6...(Min) 0.078 / mg/L 0.016486 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/26/2018 S Micross012618Se1f 0.01 / mg/L 0.00157 / lbs/day
02/01/2018 P Micross020118POTW 0.007 / mg/L 0.001677 / lbs/day
Jan 2018 Week 4 0.01 / mg/L 0.00157 / lbs/day
Feb 2018 Week 1 0.007 / mg/L 0.001677 / lbs/day
Jan 2018 Average 0.01 / mg/L 0.00157 / lbs/day
Feb 2018 Average 0.007 / mg/L 0.001677 / lbs/day
2018 Quarter 1 0.009 / mg/L 0.001623 / lbs/day
2018 1st 6 Months(Avg) 0.009 / mg/L 0.001623 / lbs/day
2018 1st 6...(Max) 0.01 / mg/L 0.001677 / lbs/day
2018 1st 6...(Min) 0.007 / mg/L 0.001570 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/26/2018 S Micross012618Self 2.2 /8 mg/L 0.3454 / lbs/day
02/01/2018 P Micross020118POTW 1.51 /8 mg/L 0.3617 / lbs/day
Jan 2018 Week 4 2.2 / mg/L 0.3454 / lbs/day
Feb 2018 Week 1 1.51 / mg/L 0.3617 / lbs/day
Jan 2018 Average 2.2 /6 mg/L 0.3454 / lbs/day
Feb 2018 Average 1.51 /6 mg/L 0.3617 / lbs/day
2018 Quarter 1 1.86 / mg/L 0.3536 / lbs/day
2018 1st 6 Months(Avg) 1.86 / mg/L 0.3536 / lbs/day
2018 1st 6...(Max) 2.2 / mg/L 0.3617 / lbs/day
2018 1st 6...(Min) 1.51 / mg/L 0.3454 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
01/26/2018 S Micross012618SeIf 0.0034 / mg/L 0.000539 / lbs/day
02/01/2018 P Micross020118POTW 0.0018 / mg/L 0.000429 / lbs/day
Jan 2018 Week 4 0.0034 / mg/L 0.000539 / lbs/day
Feb 2018 Week 1 0.0018 / mg/L 0.000429 / lbs/day
Jan 2018 Average 0.0034 / mg/L 0.000539 / lbs/day
Feb 2018 Average 0.0018 / mg/L 0.000429 / lbs/day
2018 Quarter 1 0.0026 / mg/L 0.000484 / lbs/day
2018 1st 6 Months(Avg) 0.0026 / mg/L 0.000484 / lbs/day
2018 1st 6...(Max) 0.0034 / mg/L 0.000539 / lbs/day
2018 1st 6...(Min) 0.0018 / mg/L 0.000429 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/26/2018 S Micross012618SelfHg 0.000003 /0.000142 mg/L /
04/09/2018 P Micross040918POTW 0.000003 /0.000142 mg/L /
Hg
Jan 2018 Week 4 0.000003 / mg/L /
Apr 2018 Week 2 0.000003 / mg/L /
Jan 2018 Average 0.000003 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type. Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Apr 2018 Average 0.000003 / mg/L /
0.000003 2018 Quarter 1 / mg/L /
2018 Quarter 2 0.000003 / mg/L /
2018 1st 6 Months(Avg) 0.0000030 / mg/L /
2018 1st 6...(Max) 0.0000035 / mg/L /
2018 1st 6...(Min) 0.0000026 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/26/2018 S Micross012618Se1f 0.049 / mg/L 0.0077 / lbs/day
02/01/2018 P Micross020118POTW 0.026 / mg/L 0.0063 / lbs/day
Jan 2018 Week 4 0.049 / mg/L 0.0077 / lbs/day
Feb 2018 Week 1 0.026 / mg/L 0.0063 / lbs/day
Jan 2018 Average 0.049 / mg/L 0.0077 / lbs/day
Feb 2018 Average 0.026 / mg/L 0.0063 / lbs/day
2018 Quarter 1 0.038 / mg/L 0.007 / lbs/day
2018 1st 6 Months(Avg) 0.038 / mg/L 0.0070 / lbs/day
2018 1st 6...(Max) 0.049 / mg/L 0.0077 / lbs/day
2018 1st 6...(Min) 0.026 / mg/L 0.0063 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/26/2018 S Micross012618Self 0.0052 / mg/L 0.00081 / lbs/day
02/01/2018 P Micross020118POTW 0.0587 / mg/L 0.014061 / lbs/day
Jan 2018 Week 4 0.0052 / mg/L 0.00081 / lbs/day
Feb 2018 Week 1 0.0587 / mg/L 0.014061 / lbs/day
Jan 2018 Average 0.0052 / mg/L 0.00081 / lbs/day
Feb 2018 Average 0.0587 / mg/L 0.014061 / lbs/day
2018 Quarter 1 0.0319 / mg/L 0.007436 / lbs/day
2018 1st 6 Months(Avg) 0.0319 / mg/L 0.007436 / lbs/day
2018 1st 6...(Max) 0.0587 / mg/L 0.014061 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

Micross Advanced Interconnect Technoloey.LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2018 1st 6...(Min) 0.0052 / mg/L 0.000810 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/26/2018 S Micross012618Self 0.4 / mg/L 0.069 / lbs/day
02/01/2018 P Micross020118POTW 0.4 / mg/L 0.093 / lbs/day
Jan 2018 Week 4 0.4 / mg/L 0.069 / lbs/day
Feb 2018 Week 1 0.4 / mg/L 0.093 / lbs/day
Jan 2018 Average 0.4 / mg/L 0.069 / lbs/day
Feb 2018 Average 0.4 / mg/L 0.093 / lbs/day
2018 Quarter 1 0.4 / mg/L 0.081 / lbs/day
2018 1st 6 Months(Avg) 0.4 / mg/L 0.081 / lbs/day
2018 1st 6...(Max) 0.4 / mg/L 0.093 / lbs/day
2018 1st 6...(Min) 0.4 / mg/L 0.069 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/26/2018 S Micross012618Self 11.44 / mg/L 1.796 / lbs/day
02/01/2018 P Micross020118POTW 8.31 / mg/L 1.991 / lbs/day
Jan 2018 Week 4 11.44 / mg/L . 1.796 / lbs/day
Feb 2018 Week 1 8.31 / mg/L 1.991 / lbs/day
Jan 2018 Average 11.44 / mg/L 1.796 / lbs/day
Feb 2018 Average 8.31 / mg/L 1.991 / lbs/day
2018 Quarter 1 9.88 / mg/L 1.893 / lbs/day
2018 1st 6 Months(Avg) 9.88 / mg/L 1.893 / lbs/day
2018 1st 6...(Max) 11.44 / mg/L 1.991 / lbs/day
2018 1st 6...(Min) 8.31 / mg/L 1.796 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit •
Oil&Grease,Total
01/26/2018 S Micross012618Self 13.6 /200 mg/L /
02/01/2018 P Micross020118POTW < 2.5 /200 mg/L < /
Feb 2018 Week 1 < 2.5 / mg/L < /
Jan 2018 Week 4 13.6 / mg/L /
Jan 2018 Average 13.6 / mg/L /
Feb 2018 Average < 2.5 / mg/L /
2018 Quarter 1 < 8.05 / mg/L < /
2018 1st 6 Months(Avg) < 8.05 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
2018 1st 6...(Max) 13.6 / mg/L /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/26/2018 S Micross012618Se1f 7.2 /5.5- 10.5 SU /
02/01/2018 P Micross020118POTW 8.1 /5.5- 10.5 SU /
Jan 2018 Week 4 7.2 / SU /
Feb 2018 Week 1 8.1 / SU /
Jan 2018 Average 7.2 / SU /
Feb 2018 Average 8.1 / SU /
2018 Quarter 1 7.65 / SU /
2018 1st 6 Months(Avg) 7.65 / SU /
2018 1st 6...(Max) 8.1 / SU /
2018 1st 6...(Min) 7.2 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/26/2018 S Micross012618Se1f < 0.001 / mg/L < 0.000149 / lbs/day
02/01/2018 P Micross020118POTW < 0.0003 / mg/L < 0.00006 / lbs/day
Jan 2018 Week 4 < 0.001 / mg/L < 0.000149 / lbs/day
Feb 2018 Week 1 < 0.0003 / mg/L < 0.00006 / lbs/day
Jan 2018 Average < 0.001 / mg/L < 0.000149 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outful1: '001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
Feb 2018 Average < 0.0003 / mg/L < 0.00006 / lbs/day
2018 Quarter 1 < 0.0006 / mg/L < 0.000105 / lbs/day
2018 1st 6 Months(Avg) < 0.0006 / mg/L < 0.000105 / lbs/day
2018 1st 6...(Max) < 0.0010 / mg/L < 0.000149 / lbs/day
2018 1st 6...(Min) < 0.0003 / mg/L < 0.000060 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/26/2018 S Micross012618Self 13.3 /66 °C /
02/01/2018 P Micross020118POTW 17 /66 °C /
Jan 2018 Week 4 13.3 / °C /
Feb 2018 Week 1 17 / °C /
Jan 2018 Average 13.3 / °C /
Feb 2018 Average 17 / °C /
2018 Quarter 1 15.2 / °C /
2018 1st 6 Months(Avg) 15.2 / °C /
2018 1st 6...(Max) 17 / °C /
2018 1st 6...(Min) 13.3 / °C /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
01/26/2018 S Micross012618Se1f 0.032 / mg/L 0.005055685 / lbs/day
02/01/2018 P Micross020118POTW < 0.013 / mg/L < 0.002994269 / lbs/day
Jan 2018 Week 4 0.032 / mg/L 0 / lbs/day
Feb 2018 Week 1 < 0.013 / mg/L < 0 / lbs/day
Jan 2018 Average 0.032 / mg/L 0 / lbs/day
Feb 2018 Average < 0.013 / mg/L < 0 / lbs/day
2018 Quarter 1 < 0.022 / mg/L < 0 / lbs/day
2018 1st 6 Months(Avg) < 0.022 / mg/L < 0 / lbs/day
2018 1st 6...(Max) 0.032 / mg/L 0 / lbs/day
2018 1st 6...(Min) < 0.013 / mg/L < 0 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10
V

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Tin
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Titanium
01/26/2018 S Micross012618Self < 0 / mg/L < 0 / lbs/day
Jan 2018 Week 4 < 0 / mg/L < 0 / lbs/day
Jan 2018 Average < 0 / mg/L < 0 1 lbs/day
2018 Quarter 1 < 0 / mg/L < 0 / lbs/day
2018 1st 6 Months(Avg) < 0.000 / mg/L < 0.0000 / lbs/day
2018 1st 6...(Max) < 0.000 / mg/L < 0.0000 / lbs/day
2018 1st 6...(Min) < 0.000 / mg/L < 0.0000 / lbs/day
2018 1st 6...(Count) I / I /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/26/2018 S Micross012618Self 11 / mg/L 1.727 / lbs/day
02/01/2018 P Micross020118POTW 7.92 / mg/L 1.897 / lbs/day
Jan 2018 Week 4 11 / mg/L 1.727 / lbs/day
Feb 2018 Week 1 7.92 / mg/L 1.897 1 lbs/day
Jan 2018 Average 11 / mg/L 1.727 / lbs/day
Feb 2018 Average 7.92 / mg/L 1.897 / lbs/day
2018 Quarter 1 9.46 / mg/L 1.812 / lbs/day
2018 1st 6 Months(Avg) 9.46 / mg/L 1.812 / lbs/day
2018 1st 6...(Max) 11 / mg/L 1.897 / lbs/day
2018 1st 6...(Min) 7.92 / mg/L 1.727 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/26/2018 S Micross012618Self 3.3 / mg/L 0.5181 / lbs/day
02/01/2018 P Micross020118POTW 1.67 / mg/L 0.4 / lbs/day
Jan 2018 Week 4 3.3 / mg/L 0.5181 / lbs/day
Feb 2018 Week 1 1.67 / mg/L 0.4 / lbs/day
Jan 2018 Average 3.3 / mg/L 0.5181 / lbs/day
Feb 2018 Average 1.67 / mg/L 0.4 / lbs/day
2018 Quarter 1 2.485 / mg/L 0.4591 / lbs/day
2018 1st 6 Months(Avg) 2.485 / mg/L 0.4591 / lbs/day
2018 1st 6...(Max) 3.3 / mg/L 0.5181 / lbs/day
2018 1st 6...(Min) 1.67 / mg/L 0.4000 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
01/26/2018 S Micross012618Self 0.0444 / mg/L /
Jan 2018 Week 4 0.0444 / mg/L /
Jan 2018 Average 0.0444 / mg/L /
2018 Quarter 1 0.0444 / mg/L /
2018 1st 6 Months(Avg) 0.0444 / mg/L /
2018 1st 6...(Max) 0.0444 / mg/L /
2018 1st 6...(Min) 0.0444 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/26/2018 S Micross012618Se1f 0.569 / mg/L 0.089338 / lbs/day
02/01/2018 P Micross020118POTW 0.543 / mg/L 0.130071 / lbs/day
Jan 2018 Week 4 0.569 / mg/L 0.089338 / lbs/day
Feb 2018 Week 1 0.543 / mg/L 0.130071 / lbs/day
Jan 2018 Average 0.569 / mg/L 0.089338 / lbs/day
Feb 2018 Average 0.543 / mg/L 0.130071 / lbs/day
2018 Quarter 1 0.556 / mg/L 0.109705 / lbs/day
2018 1st 6 Months(Avg) 0.556 / mg/L 0.109705 / lbs/day
2018 1st 6...(Max) 0.569 / mg/L 0.130071 / lbs/day
2018 1st 6...(Min) 0.543 / mg/L 0.089338 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10

Novan, Inc.
• SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
04/09/2018 P Novan040918POTW 0.965 / mg/L /
Apr 2018 Week 2 0.965 / mg/L /
Apr 2018 Average 0.965 / mg/L /
2018 Quarter 2 0.965 / mg/L /
2018 1st 6 Months(Avg) 0.965 / mg/L /
2018 1st 6...(Max) 0.965 / mg/L /
2018 1st 6...(Min) 0.965 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Novan0118F1ow 0.001021 / MGD /
02/28/2018 S Novan0218F1ow 0.000598 / MGD /
03/31/2018 S Novan0318F1ow 0.00089 / MGD /
04/30/2018 S Novan0418F1ow 0.0005 / MGD /
05/31/2018 S Novan0518F1ow 0.000418 / MGD /
06/30/2018 S Novan0618F1ow 0.00057 / MGD /
Jan 2018 Week 4 0.001021 / MGD /
Feb 2018 Week 4 0.000598 / MGD /
Mar 2018 Week 4 0.00089 / MGD /
Apr 2018 Week 4 0.0005 / MGD /
May 2018 Week 4 0.000418 / MGD /
Jun 2018 Week 4 0.00057 / MGD /
Jan 2018 Average 0.001021 /0.020 MGD /
Feb 2018 Average 0.000598 /0.020 MGD /
Mar 2018 Average 0.00089 /0.020 MGD /
Apr 2018 Average 0.0005 /0.020 MGD /
May 2018 Average 0.000418 /0.020 MGD /
Jun 2018 Average 0.00057 /0.020 MGD /
2018 Quarter 1 0.000836 / MGD /
2018 Quarter 2 0.000496 / MGD /
2018 1st 6 Months(Avg) 0.000666 / MGD /
2018 1st 6...(Max) 0.001021 / MGD /
2018 1st 6...(Min) 0.000418 / MGD /
2018 1st 6...(Count) 6 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 7

Novan, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/12/2018 S Novan021218Se1f < 0.001 / mg/L < /
04/09/2018 P Novan040918POTW < 0.00008 / mg/L K /
Feb 2018 Week 2 < 0.001 / mg/L < /
Apr 2018 Week 2 < 0.00008 / mg/L < /
Feb 2018 Average < 0.001 / mg/L < /
Apr 2018 Average < 0.00008 / mg/L /
2018 Quarter 1 < 0.001 / mg/L /
2018 Quarter 2 < 0.00008 / mg/L /
2018 1st 6 Months(Avg) < 0.00054 / mg/L /
2018 1st 6...(Max) < 0.001 / mg/L /
2018 1st 6...(Min) < 0.00008 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/12/2018 S Novan021218Se1f 767 / mg/L /
04/09/2018 P Novan040918POTW 582 / mg/L /
Feb 2018 Week 2 767 / mg/L /
Apr 2018 Week 2 582 / mg/L /
Feb 2018 Average 767 / mg/L /
Apr 2018 Average 582 / mg/L /
2018 Quarter 1 767 / mg/L /
2018 Quarter 2 582 / mg/L /
2018 1st 6 Months(Avg) 674.5 / mg/L /
2018 1st 6...(Max) 767 / mg/L /
2018 1st 6...(Min) 582 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/12/2018 S Novan021218Se1f 0.107 / mg/L /
04/09/2018 P Novan040918POTW 0.088 / mg/L /
Feb 2018 Week 2 0.107 / mg/L /
Monday,February ry 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 7

Novan, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Apr 2018 Week 2 0.088 / mg/L /
Feb 2018 Average 0.107 / mg/L /
Apr 2018 Average 0.088 / mg/L /
2018 Quarter 1 0.107 / mg/L /
2018 Quarter 2 0.088 / mg/L /
2018 1st 6 Months(Avg) 0.098 / mg/L /
2018 1st 6...(Max) 0.107 / mg/L /
2018 1st 6...(Min) 0.088 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
04/09/2018 P Novan040918POTW < 0.005 / mg/L < /
Apr 2018 Week 2 < 0.005 / mg/L < /
Apr 2018 Average < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
04/09/2018 P Novan040918POTW < 0.005 / mg/L < /
Apr 2018 Week 2 < 0.005 / mg/L < /
Apr 2018 Average < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/12/2018 S Novan021218Self 0.000034 /0.000142 mg/L /
04/09/2018 P Novan040918POTW 0.00003 /0.000142 mg/L /
Feb 2018 Week 2 0.000034 / mg/L /
Apr 2018 Week 2 0.00003 / mg/L /
Feb 2018 Average 0.000034 / mg/L /
Apr 2018 Average 0.00003 / mg/L /
2018 Quarter 1 0.000034 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 7

Novan, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2018 Quarter 2 0.00003 / mg/L /
2018 1st 6 Months(Avg) 0.0000319 / mg/L /
2018 1st 6...(Max) 0.0000342 / mg/L /
2018 1st 6...(Min) 0.0000296 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
04/09/2018 P Novan040918POTW < 0.005 / mg/L < /
Apr 2018 Week 2 < 0.005 / mg/L < /
Apr 2018 Average < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/12/2018 S Novan021218Se1f < 0.003 / mg/L < /
04/09/2018 P Novan040918POTW < 0.001 / mg/L < /
Feb 2018 Week 2 < 0.003 / mg/L < /
Apr 2018 Week 2 < 0.001 / mg/L < /
Feb 2018 Average < 0.003 / mg/L < /
Apr 2018 Average < 0.001 / mg/L < /
2018 Quarter 1 < 0.003 / mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) < 0.003 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 7
1I

r
Novan, Inc.
SAMPLE OVERVIEW
ff1 uent Wastewater EOutfall: 001
1/1/2018 To 6/30/2018 Sample Type:
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
04/09/2018 P Novan040918POTW < 0.005 / mg/L < /
Apr 2018 Week 2 < 0.005 / mg/L < /
Apr 2018 Average < 0.005 / mg/L < /
2018 Quarter 2 < 0.005 / mg/L < /
2018 .1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/12/2018 S Novan021218Self 6.6 /6- 10 SU /
04/09/2018 P Novan040918POTW 7.3 /6- 10 SU /
Feb 2018 Week 2 6.6 / SU /
Apr 2018 Week 2 7.3 / SU /
Feb 2018 Average 6.6 / SU /
Apr 2018 Average 7.3 / SU /
2018 Quarter 1 6.6 / SU /
2018 Quarter 2 7.3 / SU /
2018 1st 6 Months(Avg) 6.95 / SU /
2018 lst6...(Max) 7.3 / SU /
2018 1st 6...(Min) 6.6 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/12/2018 S Novan021218Self < 0.0025 / mg/L < /
04/09/2018 P Novan040918POTW < 0.0003 / mg/L < /
Feb 2018 Week 2 < 0.0025 / mg/L < /
Apr 2018 Week 2 < 0.0003 / mg/L < /
Feb 2018 Average < 0.0025 / mg/L < /
Apr 2018 Average < 0.0003 / mg/L < /
2018 Quarter 1 < 0.0025 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 7

Novan, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
2018 Quarter 2 < 0.0003 / mg/L < /
2018 1st 6 Months(Avg) < 0.0014 / mg/L /
2018 1st 6...(Max) < 0.0025 / mg/L < /
2018 1st 6...(Min) < 0.0003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/12/2018 S Novan021218Se1f 19 /66 °C /
04/09/2018 P Novan040918POTW 17 /66 °C /
Feb 2018 Week 2 19 / °C /
Apr 2018 Week 2 17 / °C /
1 Feb 2018 Average 19 / °C /
Apr 2018 Average 17 / °C /
2018 Quarter 1 19 / °C /
2018 Quarter 2 17 / °C /
2018 1st 6 Months(Avg) 18 / °C /
2018 1st 6...(Max) 19 / °C /
2018 1st 6...(Min) 17 / °C /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/12/2018 S Novan021218Se1f 14.1 / mg/L /
04/09/2018 P Novan040918POTW 4.84 / mg/L /
Feb 2018 Week 2 14.1 / mg/L /
Apr 2018 Week 2 4.84 / mg/L /
Feb 2018 Average 14.1 / mg/L /
Apr 2018 Average 4.84 / mg/L /
2018 Quarter 1 14.1 / mg/L /
2018 Quarter 2 4.84 / mg/L /
2018 1st 6 Months(Avg) 9.47 / mg/L /
2018 1st 6...(Max) 14.1 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 7

Nova'', Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
2018 1st 6...(Min) 4.84 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/12/2018 S Novan021218Se1f 3.369 / mg/L /
Feb 2018 Week 2 3.369 / mg/L /
Feb 2018 Average 3.369 / mg/L /
2018 Quarter 1 3.369 / mg/L /
2018 1st 6 Months(Avg) 3.369 / mg/L /
2018 1st 6...(Max) 3.369 / mg/L /
2018 1st 6...(Min) 3.369 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/12/2018 S Novan021218Self 0.4 / mg/L /
04/09/2018 P Novan040918POTW 0.355 / mg/L /
Feb 2018 Week 2 0.4 / mg/L /
Apr 2018 Week 2 0.355 / mg/L /
Feb 2018 Average 0.4 / mg/L /
Apr 2018 Average 0.355 / mg/L /
2018 Quarter 1 0.4 / mg/L /
2018 Quarter 2 0.355 / mg/L /
2018 1st 6 Months(Avg) 0.378 / mg/L /
2018 1st 6...(Max) 0.4 / mg/L /
2018 1st 6...(Min) 0.355 / mg/L /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 7

r
Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S Phononic0l18Flow 0.004932 / MGD /
02/28/2018 S Phononic02l8Flow 0.00951 / MGD /
03/31/2018 S Phononic0318F1ow 0.008662 / MGD /
04/30/2018 S Phononic0418F1ow 0.008764 / MGD /
05/31/2018 S Phononic0518Flow 0.014332 / MGD /
06/30/2018 S Phononic0618F1ow 0.019827 / MGD /
Jan 2018 Week 4 0.004932 / MGD /
Feb 2018 Week 4 0.00951 / MGD /
Mar 2018 Week 4 0.008662 / MGD /
Apr 2018 Week 4 0.008764 / MGD /
May 2018 Week 4 0.014332 / MGD /
Jun 2018 Week 4 0.019827 / MGD /
Jan 2018 Average 0.004932 /0.020 MGD /
Feb 2018 Average 0.00951 /0.020 MGD /
Mar 2018 Average 0.008662 /0.020 MGD /
Apr 2018 Average 0.008764 /0.020 MGD /
May 2018 Average 0.014332 /0.020 MGD /
Jun 2018 Average 0.019827 /0.020 MGD /
2018 Quarter 1 0.007221 / MGD /
2018 Quarter 1 0.008662 / MGD /
2018 Quarter 1 0.007221 / MGD /
2018 Quarter 1 0.008662 / MGD /
2018 Quarter 2 0.014308 / MGD /
2018 1st 6 Months(Avg) 0.011005 / MGD /
2018 1st 6...(Max) 0.019827 / MGD /
2018 1st 6...(Min) 0.004932 / MGD /
2018 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
01/03/2018 S Phononic010318SeIf < 0.003 / mg/L < /
01/08/2018 P Phononic010818POT < 0.05 / mg/L < /
W
01/19/2018 S Phononic011918Self 0.006 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 6

Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
02/07/2018 S Phononic020718Self 0.013 / mg/L /
03/08/2018 S Phononic030818Self 0.531 / mg/L /
04/13/2018 S Phononic041318SeIf 0.054 / mg/L /
05/17/2018 S Phononic051718Se1f 0.026 / mg/L /
06/18/2018 S Phononic061818Se1f 0.006 / mg/L /
Jan 2018 Week 1 < 0.003 / mg/L < /
Jan 2018 Week 2 < 0.05 / mg/L < /
Jan 2018 Week 3 0.006 / mg/L /
Feb 2018 Week 1 0.013 / mg/L /
Mar 2018 Week 2 0.531 / mg/L /
Apr 2018 Week 2 0.054 / mg/L /
May 2018 Week 3 0.026 / mg/L /
Jun 2018 Week 3 0.006 / mg/L /
Jan 2018 Average < 0.02 / mg/L < /
Feb 2018 0.013 Average mg/L g / g/ /
Mar 2018 Average 0.531 / mg/L /
Apr 2018 Average 0.054 / mg/L /
May 2018 Average 0.026 / mg/L /
Jun 2018 Average 0.006 / mg/L /
2018 Quarter I < 0.018 / mg/L < /
2018 Quarter 1 0.531 / mg/L /
2018 Quarter 1 < 0.018 / mg/L < /
2018 Quarter 1 0.531 / mg/L /
2018 Quarter 2 0.029 / mg/L /
2018 1st 6 Months(Avg) < 0.086 / mg/L < /
2018 1st 6...(Max) 0.531 / mg/L /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 8 / /
Sample Date SamplelD Result/Limit Mass/Limit
' Mercury- LL
01/08/2018 P Phononic010818POT 0.000001
l 0.000142 mg/L l
W
02/08/2018 S Phononic020818Selfl-1 0.000002 /0.000142 mg/L /
g
02/16/2018 S Phononic021618Selfl4 < 0.000001 /0.000142 mg/L < /
g
Jan 2018 Week 2 0.000001 / mg/L /
Feb 2018 Week 2 0.000002 / mg/L /
Feb 2018 Week 3 < 0.000001 / mg/L < /
Jan 2018 Average 0.000001 / mg/L /
Feb 2018 Average < 0.000001 / mg/L < /
2018 Quarter 1 < 0.000001 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 6
I

Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2018 1st 6 Months(Avg) < 0.000001 / mg/L < /
2018 1st 6...(Max) 0.000002 / mg/L /
2018 1st 6...(Min) < 0.000001 / mg/L < /
2018 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 2 Weeks Sampled : 3 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/08/2018 P Phononic010818POT 0.002 / mg/L 0.0003 / lbs/day
W
02/07/2018 S Phononic020718Self < 0.003 / mg/L < 0.0003 / lbs/day
Jan 2018 Week 2 0.002 / mg/L 0.0003 / lbs/day
Feb 2018 Week 1 < 0.003 / mg/L < 0.0003 / lbs/day
Jan 2018 Average 0.002 / mg/L 0.0003 / lbs/day
Feb 2018 Average < 0.003 / mg/L < 0.0003 / lbs/day
2018 Quarter 1 < 0.002 / mg/L < 0.0003 / lbs/day
2018 1st 6 Months(Avg) < 0.002 / mg/L < 0.0003 / lbs/day
2018 1st 6...(Max) < 0.003 / mg/L < 0.0003 / lbs/day
2018 1st 6...(Min) 0.002 / mg/L 0.0003 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/03/2018 S Phononic010318Self 0.188 / mg/L 0.007901 /0.02 lbs/day
01/08/2018 P Phononic010818POT 0.0083 / mg/L 0.001434 /0.02 lbs/day
W
01/19/2018 S Phononic011918Self 0.066 / mg/L 0.000511 /0.02 lbs/day
02/07/2018 S Phononic020718Self 0.088 / mg/L 0.009752 /0.02 lbs/day
03/08/2018 S Phononic030818Self 0.028 / mg/L 0.00276 /0.02 lbs/day
04/13/2018 S Phononic041318Self 0.011 / mg/L 0.000786 /0.02 lbs/day
05/17/2018 S Phononic051718Self < 0.0025 / mg/L < 0.000611 /0.02 lbs/day
06/18/2018 S Phononic061818Self 0.211 / mg/L 0.042646 /0.02 lbs/day * *
Jan 2018 Week 1 0.188 / mg/L 0.007901 / lbs/day
Jan 2018 Week 2 0.0083 / mg/L 0.001434 / lbs/day
Jan 2018 Week 3 0.066 / mg/L 0.000511 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 6

Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Feb 2018 Week 1 0.088 / mg/L 0.009752 / lbs/day
Mar 2018 Week 2 0.028 / mg/L 0.00276 / lbs/day
Apr 2018 Week 2 0.011 / mg/L 0.000786 / lbs/day
May 2018 Week 3 < 0.0025 / mg/L < 0.000611 / lbs/day
' Jun 2018 Week 3 0.211 / mg/L 0.042646 / lbs/day
Jan 2018 Average 0.0874 / mg/L 0.003282 / lbs/day
Feb 2018 Average 0.088 / mg/L 0.009752 / lbs/day
Mar 2018 Average 0.028 / mg/L 0.00276 / lbs/day
Apr 2018 Average 0.011 / mg/L 0.000786 / lbs/day
May 2018 Average < 0.0025 / mg/L < 0.000611 / lbs/day
Jun 2018 Average 0.211 / mg/L 0.042646 / lbs/day
2018 Quarter 1 0.0876 / mg/L 0.004899 / lbs/day
2018 Quarter 1 0.028 / mg/L 0.00276 / lbs/day
2018 Quarter 1 0.0876 / mg/L 0.004899 / lbs/day
2018 Quarter 1 0.028 / mg/L 0.00276 / lbs/day
2018 Quarter 2 < 0.0748 / mg/L < 0.014681 / lbs/day
2018 1st 6 Months(Avg) < 0.0754 / mg/L < 0.008300 / lbs/day
2018 1st 6...(Max) 0.211 / mg/L 0.042646 / lbs/day
2018 1st 6...(Min) < 0.0025 / mg/L < 0.000511 / lbs/day
2018 1st 6...(Count) 8 / 8 /
Sample Count: 8 Months Sampled : 6 Weeks Sampled : 8 Quarters Sampled : 5
# % # % # % # cyo
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 1 12.50 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 1 12.50 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/08/2018 P Phononic010818POT 7.6 /5.5- 10 SU /
W
02/07/2018 S Phononic020718Self 7.44 /5.5- 10 SU /
Jan 2018 Week 2 7.6 / SU /
Feb 2018 Week 1 7.44 / SU /
Jan 2018 Average 7.6 / SU /
Feb 2018 Average 7.44 / SU /
2018 Quarter 1 7.52 / SU /
2018 1st 6 Months(Avg) 7.52 / SU /
2018 1st 6...(Max) 7.6 / SU /
2018 1st 6...(Min) 7.44 / SU /
MondayFebruary, 25 2019 *Indicates Violation **In
dicates TRC Violation Page 4 of 6
l

Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
01/03/2018 S Phononic010318Self 0.005 / mg/L /
01/08/2018 P Phononic010818POT < 0.05 / mg/L < /
W
01/19/2018 S Phononic011918Self 0.147 / mg/L /
02/07/2018 S Phononic020718Self 0.117 / mg/L /
03/08/2018 S Phononic030818Se1f 0.501 / mg/L /
04/13/2018 S Phononic041318Se1f 0.07 / mg/L /
05/17/2018 S Phononic051718Se1f 0.029 / mg/L /
06/18/2018 S Phononic061818Se1f 0.024 / mg/L /
Jan 2018 Week 1 0.005 / mg/L /
Jan 2018 Week 2 < 0.05 / mg/L < /
Jan 2018 Week 3 0.147 / mg/L /
Feb 2018 Week 1 0.117 / mg/L /
Mar 2018 Week 2 0.501 / mg/L /
Apr 2018 Week 2 0.07 / mg/L /
May 2018 Week 3 0.029 / mg/L /
Jun 2018 Week 3 0.024 / mg/L /
Jan 2018 Average < 0.067 / mg/L < /
Feb 2018 Average 0.117 / mg/L /
Mar 2018 Average 0.501 / mg/L /
Apr 2018 Average 0.07 / mg/L /
May 2018 Average 0.029 / mg/L /
Jun 2018 Average 0.024 / mg/L /
2018 Quarter 1 < 0.08 / mg/L < /
2018 Quarter 1 0.501 / mg/L /
2018 Quarter 1 < 0.08 / mg/L < /
2018 Quarter 1 0.501 / mg/L /
2018 Quarter 2 0.041 / mg/L /
2018 1st 6 Months(Avg) < 0.118 / mg/L < /
2018 1st 6...(Max) 0.501 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 6

Phononic
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall:• 001
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
2018 1st 6...(Min) 0.005 / mg/L /
2018 1st 6...(Count) 8 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 6

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
06/28/2018 P PowerSecure062818P 8.29 / mg/L /
OTW
06/29/2018 S PowerSecure062918Se 6.66 / mg/L /
If
Jun 2018 Week 4 7.475 / mg/L /
Jun 2018 Average 7.475 / mg/L /
1 2018 Quarter 2 7.475 / mg/L /
2018 1st 6 Months(Avg) 7.475 / mg/L /
2018 1st 6...(Max) 8.29 / mg/L /
2018 1st 6...(Min) 6.66 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/22/2018 S PowerSecure0118Flow 0.000359 / MGD /
02/28/2018 S PowerSecure0218F1ow 0.001429 / MGD /
03/31/2018 S PowerSecure0318F1ow 0.001553 / MGD /
' 04/30/2018 S PowerSecure0418F1ow 0.001049 / MGD /
05/31/2018 S PowerSecure0518Flow 0.000782 / MGD /
06/30/2018 S PowerSecure0618Flow 0.000893 / MGD /
Jan 2018 Week 4 0.000359 / MGD /
Feb 2018 Week 4 0.001429 / MGD /
Mar 2018 Week 4 0.001553 / MGD /
Apr 2018 Week 4 0.001049 / MGD /
May 2018 Week 4 0.000782 / MGD /
Jun 2018 Week 4 0.000893 / MGD /
Jan 2018 Average 0.000359 /0.006 MGD /
Feb 2018 Average 0.001429 /0.006 MGD /
Mar 2018 Average 0.001553 /0.006 MGD /
Apr 2018 Average 0.001049 /0.006 MGD /
May 2018 Average 0.000782 /0.006 MGD /
Jun 2018 Average 0.000893 /0.006 MGD /
2018 Quarter 1 0.001114 / MGD / .
2018 Quarter 2 0.000908 / MGD /
2018 1st 6 Months(Avg) 0.001011 / MGD /
2018 1st 6...(Max) 0.001553 / MGD /
2018 1st 6...(Min) 0.000359 / MGD /
2018 1st 6...(Count) 6 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 8

PowerSecu re
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
06/28/2018 P PowerSecure062818P 0.0035 /0.11 mg/L /
OTW
06/29/2018 S PowerSecure062918Se < 0.0005 /0.11 mg/L < /
If
Jun 2018 Week 4 < 0.002 / mg/L < /
Jun 2018 Average < 0.002 /0.07 mg/L < /
2018 Quarter 2 < 0.002 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) 0.0035 / mg/L /
2018 1st 6...(Min) < 0.0005 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
06/28/2018 P PowerSecure062818P 0.003 /2.77 mg/L /
OTW
06/29/2018 S PowerSecure062918Se < 0.003 /2.77 mg/L < /
If
Jun 2018 Week 4 < 0.003 / mg/L < /
Jun 2018 Average < 0.003 / 1.71 mg/L < /
2018 Quarter 2 < 0.003 / mg/L < /
2018 1st 6 Months(Avg) < 0.003 / mg/L < /
2018 1st 6...(Max) 0.003 / mg/L /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 8
i

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: l Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
06/28/2018 P PowerSecure062818P 0.157 /3.38 mg/L /
OTW
06/29/2018 S PowerSecure062918Se 0.195 /3.38 mg/L /
if
Jun 2018 Week 4 0.176 / mg/L /
Jun 2018 Average 0.176 /2.07 mg/L /
2018 Quarter 2 0.176 / mg/L /
2018 1st 6 Months(Avg) 0.176 / mg/L /
2018 1st 6...(Max) 0.195 / mg/L /
2018 1st 6...(Min) 0.157 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
•
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
06/28/2018 P PowerSecure062818P < 0.003 /0.60 mg/L < /
OTW
06/29/2018 S PowerSecure062918Se < 0.004 /0.60 mg/L < /
if
Jun 2018 Week 4 < 0.003 / mg/L < /
Jun 2018 Average < 0.003 /0.50 mg/L < /
2018 Quarter 2 < 0.003 / mg/L < /
2018 1st 6 Months(Avg) < 0.003 / mg/L < /
2018 1st 6...(Max) < 0.004 / mg/L < /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 8

PowerSecu re
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
06/28/2018 P PowerSecure062818P 0.062 /0.69 mg/L /
OTW
06/29/2018 S PowerSecure062918Se < 0.0025 /0.69 mg/L < /
if
Jun 2018 Week 4 < 0.0323 / mg/L < /
Jun 2018 Average < 0.0323 /0.43 mg/L < /
2018 Quarter 2 < 0.0323 / mg/L < /
2018 1st 6 Months(Avg) < 0.0323 / mg/L < /
2018 1st 6...(Max) 0.062 / mg/L /
2018 1st 6...(Min) < 0.0025 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
06/28/2018 P PowerSecure062818P 0.0000014 /0.000142 mg/L /
OTWHg
06/29/2018 S PowerSecure062918Se < 0.0000005 /0.000142 mg/L < /
If
Jun 2018 Week 4 < 0.000001 / mg/L < /
Jun 2018 Average < 0.000001 / mg/L < /
2018 Quarter 2 < 0.000001 / mg/L < /
2018 1st 6 Months(Avg) < 0.0000010 / mg/L < /
2018 1st 6...(Max) 0.0000014 / mg/L /
2018 1st 6...(Min) < 0.0000005 / mg/L < /
2018 1st 6...(Count) 2 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 8
I

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: I Weeks Sampled: I Quarters Sampled : I
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit 1fass/Limit
Molybdenum
06/28/2018 P PowerSecure062818P < 0.001 / mg/L < /
OTW
06/29/2018 S PowerSecure062918Se < 0.003 / mg/L < /
If
Jun 2018 Week 4 < 0.002 / mg/L < /
Jun 2018 Average < 0.002 / mg/L < /
2018 Quarter 2 < 0.002 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) < 0.003 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
06/28/2018 P PowerSecure062818P 0.0069 / 1.3 mg/L /
OTW
06/29/2018 S PowerSecure062918Se < 0.0025 / 1.3 mg/L < /
If
Jun 2018 Week 4 < 0.0047 / mg/L < /
Jun 2018 Average < 0.0047 / 1 mg/L < /
2018 Quarter 2 < 0.0047 / mg/L < /
2018 1st 6 Months(Avg) < 0.0047 / mg/L < /
2018 1st 6...(Max) 0.0069 / mg/L /
2018 1st 6...(Min) < 0.0025 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : I Weeks Sampled : I Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 8

