HomeMy WebLinkAboutWQ0032723_Residual Annual Report 2018_20190301INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WO0032723
SUBMITTAL DATED: 2/26/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address* Phone Number*
brent.collins@emaresourcesinc.com 336-751-1441
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0032723
Reviewer*
Troy Doby
Permittee * Chuck Smith
Facility Name * City of Reidsville WTP
County* Rockingham
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Reidsville WTP Annual Report WQ0032723.pdf 2.62MB
Application Form Engineering Rans, Specifications, Calculations, Etc.)
For nein and modification permit applications, the paper copy is required to be subrrutted to the
Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic
applications have been received_ The paper copy shall include the follo-kAmig:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineenng plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Service:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigb_ NC 27699-1613
By CourieriSpecial Delivery:
Division of Water Resources- Non -Discharge Branch
Ag Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Raleigh,NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or
Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/26/2019
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series:
Acres Used: 69 Acres Permitted: 69 Site #: RC001 Field #:
37.26
CgB2
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
OW7 M-1 Com-
posite
Date
11
1213
L.4J
5
6
71
MEMmOi
L 9
10
Ill 1
1121
DT/Ac./
c
App'
Event
0.54
..
Arsenic
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Chromiuinj
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Lead
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
denum
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Nickel
0.014
TotalPhos-
__phorus"MENEENEENEEN
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Selenium
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
1213
L.4J
5
6
71
81
L 9
10
Ill 1
1121
DT/Ac./
c
App'
Event
0.54
..
Arsenic
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Chromiuinj
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Lead
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
denum
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Nickel
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Selenium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Zinc 1
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Total
Phos-
1.652
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.652
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z� 1/22/2019
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville - WTP Total Dry Tons Applied (Annual): 6.50
WQ0032723 Cation Exchange Capacity (non 503 only):
Ronnie Marshall Owner: Jane Marshall Predominant Soil Series: CgB2
15 Acres Permitted: 15 Site #: RC002 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent M -
nnua eavy e a Fie oa m2s (Calculated in lbs acre):
Total
Llj
L2J
131
non
151
a
L7J
18191
moo
110111
12
Com-
DT/Ac./
" 3
0
App.
MENEM
posite
I
tv
Event
0.43
moo
Date
14
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.013
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
_____________
0.000
0.000
0.000
0.000
0.001
Copper
0.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Chromium
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Lead
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
denum
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Nickel
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Selenium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Zinc
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Total
Phos-
1.325
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.325
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Miiiiiiiiiii
nnua eavy e a Fie oa m2s (Calculated in lbs acre):
Total
Llj
L2J
131
4
151
6
L7J
18191
110111
12
DT/Ac./
" 3
0
App.
tv
Event
0.43
14
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.013
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Chromium
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Lead
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
denum
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Nickel
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Selenium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Zinc
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Total
Phos-
1.325
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.325
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1 cerWy, under penalty of iaw, tnat this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/22/2019
Date
DENR FORM MFLSF (12/2006)
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
Operator: Ronnie Marshall Owner: Catherine Neal Predominant Soil Series:
Acres Used: 27.45 Acres Permitted: 27.45 Site #: RC004 Field #:
37.30
CgB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
WWTP
4/4/18
21
WWTP
7/13/18
31
WTP
10/2/18
L4J5
J
67
7
8
9
10
11
12
% Solids
1.46
1.1
2.18
Arsenic
3
5
15.1
Cadmium
2
1.9
1
0.07
0.66
0.62
Copper
180
204
109
Arsenic
0.000
0.007
0.019
0.000
0.000
0.000
0.000
0.000
Chromium
59.9
43.7
33.5
0.026
Cadmium
0.000
0.003
0.001
0.000
0.000
0.000
0.000
Lead
61.5
59.8
12.7
0.000
0.004
Copper
0.026
0.271
0.136
0.000
0.000
0.000
Mercury
2.96
0.8
0.0563
0.000
0.000
0.432
Chromium0.009
0.058
0.042
0.000
0.000
Molyb-
denum
5
6.84
2.84
0.000
0.000
0.000
0.108
Lead
0.009
0.079
0.016
0.000
Nickel
33.5
21.2
13.1
0.000
0.000
0.000
0.000
0.104
Mercury
0.000
0.001
0.000
Selenium
5
5
5
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.001
0.009
Zinc
509
552
32.9
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Total
Phos-
horus
15800
20500
1530
Nickel
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
L 2
31
4 1
1 51
6
7
8
9
10
11
12
DT/Ac./
oy*
App.
