WQ0030998_Residual Annual Report 2018_20190301

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0030998
SUBMITTAL DATED: 2/25/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Robert T. Branch
Email Address* Phone Number*
[e-mail] 336 312-9007
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0030998
Reviewer*
Troy Doby
Permittee*
Triple S Farms
Facility Name * Triple S Farms
County* Duplin
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Triple S DEQ 2018 AR.pdf 3.92MB
Application Form Engineering Aans, Specifications, Calculations, Etc.)

For nein and modification permit applications, the paper copy is required to be subrrutted to the
Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic
applications have been received_ The paper copy shall include the follo-kAmig:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineenng plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Service:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigb_ NC 27699-1613
By CourieriSpecial Delivery:
Division of Water Resources- Non -Discharge Branch
Ag Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Raleigh,NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or
Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/25/2019

2018 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
8646 West Market Street- Suite 111
Greensboro, North Carolina 27409
February 2019

BRANCH RESIDUALS & SOILS, LLC
8646 W. Market St. — Suite I II • Greensboro, NC 27409
PHONE [phone] • Fax [phone]
February 22, 2019
North Carolina Department of Environment and Natural Resources
Aquifer Protection Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2018 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2018 Application Summary Table, and 11) 2018 Application Condition Summaries.
A total of 1,583,165 gallons (134.07 dry tons) of Class B lime -stabilized biosolids or Class B fecal and
injected/incorporated biosolids were land applied to 66.95 acres in 2018. This material was divided as follows:
• 334,600 gallons (19.83 dry tons) from Beulaville WWTP,
• 0 gallons (0 dry tons) from Clayton Little Creek WRF,
• 0 gallons (0 dry tons) from Kenansville WWTP,
36,000 gallons (4.56 dry tons) from Rose Hill WWTP,
• 275,000 gallons (17.09 dry tons) from Warsaw WWTP,
• 37,927 gallons (3.50 dry tons) from Southwest Plantation WWTP, and
• 889,638 gallons (89.10 dry tons) from Wallace WWTP.
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Sincerely,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville
Town of Rose Hill Town of Warsaw
Southwest Plantation Town of Wallace
Town of Clayton

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2018 Application Summary Table
XI 2018 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ PermdtP: WQ0030998 County: It YearYear, 2018
Fa My Name (as shown am permit): 1gp1c S Farms tit Cleaning
Laud Application Opemdor: Triple S Farms Fc Cleantng Phone:10)
29$-3991
band appila dun of residuals se allowed by the permit ocewivil shoring the past calendar year?
El Yee L3 No - If No, skip Part A, and port B and promed do Part C. Aho, N nddwels were
mated but not land alrPRed, please attach an explanation on how the residuals were handled.
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2019. with all conditions of the land applie tion permit
(including but not limited to items 1-13 below) issued by the Division of Wates [meq. ® Yes p No
If no please, provide a wdittom description why the focilttl► was not compliant: the dates, and explain corrective
action taken.
1) Only xasiduals approved for this permit were applied to the permitted sites.
2) Soil pH wase adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Animal scuts analysis were peerformed on each site recdving residuals during the past calendar year and three (3) copies
of labotutory results am attwhaL
4) Anmad MY analysis (if required) was performed and three (3) copies of certified laboratory rrnults are attached,
5) All other monitoring was performed in accanlawe, with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) IU facility did not exceed any of the Mutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading learns in 15A NCAC 02'1' .1105(b) (applicable to 40 CFR Part 503 regulated facilift).
7) All sural requirements in as specified in the Land Application Pwait were complied with (applicable to 40 CFR Part
503 regulated > dW=).
B) All monitoring and reporting mpikepments in 15A NCAC 02T.1 I I I areae complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations acrd maintenance requiretnab in the perndt were complied with or, in the case of a devintion, prior
suftw6tation was received from the DMsion of Water Quality.
10) No coritraveatkm of Ground Watur Quality Standards occurred at a monitoring well or explanations of violations are
allacbod to include appropriate actions and remediation.
11) Vegetative cover was maintained and proper crop nionagement was performed on each site receing residuals, as
speoif ed in the permit.
12) No nmoff of residuals from the application sites oho adjacent property or nearby surf = waters has oc=mJ
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - CerifBendow
"I cast, under penalty of law, that the above information is, to the beat of my knowledge and belied, true, sae ar*64
and complete. I am aware that there are significant penaWies for su false iaia{amtl�, including the
possibility of flues and ianprhonnrt for knowing violations." J j
Mr, Eric R. Smiths, Owner
Permittee Name and Title (type or prim)
/f
See Att�hed i 1Q� 42
t
Signature of Pana* Bate Signature of Land Applid Date
(if diffeactit from Permittee) (if diner m %nun Permittee and Preparer)
* PaVarar is defined in 40 CFR Pari 503.9 (r) and 15A NCAC 02T.1 102 (26)
DENR FORM ACF (121006)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part JL- A"WfingAM §tWMMW-.
Fadllty was compliant dm 1mg calendar year 2018 with all conditions of the land application paras#
(including but nal wed to items 1-13 below) issued by the Divislon of Watear Qualky. ® Yes ❑ No
If no please, provide it written description why the fadlity Bras not menta the dates, and aWlain eo><r;lective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit ad lime was applied (if needed) to achiow a soil pH of at least 6.0 or
the limit specified in the peh7arit.
3) Annual sails analysis were performed on each site receiving residuals during the past calcar year and three (3) copies
of laboratory results are attached.
4) Animal TCU analysis (if required) was pwbrmed and three (3) copicxs of cmffW laboratory results are attached
5) All other monitoring was perfom>ed in acccmdauee with the permit and reported during the year as required and three
(3) wpi;es of ccxtfied laboratory remits arc attsched.
6) The facility did not cwzed any of the Pollutant Concentration Limits in 15A NCAC 02T.] 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T.1 105(b) (appliciblar to 40 CPR Part 503 rimed facilities).
') All gmemi requiraaments in as spedfied in the Land Application Permit wean cosraghlied with (applicable to 40 CFR Part
503 regulated facilities).
8) All, monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 rgplated facilities).
9) All operations and maintenance requiremse.nts in the permit wane complied with or, rn the case of a deviation, prier
such was received frees the Division of Water Quality.
10) No contravention ofGmund Water Quality Standards omaTed at a m ovitoft well or explanations of violations are
attac3hed to include app mpiate actions and moans.
11) Vagetadve oovrr was mdutakod and proper crop xnavagmumt was performed on each site recdmg residuals, as
specified in the permit.
1.2) No runoff of residuals fimn the application sites onto adjacent p Warty or nearby mrfi crQ waters teas occurred.
13) All buffer requirements as specified on the permit wove maintained during each application of rsaiduals.
"I ewft, Oader penalty of law, that the above iurfornutdon u, to the best of my Imewledge and beH4 frac, u nrsate,
and a mplet& I erns aware tier# Mm are sigaiflc4 at penalties for submlttiag trine infonsatlon, indndmg the
possiblity of Unites ami imprisonment for kno*ing YW& iions."
S of Date
(if diffenege,06m Permittee}
* PrODareKs defined in 40 CFR Part 503.9 .(r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TO" OF KENANSVILLE
Facility was eonpltant +luring ealeadar year 2018 withal eondltions of the Land application perroft
(including but not limited to fterns 1-13 below) leaned by the Dividon of Water Quality. L'1 Yes p No
If no please, provide a written description why the facility was not eomqdiant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (ifum ded) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving ra dduals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was perfonned and three (3) copies of certified lsboratory'results are attached.
5) All other monitoring was performed in accordance with the pmnit and reported during the year w required and throe
(3) a*= of certified laboratory results are attached.
6) The lac7rty did not exceed any of the Pollutant Coneentration limits in 15A NCAC 02T _1105(a) or the Pollutant
Loading Rates in 15A NCAC 021 .1105(b) (applicable to 40 CFR Part 503 regulated faeilities).
7) All general roquircmonts in as specified in the Land Application Permit were convIled with (applicable to 40 CFR Part
503 regulated facilities).
S) All monitoring and reporting mpiremenu in ISA NCAC 02T .1111 were cm*ieod with (applicable to 40 CFR Part
503 regulated facilities).
9) All opeaatioaas and maintenance requirements in the permit were complied with m, in the case of a deviation, pdor
authanzatwu was received from the Division of Water Quality.
10) No ocnriave n tim of Ca9ound Water Quality Standards oetsrrod at a monituring well or explanations of viobtions are
attached to include gvwp rate actions and renodmtions.
11) Vegetatives cover was maintained and p crop m mage meat was performed on each site receing residuals, as
spoct£iod in the permit.
12) No runoff of residuals fican the application sites onto adjacent property or nearby sa fi= waters has occurred.
13) All buffer requbeamts as specified on the pmnit were wed during each application of residuals.
Pit# C - (Kougm
"I ewft, carder penalty of law, haat the above Information is, to the best of my knowledge and bdK tri k accurate,
and complete. l am aware that that are suit[cant penalties for sabroidlag fain information, including the
possibi ty of fines and imprisonment for knowing Violations."
Signature a bate
(if dit%Tent $roan P ee)
0 Pwpara is defined in 40 CFR Part 503.9 (r) and 15A NCAC Mr .1102 (26)