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
06/28/2018 P PowerSecure062818P 8.6 /6- 10 SU /
OTW
06/29/2018 S PowerSecure062918Se 8.5 /6- 10 SU /
it-
Jun 2018 Week 4 8.55 / SU /
Jun 2018 Average 8.55 / . SU /
2018 Quarter 2 8.55 / SU /
2018 1st 6 Months(Avg) 8.55 / SU /
2018 1st 6...(Max) 8.6 / SU /
2018 1st 6...(Min) 8.5 / SU /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
06/28/2018 P PowerSecure062818P 0.0006 /0.43 mg/L /
OTW
06/29/2018 S PowerSecure062918Se < 0.0025 /0.43 mg/L < /
If
Jun 2018 Week 4 < 0.0016 / mg/L /
Jun 2018 Average < 0.0016 /0.24 mg/L /
2018 Quarter 2 < 0.0016 / mg/L < /
2018 1st 6 Months(Avg) < 0.0016 / mg/L < /
2018 1st 6...(Max) < 0.0025 / mg/L < /
2018 1st 6...(Min) 0.0006 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 8

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
06/28/2018 P PowerSecure062818P 27 /66 °C /
OTW
06/29/2018 S PowerSecure062918Se 22.7 /66 °C /
If
Jun 2018 Week 4 24.9 / °C /
Jun 2018 Average 24.9 / °C /
2018 Quarter 2 24.9 / °C /
2018 1st 6 Months(Avg) 24.9 / °C /
2018 1st 6...(Max) 27 / °C /
2018 1st 6...(Min) 22.7 / °C /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TTO
06/29/2018 S PowerSecure062918Se < 0.000025 /2.13 mg/L < /
If
Jun 2018 Week 4 < 0.000025 / mg/L < /
Jun 2018 Average < 0.000025 / mg/L < /
2018 Quarter 2 < 0.000025 / mg/L < /
2018 1st 6 Months(Avg) < 0.000025 / mg/L < /
2018 1st 6...(Max) < 0.000025 / mg/L < /
2018 1st 6...(Min) < 0.000025 / mg/L < /
2018 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 8

PowerSecure
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
06/28/2018 P PowerSecure062818P 0.08 /2.61 mg/L /
OTW
06/29/2018 S PowerSecure062918Se 0.035 /2.61 mg/L /
If
Jun 2018 Week 4 0.058 / mg/L /
Jun 2018 Average 0.058 / 1.48 mg/L /
2018 Quarter 2 0.058 / mg/L /
2018 1st 6 Months(Avg) 0.058 / mg/L /
2018 1st 6...(Max) 0.08 / mg/L /
2018 1st 6...(Min) 0.035 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # 04
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 8

SCM Metal Products, Inc.
SAMPLE OVERVIEW
j 1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/25/2018 S SCM012518Self 8.5 / mg/L 1.5981 / lbs/day
02/22/2018 P SCM022218POTW 6.6 / mg/L 0.9136 / lbs/day
Jan 2018 Week 4 8.5 / mg/L 1.5981 / lbs/day
Feb 2018 Week 4 6.6 / mg/L 0.9136 / lbs/day
Jan 2018 Average 8.5 / mg/L 1.5981 / lbs/day
Feb 2018 Average 6.6 / mg/L 0.9136 / lbs/day
2018 Quarter 1 7.55 / mg/L 1.2559 / lbs/day
2018 1st 6 Months(Avg) 7.55 / mg/L 1.2559 / lbs/day
2018 1st 6...(Max) 8.5 / mg/L 1.5981 / lbs/day
2018 1st 6...(Min) 6.6 / mg/L 0.9136 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S SCM0118Flow 0.011832 /0.080 MGD /
02/28/2018 S SCM0218Flow 0.010766 /0.080 MGD /
03/31/2018 S SCM0318FIow 0.010653 /0.080 MGD /
04/30/2018 S SCM0418F1ow 0.01037 /0.080 MGD /
05/31/2018 S SCM0518Flow 0.011138 /0.080 MGD /
06/30/2018 S SCM0618FIow 0.011614 /0.080 MGD /
Jan 2018 Week 4 0.011832 / MGD /
Feb 2018 Week 4 0.010766 / MGD /
Mar 2018 Week 4 0.010653 / MGD /
Apr 2018 Week 4 0.01037 / MGD /
May 2018 Week 4 0.011138 / MGD /
Jun 2018 Week 4 0.011614 / MGD /
Jan 2018 Average 0.011832 /0.050 MGD /
Feb 2018 Average 0.010766 /0.050 MGD /
Mar 2018 Average 0.010653 /0.050 MGD /
Apr 2018 Average 0.01037 /0.050 MGD /
May 2018 Average 0.011138 /0.050 MGD /
Jun 2018 Average 0.011614 /0.050 MGD /
2018 Quarter 1 0.011084 / MGD /
2018 Quarter 2 0.011041 / MGD /
2018 1st 6 Months(Avg) 0.011062 / MGD /
2018 1st 6...(Max) 0.011832 / MGD /
2018 1st 6...(Min) 0.01037 / MGD /
2018 1st 6...(Count) 6 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/25/2018 S SCM012518Self < 0.0005 / mg/L < 0.000094 / lbs/day
02/22/2018 P SCM022218POTW < 0.00008 / mg/L < 0.00001 / lbs/day
Jan 2018 Week 4 < 0.0005 / mg/L < 0.000094 / lbs/day
Feb 2018 Week 4 < 0.00008 / mg/L < 0.00001 / lbs/day
Jan 2018 Average < 0.0005 / mg/L < 0.000094 / lbs/day
Feb 2018 Average < 0.00008 / mg/L < 0.00001 / lbs/day
2018 Quarter 1 < 0.00029 / mg/L < 0.000052 / lbs/day
2018 1st 6 Months(Avg) < 0.00029 / mg/L < 0.000052 / lbs/day
2018 1st 6...(Max) < 0.0005 / mg/L < 0.000094 / lbs/day
2018 1st 6...(Min) < 0.00008 / mg/L < 0.000010 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/25/2018 S SCM012518Self 24.7 / mg/L 4.644 / lbs/day
02/22/2018 P SCM022218POTW 22 / mg/L 3.0452 / lbs/day
Jan 2018 Week 4 24.7 / mg/L 4.644 / lbs/day
Feb 2018 Week 4 22 / mg/L 3.0452 / lbs/day
Jan 2018 Average 24.7 / mg/L 4.644 / lbs/day
Feb 2018 Average 22 / mg/L 3.0452 / lbs/day
2018 Quarter 1 23.35 / mg/L 3.8446 / lbs/day
2018 1st 6 Months(Avg) 23.35 / mg/L 3.8446 / lbs/day
2018 1st 6...(Max) 24.7 / mg/L 4.6440 / lbs/day
2018 1st 6...(Min) 22 / mg/L 3.0452 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/25/2018 S SCM012518Self 0.075 /0.75 mg/L 0.014101 / lbs/day
02/22/2018 P SCM022218POTW 0.087 /0.75 mg/L 0.011987 / lbs/day
04/18/2018 S SCM041818Self 0.023 /0.75 mg/L0.026805 / lbs/day
Y
Jan 2018 Week 4 0.075 / mg/L 0.014101 / lbs/day
Feb 2018 Week 4 0.087 / mg/L 0.011987 / lbs/day
Monday,February 25,2019 *Indicates Violation s s Indicates TRC Violation Page 2 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Ouffall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Apr 2018 Week 3 0.023 / mg/L 0.026805 / lbs/day
Jan 2018 Average 0.075 /0.50 mg/L 0.014101 / lbs/day
Feb 2018 Average 0.087 /0.50 mg/L 0.011987 / lbs/day
Apr 2018 Average 0.023 /0.50 mg/L 0.026805 / lbs/day
2018 Quarter 1 0.081 / mg/L 0.013044 / lbs/day
2018 Quarter 2 0.023 / mg/L 0.026805 / lbs/day
2018 1st 6 Months(Avg) 0.062 / mg/L 0.017631 / lbs/day
2018 1st 6...(Max) 0.087 / mg/L 0.026805 / lbs/day
2018 1st 6...(Min) 0.023 / mg/L 0.011987 / lbs/day
2018 1st 6...(Count) 3 / 3 /
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/25/2018 S SCM012518Se1f 0.009 /0.04 mg/L 0.001767 / lbs/day
02/22/2018 P SCM022218POTW 0.016 /0.04 mg/L 0.002215 / lbs/day
Jan 2018 Week 4 0.009 / mg/L 0.001767 / lbs/day
Feb 2018 Week 4 0.016 / mg/L 0.002215 / lbs/day
Jan 2018 Average 0.009 /0.03 mg/L 0.001767 / lbs/day
Feb 2018 Average 0.016 /0.03 mg/L 0.002215 / lbs/day
2018 Quarter 1 0.013 / mg/L 0.001991 / lbs/day
2018 1st 6 Months(Avg) 0.013 / mg/L 0.001991 / lbs/day
2018 1st 6...(Max) 0.016 / mg/L 0.002215 / lbs/day
2018 1st 6...(Min) 0.009 / mg/L 0.001767 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/25/2018 S SCM012518Self 0.48 / mg/L 0.0902 / lbs/day
02/22/2018 P SCM022218POTW 0.6 / mg/L 0.0831 / lbs/day
Jan 2018 Week 4 0.48 / mg/L 0.0902 / lbs/day
Feb 2018 Week 4 0.6 / mg/L 0.0831 / lbs/day
Jan 2018 Average 0.48 / mg/L 0.0902 / lbs/day
Feb 2018 Average 0.6 / mg/L 0.0831 / lbs/day
2018 Quarter 1 0.54 / mg/L 0.0866 / lbs/day
2018 1st 6 Months(Avg) 0.54 / mg/L 0.0866 / lbs/day
2018 1st 6...(Max) 0.6 / mg/L 0.0902 / lbs/day
2018 1st 6...(Min) 0.48 / mg/L 0.0831 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
1 Lead
01/25/2018 S SCM012518Self < 0.0025 /0.20 mg/L < 0.00047 / lbs/day
02/22/2018 P SCM022218POTW < 0.0003 /0.20 mg/L < 0.000035 / lbs/day
04/18/2018 S SCM041818Self < 0.0025 /0.20 mg/L < 0.002926 / lbs/day
Jan 2018 Week 4 < 0.0025 / mg/L < 0.00047 / lbs/day
Feb 2018 Week 4 < 0.0003 / mg/L < 0.000035 / lbs/day
Apr 2018 Week 3 < 0.0025 / mg/L < 0.002926 / lbs/day
Jan 2018 Average < 0.0025 /0.10 mg/L < 0.00047 / lbs/day
Feb 2018 Average < 0.0003 /0.10 mg/L < 0.000035 / lbs/day
Apr 2018 Average < 0.0025 /0.10 mg/L < 0.002926 / lbs/day
2018 Quarter 1 < 0.0014 / mg/L < 0.000252 / lbs/day
2018 Quarter 2 < 0.0025 / mg/L < 0.002926 / lbs/day
2018 1st 6 Months(Avg) < 0.0018 / mg/L < 0.001144 / lbs/day
2018 1st 6...(Max) < 0.0025 / mg/L < 0.002926 / lbs/day
2018 1st 6...(Min) < 0.0003 / mg/L < 0.000035 / lbs/day
2018 1st 6...(Count) 3 / 3 /
Sample Count: 3 Months Sampled: 3 Weeks Sampled : 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/25/2018 S SCM012518Self 0.000004 /0.000142 mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Oatfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
05/11/2018 P SCM051118POTWllg 0.000069 /0.000142 mg/L /
Jan 2018 Week 4 0.000004 / mg/L /
May 2018 Week 2 0.000069 / mg/L /
Jan 2018 Average 0.000004 / mg/L /
May 2018 Average 0.000069 / mg/L /
2018 Quarter 1 0.000004 / mg/L /
2018 Quarter 2 0.000069 / mg/L /
2018 1st 6 Months(Avg) 0.0000362 / mg/L /
2018 1st 6...(Max) 0.0000685 / mg/L /
1 2018 1st 6...(Min) 0.0000039 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/22/2018 P SCM022218POTW < 0.001 / mg/L < 0.0001 / lbs/day
Feb 2018 Week 4 < 0.001 / mg/L < 0.0001 / lbs/day
Feb 2018 Average < 0.001 / mg/L < 0.0001 / lbs/day
2018 Quarter 1 < 0.001 / mg/L < 0.0001 / lbs/day
2018 1st 6 Months(Avg) < 0.001 / mg/L < 0.0001 / lbs/day
2018 1st 6...(Max) < 0.001 / mg/L < 0.0001 / lbs/day
2018 1st 6...(Min) < 0.001 / mg/L < 0.0001 / lbs/day
2018 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/25/2018 S SCM012518Self < 0.0025 / mg/L < 0.00047 / lbs/day
02/22/2018 P SCM022218POTW 0.0019 / mg/L 0.000257 / lbs/day
Jan 2018 Week 4 < 0.0025 / mg/L < 0.00047 / lbs/day
Feb 2018 Week 4 0.0019 / mg/L 0.000257 / lbs/day
Jan 2018 Average < 0.0025 / mg/L < 0.00047 / lbs/day
Feb 2018 Average 0.0019 / mg/L 0.000257 / lbs/day
2018 Quarter 1 < 0.0022 / mg/L < 0.000364 / lbs/day
2018 1st 6 Months(Avg) < 0.0022 / mg/L < 0.000364 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

SCM Metal Products. Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2018 1st 6...(Max) < 0.0025 / mg/L < 0.000470 / lbs/day
2018 1st 6...(Min) 0.0019 / mg/L 0.000257 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/25/2018 S SCM012518Self 0.3 / mg/L 0.055 / lbs/day
02/22/2018 P SCM022218POTW 0.5 / mg/L 0.069 / lbs/day
Jan 2018 Week 4 0.3 / mg/L 0.055 / lbs/day
Feb 2018 Week 4 0.5 / mg/L 0.069 / lbs/day
Jan 2018 Average 0.3 / mg/L 0.055 / lbs/day
Feb 2018 Average 0.5 / mg/L 0.069 / lbs/day
2018 Quarter 1 0.4 / mg/L 0.062 / lbs/day
2018 1st 6 Months(Avg) 0.4 / mg/L 0.062 / lbs/day
2018 1st 6...(Max) 0.5 / mg/L 0.069 / lbs/day
2018 1st 6...(Min) 0.3 / mg/L 0.055 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/25/2018 S SCM012518Self 14.5 / mg/L 2.726 / lbs/day
02/22/2018 P SCM022218POTW 11.8 / mg/L 1.633 / lbs/day
Jan 2018 Week 4 14.5 / mg/L 2.726 / lbs/day
Feb 2018 Week 4 11.8 / mg/L 1.633 / lbs/day
Jan 2018 Average 14.5 / mg/L 2.726 / lbs/day
Feb 2018 Average 11.8 / mg/L 1.633 / lbs/day
2018 Quarter 1 13.15 / mg/L 2.18 / lbs/day
2018 1st 6 Months(Avg) 13.15 / mg/L 2.180 / lbs/day
2018 1st 6...(Max) 14.5 / mg/L 2.726 / lbs/day
2018 1st 6...(Min) 11.8 / mg/L 1.633 / • lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil& Crease,Total
01/25/2018 S SCM012518Self < 2.5 /200 mg/L < /
02/22/2018 P SCM022218POTW < 2.5 /200 mg/L < /
Jan 2018 Week 4 < 2.5 / mg/L < /
Feb 2018 Week 4 < 2.5 / mg/L < /
Jan 2018 Average < 2.5 / mg/L < /
Feb 2018 Average < 2.5 / mg/L < /
2018 Quarter 1 < 2.5 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
2018 1st 6 Months(Avg) < 2.5 / mg/L < /
2018 1st 6...(Max) < 2.5 / mg/L < /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/25/2018 S SCM012518Self 8.3 /6.0- 10.5 SU /
02/22/2018 P SCM022218POTW 7.1 /6.0- 10.5 SU /
04/18/2018 S SCM041818Se1f 7.9 /6.0- 10.5 SU /
Jan 2018 Week 4 8.3 / SU /
Feb 2018 Week 4 7.1 / SU /
Apr 2018 Week 3 7.9 / SU /
Jan 2018 Average 8.3 / SU /
Feb 2018 Average 7.1 / SU /
Apr 2018 Average 7.9 / SU /
2018 Quarter 1 7.7 / SU /
2018 Quarter 2 7.9 / SU /
2018 1st 6 Months(Avg) 7.77 / SU /
2018 1st 6...(Max) 8.3 / SU /
2018 1st 6...(Min) 7.1 / SU /
2018 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
02/22/2018 P SCM022218POTW < 0.001 / mg/L < 0.000138 / lbs/day
Feb 2018 Week 4 < 0.001 / mg/L < 0.000138 / lbs/day
Feb 2018 Average < 0.001 / mg/L < 0.000138 / lbs/day
2018 Quarter 1 < 0.001 / mg/L < 0.000138 / lbs/day
2018 1st 6 Months(Avg) < 0.001 / mg/L < 0.000138 / lbs/day
2018 1st 6...(Max) < 0.001 / mg/L < 0.000138 / lbs/day
2018 1st 6...(Min) < 0.001 / mg/L < 0.000138 / lbs/day
2018 1st 6...(Count) 1 / l /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/25/2018 S SCM012518Self 14 /66 °C /
02/22/2018 P SCM022218POTW 19 /66 °C /
04/18/2018 S SCM041818Self 13.1 /66 °C /
Jan 2018 Week 4 14 / °C /
Feb 2018 Week 4 19 / °C /
Apr 2018 Week 3 13.1 / °C /
Jan 2018 Average 14 / °C /
Feb 2018 Average 19 / °C /
Apr 2018 Average 13.1 / °C /
2018 Quarter 1 16.5 / °C /
2018 Quarter 2 13.1 / °C /
2018 1st 6 Months(Avg) 15.4 / °C /
2018 1st 6...(Max) 19 / °C /
2018 1st 6...(Min) 13.1 / °C /
2018 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 3 Weeks Sampled : 3 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/25/2018 S SCM012518Self 14.2 / mg/L 2.67 / lbs/day
02/22/2018 P SCM022218POTW 11.3 / mg/L 1.564 / lbs/day
Jan 2018 Week 4 14.2 / mg/L 2.67 / lbs/day
Feb 2018 Week 4 11.3 / mg/L 1.564 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Jan 2018 Average 14.2 / mg/L 2.67 / lbs/day
Feb 2018 Average 11.3 / mg/L 1.564 / lbs/day
2018 Quarter 1 12.75 / mg/L 2.117 / lbs/day
2018 1st 6 Months(Avg) 12.75 / mg/L 2.117 / lbs/day
2018 1st 6...(Max) 14.2 / mg/L 2.670 / lbs/day
2018 1st 6...(Min) 11.3 / mg/L 1.564 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/25/2018 S SCM012518Self 2.2 / mg/L 0.4136 / lbs/day
02/22/2018 P SCM022218POTW 1.07 / mg/L 0.1481 / lbs/day
Jan 2018 Week 4 2.2 / mg/L 0.4136 / lbs/day
Feb 2018 Week 4 1.07 / mg/L 0.1481 / lbs/day
Jan 2018 Average 2.2 / mg/L 0.4136 / lbs/day
Feb 2018 Average - 1.07 / mg/L 0.1481 / lbs/day 1
2018 Quarter 1 1.635 / mg/L 0.2809 / lbs/day
2018 1st 6 Months(Avg) 1.635 / mg/L 0.2809 / lbs/day
2018 1st 6...(Max) 2.2 / mg/L 0.4136 / lbs/day
2018 1st 6...(Min) 1.07 / mg/L 0.1481 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
01/25/2018 S SCM012518Self 0.016 / mg/L /
Jan 2018 Week 4 0.016 / mg/L /
Jan 2018 Average 0.016 / mg/L /
2018 Quarter 1 0.016 / mg/L /
2018 1st 6 Months(Avg) 0.016 / mg/L /
2018 1st 6...(Max) 0.016 / mg/L /
2018 1st 6...(Min) 0.016 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/25/2018 S SCM012518Self 0.362 / mg/L 0.068062 / lbs/day
02/22/2018 P SCM022218POTW 0.555 / mg/L 0.076823 / lbs/day
Jan 2018 Week 4 0.362 / mg/L 0.068062 / lbs/day
Feb 2018 Week 4 0.555 / mg/L 0.076823 / lbs/day
Jan 2018 Average 0.362 / mg/L 0.068062 / lbs/day
Feb 2018 Average 0.555 / mg/L 0.076823 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
2018 Quarter 1 0.459 / mg/L 0.072442 / lbs/day
2018 1st 6 Months(Avg) 0.459 / mg/L 0.072442 / lbs/day
2018 1st 6...(Max) 0.555 / mg/L 0.076823 / lbs/day
2018 1st 6...(Min) 0.362 / mg/L 0.068062 / lbs/day
2018 1st 6...(Count) 2 / 2 /
Monday,February25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10
g

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/01/2018 P UTP1020118POTW 2.3 / mg/L /
02/09/2018 S UTP1020918Se1f 1.8 / mg/L /
Feb 2018 Week 1 2.3 / mg/L /
Feb 2018 Week 2 1.8 / mg/L /
Feb 2018 Average 2.05 / mg/L /
2018 Quarter 1 2.05 / mg/L /
2018 1st 6 Months(Avg) 2.05 / mg/L /
2018 1st 6...(Max) 2.3 / mg/L /
2018 1st 6...(Min) 1.8 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2018 S UTP10118F1ow 0.026127 / MGD /
02/28/2018 S UTP10218F1ow 0.03397 / MGD /
03/31/2018 S UTP 10318F1ow 0.024498 / MGD /
04/30/2018 S UTP10418F1ow 0.040425 / MGD /
05/31/2018 S UTP10518F1ow 0.042042 / MGD /
06/30/2018 S UTP 10618F1ow 0.045605 / MGD /
Jan 2018 Week 4 0.026127 / MGD /
Feb 2018 Week 4 0.03397 / MGD /
Mar 2018 Week 4 0.024498 / MGD /
Apr 2018 Week 4 0.040425 / MGD /
May 2018 Week 4 0.042042 / MGD /
Jun 2018 Week 4 0.045605 / MGD /
Jan 2018 Average 0.026127 /0.050 MGD /
Feb 2018 Average 0.03397 /0.050 MGD /
Mar 2018 Average 0.024498 /0.050 MGD /
Apr 2018 Average 0.040425 /0.050 MGD /
May 2018 Average 0.042042 /0.050 MGD / 1
i Jun 2018 Average 0.045605 /0.050 MGD /
2018 Quarter 1 0.028198 / MGD /
2018 Quarter 2 0.042691 / MGD /
2018 1st 6 Months(Avg) 0.035445 / MGD /
2018 1st 6...(Max) 0.045605 / MGD /
2018 1st 6...(Min) 0.024498 / MGD /
2018 1st 6...(Count) 6 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
I
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/01/2018 P UTP1020118POTW 120 / mg/L /
02/09/2018 S UTP1020918Self 18.5 / mg/L /
Feb 2018 Week 1 120 / mg/L /
Feb 2018 Week 2 18.5 / mg/L /
Feb 2018 Average 69.3 / mg/L /
2018 Quarter 1 69.3 / mg/L /
2018 1st 6 Months(Avg) 69.3 / mg/L /
2018 1st 6...(Max) 120 / mg/L /
2018 1st 6...(Min) 18.5 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/01/2018 P UTP1020118POTW < 0.00008 / mg/L < /
02/09/2018 S UTP1020918Se1f < 0.0005 / mg/L < /
Feb 2018 Week 1 < 0.00008 / mg/L < /
Feb 2018 Week 2 < 0.0005 / mg/L < /
Feb 2018 Average < 0.00029 / mg/L < /
2018 Quarter 1 < 0.00029 / mg/L < /
2018 1st 6 Months(Avg) < 0.00029 / mg/L < /
2018 1st 6...(Max) < 0.0005 / mg/L < /
2018 1st 6...(Min) < 0.00008 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/01/2018 P UTP1020118POTW 122 / mg/L /
02/09/2018 S UTP1020918Self 49.3 / mg/L /
Feb 2018 Week 1 122 / mg/L /
Feb 2018 Week 2 49.3 / mg/L / •
Feb 2018 Average 85.65 / mg/L /
2018 Quarter 1 85.65 / mg/L /
2018 1st 6 Months(Avg)g) 85.65 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2018 1st 6...(Max) 122 / mg/L /
2018 1st 6...(Min) 49.3 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
P P
COD
02/01/2018 P UTP1020118POTW 186 / mg/L /
02/09/2018 S UTP1020918Self 81 / mg/L /
Feb 2018 Week 1 186 / mg/L /
Feb 2018 Week 2 81 / mg/L /
Feb 2018 Average 133.5 / mg/L /
2018 Quarter 1 133.5 / mg/L /
2018 1st 6 Months(Avg) 133.5 / mg/L /
2018 1st 6...(Max) 186 / mg/L /
2018 1st 6...(Min) 81 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/01/2018 P UTP1020118POTW < 0.003 / mg/L < /
02/09/2018 S UTP1020918Self 0.008 / mg/L /
Feb 2018 Week 1 < 0.003 / mg/L < /
Feb 2018 Week 2 0.008 / mg/L /
Feb 2018 Average < 0.005 / mg/L < /
2018 Quarter 1 < 0.005 / mg/L < /
2018 1st 6 Months(Avg) < 0.005 / mg/L < /
2018 1st 6...(Max) 0.008 / mg/L /
2018 1st 6...(Min) < 0.003 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/01/2018 P UTP1020118POTW 0.76 / mg/L /
02/09/2018 S UTP1020918Self 0.6 / mg/L /
Feb 2018 Week 1 0.76 / mg/L /
Feb 2018 Week 2 0.6 / mg/L /
Feb 2018 Average 0.68 / mg/L /
2018 Quarter 1 0.68 / mg/L /
2018 1st 6 Months(Avg) 0.68 / mg/L /
2018 1st 6...(Max) 0.76 / mg/L /
2018 1st 6...(Min) 0.6 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/26/2018 S UTP1012618Se1f 0.000015 /0.000142 mg/L /
01/31/2018 P UTP1013118POTWHg 0.000017 /0.000142 mg/L /
02/09/2018 S UTP1020918Self 0.000004 /0.000142 mg/L /
03/09/2018 S UTP1030918Se1f 0.000075 /0.000142 mg/L /
04/19/2018 S UTP1041918Se1f 0.000007 /0.000142 mg/L /
05/17/2018 S UTP1051718Se1f 0.000001 /0.000142 mg/L /
06/08/2018 S UTP1060818Se1f 0.000021 /0.000142 mg/L /
Jan 2018 Week 4 0.000016 / mg/L /
Feb 2018 Week 2 0.000004 / mg/L /
Mar 2018 Week 2 0.000075 / mg/L /
Apr 2018 Week 3 0.000007 / mg/L /
May 2018 Week 3 0.000001 / mg/L /
Jun 2018 Week 2 0.000021 / mg/L /
Jan 2018 Average 0.000016 / mg/L /
Feb 2018 Average 0.000004 / mg/L /
Mar 2018 Average 0.000075 / mg/L /
Apr 2018 Average 0.000007 / mg/L /
May 2018 Average 0.000001 / mg/L /
Jun 2018 Average 0.000021 / mg/L /
2018 Quarter 1 0.000028 / mg/L /
2018 Quarter 2 0.00001 / mg/L /
2018 1st 6 Months(Avg) 0.0000200 / mg/L /
2018 1st 6...(Max) 0.0000745 / mg/L /
2018 1st 6...(Min) 0.0000015 / mg/L /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
1 # % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/01/2018 P UTP1020118POTW < 0.001 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/09/2018 S UTP1020918Se1f < 0.003 / mg/L < /
Feb 2018 Week 1 < 0.001 / mg/L < /
Feb 2018 Week 2 < 0.003 / mg/L < /
Feb 2018 Average < 0.002 / mg/L < /
2018 Quarter 1 < 0.002 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) < 0.003 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/01/2018 P UTP1020118POTW 0.6 / mg/L /
02/09/2018 S UTP1020918Self 0.4 / mg/L /
Feb 2018 Week 1 0.6 / mg/L /
Feb 2018 Week 2 0.4 / mg/L /
Feb 2018 Average 0.5 / mg/L /
2018 Quarter 1 0.5 / mg/L /
2018 1st 6 Months(Avg) 0.5 / mg/L /
2018 1st 6...(Max) 0.6 / mg/L /
2018 1st 6...(Min) 0.4 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/01/2018 P UTP1020118POTW 10.9 / mg/L /
02/09/2018 S UTP1020918Se1f 7 / mg/L /
Feb 2018 Week 1 10.9 / mg/L /
Feb 2018 Week 2 7 / mg/L /
Feb 2018 Average 8.95 / mg/L /
2018 Quarter 1 8.95 / mg/L /
2018 1st 6 Months(Avg) 8.95 / mg/L /
2018 1st 6...(Max) 10.9 / mg/L /
2018 1st 6...(Min) 7 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/01/2018 P UTP1020118POTW < 2.5 /200 mg/L < /
02/09/2018 S UTP1020918Se1f 19.1 /200 mg/L /
Feb 2018 Week 1 < 2.5 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil& Grease,Total
Feb 2018 Week 2 19.1 / mg/L /
Feb 2018 Average < 10.8 / mg/L < /
2018 Quarter 1 < 10.8 / mg/L < /
2018 1st 6 Months(Avg) < 10.8 / mg/L < /
2018 l st 6...(Max) 19.1 / mg/L /
2018 1st 6...(Min) < 2.5 / mg/L < /
2018 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/26/2018 S UTP1012618Self 8.8 /5.5- 10 SU /
02/01/2018 P UTP1020118POTW 8.7 /5.5- 10 SU /
02/09/2018 S UTP1020918Self 9.5 /5.5- 10 SU /
03/09/2018 S UTP1030918Se1f 9.4 /5.5- 10 SU /
04/19/2018 S UTP1041918Se1f 8.8 /5.5- 10 SU /
05/17/2018 S UTP1051718Se1f 7.4 /5.5- 10 SU /
06/08/2018 S UTP1060818Se1f 7.2 /5.5- 10 SU /
Jan 2018 Week 4 8.8 / SU /
Feb 2018 Week 1 8.7 / SU /
Feb 2018 Week 2 9.5 / SU /
Mar 2018 Week 2 9.4 / SU /
Apr 2018 Week 3 8.8 / SU /
May 2018 Week 3 7.4 / SU /
Jun 2018 Week 2 7.2 / SU /
Jan 2018 Average 8.8 / SU /
Feb 2018 Average 9.1 / SU /
Mar 2018 Average 9.4 / SU /
Apr 2018 Average 8.8 / SU /
May 2018 Average 7.4 / SU /
Jun 2018 Average 7.2 / SU /
2018 Quarter 1 9.1 / SU /
2018 Quarter 2 7.8 / SU /
2018 1st 6 Months(Avg) 8.54 / SU /
2018 1st 6...(Max) 9.5 / SU /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2018 1st 6...(Min) 7.2 / SU /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/26/2018 S UTP1012618Self 22.1 /66 °C /
02/01/2018 P UTP1020118POTW 17 /66 °C /
02/09/2018 S UTP1020918Self 19.5 /66 °C /
03/09/2018 S UTP1030918Self 20.4 /66 °C /
04/19/2018 S UTP1041918Self 26.4 /66 °C /
05/17/2018 S UTP1051718Self 25.4 /66 °C /
06/08/2018 S UTP1060818SeIf 24.8 /66 °C /
Jan 2018 Week 4 22.1 / °C /
Feb 2018 Week I 17 / °C /
Feb 2018 Week 2 19.5 / °C /
Mar 2018 Week 2 20.4 / °C /
Apr 2018 Week 3 26.4 / °C /
May 2018 Week 3 25.4 / °C /
Jun 2018 Week 2 24.8 / °C /
Jan 2018 Average 22.1 / °C /
Feb 2018 Average 18.3 / °C /
Mar 2018 Average 20.4 / °C /
Apr 2018 Average 26.4 / °C /
May 2018 Average 25.4 / °C /
Jun 2018 Average 24.8 / °C /
2018 Quarter 1 19.8 / °C /
2018 Quarter 2 25.5 / °C /
2018 1st 6 Months(Avg) 22.2 / °C /
2018 1st 6...(Max) 26.4 / °C /
2018 1st 6...(Min) 17 / °C /
2018 1st 6...(Count) 7 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/01/2018 P UTP1020118POTW 10.3 / mg/L /
02/09/2018 S UTP1020918Se1f 6.6 / mg/L /
Feb 2018 Week 1 10.3 / mg/L /
•
Feb 2018 Week 2 6.6 / mg/L /
Feb 2018 Average 8.45 / mg/L /
2018 Quarter 1 8.45 / mg/L /
2018 1st 6 Months(Avg) 8.45 / mg/L /
2018 1st 6...(
Max)) 10.3 / mg/L /
2018 1st 6...(Min) 6.6 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/01/2018 P UTP1020118POTW 1.25 / mg/L /
02/09/2018 S UTP1020918Se1f 1.2 / mg/L /
Feb 2018 Week 1 1.25 / mg/L /
Feb 2018 Week 2 1.2 / mg/L /
Feb 2018 Average 1.225 / mg/L /
2018 Quarter 1 1.225 / mg/L /
2018 1st 6 Months(Avg) 1.225 / mg/L /
2018 1st 6...(Max) 1.25 / mg/L /
2018 1st 6...(Min) 1.2 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/01/2018 P UTP1020118POTW 54 / mg/L /
02/09/2018 S UTP1020918Se1f 18.6 / mg/L /
Feb 2018 Week 1 54 / mg/L /
Feb 2018 Week 2 18.6 / mg/L /
Feb 2018 Average 36.3 / mg/L /
2018 Quarter 1 36.3 / mg/L /
2018 1st 6 Months(Avg) 36.3 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2018 1st 6...(Max) 54 / mg/L /
2018 1st 6...(Min) 18.6 / mg/L /
2018 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/01/2018 P UTP1020118POTW 0.316 / mg/L /
02/09/2018 S UTP1020918Se1f 0.14 / mg/L /
Feb 2018 Week 1 0.316 / mg/L /
Feb 2018 Week 2 0.14 / mg/L /
Feb 2018 Average 0.228 / mg/L /
2018 Quarter 1 0.228 / mg/L /
2018 1st 6 Months(Avg) 0.228 / mg/L /
2018 1st 6...(Max) 0.316 / mg/L /
2018 1st 6...(Min) 0.14 / mg/L /
2018 1st 6...(Count) 2 / /
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
01/26/2018 S UTP2012618Self 0.145 /20.7 mg/L /
01/31/2018 P UTP2013118POTW 1.23 /20.7 mg/L /
02/09/2018 S UTP2020918Se1f 0.352 /20.7 mg/L /
03/09/2018 S UTP2030918Se1f 0.291 /20.7 mg/L /
04/09/2018 S UTP2040918Se1f 0.034 /20.7 mg/L /
05/17/2018 S UTP2051718Self 0.015 /20.7 mg/L /
06/08/2018 S UTP2060818Self < 0.005 /20.7 mg/L < /
Jan 2018 Week 4 0.688 / mg/L /
Feb 2018 Week 2 0.352 / mg/L /
Mar 2018 Week 2 0.291 / mg/L /
Apr 2018 Week 2 0.034 / mg/L /
May 2018 Week 3 0.015 / mg/L /
Jun 2018 Week 2 < 0.005 / mg/L < /
Jan 2018 Average 0.688 /8.2 mg/L /
Feb 2018 Average 0.352 /8.2 mg/L /
Mar 2018 Average 0.291 /8.2 mg/L /
Apr 2018 Average 0.034 /8.2 mg/L /
May 2018 Average 0.015 /8.2 mg/L /
Jun 2018 Average < 0.005 /8.2 mg/L < /
2018 Quarter 1 0.505 / mg/L /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outtalk 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
2018 Quarter 2 < 0.018 / mg/L < /
2018 1st 6 Months(Avg) < 0.296 / mg/L < /
2018 1st 6...(Max) 1.23 / mg/L /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloroform
03/09/2018 S UTP2030918Se1f 0.028 / mg/L /
Mar 2018 Week 2 0.028 / mg/L /
Mar 2018 Average 0.028 / mg/L /
2018 Quarter 1 0.028 / mg/L /
2018 1st 6 Months(Avg) 0.028 / mg/L /
2018 1st 6...(Max) 0.028 / mg/L /
2018 1st 6...(Min) 0.028 / mg/L /
2018 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
01/26/2018 S UTP2012618SeIf < 0.05 /20.7 mg/L < /
01/31/2018 P UTP2013118POTW < 0.005 /20.7 mg/L < /
02/09/2018 S UTP2020918Se1f < 0.05 /20.7 mg/L < /
03/09/2018 S UTP2030918Se1f < 0.05 /20.7 mg/L < /
04/09/2018 S UTP2040918Se1f < 0.05 /20.7 mg/L < /
05/17/2018 S UTP2051718Se1f < 0.05 /20.7 mg/L < /
06/08/2018 S UTP2060818Self < 0.05 /20.7 mg/L < /
Jan 2018 Week 4 < 0.028 / mg/L < /
Feb 2018 Week 2 < 0.05 / mg/L < /
Mar 2018 Week 2 < 0.05 / mg/L < /
Apr 2018 Week 2 < 0.05 / mg/L < /
May 2018 Week 3 < 0.05 / mg/L < /
Jun 2018 Week 2 < 0.05 / mg/L < /
Jan 2018 Average < 0.028 /8.2 mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 4
I

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
Feb 2018 Average < 0.05 /8.2 mg/L < /
Mar 2018 Average < 0.05 /8.2 mg/L < /
Apr 2018 Average < 0.05 /8.2 mg/L < /
May 2018 Average < 0.05 /8.2 mg/L < /
Jun 2018 Average < 0.05 /8.2 mg/L < /
2018 Quarter 1 < 0.039 / mg/L < /
2018 Quarter 2 < 0.05 / mg/L < /
2018 1st 6 Months(Avg) < 0.044 mg/L <
( g) / P� /
2018 1st 6...(Max) < 0.05 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
01/26/2018 S UTP2012618Se1f < 0.05 /20.7 mg/L < /
01/31/2018 P UTP2013118POTW < 0.005 /20.7 mg/L < /
02/09/2018 S UTP2020918Se1f < 0.05 /20.7 mg/L < /
03/09/2018 S UTP2030918Se1f < 0.05 /20.7 mg/L < /
04/09/2018 S UTP2040918Se1f < 0.05 /20.7 mg/L < /
05/17/2018 S UTP2051718Self < 0.05 /20.7 mg/L < /
06/08/2018 S UTP2060818Self < 0.05 /20.7 mg/L < /
Jan 2018 Week 4 < 0.028 / mg/L < /
Feb 2018 Week 2 < 0.05 / mg/L < /
Mar 2018 Week 2 < 0.05 / mg/L < /
Apr 2018 Week 2 < 0.05 / mg/L < /
May 2018 Week 3 < 0.05 / mg/L < /
Jun 2018 Week 2 < 0.05 / mg/L < /
Jan 2018 Average < 0.028 /8.2 mg/L < /
Feb 2018 Average < 0.05 /8.2 mg/L < /
Mar 2018 Average < 0.05 /8.2 mg/L < /
Apr 2018 Average < 0.05 /8.2 mg/L < /
May 2018 Average < 0.05 /8.2 mg/L < /
Jun 2018 Average < 0.05 /8.2 mg/L < /
2018 Quarter 1 < 0.039 / mg/L < /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 4

