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HomeMy WebLinkAboutWQ0032723_Residual Annual Report 2018_20190301INITIAL REVIEW Reviewer Williams, Kendall Project Number* WO0032723 SUBMITTAL DATED: 2/26/2019 Project Contact Information Rease provide inforrration on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Brent Collins Email Address* Phone Number* brent.collins@emaresourcesinc.com 336-751-1441 Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0032723 Reviewer* Troy Doby Permittee * Chuck Smith Facility Name * City of Reidsville WTP County* Rockingham r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Reidsville WTP Annual Report WQ0032723.pdf 2.62MB Application Form Engineering Rans, Specifications, Calculations, Etc.) For nein and modification permit applications, the paper copy is required to be subrrutted to the Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic applications have been received_ The paper copy shall include the follo-kAmig: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineenng plan sets • 1 extra set of specifications (in addition to the set of specifications provided in the attachments) • Fee (if required) This shall be mailed to the following address: By U_S_ Postal Service: Division of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigb_ NC 27699-1613 By CourieriSpecial Delivery: Division of Water Resources- Non -Discharge Branch Ag Nathaniel Thornburg- 9th Floor, Office #942WN 512 N_ Salisbury St_ Raleigh,NC 27604 For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov. * I;W By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Sign Submission Date 2/26/2019 M N t` N M 0 a z a 0 0 M 0 0 v O O cd -a y0000 00 L.a r 'u z N N U � � O b 0000 � � 0 a o 0 0 Ln � O O � v v � �d v d o I cr w w � A � O " •CL Gni d O X y V 4i L a w 0 0 �;r��Q�•°,�QznOZC E� 0 M 9 F z 0 d a� E E E E E E o 'o 'o 'o O ' C t C y C 'Clr a Cd '_' a3 o lu O � � U � Q O N In O r r- r-- 00 a C o 0 � O 3333 aA, ,° G> cn r V� u C C O O O O 0 y Q) V 0000 0 F .�-i N M � 4n I 04 N � a � N y M `O cJ O 3� z - ai Q U 0 � M N t/ -r O M N 60 M S N'n kn' N 0 kn V1 O¢ O r- � O O O¢¢¢ ��zt L, r- N C)�zzzz Cd A a M N N M O O N M IT kn M �D r1' O O U z 0 0 N _N m LL U) U) w Z> O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): Permit #: WQ0032723 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: Acres Used: 69 Acres Permitted: 69 Site #: RC001 Field #: 37.26 CgB2 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): OW7 M-1 Com- posite Date 11 1213 L.4J 5 6 71 MEMmOi L 9 10 Ill 1 1121 DT/Ac./ c App' Event 0.54 .. Arsenic 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Chromiuinj 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Lead 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- denum 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Nickel 0.014 TotalPhos- __phorus"MENEENEENEEN 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 1213 L.4J 5 6 71 81 L 9 10 Ill 1 1121 DT/Ac./ c App' Event 0.54 .. Arsenic 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Chromiuinj 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Lead 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- denum 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Nickel 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Selenium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Zinc 1 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Total Phos- 1.652 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.652 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z� 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O, IC O ai 3 L u I i 0 0 C C4 S L G. L u L9 m 0 0 N LL LL 2 of O LL Z W 0 N w+ � _ O � U a L ^o O y 'C o ro UCL G, Z n LC y CC •4J U U U V V U y V V O O aR+ Q CY L 6� � 1"' Z U w w w w w w O •L a..� N ^' r� N O Q Q Q Qac• •z C � O aF aE as �• a; C� aF pp •Q•, Z Z Z ZQ U a� U Q en O 00 In M o O O o O 0 O o O Coo O ,� o aQ o-? 