ANNUAL LAND APMCATION CERIIKCATION FORM
TOWN OF ROSE HII.J
Part B - Anuusl Comryianee $tntemme.,
Fatdilty was cvmpilant durisrg ademdar year 2018 with, at eond[tlons of the land application permit
(including but not lfmtted to Items 1-13 below) i ew d by the DivWm of Water Qu:lt#,y. ® Yea © No
H no please, provide a written deser4ftion wby the facift was not compliant, the dates, and explain corrective
salon tawn.
1) Only residuals approved far this permit were applied to the permitted sites.
2) Soil pH was adjusted as speeiiied in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit spomfied in the permit.
3) AmW soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of labontory, results are ami hed.
4) Annual TCLP analysis (if repaired) was performed and tlnu (3) copies of certified laboratory nadta are attached.
5) All oth a monitoring was performed in accordance with the permit and reported during the year as required and three
(3) cwpirx of cernfied laboratory results are att d
6) The facility did not exosed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loa ft Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facihOc s).
7) All general require nicats in as opecif ed in the Land Applieatcon Permit w= complied with (applicable to 40 CFR Part
503 regulated facilities).
S) All munitosing and sporting mpdremcats in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
5033 rquiated facilities).
9) All opamdons and monfenance rcquinarrueuts in the permit were complied with or, in the case of a deviation, pdor
audmnzstton was received from the Div== of Water Quality.
10) No coatravmiiort of Ground Water Quality Standards ocaured at a monitoring wall or explanations of violations era
atteded to include appropriate actio and rremodistions.
11) Vcptstive cover was mainUtmod and proper crop management was perforated on each site reoeing residuals, as
specified in the permit.
12) No nmoff of residuals. from the application siks onto adjaeeat ptnpc ty or nearby surface waters has ownyed.
13) All buffer n quiranetts as gxx hied an the pa mit were maintained during each application of residuals.
"i.e r, muter penalty of Harv, that the above information % to the beet of my knowlefto and bdK true, accurate,
and complete. I am aware that tt<ere are scant penalties for submitting false information, including the
possibi ft of [bug and fmprbotmat for knowing vkde lona."
Idz LAMM,6/0
sigrmture Of Pr+epatrr* Date
(if M%rat from Permittee)
* Preparar is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T ,1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTHWEST PLANTATION
Fudlity was compliant during calendar year 2018 with all conditions of the land applicath a permit
(111*009 but ant liarlted to hems 1-13 below) issued by the Division of Water Qo ty. 0 Yes D No
If ma Pha e, provide a written description why the facility was not empllant, the dates, and c gda6 eo mctive
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the pmmit and limo was applied (if needed) to achieve a soil pH of at least 6.0 or
tie limit specified in the permit.
3) Amnue1 salla analysis wase performed on each site receiving residuals during the past ealamdar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis Of required) was performed and theca (3) copies of certified laboratory results arc attached.
5) All other monitoring was pofon ned in accordance with the permit and reported during the year as regained and three
(3) copies of certified laboratory ramlts are attached
6) Tire facility did not exceed any of the Pollutw Concentrathm Limits in 15A NCAC 02T .1105(a) or rice Pollutant
Loading Rates in 15A NCAC DZT .1105(b) (applicable to 40 CPR Part 503 regulated f dlitiea).
7) All general requirements in as specified in the Land Application Permit were compiled with (applicable to 40 CFR Part
503 regulated facilities).
8) All rnoa twing and reporting requirernsnts in 15A NCAC MT .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and nudntenance requir=muots in the permit wo v complied with or, in the case of a deviation, prior
authorization was received fivm the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or eaphoations of Violations fire
attached to include appropriate actions and remain ions.
11) Vogatab"oovcr was maintained and proper crap management was performed on each site receing rcaidwds, as
specified in the peen it.
12) No r mffof residuatla Einar the application sites aorto adjacent property or ncarby surfiKx waters has ocmured.
13) All buffer requirements as specified an the permit were maintained during each application of residuals.
Part C - Cercatfon:
"I eeMy, ander penalty of lsw, that the above inlbrm don ls, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are sigtdReant penalties for submlttiag telae information, induding the
possibility of flr"d imprisonment for knowing violations."
3 r i'�- JF orhate
(if di fim permittee)
is defined is 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)

ANNUAL LAND APPIACATKIN CIRMCATION NORM
TOTM Of WALLACE
lihaW rlw wAsnddr por , D S *0 aR amMm of to 1nd m"Swum pau t
Oodeft bs# atom" to lftm 1-13 blow) lewd hyserm I IF of Waters QaalTtlr. ® Was p No
Himpanda a a dmm%Mm wit tlW J%dVWwas nd ampAmit tine dsfW wA eWmk eme*dM
aalatah m.
1) Oidy mddmb pp wmd Jbr*b pwz mit w= goiad tp so pw it d tib.
$adl pH wsa a{ustad a epodilad in tfw paerdk end lime wsr app0od to sabfaV+e a aa� pH of at hast bA a
tlml�df sq dbe ptsmit,
3) Ammal aollr Wdysil wane pedbmod an mach site rao ift rrddeda dodng do port aalanda year and Gm (1) a*=
aflaborataty=ults aro xbchoL
d) Armad 7CU emalyds (if "ROOM ww pa hnnod and thew (3) of osrtl0ed labmdwy =who ergs attaohed,
5) All odd mo&ft vu pmemod in aaaoWmm with the pacmit ad rape W dmigg the year as roWdwW and oo
(3) oopl a of amtt& d laboratory rwaU are dhohed.
d) The heft did not a+rosed mW of do Poil bd CafteMamtioec Lints in 15A NCAC 02T.1 105(a) or dw Pdbtw
toWhrRatm to ISA MAC W. I 165(b) (q pHmbio to 90 CFRPatt 503 regaled AWIW**.
7) All IMOW roque in m RMOH d m to Land Ap$imdm Pm* wart campW WI& (Rrpliable to 40 OR Pmt
3Q3 rogulatod #hCiiidos).
8) All Mab mbg mal vVmdmg rogaim naWs In 13ANCAC 02T.1 I I I vaoro osplmdwith (appilW& to 40 CPR Ped
309 awl" ).
9) All apmdow odmnbftmmnqakmmnU in the permit wmo oamaoW wA or. in dw =w da davk*% p*w
wa �necaived Room Oma 3yivision of''OI�aEar Qgafi�r,
10) No coaftvawim of ommod Walsh Quo* Mmmbxds oo=md at a nnom g wml or uq*mdkm of vioio*m ame
to iasbtcls spQ mp ift aeticm sed »emMWlam
t 1) VegetaHm wm washed aad poopae are mmqpmu was perammd as aab she rambg redtmals, as
ape"W in #ha pGUL
M M adraddnds ftm dwmpplivaadm afters ado a4eomt pmpwW army enrl m waters has oamnmed.
1� Ab bsdyer�ts m speciti�ad seal tha paemb rw+eha Oad daeing each epp�adanaf raeidreels.
"I aero, aarcisepatafhjr oy taws flrat dta absms � � to deer bat o8 � lasowibdia ar<d balisi, treea, aacieieaLa�,
aad eaaeplels. I � stiavagre t#uet tkss+e ups cwt 1P�a � � Rrha L�rasatlas,, flee
paa�ilgr aft3aa a,act � � �"
ed pnpmaa* nate
(#ff i=Popmmw)
+P+apeasris &&a In 40 CFRPad 3039 (r) SW 15A NCAC 02T.1102 M