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
2018 Quarter 2 < 0.05 / mg/L < /
2018 1st 6 Months(Avg) < 0.044 / mg/L < /
2018 1st 6...(Max) < 0.05 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
01/26/2018 S UTP2012618Se1f < 0.001 /3 mg/L < /
01/31/2018 P UTP2013118POTW < 0.005 /3 mg/L < /
02/09/2018 S UTP2020918Se1f < 0.001 /3 mg/L < /
03/09/2018 S UTP2030918Se1f < 0.001 /3 mg/L < /
04/09/2018 S UTP2040918Se1f < 0.001 /3 mg/L < /
05/17/2018 S UTP2051718Self < 0.001 /3 mg/L < /
06/08/2018 S UTP2060818Self < 0.001 /3 mg/L < /
Jan 2018 Week 4 < 0.003 / mg/L < /
Feb 2018 Week 2 < 0.001 / mg/L < /
Mar 2018 Week 2 < 0.001 / mg/L < /
Apr 2018 Week 2 < 0.001 / mg/L < /
May 2018 Week 3 < 0.001 / mg/L < /
Jun 2018 Week 2 < 0.001 / mg/L < /
Jan 2018 Average < 0.003 /0.7 mg/L < /
Feb 2018 Average < 0.001 /0.7 mg/L < /
Mar 2018 Average < 0.001 /0.7 mg/L < /
Apr 2018 Average < 0.001 /0.7 mg/L < /
May 2018 Average < 0.001 /0.7 mg/L < /
Jun 2018 Average < 0.001 /0.7 mg/L < /
2018 Quarter 1 < 0.002 / mg/L < /
2018 Quarter 2 < 0.001 / mg/L < /
2018 1st 6 Months(Avg) < 0.002 / mg/L < /
2018 1st 6...(Max) < 0.005 / mg/L < /
2018 1st 6...(Min) < 0.001 / mg/L < /
2018 1st 6...(Count) 7 / /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 4

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2018 To 6/30/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
01/26/2018 S UTP2012618Se1f < 0.025 /20.7 mg/L < /
01/31/2018 P UTP2013118POTW < 0.005 /20.7 mg/L < /
02/09/2018 S UTP2020918Se1f < 0.025 /20.7 mg/L < /
03/09/2018 S UTP2030918Se1f < 0.025 /20.7 mg/L < /
04/09/2018 S UTP2040918Se1f < 0.025 /20.7 mg/L < /
05/17/2018 S UTP2051718Se1f < 0.025 /20.7 mg/L < /
06/08/2018 S UTP2060818Se1f < 0.025 /20.7 mg/L < /
Jan 2018 Week 4 < 0.015 / mg/L < /
Feb 2018 Week 2 < 0.025 / mg/L < /
Mar 2018 Week 2 < 0.025 / mg/L < /
Apr 2018 Week 2 < 0.025 / mg/L < /
May 2018 Week 3 < 0.025 / mg/L < /
Jun 2018 Week 2 < 0.025 / mg/L < /
Jan 2018 Average < 0.015 /8.2 mg/L < /
Feb 2018 Average < 0.025 /8.2 mg/L < /
Mar 2018 Average < 0.025 /8.2 mg/L < /
Apr 2018 Average < 0.025 /8.2 mg/L < /
May 2018 Average < 0.025 /8.2 mg/L < /
Jun 2018 Average < 0.025 /8.2 mg/L < /
2018 Quarter 1 < 0.02 / mg/L < /
2018 Quarter 2 < 0.025 / mg/L < /
2018 1st 6 Months(Avg) < 0.022 / mg/L < /
2018 1st 6...(Max) < 0.025 / mg/L < /
2018 1st 6...(Min) < 0.005 / mg/L < /
2018 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 4

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
08/01/2018 S AstraZeneca0718F1ow 0.001049 / MGD /
08/31/2018 S AstraZeneca0818F1ow 0.000655 / MGD /
10/01/2018 S AstraZeneca0918F1ow 0.00061 / MGD /
11/01/2018 S AstraZenecal018Flow 0.000678 / MGD /
12/03/2018 S AstraZenecal118Flow 0.000724 / MGD /
12/31/2018 S AstraZenecal218Flow 0.000012 / MGD /
Aug 2018 Week 1 0.001049 / MGD /
Aug 2018 Week 4 0.000655 / MGD /
Oct 2018 Week 1 0.00061 / MGD /
Nov 2018 Week 1 0.000678 / MGD /
Dec 2018 Week 1 0.000724 / MGD /
Dec 2018 Week 4 0.000012 / MGD /
Aug 2018 Average 0.000852 /0.002000 MGD /
Oct 2018 Average 0.00061 /0.002000 MGD /
Nov 2018 Average 0.000678 /0.002000 MGD /
Dec 2018 Average 0.000368 /0.002000 MGD /
2018 Quarter 3 0.000852 / MGD /
2018 Quarter 4 0.000506 / MGD /
2018 2nd 6 Months(Avg) 0.000621 / MGD /
2018 2nd 6...(Max) 0.001049 / MGD /
2018 2nd 6...(Min) 0.000012 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 4 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
1 #Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/13/2018 S AstraZeneca081318Se1 < 7.5 / mg/L < /
f
10/05/2018 P AstraZeneca100518PO 133 / mg/L /
TW
Aug 2018 Week 2 < 7.5 / mg/L < /
Oct 2018 Week 1 133 / mg/L /
Aug 2018 Average < 7.5 / mg/L < /
Oct 2018 Average 133 / mg/L /
2018 Quarter 3 < 7.5 / mg/L < /
2018 Quarter 4 133 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2018 To 12%31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Dale SamplelD Result/Limit Mass/Limit
COD
2018 2nd 6 Months(Avg) < 70.3 / mg/L < /
2018 2nd 6...(Max) 133 / mg/L /
2018 2nd 6...(Min) < 7.5 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/13/2018 S AstraZeneca081318Se1 < 0.0025 /20.7 mg/L < /
f
Aug 2018 Week 2 < 0.0025 / mg/L /
Aug 2018 Average < 0.0025 /8.2 mg/L < /
2018 Quarter 3 < 0.0025 / mg/L < /
' 2018 2nd 6 Months(Avg) < 0.0025 / mg/L /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
08/13/2018 S AstraZeneca081318Se1 < 0.0025 /20.7 mg/L < /
f
Aug 2018 Week 2 < 0.0025 / mg/L < /
Aug 2018 Average < 0.0025 /8.2 mg/L < /
2018 Quarter 3 < 0.0025 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/13/2018 S AstraZeneca081318Sel 0.000009 /0.000142 mg/L /
fHg
10/05/2018 P AstraZeneca100518PO 0.000002 /0.000142 mg/L /
TWHg
Aug 2018 Week 2 0.000009 / mg/L /
Oct 2018 Week 1 0.000002 / mg/L /
Aug 2018 Average 0.000009 / mg/L /
Oct 2018 Average 0.000002 / mg/L /
2018 Quarter 3 0.000009 / mg/L /
2018 Quarter 4 0.000002 / mg/L /
2018 2nd 6 Months(Avg) 0.000005 / mg/L /
2018 2nd 6...(Max) 0.000009 / mg/L /
2018 2nd 6...(Min) 0.000002 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/13/2018 S AstraZeneca08 1 3 1 8S el < 0.003 /3 mg/L < /
f
Aug 2018 Week 2 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /0.7 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/13/2018 S AstraZeneca081318Se1 < 0.003 /20.7 mg/L < /
f
Aug 2018 Week 2 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /8.2 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/13/2018 S AstraZeneca081318Se1 8 /6- 10 SU /
f
10/05/2018 P AstraZeneca100518PO 7.4 /6- 10 SU /
TW
Aug 2018 Week 2 8 / SU /
Oct 2018 Week 1 7.4 / SU /
Aug 2018 Average 8 / SU /
Oct 2018 Average 7.4 / SU /
2018 Quarter 3 8 / SU /
2018 Quarter 4 7.4 / SU /
2018 2nd 6 Months(Avg) 7.7 / SU /
2018 2nd 6...(Max) 8 / SU /
2018 2nd 6...(Min) 7.4 / SU /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 5

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
08/21/2018 S Aurobindo082118Se1f 0.056 / 10.35 mg/L /
Aug 2018 Week 3 0.056 / mg/L /
Aug 2018 Average 0.056 /4.1 mg/L /
2018 Quarter 3 0.056 / mg/L /
2018 2nd 6 Months(Avg) 0.056 / mg/L /
2018 2nd 6...(Max) 0.056 / mg/L /
2018 2nd 6...(Min) 0.056 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/21/2018 S Aurobindo082118Se1f 10.8 / mg/L /
09/27/2018 P Aurobindo092718POT 43.1 / mg/L /
W
Aug 2018 Week 3 10.8 / mg/L /
Sep 2018 Week 4 43.1 / mg/L /
Aug 2018 Average 10.8 / mg/L /
Sep 2018 Average 43.1 / mg/L /
2018 Quarter 3 26.95 / mg/L /
2018 2nd 6 Months(Avg) 26.95 / mg/L /
2018 2nd 6...(Max) 43.1 / mg/L /
2018 2nd 6...(Min) 10.8 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/18/2018 S Aurobindo0718F1ow 0.000946 / MGD /
08/22/2018 S Aurobindo0818F1ow 0.001825 / MGD /
09/20/2018 S Aurobindo0918F1ow 0.002022 / MGD /
10/18/2018 S Aurobindo1018F1ow 0.001359 / MGD /
11/30/2018 S Aurobindol118Flow 0.00231 / MGD /
12/20/2018 S Aurobindo1218Flow 0.002951 / MGD /
Jul 2018 Week 3 0.000946 / MGD /
Aug 2018 Week 4 0.001825 / MGD /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2018 Week 3 0.002022 / MGD /
Oct 2018 Week 3 0.001359 / MGD /
Nov 2018 Week 4 0.00231 / MGD /
Dec 2018 Week 3 0.002951 / MGD /
Jul 2018 Average 0.000946 /0.039 MGD /
Aug 2018 Average 0.001825 /0.039 MGD /
Sep 2018 Average 0.002022 /0.039 MOD /
Oct 2018 Average 0.001359 /0.039 MGD /
Nov 2018 Average 0.00231 /0.039 MGD /
Dec 2018 Average 0.002951 /0.039 MGD /
2018 Quarter 3 0.001598 / MGD /
2018 Quarter 4 0.002207 / MGD /
2018 2nd 6 Months(Avg) 0.001902 / MGD /
2018 2nd 6...(Max) 0.002951 / MGD /
2018 2nd 6...(Min) 0.000946 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
08/21/2018 S Aurobindo082118Se1f 50 / mg/L /
09/27/2018 P Aurobindo092718POT 159 / mg/L /
W
Aug 2018 Week 3 50 / mg/L /
Sep 2018 Week 4 159 / mg/L /
Aug 2018 Average 50 / mg/L /
Sep 2018 Average 159 / mg/L /
2018 Quarter 3 104.5 / mg/L /
2018 2nd 6 Months(Avg) 104.5 / mg/L /
2018 2nd 6...(Max) 159 / mg/L /
2018 2nd 6...(Min) 50 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/21/2018 S Aurobindo082118Self < 0.00008 / mg/L < /
09/27/2018 P Aurobindo092718POT 0.00023 / mg/L /
W
Aug 2018 Week 3 < 0.00008 / mg/L < /
Sep 2018 Week 4 0.00023 / mg/L /
Aug 2018 Average < 0.00008 / mg/L < /
Sep 2018 Average 0.00023 / mg/L /
2018 Quarter 3 < 0.00015 / mg/L < /
2018 2nd 6 Months(Avg) < 0.00015 / mg/L < /
2018 2nd 6...(Max) 0.00023 / mg/L /
2018 2nd 6...(Min) < 0.00008 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/21/2018 S Aurobindo082118Se1f 27 / mg/L /
09/27/2018 P Aurobindo092718POT 53.8 / mg/L /
W
Aug 2018 Week 3 27 / mg/L /
Sep 2018 Week 4 53.8 / mg/L /
Aug 2018 Average 27 / mg/L /
Sep 2018 Average 53.8 / mg/L /
2018 Quarter 3 40.4 / mg/L /
2018 2nd 6 Months(Avg) 40.4 / mg/L /
2018 2nd 6...(Max) 53.8 / mg/L /
2018 2nd 6...(Min) 27 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/21/2018 S Aurobindo082118Se1f 127 / mg/L /
09/27/2018 P Aurobindo092718POT 213 / mg/L /
W
Aug 2018 Week 3 127 / mg/L /
Sep 2018 Week 4 213 / mg/L /
Aug 2018 Average 127 / mg/L /
Sep 2018 Average 213 / mg/L /
2018 Quarter 3 170 / mg/L /
2018 2nd 6 Months(Avg) 170 / mg/L /
2018 2nd 6...(Max) 213 / mg/L /
2018 2nd 6...(Min) 127 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/21/2018 S Aurobindo082118Se1f 0.055 / mg/L /
09/27/2018 P Aurobindo092718POT 0.07 / mg/L /
W
Aug 2018 Week 3 0.055 / mg/L /
Sep 2018 Week 4 0.07 / ' mg/L /
Aug 2018 Average 0.055 / mg/L /
Sep 2018 Average 0.07 / mg/L /
2018 Quarter 3 0.063 / mg/L /
2018 2nd 6 Months(Avg) 0.063 / mg/L /
2018 2nd 6...(Max) 0.070 / mg/L /
2018 2nd 6...(Min) 0.055 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/21/2018 S Aurobindo082118Se1f 0.009 / mg/L /
09/27/2018 P Aurobindo092718POT < 0.003 / mg/L < /
W
Aug 2018 Week 3 0.009 / mg/L /
Sep 2018 Week 4 < 0.003 / mg/L < /
Aug 2018 Average 0.009 / mg/L /
Sep 2018 Average < 0.003 / mg/L < /
2018 Quarter 3 < 0.006 / mg/L < /
2018 2nd 6 Months(Avg) < 0.006 / mg/L < /
2018 2nd 6...(Max) 0.009 / mg/L /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/21/2018 S Aurobindo082118Se1f < 0.003 / 10.35 mg/L < /
Aug 2018 Week 3 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /4.1 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
' Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/21/2018 S Aurobindo082118Self < 0.05 / mg/L < /
09/27/2018 P Aurobindo092718POT < 0.05 / mg/L < /
W
Aug 2018 Week 3 < 0.05 / mg/L < /
Sep 2018 Week 4 < 0.05 / mg/L < /
Aug 2018 Average < 0.05 / mg/L < /
Sep 2018 Average < 0.05 / mg/L < /
2018 Quarter 3 < 0.05 / mg/L < /
2018 2nd 6 Months(Avg) < 0.05 / mg/L < /
2018 2nd 6...(Max) < 0.05 / mg/L < /
2018 2nd 6...(Min) < 0.05 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
08/21/2018 S Aurobindo082118Self < 0.003 / 10.35 mg/L < /
Aug 2018 Week 3 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /4.1 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
08/21/2018 S Aurobindo082118Se1f 0.000017 /0.00142 mg/L /
Hg
12/03/2018 P Aurobindo120318POT 0.000032 /0.00142 mg/L /
WHg
Aug 2018 Week 3 0.000017 / mg/L /
Dec 2018 Week 1 0.000032 / mg/L /
Aug 2018 Average 0.000017 / mg/L /
Dec 2018 Average 0.000032 / mg/L /
2018 Quarter 3 0.000017 / mg/L /
2018 Quarter 4 0.000032 / mg/L /
2018 2nd 6 Months(Avg) 0.000025 / mg/L /
2018 2nd 6...(Max) 0.000032 / mg/L /
2018 2nd 6...(Min) 0.000017 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/21/2018 S Aurobindo082118Self < 0.003 / 1.5 mg/L < /
Aug 2018 Week 3 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /0.35 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/21/2018 S Aurobindo082118Self < 0.001 / mg/L < /
09/27/2018 P Aurobindo092718POT < 0.001 / mg/L < /
W
Aug 2018 Week 3 < 0.001 / mg/L < /
Sep 2018 Week 4 < 0.001 / mg/L < /
Aug 2018 Average < 0.001 / mg/L < /
Sep 2018 Average < 0.001 / mg/L < /
2018 Quarter 3 < 0.001 / mg/L < /
2018 2nd 6 Months(Avg) < 0.001 / mg/L < /
2018 2nd 6...(Max) < 0.001 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/21/2018 S Aurobindo082118Self < 0.003 / 10.35 mg/L < /
Aug 2018 Week 3 < 0.003 / mg/L < /
Aug 2018 Average < 0.003 /4.1 mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/21/2018 S Aurobindo082118Se1f 0.4 / mg/L /
09/27/2018 P Aurobindo092718POT 0.4 / mg/L /
W
Aug 2018 Week 3 0.4 / mg/L /
Sep 2018 Week 4 0.4 / mg/L /
Aug 2018 Average 0.4 / mg/L /
Sep 2018 Average 0.4 / mg/L /
2018 Quarter 3 0.4 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2018 2nd 6 Months(Avg) 0.4 / mg/L /
2018 2nd 6...(Max) 0.4 / mg/L /
2018 2nd 6...(Min) 0.4 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/21/2018 S Aurobindo082118Self 21 / mg/L /
09/27/2018 P Aurobindo092718POT 70.7 / mg/L /
W
Aug 2018 Week 3 21 / mg/L /
Sep 2018 Week 4 70.7 / mg/L /
Aug 2018 Average 21 / mg/L /
Sep 2018 Average 70.7 / mg/L /
2018 Quarter 3 45.85 / mg/L /
2018 2nd 6 Months(Avg) 45.85 / mg/L /
2018 2nd 6...(Max) 70.7 / mg/L /
2018 2nd 6...(Min) 21 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/21/2018 S Aurobindo082118Self < 2.5 /200 mg/L < /
09/27/2018 P Aurobindo092718POT 8 /200 mg/L /
W
Aug 2018 Week 3 < 2.5 / mg/L < /
Sep 2018 Week 4 8 / mg/L /
Aug 2018 Average < 2.5 / mg/L < /
Sep 2018 Average 8 / mg/L /
2018 Quarter 3 < 5.25 / mg/L < /
2018 2nd 6 Months(Avg) < 5.25 / mg/L < /
2018 2nd 6...(Max) 8 / mg/L /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
pH
09/27/2018 P Aurobindo092718POT 9 /6.0- 10.0 SU /
W
Sep 2018 Week 4 9 / SU /
Sep 2018 Average 9 / SU /
2018 Quarter 3 9 / SU /
2018 2nd 6 Months(Avg) 9 / SU /
2018 2nd 6...(Max) 9 / SU /
2018 2nd 6...(Min) 9 / SU /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/21/2018 S Aurobindo082118Self 26 /66 °C /
09/27/2018 P Aurobindo092718POT 23 /66 °C /
W
Aug 2018 Week 3 26 / °C /
Sep 2018 Week 4 23 / °C /
Aug 2018 Average 26 / °C /
Sep 2018 Average 23 / °C /
2018 Quarter 3 24.5 / °C /
2018 2nd 6 Months(Avg) 24.5 / °C /
2018 2nd 6...(Max) 26 / °C /
2018 2nd 6...(Min) 23 / °C /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/21/2018 S Aurobindo082118Se1f 20.6 / mg/L /
09/27/2018 P Aurobindo092718POT 70.3 / mg/L /
W
Aug 2018 Week 3 20.6 / mg/L /
Sep 2018 Week 4 70.3 / mg/L /
Aug 2018 Average 20.6 / mg/L /
Sep 2018 Average 70.3 / mg/L /
2018 Quarter 3 45.45 / mg/L /
2018 2nd 6 Months(Avg) 45.45 / mg/L /
2018 2nd 6...(Max) 70.3 / mg/L /
2018 2nd 6...(Min) 20.6 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/21/2018 S Aurobindo082118Self 3 / mg/L /
09/27/2018 P Aurobindo092718POT 7.14 / mg/L /
W
Aug 2018 Week 3 3 / mg/L /
Sep 2018 Week 4 7.14 / mg/L /
Aug 2018 Average 3 / mg/L /
Sep 2018 Average 7.14 / mg/L /
2018 Quarter 3 5.07 / mg/L /
2018 2nd 6 Months(Avg) 5.07 / mg/L /
2018 2nd 6...(Max) 7.14 / mg/L /
2018 2nd 6...(Min) 3 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
08/21/2018 S Aurobindo082118Self 66 / mg/L /
09/27/2018 P Aurobindo092718POT 104 / mg/L /
W
Aug 2018 Week 3 66 / mg/L /
Sep 2018 Week 4 104 / mg/L /
Aug 2018 Average 66 / mg/L /
Sep 2018 Average 104 / mg/L /
2018 Quarter 3 85 / mg/L /
2018 2nd 6 Months(Avg) mg/L( g) 85 / g/ /
2018 2nd 6...(Max) 104 / mg/L /
2018 2nd 6...(Min) 66 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/21/2018 S Aurobindo082118Self 0.314 / mg/L /
09/27/2018 P Aurobindo092718POT 0.276 / mg/L /
W
Aug 2018 Week 3 0.314 / mg/L /
Sep 2018 Week 4 0.276 / mg/L /
Aug 2018 Average 0.314 / mg/L /
Sep 2018 Average 0.276 / mg/L /
2018 Quarter 3 0.295 / mg/L /
2018 2nd 6 Months(Avg) 0.295 / mg/L /
2018 2nd 6...(Max) 0.314 / mg/L /
2018 2nd 6...(Min) 0.276 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 11

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
09/25/2018 P Biogen092518POTW 0.329 / 12.19 mg/L 0.2277 / lbs/day
Sep 2018 Week 4 0.329 / mg/L 0.2277 / lbs/day
Sep 2018 Average 0.329 /4.83 mg/L 0.2277 / lbs/day
2018 Quarter 3 0.329 / mg/L 0.2277 / lbs/day
2018 2nd 6 Months(Avg) 0.329 / mg/L 0.2277 / lbs/day
2018 2nd 6...(Max) 0.329 / mg/L 0.2277 / lbs/day
2018 2nd 6...(Min) 0.329 / mg/L 0.2277 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/17/2018 S Biogen071718Self 2.3 / mg/L 1.6397 / lbs/day
09/25/2018 P Biogen092518POTW 1.9 / mg/L 1.3149 / lbs/day
Jul 2018 Week 3 2.3 / mg/L 1.6397 / lbs/day
Sep 2018 Week 4 1.9 / mg/L 1.3149 / lbs/day
Jul 2018 Average 2.3 / mg/L 1.6397 / lbs/day
Sep 2018 Average 1.9 / mg/L 1.3149 / lbs/day
2018 Quarter 3 2.1 / mg/L 1.4773 / lbs/day
2018 2nd 6 Months(Avg) 2.1 / mg/L 1.4773 / lbs/day
2018 2nd 6...(Max) 2.3 / mg/L 1.6397 / lbs/day 1
2018 2nd 6...(Min) 1.9 / mg/L 1.3149 / lbs/day 1
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Biogen0718Flow 0.070479 /0.375 MGD /
08/31/2018 S Biogen0818Flow 0.08515 /0.375 MGD /
09/30/2018 S Biogen0918Flow 0.092437 /0.375 MGD /
10/31/2018 S Biogen1018Flow 0.08117 /0.375 MGD /
11/30/2018 S Biogenl118Flow 0.077928 /0.375 MGD /
12/31/2018 S Biogen1218Flow 0.065762 /0.375 MGD /
Jul 2018 Week 4 0.070479 / MGD /
Aug 2018 Week 4 0.08515 / MGD /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2018 Week 4 0.092437 / MGD /
Oct 2018 Week 4 0.08117 / MGD /
Nov 2018 Week 4 0.077928 / MGD /
Dec 2018 Week 4 0.065762 / MGD /
Jul 2018 Average 0.070479 /0.250 MGD /
Aug 2018 Average 0.08515 /0.250 MGD /
Sep 2018 Average 0.092437 /0.250 MGD /
Oct 2018 Average 0.08117 /0.250 MGD /
Nov 2018 Average 0.077928 /0.250 MGD /
Dec 2018 Average 0.065762 /0.250 MGD /
2018 Quarter 3 0.082689 / MGD /
2018 Quarter 4 0.074953 / MGD /
2018 2nd 6 Months(Avg) 0.078821 / MGD /
2018 2nd 6...(Max) 0.092437 / MGD /
2018 2nd 6...(Min) 0.065762 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/17/2018 S Biogen071718Self 9 / mg/L 6.416 / lbs/day
09/25/2018 P Biogen092518POTW 38 / mg/L 26.298 / lbs/day
Jul 2018 Week 3 9 / mg/L 6.416 / lbs/day
Sep 2018 Week 4 38 / mg/L 26.298 / lbs/day
Jul2018 Average 9 / mg/L 6.416 / lbs/day
Sep 2018 Average 38 / mg/L 26.298 / lbs/day
2018 Quarter 3 23.5 / mg/L 16.357 / lbs/day
2018 2nd 6 Months(Avg) 23.5 / mg/L 16.357 / lbs/day
2018 2nd 6...(Max) 38 / mg/L 26.298 / lbs/day
2018 2nd 6...(Min) 9 / mg/L 6.416 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 9

I
Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/17/2018 S Biogen071718Self < 0.0005 / mg/L < 0.000356 / lbs/day
09/25/2018 P Biogen092518POTW < 0.00008 / mg/L < 0.000052 / lbs/day
Jul 2018 Week 3 < 0.0005 / mg/L < 0.000356 / lbs/day
Sep 2018 Week 4 < 0.00008 / mg/L < 0.000052 / lbs/day
Jul 2018 Average < 0.0005 / mg/L < 0.000356 / lbs/day
Sep 2018 Average < 0.00008 / mg/L < 0.000052 / lbs/day
2018 Quarter 3 < 0.00029 / mg/L 0.000204 / lbs/day
2018 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000204 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.000356 / lbs/day
2018 2nd 6...(Min) < 0.00008 / mg/L < 0.000052 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/17/2018 S Biogen071718Self 114 / mg/L 81.271 / lbs/day
09/25/2018 P Biogen092518POTW 149 / mg/L 103.1159 / lbs/day
Jul 2018 Week 3 114 / mg/L 81.271 / lbs/day
Sep 2018 Week 4 149 / mg/L 103.1159 / lbs/day
Jul2018 Average 114 / mg/L 81.271 / lbs/day
Sep 2018 Average 149 / mg/L 103.1159 / lbs/day
2018 Quarter 3 131.5 / mg/L 92.1934 / lbs/day
2018 2nd 6 Months(Avg) 131.5 / mg/L 92.1934 / lbs/day
2018 2nd 6...(Max) 149 / mg/L 103.1159 / lbs/day
2018 2nd 6...(Min) 114 / mg/L 81.2710 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/17/2018 S Biogen071718Self 32 / mg/L 22.81 / lbs/day
09/25/2018 P Biogen092518POTW 77 / mg/L 53.29 / lbs/day
Jul2018 Week 3 32 / mg/L 22.81 / lbs/day
Sep 2018 Week 4 77 / mg/L 53.29 / lbs/day
Jul 2018 Average 32 / mg/L 22.81 / lbs/day
Sep 2018 Average 77 / mg/L 53.29 / lbs/day
2018 Quarter 3 54.5 / mg/L 38.05 / lbs/day
2018 2nd 6 Months(Avg) 54.5 / mg/L 38.05 / lbs/day
2018 2nd 6...(Max) 77 / mg/L 53.29 / lbs/day
2018 2nd 6...(Min) 32 / mg/L 22.81 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
09/25/2018 P Biogen092518POTW < 0.005 / 12.19 mg/L < 0.0035 / lbs/day
Sep 2018 Week 4 < 0.005 / mg/L < 0.0035 / lbs/day
Sep 2018 Average < 0.005 /4.83 mg/L < 0.0035 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/17/2018 S Biogen071718Self 1 / mg/L 0.7129 / lbs/day
09/25/2018 P Biogen092518POTW 0.14 / mg/L 0.0969 / lbs/day
Jul 2018 Week 3 1 / mg/L 0.7129 / lbs/day
Sep 2018 Week 4 0.14 / mg/L 0.0969 / lbs/day
Jul2018 Average 1 / mg/L 0.7129 / lbs/day
Sep 2018 Average 0.14 / mg/L 0.0969 / lbs/day
2018 Quarter 3 0.57 / mg/L 0.4049 / lbs/day
2018 2nd 6 Months(Avg) 0.57 / mg/L 0.4049 / lbs/day
2018 2nd 6...(Max) 1 / mg/L 0.7129 / lbs/day
2018 2nd 6...(Min) 0.14 / mg/L 0.0969 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
09/25/2018 P Biogen092518POTW < 0.005 / 12.19 mg/L < 0.0035 / lbs/day
Sep 2018 Week 4 < 0.005 / mg/L < 0.0035 / lbs/day
Sep 2018 Average < 0.005 /4.83 mg/L < 0.0035 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # "A)
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/16/2018 S Biogen071618SeIflg 0.000014 /0.000142 mg/L /
09/24/2018 P Biogen092418POTWH 0.00001 /0.000142 mg/L /
g
12/03/2018 P Biogen120318POTWH 0.000011 /0.000142 mg/L /
g
Jul 2018 Week 3 0.000014 / mg/L /
Sep 2018 Week 4 0.00001 / mg/L /
Dec 2018 Week 1 0.000011 / mg/L /
Jul 2018 Average 0.000014 / mg/L /
Sep 2018 Average 0.00001 / mg/L /
Dec 2018 Average 0.000011 / mg/L /
2018 Quarter 3 0.000012 / mg/L /
2018 Quarter 4 0.000011 / mg/L /
2018 2nd 6 Months(Avg) 0.000012 / mg/L /
2018 2nd 6...(Max) 0.000014 / mg/L /
2018 2nd 6...(Min) 0.00001 / mg/L /
2018 2nd 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 3 Weeks Sampled : 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methyl Chloride
09/25/2018 P Biogen092518POTW < 0.005 / mg/L < 0.00346 / lbs/day .
Sep 2018 Week 4 < 0.005 / mg/L < 0.00346 / lbs/day
Sep 2018 Average < 0.005 / mg/L < 0.00346 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.00346 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.003460 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.003460 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.003460 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methyl Chloride
2018 2nd 6...(Count) I / I /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
09/25/2018 P Biogen092518POTW < 0.005 / 12.19 mg/L < 0.0035 / lbs/day
Sep 2018 Week 4 < 0.005 / mg/L < 0.0035 / lbs/day
Sep 2018 Average < 0.005 /4.83 mg/L < 0.0035 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.0035 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/17/2018 S Biogen071718Self 5.1 / mg/L 3.636 / lbs/day
09/25/2018 P Biogen092518POTW 3.56 / mg/L 2.464 / lbs/day
Jul2018 Week 3 5.1 / mg/L 3.636 / lbs/day
Sep 2018 Week 4 3.56 / mg/L 2.464 / lbs/day
Jul 2018 Average 5.1 / mg/L 3.636 / lbs/day
Sep 2018 Average 3.56 / mg/L 2.464 / lbs/day
2018 Quarter 3 4.33 / mg/L 3.05 / lbs/day
2018 2nd 6 Months(Avg) 4.33 / mg/L 3.050 / lbs/day
2018 2nd 6...(Max) 5.1 / mg/L 3.636 / lbs/day
2018 2nd 6...(Min) 3.56 / mg/L 2.464 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil &Grease,Total
07/17/2018 S Biogen071718Self < 2.5 /200 mg/L < /
09/25/2018 P Biogen092518POTW 6 /200 mg/L /
Jul 2018 Week 3 < 2.5 / mg/L < /
Sep 2018 Week 4 6 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
Jul2018 Average < 2.5 / mg/L < /
Sep 2018 Average 6 / mg/L /
2018 Quarter 3 < 4.25 / mg/L < /
2018 2nd 6 Months(Avg) < 4.25 / mg/L < /
2018 2nd 6...(Max) 6 / mg/L /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/17/2018 S Biogen071718Se1f 7.2 /5.5- 10.5 SU /
09/25/2018 P Biogen092518POTW 8.3 /5.5- 10.5 SU /
Jul 2018 Week 3 7.2 / SU /
Sep 2018 Week 4 8.3 / SU /
Jul2018 Average 7.2 / SU /
Sep 2018 Average 8.3 / SU /
2018 Quarter 3 7.75 / SU /
2018 2nd 6 Months(Avg) 7.75 / SU /
2018 2nd 6...(Max) 8.3 / SU /
2018 2nd 6...(Min) 7.2 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/25/2018 P Biogen092518POTW 25 /66 °C /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Sep 2018 Week 4 25 / °C /
Sep 2018 Average 25 / °C /
2018 Quarter 3 25 / °C /
2018 2nd 6 Months(Avg) 25 / °C /
2018 2nd 6...(Max) 25 / °C /
2018 2nd 6...(Min) 25 / °C /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/17/2018 S Biogen071718Self 0.95 / mg/L 0.6773 / lbs/day
09/25/2018 P Biogen092518POTW 0.932 / mg/L 0.645 / lbs/day
Jul 2018 Week 3 0.95 / mg/L 0.6773 / lbs/day
Sep 2018 Week 4 0.932 / mg/L 0.645 / lbs/day
Jul 2018 Average 0.95 / mg/L 0.6773 / lbs/day
Sep 2018 Average 0.932 / mg/L 0.645 / lbs/day
2018 Quarter 3 0.941 / mg/L 0.6611 / lbs/day
2018 2nd 6 Months(Avg) 0.941 / mg/L 0.6611 / lbs/day
2018 2nd 6...(Max) 0.95 / mg/L 0.6773 / lbs/day
2018 2nd 6...(Min) 0.932 / mg/L 0.6450 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/17/2018 S Biogen071718Self 9.1 / mg/L 6.487419 / lbs/day
09/25/2018 P Biogen092518POTW 28 / mg/L 19.37749 / lbs/day
Jul2018 Week 3 9.1 / mg/L 6.487419 / lbs/day
Sep 2018 Week 4 28 / mg/L 19.37749 / lbs/day
Jul 2018 Average 9.1 / mg/L 6.487419 / lbs/day
Sep 2018 Average 28 / mg/L 19.37749 / lbs/day
2018 Quarter 3 18.6 / mg/L 12.932454 / lbs/day
2018 2nd 6 Months(Avg) 18.6 / mg/L 12.9325 / lbs/day
2018 2nd 6...(Max) 28 / mg/L 19.377490 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 9

Biogen
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2018 2nd 6...(Min) 9.1 / mg/L 6.487419 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
07/17/2018 S Biogen071718Self < 0.001 / mg/L < /
Jul 2018 Week 3 < 0.001 / mg/L < /
Jul2018 Average < 0.001 / mg/L < /
2018 Quarter 3 < 0.001 / mg/L < /
2018 2nd 6 Months(Avg) < 0.001 / mg/L < /
2018 2nd 6...(Max) < 0.001 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/17/2018 S Biogen071718Self 0.082 / mg/L 0.058458 / lbs/day
09/25/2018 P Biogen092518POTW 0.124 / mg/L 0.085815 / lbs/day
Jul 2018 Week 3 0.082 / mg/L 0.058458 / lbs/day
Sep 2018 Week 4 0.124 / mg/L 0.085815 / lbs/day
Jul 2018 Average 0.082 / mg/L 0.058458 / lbs/day
Sep 2018 Average 0.124 / mg/L 0.085815 / lbs/day
2018 Quarter 3 0.103 / mg/L 0.072136 / lbs/day
2018 2nd 6 Months(Avg) 0.103 / mg/L 0.072136 / lbs/day
2018 2nd 6...(Max) 0.124 / mg/L 0.085815 / lbs/day
2018 2nd 6...(Min) 0.082 / mg/L 0.058458 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sam leID Result/Limit Mass/Limit
P P
Acetone
07/12/2018 P Braeburn071218POT < 0.005 / 13.1 mg/L < /
W
Jul 2018 Week 2 < 0.005 / mg/L < /
Jul 2018 Average < 0.005 /5.1 mg/L < /
2018 Quarter 3 < 0.005 / mg/L < /
2018 2nd 6 Months(Avg) < 0.005 / mg/L < /
2018 2nd 6...(Max) < 0.005 / mg/L < /
2018 2nd 6...(Min) < 0.005 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/18/2018 S Braeburn0718F1ow 0.000235 / MGD /
08/23/2018 S Braeburn0818Flow 0.000238 / MGD /
09/20/2018 S Braeburn0918Flow 0.000255 / MGD /
10/08/2018 S Braeburn 100818Flow 0.000186 / MGD /
Jul2018 Week 3 0.000235 / MGD /
Aug 2018 Week 4 0.000238 / MGD /
Sep 2018 Week 3 0.000255 / MGD /
Oct 2018 Week 2 0.000186 / MGD /
Jul 2018 Average 0.000235 0.010 MGD/ /
Aug 2018 Average 0.000238 /0.010 MGD /
Sep 2018 Average 0.000255 /0.010 MGD /
Oct 2018 Average 0.000186 /0.010 MGD /
2018 Quarter 3 0.000243 / MGD /
2018 Quarter 4 0.000186 / MGD /
2018 2nd 6 Months(Avg) 0.000228 / MGD /
2018 2nd 6...(Max) 0.000255 / MGD /
2018 2nd 6...(Min) 0.000186 / MGD /
2018 2nd 6...(Count) 4 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 4

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Count: 4 Months Sampled: 4 Weeks Sampled: 4 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
' #Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
09/25/2018 P Braeburn092518POT < 0.00008 / mg/L < /
W
Sep 2018 Week 4 < 0.00008 / mg/L < /
Sep 2018 Average < 0.00008 / mg/L < /
2018 Quarter 3 < 0.00008 / mg/L < /
2018 2nd 6 Months(Avg) < 0.00008 / mg/L < /
2018 2nd 6...(Max) < 0.00008 / mg/L < /
2018 2nd 6...(Min) < 0.00008 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
09/25/2018 P Braeburn092518POT < 7.5 / mg/L < /
W
Sep 2018 Week 4 < 7.5 / mg/L < /
Sep 2018 Average < 7.5 / mg/L < /
2018 Quarter 3 < 7.5 / mg/L < /
2018 2nd 6 Months(Avg) < 7.5 / mg/L < /
2018 2nd 6...(Max) < 7.5 / mg/L < /
2018 2nd 6...(Min) < 7.5 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
09/24/2018 P Braebum092418POT 0.000007 /0.000142 mg/L /
WHg
Sep 2018 Week 4 0.000007 / mg/L /
Sep 2018 Average 0.000007 / mg/L /
2018 Quarter 3 0.000007 / mg/L /
2018 2nd 6 Months(Avg) 0.000007 / mg/L /
2018 2nd 6...(Max) 0.000007 / mg/L /
2018 2nd 6...(Min) 0.000007 / mg/L /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 4

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
' #Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
09/25/2018 P Braeburn092518POT 3.7 /6- 10 SU * /
W
09/28/2018 P Braeburn092818POT 7.1 /6- 10 SU /
W
Sep 2018 Week 4 5.4 / SU /
Sep 2018 Average 5.4 / SU /
2018 Quarter 3 5.4 / SU /
2018 2nd 6 Months(Avg) 5.4 / SU /
2018 2nd 6...(Max) 7.1 / SU /
2018 2nd 6...(Min) 3.7 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % - # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 1 50.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/25/2018 P Braebum092518POT 25 /66 °C /
W
09/28/2018 P Braeburn092818POT 26 /66 °C /
W
Sep 2018 Week 4 25.5 / °C /
Sep 2018 Average 25.5 / °C /
2018 Quarter 3 25.5 / °C /
2018 2nd 6 Months(Avg) 25.5 / °C /
2018 2nd 6...(Max) 26 / °C /
2018 2nd 6...(Min) 25 / °C /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 4

Braeburn Pharmaceuticals, Inc.
SAMPLE OVERVIEW
771/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : l
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
09/25/2018 P Braebum092518POT 0.01 / mg/L /
W
Sep 2018 Week 4 0.01 / mg/L /
Sep 2018 Average 0.01 / mg/L /
2018 Quarter 3 0.01 / mg/L /
2018 2nd 6 Months(Avg) 0.01 / mg/L /
2018 2nd 6...(Max) 0.01 / mg/L /
2018 2nd 6...(Min) 0.01 / mg/L /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 4