0o o O ? U M 00 Ci -n N O C O C O O � y Y "0 O CT a z �z E . w s \C � m Ammonia � 0 0 0 0 0 0 Nitrogen E � v �t "t � � 't � a a 7 :. vi m E v'i vi M GTr C O O 00 o 0 0 .. Mineralization Rate*** 0 0 0 0 0 0 z O N N M O 0 O O Volatilization w) n v, . kn n c° o Rate** o 0 0 0 0 o n S 0 0 Lz. w $ Application V� cl� CIO V� �n V� o o Method* 0 0 0 .�. 4 - V V V V V V m R O v V Q Q Q Q Ca D Q O U o d rr U a 00 0C� C, �a� - � 9L4H H a. � 3 3 3 3 3 3 3 Q v" CA QvN Lia cd y 5 -R rn 'C ;'O 5in t d N 7G LL Ce CG 04 C4 C4 U O O O L V et O Cn M O O O O O O .� �• Q o 0 0 0 0 0 0 0 0 0 0 o c o d a z Q o � DD 00 DD 00 DD o N N N N _� N N � U O 00 O CO o o CP\ c 'C� U >_ E z ujuOw M aoaooa � �� .toa� �•�}_o+� � L9 m 0 0 N LL LL 2 of O LL Z W 0 w+ � _ O � a L ^o O y 'C Q G, Z LC y CC w 'Ci y V V O O aR+ L 6� O � O •L a..� N ^' r� Qac• •z C � O aF aE as �• a; C� aF L9 m 0 0 N LL LL 2 of O LL Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville - WTP Total Dry Tons Applied (Annual): 6.50 WQ0032723 Cation Exchange Capacity (non 503 only): Ronnie Marshall Owner: Jane Marshall Predominant Soil Series: CgB2 15 Acres Permitted: 15 Site #: RC002 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent M - nnua eavy e a Fie oa m2s (Calculated in lbs acre): Total Llj L2J 131 non 151 a L7J 18191 moo 110111 12 Com- DT/Ac./ " 3 0 App. MENEM posite I tv Event 0.43 moo Date 14 Arsenic 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.013 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 _____________ 0.000 0.000 0.000 0.000 0.001 Copper 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Chromium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Lead 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- denum 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Nickel 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Selenium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Zinc 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Total Phos- 1.325 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.325 horus � Miiiiiiiiiii nnua eavy e a Fie oa m2s (Calculated in lbs acre): Total Llj L2J 131 4 151 6 L7J 18191 110111 12 DT/Ac./ " 3 0 App. tv Event 0.43 14 Arsenic 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.013 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Chromium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Lead 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- denum 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Nickel 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Selenium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Zinc 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Total Phos- 1.325 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.325 horus 1 cerWy, under penalty of iaw, tnat this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) n n ai O L Zj U y in i I Aw is 0 0 N_ LL CO LL 0 LL w Z W 0 a N " ¢ cOi � z U N O. Q' dO O p O O C O O O O p b b O O Z O O O O O O O O O O O O C4 U U C O C C O C C C C O C C Q z ^ 0. N O O O O OO O O O O O O O O O O O C O O O O N U N C C O C C O O C CO O C N 0,2 Z � P. M : E d i r.......... 4° 00 N t � N OC Amnioma O) Nitrogen E - -* p w N O C N M v •�: N n. d eF O 7 00 O O m z d dv m Vim] 66 V� pOp Mineralization O vim,' Rate*** C rs z o N C w Volatilization Rate** " 0 0 0 a w Application Method* C o o ^ ° a.. o 0 o N a a. 0 • � 0 �,' N .O i G N M �p U O et eh a� w d x z x C d C s. U U p O O O d O 0 0 d 0 '-+ t O U F a 7 0 0 0 0 0 0 0 0 0 0 0 Q' O O O ? O C O G C C C C C O C C C O C Q O o b � O nj U U d c O * o (d iF N O ads+ '�• U (; � G, ' n U ya gluo N Q QCL. Uaw I Aw is 0 0 N_ LL CO LL 0 LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): Permit #: WQ0032723 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: Catherine Neal Predominant Soil Series: Acres Used: 27.45 Acres Permitted: 27.45 Site #: RC004 Field #: 37.30 CgB2 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 WWTP 4/4/18 21 WWTP 7/13/18 31 WTP 10/2/18 L4J5 J 67 7 8 9 10 11 12 % Solids 1.46 1.1 2.18 Arsenic 3 5 15.1 Cadmium 2 1.9 1 0.07 