ANNUAL LAND APPLICATION CERTMCATION FORM
TOWN OF WARSAW
s - Annum Coaruotance apart:
Faulty was compliant durful a dendar year 2118 with all conditions of the land application permit
(Including but Bot ]united to Racers 1-13 below) hued by the Dividen of Water Quality. ® Yes 0 No
U no please, provide a written description why the &dft was not compliant, the dates, and explain corrective
sett bicep.
1) Chrly residuals approved for this permit wane applied to the permitted sites.
2) Soil pia was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in time permxt.
3) Amul soils analysis were paformed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory rests are attached.
4) Awmal TCLP analysis (if required) was performed and three (3) c*es of certified laboratory results are attached.
5) All curer monitoring was parfofmd in accordance with the peamit and reported dancing the year as required and three
. (3) copies of certified laboratory ronft are attached.
6) The facility did not exceed any of the Pollutant Canceration Limits in 15A NCAC 0717.1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T.1 10*) (aMiicable to 40 CFR Part 503 regulated beilities).
7) All ga ml rcquiremews in as spoked in the Land Application Permit were ca*licd with (applicable to 40 CFR Part
503 regulated facilities).
8) All monAoring and reporting requircmnts in 15A NCAC 02T.1 I i 1 were complied with (applicable to 40 CFR Part
503 regulated hailitics).
9) All operatics,$ and maintenance requirements in the permit were complied with or, in the can of a deviation, prier
atutharizWon was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
atts&cd to include appropriate actions and remediation.
11) Vegettstive cover was maintained and proper crop management was performed on each site receeirrrg residuals, as
specined in flue pexmiL
12) No runoff of residuals from the application sites onto adjacent pxapaty or nearby surface waters has oom red.
13) All buffos rcgmrcnmts as specified on the peanut were maintained drug each application of residuals.
PKtC cKdARK".
"I fir, ander penally of low, that the above information is, to the best of my knowledge and bdW, true, aeeurate,
and complete. I nen aware that there are signillcant penalties for mbndtdng false information, iaeluding the
ir of tines and ibPrisonn>ent for lamming violations."
11/1 — 7, - C-0
8 -O irate
(ifdi&rent fin m Permittee)
* Preparer is defined in 40 CFR Part 5039 (r) and 15A NCAC OZT .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

ANNUAL RESEIUAL SAMPLING SUNV"RY FORM
Please note that your permit may contain additional parameters to he analyzal. The parameten can be reported is FORM RSSF - B
WQ Permit Nmnbez. WQ0030999 Laboratory: 1) FmviromneaW Chmdsts
Facility Name: Triple S Fams & Cleaning 2)
Residual Source WQ # or NCO026019 3)
NPDES #: d)
WWTP Name: Town ofBeulmille WWI? 5)
gsmifinal Alnelvwat no-i'm
=[er I M 4 4 111 1FAlt:
11
{
-� li Ill Leif iF�41_-1
"I eerbil?jr, under penalty of law, that this doeuumeat was prepared ander my direction or supervMm In accordance wlth s system dm*DAd
to am m that gaaMed peel preiieft pthered and avoluMed the htformstion submittedf. i am aware that thM are slgniflcant
peaalt[ea for subqdt&g fdse iifornlatlon, kdadiag the pomdbMy of fines and hnptisoument for knowing vlohdk na."
Signature of * — Date .r
"InVow is defined in 40 CFR Part 503.9(r) and 15A NCAC ZT .1102 (26)
DENR FORM RSSF (i MM

ANNUAL RESIDUAL SAMPLING SUNEM"Y FORM
Please aoft that ymr permit may conemb adAtlond parameters to be analym& lNe parameters can be rep nft d is FORM RM - B
WQ Permit Number: WQM0998 _ ` Laboratory:
Faeft Name: Triple S Fams & Clssttixjg
Residual Source WQ p or
NMES #:
NCO056863
WWTP Name: Town ofRose Hill WWTI'1
�....1--s..1%-A-
1)
%-A ,.
1) Environmental Cbamists
2)
3)
4)
5)
r•
13 011
IIS. �1lai.y+l 1!
�
' palcanta�wae aac oaweoiea an lying F-aliP4 wnl.raar! s
"Iesrft, ander penalty of law, that this dot was prepared under my direction or supervision in accordance with a system designed
to assure that quaMed persomel properly gathered and evahtated the informtion submitted. I am aware that there are sfigpiilcant
penalties for submdtdag f dw informatlon, including tate possr'bi[ity of #ince and imprisonment for knowing violadmo
Signaum of Pnq mer • Date
*Par is defined in 40 CFR Pett 303.9(r) and 15A NCAC 2T.1 102 (26)
DENR FORM RSSF (12MM)

ANNUAL RESIDUAL SAMPLING SUNWARY FORM
Please vote that your permit may eoDtain addkba d paramciars to be andyaed. The parnumbn can be reported in FORM RSSF - B
WQ Permit Number. WQ0030998
Facility Name: Th
' le S Farms & Oes
Realdnal Source WQ # or
NPDRS ft
WQ0029601
WWTPName: SouthwestPlantedon. WWTA
Residual Anaivsls Data
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
'I certify, awder pen of law, document was prepared under my direction or supervision in accordance with a system deigned
to assure that N el perly gathered and evaluated the information submitted. I am swam that there a
W
Si ' Data
'P is defi=ed in 4Q C3; R Pmt So3Xr) and ISA NCAC 2T .1102 (M
DENR FORM RSSF (92/2000)
1{{' r �a
'I certify, awder pen of law, document was prepared under my direction or supervision in accordance with a system deigned
to assure that N el perly gathered and evaluated the information submitted. I am swam that there a
W
Si ' Data
'P is defi=ed in 4Q C3; R Pmt So3Xr) and ISA NCAC 2T .1102 (M
DENR FORM RSSF (92/2000)

ANWAL F KK L p 6
ww . hm
$Fmm& 2'!
RsdftlsmnwQdar NCDD2D7Q2 3)
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'W w mmm Tomn of Wnnnm ww Y py
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wwwpmft orbw, *at MA Am mom wn pnpan d 1 aft mw ArNgkm or s%mvmm in Ka se vial a N ft ft" ft
aed l�/ :�Otl 6d. I e tlese m P
Air �,itds mapos of&= sed �t�er vlalstlons:'
ORRMO$rloftediSIMCMI*t-%&K*WAl.# MM2TJ102M
MR FOM FMF (IZZW

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please mote tbst yom permn msy wilt&% Idgiftloml parameters to lie aas4wL The posme gm can be nVerted to FORM MSF - B
WQ Permit Number: WQ9030998 Laboratory: 1) Envirom ental Chemists
Facility Name: ^ Triple S Farms & Cleaning 2)
Residual Source WQ # or 3)
NPDES #: Nt"U021903 4)
WWTP Name: Town OfWarsaw WWTP 5)
Reddual Analvais Data
"I cerfY, +order penalty of law, that this document wait prepared under my direcOm or supervision In. aceordance wftk a Srtem designed
to assure that qu*Hf rl personnel property gathered and evaluated the information submitted. 1 am *ware dist Then am sig KkAnt
pen#des for sgb;pkfing false informatpan, ioneladiug the pumdbEty of fines and Imprbonmea'for knowing rtulatim&"
Daae
4'rgww is dafhM M40 CFR Part 503.9(r) and 1 SA NGAiC 2T .1102 (26)
bENR FOWA RSSF (721 006)
SEMI
" �I •
�����-��,
!moi �_��
I 4 I1 IIF
��__-��
i ■ ��i
■
�L fl�i
"I cerfY, +order penalty of law, that this document wait prepared under my direcOm or supervision In. aceordance wftk a Srtem designed
to assure that qu*Hf rl personnel property gathered and evaluated the information submitted. 1 am *ware dist Then am sig KkAnt
pen#des for sgb;pkfing false informatpan, ioneladiug the pumdbEty of fines and Imprbonmea'for knowing rtulatim&"
Daae
4'rgww is dafhM M40 CFR Part 503.9(r) and 1 SA NGAiC 2T .1102 (26)
bENR FOWA RSSF (721 006)

ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Much this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Faddy Name: Triple S Farms Total Dry Taus Appkd (Annul): 73.89
Permit #: WQ0030998 Cation Lkeha np Capacity (non 393 enly): 111s
Operaton. Brie Smith Owner: Eric Smith Fridmubmat Solt Sepias NoA
Acres Used: 34.2 Aeras Fl=uted: 34.2 Site #: 1 Fldd #: 1
ReddtW Analysis Data (Heavy Metals and Total Phosphorus an mg/ q6 % Solids use Raw Pereent #):
B2018118P2018148 WR201914 Wa.2D181.B20181-18 SWP2018:WR20181-W120183. W=194 -
or Com-
P06ite
&g4/18
12126/18
8114/18
3/21118
8/14118
1?1?a6J18
8/100
915118
10/18118
%Solids
1.38
2.21
1A9
1.67
1.38
2.21
1.49
2,78
2.53
0.01
Arsenic
39.90
25.70
32.50
30.40
39.90
25.70
32.50
18.30
20.20
0.03
0.01
CWmium
39.90
25.70
32.50
61.10
39.90
2510
32.30
18.30
20.211
0.02
0.10
0.01
Ck=iw
39.90
25.70
32.50
61.10
3990
25.70
32.50
54.00
35.20
0.01
0.27
1.32
Copper
93.50
210.00
533,00
904.00
93.50
210.00
533.00
737.00
.992.00
0.01
0.00
0.02
Lead
39,90
25.70
32.50
67.10
39.90
25.70
32.50
98.60
65.20
0.00
0.00
0.00
Memory
1.16
0.63
2.35
1.50
1.16
0.63
2.35
1.04
0.79
0.02
0.01
0.01
Molyb-
39.90
25.'70
32.50
30.40
39.90
25.70
32.50
18.30
20.20
0.00
0.02
0.03
Mdse]
39.90
25.70
3,2.50
61.10
39.90
2570
32.50
39.60
25AO
0.01
0.00
0.02
Selenium
39.90
25.70
32.30
61.10
39.94
25.70
32.50
18.30
20.20
Zinc
0.07
0.09
Zkw
258.00
1260.00
1570.00
1580.00
258.00
1260.00
1570.00
1318.00
1760.00
5.58
TOW
Phos-
33.61
Totef
Phos-
117,500
M200
14,200
30,5W
117,,500
18,200
14,200
22, 300
23,900
148.29
Annual Seavy Metal Field Losdinaa [lelculated is 1bd11acre):
"I caft, under penalty of law, that this document was prepared under sly direction or supervision in
aceordanee with a system designed to more that qualified pe rsound properly gathered and evadnaated the
information snub I am aware that there are adggi$caut penalties for submitting fabe laformalion,
�cludin� of fines and iinprlsonment for knowing violations"
Signat(w oftaud Appficr rk"
Au dwr Beryl D. Mwft DENR FORM MFLSF (7=2)
0.14
0.03
0.25
0.22
0.15
0.03
0.25
0.90
0.18
A111Cn1C
0.01
000
0.02
0.01
0.01
0.00
0.02
0.03
0.01
0.11
001
0.00
0.02
0.03
0.01
0.00
0.02
0.03
0.01
0.13
0.01
0,00
0.02
0.03
0.01
0.00
0.02
0.10
0.01
0.20
0.03
0.01
0.27
0.39
0.03
0.01
0.27
1.32
0.36
2.70
Lmd
0.01
0.00
0.02
0.03
0.01
0.00
0.02
0..18
0.02
0.29
motwy
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
0.01
0.00
0.02
0.01
0.01
0.00
0.02
0.03
0.01
0.11
Niche!
0.01
0.00
0.02
0.03
OVI
0.00
0.02
0.07
0.01
0.17
Seknium
0.01
0.00
0.02
0.03
0.01
0.00
0.02
0.03
0.01
0.13
Zinc
0.07
0.09
0.78
0.69
0.08
0.09
0.79
2.35
0.64
5.58
TOW
Phos-
33.61
1.24
7.07
13.30
35.59
1.25
7.12
40.36
8.76
148.29
"I caft, under penalty of law, that this document was prepared under sly direction or supervision in
aceordanee with a system designed to more that qualified pe rsound properly gathered and evadnaated the
information snub I am aware that there are adggi$caut penalties for submitting fabe laformalion,
�cludin� of fines and iinprlsonment for knowing violations"
Signat(w oftaud Appficr rk"
Au dwr Beryl D. Mwft DENR FORM MFLSF (7=2)