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/14/2018 S Cintas081418Se1f 2.4 / mg/L 1.393154 / lbs/day
Aug 2018 Week 2 2.4 / mg/L 1.393154 / lbs/day
Aug 2018 Average 2.4 / mg/L 1.393154 / lbs/day
2018 Quarter 3 2.4 / mg/L 1.393154 / lbs/day
2018 2nd 6 Months(Avg) 2.4 / mg/L 1.39315 / lbs/day
2018 2nd 6...(Max) 2.4 / mg/L 1.393154 / lbs/day
2018 2nd 6...(Min) 2.4 / mg/L 1.393154 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/17/2018 S Cintas071718Self 14.1 / mg/L 7.2892 / lbs/day
07/31/2018 P Cintas073118POTW 25.4 / mg/L 14.3385 / lbs/day
08/14/2018 S Cintas081418Self 27.3 / mg/L 15.8471 / lbs/day
09/25/2018 S Cintas092518Self 43.9 / mg/L 23.1794 / lbs/day
10/09/2018 S Cintas100918Self 26 / mg/L 14.7304 / lbs/day
11/09/2018 S Cintasl10918Self 3.3 / mg/L 2.1892 / lbs/day
12/14/2018 S Cintas121418Self 12.6 / mg/L 9.6383 / lbs/day
Jul 2018 Week 3 14.1 / mg/L 7.2892 / lbs/day
Jul 2018 Week 4 25.4 / mg/L 14.3385 / lbs/day
Aug 2018 Week 2 27.3 / mg/L 15.8471 / lbs/day
Sep 2018 Week 4 43.9 / mg/L 23.1794 / lbs/day
Oct 2018 Week 2 26 / mg/L 14.7304 / lbs/day
Nov 2018 Week 2 3.3 / mg/L 2.1892 / lbs/day
Dec 2018 Week 2 12.6 / mg/L 9.6383 / lbs/day
Jul2018 Average 19.75 / mg/L 10.8139 / lbs/day
Aug 2018 Average 27.3 / mg/L 15.8471 / lbs/day
Sep 2018 Average 43.9 / mg/L 23.1794 / lbs/day
Oct 2018 Average 26 / mg/L 14.7304 / lbs/day
Nov 2018 Average 3.3 / mg/L 2.1892 / lbs/day
Dec 2018 Average 12.6 / mg/L 9.6383 / lbs/day
2018 Quarter 3 27.68 / mg/L 15.1636 / lbs/day
2018 Quarter 4 13.97 / mg/L 8.8526 / lbs/day
2018 2nd 6 Months(Avg) 21.8 / mg/L 12.4589 / lbs/day
2018 2nd 6...(Max) 43.9 / mg/L 23.1794 / lbs/day
2018 2nd 6...(Min) 3.3 / mg/L 2.1892 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Cintas0718Flow 0.058131 /0.180 MGD /
08/31/2018 S Cintas0818Flow 0.060812 /0.180 MGD /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfull: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
09/30/2018 S Cintas0918Flow 0.057218 /0.180 MGD /
10/31/2018 S Cintas1018Flow 0.057663 /0.180 MGD /
11/30/2018 S Cintas1118Flow 0.060599 /0.180 MGD /
12/31/2018 S Cintas1218Flow 0.061729 /0.180 MGD /
Jul 2018 Week 4 0.058131 / MGD /
Aug 2018 Week 4 0.060812 / MGD /
Sep 2018 Week 4 0.057218 / MGD /
Oct 2018 Week 4 0.057663 / MGD /
Nov 2018 Week 4 0.060599 / MGD /
Dec 2018 Week 4 0.061729 / MGD /
Jul2018 Average 0.058131 /0.120 MGD /
Aug 2018 Average 0.060812 /0.120 MGD /
Sep 2018 Average 0.057218 /0.120 MGD /
Oct 2018 Average 0.057663 /0.120 MGD /
Nov 2018 Average 0.060599 /0.120 MGD /
Dec 2018 Average 0.061729 /0.120 MGD /
2018 Quarter 3 0.05872 / MGD /
2018 Quarter 4 0.059997 / MGD /
2018 2nd 6 Months(Avg) 0.059359 / MGD /
2018 2nd 6...(Max) 0.061729 / MGD /
2018 2nd 6...(Min) 0.057218 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/17/2018 S Cintas071718Self 246 / mg/L 127.173 / lbs/day
07/31/2018 P Cintas073118POTW 325 / mg/L 183.466 / lbs/day
08/14/2018 S Cintas081418Self 403 / mg/L 233.934 / lbs/day
08/28/2018 P Cintas082818POTW 407 / mg/L /
09/21/2018 P Cintas092118POTW 633 / mg/L /
09/25/2018 S Cintas092518Self 177 / mg/L 93.457 / lbs/day
10/09/2018 S Cintas100918Self 168 / mg/L 95.181 / lbs/day
10/23/2018 P Cintas102318POTW 461 / mg/L /
11/09/2018 S Cintas110918Self 157 / mg/L 104.155 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
11/15/2018 P Cintas111518POTW 357 / mg/L /
12/06/2018 P Cintas120618POTW 317 / mg/L /
12/14/2018 S Cintas121418Self 280 / mg/L 214.185 / lbs/day
Jul 2018 Week 3 246 / mg/L 127.173 / lbs/day
Jul 2018 Week 4 325 / mg/L 183.466 / lbs/day
Aug 2018 Week 2 403 / mg/L 233.934 / lbs/day
Aug 2018 Week 4 407 / mg/L /
Sep 2018 Week 3 633 / mg/L /
Sep 2018 Week 4 177 / mg/L 93.457 / lbs/day
Oct 2018 Week 2 168 / mg/L 95.181 / lbs/day
Nov 2018 Week 2 157 / mg/L 104.155 / lbs/day
Oct 2018 Week 4 461 / mg/L /
Nov 2018 Week 3 357 / mg/L /
Dec 2018 Week 1 317 / mg/L /
Dec 2018 Week 2 280 / mg/L 214.185 / lbs/day
Jul2018 Average 285.5 / mg/L 155.319 / lbs/day
Aug 2018 Average 405 / mg/L 233.934 / lbs/day
Sep 2018 Average 405 / mg/L 93.457 / lbs/day
Oct 2018 Average 314.5 / mg/L 95.181 / lbs/day
Nov 2018 Average 257 / mg/L 104.155 / lbs/day
Dec 2018 Average 298.5 / mg/L 214.185 / lbs/day
2018 Quarter 3 365.2 / mg/L 159.507 / lbs/day
2018 Quarter 4 290 / mg/L 137.84 / lbs/day
2018 2nd 6 Months(Avg) 327.6 / mg/L 150.221 / lbs/day
2018 2nd 6...(Max) 633 / mg/L 233.934 / lbs/day
2018 2nd 6...(Min) 157 / mg/L /
2018 2nd 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/14/2018 S Cintas081418Self 0.0014 / mg/L 0.000813 / lbs/day
Aug 2018 Week 2 0.0014 / mg/L 0.000813 / lbs/day
Aug 2018 Average 0.0014 / mg/L 0.000813 / lbs/day
2018 Quarter 3 0.0014 / mg/L 0.000813 / lbs/day
2018 2nd 6 Months(Avg) 0.0014 / mg/L 0.000813 / lbs/day
2018 2nd 6...(Max) 0.0014 / mg/L 0.000813 / lbs/day
2018 2nd 6...(Min) 0.0014 / mg/L 0.000813 / lbs/day
2018 2nd 6...(Count) 1 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/31/2018 P Cintas073118POTW 107 / mg/L 60.4025 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/14/2018 S Cintas081418Self 134 / mg/L 77.7844 / lbs/day
Jul 2018 Week 4 107 / mg/L 60.4025 / lbs/day
Aug 2018 Week 2 134 / mg/L 77.7844 / lbs/day
Jul2018 Average 107 / mg/L 60.4025 / lbs/day
Aug 2018 Average 134 / mg/L 77.7844 / lbs/day
2018 Quarter 3 120.5 / mg/L 69.0935 / lbs/day
2018 2nd 6 Months(Avg) 120.5 / mg/L 69.0935 / lbs/day
2018 2nd 6...(Max) 134 / mg/L 77.7844 / lbs/day
2018 2nd 6...(Min) 107 / mg/L 60.4025 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
07/17/2018 S Cintas071718Self 0.005 / mg/L 0.00274 / lbs/day
08/14/2018 S Cintas081418Self 0.02 / mg/L 0.01161 / lbs/day
09/25/2018 S Cintas092518Se1f 0.005 / mg/L 0.002746 / lbs/day
10/09/2018 S Cintas100918Se1f 0.01 / mg/L 0.005382 / lbs/day
11/09/2018 S Cintas110918Self 0.017 / mg/L 0.011145 / lbs/day
12/14/2018 S Cintas121418Se1f 0.013 / mg/L 0.009868 / lbs/day
Jul 2018 Week 3 0.005 / mg/L 0.00274 / lbs/day
Aug 2018 Week 2 0.02 / mg/L 0.01161 / lbs/day
Sep 2018 Week 4 0.005 / mg/L 0.002746 / lbs/day
Oct 2018 Week 2 0.01 / mg/L 0.005382 / lbs/day
Nov 2018 Week 2 0.017 / mg/L 0.011145 / lbs/day
Dec 2018 Week 2 0.013 / mg/L 0.009868 / lbs/day
Jul 2018 Average 0.005 / mg/L 0.00274 / lbs/day
Aug 2018 Average 0.02 / mg/L 0.01161 / lbs/day
Sep 2018 Average 0.005 / mg/L 0.002746 / lbs/day
Oct 2018 Average 0.01 / mg/L 0.005382 / lbs/day
Nov 2018 Average 0.017 / mg/L 0.011145 / lbs/day
Dec 2018 Average 0.013 / mg/L 0.009868 / lbs/day
2018 Quarter 3 0.01 / mg/L 0.005698 / lbs/day
2018 Quarter 4 0.013 / mg/L 0.008798 / lbs/day
2018 2nd 6 Months(Avg) 0.012 / mg/L 0.007248 / lbs/day
2018 2nd 6...(Max) 0.02 / mg/L 0.011610 / lbs/day
2018 2nd 6...(Min) 0.005 / mg/L 0.002740 / lbs/day
2018 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/17/2018 S Cintas071718Self 0.068 / mg/L 0.03536 / lbs/day
08/14/2018 S Cintas081418Self 0.122 / mg/L 0.070819 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
1 09/25/2018 S Cintas092518Self 0.045 / mg/L 0.023866 / lbs/day
10/09/2018 S Cintas100918Self 0.09 / mg/L 0.050763 / lbs/day
11/09/2018 S Cintas110918Self 0.124 / mg/L 0.082262 / lbs/day
12/14/2018 S Cintas121418Self 0.094 / mg/L 0.071828 / lbs/day
Jul 2018 Week 3 0.068 / mg/L 0.03536 / lbs/day
Aug 2018 Week 2 0.122 / mg/L 0.070819 / lbs/day
Sep 2018 Week 4 0.045 / mg/L 0.023866 / lbs/day
Oct 2018 Week 2 0.09 / mg/L 0.050763 / lbs/day
Nov 2018 Week 2 0.124 / mg/L 0.082262 / lbs/day
Dec 2018 Week 2 0.094 / mg/L 0.071828 / lbs/day
Jul 2018 Average 0.068 / mg/L 0.03536 / lbs/day
Aug 2018 Average 0.122 / mg/L 0.070819 / lbs/day
Sep 2018 Average 0.045 / mg/L 0.023866 / lbs/day
Oct 2018 Average 0.09 / mg/L 0.050763 / lbs/day
Nov 2018 Average 0.124 / mg/L 0.082262 / lbs/day
Dec 2018 Average 0.094 / mg/L 0.071828 / lbs/day
2018 Quarter 3 0.079 / mg/L 0.043348 / lbs/day
2018 Quarter 4 0.103 / mg/L 0.068285 / lbs/day
2018 2nd 6 Months(Avg) 0.091 / mg/L 0.055816 / lbs/day
2018 2nd 6...(Max) 0.124 / mg/L 0.082262 / lbs/day
2018 2nd 6...(Min) 0.045 / mg/L 0.023866 / lbs/day
2018 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/17/2018 S Cintas071718Self 0.36 / mg/L 0.1861 / lbs/day
07/31/2018 P Cintas073118POTW 0.14 / mg/L 0.079 / lbs/day
08/14/2018 S Cintas081418Self < 0.05 / mg/L < 0.029 / lbs/day
09/25/2018 S Cintas092518Self < 0.05 / mg/L < 0.0264 / lbs/day
10/09/2018 S Cintas100918Self 0.15 / mg/L 0.085 / lbs/day
11/09/2018 S Cintas110918Self < 0.05 / mg/L < 0.0332 / lbs/day
12/14/2018 S Cintas121418Self 0.13 / mg/L 0.0994 / lbs/day
Jul2018 Week 3 0.36 / mg/L 0.1861 / lbs/day
Jul2018 Week 4 0.14 / mg/L 0.079 / lbs/day
Aug 2018 Week 2 < 0.05 / mg/L < 0.029 / lbs/day
Sep 2018 Week 4 < 0.05 / mg/L < 0.0264 / lbs/day
Oct 2018 Week 2 0.15 / mg/L 0.085 / lbs/day
Nov 2018 Week 2 < 0.05 / mg/L < 0.0332 / lbs/day
Dec 2018 Week 2 0.13 / mg/L 0.0994 / lbs/day
Jul2018 Average 0.25 / mg/L 0.1326 / lbs/day
Aug 2018 Average < 0.05 / mg/L < 0.029 / lbs/day
Sep 2018 Average < 0.05 / mg/L < 0.0264 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Oct 2018 Average 0.15 / mg/L 0.085 / lbs/day
Nov 2018 Average < 0.05 / mg/L < 0.0332 / lbs/day
Dec 2018 Average 0.13 / mg/L 0.0994 / lbs/day
2018 Quarter 3 < 0.15 / mg/L < 0.0801 / lbs/day
2018 Quarter 4 < 0.11 / mg/L < 0.0725 / lbs/day
2018 2nd 6 Months(Avg) < 0.13 / mg/L < 0.0769 / lbs/day
2018 2nd 6...(Max) 0.36 / mg/L 0.1861 / lbs/day
2018 2nd 6...(Min) < 0.05 / mg/L < 0.0264 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/17/2018 S Cintas071718Self 0.0177 / mg/L 0.00915 / lbs/day
08/14/2018 S Cintas081418Self 0.0243 / mg/L 0.014106 / lbs/day
09/25/2018 S Cintas092518Self 0.0073 / mg/L 0.003854 / lbs/day
10/09/2018 S Cintas100918Self 0.0153 / mg/L 0.008668 / lbs/day
11/09/2018 S Cintas110918Self 0.026 / mg/L 0.017249 / lbs/day
12/14/2018 S Cintas121418Self 0.0215 / mg/L 0.016446 / lbs/day
Jul 2018 Week 3 0.0177 / mg/L 0.00915 / lbs/day
Aug 2018 Week 2 0.0243 / mg/L 0.014106 / lbs/day
Sep 2018 Week 4 0.0073 / mg/L 0.003854 / lbs/day
Oct 2018 Week 2 0.0153 / mg/L 0.008668 / lbs/day
Nov 2018 Week 2 0.026 / mg/L 0.017249 / lbs/day
Dec 2018 Week 2 0.0215 / mg/L 0.016446 / lbs/day
Jul 2018 Average 0.0177 / mg/L 0.00915 / lbs/day
Aug 2018 Average 0.0243 / mg/L 0.014106 / lbs/day
Sep 2018 Average 0.0073 / mg/L 0.003854 / lbs/day
Oct 2018 Average 0.0153 / mg/L 0.008668 / lbs/day
1 Nov 2018 Average 0.026 / mg/L 0.017249 / lbs/day
Dec 2018 Average 0.0215 / mg/L 0.016446 / lbs/day
2018 Quarter 3 0.0164 / mg/L 0.009037 / lbs/day
2018 Quarter 4 0.0209 / mg/L 0.014121 / lbs/day
2018 2nd 6 Months(Avg) 0.0187 / mg/L 0.011579 / lbs/day
2018 2nd 6...(Max) 0.026 / mg/L 0.017249 / lbs/day
2018 2nd 6...(Min) 0.0073 / mg/L 0.003854 / lbs/day
2018 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/20/2018 S Cintas072018SelfHg 0.000146 /0.000142 mg/L * /
07/30/2018 P Cintas073018POTWH 0.000084 /0.000142 mg/L /
g
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/09/2018 S Cintas080918SelfHg 0.000005 /0.000142 mg/L /
08/14/2018 S Cintas081418Se1fHg 0.000006 /0.000142 mg/L /
Jul 2018 Week 3 0.000146 / mg/L /
Jul 2018 Week 4 0.000084 / mg/L /
Aug 2018 Week 2 0.000006 / mg/L /
Jul2018 Average 0.000115 / mg/L /
Aug 2018 Average 0.000006 / mg/L /
2018 Quarter 3 0.00006 / mg/L /
2018 2nd 6 Months(Avg) 0.000060 / mg/L /
2018 2nd 6...(Max) 0.000146 / mg/L /
2018 2nd 6...(Min) 0.000005 / mg/L /
2018 2nd 6...(Count) 4 / /
Sample Count: 4 Months Sampled: 2 Weeks Sampled : 3 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: I 25.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/14/2018 S Cintas081418Self 0 / mg/L 0.0203 / lbs/day
Aug 2018 Week 2 0 / mg/L 0.0203 / lbs/day
Aug 2018 Average 0 / mg/L 0.0203 / lbs/day
2018 Quarter 3 0 / mg/L 0.0203 / lbs/day
2018 2nd 6 Months(Avg) 0.035 / mg/L 0.0203 / lbs/day
2018 2nd 6...(Max) 0.035 / mg/L 0.0203 / lbs/day
2018 2nd 6...(Min) 0.035 / mg/L 0.0203 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/17/2018 S Cintas071718Self 0.0212 / mg/L 0.01096 / lbs/day
08/14/2018 S Cintas081418Self 0.0313 / mg/L 0.018169 / lbs/day
09/25/2018 S Cintas092518Self 0.0202 / mg/L 0.010666 / lbs/day
10/09/2018 S Cintas100918Self 0.0341 / mg/L 0.019319 / lbs/day
11/09/2018 S Cintas110918Self 0.0287 / mg/L 0.01904 / lbs/day
12/14/2018 S Cintas121418Self 0.0222 / mg/L 0.016982 / lbs/day
Jul2018 Week 3 0.0212 / mg/L 0.01096 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Aug 2018 Week 2 0.0313 / mg/L 0.018169 / lbs/day
Sep 2018 Week 4 0.0202 / mg/L 0.010666 / lbs/day
Oct 2018 Week 2 0.0341 / mg/L 0.019319 / lbs/day
Nov 2018 Week 2 0.0287 / mg/L 0.01904 / lbs/day
Dec 2018 Week 2 0.0222 / mg/L 0.016982 / lbs/day
Jul2018 Average 0.0212 / mg/L 0.01096 / lbs/day
Aug 2018 Average 0.0313 / mg/L 0.018169 / lbs/day
Sep 2018 Average 0.0202 / mg/L 0.010666 / lbs/day
Oct 2018 Average 0.0341 / mg/L 0.019319 / lbs/day
Nov 2018 Average 0.0287 / mg/L 0.01904 / lbs/day
Dec 2018 Average 0.0222 / mg/L 0.016982 / lbs/day
2018 Quarter 3 0.0242 / mg/L 0.013265 / lbs/day
2018 Quarter 4 0.0283 / mg/L 0.018447 / lbs/day
2018 2nd 6 Months(Avg) 0.0263 / mg/L 0.015856 / lbs/day
2018 2nd 6...(Max) 0.0341 / mg/L 0.019319 / lbs/day
2018 2nd 6...(Min) 0.0202 / mg/L 0.010666 / lbs/day
2018 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/17/2018 S Cintas071718Self < 0.1 / mg/L < 0.026 / lbs/day
07/31/2018 P Cintas073118POTW < 0.1 / mg/L < 0.028 / lbs/day
08/14/2018 S Cintas081418Self < 0.1 / mg/L < 0.029 / lbs/day
09/25/2018 S Cintas092518Se1f < 0.1 / mg/L < 0.026 / lbs/day
10/09/2018 S Cintas100918Self < 0.1 / mg/L < 0.028 / lbs/day
11/09/2018 S Cintas110918Self < 0.1 / mg/L < 0.033 / lbs/day
12/14/2018 S Cintas121418Self < 0.1 / mg/L < 0.038 / lbs/day
Jul 2018 Week 3 < 0.1 / mg/L < 0.026 / lbs/day
Jul 2018 Week 4 < 0.1 / mg/L < 0.028 / lbs/day
Aug 2018 Week 2 < 0.1 / mg/L < 0.029 / lbs/day
Sep 2018 Week 4 < 0.1 / mg/L < 0.026 / lbs/day
Oct 2018 Week 2 < 0.1 / mg/L < 0.028 / lbs/day
Nov 2018 Week 2 < 0.1 / mg/L < 0.033 / lbs/day
Dec 2018 Week 2 < 0.1 / mg/L < 0.038 / lbs/day
Jul 2018 Average < 0.1 / mg/L < 0.027 / lbs/day
Aug 2018 Average < 0.1 / mg/L < 0.029 / lbs/day
Sep 2018 Average < 0.1 / mg/L < 0.026 / lbs/day
Oct 2018 Average < 0.1 / mg/L < 0.028 / lbs/day
Nov 2018 Average < 0.1 / mg/L < 0.033 / lbs/day
Dec 2018 Average < 0.1 / mg/L < 0.038 / lbs/day
2018 Quarter 3 < 0.1 / mg/L < 0.027 / lbs/day
2018 Quarter 4 < 0.1 / mg/L < 0.033 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2018 2nd 6 Months(Avg) < 0.1 / mg/L < 0.030 / lbs/day
2018 2nd 6...(Max) < 0.1 / mg/L < 0.038 / lbs/day
2018 2nd 6...(Min) < 0.1 / mg/L < 0.026 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total l
29.7mg/L15.354 / lbs/day
S Cintas071718Self /
07/31/2018 P Cintas073118POTW 43.7 / mg/L 24.669 / lbs/day
08/14/2018 S Cintas081418Self 55.2 / mg/L 32.043 / lbs/day
09/25/2018 S Cintas092518Self 69.7 / mg/L 36.802 / lbs/day
10/09/2018 S Cintas100918Se1f 67.3 / mg/L 38.129 / lbs/day
11/09/2018 S Cintas110918Self 15.1 / mg/L 10.017 / lbs/day
12/14/2018 S Cintas121418Self 30.3 / mg/L 23.178 / lbs/day
Jul 2018 Week 3 29.7 / mg/L 15.354 / lbs/day
Jul 2018 Week 4 43.7 / mg/L 24.669 / lbs/day
Aug 2018 Week 2 55.2 / mg/L 32.043 / lbs/day
Oct 2018 Week 2 67.3 / mg/L 38.129 / lbs/day
Sep 2018 Week 4 69.7 / mg/L 36.802 / lbs/day
Nov 2018 Week 2 15.1 / mg/L 10.017 / lbs/day
Dec 2018 Week 2 30.3 / mg/L 23.178 / lbs/day
Jul2018 Average 36.7 / mg/L 20.011 / lbs/day
Aug 2018 Average 55.2 / mg/L 32.043 / lbs/day
Sep 2018 Average 69.7 / mg/L 36.802 / lbs/day
Oct 2018 Average 67.3 / mg/L 38.129 / lbs/day
Nov 2018 Average 15.1 / mg/L 10.017 / lbs/day
Dec 2018 Average 30.3 / mg/L 23.178 / lbs/day
2018 Quarter 3 49.58 / mg/L 27.217 / lbs/day
2018 Quarter 4 37.57 / mg/L 23.775 / lbs/day
2018 2nd 6 Months(Avg) 44.43 / mg/L 25.742 / lbs/day
2018 2nd 6...(Max) 69.7 / mg/L 38.129 / lbs/day
2018 2nd 6...(Min) 15.1 / mg/L 10.017 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
07/17/2018 S Cintas071718Self 84.2 / 100 mg/L 43.528305 / lbs/day
07/31/2018 P Cintas073118POTW < 2.5 / 100 mg/L < 1.411274 / lbs/day
08/14/2018 S Cintas081418Self 11.1 / 100 mg/L 6.443336 / lbs/day
09/25/2018 S Cintas092518Self 8.6 / 100 mg/L 4.540846 / lbs/day
10/09/2018 S Cintas1009I8Self 11.2 / 100 mg/L 6.345392 / lbs/day
11/09/2018 S Cintas110918Self 149 / 100 mg/L * * 98.84739 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM (Polar)
12/13/2018 S Cintas121318Self 85.1 / 100 mg/L 65.096802 / lbs/day
12/14/2018 S Cintas121418Self 6.9 / 100 mg/L 5.278119 / lbs/day
Jul 2018 Week 3 84.2 / mg/L 43.528305 / lbs/day
Jul 2018 Week 4 < 2.5 / mg/L < 1.411274 / lbs/day
Aug 2018 Week 2 11.1 / mg/L 6.443336 / lbs/day
Sep 2018 Week 4 8.6 / mg/L 4.540846 / lbs/day
Oct 2018 Week 2 11.2 / mg/L 6.345392 / lbs/day
Nov 2018 Week 2 149 / mg/L 98.84739 / lbs/day
Dec 2018 Week 2 46 / mg/L 35.187461 / lbs/day
Jul 2018 Average < 43.4 / mg/L < 22.469789 / lbs/day
Aug 2018 Average 11.1 / mg/L 6.443336 / lbs/day
Sep 2018 Average 8.6 / mg/L 4.540846 / lbs/day
Oct 2018 Average 11.2 / mg/L 6.345392 / lbs/day
Nov 2018 Average 149 / mg/L 98.84739 / lbs/day
Dec 2018 Average 46 / mg/L 35.187461 / lbs/day
2018 Quarter 3 < 26.6 / mg/L < 13.98094 / lbs/day
2018 Quarter 4 63.1 / mg/L 43.891926 / lbs/day
2018 2nd 6 Months(Avg) < 44.8 / mg/L < 28.9364 / lbs/day
2018 2nd 6...(Max) 149 / mg/L 98.847390 / lbs/day
2018 2nd 6...(Min) < 2.5 / mg/L < 1.411274 / lbs/day
2018 2nd 6...(Count) 8 / 8 /
Sample Count: 8 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 1 12.50 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 1 12.50 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM(Non-Polar)
07/17/2018 S Cintas071718Self 29 / 100 mg/L 14.9919 / lbs/day
07/31/2018 P Cintas073118POTW 9.7 / 100 mg/L 5.4757 / lbs/day
08/14/2018 S Cintas081418Self < 2.4 / 100 mg/L < 1.3932 / lbs/day
09/25/2018 S Cintas092518Self 4.9 / 100 mg/L 2.5872 / lbs/day
10/09/2018 S Cintas100918Self < 2.4 / 100 mg/L < 1.3597 / lbs/day
11/09/2018 S Cintas110918Self 71.2 / 100 mg/L 47.2345 / lbs/day
12/14/2018 S Cintas121418Self < 2.5 / 100 mg/L < 1.9124 / lbs/day
Jul 2018 Week 3 29 / mg/L 14.9919 / lbs/day
Jul 2018 Week 4 9.7 / mg/L 5.4757 / lbs/day
Aug 2018 Week 2 < 2.4 / mg/L < 1.3932 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM(Non-Polar)
Sep 2018 Week 4 4.9 / mg/L 2.5872 / lbs/day
Oct 2018 Week 2 < 2.4 / mg/L < 1.3597 / lbs/day
Nov 2018 Week 2 71.2 / mg/L 47.2345 / lbs/day
Dec 2018 Week 2 < 2.5 / mg/L < 1.9124 / lbs/day
Jul 2018 Average 19.4 / mg/L 10.2338 / lbs/day
Aug 2018 Average < 2.4 / mg/L < 1.3932 / lbs/day
Sep 2018 Average 4.9 / mg/L 2.5872 / lbs/day
Oct 2018 Average < 2.4 / mg/L < 1.3597 / lbs/day
Nov 2018 Average 71.2 / mg/L 47.2345 / lbs/day
Dec 2018 Average < 2.5 / mg/L < 1.9124 / lbs/day
2018 Quarter 3 < 11.5 / mg/L < 6.112 / lbs/day
2018 Quarter 4 < 25.4 / mg/L < 16.8355 / lbs/day
2018 2nd 6 Months(Avg) < 17.4 / mg/L < 10.7078 / lbs/day
2018 2nd 6...(Max) 71.2 / mg/L 47.2345 / lbs/day
2018 2nd 6...(Min) < 2.4 / mg/L < 1.3597 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
' #Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/17/2018 S Cintas071718Self 7.1 /6.0- 10.5 SU /
07/31/2018 P Cintas073118POTW 7.2 /6.0- 10.5 SU /
08/14/2018 S Cintas081418Self 7.5 /6.0- 10.5 SU /
09/25/2018 S Cintas092518Self 7.1 /6.0- 10.5 SU /
10/09/2018 S Cintas100918Self 7.4 /6.0- 10.5 SU /
11/09/2018 S Cintas110918Self 7.3 /6.0- 10.5 SU /
12/14/2018 S Cintas121418Self 8.8 /6.0- 10.5 SU /
Jul 2018 Week 3 7.1 / SU /
Jul 2018 Week 4 7.2 / SU /
Aug 2018 Week 2 7.5 / SU /
Sep 2018 Week 4 7.1 / SU /
Oct 2018 Week 2 7.4 / SU /
Nov 2018 Week 2 7.3 / SU /
Dec 2018 Week 2 8.8 / SU /
Jul 2018 Average 7.15 / SU /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
Aug 2018 Average 7.5 / SU /
Sep 2018 Average 7.1 / SU /
Oct 2018 Average 7.4 / SU /
Nov 2018 Average 7.3 / SU /
Dec 2018 Average 8.8 / SU /
2018 Quarter 3 7.23 / SU /
2018 Quarter 4 7.83 / SU /
2018 2nd 6 Months(Avg) 7.49 / SU /
2018 2nd 6...(Max) 8.8 / SU /
2018 2nd 6...(Min) 7.1 / SU /
2018 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/14/2018 S Cintas081418SeIf < 0.0025 / mg/L < 0.001451 / lbs/day
Aug 2018 Week 2 < 0.0025 / mg/L < 0.001451 / lbs/day
Aug 2018 Average < 0.0025 / mg/L < 0.001451 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.001451 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.001451 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.001451 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.001451 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/17/2018 S Cintas071718Self 38.3 /66 °C /
07/31/2018 P Cintas073118POTW 29 /66 °C /
08/14/2018 S Cintas081418Self 25.8 /66 °C /
09/25/2018 S Cintas092518Self 33.9 /66 °C /
10/09/2018 S Cintas100918Self 36 /66 °C /
11/09/2018 S Cintas110918Self 23.2 /66 °C /
12/14/2018 S Cintas121418Self 29.2 /66 °C /
Jul 2018 Week 3 38.3 / °C /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 12 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Jul 2018 Week 4 29 / °C /
Aug 2018 Week 2 25.8 / °C /
Sep 2018 Week 4 33.9 / °C /
Oct 2018 Week 2 36 / °C /
Nov 2018 Week 2 23.2 / °C /
Dec 2018 Week 2 29.2 / °C /
Jul2018 Average 33.7 / °C /
Aug 2018 Average 25.8 / °C /
Sep 2018 Average 33.9 / °C /
Oct 2018 Average 36 / °C /
Nov 2018 Average 23.2 / °C /
Dec 2018 Average 29.2 / °C /
2018 Quarter 3 31.8 / °C /
2018 Quarter 4 29.5 / °C /
2018 2nd 6 Months(Avg) 30.8 / °C /
2018 2nd 6...(Max) 38.3 / °C /
2018 2nd 6...(Min) 23.2 / °C /
2018 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/17/2018 S Cintas071718Se1f 29.6 / mg/L 15.302 / lbs/day
07/31/2018 P Cintas073118POTW 43.7 / mg/L 24.669 / lbs/day
08/14/2018 S Cintas081418Self 55.1 / mg/L 31.984 / lbs/day
08/28/2018 P Cintas082818POTW 55.6 / mg/L /
09/21/2018 P Cintas092118POTW 20.7 / mg/L /
09/25/2018 S Cintas092518Se1f 69.7 / mg/L 36.802 / lbs/day
10/09/2018 S Cintas100918Self 67.3 / mg/L 38.129 / lbs/day
10/23/2018 P Cintas102318POTW 88 / mg/L /
11/09/2018 S Cintas110918Self 15 / mg/L 9.951 / lbs/day
11/15/2018 P Cintas111518POTW 19 / mg/L /
12/06/2018 P Cintas120618POTW 33 / mg/L /
12/14/2018 S Cintas121418Self 30.3 / mg/L 23.178 / lbs/day
Jul 2018 Week 3 29.6 / mg/L 15.302 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 13 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Ouffall: 001
Sample Date SamplelD Result/Limit Mass/Limit
P P
TKN
Jul 2018 Week 4 43.7 / mg/L 24.669 / lbs/day
Aug 2018 Week 2 55.1 / mg/L 31.984 / lbs/day
Aug 2018 Week 4 55.6 / mg/L /
Sep 2018 Week 3 20.7 / mg/L /
Sep 2018 Week 4 69.7 / mg/L 36.802 / lbs/day
Oct 2018 Week 2 67.3 / mg/L 38.129 / lbs/day
Oct 2018 Week 4 88 / mg/L /
Nov 2018 Week 2 15 / mg/L 9.951 / lbs/day
Nov 2018 Week 3 19 / mg/L /
Dec 2018 Week 1 33 / mg/L /
Dec 2018 Week 2 30.3 / mg/L 23.178 / lbs/day
Jul 2018 Average 36.65 / mg/L 19.986 / lbs/day
Aug 2018 Average 55.35 / mg/L 31.984 / lbs/day
Sep 2018 Average 45.2 / mg/L 36.802 / lbs/day
Oct 2018 Average 77.65 / mg/L 38.129 / lbs/day
Nov 2018 Average 17 / mg/L 9.951 / lbs/day
Dec 2018 Average 31.65 / mg/L 23.178 / lbs/day
2018 Quarter 3 45.73 / mg/L 27.189 / lbs/day
2018 Quarter 4 42.1 / mg/L 23.753 / lbs/day
2018 2nd 6 Months(Avg) 43.92 / mg/L 25.717 / lbs/day
2018 2nd 6...(Max) 88 / mg/L 38.129 / lbs/day
2018 2nd 6...(Min) 15 / mg/L /
2018 2nd 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/17/2018 S Cintas071718Self 2 / mg/L 1.0339 / lbs/day
07/31/2018 P Cintas073118POTW 4.18 / mg/L 2.3597 / lbs/day
08/14/2018 S Cintas081418Self 8.3 / mg/L 4.818 / lbs/day
08/28/2018 P Cintas082818POTW 4.25 / mg/L /
09/21/2018 P Cintas092118POTW 2.56 / mg/L /
09/25/2018 S Cintas092518Se1f 5.3 / mg/L 2.7984 / lbs/day
10/09/2018 S Cintas100918Self 6 / mg/L 3.3993 / lbs/day
10/23/2018 P Cintas102318POTW 6.52 / mg/L /
11/09/2018 S Cintas110918Self 1.8 / mg/L 1.1941 / lbs/day
11/15/2018 P Cintas111518POTW 2.75 / mg/L /
12/06/2018 P Cintas120618POTW 3.27 / mg/L /
12/14/2018 S Cintas121418Self 2.9 / mg/L 2.2183 / lbs/day
Jul 2018 Week 3 2 / mg/L 1.0339 / lbs/day
Jul2018 Week 4 4.18 / mg/L 2.3597 / lbs/day
Aug 2018 Week 2 8.3 / mg/L 4.818 / lbs/day
Aug 2018 Week 4 4.25 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 14 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Sep 2018 Week 3 2.56 / mg/L /
Sep 2018 Week 4 5.3 / mg/L 2.7984 / lbs/day
Oct 2018 Week 2 6 / mg/L 3.3993 / lbs/day
Oct 2018 Week 4 6.52 / mg/L /
Nov 2018 Week 2 1.8 / mg/L 1.1941 / lbs/day
Nov 2018 Week 3 2.75 / mg/L /
Dec 2018 Week 1 3.27 / mg/L /
Dec 2018 Week 2 2.9 / mg/L 2.2183 / lbs/day
Jul2018 Average 3.09 / mg/L 1.6968 / lbs/day
Aug 2018 Average 6.275 / mg/L 4.818 / lbs/day
Sep 2018 Average 3.93 / mg/L 2.7984 / lbs/day
Oct 2018 Average 6.26 / mg/L 3.3993 / lbs/day
Nov 2018 Average 2.275 / mg/L 1.1941 / lbs/day
Dec 2018 Average 3.085 / mg/L 2.2183 / lbs/day
2018 Quarter 3 4.432 / mg/L 2.7525 / lbs/day
2018 Quarter 4 3.873 / mg/L 2.2706 / lbs/day
2018 2nd 6 Months(Avg) 4.153 / mg/L 2.5460 / lbs/day
2018 2nd 6...(Max) 8.3 / mg/L 4.8180 / lbs/day
2018 2nd 6...(Min) 1.8 / mg/L /
2018 2nd 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
07/17/2018 S Cintas071718Se1f 61.8 / mg/L 31.948328 / lbs/day
07/31/2018 P Cintas073118POTW 390 / mg/L 220.158736 / lbs/day
08/14/2018 S Cintas081418Self 217 / mg/L 125.964308 / lbs/day
08/28/2018 P Cintas082818POTW 848 / mg/L /
09/21/2018 P Cintas092118POTW 1260 / mg/L /
09/25/2018 S Cintas092518Self 105 / mg/L 55.440567 / lbs/day
10/09/2018 S Cintas100918Self 135 / mg/L 76.484639 / lbs/day
10/23/2018 P Cintas102318POTW 808 / mg/L /
11/09/2018 S Cintas110918Self 122 / mg/L 80.935447 / lbs/day
11/15/2018 P Cintas111518POTW 594 / mg/L /
12/06/2018 P Cintas120618POTW 668 / mg/L /
12/14/2018 S Cintas121418Self 167 / mg/L 127.745782 / lbs/day
Jul2018 Week 3 61.8 / mg/L 31.948328 / lbs/day
Jul 2018 Week 4 390 / mg/L 220.158736 / lbs/day
Aug 2018 Week 2 217 / mg/L 125.964308 / lbs/day
Aug 2018 Week 4 848 / mg/L /
Sep 2018 Week 3 1260 / mg/L /
Sep 2018 Week 4 105 / mg/L 55.440567 / lbs/day
Oct 2018 Week 2 135 / mg/L 76.484639 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 15 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
Oct 2018 Week 4 808 / mg/L /
Nov 2018 Week 2 122 / mg/L 80.935447 / lbs/day
Nov 2018 Week 3 594 / mg/L /
Dec 2018 Week 1 668 / mg/L /
Dec 2018 Week 2 167 / mg/L 127.745782 / lbs/day
Jul2018 Average 225.9 / mg/L 126.053532 / lbs/day
Aug 2018 Average 532.5 / mg/L 125.964308 / lbs/day
Sep 2018 Average 682.5 / mg/L 55.440567 / lbs/day
Oct 2018 Average 471.5 / mg/L 76.484639 / lbs/day
Nov 2018 Average 358 / mg/L 80.935447 / lbs/day
Dec 2018 Average 417.5 / mg/L 127.745782 / lbs/day
2018 Quarter 3 480.3 / mg/L 108.377985 / lbs/day
2018 Quarter 4 415.7 / mg/L 95.055289 / lbs/day
2018 2nd 6 Months(Avg) 448.0 / mg/L 102.668 / lbs/day
2018 2nd 6...(Max) 1260 / mg/L 220.158736 / lbs/day
2018 2nd 6...(Min) 61.8 / mg/L /
2018 2nd 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
08/14/2018 S Cintas081418Self 0.0307 / mg/L /
Aug 2018 Week 2 0.0307 / mg/L /
Aug 2018 Average 0.0307 / mg/L /
2018 Quarter 3 0.0307 / mg/L /
2018 2nd 6 Months(Avg) 0.0307 / mg/L /
2018 2nd 6...(Max) 0.0307 / mg/L /
2018 2nd 6...(Min) 0.0307 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/17/2018 S Cintas071718Self 1.06 / mg/L 0.547981 / lbs/day
09/25/2018 S Cintas092518Self 0.623 / mg/L 0.328947 / lbs/day
10/09/2018 S Cintas100918Self 0.98 / mg/L 0.555222 / lbs/day
11/09/2018 S Cintas110918Self 1.02 / mg/L 0.676673 / lbs/day
12/14/2018 S Cintas121418Self 0.833 / mg/L 0.637199 / lbs/day
Jul 2018 Week 3 1.06 / mg/L 0.547981 / lbs/day
Sep 2018 Week 4 0.623 / mg/L 0.328947 / lbs/day
Oct 2018 Week 2 0.98 / mg/L 0.555222 / lbs/day
Nov 2018 Week 2 1.02 / mg/L 0.676673 / lbs/day
Dec 2018 Week 2 0.833 / mg/L 0.637199 / lbs/day
Jul 2018 Average 1.06 / mg/L 0.547981 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 16 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit 1
Zinc
Sep 2018 Average 0.623 / mg/L 0.328947 / lbs/day
Oct 2018 Average 0.98 / mg/L 0.555222 / lbs/day
Nov 2018 Average 1.02 / mg/L 0.676673 / lbs/day
Dec 2018 Average 0.833 / mg/L 0.637199 / lbs/day
2018 Quarter 3 0.842 / mg/L 0.438464 / lbs/day
2018 Quarter 4 0.944 / mg/L 0.623031 / lbs/day
2018 2nd 6 Months(Avg) 0.903 / mg/L 0.549205 / lbs/day
2018 2nd 6...(Max) 1.06 / mg/L 0.676673 / lbs/day
2018 2nd 6...(Min) 0.623 / mg/L 0.328947 / lbs/day
2018 2nd 6...(Count) 5 / 5 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 17 of 17