0.66 0.62 Copper 180 204 109 Arsenic 0.000 0.007 0.019 0.000 0.000 0.000 0.000 0.000 Chromium 59.9 43.7 33.5 0.026 Cadmium 0.000 0.003 0.001 0.000 0.000 0.000 0.000 Lead 61.5 59.8 12.7 0.000 0.004 Copper 0.026 0.271 0.136 0.000 0.000 0.000 Mercury 2.96 0.8 0.0563 0.000 0.000 0.432 Chromium0.009 0.058 0.042 0.000 0.000 Molyb- denum 5 6.84 2.84 0.000 0.000 0.000 0.108 Lead 0.009 0.079 0.016 0.000 Nickel 33.5 21.2 13.1 0.000 0.000 0.000 0.000 0.104 Mercury 0.000 0.001 0.000 Selenium 5 5 5 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.001 0.009 Zinc 509 552 32.9 0.000 0.000 0.000 0.000 0.000 0.000 0.013 denum Total Phos- horus 15800 20500 1530 Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 L 2 31 4 1 1 51 6 7 8 9 10 11 12 DT/Ac./ oy* App. Event 0.07 0.66 0.62 Arsenic 0.000 0.007 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Cadmium 0.000 0.003 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.026 0.271 0.136 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.432 Chromium0.009 0.058 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Lead 0.009 0.079 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Mercury 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.001 0.009 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 denum Nickel 0.005 0.028 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Selenium 0.001 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Zinc 0.073 0.732 0.041 0.000 0.000 0.000 10.000 0.000 0.000 0.000 0.000 0.000 0.846 Total Phos- 2.275 27.183 1.909 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 31.368 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) t\ N O 0. r.+ C0 N .L" r•.i L ILI C O_ N W1 4py V .Q �+ M.tl w to C v�a p y p n i C • y O � � •p C y U Cc, N opo ON j 3 o.o :3U 2N N' N d Cj u Z� 0a U rUn w w w vVi w w vVi w u°.' 0 0 O •�y Z Z Z Z z Z 0 :: s0-, U '� a� d � N d .,. ..r M H .�•� m eF 0 0 5 0 25 0 25 0 `'O O 00 L-: N O 6 6 6 6 6 : � N � y Z cC zN N N N N d' O m.......:.:... w Ammonia 0 0 0 0 000 Nitrogen E` c c w N c v vi N a a m Z x O O O O O O O m w /) s� 00 1.0r a E- E w o 0 0 w a •� � d• r � Mineralization M M M M M r1 v O �V N N Rate*** r+ Volatilization w-, w% .n . - 0 0 0 Rate** o 0 0 0 0 0 o nc o 0 0 7 h w Application o o c Method* V N L V'1 V'1 V'1 Vl V'1 V1 `. JD yam', a g v v v v v v' v t+ y U c o 0 w_ 00 3 3 3 3 3 3 3 3 Q ULn O N M •�� 33333 d - - Z 3 v S o o M a w ; ;v o .2 72 v U Z tx a�, C a! o o O x 0 0 0 0 0 N n s0. c 7 v O O O ••-� c�+i N •r-� N vNi 0 0 0 u7 4 d C C CO C O O C O O C C C C C CO d � -d p o0 DD N N U «3 a � •x• y o 0 0 0 o 00000�no p (Q N 00 W) N wi • ftS N ry/1 U O w V .. c, U ti Q 00 00 00 00 0 0 0 � •�. � a� � �- Ra Ua a r.+ C0 .L" r•.i L ILI C O_ N W1 4py V .Q �+ M.tl w to C v�a p y p n i C • y O � � •p C y U Cc, N opo ON j 3 o.o :3U Zi 0 0 0 N N LL CO LL O LL w Z w 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): 29.36 Permit #: WQ0032723 Cation Exchange Capacity (non 503 only): Operator: Harry Sharpe Owner: Daisy Purgason Predominant Soil Series: NaB Acres Used: 19 Acres Permitted: 19 Site #: RC011 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): •-. Com- posite Date LIJ WTP 10/2/18 3 141L5J 6 71 L8 1 91 110111 J 1121 y DT/Ac./ 0 App. Event 0.61 0.93 Arsenic 1 0.004 0.028 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.032 Cadmium 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.207 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.410 hromium 0.054 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Lead 0.074 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 denum Total • phorus'MENEEMENEEN. M Nickel Annual Heavv Metal Field Loadinus (Calculated in lbs/acre): Total LIJ L2 3 141L5J 6 71 L8 1 91 110111 J 1121 y DT/Ac./ 0 App. Event 0.61 0.93 Arsenic 1 0.004 0.028 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.032 Cadmium 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.207 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.410 hromium 0.054 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Lead 0.074 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 denum Nickel 0.028 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.052 Selenium 0.006 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Zinc 0.682 0.061 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.743 Total Phos- 27.540 2.855 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 30.395 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". zzz 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Z ', O O U A 00 r- Tii RS *' G +" L N � CiC O O O y � Q CG y try + C W C y u t«. 