ANNUAL METALS FMD LOADING SUbOdARY FORM
Attach this form to the eolresposdiag Field Loading; Summory Form to be imbu tted in Annual Report
Facility Nene: Triple S Farups ToW Dry Tou Appiled (Armed): 31.98
Permit d: W00030M Callon Exclimp Capacity (um 03 only): nfa
Operator: Baia s"Ift Dimer: Eric Suritb Prcdomhmd &W 8erles FbA
Acm Used: SAS Amer Penal t ah 8.48 Ske 0: 1 Field p: - Z
R WtW Analis Darts (Heavy Metals and Total Phosphorus use mg&& % Solids use Raw Perwit #):
Nos,
LWI
��-----�--
Em
,
Anapasl l3<vy Metati I+'teld Loadinos iCdealated bn lllslsrere):
"I twft, alder penalty of law, that ft dominant was prepared ander my direction or supmThlon in
accordance rrM a systesu designed to assure that qualified personnel properly gathered and +evolustad the
information submitted. I auos aware that there we eigofficast pesddes for submf tdng idle iddormadou,
A W fines and imprisonment for knowing viokstlont"
Signature of Land ApplW Date
AuNwr Daryl D. Merritt DENR FORM MFLSF (7!2002)
Em
,
"I twft, alder penalty of law, that ft dominant was prepared ander my direction or supmThlon in
accordance rrM a systesu designed to assure that qualified personnel properly gathered and +evolustad the
information submitted. I auos aware that there we eigofficast pesddes for submf tdng idle iddormadou,
A W fines and imprisonment for knowing viokstlont"
Signature of Land ApplW Date
AuNwr Daryl D. Merritt DENR FORM MFLSF (7!2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the correspending Fwd Leading Summary Form to be submitted in Ananal Report
Fadllty' Nal ne; Tiiple S Farm Trial Dry Teas AppSed (Amu* 4.56
Pathan #: WQD03MB Cion Exchange Capadty (non 50 o*): n!a
operater; FAc smith Owner: Birk Smith Predemiaw && sane. FM
Aaa Used: 4.14 Acne Pennritted: 4.14 She #: 1 Field4
R=Wual Analy & Data (Heavy Metals and Total Phosphorus an mglkg, % SoNds'use Raw Perment #).
RM2011 1-18
Em.
4: f 11
1 S 1
©
OEM
,.:
FR
1NEENNEEN.E.Nom
I,I��rl
Annual Heavy MeW Field Loadlnes (Ceigulated in % daarel:
"I certify, adder pen*W of law, that this document was prepared *oder my dirveden. or supervision in
accordance with a ay t m designed to assure that qualiflled personnel preper(y gatMo d and evsluated the
latanua11on. mhmitkd. i am aware that there are sigaScant penalties for submitting false Information,
1n, Whit thq pa#ft of" and huprismateat far MowhW vlolaam"
Signature of Land Applier " Bite
Author Daryl D. MarMl DENR FORM MFLSF (7=02)
©
OEM
,.:
FR
1NEENNEEN.E.Nom
"I certify, adder pen*W of law, that this document was prepared *oder my dirveden. or supervision in
accordance with a ay t m designed to assure that qualiflled personnel preper(y gatMo d and evsluated the
latanua11on. mhmitkd. i am aware that there are sigaScant penalties for submitting false Information,
1n, Whit thq pa#ft of" and huprismateat far MowhW vlolaam"
Signature of Land Applier " Bite
Author Daryl D. MarMl DENR FORM MFLSF (7=02)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach tbh form to the corresponding FWd Loading Summary Form to be anbaaittad in Anand Report
Fadft Name: -- - Triple S 1;ww ... _.. ToW Dry rem Applied (Annual): 1092
Permit #: WQDM0998 , Caton Exchange Capacity {mom w onlyj: n1a
Operator: B& Smith Owasr. Etc Smith Pnxlawhmt Siad SeAln FoA
Acres Asad: 11.2 Acro Pm1ltted: 11.2 Site #: 1 Field #: S
iResidnal Anal do Delta (near Metals and Total Pbowhorus use mgll<g % Solids use Raw Percent #):
SWP20121-181 otslids
Annual Sesvy Metal Feld Loadinos (Cokslated in Ibdacre):
s
! t
1
"17, 1 I
i F
MUM
-1'..111®--�-�-----
1!I ,
Annual Sesvy Metal Feld Loadinos (Cokslated in Ibdacre):
s
! t
1
i F
MUM
"I ew tp, under poaalty of low, that thh documest was prepared ander my dhvetlon i supervl*ioar hie
laecorol nce with a system designed to assure that qus1HW personnel properly gathered and evaluated the
inforomoll a submitted. I am swan that thine in signMalnt penalties for submitting false hOrmodoik
inlduding the po#wijq offl#esand imprlsoo mlent ifor bwwieg viol ft="
lguattu+e of Land AppHer Data
Aut w Daryl O. Merritt OENR FORM MFLSF (712002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the correaponAng Reid Loading Samnaary Form to be submitted in Anand Repoat
Faddy Name: Triple 8 Farms Todd Dry To= Applied (Axossi ; 12.72
WQOM0998 Cation Enhonge Capocfty (non 503 only): nla
OP111"': Eric Smith Owner: Faic Smith Predowhisat &d Scrim GoA
Acres Used: 8.93 Acm Pte: 8.93 filte #: 1 Field #: 9
Ra:ddual Analyds Duca (Heavy Metals and Total Phosphorus use mg&& % Solids use Raw Paust 0):
W12019 1-18
I lil
1` a II
,, _.II Ili!.
I {
OEM
e I;
'I,>
1.1 1, OENNEEMENEEN
k 41
Arcual Hewm Metal Field Loadfnes (.Calculated in ibolacre):
"I earthy, under penally of law, that Ibis document was prepared under my d cation or supervfdon 11
accordance with a system dem%ned to assnra that qualified persennd propat gathered and evaluated the
information subedited. f am aware that tbere are isWficant penatti s for subm#dag false h4brmatifolu,
0 in of & a and imprhonm+ent for loco+ bg vklafiom" i r
1" k- I..—. -N.� l
Sisnatura of LAM Applier Dine
Author Daryl D. Merritt OENR FORM MFLSF (7!2002)
e I;
"I earthy, under penally of law, that Ibis document was prepared under my d cation or supervfdon 11
accordance with a system dem%ned to assnra that qualified persennd propat gathered and evaluated the
information subedited. f am aware that tbere are isWficant penatti s for subm#dag false h4brmatifolu,
0 in of & a and imprhonm+ent for loco+ bg vklafiom" i r
1" k- I..—. -N.� l
Sisnatura of LAM Applier Dine
Author Daryl D. Merritt OENR FORM MFLSF (7!2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac
As —
Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients lbs/ac
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLRASE MAKE A COPY OF THIS BLANK FORM TO BE CONMATED AND SUBM WED FOR EACH APPLICATION .FIRED.
PLACE A "NIA" IIs' A BLANK OR BOX WHEN NOT APPLICABLE.
Facfky Nance: Triple S Fwms WQ Permit #:
Owner. Ed* 11mi* -anaal Dry Tons Appno&
Operator. 1srlc
Crop I Name: 9=10mil,
WQGOM998
73.84
Milt
site #:
Antes UtMaed: 34.20
Acres Permitted: 34.20
Predomieat Soft Series NoA Cation age Capmdty (rt m my. NA
Crop 1 Max PAN: 136.00 Crop 2 Name: 8amaemama Crop 2 Mat. PAN---.. 50.00
�
iXWAA
t.-r
% Sands
qs
Dacaaml
volume
AppHed per
Acre
Residual Souam
(NPDES A W�QC
Fat, Animal Waste,(Dr
°e')
C 1.
Wakf
Moist)
predp
Pad 24
idea
�
�
+2
�
TTN
x
Nitnft
and
Nitrite
PAN Applied M1rst Select
�g/g } Crop l of Crap
Crap1 Cmp2.
Ian -18 83.00 ,485
138
014
OvAmib WWW
s
250
0.30
51.800
2,906
141
4.65
x
Feb -18 121M 368
2.21
0.03
scudwWrbsu m
s
0.50
0.30
76,500
723
I00
IA
x
Mar -18 137,000 4,m
149
tk25
WUMW W WrP
s
0.30
0.30
40,300
2.300
302
b.40
x
MsL%18 107,100 3,132
1.67
022
Wdb=WWTP
IN
1.00
0.30
64,606
2,100
1
9.09
x
18 90AN 2,632
1.38
0.13
1ladavlAe Wim
s
0.30
0.30
51.800
2,900
141
493
x
18 12.127 372
221
a,03
5006me
s
OM
030
ZIM
723
100
1.59
x
.Fun -IS 138,000 4,W5
I.49
US
Wunv►
w WrP
8
0.50
030
40.300
2,.300
302
6.44
X
A0108 264,600 7,737
2.78
0.90
WadwWwrP
IN
1.00
Q3D
47AN
337
151
26.20
x
Doc -I8 59,400 1,737
2.53
0.18
wwbmv"
IN
1.00
036
49,400
VW
159
6.34
x
ALS: 26,W I
As I
Cd Cr
Cn.
Pb
11st
Mo
Ni
So
7sa
P
PAN 1 PAN 2
Lime AmW
lAnnual lbs/age
0.11
0.13 0.20
2.70
0.29
201
a l 1
0.17
0.13
5.58
.901
28,05 1 39.16
Daae
l
Cmmt Cumulative lbsla=
Prim Yeats Cu:anlstive RWacre
Pa04V C_ P. L.li. *
FenMt
0.64
0.53
36
0.61 NA
OA9 KA
34 NA
39.17
37.07
1,338
1%
SAS
267
0.07
0.06
15
NA
NA
NA
137
1.21
374
0.79
0.66
89
80.18
7460
2,498
136 1 54001
1
--1 eaury, under penalty onow, that this document was prepared under my direction or mpervhbn flu *Gcordanee wftb a system
dedped to assure drat quaRM parsom d property gathered end evaded the infarmation ubmitbd. I am aware ftt diem are
do"Iftsat peealtfra sea g false bdbrmatbm, including the pesdbil W of Baas said baprieumnant for knowing vioiatiees."
*AppH*Miau MD&Od: S - sw&Kr, IN - bject[m INC - heorpm tLm
,- **Volit�aHan Rabe: Sariace - 0.3, igjeeEbsdfgeorporartielt -1.Q
Sigostame of bated Applier Date ***MimaSaatbn Bata: Compost - 0.1, Anaoer+obkally Digested - 01,
Aerobically Digested - 0.3, Rai► Sledge - Q.4
****C.PJ,JL: Cum bdiive Pnpatant Loading Raft
DEMR FORM FW (1 218006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BANK FORM TO BE COAD AND SUB1VIITl'ED FOR EACH APPLICATION MID.
PLACE A"MA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Fae ty Name: Triple 5 Farms WQ Permlt #: WQO030998 Field #:
Omer: Mo W& .nodal Dry Tons AFplted; 31.98 Sloe #:
Operator:
_ Edo Smith Predomintit &W Steri" FoA
Crop 1 Name: Crop 1 Max PAN: 276.00 Crop 2 Nam:
1 Aeras Utllfeoed:
MS
2 Acres Pend ted:
SAS
Cation Ffaehsp Capedo (non SM:
NA
Mtn Crop 2 Man. PAN
MA
I
��
���}�
• SS 1.. il'
S Ir•
I
r
IS I
��k 4- f �1
OEM
"I ftftfy, malar peaolty of lawn, tint tltts documeslt was prepared muter my Ration or supervision in acordmnea wM a system
deftned to assure titin gaa*W persound propel gathered and erabwmd ft bttormadou submitted. I am swam &at thea& an
siccant penalfbs fors A&o h9ormation, iadading So pommy of tines and imprisnmnent for knowlag violudevul "
c�-- L eApplleatlon Ma#hod: S - Sorfaee, IN - �ecdon, INC - Incorpoeaflom
paz, le JM.-Mu**Vontgbwtba Rhe: Saurbee - 0.5, bjection/"rorpoe;adon -1.0
Sigutue of Land Applier Data ***Mlaeraff atlon Rates: Compost - 0.1, AnssrobiesW - OX
Aerobically Dkested - 03, Raw SWdge - OA
a***C.P.L R.: Camohttve Poliatimt Loading R@W
DENR FORM FSF (==)