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SampleID Result/Limit Mass/Limit
Ammonia
07/27/2018 P CreeP8072718POTW 16.2 / mg/L 44.3154 / lbs/day
10/16/2018 S CreeP8101618Self 24.4 / mg/L 64.5082 / lbs/day
Jul2018 Week 4 16.2 / mg/L 44.3154 / lbs/day
Oct 2018 Week 3 24.4 / mg/L 64.5082 / lbs/day
Jul 2018 Average 16.2 / mg/L 44.3154 / lbs/day
Oct 2018 Average 24.4 / mg/L 64.5082 / lbs/day
2018 Quarter 3 16.2 / mg/L 44.3154 / lbs/day
2018 Quarter 4 24.4 / mg/L 64.5082 / lbs/day
2018 2nd 6 Months(Avg) 20.3 / mg/L 54.4118 / lbs/day
2018 2nd 6...(Max) 24.4 / mg/L 64.5082 / lbs/day
2018 2nd 6...(Min) 16.2 / mg/L 44.3154 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S CreeP80718Flow 0.29376 / MGD /
08/31/2018 S CreeP80818Flow 0.363642 / MGD /
09/30/2018 S CreeP80918Flow 0.338496 / MGD /
10/31/2018 S CreeP81018Flow 0.312033 / MGD /
11/30/2018 S CreeP81118Flow 0.317904 / MGD /
12/31/2018 S CreeP81218Flow 0.298268 / MGD /
Jul2018 Week 4 0.29376 / MGD /
Aug 2018 Week 4 0.363642 / MGD /
Sep 2018 Week 4 0.338496 / MGD /
Oct 2018 Week 4 0.312033 / MGD /
Nov 2018 Week 4 0.317904 / MGD /
Dec 2018 Week 4 0.298268 / MGD /
Jul2018 Average 0.29376 / MGD /
Aug 2018 Average 0.363642 / MGD /
Sep 2018 Average 0.338496 / MGD /
Oct 2018 Average 0.312033 / MGD /
Nov 2018 Average 0.317904 / MGD /
Dec 2018 Average 0.298268 / MGD /
2018 Quarter 3 0.331966 / MGD /
2018 Quarter 4 0.309402 / MGD /
2018 2nd 6 Months(Avg) 0.320684 / MGD /
2018 2nd 6...(Max) 0.363642 / MGD /
2018 2nd 6...(Min) 0.29376 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 7

Cree, Inc.(AI1)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 008
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
10/16/2018 S CreeP8101618Self < 0.0005 / mg/L < 0.001322 / lbs/day
Oct 2018 Week 3 < 0.0005 / mg/L < 0.001322 / lbs/day
Oct 2018 Average < 0.0005 / mg/L < 0.001322 / lbs/day
2018 Quarter 4 < 0.0005 / mg/L < 0.001322 / lbs/day
2018 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.001322 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.001322 / lbs/day
2018 2nd 6...(Min) < 0.0005 / mg/L < 0.001322 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/27/2018 P CreeP8072718POTW 146 / mg/L 399.3859 / lbs/day
10/16/2018 S CreeP8101618Self 141 / mg/L 372.773 / lbs/day
Jul 2018 Week 4 146 / mg/L 399.3859 / lbs/day
Oct 2018 Week 3 141 / mg/L 372.773 / lbs/day
Jul2018 Average 146 / mg/L 399.3859 / lbs/day
Oct 2018 Average 141 / mg/L 372.773 / lbs/day
2018 Quarter 3 146 / mg/L 399.3859 / lbs/day
2018 Quarter 4 141 / mg/L 372.773 / lbs/day
2018 2nd 6 Months(Avg) 143.5 / mg/L 386.079 / lbs/day
2018 2nd 6...(Max) 146 / mg/L 399.3859 / lbs/day
2018 2nd 6...(Min) 141 / mg/L 372.7730 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/27/2018 P CreeP8,072718POTW 0.01 / mg/L 0.027355 / lbs/day
10/16/2018 S CreeP8101618Self 0.012 / mg/L 0.031725 / lbs/day
Jul 2018 Week 4 0.01 / mg/L 0.027355 / lbs/day
Oct 2018 Week 3 0.012 / mg/L 0.031725 / lbs/day
Jul2018 Average 0.01 / mg/L 0.027355 / lbs/day
Oct 2018 Average 0.012 / mg/L 0.031725 / lbs/day
2018 Quarter 3 0.01 / mg/L 0.027355 / lbs/day
2018 Quarter 4 0.012 / mg/L 0.031725 / lbs/day
2018 2nd 6 Months(Avg) 0.011 / mg/L 0.029540 / lbs/day
2018 2nd 6...(Max) 0.012 / mg/L 0.031725 / lbs/day
2018 2nd 6...(Min) 0.01 / mg/L 0.027355 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/27/2018 P CreeP8072718POTW 1.24 / mg/L 3.392 / lbs/day
10/16/2018 S CreeP8101618Self 1.2 / mg/L 3.1725 / lbs/day
Jul 2018 Week 4 1.24 / mg/L 3.392 / lbs/day
Oct 2018 Week 3 1.2 / mg/L 3.1725 / lbs/day
Jul 2018 Average 1.24 / mg/L 3.392 / lbs/day
Oct 2018 Average 1.2 / mg/L 3.1725 / lbs/day
2018 Quarter 3 1.24 / mg/L 3.392 / lbs/day
2018 Quarter 4 1.2 / mg/L 3.1725 / lbs/day
2018 2nd 6 Months(Avg) 1.22 / mg/L 3.2823 / lbs/day
2018 2nd 6...(Max) 1.24 / mg/L 3.3920 / lbs/day
2018 2nd 6...(Min) 1.2 / mg/L 3.1725 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
10/09/2018 P CreeP8100918POTW 0.000012 / mg/L /
Hg
10/16/2018 S CreeP8101618Self 0.000006 / mg/L /
Oct 2018 Week 2 0.000012 / mg/L /
Oct 2018 Week 3 0.000006 / mg/L /
Oct 2018 Average 0.000009 / mg/L /
2018 Quarter 4 0.000009 / mg/L /
2018 2nd 6 Months(Avg) 0.0000089 / mg/L /
2018 2nd 6...(Max) 0.0000123 / mg/L /
2018 2nd 6...(Min) 0.0000055 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/27/2018 P CreeP8072718POTW 0.004 / mg/L 0.0109 / 0.457 lbs/day
10/16/2018 S CreeP8101618Self < 0.003 / mg/L < 0.0066 / 0.457 lbs/day
Jul 2018 Week 4 0.004 / mg/L 0.0109 / lbs/day
Oct 2018 Week 3 < 0.003 / mg/L < 0.0066 / lbs/day
Jul2018 Average 0.004 / mg/L 0.0109 / lbs/day
Oct 2018 Average < 0.003 / mg/L < 0.0066 / lbs/day
2018 Quarter 3 0.004 / mg/L 0.0109 / lbs/day
2018 Quarter 4 < 0.003 / mg/L < 0.0066 / lbs/day
2018 2nd 6 Months(Avg) < 0.003 / mg/L < 0.0088 / lbs/day
2018 2nd 6...(Max) 0.004 / mg/L 0.0109 / lbs/day
2018 2nd 6...(Min) < 0.003 / mg/L < 0.0066 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12%31/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
N itrate-Nitrite
07/27/2018 P CreeP8072718POTW I.1 / mg/L 3.091 / lbs/day
10/16/2018 S CreeP8101618Self 2.3 / mg/L 6.081 / lbs/day
Jul 2018 Week 4 1.1 / mg/L 3.091 / lbs/day
Oct 2018 Week 3 2.3 / mg/L 6.081 / lbs/day
Jul 2018 Average 1.1 / mg/L 3.091 / lbs/day
Oct 2018 Average 2.3 / mg/L 6.081 / lbs/day
2018 Quarter 3 1.1 / mg/L 3.091 / lbs/day
2018 Quarter 4 2.3 / mg/L 6.081 / lbs/day
2018 2nd 6 Months(Avg) 1.7 / mg/L 4.586 / lbs/day
2018 2nd 6...(Max) 2.3 / mg/L 6.081 / lbs/day
2018 2nd 6...(Min) 1.1 / mg/L 3.091 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/27/2018 P CreeP8072718POTW 17.8 / mg/L 48.692 / lbs/day
10/16/2018 S CreeP8101618Self 35.6 / mg/L 94.119 / lbs/day
Jul 2018 Week 4 17.8 / mg/L 48.692 / lbs/day
Oct 2018 Week 3 35.6 / mg/L 94.119 / lbs/day
Jul 2018 Average 17.8 / mg/L 48.692 / lbs/day
Oct 2018 Average 35.6 / mg/L 94.119 / lbs/day
2018 Quarter 3 17.8 / mg/L48.692 lbs/day
/
2018 Quarter 4 35.6 / mg/L 94.119 / lbs/day
2018 2nd 6 Months(Avg) 26.7 / mg/L 71.405 / lbs/day
2018 2nd 6...(Max) 35.6 / mg/L 94.119 / lbs/day
2018 2nd 6...(Min) 17.8 / mg/L 48.692 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil &Grease,Total
07/27/2018 P •CreeP8072718POTW < 2.5 / mg/L < /
Jul 2018 Week 4 < 2.5 / mg/L < /
Jul 2018 Average < 2.5 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Lim&
Oil&Grease,Total
2018 Quarter 3 < 2.5 / mg/L < /
2018 2nd 6 Months(Avg) < 2.5 / mg/L < /
2018 2nd 6...(Max) < 2.5 / mg/L < /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/27/2018 P CreeP8072718POTW 9.3 /5.0- 10.5 SU /
10/16/2018 S CreeP8101618Self 9.7 /5.0- 10.5 SU /
Jul 2018 Week 4 9.3 / SU /
Oct 2018 Week 3 9.7 / SU /
Jul 2018 Average 9.3 / SU /
Oct 2018 Average 9.7 / SU /
2018 Quarter 3 9.3 / SU /
2018 Quarter 4 9.7 / SU /
2018 2nd 6 Months(Avg) 9.5 / SU /
2018 2nd 6...(Max) 9.7 / SU /
2018 2nd 6...(Min) 9.3 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/27/2018 P CreeP8072718POTW 28 /66 °C /
Jul 2018 Week 4 28 / °C /
Jul 2018 Average 28 / °C /
2018 Quarter 3 28 / °C /
2018 2nd 6 Months(Avg) 28 / °C /
2018 2nd 6...(Max) 28 / °C /
2018 2nd 6...(Min) 28 / °C /
2018 2nd 6...(Count) 1 / /
1 Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 008
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
% % # % 0
# /o
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/27/2018 P CreeP8072718POTW 16.7 / mg/L 45.683 / lbs/day
08/21/2018 P CreeP8082118POTW 28 / mg/L 84.918 / lbs/day
09/13/2018 P CreeP8091318POTW 25.7 / mg/L 99.453 / lbs/day
10/09/2018 P CreeP8100918POTW 26.4 / mg/L 74.199 / lbs/day
10/16/2018 S CreeP8101618Self 33.3 / mg/L 88.038 / lbs/day
11/15/2018 P CreeP8111518POTW 30.4 / mg/L 70.229 / lbs/day
12/20/2018 P CreeP8122018POTW 27.7 / mg/L 61.22 / lbs/day
Jul 2018 Week 4 16.7 / mg/L 45.683 / lbs/day
Aug 2018 Week 3 28 / mg/L 84.918 / lbs/day
Sep 2018 Week 2 25.7 / mg/L 99.453 / lbs/day
Oct 2018 Week 2 26.4 / mg/L 74.199 / lbs/day
Oct 2018 Week 3 33.3 / mg/L 88.038 / lbs/day
Nov 2018 Week 3 30.4 / mg/L 70.229 / lbs/day
Dec 2018 Week 3 27.7 / mg/L 61.22 / lbs/day
Jul 2018 Average 16.7 / mg/L 45.683 / lbs/day
Aug 2018 Average 28 / mg/L 84.918 / lbs/day
Sep 2018 Average 25.7 / mg/L 99.453 / lbs/day
Oct 2018 Average 29.85 / mg/L 81.119 / lbs/day
Nov 2018 Average 30.4 / mg/L 70.229 / lbs/day
Dec 2018 Average 27.7 / mg/L 61.22 / lbs/day
2018 Quarter 3 23.47 / mg/L 76.685 / lbs/day
2018 Quarter 4 29.45 / mg/L 73.422 / lbs/day
2018 2nd 6 Months(Avg) 26.89 / mg/L 74.82 / lbs/day
2018 2nd 6...(Max) 33.3 / mg/L 99.453 / lbs/day
2018 2nd 6...(Min) 16.7 / mg/L 45.683 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/27/2018 P CreeP8072718POTW 2.5 / mg/L 6.8388 / lbs/day
08/21/2018 P CreeP8082118POTW 2.1 / mg/L 6.3688 / lbs/day
09/13/2018 P CreeP8091318POTW . 2.86 / mg/L 11.0675 / lbs/day
10/09/2018 P CreeP8100918POTW 2.52 / mg/L 7.0827 / lbs/day
11/15/2018 P CreeP8111518POTW 2.78 / mg/L 6.4223 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 T Sample e: Effluent Wastewater Out all: 008
P Y EP .f.� f
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
12/20/2018 P CreeP8122018POTW 2.34 / mg/L 5.1716 / lbs/day
Jul 2018 Week 4 2.5 / mg/L 6.8388 / lbs/day
Aug 2018 Week 3 2.1 / mg/L 6.3688 / lbs/day
Sep 2018 Week 2 2.86 / mg/L 11.0675 / lbs/day
Oct 2018 Week 2 2.52 / mg/L 7.0827 / lbs/day
Nov 2018 Week 3 2.78 / mg/L 6.4223 / lbs/day
Dec 2018 Week 3 2.34 / mg/L 5.1716 / lbs/day
Jul 2018 Average 2.5 / mg/L 6.8388 / lbs/day
Aug 2018 Average 2.1 / mg/L 6.3688 / lbs/day
Sep 2018 Average 2.86 / mg/L 11.0675 / lbs/day
Oct 2018 Average 2.52 / mg/L 7.0827 / lbs/day
Nov 2018 Average 2.78 / mg/L 6.4223 / lbs/day
Dec 2018 Average 2.34 / mg/L 5.1716 / lbs/day
2018 Quarter 3 2.487 / mg/L 8.0917 / lbs/day
2018 Quarter 4 2.547 / mg/L 6.2255 / lbs/day
2018 2nd 6 Months(Avg) 2.517 / mg/L 7.1586 / lbs/day
2018 2nd 6...(Max) 2.86 / mg/L 11.0675 / lbs/day
2018 2nd 6...(Min) 2.1 / mg/L 5.1716 / lbs/day
2018 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
TTO
12/21/2018 S CreeP8122118Self < 0.0025 / mg/L < /
Dec 2018 Week 3 < 0.0025 / mg/L < /
Dec 2018 Average < 0.0025 / mg/L < /
2018 Quarter 4 < 0.0025 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
10/16/2018 S CreeP8101618Self 0.758 / mg/L 2.003985 / lbs/day
Oct 2018 Week 3 0.758 / mg/L 2.003985 / lbs/day
Oct2018 Average 0.758 / mg/L 2.003985 / lbs/day
2018 Quarter 4 0.758 / mg/L 2.003985 / lbs/day
2018 2nd 6 Months(Avg) 0.758 / mg/L 2.00399 / lbs/day
2018 2nd 6...(Max) 0.758 / mg/L 2.003985 / lbs/day
2018 2nd 6...(Min) 0.758 / mg/L 2.003985 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 7

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S CreeP90718F1ow 0.02102 / MGD /
08/31/2018 S CreeP90818F1ow 0.019741 / MGD /
09/30/2018 S CreeP90918F1ow 0.01888 / MGD /
10/31/2018 S CreeP91018F1ow 0.022857 / MGD /
11/30/2018 S CreeP91118Flow 0.021405 / MGD /
12/31/2018 S CreeP91218F1ow 0.018658 / MGD /
Jul 2018 Week 4 0.02102 / MGD /
Aug 2018 Week 4 0.019741 / MGD /
Sep 2018 Week 4 0.01888 / MGD /
Oct 2018 Week 4 0.022857 / MGD /
Nov 2018 Week 4 0.021405 / MGD /
Dec 2018 Week 4 0.018658 / MGD /
Jul2018 Average 0.02102 / MGD /
Aug 2018 Average 0.019741 / MGD /
Sep 2018 Average 0.01888 / MGD /
Oct 2018 Average 0.022857 / MGD /
Nov 2018 Average 0.021405 / MGD /
Dec 2018 Average 0.018658 / MGD /
2018 Quarter 3 0.01988 / MGD /
2018 Quarter 4 0.020973 / MGD /
2018 2nd 6 Months(Avg) 0.020427 / MGD /
2018 2nd 6...(Max) 0.022857 / MGD /
2018 2nd 6...(Min) 0.018658 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/27/2018 P CreeP9072718POTW 57 / mg/L /
10/16/2018 S CreeP9101618Se1f 38.8 / mg/L /
Jul 2018 Week 4 57 / mg/L /
Oct 2018 Week 3 38.8 / mg/L /
Jul 2018 Average 57 / mg/L /
Oct 2018 Average 38.8 / mg/L /
2018 Quarter 3 57 / mg/L /
2018 Quarter 4 38.8 / mg/L /
2018 2nd 6 Months(Avg) 47.9 / mg/L /
2018 2nd 6...(Max) 57 / mg/L /
2018 2nd 6...(Min) 38.8 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Copper
10/16/2018 S CreeP9101618Se1f 0.038 / mg/L /
Oct 2018 Week 3 0.038 / mg/L /
Oct 2018 Average 0.038 / mg/L /
2018 Quarter 4 0.038 / mg/L /
2018 2nd 6 Months(Avg) 0.038 / mg/L /
2018 2nd 6...(Max) 0.038 / mg/L /
2018 2nd 6...(Min) 0.038 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/27/2018 P CreeP9072718POTW < 0.003 / mg/L < /
Jul2018 Week 4 < 0.003 / mg/L < /
Jul2018 Average < 0.003 / mg/L < /
2018 Quarter 3 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/27/2018 P CreeP9072718POTW 0.2 / mg/L /
10/16/2018 S CreeP9101618Se1f 0.21 / mg/L /
Jul 2018 Week 4 0.2 / mg/L /
Oct 2018 Week 3 0.21 / mg/L /
Jul2018 Average 0.2 / mg/L /
Oct 2018 Average 0.21 / mg/L g/L /
2018 Quarter 3 0.2 / mg/L /
2018 Quarter 4 0.21 / mg/L /
2018 2nd 6 Months(Avg) 0.21 / mg/L /
2018 2nd 6...(Max) 0.21 / mg/L /
2018 2nd 6...(Min) 0.2 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
10/09/2018 P CreeP9100918POTW 0.000054 / mg/L /
Hg
10/16/2018 S CreeP9101618Self 0.000018 / mg/L /
Oct 2018 Week 2 0.000054 / mg/L /
Oct 2018 Week 3 0.000018 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Oct 2018 Average 0.000036 / mg/L /
2018 Quarter 4 0.000036 / mg/L /
2018 2nd 6 Months(Avg) 0.0000359 / mg/L /
2018 2nd 6...(Max) 0.000054 / mg/L /
2018 2nd 6...(Min) 0.0000177 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/27/2018 P CreeP9072718POTW < 0.001 / mg/L < /
Jul 2018 Week 4 < 0.001 / mg/L < /
Jul2018 Average < 0.001 / mg/L < /
2018 Quarter 3 < 0.001 / mg/L < /
2018 2nd 6 Months(Avg) < 0.001 / mg/L < /
2018 2nd 6...(Max) < 0.001 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
07/27/2018 P CreeP9072718POTW 5 / mg/L /
Jul2018 Week 4 5 / mg/L /
Jul2018 Average 5 / mg/L /
2018 Quarter 3 5 / mg/L /
2018 2nd 6 Months(Avg) 5 / mg/L /
2018 2nd 6...(Max) 5 / mg/L /
2018 2nd 6...(Min) 5 / mg/L /
2018 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
pH .
10/16/2018 S CreeP9101618Se1f 7.6 /5.0- 10.5 SU /
Oct 2018 Week 3 7.6 / SU /
Oct 2018 Average 7.6 / SU /
2018 Quarter 4 7.6 / SU /
2018 2nd 6 Months(Avg) 7.6 / SU /
2018 2nd 6...(Max) 7.6 / SU /
2018 2nd 6...(Min) 7.6 / SU /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 009
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/27/2018 P CreeP9072718POTW 28 / °C /
Jul 2018 Week 4 28 / °C /
Jul2018 Average 28 / °C /
2018 Quarter 3 28 / °C /
2018 2nd 6 Months(Avg) 28 / °C /
2018 2nd 6...(Max) 28 / °C /
2018 2nd 6...(Min) 28 / °C /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/27/2018 P CreeP9072718POTW 31.8 / mg/L /
08/21/2018 P CreeP9082118POTW 54.7 / mg/L /
09/13/2018 P CreeP9091318POTW 20.4 / mg/L /
10/09/2018 P CreeP9100918POTW 40.6 / mg/L /
11/15/2018 P CreeP9111518POTW 34.5 / mg/L /
12/20/2018 P CreeP9122018POTW 31.2 / mg/L /
Jul 2018 Week 4 31.8 / mg/L /
Aug 2018 Week 3 54.7 / mg/L /
Sep 2018 Week 2 20.4 / mg/L /
Oct 2018 Week 2 40.6 / mg/L /
Nov 2018 Week 3 34.5 / mg/L /
Dec 2018 Week 3 31.2 / mg/L /
Jul2018 Average 31.8 / mg/L /
Aug 2018 Average 54.7 / mg/L /
Sep 2018 Average 20.4 / mg/L /
Oct 2018 Average 40.6 / mg/L /
Nov 2018 Average 34.5 / mg/L /
Dec 2018 Average 31.2 / mg/L /
2018 Quarter 3 35.63 / mg/L /
2018 Quarter 4 35.43 / mg/L /
2018 2nd 6 Months(Avg) 35.53 / mg/L /
2018 2nd 6...(Max) 54.7 / mg/L /
2018 2nd 6...(Min) 20.4 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 009
' Sample Date SamplelD Result/Limit Mass/Limit
TKN
2018 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/27/2018 P CreeP9072718POTW 5.47 / mg/L /
08/21/2018 P CreeP9082118POTW 5.69 / mg/L /
09/13/2018 P CreeP9091318POTW 4.19 / mg/L /
10/09/2018 P CreeP9100918POTW 5.09 / mg/L /
11/15/2018 P CreeP9111518POTW 3.8 / mg/L /
12/20/2018 P CreeP9122018POTW 3.28 / mg/L /
Jul 2018 Week 4 5.47 / mg/L /
Aug 2018 Week 3 5.69 / mg/L /
Sep 2018 Week 2 4.19 / mg/L /
Oct 2018 Week 2 5.09 / mg/L /
Nov 2018 Week 3 3.8 / mg/L /
Dec 2018 Week 3 3.28 / mg/L /
Jul2018 Average 5.47 / mg/L /
Aug 2018 Average 5.69 / mg/L /
Sep 2018 Average 4.19 / mg/L /
Oct 2018 Average 5.09 / mg/L /
Nov 2018 Average 3.8 / mg/L /
Dec 2018 Average 3.28 / mg/L /
2018 Quarter 3 5.117 / mg/L /
2018 Quarter 4 4.057 / mg/L /
2018 2nd 6 Months(Avg) 4.587 / mg/L /
2018 2nd 6...(Max) 5.69 / mg/L /
2018 2nd 6...(Min) 3.28 / mg/L /
2018 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
TTO
12/21/2018 S CreeP9122118Self 0.0154 / mg/L /
Dec 2018 Week 3 0.0154 / mg/L /
Dec 2018 Average 0.0154 / mg/L /
2018 Quarter 4 0.0154 / mg/L /
2018 2nd 6 Months(Avg) 0.0154 / mg/L /
2018 2nd 6...(Max) 0.0154 / mg/L /
2018 2nd 6...(Min) 0.0154 / mg/L /
2018 2nd 6...(Count) 1 / /
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: All
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Cree0718F1ow 0.31478 /0.600 MGD /
08/31/2018 S Cree0818F1ow 0.383383 /0.600 MGD /
09/30/2018 S Cree0918F1ow 0.357376 /0.600 MGD /
10/31/2018 S Cree1018Flow 0.33489 /0.600 MGD /
11/30/2018 S Creel 118Flow 0.339309 /0.600 MGD /
12/31/2018 S Cree1218Flow 0.316925 /0.600 MGD /
Jul 2018 Week 4 0.31478 / MGD /
Aug 2018 Week 4 0.383383 / MGD /
Sep 2018 Week 4 0.357376 / MGD /
Oct 2018 Week 4 0.33489 / MGD /
Nov 2018 Week 4 0.339309 / MGD /
Dec 2018 Week 4 0.316925 / MGD /
Jul2018 Average 0.31478 /0.451 MGD /
Aug 2018 Average 0.383383 /0.451 MGD /
Sep 2018 Average 0.357376 /0.451 MGD /
Oct 2018 Average 0.33489 /0.451 MGD /
Nov 2018 Average 0.339309 /0.451 MGD /
Dec 2018 Average 0.316925 /0.451 MGD /
2018 Quarter 3 0.351846 / MGD /
2018 Quarter 4 0.330375 / MGD /
2018 2nd 6 Months(Avg) 0.341111 / MGD /
2018 2nd 6...(Max) 0.383383 / MGD /
2018 2nd 6...(Min) 0.31478 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/27/2018 P Cree072718POTW 1.24 /8 mg/L /
10/16/2018 S Cree101618Self 1.13 /8 mg/L /
Jul2018 Week 4 1.24 / mg/L /
Oct 2018 Week 3 1.13 / mg/L /
Jul 2018 Average 1.24 /7 mg/L /
Oct 2018 Average 1.13 /7 mg/L /
2018 Quarter 3 1.24 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 3

Creel Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2018 Quarter 4 1.13 / mg/L /
2018 2nd 6 Months(Avg) 1.18 / mg/L /
2018 2nd 6...(Max) 1.24 / mg/L /
2018 2nd 6...(Min) 1.13 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury
10/09/2018 P Cree100918POTWHg 0.00002 / mg/L /
Oct 2018 Week 2 0.00002 / mg/L /
Oct 2018 Average 0.00002 / mg/L /
2018 Quarter 4 0.00002 / mg/L /
2018 2nd 6 Months(Avg) 0.00002 / mg/L /
2018 2nd 6...(Max) 0.00002 / mg/L /
2018 2nd 6...(Min) 0.00002 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
10/16/2018 S Cree101618Selfl-Ig 0.000006 /0.000142 mg/L /
Oct 2018 Week 3 0.000006 / mg/L /
Oct 2018 Average 0.000006 / mg/L /
2018 Quarter 4 0.000006 / mg/L /
2018 2nd 6 Months(Avg) 0.0000063 / mg/L /
2018 2nd 6...(Max) 0.0000063 / mg/L /
2018 2nd 6...(Min) 0.0000063 / mg/L /
2018 2nd 6...(Count) 1 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 3

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: All
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
07/27/2018 P Cree072718POTW < 2.5 /200 mg/L < /
Jul 2018 Week 4 < 2.5 / mg/L < /
Jul2018 Average < 2.5 / mg/L < /
2018 Quarter 3 < 2.5 / mg/L < /
2018 2nd 6 Months(Avg) < 2.5 / mg/L < /
2018 2nd 6...(Max) < 2.5 / mg/L < /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) I / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 3

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
09/11/2018 S CreeRTPP12091118Sel < 0.05 / mg/L < 0.057003 / lbs/day
f
Sep 2018 Week 2 < 0.05 / mg/L < 0.057003 / lbs/day
Sep 2018 Average < 0.05 / mg/L < 0.057003 / lbs/day
2018 Quarter 3 < 0.05 / mg/L < 0.057003 / lbs/day
2018 2nd 6 Months(Avg) < 0.05 / mg/L < 0.057003 / lbs/day
2018 2nd 6...(Max) < 0.05 / mg/L < 0.057003 / lbs/day
2018 2nd 6...(Min) < 0.05 / mg/L < 0.057003 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/27/2018 P CreeRTPP12072718P 4.4 / mg/L 5.0047 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 4 / mg/L 4.1374 / lbs/day
If
Jul 2018 Week 4 4.4 / mg/L 5.0047 / lbs/day
Oct 2018 Week 3 4 / mg/L 4.1374 / lbs/day
Jul 2018 Average 4.4 / mg/L 5.0047 / lbs/day
Oct 2018 Average 4 / mg/L 4.1374 / lbs/day
2018 Quarter 3 4.4 / mg/L 5.0047 / lbs/day
2018 Quarter 4 4 / mg/L 4.1374 / lbs/day
2018 2nd 6 Months(Avg) 4.2 / mg/L 4.5711 / lbs/day
2018 2nd 6...(Max) 4.4 / mg/L 5.0047 / lbs/day
2018 2nd 6...(Min) 4 / mg/L 4.1374 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
09/11/2018 S CreeRTPP12091118Sel < 0.005 / mg/L < 0.0057 / lbs/day
f
10/16/2018 S CreeRTPP12101618Se < 0.005 / mg/L < 0.005172 / lbs/day
if
Sep 2018 Week 2 < 0.005 / mg/L < 0.0057 / lbs/day
Oct 2018 Week 3 < 0.005 / mg/L < 0.005172 / lbs/day
Sep 2018 Average < 0.005 / mg/L < 0.0057 / lbs/day
Oct 2018 Average < 0.005 / mg/L < 0.005172 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.0057 / lbs/day
2018 Quarter 4 < 0.005 / mg/L < 0.005172 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.005436 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.005700 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.005172 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/18/2018 S CreeRTPP120718Flow 0.136384 /0.469 MGD /
08/22/2018 S CreeRTPP120818F1ow 0.172412 /0.469 MGD /
09/20/2018 S CreeRTPP120918Flow 0.136697 /0.469 MGD /
10/18/2018 S CreeRTPP121018F1ow 0.124022 /0.469 MGD /
11/21/2018 S CreeRTPP121118F1ow 0.109001 /0.469 MGD /
12/20/2018 S CreeRTPP121218Flow 0.113575 /0.469 MGD /
Jul2018 Week 3 0.136384 / MGD /
Aug 2018 Week 4 0.172412 / MGD /
Sep 2018 Week 3 0.136697 / MGD /
Oct 2018 Week 3 0.124022 / MGD /
Nov 2018 Week 3 0.109001 / MGD /
Dec 2018 Week 3 0.113575 / MGD /
Jul 2018 Average 0.136384 /0.329 MGD /
Aug 2018 Average 0.172412 /0.329 MGD /
Sep 2018 Average 0.136697 /0.329 MGD /
Oct 2018 Average 0.124022 /0.329 MGD /
Nov 2018 Average 0.109001 /0.329 MGD /
Dec 2018 Average 0.113575 /0.329 MGD /
2018 Quarter 3 0.148498 / MGD /
2018 Quarter 4 0.115533 / MGD /
2018 2nd 6 Months(Avg) 0.132015 / MGD /
2018 2nd 6...(Max) 0.172412 / MGD /
2018 2nd 6...(Min) 0.109001 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Barium
09/11/2018 S CreeRTPP12091118Se1 < 0.0025 / mg/L < 0.00285 / lbs/day
f
Sep 2018 Week 2 < 0.0025 / mg/L < 0.00285 / lbs/day
Sep 2018 Average < 0.0025 / mg/L < 0.00285 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.00285 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.002850 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall. 012
Sample Date SamplelD Result/Limit Mass/Limit
Barium
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
09/11/2018 S CreeRTPP12091118Sel < 0.0005 / mg/L < 0.00057 / lbs/day
f
Sep 2018 Week 2 < 0.0005 / mg/L < 0.00057 / lbs/day
Sep 2018 Average < 0.0005 / mg/L < 0.00057 / lbs/day
2018 Quarter 3 < 0.0005 / mg/L < 0.00057 / lbs/day
2018 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.000570 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.000570 / lbs/day
2018 2nd 6...(Min) < 0.0005 / mg/L < 0.000570 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/27/2018 P CreeRTPP12072718P 54 / mg/L 61.4219 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 73.9 / mg/L 76.438 / lbs/day
If
Jul 2018 Week 4 54 / mg/L 61.4219 / lbs/day
Oct 2018 Week 3 73.9 / mg/L 76.438 / lbs/day
Jul 2018 Average 54 / mg/L 61.4219 / lbs/day
Oct 2018 Average 73.9 / mg/L 76.438 / lbs/day
2018 Quarter 3 54 / mg/L 61.4219 / lbs/day
2018 Quarter 4 73.9 / mg/L 76.438 / lbs/day
2018 2nd 6 Months(Avg) 63.95 / mg/L 68.9299 / lbs/day
2018 2nd 6...(Max) 73.9 / mg/L 76.4380 / lbs/day
2018 2nd 6...(Min) 54 / mg/L 61.4219 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
09/11/2018 S CreeRTPP12091118Sel < 0.003 / mg/L < 0.00285 / lbs/day
f
Sep 2018 Week 2 < 0.003 / mg/L < 0.00285 / lbs/day
Sep 2018 Average < 0.003 / mg/L < 0.00285 / lbs/day
2018 Quarter 3 < 0.003 / mg/L < 0.00285 / lbs/day
2018 2nd 6 Months(Avg) < 0.003 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Max) < 0.003 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Min) < 0.003 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Copper
09/11/2018 S CreeRTPP12091118Sel 0.016 / mg/L 0.018355 / lbs/day
f
Sep 2018 Week 2 0.016 / mg/L 0.018355 / lbs/day
Sep 2018 Average 0.016 / mg/L 0.018355 / lbs/day
2018 Quarter 3 0.016 / mg/L 0.018355 / lbs/day
2018 2nd 6 Months(Avg) 0.016 / mg/L 0.018355 / lbs/day
2018 2nd 6...(Max) 0.016 / mg/L 0.018355 / lbs/day
2018 2nd 6...(Min) 0.016 / mg/L 0.018355 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/13/2018 S CreeRTPP12071318Se < 0.002 / mg/L < 0.002 /0.05 lbs/day
If
07/24/2018 S CreeRTPP12072418Se 0.008 / mg/L 0.009 /0.05 lbs/day
if
07/27/2018 P CreeRTPP12072718P < 0.003 / mg/L < 0.003 /0.05 lbs/day
OTW
08/02/2018 S CreeRTPP12080218Se < 0.004 / mg/L < 0.006 /0.05 lbs/day
If
08/20/2018 S CreeRTPP12082018Se < 0.004 / mg/L < 0.006 /0.05 lbs/day
If
09/11/2018 S CreeRTPP12091118Sel < 0.004 / mg/L < 0.005 /0.05 lbs/day
f
09/25/2018 S CreeRTPP12092518Se < 0.004 / mg/L < 0.005 /0.05 lbs/day
if
10/16/2018 S CreeRTPP12101618Se < 0.004 / mg/L < 0.004 /0.05 lbs/day
If
10/29/2018 S CreeRTPP12102918Se < 0.004 / mg/L < 0.004 /0.05 lbs/day
if
11/15/2018 S CreeRTPP12111518Sel 0.011 / mg/L 0.01 /0.05 lbs/day
f
11/30/2018 S CreeRTPP12113018Se 0.008 / mg/L 0.007 /0.05 lbs/day
If
12/11/2018 S CreeRTPP12121118Sel < 0.004 / mg/L < 0.004 /0.05 lbs/day
f
12/21/2018 S CreeRTPP12122118Se < 0.004 / mg/L < 0.004 /0.05 lbs/day
If
Jul 2018 Week 2 < 0.002 / mg/L < 0.002 / lbs/day
Jul 2018 Week 4 < 0.005 / mg/L < 0.006 / lbs/day
Aug 2018 Week 1 < 0.004 / mg/L < 0.006 / lbs/day
Aug 2018 Week 3 < 0.004 / mg/L < 0.006 / lbs/day
Sep 2018 Week 2 < 0.004 / mg/L < 0.005 / lbs/day
Sep 2018 Week 4 < 0.004 / mg/L < 0.005 / lbs/day
Oct 2018 Week 3 < 0.004 / mg/L < 0.004 / lbs/day
Oct 2018 Week 4 < 0.004 / mg/L < 0.004 / lbs/day
Nov 2018 Week 3 0.011 / mg/L 0.01 / lbs/day
Nov 2018 Week 4 0.008 / mg/L 0.007 / lbs/day
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Dec 2018 Week 2 < 0.004 / mg/L < 0.004 / lbs/day
Dec 2018 Week 3 < 0.004 / mg/L < 0.004 / lbs/day
Jul 2018 Average < 0.004 / mg/L < 0.005 / lbs/day
Aug 2018 Average < 0.004 / mg/L < 0.006 / lbs/day
Sep 2018 Average < 0.004 / mg/L < 0.005 / lbs/day
Oct 2018 Average < 0.004 / mg/L < 0.004 / lbs/day
Nov 2018 Average 0.01 / mg/L 0.009 / lbs/day
Dec 2018 Average < 0.004 / mg/L < 0.004 / lbs/day
2018 Quarter 3 < 0.004 / mg/L < 0.005 / lbs/day
2018 Quarter 4 < 0.006 / mg/L < 0.006 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.005 / lbs/day
2018 2nd 6...(Max) 0.011 / mg/L 0.010 / lbs/day
2018 2nd 6...(Min) < 0.002 / mg/L < 0.002 / lbs/day
2018 2nd 6...(Count) 13 / 13 /
Sample Count: 13 Months Sampled: 6 Weeks Sampled: 12 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/27/2018 P CreeRTPP12072718P 0.39 /8 mg/L 0.4436 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 0.57 /8 mg/L 0.5896 / lbs/day
If
Jul 2018 Week 4 0.39 / mg/L 0.4436 / lbs/day
Oct 2018 Week 3 0.57 / mg/L 0.5896 / lbs/day
Jul 2018 Average 0.39 /7 mg/L 0.4436 / lbs/day
Oct 2018 Average 0.57 /7 mg/L 0.5896 / lbs/day
2018 Quarter 3 0.39 / mg/L 0.4436 / lbs/day
2018 Quarter 4 0.57 / mg/L 0.5896 / lbs/day
2018 2nd 6 Months(Avg) 0.48 / mg/L 0.5166 / lbs/day
2018 2nd 6...(Max) 0.57 / mg/L 0.5896 / lbs/day
2018 2nd 6...(Min) 0.39 / mg/L 0.4436 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
•
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
09/11/2018 S CreeRTPP12091118Se1 < 0.0025 / mg/L < 0.00285 / lbs/day
f
Sep 2018 Week 2 < 0.0025 / mg/L < 0.00285 / lbs/day
Sep 2018 Average < 0.0025 / mg/L < 0.00285 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.00285 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
10/09/2018 P CreeRTPP12100918P 0.000019 /0.000142 mg/L /
OTWHg
10/16/2018 S CreeRTPP12101618Se 0.000002 /0.000142 mg/L /
If
Oct 2018 Week 2 0.000019 / mg/L /
Oct 2018 Week 3 0.000002 / mg/L /
Oct 2018 Average 0.000011 / mg/L /
2018 Quarter 4 0.000011 / mg/L /
2018 2nd 6 Months(Avg) 0.000011 / mg/L /
2018 2nd 6...(Max) 0.000019 / mg/L /
2018 2nd 6...(Min) 0.000002 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/27/2018 P CreeRTPP12072718P < 0.001 / mg/L < 0.0011 / lbs/day
OTW
reeRTPP12091118Sel < 0.003 mg/L < 0.0029 / lbs/day
S C /
f
Jul 2018 Week 4 < 0.001 / mg/L < 0.0011 / lbs/day
Sep 2018 Week 2 < 0.003 / mg/L < 0.0029 / lbs/day
Jul2018 Average < 0.001 / mg/L < 0.0011 / lbs/day
Sep 2018 Average < 0.003 / mg/L < 0.0029 / lbs/day
2018 Quarter 3 < 0.002 / mg/L < 0.002 / lbs/day
2018 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0020 / lbs/day
2018 2nd 6...(Max) < 0.003 / mg/L < 0.0029 / lbs/day
2018 2nd 6...(Min) < 0.001 / mg/L < 0.0011 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
09/11/2018 S CreeRTPP12091118Se1 < 0.0025 / mg/L < 0.00285 / lbs/day
f
Sep 2018 Week 2 < 0.0025 / mg/L < 0.00285 / lbs/day
Sep 2018 Average < 0.0025 / mg/L < 0.00285 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.00285 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/27/2018 P CreeRTPP12072718P 2.2 / mg/L 2.446 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 3.9 / mg/L 4.034 / lbs/day
If
Jul 2018 Week 4 2.2 / mg/L 2.446 / lbs/day
Oct 2018 Week 3 3.9 / mg/L 4.034 / lbs/day
Jul 2018 Average 2.2 / mg/L 2.446 / lbs/day
Oct 2018 Average 3.9 / mg/L 4.034 / lbs/day
2018 Quarter 3 2.2 / mg/L 2.446 / lbs/day
2018 Quarter 4 3.9 / mg/L 4.034 / lbs/day
2018 2nd 6 Months(Avg) 3.0 / mg/L 3.240 / lbs/day
2018 2nd 6...(Max) 3.9 / mg/L 4.034 / lbs/day
2018 2nd 6...(Min) 2.2 / mg/L 2.446 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Oapt fall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/27/2018 P CreeRTPP12072718P 12.9 / mg/L 14.673 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 13.4 / mg/L 13.86 / lbs/day
if
Jul 2018 Week 4 12.9 / mg/L 14.673 / lbs/day
Oct 2018 Week 3 13.4 / mg/L 13.86 / lbs/day
Jul2018 Average 12.9 / mg/L 14.673 / lbs/day
Oct 2018 Average 13.4 / mg/L 13.86 / lbs/day
2018 Quarter 3 12.9 / mg/L 14.673 / lbs/day
2018 Quarter 4 13.4 / mg/L 13.86 / lbs/day
2018 2nd 6 Months(Avg) 13.15 / mg/L 14.267 / lbs/day
2018 2nd 6...(Max) 13.4 / mg/L 14.673 / lbs/day
2018 2nd 6...(Min) 12.9 / mg/L 13.860 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil &Grease,Total
07/27/2018 P CreeRTPP12072718P < 2.5 /200 mg/L < /
OTW
Jul 2018 Week 4 < 2.5 / mg/L s. /
Jul 2018 Average < 2.5 / mg/L /
2018 Quarter 3 < 2.5 / mg/L < /
2018 2nd 6 Months(Avg) < 2.5 / mg/L /
2018 2nd 6...(Max) < 2.5 / mg/L /
• 2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/27/2018 P CreeRTPP12072718P 8.6 /5.0- 10.5 SU /
OTW
09/11/2018 S CreeRTPP12091118Sel 6.7 /5.0- 10.5 SU /
f
09/25/2018 S CreeRTPP12092518Se 6.9 /5.0- 10.5 SU /
If
Monday,February25,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
pH
10/16/2018 S CreeRTPP12101618Se 6.6 /5.0- 10.5 SU /
if
11/15/2018 S CreeRTPP12111518Se1 9.1 /5.0- 10.5 SU /
f
11/30/2018 S CreeRTPP12113018Se 7.5 /5.0- 10.5 SU /
tf
Jul 2018 Week 4 8.6 / SU /
Sep 2018 Week 2 6.7 / SU /
Sep 2018 Week 4 6.9 / SU /
Oct 2018 Week 3 6.6 / SU /
Nov 2018 Week 3 9.1 / SU /
Nov 2018 Week 4 7.5 / SU /
Jul 2018 Average 8.6 / SU /
1 Sep 2018 Average 6.8 / SU /
Oct 2018 Average 6.6 / SU /
Nov 2018 Average 8.3 / SU /
2018 Quarter 3 7.4 / SU /
2018 Quarter 4 7.73 / SU /
2018 2nd 6 Months(Avg) 7.57 / SU /
2018 2nd 6...(Max) 9.1 / SU /
2018 2nd 6...(Min) 6.6 / SU /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 4 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
09/11/2018 S CreeRTPP12091118Sel < 0.005 / mg/L < 0.0057 / lbs/day
f
Sep 2018 Week 2 < 0.005 / mg/L < 0.0057 / lbs/day
Sep 2018 Average < 0.005 / mg/L < 0.0057 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.0057 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.005700 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.005700 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.005700 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 12