2 S a q 0 3 0 a ° o a y u U c O � � z N O Q ¢ ¢ Q Q ¢ O O p O O O S. •—p, 2 z z z z z O O a� J o co co 0 0 0 0 .: `t `-' o � `R '•*. p o 0 0 0 0 0 0 0 0 0 o0 o�Oj v`ri ' CC •b Y M M M M O, O, ^••\ Q� V° +� � �r .......... o d• p ... Ammonia � 0 0 0 0 0 0 0 0 ,r, ,,, Nitrogen EN N N N o v v N G, d O O Z .v, 0 0 0 0 0 0 Ex- E 00 � 00 0000 � OC Ch U] O opo Mineralization M M M K v O vNi o� Rate*** o 0 0 0 0 o GTy r Z O o N M M 0 0 w Volatilization n v° o o Rate** 0 0 0 0 0 0 0 0 0 O fs w _ S o o Application Method* V� �r �n U� C10 0 0 0 d a r p `o .'. a �y V V V V V V O O O O N�� O _ O N U Q 3 Q Q Ca Q Q Q o U o 0 0 a u d 0 3 0 3 3 3 3 3 3 u11: ... C4 U 0 0 0 t-. U N Q Q00 c N N 0 0 0 C cjO x O N h N O �D d' N O O 0 O O 0 O 0 O 0 v. Q' rNi D 0 er 000 O O M 0 0 0 0 0 0 0 0 0 0 0 0 0 Q � 10 N (-i U o M a> * C v p c o 0 0 0 p W) �_ S].f6 VD in r U c'sU'Z:�Q t1juOW W 00 10 211'Q E- Q a. U Gy a. RS *' G +" L N � CiC O O O y � O y try + C W C y u t«. 2 S a q 0 3 0 a ° o a y u U c O � � M a 0 0 N N_ LL U) LL O LL w Z W 0 Waypointw ANALYTICAL 10/11/2018 EMA Resources Inc 755 Yadkinville Road Mocksville, NC, 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-4401 ° Fax 804-271-6446 www.waypointanalytical.com Ref: Analytical Testing Report Number: 18-276-0204 Project Description: Reidsville WTP Waypoint Analytical Virginia, Inc, received sample(s) on 10/3/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 257 South Carolina 93007 Page 1 of 6 WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 07621 Whitepine Road, Rithmond, VA 23237Waypaint . Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-276-0204 Client Project Description: Reidsville WTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 SM -2540G WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 SW -74716 WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 SM-4500-NH3C-TKN WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 4500NO3F-2011 WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 6010D WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 SM-4500-NH3C WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 9045D WTN 62983 Reidsville WTP Solids 10/02/2018 09:30 10/03/2018 AOAC 955.01 WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 M E U M CD N .-4 V 9 N T 0 C M LL C a .60 3 o O1 3 OC M c h 3fi d0c0 L 3 Cm *4 C N h J OJ w 0 N O LO h N 00 to d E 7 7 Z Z +� c a °u � a O M O 0 0000 — - O O O N N N ( ) to N O T 0 0 0 a F - v 00 N � N E M a Z E a 10 � h Z Y U Z r (� U 2 - N t 0 _ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ Z Q LL Z O O O O O MOvNoowowwww000UZco o mcococo CD /i U} L <O U LO 7 M M CO 00 O N N tt mt O M In o w M o 6i 6i o 0 6i 6; v o o ao cYi 6 r r N r r N N r r r r N N T T r 0w O O 00 00 w N O 00 00 w 00 00 W 00 O T r r r T r T r r T r D O O O O O O O O O O O Co O O O O V N N N N N N N N N N N N N N N N O O m m r O O O O O O O O O O O O O O O O r r T T r r r r r r r r T r T r Y d Z x 2 2 x w 2 2 x w d ❑ mF- Y Y�F- Y Y U N O O p O O O p O p O p O O O O p O O O N O O O O O if i O O O Lq O O N CD Or r U-) U-) LO `' 0 N to to LO N U.) U-) 0 000 L M d O 00 0000 O W C) O 0.) N Ln 0) COO �t I- CO - CO f� M N M � co V N h OT OR O CWO• r O O ? C? N fes• O O O O O O O CD c N O c O Z O Z w � L h Nz E 0 0 7 Z Z cn O Y a .N m c m o E a+i ca o C E H d d n 0 2 ) 2 Q 2 U N a o z c M :d c0 N O O c O N 15 LOm M tD 0 N z m > co c— It e - CMO j N 'L O O W m (� a m M ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ C C O O e- O O <- O — O r ^ O r M tt O 0 O r O IO E �Z Z H o E E N E U m c H C O .