ANNUAL LAND APPLICATION Ffl" GARY DORM
PLEASE MAKS A COPY OF THIS BLANK FORM TO BE COMPLETED AND R)BINIITTED FOR EACH APPLICATION FIELD.
PLACE AMA" INA BLANK OR BOX WEMN NOT APPLICABLE.
Facility Name: rE`A$,c S Pff= WQ Permit #: WQ0030M Field M. I Atm Utilized: 4. t4
Owner: Elic smii imu l Dry Toxo Aplplie d: 4-56 Site M 4 Atres Pwndtled: 4-14
Operator: k sudffi Predooduat Sad Sarin FGA CRUM Exeikange Capacity (Ron 50): NTA
Crop 1 N�: awf {Double crcww - PAm
Crop 1 Maar PAN: 133.00 Crop 2 Name: WA Crap 2 Naz. PAN #N/A
MF 7
6 .
It -
R
Mr -7,77f I f_
I! -'
f f f i
®
1 1
! 9 1
! I
f 7-
NEER
a
ie1 eert[W, abler paaaW of hww, that this d6emnmt was prepared pier my directlan or supervision in accordance with a system
deslg ed to anure *at gaalliled persommi properly ga&ex°ed wo evaluated the information submitted. I an aware that there are
signifleaut pansltks for s false ffornudion, inebedhrg the posslbiligr of tlam and huprbmument for Imawing violatioas."
h *Appiicathm Medkod: S - Surface, IN - h#ecdoo, INC - DMrpandon
**Vomition Rate: Barbee - 0.8, injectionfUmgwradea -1.0
amsc of Lad Appiier Dcie #**Mineralization Rates: Compost - 0,1, Anawrobieall+ Digested -' GJ6
ftmAerobically Domed - 03, Raw Sludge - 0.4
* I **C.PJ.JL: CumWsd" Pollutant Loading Rate
DENIR FORM FSF (121Z0M

ANNUAL LAND APPLICATION FEUD SUIVIIVIARY FORM
PLEASK MAKE A COPY OF TMS K ANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION F=D.
PLACE A "NIA" IN A BLANK OR 13OX WMW NOT APPLICABLE.
Foeilt€y Nm m Triple S Farms WQ Permit #: WQM30998 Field #: 1 Acres UMmed: 11.20
Chmer: Eric Smit, Dry Tons Applied: 10.99 Ste#: 5 Acres Por d: 11.20
Oper br: Eric smbb Predominat Sohl Series FOA CaBob Exchange Capacity (non SQV: NA
Crop 1 Name: sFF,a1cmim Crop 1 Max PAN: 115,00 Crap 2 Name: NWA Crop 2 bfkxa PAN #1y/A
"I eer ffy, under penally of 4w, tbat iRb doemotent was prepared under my dh etion or auptarvidm in accordenee with a systm
wed to assure that gaaWW perromnd p mpe* gsdwn d and ev of mftd the information submitted. I am aware that uteri an
siert pen for snbai11 d g Wa informadom, ioaelufag the paidbft of fires and bmprbouumt for hsowiag vbladom.s
w *AppHcatim Modmd: S - Surface, IN - Isjeet omr , INC - ftorporstlon
_-, **V'oRttlmtb:a Rabe: Smftw - 0.5, N. 11 j orparatheas - Le
Signature of Land Appher Date ***fin Rates: Compost - 0.1, AuaerobdeaBy D4pseed - 0,2,
Aerobbalhy+ ft abed - 03, Raw Sludge - OA
****CJ'J..R.: Cumulm im PoEMsnt Loading Rate
DOR FORM FSF (12PAM
SIJ•
,'
_
—MR,-
Or
i i � t� a s
�1[arV�� ��■^ ail 1 ti'.r/r���
"I eer ffy, under penally of 4w, tbat iRb doemotent was prepared under my dh etion or auptarvidm in accordenee with a systm
wed to assure that gaaWW perromnd p mpe* gsdwn d and ev of mftd the information submitted. I am aware that uteri an
siert pen for snbai11 d g Wa informadom, ioaelufag the paidbft of fires and bmprbouumt for hsowiag vbladom.s
w *AppHcatim Modmd: S - Surface, IN - Isjeet omr , INC - ftorporstlon
_-, **V'oRttlmtb:a Rabe: Smftw - 0.5, N. 11 j orparatheas - Le
Signature of Land Appher Date ***fin Rates: Compost - 0.1, AuaerobdeaBy D4pseed - 0,2,
Aerobbalhy+ ft abed - 03, Raw Sludge - OA
****CJ'J..R.: Cumulm im PoEMsnt Loading Rate
DOR FORM FSF (12PAM

ANNUAL LAND APPLICATION FIELD S[}AOOUXY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND KMNff 'TED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR DOX WHEN NOT APPLICABLE.
Fad ty Nsme: Triple S ftm WQ Peace #: WQfaQ OM Field #:
Owner: Eric f w Lnu>amt Dry Tons Applied: 12.92 Sita #:
Acres Utfllzm :
Acres Permitted:
Fuc Predomhmt SUR Series G*A Cation Ewe Capacity ion S03):
Crop 1-Nwllne: Mfild Craps i Max PAN: 140.00 Crop 2 Name: #WA Crop 2 Marx. PAN
8.13
8.93
.PYA
#NIA
s0 [.-177�.S
o ".,
.,+: fir: :. >•,\
f i'
®�.S' 7a��
1 i1
i k'
i
���
k 1!
1 7.9M, , r; Rm 3
�'�,�I
411 ewM, =&w p waW of bm, that lids docemen# wws prepared under my dir ftm or snpervlalan in wwrdance with a system
defgaed to amwe that qa §%W personal properly gatbered and evaluated *a information wbmlued. I am mare that there m
si�rHlcasit for g fibe hdormadan, huiadkg. the pomdd ty' of fines mud hasprLonnxW &r knowing vlmlatkrns\"
p, *Appltatton Melhod: S - Surbme, IN - h dwAaas, WC-1worporatimn
C2 71QQ `t _ r **Yolitihaiion Rate: Surface - 0, 5, Iniectlonlineorpaniion -1.0
S4mfftxn of Lancs Applier Daae ***Mherametion Rates: Compost - 0.1, Aemerobically Digested - 0.2,
Amolak*W Digested - 0-% Raw Sludge - OA
****C.PI-JL: Ca nalative Pollutant Loading Rate
DENR FORM FSF (1=W