Cree. Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Out fall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Silver
09/11/2018 S CreeRTPP12091118Se1 < 0.0025 / mg/L < 0.00285 / lbs/day
f
Sep 2018 Week 2 < 0.0025 / mg/L < 0.00285 / lbs/day
Sep 2018 Average < 0.0025 / mg/L < 0.00285 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.00285 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.002850 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/27/2018 P CreeRTPP12072718P 27 /66 °C /
OTW
09/11/2018 S CreeRTPP12091118Sel 24.6 /66 °C /
f
09/25/2018 S CreeRTPP12092518Se 24.6 /66 °C /
If
11/15/2018 S CreeRTPP12111518Sel 20 /66 °C /
f
11/30/2018 S CreeRTPP12113018Se 20.4 /66 °C /
if
Jul 2018 Week 4 27 / °C /
Sep 2018 Week 2 24.6 / °C /
Sep 2018 Week 4 24.6 / °C /
Nov 2018 Week 3 20 / °C /
Nov 2018 Week 4 20.4 / °C /
Jul2018 Average 27 / °C /
Sep 2018 Average 24.6 / °C /
Nov 2018 Average 20.2 / °C /
2018 Quarter 3 25.4 / °C /
2018 Quarter 4 20.2 / °C /
2018 2nd 6 Months(Avg) 23.3 / °C /
2018 2nd 6...(Max) 27 / °C /
2018 2nd 6...(Min) 20 / °C /
2018 2nd 6...(Count) 5 / /
Sample Count: 5 Months Sampled: 3 Weeks Sampled: 5 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 12

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/27/2018 P CreeRTPP12072718P 10.7 / mg/L 12.171 / lbs/day
OTW
10/16/2018 S CreeRTPP12101618Se 9.5 / mg/L 9.826 / lbs/day
If
Jul 2018 Week 4 10.7 / mg/L 12.171 / lbs/day
Oct 2018 Week 3 9.5 / mg/L 9.826 / lbs/day
' Jul 2018 Average 10.7 / mg/L 12.171 / lbs/day
Oct 2018 Average 9.5 / mg/L 9.826 / lbs/day
2018 Quarter 3 10.7 / mg/L 12.171 / lbs/day
2018 Quarter 4 9.5 / mg/L 9.826 / lbs/day
2018 2nd 6 Months(Avg) 10.1 / mg/L 10.998 / lbs/day
2018 2nd 6...(Max) 10.7 / mg/L 12.171 / lbs/day
2018 2nd 6...(Min) 9.5 / mg/L 9.826 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/27/2018 P CreeRTPP12072718P 2.11 / mg/L 2.4 / lbs/day
OTW
Jul 2018 Week 4 2.11 / mg/L 2.4 / lbs/day
Jul2018 Average 2.11 / mg/L 2.4 / lbs/day
2018 Quarter 3 2.11 / mg/L 2.4 / lbs/day
2018 2nd 6 Months(Avg) 2.11 / mg/L 2.4 / lbs/day
2018 2nd 6...(Max) 2.11 / mg/L 2.4000 / lbs/day
2018 2nd 6...(Min) 2.11 / mg/L 2.4000 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TTO
12/21/2018 S CreeRTPP12122118Se 0.0089 / mg/L 0.00843 / lbs/day
If
Dec 2018 Week 3 0.0089 / mg/L 0.00843 / lbs/day
Dec 2018 Average 0.0089 / mg/L 0.00843 / lbs/day
2018 Quarter 4 0.0089 / mg/L 0.00843 / lbs/day
2018 2nd 6 Months(Avg) 0.0089 / mg/L 0.008430 / lbs/day
2018 2nd 6...(Max) 0.0089 / mg/L 0.008430 / lbs/day
2018 2nd 6...(Min) 0.0089 / mg/L 0.008430 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
09/11/2018 S CreeRTPP12091118Sel 0.131 / mg/L 0.149347 / lbs/day
f
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 11 of 12
_J

Cree, Inc (RTP)
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Sep 2018 Week 2 0.131 / mg/L 0.149347 / lbs/day
Sep 2018 Average 0.131 / mg/L 0.149347 / lbs/day
2018 Quarter 3 0.131 / mg/L 0.149347 / lbs/day
2018 2nd 6 Months(Avg) 0.131 / mg/L 0.149347 / lbs/day
2018 2nd 6...(Max) 0.131 / mg/L 0.149347 / lbs/day
2018 2nd 6...(Min) 0.131 / mg/L 0.149347 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Monday,February 25,2019 *Indicates Violation **Indicates TRC Violation Page 12 of 12

JMC (USA). Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/07/2018 S JMC080718Self 0.51 / mg/L 0.005087 / lbs/day
09/27/2018 P JMC092718POTW 0.856 / mg/L 0.009859 / lbs/day
Aug 2018 Week 1 0.51 / mg/L 0.005087 / lbs/day
Sep 2018 Week 4 0.856 / mg/L 0.009859 / lbs/day
Aug 2018 Average 0.51 / mg/L 0.005087 / lbs/day
Sep 2018 Average 0.856 / mg/L 0.009859 / lbs/day
2018 Quarter 3 0.683 / mg/L 0.007473 / lbs/day
2018 2nd 6 Months(Avg) 0.683 / mg/L 0.007473 / lbs/day
2018 2nd 6...(Max) 0.856 / mg/L 0.009859 / lbs/day
2018 2nd 6...(Min) 0.51 / mg/L 0.005087 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/07/2018 S JMC080718Self 2.2 / mg/L 0.0219 / lbs/day
09/27/2018 P JMC092718POTW 3.6 / mg/L 0.0415 / lbs/day
Aug 2018 Week 1 2.2 / mg/L 0.0219 / lbs/day
Sep 2018 Week 4 3.6 / mg/L 0.0415 / lbs/day
Aug 2018 Average 2.2 / mg/L 0.0219 / lbs/day
Sep 2018 Average 3.6 / mg/L 0.0415 / lbs/day
2018 Quarter 3 2.9 / mg/L 0.0317 / lbs/day
2018 2nd 6 Months(Avg) 2.9 / mg/L 0.0317 / lbs/day
2018 2nd 6...(Max) 3.6 / mg/L 0.0415 / lbs/day
2018 2nd 6...(Min) 2.2 / mg/L 0.0219 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S JMC0718Flow 0.000407 / MGD /
08/31/2018 S JMC0818Flow 0.000257 / MGD /
09/30/2018 S JMC0918Flow 0.000272 / MGD /
10/31/2018 S JMC1018F1ow 0.000131 / MGD /
11/30/2018 S JMC1118Flow 0.000161 / MGD /
12/31/2018 S JMC1218Flow 0.000228 / MGD /
Jul 2018 Week 4 0.000407 / MGD /
Aug 2018 Week 4 0.000257 / MGD /
Sep 2018 Week 4 0.000272 / MGD /
Oct 2018 Week 4 0.000131 / MGD /
Nov 2018 Week 4 0.000161 / MGD /
Dec 2018 Week 4 0.000228 / MGD /
Jul 2018 Average 0.000407 /0.01 MGD / 1
Aug 2018 Average 0.000257 /0.01 MGD /
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2018 Average 0.000272 /0.01 MGD /
Oct 2018 Average 0.000131 /0.01 MGD /
Nov 2018 Average 0.000161 /0.01 MGD /
Dec 2018 Average 0.000228 /0.01 MGD /
2018 Quarter 3 0.000312 / MGD /
2018 Quarter 4 0.000173 / MGD /
2018 2nd 6 Months(Avg) 0.000243 / MGD /
2018 2nd 6...(Max) 0.000407 / MGD /
2018 2nd 6...(Min) 0.000131 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/07/2018 S JMC080718Self < 0.0025 /0.04 mg/L < 0.000025 / lbs/day
09/27/2018 P JMC092718POTW < 0.0005 /0.04 mg/L < 0.000006 / lbs/day
Aug 2018 Week 1 < 0.0025 / mg/L < 0.000025 / lbs/day
Sep 2018 Week 4 < 0.0005 / mg/L < 0.000006 / lbs/day
Aug 2018 Average < 0.0025 /0.025 mg/L < 0.000025 / lbs/day
Sep 2018 Average < 0.0005 /0.025 mg/L < 0.000006 / lbs/day
2018 Quarter 3 < 0.0015 / mg/L < 0.000015 / lbs/day
2018 2nd 6 Months(Avg) < 0.0015 / mg/L < 0.000015 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.000025 / lbs/day
2018 2nd 6...(Min) < 0.0005 / mg/L < 0.000006 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 10

JMC (USA). Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/07/2018 S JMC080718Se1f 3600 / mg/L 35.9087 / lbs/day
09/27/2018 P JMC092718POTW 80.2 / mg/L 0.9237 / lbs/day
Aug 2018 Week 1 3600 / mg/L 35.9087 / lbs/day
Sep 2018 Week 4 80.2 / mg/L 0.9237 / lbs/day
Aug 2018 Average 3600 / mg/L 35.9087 / lbs/day
Sep 2018 Average 80.2 / mg/L 0.9237 / lbs/day
2018 Quarter 3 1840.1 / mg/L 18.4162 / lbs/day
2018 2nd 6 Months(Avg) 1840.1 / mg/L 18.4162 / lbs/day
2018 2nd 6...(Max) 3600 / mg/L 35.9087 / lbs/day
2018 2nd 6...(Min) 80.2 / mg/L 0.9237 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
08/07/2018 S JMC080718Self 0.022 / 1 mg/L 0.000219 / lbs/day
09/27/2018 P JMC092718POTW < 0.01 / 1 mg/L < 0.000115 / lbs/day
Aug 2018 Week 1 0.022 / mg/L 0.000219 / lbs/day
Sep 2018 Week 4 < 0.01 / mg/L < 0.000115 / lbs/day
Aug 2018 Average 0.022 /0.650 mg/L 0.000219 / lbs/day
Sep 2018 Average < 0.01 /0.650 mg/L < 0.000115 / lbs/day
2018 Quarter 3 < 0.016 / mg/L < 0.000167 / lbs/day
2018 2nd 6 Months(Avg) < 0.016 / mg/L < 0.000167 / lbs/day
2018 2nd 6...(Max) 0.022 / mg/L 0.000219 / lbs/day
2018 2nd 6...(Min) < 0.01 / mg/L < 0.000115 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/07/2018 S JMC080718Self 0.073 /1 mg/L 0.000728 / lbs/day
09/27/2018 P JMC092718POTW 0.158 /1 mg/L 0.00182 / lbs/day
Aug 2018 Week 1 0.073 / mg/L 0.000728 / lbs/day
Sep 2018 Week 4 0.158 / mg/L 0.00182 / lbs/day
Aug 2018 Average 0.073 /0.7 mg/L 0.000728 / lbs/day
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

JMC (USA). Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Sep 2018 Average 0.158 /0.7 mg/L 0.00182 / lbs/day
2018 Quarter 3 0.116 / mg/L 0.001274 / lbs/day
2018 2nd 6 Months(Avg) 0.116 / mg/L 0.001274 / lbs/day
2018 2nd 6...(Max) 0.158 / mg/L 0.001820 / lbs/day
2018 2nd 6...(Min) 0.073 / mg/L 0.000728 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/07/2018 S JMC080718Self 0.012 /0.04 mg/L 0.00012 / lbs/day
09/27/2018 P JMC092718POTW < 0.003 /0.04 mg/L < 0.000029 / lbs/day
Aug 2018 Week 1 0.012 / mg/L 0.00012 / lbs/day
Sep 2018 Week 4 < 0.003 / mg/L < 0.000029 / lbs/day
Aug 2018 Average 0.012 /0.03 mg/L 0.00012 / lbs/day
Sep 2018 Average < 0.003 /0.03 mg/L < 0.000029 / lbs/day
2018 Quarter 3 < 0.007 / mg/L < 0.000074 / lbs/day
2018 2nd 6 Months(Avg) < 0.007 / mg/L < 0.000074 / lbs/day
2018 2nd 6...(Max) 0.012 / mg/L 0.000120 / lbs/day
2018 2nd 6...(Min) < 0.003 / mg/L < 0.000029 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/07/2018 S JMC080718Self < 0.1 / mg/L < 0.001 / lbs/day
09/27/2018 P JMC092718POTW < 0.05 / mg/L < 0.0006 / lbs/day
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Aug 2018 Week 1 < 0.1 / mg/L < 0.001 / lbs/day
Sep 2018 Week 4 < 0.05 / mg/L < 0.0006 / lbs/day
Aug 2018 Average < 0.1 / mg/L < 0.001 / lbs/day
Sep 2018 Average < 0.05 / mg/L < 0.0006 / lbs/day
2018 Quarter 3 < 0.08 / mg/L < 0.0008 / lbs/day
2018 2nd 6 Months(Avg) < 0.08 / mg/L < 0.0008 / lbs/day
2018 2nd 6...(Max) < 0.1 / mg/L < 0.0010 / lbs/day
2018 2nd 6...(Min) < 0.05 / mg/L < 0.0006 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/07/2018 S JMC080718Self 0.0093 /0.260 mg/L 0.000093 / lbs/day
09/27/2018 P JMC092718POTW 0.0077 /0.260 mg/L 0.000088 / lbs/day
Aug 2018 Week 1 0.0093 / mg/L 0.000093 / lbs/day
Sep 2018 Week 4 0.0077 / mg/L 0.000088 / lbs/day
Aug 2018 Average 0.0093 /0.160 mg/L 0.000093 / lbs/day
Sep 2018 Average 0.0077 /0.160 mg/L 0.000088 / lbs/day
2018 Quarter 3 0.0085 / mg/L 0.000091 / lbs/day
2018 2nd 6 Months(Avg) 0.0085 / mg/L 0.000091 / lbs/day
2018 2nd 6...(Max) 0.0093 / mg/L 0.000093 / lbs/day
2018 2nd 6...(Min) 0.0077 / mg/L 0.000088 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/07/2018 S JMC080718Self 0.000003 /0.000142 mg/L /
12/13/2018 P JMC121318POTWHg 0.00001 /0.000142 mg/L /
Aug 2018 Week 1 0.000003 / mg/L /
Dec 2018 Week 2 0.00001 / mg/L /
Aug 2018 Average 0.000003 / mg/L /
Dec 2018 Average 0.00001 / mg/L /
2018 Quarter 3 0.000003 / mg/L /
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
Mercury-LL
2018 Quarter 4 0.00001 / mg/L /
2018 2nd 6 Months(Avg) 0.000006 / mg/L /
2018 2nd 6...(Max) 0.000010 / mg/L /
2018 2nd 6...(Min) 0.000003 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/07/2018 S JMC080718Self 0.012 /0.3 mg/L 0.00012 / lbs/day
09/27/2018 P JMC092718POTW 0.0471 /0.3 mg/L 0.000542 / lbs/day
Aug 2018 Week 1 0.012 / mg/L 0.00012 / lbs/day
Sep 2018 Week 4 0.0471 / mg/L 0.000542 / lbs/day
Aug 2018 Average 0.012 /0.2 mg/L 0.00012 / lbs/day
Sep 2018 Average 0.0471 /0.2 mg/L 0.000542 / lbs/day
2018 Quarter 3 0.0296 / mg/L 0.000331 / lbs/day
2018 2nd 6 Months(Avg) 0.0296 / mg/L 0.000331 / lbs/day
2018 2nd 6...(Max) 0.0471 / mg/L 0.000542 / lbs/day
2018 2nd 6...(Min) 0.012 / mg/L 0.000120 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/07/2018 S JMC080718Self 79 / mg/L 0.788 / lbs/day
09/27/2018 P JMC092718POTW 150 / mg/L 1.728 / lbs/day
Aug 2018 Week 1 79 / mg/L 0.788 / lbs/day
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
Sep 2018 Week 4 150 / mg/L 1.728 / lbs/day
Aug 2018 Average 79 / mg/L 0.788 / lbs/day
Sep 2018 Average 150 / mg/L 1.728 / lbs/day
2018 Quarter 3 114.5 / mg/L 1.258 / lbs/day
' 2018 2nd 6 Months(Avg) 114.5 / mg/L 1.258 / lbs/day
2018 2nd 6...(Max) 150 / mg/L 1.728 / lbs/day
2018 2nd 6...(Min) 79 / mg/L 0.788 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/07/2018 S JMC080718Self 79 / mg/L 0.788 / lbs/day
09/27/2018 P JMC092718POTW 155 / mg/L 1.785 / lbs/day
Aug 2018 Week 1 79 / mg/L 0.788 / lbs/day
Sep 2018 Week 4 155 / mg/L 1.785 / lbs/day
Aug 2018 Average 79 / mg/L 0.788 / lbs/day
Sep 2018 Average 155 / mg/L 1.785 / lbs/day
2018 Quarter 3 117 / mg/L 1.287 / lbs/day
2018 2nd 6 Months(Avg) 117 / mg/L 1.287 / lbs/day
2018 2nd 6...(Max) 155 / mg/L 1.785 / lbs/day
2018 2nd 6...(Min) 79 / mg/L 0.788 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
09/27/2018 P JMC092718POTW < 2.5 /200 mg/L < /
Sep 2018 Week 4 < 2.5 / mg/L < /
Sep 2018 Average < 2.5 / mg/L < /
2018 Quarter 3 < 2.5 / mg/L < /
2018 2nd 6 Months(Avg) < 2.5 / mg/L < /
2018 2nd 6...(Max) < 2.5 / mg/L /
2018 2nd 6...(Min) 2.5 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : I
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/07/2018 S JMC080718SeIf 7.3 /6- 10.5 SU /
09/27/2018 P JMC092718POTW 8.4 /6- 10.5 SU /
09/27/2018 S JMC092718SeIf 8.1 /6- 10.5 SU /
Aug 2018 Week 1 7.3 / SU /
Sep 2018 Week 4 8.25 / SU /
Aug 2018 Average 7.3 / SU /
Sep 2018 Average 8.25 / SU /
2018 Quarter 3 7.93 / SU /
2018 2nd 6 Months(Avg) 7.93 / SU /
2018 2nd 6...(Max) 8.4 / SU /
2018 2nd 6...(Min) 7.3 / SU /
2018 2nd 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/07/2018 S JMC080718Self < 0.0025 /0.160 mg/L < 0.000025 / lbs/day
09/27/2018 P JMC092718POTW < 0.0025 /0.160 mg/L < 0.000029 / lbs/day
Aug 2018 Week I < 0.0025 / mg/L < 0.000025 / lbs/day
Sep 2018 Week 4 < 0.0025 / mg/L < 0.000029 / lbs/day
Aug 2018 Average < 0.0025 /0.090 mg/L < 0.000025 / lbs/day
Sep 2018 Average < 0.0025 /0.090 mg/L < 0.000029 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.000027 / lbs/day
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.000027 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.000029 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.000025 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/27/2018 P JMC092718POTW 24 /66 °C /
Sep 2018 Week 4 24 / °C /
Sep 2018 Average 24 / °C /
2018 Quarter 3 24 / °C /
2018 2nd 6 Months(Avg) 24 / °C /
2018 2nd 6...(Max) 24 / °C /
2018 2nd 6...(Min) 24 / °C /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/07/2018 S JMC080718Self < 0.25 / mg/L < 0.002 / lbs/day
09/27/2018 P JMC092718POTW 4.88 / mg/L 0.056 / lbs/day
Aug 2018 Week 1 < 0.25 / mg/L < 0.002 / lbs/day
Sep 2018 Week 4 4.88 / mg/L 0.056 / lbs/day
Aug 2018 Average < 0.25 / mg/L < 0.002 / lbs/day
Sep 2018 Average 4.88 / mg/L 0.056 / lbs/day
2018 Quarter 3 < 2.57 / mg/L < 0.029 / lbs/day
2018 2nd 6 Months(Avg) < 2.57 / mg/L < 0.029 / lbs/day
2018 2nd 6...(Max) 4.88 / mg/L 0.056 / lbs/day
2018 2nd 6...(Min) < 0.25 / mg/L < 0.002 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/07/2018 S JMC080718Self 0.17 /0.9 mg/L 0.001696 / lbs/day
09/27/2018 P JMC092718POTW 0.05 /0.9 mg/L 0.000577 / lbs/day
Aug 2018 Week 1 0.17 / mg/L 0.001696 / lbs/day
Sep 2018 Week 4 0.05 / mg/L 0.000577 / lbs/day
Aug 2018 Average 0.17 /0.56 mg/L 0.001696 / lbs/day
Sep 2018 Average 0.05 /0.56 mg/L 0.000577 / lbs/day
2018 Quarter 3 0.11 / mg/L 0.001136 / lbs/day
2018 2nd 6 Months(Avg) 0.110 / mg/L 0.001136 / lbs/day
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
2018 2nd 6...(Max) 0.17 / mg/L 0.001696 / lbs/day
2018 2nd 6...(Min) 0.050 / mg/L 0.000577 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Tuesday,February 26,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/20/2018 S Micross072018Se1f 4 / mg/L 1.4501 / lbs/day
10/30/2018 P Micross103018POTW 3.6 / mg/L 0.9453 / lbs/day
Jul 2018 Week 3 4 / mg/L 1.4501 / lbs/day
Oct 2018 Week 4 3.6 / mg/L 0.9453 / lbs/day
Jul2018 Average 4 / mg/L 1.4501 / lbs/day
Oct 2018 Average 3.6 / mg/L 0.9453 / lbs/day
2018 Quarter 3 4 / mg/L 1.4501 / lbs/day
2018 Quarter 4 3.6 / mg/L 0.9453 / lbs/day
2018 2nd 6 Months(Avg) 3.8 / mg/L 1.1977 / lbs/day
2018 2nd 6...(Max) 4 / mg/L 1.4501 / lbs/day
2018 2nd 6...(Min) 3.6 / mg/L 0.9453 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Micross0718Flow 0.05087 /0.100 MGD /
08/31/2018 S Micross0818Flow 0.046017 /0.100 MGD /
09/30/2018 S Micross0918Flow 0.046736 /0.100 MGD /
10/31/2018 S Micross1018Flow 0.040111 /0.100 MGD /
11/30/2018 S Micross1118Flow 0.027729 /0.100 MGD /
12/31/2018 S Micross1218Flow 0.020834 /0.100 MGD /
Jul 2018 Week 4 0.05087 / MGD /
Aug 2018 Week 4 0.046017 / MGD /
Sep 2018 Week 4 0.046736 / MGD /
Oct 2018 Week 4 0.040111 / MGD /
Nov 2018 Week 4 0.027729 / MGD /
Dec 2018 Week 4 0.020834 / MGD /
Jul 2018 Average 0.05087 /0.075 MGD /
Aug 2018 Average 0.046017 /0.075 MGD /
Sep 2018 Average 0.046736 /0.075 MGD /
Oct 2018 Average 0.040111 /0.075 MGD /
Nov 2018 Average 0.027729 /0.075 MGD /
Dec 2018 Average 0.020834 /0.075 MGD /
2018 Quarter 3 0.047874 / MGD /
2018 Quarter 4 0.029558 / MGD /
2018 2nd 6 Months(Avg) 0.038716 / MGD /
2018 2nd 6...(Max) 0.05087 / MGD /
2018 2nd 6...(Min) 0.020834 / MGD /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk '001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/20/2018 S Micross072018Self < 0.0005 / mg/L < 0.000181 / lbs/day
Jul 2018 Week 3 < 0.0005 / mg/L < 0.000181 / lbs/day
Jul2018 Average < 0.0005 / mg/L < 0.000181 / lbs/day
2018 Quarter 3 < 0.0005 / mg/L < 0.000181 / lbs/day
2018 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.000181 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.000181 / lbs/day
2018 2nd 6...(Min) < 0.0005 / mg/L < 0.000181 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/20/2018 S Micross072018Self 25 / mg/L 9.0629 / lbs/day
10/30/2018 P Micross103018POTW 25.6 / mg/L 6.7224 / lbs/day
Jul2018 Week 3 25 / mg/L 9.0629 / lbs/day
Oct 2018 Week 4 25.6 / mg/L 6.7224 / lbs/day
Jul 2018 Average 25 / mg/L 9.0629 / lbs/day
Oct 2018 Average 25.6 / mg/L 6.7224 / lbs/day
2018 Quarter 3 25 / mg/L 9.0629 / lbs/day
2018 Quarter 4 25.6 / mg/L 6.7224 / lbs/day
2018 2nd 6 Months(Avg) 25.3 / mg/L 7.8926 / lbs/day
2018 2nd 6...(Max) 25.6 / mg/L 9.0629 / lbs/day
2018 2nd 6...(Min) 25 / mg/L 6.7224 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/20/2018 S Micross072018Self 0.029 / mg/L 0.010332 / lbs/day
10/30/2018 P Micross103018POTW 0.057 / mg/L 0.015047 / lbs/day
Jul 2018 Week 3 0.029 / mg/L 0.010332 / lbs/day
Oct 2018 Week 4 0.057 / mg/L 0.015047 / lbs/day
Jul2018 Average 0.029 / mg/L 0.010332 / lbs/day
Oct 2018 Average 0.057 / mg/L 0.015047 / lbs/day
2018 Quarter 3 0.029 / mg/L 0.010332 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
2018 Quarter 4 0.057 / mg/L 0.015047 / lbs/day
2018 2nd 6 Months(Avg) 0.043 / mg/L 0.012689 / lbs/day
2018 2nd 6...(Max) 0.057 / mg/L 0.015047 / lbs/day
2018 2nd 6...(Min) 0.029 / mg/L 0.010332 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/20/2018 S Micross072018Self 0.012 / mg/L 0.00435 / lbs/day
10/30/2018 P Micross103018POTW 0.006 / mg/L 0.001576 / lbs/day
Jul 2018 Week 3 0.012 / mg/L 0.00435 / lbs/day
Oct 2018 Week 4 0.006 / mg/L 0.001576 / lbs/day
Jul2018 Average 0.012 / mg/L 0.00435 / lbs/day
Oct 2018 Average 0.006 / mg/L 0.001576 / lbs/day
2018 Quarter 3 0.012 / mg/L 0.00435 / lbs/day
2018 Quarter 4 0.006 / mg/L 0.001576 / lbs/day
2018 2nd 6 Months(Avg) 0.009 / mg/L 0.002963 / lbs/day
2018 2nd 6...(Max) 0.012 / mg/L 0.004350 / lbs/day
2018 2nd 6...(Min) 0.006 / mg/L 0.001576 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/20/2018 S Micross072018Self 1.7 /8 mg/L 0.6163 / lbs/day
10/30/2018 P Micross103018POTW 1.47 /8 mg/L 0.386 / lbs/day
Jul2018 Week 3 1.7 / mg/L 0.6163 / lbs/day
Oct 2018 Week 4 1.47 / mg/L 0.386 / lbs/day
Jul 2018 Average 1.7 /6 mg/L 0.6163 / lbs/day
Oct 2018 Average 1.47 /6 mg/L 0.386 / lbs/day
2018 Quarter 3 1.7 / mg/L 0.6163 / lbs/day
2018 Quarter 4 1.47 / mg/L 0.386 / lbs/day
2018 2nd 6 Months(Avg) 1.59 / mg/L 0.5011 / lbs/day
2018 2nd 6...(Max) 1.7 / mg/L 0.6163 / lbs/day
2018 2nd 6...(Min) 1.47 / mg/L 0.3860 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/20/2018 S Micross072018Self < 0.005 / mg/L < 0.001813 / lbs/day
10/30/2018 P Micross103018POTW 0.011 / mg/L 0.002889 / lbs/day
Jul2018 Week 3 < 0.005 / mg/L < 0.001813 / lbs/day
Oct 2018 Week 4 0.011 / mg/L 0.002889 / lbs/day
Jul2018 Average < 0.005 / mg/L < 0.001813 / lbs/day
Oct 2018 Average 0.011 / mg/L 0.002889 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.001813 / lbs/day
2018 Quarter 4 0.011 / mg/L 0.002889 / lbs/day
2018 2nd 6 Months(Avg) < 0.008 / mg/L < 0.002351 / lbs/day
2018 2nd 6...(Max) 0.011 / mg/L 0.002889 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.001813 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/13/2018 S Micross071318SelfHg 0.00001 /0.000142 mg/L /
10/29/2018 P Micross102918POTW 0.000004 /0.000142 mg/L /
Hg
Jul 2018 Week 2 0.00001 / mg/L /
Oct 2018 Week 4 0.000004 / mg/L /
Jul 2018 Average 0.00001 / mg/L /
Oct 2018 Average 0.000004 / mg/L /
2018 Quarter 3 0.00001 / mg/L /
2018 Quarter 4 0.000004 / mg/L /
2018 2nd 6 Months(Avg) 0.000007 / mg/L /
2018 2nd 6...(Max) 0.000010 / mg/L /
2018 2nd 6...(Min) 0.000004 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/20/2018 S Micross072018Self 0.011 / mg/L 0.0038 / lbs/day
Jul 2018 Week 3 0.011 / mg/L 0.0038 / lbs/day
Jul2018 Average 0.011 / mg/L 0.0038 / lbs/day
2018 Quarter 3 0.011 / mg/L 0.0038 / lbs/day
2018 2nd 6 Months(Avg) 0.011 / mg/L 0.0038 / lbs/day
2018 2nd 6...(Max) 0.011 / mg/L 0.0038 / lbs/day
2018 2nd 6...(Min) 0.011 / mg/L 0.0038 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/20/2018 S Micross072018Self 0.0056 / mg/L 0.002037 / lbs/day
10/30/2018 P Micross103018POTW 0.0444 / mg/L 0.011659 / lbs/day
Jul 2018 Week 3 0.0056 / mg/L 0.002037 / lbs/day
Oct 2018 Week 4 0.0444 / mg/L 0.011659 / lbs/day
Jul 2018 Average 0.0056 / mg/L 0.002037 / lbs/day
Oct 2018 Average 0.0444 / mg/L 0.011659 / lbs/day
2018 Quarter 3 0.0056 / mg/L 0.002037 / lbs/day
2018 Quarter 4 0.0444 / mg/L 0.011659 / lbs/day
2018 2nd 6 Months(Avg) 0.0250 / mg/L 0.006848 / lbs/day
2018 2nd 6...(Max) 0.0444 / mg/L 0.011659 / lbs/day
2018 2nd 6...(Min) 0.0056 / mg/L 0.002037 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/20/2018 S Micross072018Self 0.5 / mg/L 0.189 / lbs/day
10/30/2018 P Micross103018POTW 1.5 / mg/L 0.391 / lbs/day
Jul2018 Week 3 0.5 / mg/L 0.189 / lbs/day
Oct 2018 Week 4 1.5 / mg/L 0.391 / lbs/day
Jul2018 Average 0.5 / mg/L 0.189 / lbs/day
Oct 2018 Average 1.5 / mg/L 0.391 / lbs/day
2018 Quarter 3 0.5 / mg/L 0.189 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2018 Quarter 4 1.5 / mg/L 0.391 / lbs/day
2018 2nd 6 Months(Avg) 1.0 / mg/L 0.290 / lbs/day
2018 2nd 6...(Max) 1.5 / mg/L 0.391 / lbs/day
2018 2nd 6...(Min) 0.5 / mg/L 0.189 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/20/2018 S Micross072018Se1f 8.42 / mg/L 3.052 / lbs/day
10/30/2018 P Micross103018POTW 11.2 / mg/L 2.941 / lbs/day
Jul2018 Week 3 8.42 / mg/L 3.052 / lbs/day
Oct 2018 Week 4 11.2 / mg/L 2.941 / lbs/day
Jul 2018 Average 8.42 / mg/L 3.052 / lbs/day
Oct 2018 Average 11.2 / mg/L 2.941 / lbs/day
2018 Quarter 3 8.42 / mg/L 3.052 / lbs/day
2018 Quarter 4 11.2 / mg/L 2.941 / lbs/day
2018 2nd 6 Months(Avg) 9.81 / mg/L 2.997 / lbs/day
2018 2nd 6...(Max) 11.2 / mg/L 3.052 / . lbs/day
2018 2nd 6...(Min) 8.42 / mg/L 2.941 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/30/2018 P Micross103018POTW < 2.5 /200 mg/L /
Oct 2018 Week 4 < 2.5 / mg/L /
Oct 2018 Average < 2.5 / mg/L < /
2018 Quarter 4 < 2.5 / mg/L /
2018 2nd 6 Months(Avg) < 2.5 / mg/L /
2018 2nd 6...(Max) < 2.5 / mg/L /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Micross Advanced Interconnect Technoloey, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/20/2018 S Micross072018Self 7 /5.5- 10.5 SU /
10/30/2018 P Micross103018POTW 7.3 /5.5- 10.5 SU /
Jul 2018 Week 3 7 / SU /
Oct 2018 Week 4 7.3 / SU /
Jul2018 Average 7 / SU /
Oct 2018 Average 7.3 / SU /
2018 Quarter 3 7 / SU /
2018 Quarter 4 7.3 / SU /
2018 2nd 6 Months(Avg) 7.15 / SU /
2018 2nd 6...(Max) 7.3 / SU /
2018 2nd 6...(Min) 7 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
07/20/2018 S Micross072018Se1f < 0.005 / mg/L < 0.001813 / lbs/day
Jul2018 Week 3 < 0.005 / mg/L < 0.001813 / lbs/day
Jul2018 Average < 0.005 / mg/L < 0.001813 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0.001813 / lbs/day
2018 2nd 6 Months(Avg) < 0.005 / mg/L < 0.001813 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.001813 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0.001813 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/20/2018 S Micross072018Self 23.6 /66 °C /
10/30/2018 P Micross103018POTW 20 /66 °C /
Jul 2018 Week 3 23.6 / °C /
Oct 2018 Week 4 20 / °C /
Jul2018 Average 23.6 / °C /
Oct 2018 Average 20 / °C /
2018 Quarter 3 23.6 / °C /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2018 Quarter 4 20 / °C /
2018 2nd 6 Months(Avg) 21.8 / °C /
2018 2nd 6...(Max) 23.6 / °C /
2018 2nd 6...(Min) 20 / °C /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
07/20/2018 S Micross072018Self < 0.005 / mg/L < 0.001812574 / lbs/day
10/30/2018 P Micross103018POTW < 0.013 / mg/L < 0.003282416 / lbs/day
Jul 2018 Week 3 < 0.005 / mg/L < 0 / lbs/day
Oct 2018 Week 4 < 0.013 / mg/L < 0 / lbs/day
Jul 2018 Average < 0.005 / mg/L < 0 / lbs/day
Oct 2018 Average < 0.013 / mg/L < 0 / lbs/day
2018 Quarter 3 < 0.005 / mg/L < 0 / lbs/day
2018 Quarter 4 < 0.013 / mg/L < 0 / lbs/day
2018 2nd 6 Months(Avg) < 0.009 / mg/L < 0 / lbs/day
2018 2nd 6...(Max) < 0.013 / mg/L < 0 / lbs/day
2018 2nd 6...(Min) < 0.005 / mg/L < 0 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
1 TKN
07/20/2018 S Micross072018Self 7.9 / mg/L 2.864 / lbs/day
10/30/2018 P Micross103018POTW 9.71 / mg/L 2.55 / lbs/day
Jul 2018 Week 3 7.9 / mg/L 2.864 / lbs/day
Oct 2018 Week 4 9.71 / mg/L 2.55 / lbs/day
Jul 2018 Average 7.9 / mg/L 2.864 / lbs/day
Oct 2018 Average 9.71 / mg/L 2.55 / lbs/day
2018 Quarter 3 7.9 / mg/L 2.864 / lbs/day
2018 Quarter 4 9.71 / mg/L 2.55 / lbs/day
2018 2nd 6 Months(Avg) 8.81 / mg/L 2.707 / lbs/day
2018 2nd 6...(Max) 9.71 / mg/L 2.864 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2018 2nd 6...(Min) 7.9 / mg/L 2.550 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TTO
12/19/2018 P Micross121918POTW 0.0059 /0.670 mg/L /
Dec 2018 Week 3 0.0059 / mg/L /
Dec 2018 Average 0.0059 / mg/L /
2018 Quarter 4 0.0059 / mg/L /
2018 2nd 6 Months(Avg) 0.0059 / mg/L /
2018 2nd 6...(Max) 0.0059 / mg/L /
2018 2nd 6...(Min) 0.0059 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/20/2018 S Micross072018Se1f 0.294 / mg/L 0.106579 / lbs/day
Jul 2018 Week 3 0.294 / mg/L 0.106579 / lbs/day
Jul 2018 Average 0.294 / mg/L 0.106579 / lbs/day
2018 Quarter 3 0.294 / mg/L 0.106579 / lbs/day
2018 2nd 6 Months(Avg) 0.294 / mg/L 0.106579 / lbs/day
2018 2nd 6...(Max) 0.294 / mg/L 0.106579 / lbs/day
2018 2nd 6...(Min) 0.294 / mg/L 0.106579 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Novan, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
10/05/2018 P Novan100518POTW 0.338 / mg/L /
Oct 2018 Week 1 0.338 / mg/L /
Oct 2018 Average 0.338 / mg/L /
2018 Quarter 4 0.338 / mg/L /
2018 2nd 6 Months(Avg) 0.338 / mg/L /
2018 2nd 6...(Max) 0.338 / mg/L /
2018 2nd 6...(Min) 0.338 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Novan0718F1ow 0.000388 / MGD /
08/31/2018 S Novan0818Flow 0.00048 / MGD /
09/30/2018 S Novan0918Flow 0.000427 / MGD /
10/30/2018 S Novan1018Flow 0.000542 / MGD /
11/30/2018 S Novan1118Flow 0.014037 / MGD /
12/31/2018 S Novan1218Flow 0.000335 / MGD /
Jul 2018 Week 4 0.000388 / MGD /
Aug 2018 Week 4 0.00048 / MGD /
Sep 2018 Week 4 0.000427 / MGD /
Oct 2018 Week 4 0.000542 / MGD /
Nov 2018 Week 4 0.014037 / MGD /
Dec 2018 Week 4 0.000335 / MGD /
Jul 2018 Average 0.000388 /0.020 MGD /
Aug 2018 Average 0.00048 /0.020 MGD /
Sep 2018 Average 0.000427 / MGD /
Oct 2018 Average 0.000542 / MGD /
Nov 2018 Average 0.014037 / MGD /
Dec 2018 Average 0.000335 / MGD /
2018 Quarter 3 0.000427 / MGD /
2018 Quarter 3 0.000434 / MGD /
2018 Quarter 3 0.000427 / MGD /
2018 Quarter 3 0.000434 / MGD /
2018 Quarter 4 0.004971 / MGD /
2018 2nd 6 Months(Avg) 0.002701 / MGD /
2018 2nd 6...(Max) 0.014037 / MGD /
2018 2nd 6...(Min) 0.000335 / MGD /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 7