� U o O T O N N d �p 0_ i Q C rl N M Lo Q m ccn =a V m U N O ` c 3 m COW 'm 0 d E Q of of O O M ai o0 6> W of .0 C V N N 3 00 00 co 00 co 00 00 00 00 oo ,4 N ;; m R m o N o N 0 N 0 N_ O N 0 N O N 0 N 0 N 0 0 N N ❑ ❑ ❑ O O O O O Q O O O a O O F- O O O O O O O O O O O > T r r r r — r T r — r m 0 Y � Y�� m w v m � vj � Z Cl) v O O OLf) O O O O p O o Lo N N M to O L6N O ►i Q �Z a a W n T Cl) O Q p O O 00 r• M M M r to — p L6 O e' r N V O V N O O r r N d' N Zn Qi 3 m c O .T m m m z f0 C O E c 0 U m ❑ v C IZ wr m 3m L7 �t c0 N O c O N 15 LOm 0 N z m > co c— It O C m CMO y O W wea N d Q U CO O @ E 3 w � E �Z Z H o E E E U m c H C O .� U :3E O C d �p 0_ i Nco O Q m ccn =a U N Zn Qi 3 m c O .T m m m z f0 C O E c 0 U m ❑ v C IZ wr m 3m L7 �t Waypoint-Q) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 18-276-0204 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received F1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) _ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: lBrandi Watson Date & Time: 10/03/201814:49:48 Page 5 of 6 L - Page 6 of(i aceAnaiyticai® ANALYTICAL REPORT i National Center /or Testing 8 Innovation October 12, 2018 i EMA Resources Sample Delivery Group: L1031256 Samples Received: 10/03/2018 Project Number: Description: Reidsville WTP Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By: , Cassandra Foster Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. this test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. TABLE OF CONTENTS ONE LAB. NATIONWIDE. * Ss: Sample Summary 3 Im Cn: Case Narrative Sr: Sample Results 4 5 FS REIDSVILLE WTP L1031256-01 5 Qc: Quality Control Summary 7 Fn Wet Chemistry by Method 9012 B 7 Fr Wet Chemistry by Method 9034-90308 Wet Chemistry by Method 9045D 8 9 FQc Wet Chemistry by Method D93/1010A 10 Fil Mercury by Method 7470A 12 Metals (ICP) by Method 6010D 13 Volatile Organic Compounds (GC/MS) by Method 8260B 14 Chlorinated Acid Herbicides (GC) by Method 8151A 16 9SC Pesticides (GC) by Method 80818 17 Semi Volatile Organic Compounds (GC/MS) by Method 8270D 18 Glossary of Terms 20 ,AGI: I^' NA.c ,dr. i:'. 4 �o ."^ ii-' e_..t ... ',. psi... •... Sc: Sample Chain of Custody 22 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1031256 10/12/1813:36 2 Of 22 SAMPLE SUMMARY ONE LAB. NATIONWIDE. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1091256 10/12/18 13:36 3 of 22 RC Collected by Collected date/time Received date/time REIDSVILLE WTP L1031256-01 Waste Brent Collins 10/02/1809:35 10/03/1809:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Preparation by Method 1311 WG1175874 1 10/04/1813:57 10/04/1813:57 RT Preparation by Method 1311 WG1177292 1 10/07/1811:06 10/07/1811:06 TM Wet Chemistry by Method 9012 B WG1178216 1 10/09/1815:51 10/10/18 07:45 KK Wet Chemistry by Method 9034-9030B WG1178257 1 10/10/1814:50 10/10/1814:50 MJA Wet Chemistry by Method 9045D WG1176301 1 10/05/18 07:30 10/05/1811:30 AMB Wet Chemistry by Method D93/1010A WG1175868 1 10/08/1817:16 10/08/1817:16 TH Mercury by Method 7470A WG1177525 1 10/08/18 09:10 10/08/1818:04 ABL Metals (ICP) by Method 6010D WG1177581 1 10/08/1810:30 10/08/1814:53 ST Volatile Organic Compounds (GC/MS) by Method 82606 WG1176411 1 10/05/1817:59 10/05/1817:59 JHH Chlorinated Acid Herbicides (GC) by Method 8151A WG1177879 1 10/10/18 07:30 10/11/1817:43 KLM Pesticides (GC) by Method 80818 WG1177768 1 10/09/1814:32 10/11/1815:31 RP Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1177583 1 10/11/18 06:55 10/11/18 20:26 AO ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1091256 10/12/18 13:36 3 of 22 RC CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within r the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my RSknowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 M El Cassandra Foster Project Manager BSc Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 90126. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1031256 10/12/18 1336 4 of 22 REIDSVILLE WTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 10/02/18 09:35 L1031256 Preparation by Method 1311 Result Qualifier Prep Batch Analyte date / time TCLP Extraction 10/7/201811:06:28 AM WG1177292 TCLP ZHE Extraction 10/4/20181:57:37 PM WG1175874 Fluid 1 10/7/201811:06:28 AM WG1177292 Initial pH 6.84 10/7/201811:06:28 AM WG1177292 Final pH 4.95 10/7/201811:06:28 AM WG1177292 Wet Chemistry by Method 9012 B Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date / time Reactive Cyanide ND 0.250 1 10/10/2018 07:45 w Wet Chemistry by Method 9034-9030B Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date / time Reactive Sulfide 84.4 25.0 1 10/10/201814:50 Wet Chemistry by Method 9045D Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 6.99 T3 1 10/05/201811:30 Sample Narrative: L1031256-01 WG1176301: 6.99 at 20.6C Wet Chemistry by Method D93/1010A Result Qualifier Dilution Analysis Batch Analyte Deg. F date / time Ignitability DNI at 170 1 10/08/201817:16 Mercury by Method 7470A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Mercury ND 0.0100 0.20 1 10/08/201818:04 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Arsenic ND 0.100 5 1 10/08/201814:53 Barium ND 0.100 100 1 10/08/201814:53 Cadmium ND 0.100 1 1 10/08/201814:53 Chromium ND 0.100 5 1 10/08/201814:53 Lead ND 0.100 5 1 10/08/201814:53 Selenium ND 0.100 1 1 10/08/201814:53 v Silver ND 0.100 5 1 10/08/201814:53 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Benzene ND 0.0500 0.50 1 10/05/201817:59 Carbon tetrachloride ND 0.0500 0.50 1 10/05/201817:59 Chlorobenzene ND 0.0500 100 1 10/05/201817:59 Chloroform ND 0.250 6 1 10/05/201817:59,' ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1031256 10/12/18 13:36 5 of 22 BSc REIDSVILLE WTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 10/02/18 09:35 L1031256 Volatile Organic Compounds (GC/MS) by Method 8260B ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: FMA Resources L1031256 10/12/1813:36 6 of 22 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time 1,2-Dichloroethane ND 0.0500 0.50 1 10/05/201817:59 1,1-Dichloroethene ND 0.0500 0.70 1 10/05/201817:59 2-Butanone (MEK) ND 0.500 200 1 10/05/201817:59 V,a Tetrachloroethene ND 0.0500 0.70 1 10/05/201817:59 SS Trichloroethene ND 0.0500 0.50 1 10/05/201817:59 Vinyl chloride ND 0.0500 0.20 1 10/05/201817:59 FCn] (S) Toluene -d8 112 80.0-120 10/05/201817:59 (S) Dibromofluoromethone 91.8 75.0-120 10/05/201817:59 (S)o,o,a-Trifluorofoluene 105 80.0-120 10/05/20181759 (S)4-Bromofluorobenzene 95.6 77.0-126 10/05/201817,59 Chlorinated Acid Herbicides by Method 8151A �QC (GC) Result Qualifier RDL Limit Dilution Analysis Batch 7G) Analyte mg/I mg/I mg/I date / time 2,4,5 -TP (Silvex) ND 0.00200 1 1 10/11/201817:43 - 2,4-5 ND 0.00200 10 1 10/11/201817:43 (S) 2,4-Dichlorophenyl Acetic Acid 77.0 14.0-158 10/11/20181743 Pesticides by Method 8081B Rc (GC) Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time Chlordane ND 0.00500 0.03 1 10/11/201815:31 Endrin ND 0.00500 0.02 1 10/11/201815:31 Heptachlor ND 0.00500 0.0080 1 10/11/201815:31 Lindane ND 0.00500 0.40 1 10111/201815:31 Methoxychlor ND 0.00500 10 1 10/11/201815:31 Toxaphene ND 0.0100 0.50 1 10/11/201815:31 (S) Decochlorobiphenyl 86.5 10.0-128 10/11/201815.'31 (S) Tetrochloro-m-xylene 83.1 10.0-127 10/11/201815:31 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,4 -Dichlorobenzene ND 0.100 7.50 1 10/11/2018 20:26 2,4-Dinitrotoluene ND 0.100 0.13 1 10/11/2018 20:26-' Hexachlorobenzene ND 0.100 0.13 1 10/11/2018 20:26 Hexachloro-1,3-butadiene ND 0.100 0.50 1 10/11/2018 20:26 Hexachloroethane ND 0.100 3 1 10/11/2018 20:26 Nitrobenzene ND 0.100 2 1 10/11/2018 20:26 Pyridine ND 0.100 5 1 10/11/2018 20:26 3&4 -Methyl Phenol ND 0.100 400 1 10/11/2018 2026 2-Methylphenol ND 0.100 200 1 10/11/2018 20:26 Pentachlorophenol ND J3 J4 0.100 100 1 10/11/2018 20:26 2,4,5 -Trichlorophenol ND 