Event
0.07
0.66
0.62
Arsenic
0.000
0.007
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.003
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.026
0.271
0.136
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.432
Chromium0.009
0.058
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Lead
0.009
0.079
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Mercury
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.001
0.009
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Nickel
0.005
0.028
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Selenium
0.001
0.007
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Zinc
0.073
0.732
0.041
0.000
0.000
0.000
10.000
0.000
0.000
0.000
0.000
0.000
0.846
Total
Phos-
2.275
27.183
1.909
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
31.368
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/22/2019
Date
DENR FORM MFLSF (12/2006)
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): 29.36
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
Operator: Harry Sharpe Owner: Daisy Purgason Predominant Soil Series: NaB
Acres Used: 19 Acres Permitted: 19 Site #: RC011 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
•-.
Com-
posite
Date
LIJ
WTP
10/2/18
3
141L5J
6
71
L8
1 91
110111
J
1121
y
DT/Ac./
0
App.
Event
0.61
0.93
Arsenic
1 0.004
0.028
0.000
1 0.000
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.032
Cadmium
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.207
0.203
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.410
hromium
0.054
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Lead
0.074
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.097
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.007
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
denum
Total
•
phorus'MENEEMENEEN.
M
Nickel
Annual Heavv Metal Field Loadinus (Calculated in lbs/acre):
Total
LIJ
L2
3
141L5J
6
71
L8
1 91
110111
J
1121
y
DT/Ac./
0
App.
Event
0.61
0.93
Arsenic
1 0.004
0.028
0.000
1 0.000
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.032
Cadmium
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.207
0.203
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.410
hromium
0.054
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Lead
0.074
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.097
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.007
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
denum
Nickel
0.028
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.052
Selenium
0.006
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.682
0.061
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.743
Total
Phos-
27.540
2.855
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
30.395
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zzz 1/22/2019
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)
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Waypointw
ANALYTICAL
10/11/2018
EMA Resources Inc
755 Yadkinville Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-4401 ° Fax 804-271-6446
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 18-276-0204
Project Description: Reidsville WTP
Waypoint Analytical Virginia, Inc, received sample(s) on 10/3/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Page 1 of 6
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
07621
Whitepine Road, Rithmond,
VA 23237Waypaint
.
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number: 18-276-0204
Client Project Description: Reidsville WTP
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
SM -2540G
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
SW -74716
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
SM-4500-NH3C-TKN
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
4500NO3F-2011
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
6010D
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
SM-4500-NH3C
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
9045D
WTN
62983
Reidsville WTP
Solids
10/02/2018 09:30
10/03/2018
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
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Waypoint-Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 18-276-0204
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 10/03/201814:49:48
Page 5 of 6
L -
Page 6 of(i
aceAnaiyticai® ANALYTICAL REPORT
i National Center /or Testing 8 Innovation October 12, 2018
i
EMA Resources
Sample Delivery Group: L1031256
Samples Received: 10/03/2018
Project Number:
Description: Reidsville WTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: ,
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. this test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
TABLE OF CONTENTS ONE LAB. NATIONWIDE. *
Ss: Sample Summary
3
Im
Cn: Case Narrative
Sr: Sample Results
4
5
FS
REIDSVILLE WTP L1031256-01
5
Qc: Quality Control Summary
7
Fn
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-90308
Wet Chemistry by Method 9045D
8
9
FQc
Wet Chemistry by Method D93/1010A
10
Fil
Mercury by Method 7470A
12
Metals (ICP) by Method 6010D
13
Volatile Organic Compounds (GC/MS) by Method 8260B
14
Chlorinated Acid Herbicides (GC) by Method 8151A
16
9SC
Pesticides (GC) by Method 80818
17
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
18
Glossary of Terms
20
,AGI:
I^' NA.c ,dr. i:'. 4 �o ."^ ii-' e_..t ... ',. psi...