Novan Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/20/2018 S Novan082018Se1f < 0.00008 / mg/L < /
10/05/2018 P Novan100518POTW 0.0029 / mg/L /
Aug 2018 Week 3 < 0.00008 / mg/L < /
Oct 2018 Week 1 0.0029 / mg/L /
Aug 2018 Average < 0.00008 / mg/L < /
Oct 2018 Average 0.0029 / mg/L /
2018 Quarter 3 < 0.00008 / mg/L < /
2018 Quarter 4 0.0029 / mg/L /
2018 2nd 6 Months(Avg) < 0.00149 / mg/L < /
2018 2nd 6...(Max) 0.0029 / mg/L /
2018 2nd 6...(Min) < 0.00008 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD •
08/20/2018 S Novan082018Se1f 922 / mg/L /
10/05/2018 P Novan100518POTW 1050 / mg/L /
Aug 2018 Week 3 922 / mg/L /
Oct 2018 Week 1 1050 / mg/L /
Aug 2018 Average 922 / mg/L /
Oct 2018 Average 1050 / mg/L /
2018 Quarter 3 922 / mg/L /
2018 Quarter 4 1050 / mg/L /
2018 2nd 6 Months(Avg) 986 / mg/L /
2018 2nd 6...(Max) 1050 / mg/L /
2018 2nd 6...(Min) 922 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/20/2018 S Novan082018Se1f 0.147 / mg/L /
10/05/2018 P Novan100518POTW 0.706 / mg/L /
Aug 2018 Week 3 0.147 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 7

Nova'', Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Oct 2018 Week 1 0.706 / mg/L /
Aug 2018 Average 0.147 / mg/L /
Oct 2018 Average 0.706 / mg/L /
2018 Quarter 3 0.147 / mg/L /
2018 Quarter 4 0.706 / mg/L /
2018 2nd 6 Months(Avg) 0.427 / mg/L /
2018 2nd 6...(Max) 0.706 / mg/L /
2018 2nd 6...(Min) 0.147 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
10/05/2018 P Novan100518POTW < 0.003 / mg/L < /
Oct 2018 Week 1 < 0.003 / mg/L < /
Oct 2018 Average < 0.003 / mg/L < /
2018 Quarter 4 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
10/05/2018 P Novan100518POTW < 0.003 / mg/L < /
Oct 2018 Week 1 < 0.003 / mg/L < /
Oct 2018 Average < 0.003 / mg/L g/L < /
2018 Quarter 4 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) < 0.0025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/20/2018 S Novan082018Self 0.000035 /0.000142 mg/L /
10/05/2018 P Novan100518POTWH 0.000025 /0.000142 mg/L /
g 1
Aug 2018 Week 3 0.000035 / mg/L /
Oct 2018 Week 1 0.000025 / mg/L /
Aug 2018 Average 0.000035 / mg/L /
Oct 2018 Average 0.000025 / mg/L /
2018 Quarter 3 0.000035 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 7

Novan, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2018 Quarter 4 0.000025 / mg/L / .
2018 2nd 6 Months(Avg) 0.000030 / mg/L /
2018 2nd 6...(Max) 0.000035 / mg/L /
2018 2nd 6...(Min) 0.000025 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
10/05/2018 P Novan100518POTW < 0.003 / mg/L < /
Oct 2018 Week 1 < 0.003 / mg/L < /
Oct 2018 Average < 0.003 / mg/L < /
2018 Quarter 4 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/20/2018 S Novan082018Se1f < 0.001 / mg/L < /
10/05/2018 P Novan100518POTW < 0.001 / mg/L < /
Aug 2018 Week 3 < 0.001 / mg/L < /
Oct 2018 Week 1 < 0.001 / mg/L < /
Aug 2018 Average < 0.001 / mg/L < /
Oct 2018 Average < 0.001 / mg/L < /
2018 Quarter 3 < 0.001 / mg/L < /
2018 Quarter 4 < 0.001 / mg/L < /
2018 2nd 6 Months(Avg) < 0.001 / mg/L < /
2018 2nd 6...(Max) < 0.001 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 7

Novan, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
10/05/2018 P Novan100518POTW < 0.003 / mg/L < /
Oct 2018 Week 1 < 0.003 / mg/L < /
Oct 2018 Average < 0.003 / mg/L < /
2018 Quarter 4 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/20/2018 S Novan082018Self 9.1 /6- 10 SU /
10/05/2018 P Novan100518POTW 5.1 /6.0- 10.0 SU * /
10/12/2018 P Novan101218POTW 6.9 /6.0- 10.0 SU /
Aug 2018 Week 3 9.1 / SU /
Oct 2018 Week 1 5.1 / SU /
Oct 2018 Week 2 6.9 / SU /
Aug 2018 Average 9.1 / SU /
Oct 2018 Average 6 / SU /
2018 Quarter 3 9.1 / SU /
2018 Quarter 4 6 / SU /
2018 2nd 6 Months(Avg) 7.03 / SU /
2018 2nd 6...(Max) 9.1 / SU /
2018 2nd 6...(Min) 5.1 / SU /
2018 2nd 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 3 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 1 33.33
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/20/2018 S Novan082018Se1f < 0.0003 / mg/L < /
10/05/2018 P Novan100518POTW < 0.0003 / mg/L < /
Aug 2018 Week 3 < 0.0003 / mg/L <
Oct 2018 Week 1 < 0.0003 / mg/L < /
Aug 2018 Average < 0.0003 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 7

Novan, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
Oct 2018 Average < 0.0003 / mg/L < /
2018 Quarter 3 < 0.0003 / mg/L < /
2018 Quarter 4 < 0.0003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0003 / mg/L < /
2018 2nd 6...(Max) < 0.0003 / mg/L < /
2018 2nd 6...(Min) < 0.0003 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/20/2018 S Novan082018Self 29 /66 °C /
10/05/2018 P Novan100518POTW 26 /66 °C /
Aug 2018 Week 3 29 / °C /
Oct 2018 Week 1 26 / °C /
Aug 2018 Average 29 / °C /
I Oct 2018 Average 26 / °C /
2018 Quarter 3 29 / °C /
2018 Quarter 4 26 / °C /
2018 2nd 6 Months(Avg) 27.5 / °C /
2018 2nd 6...(Max) 29 / °C /
2018 2nd 6...(Min) 26 / °C /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2
p p Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/20/2018 S Novan082018Se1f 9.96 / mg/L /
10/05/2018 P Novan100518POTW 19.2 / mg/L /
Aug 2018 Week 3 9.96 / mg/L /
Oct 2018 Week 1 19.2 / mg/L /
Aug 2018 Average 9.96 / mg/L /
Oct 2018 Average 19.2 / mg/L /
2018 Quarter 3 9.96 / mg/L /
2018 Quarter 4 19.2 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 7

Novan, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
2018 2nd 6 Months(Avg) 14.58 / mg/L /
2018 2nd 6...(Max) 19.2 / mg/L /
2018 2nd 6...(Min) 9.96 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
08/20/2018 S Novan082018SeIf 2.3429 / mg/L /
Aug 2018 Week 3 2.3429 / mg/L /
Aug 2018 Average 2.3429 / mg/L /
2018 Quarter 3 2.3429 / mg/L /
2018 2nd 6 Months(Avg) 2.3429 / mg/L /
2018 2nd 6...(Max) 2.3429 / mg/L /
2018 2nd 6...(Min) 2.3429 / mg/L /
2018 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/20/2018 S Novan082018Self 0.423 / mg/L /
10/05/2018 P Novan100518POTW 0.855 / mg/L /
Aug 2018 Week 3 0.423 / mg/L /
Oct 2018 Week 1 0.855 / mg/L /
Aug 2018 Average 0.423 / mg/L /
Oct 2018 Average 0.855 / mg/L /
2018 Quarter 3 0.423 / mg/L /
2018 Quarter 4 0.855 / mg/L /
2018 2nd 6 Months(Avg) 0.639 / mg/L /
2018 2nd 6...(Max) 0.855 / mg/L /
2018 2nd 6...(Min) 0.423 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 7

Phononic
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S Phononic0718F1ow 0.02313 / MGD /
08/31/2018 S Phononic0818F1ow 0.020424 / MGD /
09/30/2018 S Phononic0918F1ow 0.019495 / MGD /
10/31/2018 S Phononic1018Flow 0.023991 / MGD /
11/30/2018 S Phononic1118Flow 0.022915 / MGD /
12/31/2018 S Phononic1218Flow 0.008969 / MGD /
Jul 2018 Week 4 0.02313 / MGD /
Aug 2018 Week 4 0.020424 / MGD /
Sep 2018 Week 4 0.019495 / MGD /
Oct 2018 Week 4 0.023991 / MGD /
Nov 2018 Week 4 0.022915 / MGD /
Dec 2018 Week 4 0.008969 / MGD /
Jul 2018 Average 0.02313 /0.020 MOD * /
Aug 2018 Average 0.020424 /0.020 MGD * /
Sep 2018 Average 0.019495 /0.020 MGD /
Oct 2018 Average 0.023991 /0.020 MGD * /
Nov 2018 Average 0.022915 /0.020 MGD * /
Dec 2018 Average 0.008969 /0.020 MGD /
2018 Quarter 3 0.021016 / MGD /
2018 Quarter 4 0.018625 / MGD /
2018 2nd 6 Months(Avg) 0.019821 / MGD /
2018 2nd 6...(Max) 0.023991 / MGD /
2018 2nd 6...(Min) 0.008969 / MGD /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 4 66.67 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
07/18/2018 S Phononic071818Se1f 0.006 / mg/L /
08/03/2018 P Phononic080318POT < 0.05 / mg/L < I
W
08/21/2018 S Phononic082118Self 0.036 / mg/L /
09/24/2018 S Phononic092418Self 0.019 / mg/L /
10/25/2018 S Phononic102518Se1f < 0.003 / mg/L < /
11/27/2018 S Phononic112718Self 0.029 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 5

Phononic
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
12/11/2018 S Phononic121118Self < 0.003 / mg/L < /
Jul 2018 Week 3 0.006 / mg/L /
Aug 2018 Week 1 < 0.05 / mg/L < /
Aug 2018 Week 3 0.036 / mg/L /
Sep 2018 Week 4 0.019 / mg/L /
Oct 2018 Week 4 < 0.003 / mg/L < /
Nov 2018 Week 4 0.029 / mg/L /
Dec 2018 Week 2 < 0.003 / mg/L < /
Jul2018 Average 0.006 / mg/L /
Aug 2018 Average < 0.043 / mg/L < /
Sep 2018 Average 0.019 / mg/L /
Oct 2018 Average < 0.003 / mg/L < /
Nov 2018 Average 0.029 / mg/L /
Dec 2018 Average < 0.003 / mg/L < /
2018 Quarter 3 < 0.028 / mg/L < /
2018 Quarter 4 < 0.011 / mg/L < /
2018 2nd 6 Months(Avg) < 0.021 / mg/L < /
2018 2nd 6...(Max) < 0.05 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 7 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
08/03/2018 P Phononic080318POT 0.000006 /0.000142 mg/L /
WHg
11/12/2018 S Phononicl l 1218Self1-I 0.000012 /0.000142 mg/L /
g
Aug 2018 Week I 0.000006 / mg/L /
Nov 2018 Week 2 0.000012 / mg/L /
Aug 2018 Average 0.000006 / mg/L /
Nov 2018 Average 0.000012 / mg/L /
2018 Quarter 3 0.000006 / mg/L /
2018 Quarter 4 0.000012 / mg/L /
2018 2nd 6 Months(Avg) 0.000009 / mg/L /
2018 2nd 6...(Max) 0.000012 / mg/L /
2018 2nd 6...(Min) 0.000006 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Phononic
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Muss/Limit
Molybdenum
08/03/2018 P Phononic080318POT < 0.003 / mg/L < 0.0004 / lbs/day
W 1
09/24/2018 S Phononic092418Self < 0.003 / mg/L < 0.0005 / lbs/day
Aug 2018 Week 1 < 0.003 / mg/L < 0.0004 / lbs/day
Sep 2018 Week 4 < 0.003 / mg/L < 0.0005 / lbs/day
Aug 2018 Average < 0.003 / mg/L < 0.0004 / lbs/day
Sep 2018 Average < 0.003 / mg/L < 0.0005 / lbs/day
2018 Quarter 3 < 0.003 / mg/L < 0.0005 / lbs/day
2018 2nd 6 Months(Avg) < 0.003 / mg/L < 0.0005 / lbs/day
2018 2nd 6...(Max) < 0.003 / mg/L < 0.0005 / lbs/day
2018 2nd 6...(Min) < 0.003 / mg/L < 0.0004 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/18/2018 S Phononic071818Self < 0.0025 / mg/L < 0.00058 / 0.02 lbs/day
08/03/2018 P Phononic080318POT 0.024 / mg/L 0.004317 / 0.02 lbs/day
W
08/21/2018 S Phononic082118Self 0.035 / mg/L 0.007351 / 0.02 lbs/day
09/24/2018 S Phononic092418Self 0.073 / mg/L 0.014934 / 0.02 lbs/day
10/25/2018 S Phononic102518Self 0.063 / mg/L 0.015924 /0.02 lbs/day
11/27/2018 S Phononic112718Self 0.088 / mg/L 0.015824 /0.02 lbs/day
12/11/2018 S Phononic121118Self 0.014 / mg/L 0.002087 /0.02 lbs/day
Jul 2018 Week 3 < 0.0025 / mg/L < 0.00058 / lbs/day
Aug 2018 Week 1 0.024 / mg/L 0.004317 / lbs/day
Aug 2018 Week 3 0.035 / mg/L 0.007351 / lbs/day
Sep 2018 Week 4 0.073 / mg/L 0.014934 / lbs/day
Oct 2018 Week 4 0.063 / mg/L 0.015924 / lbs/day
Nov 2018 Week 4 0.088 / mg/L 0.015824 / lbs/day
Dec 2018 Week 2 0.014 / mg/L 0.002087 / lbs/day
Jul 2018 Average < 0.0025 / mg/L < 0.00058 / lbs/day 1
Aug 2018 Average 0.0295 / mg/L 0.005834 / lbs/day
Sep 2018 Average 0.073 / mg/L 0.014934 / lbs/day
Oct 2018 Average 0.063 / mg/L 0.015924 / lbs/day
Nov 2018 Average 0.088 / mg/L 0.015824 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Phononic
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Dec 2018 Average 0.014 / mg/L 0.002087 / lbs/day
2018 Quarter 3 < 0.0336 / mg/L < 0.006795 / lbs/day
2018 Quarter 4 0.055 / mg/L 0.011278 / lbs/day
2018 2nd 6 Months(Avg) < 0.0428 / mg/L < 0.008717 / lbs/day
2018 2nd 6...(Max) 0.088 / mg/L 0.015924 / lbs/day
2018 2nd 6...(Min) < 0.0025 / mg/L < 0.000580 / lbs/day
2018 2nd 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo AvgM TRC: 0 0.00 #Over Wk AvgM TRC: 0 0.00 #Over Qtr AvgM TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/03/2018 P Phononic080318POT 8.2 /5.5- 10 SU /
W
09/24/2018 S Phononic092418Se1f 7.51 /5.5-10 SU /
Aug 2018 Week 1 8.2 / SU /
Sep 2018 Week 4 7.51 / SU /
Aug
2018 Average ag 8.2 / SU /
Sep 2018 Average 7.51 / SU /
2018 Quarter 3 7.86 / SU /
2018 2nd 6 Months(Avg) 7.86 / SU /
2018 2nd 6...(Max) 8.2 / SU /
2018 2nd 6...(Min) 7.51 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
07/18/2018 S Phononic071818Self 0.018 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Phononic
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
08/03/2018 P Phononic080318POT < 0.05 / mg/L < /
W
08/21/2018 S Phononic082118Self 0.168 / mg/L /
09/24/2018 S Phononic092418Se1f 0.159 / mg/L /
10/25/2018 S Phononic102518Se1f 0.206 / mg/L /
11/27/2018 S Phononic112718Self 0.165 / mg/L /
12/11/2018 S Phononic121118Self 0.041 / mg/L /
Aug 2018 Week 1 < 0.05 / mg/L < /
Jul 2018 Week 3 0.018 / mg/L /
Aug 2018 Week 3 0.168 / mg/L /
Sep 2018 Week 4 0.159 / mg/L /
Oct 2018 Week 4 0.206 / mg/L /
Dec 2018 Week 2 0.041 / mg/L /
Nov 2018 Week 4 0.165 / mg/L /
Jul2018 Average 0.018 / mg/L /
Aug 2018 Average < 0.109 / mg/L < /
Sep 2018 Average 0.159 / mg/L /
Oct 2018 Average 0.206 / mg/L /
Nov 2018 Average 0.165 / mg/L /
Dec 2018 Average 0.041 / mg/L /
2018 Quarter 3 < 0.099 / mg/L < /
2018 Quarter 4 0.137 / mg/L /
2018 2nd 6 Months(Avg) < 0.115 / mg/L < /
2018 2nd 6...(Max) 0.206 / mg/L /
2018 2nd 6...(Min) 0.018 / mg/L /
2018 2nd 6...(Count) 7 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 5

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
10/12/2018 S PowerSecure101218Se 3.29 / mg/L /
1f
12/19/2018 P PowerSecure121918P 112 / mg/L /
OTW
Oct 2018 Week 2 3.29 / mg/L /
Dec 2018 Week 3 112 / mg/L /
Oct 2018 Average 3.29 / mg/L /
Dec 2018 Average 112 / mg/L /
2018 Quarter 4 57.645 / mg/L /
2018 2nd 6 Months(Avg) 57.645 / mg/L /
2018 2nd 6...(Max) 112 / mg/L /
2018 2nd 6...(Min) 3.29 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S PowerSecure0718F1ow 0.001746 / MGD /
08/31/2018 S PowerSecure0818FIow 0.00166 / MGD /
09/30/2018 S PowerSecure0918F1ow 0.001797 / MGD /
10/31/2018 S PowerSecure1018Flow 0.00267 / MGD /
11/30/2018 S PowerSecure1118Flow 0.003366 / MGD /
12/31/2018 S PowerSecure1218Flow 0.002765 / MGD /
Jul2018 Week 4 0.001746 / MGD /
Aug 2018 Week 4 0.00166 / MGD /
Sep 2018 Week 4 0.001797 / MGD /
Oct 2018 Week 4 0.00267 / MGD /
Nov 2018 Week 4 0.003366 / MGD /
Dec 2018 Week 4 0.002765 / MGD /
Jul 2018 Average 0.001746 /0.006 MGD /
Aug 2018 Average 0.00166 /0.006 MGD /
Sep 2018 Average 0.001797 /0.006 MGD /
Oct 2018 Average 0.00267 /0.006 MGD /
Nov 2018 Average 0.003366 /0.006 MGD /
Dec 2018 Average 0.002765 /0.006 MGD /
2018 Quarter 3 0.001734 / MGD /
2018 Quarter 4 0.002934 / MGD /
2018 2nd 6 Months(Avg) 0.002334 / MGD /
2018 2nd 6...(Max) 0.003366 / MGD /
2018 2nd 6...(Min) 0.00166 / MGD /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page I of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018To 12/ 1/2 1 SampleType: Effluent
3 0 8 Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
10/12/2018 S PowerSecure101218Se < 0.0005 /0.11 mg/L < /
If
12/19/2018 P PowerSecure121918P 0.011 /0.11 mg/L /
OTW
Oct 2018 Week 2 < 0.0005 / mg/L < /
Dec 2018 Week 3 0.011 / mg/L /
Oct 2018 Average < 0.0005 /0.07 mg/L < /
Dec 2018 Average 0.011 /0.07 mg/L /
2018 Quarter 4 < 0.00575 / mg/L < /
2018 2nd 6 Months(Avg) < 0.00575 / mg/L < /
2018 2nd 6...(Max) 0.011 / mg/L /
2018 2nd 6...(Min) < 0.0005 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
10/12/2018 S PowerSecure101218Se < 0.003 /2.77 mg/L < /
If
12/19/2018 P PowerSecure121918P 0.01 /2.77 mg/L /
OTW
Oct 2018 Week 2 < 0.003 / mg/L < /
Dec 2018 Week 3 0.01 / mg/L /
Oct 2018 Average < 0.003 / 1.71 mg/L < /
Dec 2018 Average 0.01 / 1.71 mg/L /
2018 Quarter 4 < 0.006 / mg/L < /
2018 2nd 6 Months(Avg) < 0.006 / mg/L < /
2018 2nd 6...(Max) 0.01 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2018 2nd 6...(Min) < 0.003 / mg/1, < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
10/12/2018 S PowerSecurel01218Se 0.051 /3.38 mg/L /
if
12/19/2018 P PowerSecure121918P 0.107 /3.38 mg/L /
OTW
Oct 2018 Week 2 0.051 / mg/L /
Dec 2018 Week 3 0.107 / mg/L /
Oct 2018 Average 0.051 /2.07 mg/L /
Dec 2018 Average 0.107 /2.07 mg/L /
2018 Quarter 4 0.079 / mg/L /
2018 2nd 6 Months(Avg) 0.079 / mg/L /
2018 2nd 6...(Max) 0.107 / mg/L /
2018 2nd 6...(Min) 0.051 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
10/12/2018 S PowerSecure101218Se < 0.004 /0.60 mg/L < /
if
12/19/2018 P PowerSecure121918P < 0.003 /0.60 mg/L < /
OTW
Oct 2018 Week 2 < 0.004 / mg/L < /
Dec 2018 Week 3 < 0.003 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Oct 2018 Average < 0.004 /0.50 mg/L < /
Dec 2018 Average < 0.003 /0.50 mg/L < /
2018 Quarter 4 < 0.003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.003 / mg/L < /
2018 2nd 6...(Max) < 0.004 / mg/L < /
2018 2nd 6...(Min) < 0.003 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
10/12/2018 S PowerSecure101218Se < 0.0025 /0.69 mg/L < /
If
12/19/2018 P PowerSecure121918P 0.0014 /0.69 mg/L /
OTW
Oct 2018 Week 2 < 0.0025 / mg/L < /
Dec 2018 Week 3 0.0014 / mg/L /
Oct 2018 Average < 0.0025 /0.43 mg/L < /
Dec 2018 Average 0.0014 /0.43 mg/L /
2018 Quarter 4 < 0.002 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0020 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) 0.0014 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
10/12/2018 S PowerSecure101218Se < 0.0000005 /0.000142 mg/L < /
if
12/19/2018 P PowerSecure121918P 0.0000055 /0.000142 mg/L /
OTWHg
Oct 2018 Week 2 < 0.0000005 / mg/L < /
Dec 2018 Week 3 0.0000055 / mg/L /
Oct 2018 Average < 0.0000005 / mg/L < /
Dec 2018 Average 0.0000055 / mg/L /
2018 Quarter 4 < 0.000003 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0000030 / mg/L < /
2018 2nd 6...(Max) 0.0000055 / mg/L /
2018 2nd 6...(Min) < 0.0000005 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
10/12/2018 S PowerSecure101218Se < 0.003 / mg/L < /
If
12/19/2018 P PowerSecure121918P < 0.001 / mg/L < /
OTW
Oct 2018 Week 2 < 0.003 / mg/L < /
Dec 2018 Week 3 < 0.001 / mg/L , < /
Oct 2018 Average < 0.003 / mg/L < /
Dec 2018 Average < 0.001 / mg/L < /
2018 Quarter 4 < 0.002 / mg/L < /
2018 2nd 6 Months(Avg) < 0.002 / mg/L < /
2018 2nd 6...(Max) < 0.003 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
10/12/2018 S PowerSecure101218Se < 0.0025 / 1.3 mg/L < /
if
12/19/2018 P PowerSecure121918P 0.0038 / 1.3 mg/L /
OTW
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Oct 2018 Week 2 < 0.0025 / mg/L < /
Dec 2018 Week 3 0.0038 / mg/L /
Oct 2018 Average < 0.0025 / 1 mg/L < /
Dec 2018 Average 0.0038 / 1 mg/L /
2018 Quarter 4 < 0.0032 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0032 / mg/L < /
2018 2nd 6...(Max) 0.0038 / mg/L /
2018 2nd 6...(Min) < 0.0025 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
10/12/2018 S PowerSecure101218Se 7.4 /6- 10 SU /
If
12/19/2018 P PowerSecure121918P 10.6 /6- 10 SU * /
OTW
Oct 2018 Week 2 7.4 / SU /
Dec 2018 Week 3 10.6 / SU /
Oct 2018 Average 7.4 / SU /
Dec 2018 Average 10.6 / SU /
2018 Quarter 4 9 / SU /
2018 2nd 6 Months(Avg) 9 / SU /
2018 2nd 6...(Max) 10.6 / SU /
2018 2nd 6...(Min) 7.4 / SU /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 1 50.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 9

PowerSecu re
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
10/12/2018 S PowerSecure101218Se < 0.0025 /0.43 mg/L < /
If
12/19/2018 P PowerSecure121918P 0.0019 /0.43 mg/L /
OTW
Oct 2018 Week 2 < 0.0025 / mg/L < /
Dec 2018 Week 3 0.0019 / mg/L /
Oct 2018 Average < 0.0025 /0.24 mg/L < /
Dec 2018 Average 0.0019 /0.24 mg/L /
2018 Quarter 4 < 0.0022 / mg/L < /
2018 2nd 6 Months(Avg) < 0.0022 / mg/L < /
2018 2nd 6...(Max) < 0.0025 / mg/L < /
2018 2nd 6...(Min) 0.0019 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
10/12/2018 S PowerSecure101218Se 23.1 /66 °C /
If
12/19/2018 P PowerSecure121918P 19 /66 °C /
OTW
Oct 2018 Week 2 23.1 / °C /
Dec 2018 Week 3 19 / °C /
Oct 2018 Average 23.1 / °C /
Dec 2018 Average 19 / °C /
2018 Quarter 4 21.1 / °C /
2018 2nd 6 Months(Avg) 21.1 / °C /
2018 2nd 6...(Max) 23.1 / °C /
2018 2nd 6...(Min) 19 / °C /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TTO
10/12/2018 S PowerSecure101218Se < 0.000025 /2.13 mg/L < /
If
Oct 2018 Week 2 < 0.000025 / mg/L < /
Oct 2018 Average < 0.000025 / mg/L < /
2018 Quarter 4 < 0.000025 / mg/L < /
2018 2nd 6 Months(Avg) < 0.000025 / mg/L < /
2018 2nd 6...(Max) < 0.000025 / mg/L < /
2018 2nd 6...(Min) < 0.000025 / mg/L < /
2018 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
10/12/2018 S PowerSecure101218Se 0.02 /2.61 mg/L /
If
12/19/2018 P PowerSecure121918P 0.561 /2.61 mg/L /
OTW
Oct 2018 Week 2 0.02 / mg/L /
Dec 2018 Week 3 0.561 / mg/L /
Oct 2018 Average 0.02 / 1.48 mg/L /
Dec 2018 Average 0.561 / 1.48 mg/L /
2018 Quarter 4 0.29 / mg/L /
2018 2nd 6 Months(Avg) 0.290 / mg/L /
2018 2nd 6...(Max) 0.561 / mg/L /
2018 2nd 6...(Min) 0.020 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 9