RESIDUAL ANALYSIS LAB SHEETS

Dec 10 2018 01:22PM Nrnberly G. Quinn 9102984977
page 1
Environmental Chemists, Inc.
• 6602 Windmin Way, Wdn*% ot%, NC 28405 • 910.392.0273 Lab • 91D MA424 Fax
710 Eoweertowft Road, Manko, NC 27954 • 252.473.5702isb/Fax
25frA Wdminginn Highway, jadmnvikle, NC 28540 • 910.3475843 Lab/Fax
ANALYTICAL 8, CONSULTING CHEMISTS info@environmeoLalchwW ts.com
Town of Bmdavllle Debs of Report: Oct 42, 2418
Post Office Sox 130 Custorrier PO O:
Beulaville NC 28518 Customer 10; 08100015
AtIendon: Angie Miller Report Ik 2018-13369
Project ID; Sludge
Lab ID � Sample 10:
18-33636 Oft. %Was
Cdlect Daib mme Mau Sampled by
8/1412018 8:30 AM SolkUSludge client
Teet
Method
Resulis
Date An&Vnd
Sludge Reel kwk
Aluminum
EPA 200.7
2420mgrq
06MUM16
Arsenic
EPA2W.7
49.9mgAt
06MMOI8
Cadmium
EPA X00.7
X39.9 mgft
08/762018
Calcium
M2ao-7
18000moft
08/1 620 1 8
Chromium
EPA 2W7
<39.9 mgft
08/182018
Copper
EPA200.7
93.5 mglkg
08/16018
Lead
Em2w*
<39.9 mgft
08116=18
Magnesium
EPAX0.7
1260 Mgft
48/15078
Molybdenum
ffA2W.T
<39.9 mgft
08/17/2418
Nickel
EPA2W.7
'439.9 mg"
08/16201$
Potassium
EPAM7
3034 mglkg
08!1512478
Selenium
WA2W7
<39.9 nft
0811602018
Sodium
EPA 200.7
3880 rnWIcg
0801502018
Zinc-
EPA 2ao.7
268 mV -kg
08116/2018
Mercury
M X&I
<1.16 mgft
08117/2418
Nit t&+Nitriile-Nitrogen
EPA3M
141 mgft
0824/2018
TOW Solids (96)
SM 2W a
1.36%
4811812018
pH
SM4W N 8
6.23 unlls
08221707$
Ammonia Nitrogen
SM 4M NHS C
2900 rngAgg
49!0702018
Total KPIdahl Nitrogen (TKN)
SM 4= Ora B
51800mgft
0901202018
Total Phosphorus
SU4= P F
17540 Meet
4802212018
Comment. Residuals, G=W
pH, reporled on a dryweight basis.
Reviewed by: HQI;,r.
011��
fUW t &t: 2We-133at P"01011

00
4m
N
CD
%J
0
0
~, viroche"m
r
ENVIRONMENTAL CHEMISTS, INC
NCDENR: OWQ CERTIFICATION 8 W NCD OM DLS CERI7FI[`ATM i 37729
COLLECTION AND CHAIN OF CUSTODY
*W VPAWk iN W&Y Wft0k%9W% IAC 28403
OFFICE: NO FAX [phone]
in hft=M
Cliod: PROJECT NAME:
REPORT NO: led— 1 -3
ADDRESS: CONTACT NAME:
PO NO:
REPORT TO'
PHONE/FAX:
COPY TO:
wmm:
Sarealed Bv: SdIMPLE TWE: I a Mflu" E a RMumd, lW = WWI. ST a Stam, SO = So% SL = 8lud ^ 00w.
Tomperature when

Environmental Chemists, Inc.
i 6602 Windmill Way, W hni gton, NC nQ5 . 910.392.0223 Lab . 910 392.4424 Fax
710 Bowsertown Roar/, ll+lanteo, NC 29954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info r@environmentalchemists,com
Town of Kenansville
EPA 335A
Date of Report: Apr 30, 2018
4/16/2018
PO Box 370
SM 450D H 8
Customer PO #:
04106/2018
Kenansville NC
28349
Customer ID. 09020018
04/1612018
Attention: Garry Benson
matrix interference.
Report #: 2018-05250
Ignitability
SW 846 method 1010
Project ID; Sludge
04/24/2018
Chlorobenzene
SW846 Method 82WM030
<0.01 mg1L
04/1312018
Chloroform
SW846 Method 826015030
<0.01 mg1L
0411312018
Methyl ethyl ketone
SW846 Method 826015030
<0.05 mg1L
04113/2018
Tetrachloroethylene
SW046 Method 8260/5030
<0.01 mg/L
04/13/2018
Trichloroethylene
SW846 Method 826015030
<0,01 mg/L
04/13/2018
Vinyl Chloride
SW846 Method 82601503D
<0.01 mg/L
04113/2018
RCI
Cyanide
EPA 335A
<0.05 mg/kg
4/16/2018
pH
SM 450D H 8
7.11 units
04106/2018
Sulfide
SM 450D S 0
<0.1 mg/kg
04/1612018
Reporting limit elevated dire to
matrix interference.
Ignitability
SW 846 method 1010
>212 °F
04/24/2018
Sludge Residuals
Aluminum
EPA 20D.7
4450 mg/kg
04/10/2016
Arsenic
EPA 200.7
<32.8 mg/kg
04/10/2018
Cadmium
EPA 200.7
<32.8 mg/kg
04/10/2018
Calcium
EPA 200.7
30500 mg/kg
04/1112018
Chromium
EPA 200.7
<32.8 mg/kg
04/10/2018
Copper
EPA 200.7
446mglkg
04/10/2018
Lead
EPA 200.7
<32.8 mg/kg
04/10/2018
Magnesium
EPA 200.7
2190 mg/kg
04/11/2018
Nickel
EPA 200.7
<32.8 mg/kg
04/10/2018
Potassium
EPA 200.7
3270 mg/kg
04/11/2018
Selenium
EPA200.7
<32.8 mg/kg
04/10/2018
Sodium
EPA 200.7
6890mg1kg
04/11/2018
Zinc
EPA 200.7
743 mg/kg
04110/2018
Molybdenum
EPA 200.8
<32.8 mg/kg
04/17/2018
Nitrate}Nitrite-Nitrogen
EPA 353.2
34.3 mg/kg
04/18/2018
Total Solids N
SM 2540 8
1.5210/6
04/06/2018
Ammonia Nitrogen
SM 4500 NH3 C
912 mg/kg
04/1112018
Report k 2018-05260 Page 2 of 3

Environmental Chemists, Inc.
• 6502 Wmdrnill Way, Wihnington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Pax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347:5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town of Kenansvllle
Date of Report: Apr 30, 2018
PO Box 370
Customer PO #:
Kenansville NC 28349
Customer ID: 09020018
Attention: Garry Benson
Report #: 2018-05250
Cadmium
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4590 Org 8
3850 mg/kg 04119201 B
Total Phosphorus SM 4500 P F
20000 mglkg 0411612018
Mercury SWM7471B
22.4 mg/kg 04/10/2018
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg1L
04/17/2018
Barium
EPA 2-00.7
<1.0 mg/L
04/17/2018
Cadmium
EPA 200.7
<1.0 mg/L
04/2012018
Chromium
EPA 200,7
<1.0mg/L
0411712018
Lead
EPA 200..7
<1.0 mg/L
04/17/2018
Selenium
EPA 290.7
<1.0mg/L
04117/2018
Silver
EPA 200.7
<1.0mg1L
04/17/2018
Mercury
EPA 245.1
- <0.0020 mg1L
04/11/2018
Comment; Sludge residuals reported on a dry weight basis.
Reviewed by: _ RQJlk0
Report &:: 2018.05250 Page 3 of 3

• ENVIRONMENTAL CHEMISTS, INC NC 29405
910431924424
Analytical & Consulting Chemists NCDENR: DWC CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Town of Kenansville
PROJECT NAME: Annual Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Garry Benson
PO NO:
PRESERVATION
REPORT TO:
PHONEAFAX:
COPY TO:
Ismail:
Sampled Bv: SAMPLE TYPE: I = Influent E = Effluent. W = Well. ST = Sbwm. SO = Soil. SL = Sludge. Other:
Sample Identification
UMMME
PRESERVATION
I W I I jv
IN ���Mmq
Full TUP/RCUNWients/Metals
0Relinquished By.
Temperature when Received: .� Accepted: "ectea: IKesample meguemea:
041
Delivered By: Received By. ,. .1/, L."---�l�te: Time; f