•...
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1031256
10/12/1813:36
2 Of 22
SAMPLE SUMMARY ONE LAB. NATIONWIDE.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091256 10/12/18 13:36 3 of 22
RC
Collected by
Collected date/time
Received date/time
REIDSVILLE WTP L1031256-01 Waste
Brent Collins
10/02/1809:35
10/03/1809:00
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1175874
1 10/04/1813:57
10/04/1813:57
RT
Preparation by Method 1311
WG1177292
1 10/07/1811:06
10/07/1811:06
TM
Wet Chemistry by Method 9012 B
WG1178216
1 10/09/1815:51
10/10/18 07:45
KK
Wet Chemistry by Method 9034-9030B
WG1178257
1 10/10/1814:50
10/10/1814:50
MJA
Wet Chemistry by Method 9045D
WG1176301
1 10/05/18 07:30
10/05/1811:30
AMB
Wet Chemistry by Method D93/1010A
WG1175868
1 10/08/1817:16
10/08/1817:16
TH
Mercury by Method 7470A
WG1177525
1 10/08/18 09:10
10/08/1818:04
ABL
Metals (ICP) by Method 6010D
WG1177581
1 10/08/1810:30
10/08/1814:53
ST
Volatile Organic Compounds (GC/MS) by Method 82606
WG1176411
1 10/05/1817:59
10/05/1817:59
JHH
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1177879
1 10/10/18 07:30
10/11/1817:43
KLM
Pesticides (GC) by Method 80818
WG1177768
1 10/09/1814:32
10/11/1815:31
RP
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
WG1177583
1 10/11/18 06:55
10/11/18 20:26
AO
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091256 10/12/18 13:36 3 of 22
RC
CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within r
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my RSknowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
M
El
Cassandra Foster
Project Manager
BSc
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 90126.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1031256 10/12/18 1336 4 of 22
REIDSVILLE WTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 10/02/18 09:35 L1031256
Preparation by Method 1311
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
10/7/201811:06:28 AM
WG1177292
TCLP ZHE Extraction
10/4/20181:57:37 PM
WG1175874
Fluid 1
10/7/201811:06:28 AM
WG1177292
Initial pH 6.84
10/7/201811:06:28 AM
WG1177292
Final pH 4.95
10/7/201811:06:28 AM
WG1177292
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
10/10/2018 07:45
w
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide 84.4
25.0 1
10/10/201814:50
Wet Chemistry by Method 9045D
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
Corrosivity by pH 6.99 T3
1 10/05/201811:30
Sample Narrative:
L1031256-01 WG1176301: 6.99 at 20.6C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at 170
1 10/08/201817:16
Mercury by Method 7470A
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1
10/08/201818:04
Metals (ICP) by Method 6010D
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Arsenic ND
0.100 5
1
10/08/201814:53
Barium ND
0.100 100
1
10/08/201814:53
Cadmium ND
0.100 1
1
10/08/201814:53
Chromium ND
0.100 5
1
10/08/201814:53
Lead ND
0.100 5
1
10/08/201814:53
Selenium ND
0.100 1
1
10/08/201814:53
v
Silver ND
0.100 5
1
10/08/201814:53
Volatile Organic Compounds (GC/MS) by Method
8260B
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Benzene ND
0.0500 0.50
1
10/05/201817:59
Carbon tetrachloride ND