PowerSecure
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall. 001
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: EffluentWastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
10/09/2018 S SCM100918Self 9.1 / mg/L 1.1611 / lbs/day
11/30/2018 P SCM113018POTW 10.1 / mg/L 1.4864 / lbs/day
Oct 2018 Week 2 9.1 / mg/L 1.1611 / lbs/day
Nov 2018 Week 4 10.1 / mg/L 1.4864 / lbs/day
Oct 2018 Average 9.1 / mg/L 1.1611 / lbs/day
Nov 2018 Average 10.1 / mg/L 1.4864 / lbs/day
2018 Quarter 4 9.6 / mg/L 1.3237 / lbs/day
2018 2nd 6 Months(Avg) 9.6 / mg/L 1.3238 / lbs/day
2018 2nd 6...(Max) 10.1 / mg/L 1.4864 / lbs/day
2018 2nd 6...(Min) 9.1 / mg/L 1.1611 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
•
Average Flow for Month
07/31/2018 S SCM0718Flow 0.011115 /0.080 MGD /
08/31/2018 S SCM0818Flow 0.011737 /0.080 MGD /
09/30/2018 S SCM0918Flow 0.011095 /0.080 MGD /
10/31/2018 S SCM1018Flow 0.010434 /0.080 MGD /
11/30/2018 S SCM1118Flow 0.020677 /0.080 MGD /
12/31/2018 S SCM1218Flow 0.020785 /0.080 MGD /
Jul 2018 Week 4 0.011115 / MGD /
Aug 2018 Week 4 0.011737 / MGD /
Sep 2018 Week 4 0.011095 / MGD /
Oct 2018 Week 4 0.010434 / MGD /
Nov 2018 Week 4 0.020677 / MGD /
Dec 2018 Week 4 0.020785 / MGD /
Jul 2018 Average 0.011115 /0.050 MGD /
Aug 2018 Average 0.011737 /0.050 MGD /
Sep 2018 Average 0.011095 /0.050 MGD /
Oct 2018 Average 0.010434 /0.050 MGD /
Nov 2018 Average 0.020677 /0.050 MGD /
Dec 2018 Average 0.020785 /0.050 MGD /
2018 Quarter 3 0.011316 / MGD /
2018 Quarter 4 0.017299 / MGD /
2018 2nd 6 Months(Avg) 0.014307 / MGD /
2018 2nd 6...(Max) 0.020785 / MGD /
2018 2nd 6...(Min) 0.010434 / MGD /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation "Indicates TRC Violation Page 1 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 T Sample e: Effluent Wastewater Ou
P Y all: 001P �
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
10/09/2018 S SCM100918Self < 0.0005 / mg/L < 0.000064 / lbs/day
11/30/2018 P SCM113018POTW < 0.00008 / mg/L < 0.000011 / lbs/day
Oct 2018 Week 2 < 0.0005 / mg/L < 0.000064 / lbs/day
Nov 2018 Week 4 < 0.00008 / mg/L < 0.000011 / lbs/day
Oct 2018 Average < 0.0005 / mg/L < 0.000064 / lbs/day
Nov 2018 Average < 0.00008 / mg/L < 0.000011 / lbs/day
2018 Quarter 4 < 0.00029 / mg/L < 0.000037 / lbs/day
2018 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000037 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.000064 / lbs/day
2018 2nd 6...(Min) < 0.00008 / mg/L < 0.000011 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
10/09/2018 S SCM100918Self 15.4 / mg/L 1.9649 / lbs/day
11/30/2018 P SCM113018POTW 20 / mg/L 2.9434 / lbs/day
Oct 2018 Week 2 15.4 / mg/L 1.9649 / lbs/day
Nov 2018 Week 4 20 / mg/L 2.9434 / lbs/day
Oct 2018 Average 15.4 / mg/L 1.9649 / lbs/day
Nov 2018 Average 20 / mg/L 2.9434 / lbs/day
2018 Quarter 4 17.7 / mg/L 2.4541 / lbs/day
2018 2nd 6 Months(Avg) 17.7 / mg/L 2.4542 / lbs/day
2018 2nd 6...(Max) 20 / mg/L 2.9434 / lbs/day
2018 2nd 6...(Min) 15.4 / mg/L 1.9649 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/17/2018 S SCM071718Self 1.36 /0.75 mg/L * * 0.178303 / lbs/day
08/16/2018 S SCM081618Self 0.042 /0.75 mg/L 0.010899 / lbs/day
09/07/2018 S SCM090718Self 0.084 /0.75 mg/L 0.009993 / lbs/day
10/09/2018 S SCM100918Self 0.107 /0.75 mg/L 0.013653 / lbs/day
11/30/2018 P SCM113018POTW 0.119 /0.75 mg/L 0.017513 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Jul 2018 Week 3 1.36 / mg/L 0.178303 / lbs/day
Sep 2018 Week 1 0.084 / mg/L 0.009993 / lbs/day
Aug 2018 Week 3 0.042 / mg/L 0.010899 / lbs/day
1 Oct 2018 Week 2 0.107 / mg/L 0.013653 / lbs/day
Nov 2018 Week 4 0.119 m 0.017513 / lbs/day
�-
Jul 2018 Average 1.36 /0.50 mg/L 0.178303 / lbs/day
Aug 2018 Average 0.042 /0.50 mg/L 0.010899 / lbs/day
Sep 2018 Average 0.084 /0.50 mg/L 0.009993 / lbs/day
Oct 2018 Average 0.107 /0.50 mg/L 0.013653 / lbs/day
Nov 2018 Average 0.119 /0.50 mg/L 0.017513 / lbs/day
2018 Quarter 3 0.495 / mg/L 0.066398 / lbs/day
2018 Quarter4 0.113 / mg/L 0.015583 / lbs/day
2018 2nd 6 Months(Avg) 0.342 / mg/L 0.046072 / lbs/day
2018 2nd 6...(Max) 1.36 / mg/L 0.178303 / lbs/day
2018 2nd 6...(Min) 0.042 / mg/L 0.009993 / lbs/day
2018 2nd 6...(Count) 5 / 5 /
Sample Count: 5 Months Sampled: 5 Weeks Sampled: 5 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 1 20.00 #Over Mo Avg C: 1 20.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 1 20.00 #Over Mo Avg C TRC: 1 20.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
1 #Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
10/09/2018 S SCM100918Self < 0.004 /0.04 mg/L < 0.00051 / lbs/day
11/30/2018 P SCM113018POTW < 0.003 /0.04 mg/L < 0.000368 / lbs/day
Oct 2018 Week 2 < 0.004 / mg/L < 0.00051 / lbs/day
Nov 2018 Week 4 < 0.003 / mg/L < 0.000368 / lbs/day
Oct 2018 Average < 0.004 /0.03 mg/L < 0.00051 / lbs/day
Nov 2018 Average < 0.003 /0.03 mg/L < 0.000368 / lbs/day
2018 Quarter 4 < 0.003 / mg/L < 0.000439 / lbs/day
2018 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000439 / lbs/day
2018 2nd 6...(Max) < 0.004 / mg/L < 0.000510 / lbs/day
2018 2nd 6...(Min) < 0.003 / mg/L < 0.000368 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
10/09/2018 S SCM100918Self < 0.05 / mg/L < 0.0064 / lbs/day
11/30/2018 P SCM113018POTW 1.5 / mg/L 0.2208 / lbs/day
Oct 2018 Week 2 < 0.05 / mg/L < 0.0064 / lbs/day
Nov 2018 Week 4 1.5 / mg/L 0.2208 / lbs/day
Oct 2018 Average < 0.05 / mg/L < 0.0064 / lbs/day
Nov 2018 Average 1.5 / mg/L 0.2208 / lbs/day
2018 Quarter 4 < 0.78 / mg/L < 0.1136 / lbs/day
2018 2nd 6 Months(Avg) < 0.78 / mg/L < 0.1136 / lbs/day
2018 2nd 6...(Max) 1.5 / mg/L 0.2208 / lbs/day
2018 2nd 6...(Min) < 0.05 / mg/L < 0.0064 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/17/2018 S SCM071718Self < 0.0025 /0.20 mg/L < 0.000328 / lbs/day
10/09/2018 S SCM100918Self < 0.0025 /0.20 mg/L < 0.000319 / lbs/day
11/30/2018 P SCM113018POTW 0.0007 /0.20 mg/L 0.000097 / lbs/day
Jul 2018 Week 3 < 0.0025 / mg/L < 0.000328 / lbs/day
Oct 2018 Week 2 < 0.0025 / mg/L < 0.000319 / lbs/day
Nov 2018 Week 4 0.0007 / mg/L 0.000097 / lbs/day
Jul 2018 Average < 0.0025 /0.10 mg/L < 0.000328 / lbs/day
Oct 2018 Average < 0.0025 /0.10 mg/L < 0.000319 / lbs/day
Nov 2018 Average 0.0007 /0.10 mg/L 0.000097 / lbs/day
2018 Quarter 3 < 0.0025 / mg/L < 0.000328 / lbs/day
2018 Quarter 4 < 0.0016 / mg/L < 0.000208 / lbs/day
2018 2nd 6 Months(Avg) < 0.0019 / mg/L < 0.000248 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.000328 / lbs/day
2018 2nd 6...(Min) 0.0007 / mg/L 0.000097 / lbs/day
2018 2nd 6...(Count) 3 / 3 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
10/09/2018 S SCM100918Se1f 0.000005 /0.000142 mg/L /
11/29/2018 P SCM112918POTWHg 0.000008 /0.000142 mg/L /
Oct 2018 Week 2 0.000005 / mg/L /
Nov 2018 Week 4 0.000008 / mg/L /
Oct 2018 Average 0.000005 / mg/L /
Nov 2018 Average 0.000008 / mg/L /
2018 Quarter 4 0.000006 / mg/L /
2018 2nd 6 Months(Avg) 0.0000063 / mg/L /
2018 2nd 6...(Max) 0.0000080 / mg/L /
2018 2nd 6...(Min) 0.0000046 / mg/L /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
10/09/2018 S SCM100918Self < 0.003 / mg/L < 0.0003 / lbs/day
11/30/2018 P SCM113018POTW < 0.001 / mg/L < 0.0001 / lbs/day
Oct 2018 Week 2 < 0.003 / mg/L < 0.0003 / lbs/day
Nov 2018 Week 4 < 0.001 / mg/L < 0.0001 / lbs/day
Oct 2018 Average < 0.003 / mg/L < 0.0003 / lbs/day
Nov 2018 Average < 0.001 / mg/L < 0.0001 / lbs/day
2018 Quarter 4 < 0.002 / mg/L < 0.0002 / lbs/day
2018 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0002 / lbs/day
2018 2nd 6...(Max) < 0.003 / mg/L < 0.0003 / lbs/day
2018 2nd 6...(Min) < 0.001 / mg/L < 0.0001 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
10/09/2018 S SCM100918Self < 0.0025 / mg/L < 0.000319 / lbs/day
11/30/2018 P SCM113018POTW 0.0024 / mg/L 0.000349 / lbs/day
Oct 2018 Week 2 < 0.0025 / mg/L < 0.000319 / lbs/day
Nov 2018 Week 4 0.0024 / mg/L 0.000349 / lbs/day
Oct 2018 Average < 0.0025 / mg/L < 0.000319 / lbs/day
Nov 2018 Average 0.0024 / mg/L 0.000349 / lbs/day
2018 Quarter 4 < 0.0024 / mg/L < 0.000334 / lbs/day
2018 2nd 6 Months(Avg) < 0.0024 / mg/L < 0.000334 / lbs/day
2018 2nd 6...(Max) < 0.0025 / mg/L < 0.000349 / lbs/day
2018 2nd 6...(Min) 0.0024 / mg/L 0.000319 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
10/09/2018 S SCM100918Self 0.6 / mg/L 0.075 / lbs/day
11/30/2018 P SCM113018POTW 0.6 / mg/L 0.087 / lbs/day
Oct 2018 Week 2 0.6 / mg/L 0.075 / lbs/day
Nov 2018 Week 4 0.6 / mg/L 0.087 / lbs/day
Oct 2018 Average 0.6 / mg/L 0.075 / lbs/day
Nov 2018 Average 0.6 / mg/L 0.087 / lbs/day
2018 Quarter 4 0.6 / mg/L 0.081 / lbs/day
2018 2nd 6 Months(Avg) 0.6 / mg/L 0.081 / lbs/day
2018 2nd 6...(Max) 0.6 / mg/L 0.087 / lbs/day
2018 2nd 6...(Min) 0.6 / mg/L 0.075 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
10/09/2018 S SCM100918Self 15.5 / mg/L 1.978 / lbs/day
11/30/2018 P SCM113018POTW 28.6 / mg/L 4.209 / lbs/day
Oct 2018 Week 2 15.5 / mg/L 1.978 / lbs/day
Nov 2018 Week 4 28.6 / mg/L 4.209 / lbs/day
Oct 2018 Average 15.5 / mg/L 1.978 / lbs/day
Nov 2018 Average 28.6 / mg/L 4.209 / lbs/day
2018 Quarter 4 22.05 / mg/L 3.093 / lbs/day
2018 2nd 6 Months(Avg) 22.05 / mg/L 3.093 / lbs/day
2018 2nd 6...(Max) 28.6 / mg/L 4.209 / lbs/day
2018 2nd 6...(Min) 15.5 / mg/L 1.978 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/09/2018 S SCM 100918Se1f < 2.5 /200 mg/L < /
11/30/2018 P SCM113018POTW 7 /200 mg/L /
Oct 2018 Week 2 < 2.5 / mg/L < /
Nov 2018 Week 4 7 / mg/L /
Oct 2018 Average < 2.5 / mg/L < /
Nov 2018 Average 7 / mg/L /
2018 Quarter 4 < 4.75 / mg/L < /
2018 2nd 6 Months(Avg) < 4.75 / mg/L < /
2018 2nd 6...(Max) 7 / mg/L /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/17/2018 S SCM071718Self 6.6 /6.0- 10.5 SU /
08/16/2018 S SCM081618Self 7.2 /6.0- 10.5 SU /
09/07/2018 S SCM090718Self 6.9 /6.0- 10.5 SU /
10/09/2018 S SCM100918Se1f 6.9 /6.0- 10.5 SU /
11/30/2018 P SCM113018POTW 7.3 /6.0- 10.5 SU /
Jul 2018 Week 3 6.6 / SU /
Aug 2018 Week 3 7.2 / SU /
Sep 2018 Week 1 6.9 / SU /
Oct 2018 Week 2 6.9 / SU /
Nov 2018 Week 4 7.3 / SU /
Jul2018 Average 6.6 / SU /
Aug 2018 Average 7.2 / SU /
Sep 2018 Average 6.9 / SU /
Oct 2018 Average 6.9 / SU /
Nov 2018 Average 7.3 / SU /
2018 Quarter 3 6.9 / SU /
2018 Quarter 4 7.1 / SU /
2018 2nd 6 Months(Avg) 6.98 / SU /
2018 2nd 6...(Max) 7.3 / SU /
2018 2nd 6...(Min) 6.6 / SU /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2018 2nd 6...(Count) 5 / /
Sample Count: 5 Months Sampled: 5 Weeks Sampled: 5 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
10/09/2018 S SCM100918Se1f < 0.005 / mg/L < 0.000638 / lbs/day
11/30/2018 P SCM113018POTW < 0.001 / mg/L < 0.000147 / lbs/day
Oct 2018 Week 2 < 0.005 / mg/L < 0.000638 / lbs/day
Nov 2018 Week 4 < 0.001 / mg/L < 0.000147 / lbs/day
Oct 2018 Average < 0.005 / mg/L < 0.000638 / lbs/day
Nov 2018 Average < 0.001 / mg/L < 0.000147 / lbs/day
2018 Quarter 4 < 0.003 / mg/L < 0.000393 / lbs/day
2018 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000393 / lbs/day
2018 2nd 6...(Max) < 0.005 / mg/L < 0.000638 / lbs/day
2018 2nd 6...(Min) < 0.001 / mg/L < 0.000147 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/17/2018 S SCM071718Self 30.5 /66 °C /
08/16/2018 S SCM081618Self 25.1 /66 °C /
09/07/2018 S SCM090718Self 26.5 /66 °C /
10/09/2018 S SCM100918Self 25.5 /66 °C /
11/30/2018 P SCM113018POTW 10 /66 °C /
Jul2018 Week 3 30.5 / °C /
Aug 2018 Week 3 25.1 / °C /
Sep 2018 Week 1 26.5 / °C /
Oct 2018 Week 2 25.5 / °C /
Nov 2018 Week 4 10 / °C /
Jul 2018 Average 30.5 / °C /
Aug 2018 Average 25.1 / °C /
Sep 2018 Average 26.5 / °C /
Oct 2018 Average 25.5 / °C /
Nov 2018 Average 10 / °C /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2018 Quarter 3 27.4 / °C /
2018 Quarter 4 17.8 / °C /
2018 2nd 6 Months(Avg) 23.5 / °C /
2018 2nd 6...(Max) 30.5 / °C /
2018 2nd 6...(Min) 10 / °C /
2018 2nd 6...(Count) 5 / /
Sample Count: 5 Months Sampled: 5 Weeks Sampled : 5 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
10/09/2018 S SCM100918Se1f 14.9 / mg/L 1.901 / lbs/day
11/30/2018 P SCM113018POTW 28 / mg/L 4.121 / lbs/day
Oct 2018 Week 2 14.9 / mg/L 1.901 / lbs/day
Nov 2018 Week 4 28 / mg/L 4.121 / lbs/day
Oct 2018 Average 14.9 / mg/L 1.901 / lbs/day
Nov 2018 Average 28 / mg/L 4.121 / lbs/day
2018 Quarter 4 21.45 / mg/L 3.011 / lbs/day
2018 2nd 6 Months(Avg) 21.45 / mg/L 3.011 / lbs/day
2018 2nd 6...(Max) 28 / mg/L 4.121 / lbs/day
2018 2nd 6...(Min) 14.9 / mg/L 1.901 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
10/09/2018 S SCM100918Self 2.1 / mg/L 0.2679 / lbs/day
11/30/2018 P SCM113018POTW 2.87 / mg/L 0.4224 / lbs/day
Oct 2018 Week 2 2.1 / mg/L 0.2679 / lbs/day
Nov 2018 Week 4 2.87 / mg/L 0.4224 / lbs/day
Oct 2018 Average 2.1 / mg/L 0.2679 / lbs/day
Nov 2018 Average 2.87 / mg/L 0.4224 / lbs/day
2018 Quarter 4 2.485 / mg/L 0.3452 / lbs/day
2018 2nd 6 Months(Avg) 2.485 / mg/L 0.3452 / lbs/day
2018 2nd 6...(Max) 2.87 / mg/L 0.4224 / lbs/day
2018 2nd 6...(Min) 2.1 / mg/L 0.2679 / lbs/day
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
2018 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
10/09/2018 S SCM100918Se1f 1.86 / mg/L /
Oct 2018 Week 2 1.86 / mg/L /
Oct 2018 Average 1.86 / mg/L /
2018 Quarter 4 1.86 / mg/L /
2018 2nd 6 Months(Avg) 1.86 / mg/L /
2018 2nd 6...(Max) 1.86 / mg/L /
2018 2nd 6...(Min) 1.86 / mg/L /
2018 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
10/09/2018 S SCM100918Se1f 0.31 / mg/L 0.039554 / lbs/day
11/30/2018 P SCM I13018POTW 0.444 / mg/L 0.065342 / lbs/day
Oct 2018 Week 2 0.31 / mg/L 0.039554 / lbs/day
Nov 2018 Week 4 0.444 / mg/L 0.065342 / lbs/day
Oct 2018 Average 0.31 / mg/L 0.039554 / lbs/day
Nov 2018 Average 0.444 / mg/L 0.065342 / lbs/day
2018 Quarter 4 0.377 / mg/L 0.052448 / lbs/day
2018 2nd 6 Months(Avg) 0.377 / mg/L 0.052448 / lbs/day
2018 2nd 6...(Max) 0.444 / mg/L 0.065342 / lbs/day
2018 2nd 6...(Min) 0.31 / mg/L 0.039554 / lbs/day
2018 2nd 6...(Count) 2 / 2 /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/09/2018 S UTP1080918Se1f 1.3 / mg/L /
11/28/2018 P UTP1112818POTW 2 / mg/L 0.7086 / lbs/day
Aug 2018 Week 2 1.3 / mg/L /
Nov 2018 Week 4 2 / mg/L 0.7086 / lbs/day
Aug 2018 Average 1.3 / mg/L /
Nov 2018 Average 2 / mg/L 0.7086 / lbs/day
2018 Quarter 3 1.3 / mg/L /
2018 Quarter 4 2 / mg/L 0.7086 / lbs/day
2018 2nd 6 Months(Avg) 1.65 / mg/L 0.7086 / lbs/day
2018 2nd 6...(Max) 2 / mg/L 0.7086 / lbs/day
2018 2nd 6...(Min) 1.3 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2018 S UTP10718F1ow 0.045459 / MGD /
08/31/2018 S UTP10818Flow 0.0505 / MGD /
09/30/2018 S UTP10918Flow 0.045267 / MGD /
10/31/2018 S UTP11018F1ow 0.042351 / MGD /
11/30/2018 S UTP11118F1ow 0.03361 / MGD /
12/31/2018 S UTP11218Flow 0.029677 / MGD /
Jul 2018 Week 4 0.045459 / MGD /
Aug 2018 Week 4 0.0505 / MGD /
Sep 2018 Week 4 0.045267 / MGD /
Oct 2018 Week 4 0.042351 / MGD /
Nov 2018 Week 4 0.03361 / MGD /
Dec 2018 Week 4 0.029677 / MGD /
Jul 2018 Average 0.045459 /0.050 MGD /
Aug 2018 Average 0.0505 /0.050 MOD * /
Sep 2018 Average 0.045267 /0.050 MGD /
Oct 2018 Average 0.042351 /0.050 MGD /
Nov 2018 Average 0.03361 /0.050 MGD /
Dec 2018 Average 0.029677 /0.050 MGD /
2018 Quarter 3 0.047075 / MGD /
2018 Quarter 4 0.035213 / MGD /
2018 2nd 6 Months(Avg) 0.041144 / MGD /
2018 2nd 6...(Max) 0.0505 / MGD /
2018 2nd 6...(Min) 0.029677 / MGD /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Ouffall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 1 16.67 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
11/28/2018 P UTP1112818POTW 71.9 / mg/L 25.473 / lbs/day
Nov 2018 Week 4 71.9 / mg/L 25.473 / lbs/day
Nov 2018 Average 71.9 / mg/L 25.473 / lbs/day
2018 Quarter 4 71.9 / mg/L 25.473 / lbs/day
2018 2nd 6 Months(Avg) 71.9 / mg/L 25.473 / lbs/day
2018 2nd 6...(Max) 71.9 / mg/L 25.473 / lbs/day
2018 2nd 6...(Min) 71.9 / mg/L 25.473 / lbs/day
2018 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/09/2018 S UTP1080918Self < 0.0005 / mg/L < /
11/28/2018 P UTP1112818POTW < 0.00008 / mg/L < 0.000027 / lbs/day
Aug 2018 Week 2 < 0.0005 / mg/L < /
Nov 2018 Week 4 < 0.00008 / mg/L < 0.000027 / lbs/day
Aug 2018 Average < 0.0005 / mg/L < /
Nov 2018 Average < 0.00008 / mg/L < 0.000027 / lbs/day
2018 Quarter 3 < 0.0005 / mg/L < /
2018 Quarter 4 < 0.00008 / mg/L < 0.000027 / lbs/day
2018 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000027 / lbs/day
2018 2nd 6...(Max) < 0.0005 / mg/L < 0.000027 / lbs/day
2018 2nd 6...(Min) < 0.00008 / mg/L < /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/09/2018 S UTP1080918Self 28.9 / mg/L /
11/28/2018 P UTP1112818POTW 30 / mg/L 10.6285 / lbs/day
Aug 2018 Week 2 28.9 / mg/L /
Nov 2018 Week 4 30 / mg/L 10.6285 / lbs/day
Aug 2018 Average 28.9 / mg/L /
Nov 2018 Average 30 / mg/L 10.6285 / lbs/day
2018 Quarter 3 28.9 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 10
l

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2018 Quarter 4 30 / mg/L
10.6285 / lbs/day
2018 2nd 6 Months(Avg) 29.45 / mg/L 10.6285 / lbs/day
2018 2nd 6...(Max) 30 / mg/L 10.6285 / lbs/day
2018 2nd 6...(Min) 28.9 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/09/2018 S UTP1080918Self 163 / mg/L /
11/28/2018 P UTP1112818POTW 138 / mg/L 48.89 / lbs/day
Aug 2018 Week 2 163 / mg/L /
Nov 2018 Week 4 138 / mg/L 48.89 / lbs/day
Aug 2018 Average 163 / mg/L /
Nov 2018 Average 138 / mg/L 48.89 / lbs/day
2018 Quarter 3 163 / mg/L /
2018 Quarter 4 138 / mg/L 48.89 / lbs/day
2018 2nd 6 Months(Avg) 150.5 / mg/L 48.89 / lbs/day
2018 2nd 6...(Max) 163 / mg/L 48.89 / lbs/day
2018 2nd 6...(Min) 138 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/09/2018 S UTP1080918Self < 0.004 / mg/L < /
11/28/2018 P UTP1112818POTW 0.008 / mg/L 0.002834 / lbs/day
Aug 2018 Week 2 < 0.004 / mg/L < /
Nov 2018 Week 4 0.008 / mg/L 0.002834 / lbs/day
Aug 2018 Average < 0.004 / mg/L < /
Nov 2018 Average 0.008 / mg/L 0.002834 / lbs/day
2018 Quarter 3 < 0.004 / mg/L < /
2018 Quarter 4 0.008 / mg/L 0.002834 / lbs/day
2018 2nd 6 Months(Avg) < 0.006 / mg/L < 0.002834 / lbs/day
2018 2nd 6...(Max) 0.008 / mg/L 0.002834 / lbs/day
2018 2nd 6...(Min) < 0.004 / mg/L < /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/09/2018 S UTP1080918Self < 0.05 / mg/L < /
11/28/2018 P UTP1112818POTW 0.13 / mg/L 0.0461 / lbs/day
Aug 2018 Week 2 < 0.05 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Nov 2018 Week 4 0.13 / mg/L 0.0461 / lbs/day
Aug 2018 Average < 0.05 / mg/L < /
Nov 2018 Average 0.13 / mg/L 0.0461 / lbs/day
2018 Quarter 3 < 0.05 / mg/L < /
2018 Quarter 4 0.13 / mg/L 0.0461 / lbs/day
2018 2nd 6 Months(Avg) < 0.09 / mg/L < 0.0461 / lbs/day
2018 2nd 6...(Max) 0.13 / mg/L 0.0461 / lbs/day
2018 2nd 6...(Min) < 0.05 / mg/L < /
2018 2nd 6...(Count) 2 / 1 /
Sample Date Sample/D Result/Limit Mass/Limit
Mercury-LL
08/09/2018 S UTP1080918Self 0.000002 /0.000142 mg/L /
09/13/2018 S UTP1091318Se1f 0.000001 /0.000142 mg/L /
10/05/2018 S UTP1100518Self 0.000006 /0.000142 mg/L /
11/16/2018 S UTP1111618Se1f 0.000004 /0.000142 mg/L /
11/27/2018 P UTP1112718POTWHg 0.000015 /0.000142 mg/L /
12/07/2018 S UTP1120718Se1f 0.000003 /0.000142 mg/L /
Aug 2018 Week 2 0.000002 / mg/L /
Sep 2018 Week 2 0.000001 / mg/L /
Oct 2018 Week 1 0.000006 / mg/L /
Nov 2018 Week 3 0.000004 / mg/L /
Nov 2018 Week 4 •
0.000015 / mg/L /
Dec 2018 Week 1 0.000003 / mg/L /
Aug 2018 Average 0.000002 / mg/L /
Sep 2018 Average 0.000001 / mg/L /
Oct 2018 Average 0.000006 / mg/L /
Nov 2018 Average 0.00001 / mg/L /
Dec 2018 Average 0.000003 / mg/L /
2018 Quarter 3 0.000001 / mg/L /
2018 Quarter 4 0.000007 / mg/L /
2018 2nd 6 Months(Avg) 0.0000051 / mg/L /
2018 2nd 6...(Max) 0.000015 / mg/L /
2018 2nd 6...(Min) 0.0000008 / mg/L /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 5 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/09/2018 S UTP1080918Self < 0.003 / mg/L < /
11/28/2018 P UTP1112818POTW < 0.001 / mg/L < 0.0004 / lbs/day
Aug 2018 Week 2 < 0.003 / mg/L < /
Nov 2018 Week 4 < 0.001 / mg/L < 0.0004 / lbs/day
Aug 2018 Average < 0.003 / mg/L < /
Nov 2018 Average < 0.001 / mg/L < 0.0004 / lbs/day
2018 Quarter 3 < 0.003 / mg/L < /
2018 Quarter 4 < 0.001 / mg/L < 0.0004 / lbs/day
2018 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0004 / lbs/day
2018 2nd 6...(Max) < 0.003 / mg/L < 0.0004 / lbs/day
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
08/09/2018 S UTP1080918Self 0.2 / mg/L /
11/28/2018 P UTP1112818POTW 0.8 / mg/L 0.273 / lbs/day
Aug 2018 Week 2 0.2 / mg/L /
Nov 2018 Week 4 0.8 / mg/L 0.273 / lbs/day
Aug 2018 Average 0.2 / mg/L /
Nov 2018 Average 0.8 / mg/L 0.273 / lbs/day
2018 Quarter 3 0.2 / mg/L /
2018 Quarter 4 0.8 / mg/L 0.273 / lbs/day
2018 2nd 6 Months(Avg) 0.5 / mg/L 0.273 / lbs/day
2018 2nd 6...(Max) 0.8 / mg/L 0.273 / lbs/day
2018 2nd 6...(Min) 0.2 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/09/2018 S UTP1080918Self 6.3 / mg/L /
11/28/2018 P UTP1112818POTW 11.8 / mg/L4.181 / lbs/day
Y
Aug 2018 Week 2 6.3 / mg/L /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 5 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
Nov 2018 Week 4 11.8 / mg/L 4.181 / lbs/day
Aug 2018 Average 6.3 / mg/L /
Nov 2018 Average 11.8 / mg/L 4.181 / lbs/day
2018 Quarter 3 6.3 / mg/L /
2018 Quarter 4 11.8 / mg/L 4.181 / lbs/day
2018 2nd 6 Months(Avg) 9.05 / mg/L 4.181 / lbs/day
2018 2nd 6...(Max) 11.8 / mg/L 4.181 / lbs/day
2018 2nd 6...(Min) 6.3 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/09/2018 S UTP1080918Self 6.8 /200 mg/L /
11/28/2018 P UTP1112818POTW < 2.5 /200 mg/L < /
Aug 2018 Week 2 6.8 / mg/L /
Nov 2018 Week 4 < 2.5 / mg/L < /
Aug 2018 Average 6.8 / mg/L /
Nov 2018 Average < 2.5 / mg/L < /
2018 Quarter 3 6.8 / mg/L /
2018 Quarter 4 < 2.5 / mg/L < /
2018 2nd 6 Months(Avg) < 4.65 / mg/L < /
2018 2nd 6...(Max) 6.8 / mg/L /
2018 2nd 6...(Min) < 2.5 / mg/L < /
2018 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/13/2018 S UTP1071318Self 8.6 /5.5- 10 SU /
08/09/2018 S UTP1080918Se1f 6.4 /5.5- 10 SU /
09/13/2018 S UTP1091318Self 6.7 /5.5- 10 SU /
10/05/2018 S UTP1100518Se1f 6.2 /5.5- 10 SU /
11/16/2018 S UTP1111618Se1f 8.6 /5.5- 10 SU /
11/28/2018 P UTP1112818POTW 6.9 /5.5- 10 SU /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 6 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
12/07/2018 S UTP1120718Self 8.7 /5.5- 10 SU /
Jul 2018 Week 2 8.6 / SU /
Aug 2018 Week 2 6.4 / SU /
Sep 2018 Week 2 6.7 / SU /
Oct 2018 Week 1 6.2 / SU /
Nov 2018 Week 3 8.6 / SU /
Nov 2018 Week 4 6.9 / SU /
Dec 2018 Week 1 8.7 / SU /
Jul2018 Average 8.6 / SU /
Aug 2018 Average 6.4 / SU /
Sep 2018 Average 6.7 / SU /
Oct 2018 Average 6.2 / SU /
Nov 2018 Average 7.75 / SU /
Dec 2018 Average 8.7 / SU /
2018 Quarter 3 7.23 / SU /
2018 Quarter 4 7.6 / SU /
2018 2nd 6 Months(Avg) 7.44 / SU /
2018 2nd 6...(Max) 8.7 / SU /
2018 2nd 6...(Min) 6.2 / SU /
2018 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
1 #Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/13/2018 S UTP1071318Self 26.2 /66 °C /
08/09/2018 S UTP1080918Se1f 23.4 /66 °C /
09/13/2018 S UTP1091318Se1f 21.8 /66 °C /
10/05/2018 S UTP1100518SeIf 24.5 /66 °C /
1 11/16/2018 S UTP1111618Self 21.6 /66 °C /
11/28/2018 P UTP1112818POTW 14 /66 °C /
12/07/2018 S UTP1120718SeIf 21.1 /66 °C /
Jul 2018 Week 2 26.2 / °C /
Aug 2018 Week 2 23.4 / °C /
Sep 2018 Week 2 21.8 / °C /
Oct 2018 Week 1 24.5 / °C /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 7 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Nov 2018 Week 3 21.6 / °C /
Nov 2018 Week 4 14 / °C /
Dec 2018 Week 1 21.1 / °C /
Jul2018 Average 26.2 / °C /
Aug 2018 Average 23.4 / °C /
Sep 2018 Average 21.8 / °C /
Oct 2018 Average 24.5 / °C /
Nov 2018 Average 17.8 / °C /
Dec 2018 Average 21.1 / °C /
2018 Quarter 3 23.8 / °C /
2018 Quarter 4 20.3 / °C /
2018 2nd 6 Months(Avg) 21.8 / °C /
2018 2nd 6...(Max) 26.2 / °C /
2018 2nd 6...(Min) 14 / °C /
2018 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/09/2018 S UTP1080918Self 6.1 / mg/L /
11/28/2018 P UTP1112818POTW 11 / mg/L 3.897 / lbs/day
Aug 2018 Week 2 6.1 / mg/L /
Nov 2018 Week 4 11 / mg/L 3.897 / lbs/day
Aug 2018 Average 6.1 / mg/L /
Nov 2018 Average 11 / mg/L 3.897 / lbs/day
2018 Quarter 3 6.1 / mg/L /
2018 Quarter 4 11 / mg/L 3.897 / lbs/day
2018 2nd 6 Months(Avg) 8.55 / mg/L 3.897 / lbs/day
2018 2nd 6...(Max) 11 / mg/L 3.897 / lbs/day
2018 2nd 6...(Min) 6.1 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 8 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/09/2018 S UTP1080918Self 1.1 / mg/L /
11/28/2018 P UTP1112818POTW 1.79 / mg/L 0.6342 / lbs/day
Aug 2018 Week 2 1.1 / mg/L /
Nov 2018 Week 4 1.79 / mg/L 0.6342 / lbs/day
Aug 2018 Average 1.1 / mg/L /
Nov 2018 Average 1.79 / mg/L 0.6342 / lbs/day
2018 Quarter 3 1.1 / mg/L /
2018 Quarter 4 1.79 / mg/L 0.6342 / lbs/day
2018 2nd 6 Months(Avg) 1.445 / mg/L 0.6342 / lbs/day
2018 2nd 6...(Max) 1.79 / mg/L 0.6342 / lbs/day
2018 2nd 6...(Min) 1.1 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
08/09/2018 S UTP1080918Self 63.5 / mg/L /
11/28/2018 P UTP1112818POTW 64 / mg/L 22.674125 / lbs/day
Aug 2018 Week 2 63.5 / mg/L /
Nov 2018 Week 4 64 / mg/L 22.674125 / lbs/day
Aug 2018 Average 63.5 / mg/L /
Nov 2018 Average 64 / mg/L 22.674125 / lbs/day
2018 Quarter 3 63.5 / mg/L /
2018 Quarter 4 64 / mg/L 22.674125 / lbs/day
2018 2nd 6 Months(Avg) 63.8 / mg/L 22.6741 / lbs/day
2018 2nd 6...(Max) 64 / mg/L 22.674125 / lbs/day
2018 2nd 6...(Min) 63.5 / mg/L /
2018 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
07/13/2018 S UTP1071318Self 0.169 / mg/L /
08/09/2018 S UTP1080918Self 0.0578 / mg/L /
Jul 2018 Week 2 0.169 / mg/L /
Aug 2018 Week 2 0.0578 / mg/L /
Jul2018 Average 0.169 / mg/L /
Aug 2018 Average 0.0578 / mg/L /
2018 Quarter 3 0.1134 / mg/L /
2018 2nd 6 Months(Avg) 0.1134 / mg/L /
2018 2nd 6...(Max) 0.169 / mg/L /
2018 2nd 6...(Min) 0.0578 / mg/L /
2018 2nd 6...(Count) 2 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 9 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/09/2018 S UTP1080918Self < 0.06 / mg/L < /
11/28/2018 P UTP1112818POTW 0.247 / mg/L 0.087508 / lbs/day
Aug 2018 Week 2 < 0.06 / mg/L < /
Nov 2018 Week 4 0.247 / mg/L 0.087508 / lbs/day
Aug 2018 Average < 0.06 / mg/L < /
Nov 2018 Average 0.247 / mg/L 0.087508 / lbs/day
2018 Quarter 3 < 0.06 / mg/L < /
2018 Quarter 4 0.247 / mg/L 0.087508 / lbs/day
2018 2nd 6 Months(Avg) < 0.154 / mg/L < 0.087508 / lbs/day
2018 2nd 6...(Max) 0.247 / mg/L 0.087508 / lbs/day
2018 2nd 6...(Min) < 0.06 / mg/L < /
2018 2nd 6...(Count) 2 / 1 /
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/13/2018 S UTP2071318Se1f 0.169 /20.7 mg/L /
08/09/2018 S UTP2080918Self 0.017 /20.7 mg/L /
09/13/2018 S UTP2091318Self < 0.005 /20.7 mg/L < /
10/05/2018 S UTP2100518Self < 0.005 /20.7 mg/L < /
11/16/2018 S UTP2111618Se1f 0.022 /20.7 mg/L /
12/07/2018 S UTP2120718Self 0.077 /20.7 mg/L /
Jul 2018 Week 2 0.169 / mg/L /
Aug 2018 Week 2 0.017 / mg/L /
Sep 2018 Week 2 < 0.005 / mg/L < /
Oct 2018 Week 1 < 0.005 / mg/L < /
Nov 2018 Week 3 0.022 / mg/L /
Dec 2018 Week 1 0.077 / mg/L /
Jul 2018 Average 0.169 /8.2 mg/L /
Aug 2018 Average 0.017 /8.2 mg/L /
Sep 2018 Average < 0.005 /8.2 mg/L < /
Oct 2018 Average < 0.005 /8.2 mg/L < /
Nov 2018 Average 0.022 /8.2 mg/L /
Dec 2018 Average 0.077 /8.2 mg/L /
2018 Quarter 3 < 0.064 / mg/L < /
2018 Quarter 4 < 0.035 / mg/L < /
2018 2nd 6 Months(Avg) < 0.049 / mg/L < /
2018 2nd 6...(Max) 0.169 / mg/L /
2018 2nd 6...(Min) < 0.005 / mg/L < /
2018 2nd 6...(Count) 6 / /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/13/2018 S UTP2071318Self < 0.05 /20.7 mg/L < /
08/09/2018 S UTP2080918Self < 0.05 /20.7 mg/L < /
09/13/2018 S UTP2091318Se1f < 0.05 /20.7 mg/L < /
10/05/2018 S UTP2100518Self < 0.05 /20.7 mg/L < /
11/16/2018 S UTP2111618Se1f < 0.05 /20.7 mg/L < /
12/07/2018 S UTP2120718Se1f < 0.05 /20.7 mg/L < /
Jul2018 Week 2 < 0.05 / mg/L < /
Aug 2018 Week 2 < 0.05 / mg/L < /
Sep 2018 Week 2 < 0.05 / mg/L < /
Oct 2018 Week 1 < 0.05 / mg/L < /
Nov 2018 Week 3 < 0.05 / mg/L < /
Dec 2018 Week 1 < 0.05 / mg/L < /
Jul 2018 Average < 0.05 /8.2 mg/L < /
Aug 2018 Average < 0.05 /8.2 mg/L < /
Sep 2018 Average < 0.05 /8.2 mg/L < /
Oct 2018 Average < 0.05 /8.2 mg/L < /
Nov 2018 Average < 0.05 /8.2 mg/L < /
Dec 2018 Average < 0.05 /8.2 mg/L < /
2018 Quarter 3 < 0.05 / mg/L < /
2018 Quarter 4 < 0.05 / mg/L < /
2018 2nd 6 Months(Avg) < 0.05 / mg/L < /
2018 2nd 6...(Max) < 0.05 / mg/L < /
2018 2nd 6...(Min) < 0.05 / mg/L < /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 1 of 4
I

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/13/2018 S UTP2071318Se1f < 0.05 /20.7 mg/L < /
08/09/2018 S UTP2080918Se1f < 0.05 /20.7 mg/L < /
09/13/2018 S UTP2091318Self < 0.05 /20.7 mg/L < /
10/05/2018 S UTP2100518Se1f < 0.05 /20.7 mg/L < /
11/16/2018 S UTP2111618Se1f < 0.05 /20.7 mg/L < /
12/07/2018 S UTP2120718Self < 0.05 /20.7 mg/L < /
Jul2018 Week 2 < 0.05 / mg/L < /
Aug 2018 Week 2 < 0.05 / mg/L < /
Sep 2018 Week 2 < 0.05 / mg/L < /
Oct 2018 Week 1 < 0.05 / mg/L < /
Nov 2018 Week 3 < 0.05 / mg/L < /
Dec 2018 Week 1 < 0.05 / mg/L < /
Jul 2018 Average < 0.05 /8.2 mg/L < /
Aug 2018 Average < 0.05 /8.2 mg/L < /
Sep 2018 Average < 0.05 /8.2 mg/L < /
Oct 2018 Average < 0.05 /8.2 mg/L < /
Nov 2018 Average < 0.05 /8.2 mg/L < /
Dec 2018 Average < 0.05 /8.2 mg/L < /
2018 Quarter 3 < 0.05 / mg/L < /
2018 Quarter 4 < 0.05 / mg/L < /
2018 2nd 6 Months(Avg) < 0.05 / mg/L < /
2018 2nd 6...(Max) < 0.05 / mg/L < /
2018 2nd 6...(Min) < 0.05 / mg/L < /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/13/2018 S UTP2071318Self < 0.001 /3 mg/L < /
08/09/2018 S UTP2080918Se1f < 0.001 /3 mg/L < /
09/13/2018 S UTP2091318Self < 0.001 /3 mg/L < /
10/05/2018 S UTP21005I8Self < 0.001 /3 mg/L < /
' 11/16/2018 S UTP2111618Self < 0.001 /3 mg/L < /
12/07/2018 S UTP2120718Se1f < 0.001 /3 mg/L < /
Jul 2018 Week 2 < 0.001 / mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 2 of 4

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outfall.: 002
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
Aug 2018 Week 2 < 0.001 / mg/L < /
Sep 2018 Week 2 < 0.001 / mg/L < /
Oct 2018 Week 1 < 0.001 / mg/L < /
Nov 2018 Week 3 < 0.001 / mg/L < /
Dec 2018 Week 1 < 0.001 / mg/L < /
Jul2018 Average < 0.001 /0.7 mg/L < /
Aug 2018 Average < 0.001 /0.7 mg/L < /
Sep 2018 Average < 0.001 /0.7 mg/L < /
Oct 2018 Average < 0.001 /0.7 mg/L < /
Nov 2018 Average < 0.001 /0.7 mg/L < /
Dec 2018 Average < 0.001 /0.7 mg/L < /
2018 Quarter 3 < 0.001 / mg/L < /
2018 Quarter 4 < 0.001 / mg/L < /
2018 2nd 6 Months(Avg) < 0.001 / mg/L < /
2018 2nd 6...(Max) < 0.001 / mg/L < /
2018 2nd 6...(Min) < 0.001 / mg/L < /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/13/2018 S UTP2071318Se1f < 0.025 /20.7 mg/L < /
08/09/2018 S UTP2080918Se1f < 0.05 /20.7 mg/L < /
09/13/2018 S UTP2091318Se1f < 0.025 /20.7 mg/L < /
10/05/2018 S UTP2100518Self < 0.025 /20.7 mg/L < /
11/16/2018 S UTP2111618Se1f < 0.025 /20.7 mg/L < /
12/07/2018 S UTP2120718Self < 0.025 /20.7 mg/L < /
Jul 2018 Week 2 < 0.025 / mg/L < /
Aug 2018 Week 2 < 0.05 / mg/L < /
Sep 2018 Week 2 < 0.025 / mg/L < /
Oct 2018 Week 1 < 0.025 / mg/L < /
Nov 2018 Week 3 < 0.025 / mg/L < /
Dec 2018 Week 1 < 0.025 / mg/L < /
Jul 2018 Average < 0.025 /8.2 mg/L < /
Aug 2018 Average < 0.05 /8.2 mg/L < /
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 3 of 4

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2018 To 12/31/2018 Sample Type: Effluent Wastewater Outtalk 002
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Sep 2018 Average < 0.025 /8.2 mg/L < /
Oct 2018 Average < 0.025 /8.2 mg/L < /
Nov 2018 Average < 0.025 /8.2 mg/L < /
Dec 2018 Average < 0.025 /8.2 mg/L < /
2018 Quarter 3 < 0.033 / mg/L < /
2018 Quarter 4 < 0.025 / mg/L < /
2018 2nd 6 Months(Avg) < 0.029 / mg/L < /
2018 2nd 6...(Max) < 0.05 / mg/L < /
2018 2nd 6...(Min) < 0.025 / mg/L < /
2018 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Friday,February 22,2019 *Indicates Violation **Indicates TRC Violation Page 4 of 4