0.100 400 1 10/11/2018 20:26 2,4,6 -Trichlorophenol ND J30.100 e 2 1 10/11/2018 20:26 _ (S) 2-Fluorophenol 29.6 10.0-120 10/11/2018 20:26 (S) Phenol -d5 16.3 10.0-120 10/11/2018 2016 (S) Nitrobenzene -d5 59.1 10.0-127 10!11/2018 20:26 _ d_ (S)2-Fluoroblphenyl 64,0 10.0-130 10/11/201820:26 (5) 2, 4,6-Tribromophenol 31.6 10.0-155 10/11/2018 20.26 (S) p-Terphenyl-d14 72.8 10.0-128 10/11/2018 20:26 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: FMA Resources L1031256 10/12/1813:36 6 of 22 0 m N 2 E O iZ Q Q) U .Q D d O Q^) � L E cn ti C Q m O M O mi O J Q c6 U Q O Q) cQ L cc co C CD O O 00 O N M O J 0 Cf) U Q Q U7 X c� C co 2 Q) a X 4-1 Q) Q- E E M C�} C O N O of N m O J D W S z O r Q z ai Q J LU z 0 0 0 m v 0 a O .0 N m N 00m E e— t O QD w Y� G L. 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Z IL) O O O O O O O o O O O O M s O O O O O O O O O O O O OO OO Q O O O m E o 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 J M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M m O O O O O O O O O O O O 2E Cl o O O O O O O o O O CO s... 7 d N — N N O In R O y O s 0 o M O 3o o O o v o u t C 1p Cm c d axi -o v` v v_ ` c- i ca i �. v Q r N S Z S Z d N M d N N 4 E O_ O O N O w O O n . �-, 00 M r P M V n N a vIc� N .E O N O p p O O CD O C� O o R O J U O O p p O O O O O O O O O O u d o: V) N N O OO O } CO OJ tLDCD N O <V L2 W J o w m m n w t m - N m d n co a1 V d O O � O N N � W W U l0 I� O h l0 M u7 O N 00 M c p Oj lt) to to V l0 CD N N CO CO � N D O O 10 M N 61 In m ON d7 W Q1 OJ `M, CO e7- Oj U O O o O O O O O O O O O J E O O O o O O O O O O O o 0 L l0- C? 0MO o M J E O o 0 0 0 o O o 0 0 o 0 D u 0 U E J Q O O O O O O O O O O O o • d o o O o 0 0 0 0 o O O o � Y � In L.() Ln I.P L[) In LCJ LC) LCJ I.n Ln LCl Lp 'a 'p) O O o O O O O O O O O O CO In E o 0 o O o 0 0 0 0 o o O 00 IZy ol Ll1 v o o .c v .c a n ?. M o 0 0 0 M o o 0 o n L o u L — O/ L p~Ci u u V) r� d N W N 0 CL CO u U w O a 4 E m = a O O -0 N UP Fo-I Pul L --j E J Q o, o o O- o 'o r� V M M M M M M M N O O O M O O ^ M W M N O O O CLO M O M 61 N M O O = Cl O V M I.f) O O �I in Ln In M MI 01 19I (D N' w mlV) o O O O O O O O o O O O OO O OO O OO OO o Lri M M o o- - - - - - � O O W M f m� O n N c0 F, N o o O Oj Q ei O 07 1� h � h CO O 0 N N �2 V Q O O .-- d' O N V O N O O O N (p V 4) � v)� O O N l0 D7 O O O O 0 0 0 �o c0 6t n .- r W W o0 W m M N In ... rn O d MIx _ O M O O W O r OV CD .- � p E o 0 0 0 0 0 0 0 o cS z z . 3 (� N M L M N N O W N Cl In (D r N <n 6i V M M d0', O O 0 O o v V � c :rn — � O E z z z z z z z z z z z z M M C N o ? a yO O O O O O O O O O O O Y — O O O O O O O O O O O O 77 M a ai in m in Lq - in Lsi i Lo L,n n E O O O O O O CJ O O O O O N co a o C � v � C s o~a QO 's, 0 u u ao W U NQ Q a rn GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec, Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was Result no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results ofthe laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to This Custody (Sc) perform. chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1031256 10/12/1813:36 20 of 22 FS] a Cn D TQC 0 ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIQE. # Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Alabama 40660 Nebraska NE -OS -15-05 Alaska 17-026 Nevada TN -03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico' Colorado TNO0003 New York 117 11742 Connecticut PH -0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 41 Georgia' 923 North Dakota R-140 Idaho TNO0003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C -TN -01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky's 90010 South Carolina 84004 Kentucky l 16 South Dakota n/a Louisiana A130792 Tennessee' ° 2006 Louisiana' LA180010 Texas T 104704245-17-14 Maine TN0002 TexaS 5 LA80152 Maryland 324 Utah TNO0003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047.999-395 Washington C847 Mississippi TNO0003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA A2LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA — ISO 17025 s 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TNO0003 'Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological ' Mold a Wastewater n/a Accreditation not applicable Pace ational has sixty-four client support ---------- centers that provide sample pickup and/or the delivery of sampling supplies If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. SNA i . _.. ._ r MT ;D v SO -: 114 y ry A 1 PA NE CA ,.. CO KS %KY VA? 3dO T Az _ Nr,9 A -R P.rS AL ,A TX LA AK {.. =L .. ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1031256 10/12/18 13:36 PAGE: 21 of 22 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: Reidsville WTP Reidsville WTP Monitoring Period: From 1/1/2018 To Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level 5,vhiPVPf, and aitoo-.,a* .— a,oa.r ,.,.,tea WQ Permit Number: WQ0032723 PWS Number: NCO046345 12/31/2018 Class A: Alt. A (time/temp) ❑ T Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost E3Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density 211 Alt. (2) Process to Significantly Reduce Pathogens El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g y er o Excee- Frequency of Anal y s si Sample Type YP Analytical Tech-ni ue q inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 651 670 692 MPN/g 0 Annualy G SM92210E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform)—__weight) 17-4i... A aa_.—._ 3 MPN per 4 grams total solid (dry J__ _ _ _ __ !1 � ♦ � � .. �. �. _ _ _ _ VA.1 .11vi - l,GUMC ll,uicate auernaTlve perIormea: Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Q !'STT TTTT/'1 1 TT/lla• n 111' JL%-,t111V1\ D 1 Ei 1 Jmvlr IN 1 tpiease cnecx the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." A,, %S S C �/ e we l( .��q ,¢,fit„ Brent Collins - Director of Technical Services Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable)(type or print) 0 - S��a -.,J) — ads -r 9 ��1/22/2019 Signature of PrepareOl Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Analytical Resultsiff r `,;'s N EMA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Date: 10/04/2018 Reported: 10/05/2018 For: Reidsville WTP Comments: Geometric Mean <670 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 181004-21-01 Fecal Coliforms 1 <673 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-01 Percent Solids 1 2.97 % SM254OB-2011 10/04/2018 WC 181004-21-02 Fecal Coliforms 2 <651 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-02 Percent Solids 2 3.07 % SM2540B-2011 10/04/2018 WC 181004-21-03 Fecal Coliforms 3 <662 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-03 Percent Solids 3 3.02 % SM254OB-2011 10/04/2018 WC 181004-21-04 Fecal Coliforms 4 <692 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-04 Percent Solids 4 2.89 % SM254OB-2011 10/04/2018 WC 181004-21-05 Fecal Coliforms 5 <669 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-05 Percent Solids 5 2.99 % SM2540B-2011 10/04/2018 WC 181004-21-06 Fecal Coliforms 6 <667 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-06 Percent Solids 6 3.00 % SM25408-2011 10/04/2018 WC 181004-21-07 Fecal Coliforms 7 <676 MPN/g SM92210E-2006 10/04/2018 WC 181004-21-07 Percent Solids 7 2.96 oda SM2540B-2011 10/04/2018 WC Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 181004-21-01 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-02 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-03 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-04 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-05 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-06 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 181004-21-07 Temp on Arrival: 2.3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 q 10 b 96ed L69b/ZL8/ti0L • L898Z JN 'ajynsa}ejS • 8ZZ Xo8 Od U� 'E i N ez� c 4i c ao � �•+ � 7 �` V Y N � C ' N G p C o EQc� o u] N = CJ Z t ga E a n o.owc w a ao t a o ? CD IL ¢ r i e cr Lp M O i 0 D ! v a n a a E E E E N M W I mo v� rn to m s — •� m C _ > •� � CD .0 N �$ Grr