0.0500 0.50
1
10/05/201817:59
Chlorobenzene ND
0.0500 100
1
10/05/201817:59
Chloroform ND
0.250 6
1
10/05/201817:59,'
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1031256
10/12/18 13:36 5 of 22
BSc
REIDSVILLE WTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 10/02/18 09:35 L1031256
Volatile Organic Compounds (GC/MS) by Method 8260B
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
FMA Resources L1031256 10/12/1813:36 6 of 22
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
1,2-Dichloroethane
ND
0.0500
0.50
1
10/05/201817:59
1,1-Dichloroethene
ND
0.0500
0.70
1
10/05/201817:59
2-Butanone (MEK)
ND
0.500
200
1
10/05/201817:59
V,a
Tetrachloroethene
ND
0.0500
0.70
1
10/05/201817:59
SS
Trichloroethene
ND
0.0500
0.50
1
10/05/201817:59
Vinyl chloride
ND
0.0500
0.20
1
10/05/201817:59
FCn]
(S) Toluene -d8
112
80.0-120
10/05/201817:59
(S) Dibromofluoromethone
91.8
75.0-120
10/05/201817:59
(S)o,o,a-Trifluorofoluene
105
80.0-120
10/05/20181759
(S)4-Bromofluorobenzene
95.6
77.0-126
10/05/201817,59
Chlorinated Acid Herbicides
by
Method 8151A
�QC
(GC)
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
7G)
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5 -TP (Silvex)
ND
0.00200
1
1
10/11/201817:43
-
2,4-5
ND
0.00200
10
1
10/11/201817:43
(S) 2,4-Dichlorophenyl Acetic Acid
77.0
14.0-158
10/11/20181743
Pesticides by Method
8081B
Rc
(GC)
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1
10/11/201815:31
Endrin
ND
0.00500
0.02
1
10/11/201815:31
Heptachlor
ND
0.00500
0.0080
1
10/11/201815:31
Lindane
ND
0.00500
0.40
1
10111/201815:31
Methoxychlor
ND
0.00500
10
1
10/11/201815:31
Toxaphene
ND
0.0100
0.50
1
10/11/201815:31
(S) Decochlorobiphenyl
86.5
10.0-128
10/11/201815.'31
(S) Tetrochloro-m-xylene
83.1
10.0-127
10/11/201815:31
Semi Volatile Organic Compounds
(GC/MS) by Method 8270D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4 -Dichlorobenzene
ND
0.100
7.50
1
10/11/2018 20:26
2,4-Dinitrotoluene
ND
0.100
0.13
1
10/11/2018 20:26-'
Hexachlorobenzene
ND
0.100
0.13
1
10/11/2018 20:26
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
10/11/2018 20:26
Hexachloroethane
ND
0.100
3
1
10/11/2018 20:26
Nitrobenzene
ND
0.100
2
1
10/11/2018 20:26
Pyridine
ND
0.100
5
1
10/11/2018 20:26
3&4 -Methyl Phenol
ND
0.100
400
1
10/11/2018 2026
2-Methylphenol
ND
0.100
200
1
10/11/2018 20:26
Pentachlorophenol
ND
J3 J4 0.100
100
1
10/11/2018 20:26
2,4,5 -Trichlorophenol
ND
0.100
400
1
10/11/2018 20:26
2,4,6 -Trichlorophenol
ND
J30.100
e
2
1
10/11/2018 20:26
_
(S) 2-Fluorophenol
29.6
10.0-120
10/11/2018 20:26
(S) Phenol -d5
16.3
10.0-120
10/11/2018 2016
(S) Nitrobenzene -d5
59.1
10.0-127
10!11/2018 20:26
_ d_
(S)2-Fluoroblphenyl
64,0
10.0-130
10/11/201820:26
(5) 2, 4,6-Tribromophenol
31.6
10.0-155
10/11/2018 20.26
(S) p-Terphenyl-d14
72.8
10.0-128
10/11/2018 20:26
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
FMA Resources L1031256 10/12/1813:36 6 of 22
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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec,
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
Result
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to This
Custody (Sc)
perform.
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1031256 10/12/1813:36 20 of 22
FS]
a
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TQC
0
ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIQE. #
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
Alabama
40660
Nebraska
NE -OS -15-05
Alaska
17-026
Nevada
TN -03-2002-34
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico'
Colorado
TNO0003
New York
117 11742
Connecticut
PH -0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina
41
Georgia'
923
North Dakota
R-140
Idaho
TNO0003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C -TN -01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky's
90010
South Carolina
84004
Kentucky l
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana'
LA180010
Texas
T 104704245-17-14
Maine
TN0002
TexaS 5
LA80152
Maryland
324
Utah
TNO0003
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047.999-395
Washington
C847
Mississippi
TNO0003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
A2LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2LA — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TNO0003
'Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological
' Mold a Wastewater n/a Accreditation not applicable
Pace ational has sixty-four client support
----------
centers that provide sample pickup and/or the delivery of sampling supplies If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
SNA
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ACCOUNT:
PROJECT: SDG:
DATE/TIME:
EMA Resources
L1031256
10/12/18 13:36
PAGE:
21 of 22
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Reidsville WTP
Reidsville WTP
Monitoring Period: From 1/1/2018 To
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level 5,vhiPVPf, and aitoo-.,a* .— a,oa.r ,.,.,tea
WQ Permit Number: WQ0032723
PWS Number: NCO046345
12/31/2018
Class A: Alt. A (time/temp) ❑ T Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost E3Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1) Fecal Density 211 Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
er o
Excee-
Frequency
of Anal y s
si
Sample
Type
YP
Analytical
Tech-ni ue
q
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
651
670
692
MPN/g
0
Annualy
G
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)—__weight)
17-4i... A aa_.—._
3 MPN per 4 grams
total solid (dry
J__ _ _ _ __ !1 �
♦
� � .. �.
�. _
_ _ _
VA.1 .11vi - l,GUMC ll,uicate auernaTlve perIormea:
Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Q
!'STT TTTT/'1 1 TT/lla• n
111' JL%-,t111V1\ D 1 Ei 1 Jmvlr IN 1 tpiease cnecx the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
A,, %S S C �/ e we l( .��q ,¢,fit„ Brent Collins - Director of Technical Services
Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable)(type or print)
0 - S��a -.,J) — ads -r
9 ��1/22/2019
Signature of PrepareOl Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
Analytical Resultsiff
r
`,;'s
N
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 10/04/2018
Reported: 10/05/2018
For: Reidsville WTP
Comments: Geometric Mean <670 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
181004-21-01
Fecal Coliforms
1
<673
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-01
Percent Solids
1
2.97
%
SM254OB-2011
10/04/2018
WC
181004-21-02
Fecal Coliforms
2
<651
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-02
Percent Solids
2
3.07
%
SM2540B-2011
10/04/2018
WC
181004-21-03
Fecal Coliforms
3
<662
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-03
Percent Solids
3
3.02
%
SM254OB-2011
10/04/2018
WC
181004-21-04
Fecal Coliforms
4
<692
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-04
Percent Solids
4
2.89
%
SM254OB-2011
10/04/2018
WC
181004-21-05
Fecal Coliforms
5
<669
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-05
Percent Solids
5
2.99
%
SM2540B-2011
10/04/2018
WC
181004-21-06
Fecal Coliforms
6
<667
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-06
Percent Solids
6
3.00
%
SM25408-2011
10/04/2018
WC
181004-21-07
Fecal Coliforms
7
<676
MPN/g
SM92210E-2006
10/04/2018
WC
181004-21-07
Percent Solids
7
2.96
oda
SM2540B-2011
10/04/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4
Condition of Receipt
Sample Number 181004-21-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 181004-21-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4
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