Dec 10 2018 01:29PM Kimberly G. Quinn 9102984977
page 12
ron in c,-
ntal. Chemists,ji-je.
ti f="" hhi13 W iritlntiil W'-,Iy, Wifininglan, NC 2840 910,39102-23 Lab . 711i.3a)�: i i7; Fay
4 - _ Wit' 1L) fbJw'ticrtuwn Read, Moto au. NC:. -'t.5 F a 2K.473 -5702 i ih!l,,Ix
2,5—A Wilmingt,m "i9iuvap,JMbonviile.QVC. 2K.W 910.3x;. ji, f.atsf.Fax
ANAi_tTCAL & t'ONSULrING G>i�ivlls 48
JIS i iHu CJ7�it ihLilii- ilia �::It'I1Tf tilCti3r-t
Town of Rcse Hill Date of Report: Apr 28, 2018
P. O, Bax 8 Neu~ PO tk
Rose Hifi NC 28458 Cuebarner tD: 06020035RtGention: Carl Wheeler Repart 0., 241.8,04859
prolm a Sludge
L*b 10 Sample in:
Collect DateMme
lilainc� Sampled—by
18-12122 Site: Sludgy
3/2B/2018 9:00 AM
Sd[d/Sludge Carl Wheeler
Test
—""
Methtyd
Results
Data Analyzed
C snide
y F4S1"4iV IM*I*VGW duM tO.1w.h C I , �itsrt wC*,
<0.05 mg*g
04I041201 B
pl i
SM4wo �+ B
7.Oe unIs
04/tll
O2Q18
SulfidesM
Anaiynd outside or hulding ffne.
oeao s n
2:QO rliq%
04MIMM18
Ignittawtibi
Sw ass Mew ,oio
Sludge Residuals
X220 °F
04/2412018
Aluminum
evA 2sa.r
Arsenic
TEPA 2%'?
8450 m9ft
ONX4019
Cadmium
•17,8 mak$
43f3wO18
Calcium
EPA 400.7
07-5 mg9
0313t>s12018
Chrsmktm
i"cPA 200.7
1 "w mgfkg
D4A0412018
Copper
EPA X0.7
30.Smgilcg
Q31a(MIS
1_eatlSa+
� �Q7
9
OV30=16
Magnesium
EFAo
S 2
011IM2018
Mdybdonum
EPA=100r
r
1140mglkg
04/0 nate
Nickel
9'A 2sa7
•17.5 mllg
0313012018
Potassium
i�A2ao.7
•17.5mg/kq
0313q►201g
Sela nllin7
EPA 200,7
2230 fi¢►l�g
�1.$
Sodium
EPA
<17;5 m13�9
03130121!18
2•rncEPA
sPA 2w 7
984 m9ft
04i /2018
Nftr9WNitr4e-Nitrogen.
208.7
EPA35a2
9M. 5
03i' M018
Total Sands (%)
am 260 a
3.88 mglkg
04/181201B
Ammonia N �g�
5M 4500 wis C
3.04%
031281Z018
Torsi Kjeldahl Nlbogen (M)
sM4aotQa
2560 mglkq
04/O�A18
Tots) Phosphorus
SM 4800 P F
48700 mpg
04✓G tla
13400 mglisg
0410412018
ROpwls. PdlBW869
^�_
Pamn i of 7

Dec 10 2018 01:30PM [Imberly G. Quinn 9102984977
page 13
nNiron me ta.i Chemists, Inc.
1O�4,A). w{ 7^ilki; 17,
0. Box
Rx 8 ose Hill
P. Dato of Report: Apr 25, 2018
P. 4.
Customer PO N:
Rase Hill NC 28458 Castomer ED: 09020035
At#entian: Can Wheeler Report 2: 2018-04658
Project ID: Sludge
Mercury suva�4r�e 1..74.mglkg 04/1(112098
Comment Sludge residuals reported on a dry weight basis,
Reviewed by:;.
Pepe 2 of 2

9
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ENVIRONMENTAL CHEMISTS, INC � FAX
+icy MQ COW"Uoa"I MCCWM: OLS CBMMATIM *arm
1 UlMAROUNQ*

envirochem
6h� M)
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab , 910.392.4424 Pax
710 Bowsertown Road, Manteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Environmental Services Date of Report: Jan 21, 2019
PO Box 1054 Customer PO #:
Jacksonville NC 28541 Customer ID: 14110017
Attention: Sonny Scozzari Report #: 2018-21339
Project ID: Bear Trail Goff Course
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-53717 Site: Sludge 12/26/2018 9:00 AM Solid/Sludge Sonny Scozzari
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
3560mglkg
12/31/2018
Arsenic
EPA 200.7
<25.7 mg/kg
1213112018
Cadmium
EPA 200.7
<25.7 mg/kg
12131/2018
Calcium
EPA 200.7
23300 mglkg
01/01/2019
Chromium
EPA 200.7
<25.7 mg/kg
12/31/2018
Copper
EPA 200.7
210 mglkg
12/31/2018
Lead
EPA 2001
<25.7 mglkg
12/31/2018
Magnesium
EPA 200.7
2320 mg/kg
01/01/2019
Molybdenum
EPA 200.7
<25.7 mg/kg
12/31/2018
Nickel
EPA 200.7
<25.7 mg/kg
1213112018
Potassium
EPA 200.7
3920 mg/kg
01/01/2019
Selenium
EPA 200.7
<26.7 mg/kg
01/06/2019
Sodium
EPA 200.7
11800 mg/kg
01101/2019
Zinc
EPA 200.7
1260 mg/kg
12/3112018
Nitrate+Nitrite-Nitrogen
EPA 353.2
100 mg/kg
01/18/2019
Total Solids (96}
SM 2640 8
2.21%
1 212 7120 1 8
pH
SM 4600 H B
6.58 units
01/08/2019
Ammonia Nitrogen
5M 4500 NH3 c
723 mglkg
01/11/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 are B
76500 mg/kg
01/11/2019
Total Phosphorus
SM 4500 P F
18200 mg/kg
01/08/2019
Mercury
Sw84874718
X0.633 mg/kg
01/09/2019
Comment: Sludge residuals results, Except pH, reported on a dry weight basis.
pH reported on an
as received
basis.
Reviewed by
104-1e
Report #.: 2018-21339 Page 1 011

ENVIRONMENTAL CHEMISTS, INC
Analytical & Ccnsuk1rS Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
0602 Windmill way MIntingWn, INC 26405
OFFICE: 910.3924223 FAX [phone]
info&nvlranmwrtaWA=isWwm
CLIENT: ENVIRONMENTAL
PROJECT NAME; Bear Trail Golf
REPORT NO: 91 o-``% = CI' L(
ADDRESS: 103 Troy Avenue
CONTACT NAME: Sonn Sg=ari
PO NO:
Jacksonville NC 28540
REPORT TO; Sonny Scmari / Albeaa Y. QkjjmojQ
PHONFJFAX: 910-54544991808-342-5847
COpY TO:
a es. trsmc.mi
email•
warn 19Gt Rs :
Sample Identification
[
Collection
SAMPLE TYPE:
I
I is
, is a 0
`
w y
I = lnfluseM;
"
E C Efliuen%
$ � PRESERVATION
m W
5 x
W 9 Well, ST = Stream SO - Soil, $1. m Sludge, Other:
ANALYSIS REWESTED
Date Time
Tem
Bear Trail Golf
E
C P
�3 444
X
BOD, TSS, NO2
EFF pH:
C P
X
NH3, NO3
G G
1 /Month sampling
P
X
Fecal Coliform
G
C P
G
X
TKN, Total Phosphorus
.�..�C, i
1'4Wl 0100
13 #
C P
G
C P
G G
C P
G G
C P
G G
C P
G G
C P
PTO]
G G
Transfer Reil ished the Received DabeTme
2.
temperature when Race ed: 9 ic � Accepted
Delivered By: Received By: Date: N Time. 3 L.Ya,
Comments, TUftNAROUND:

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsert+own Road, Manteo, NC 27954 . 252.473.570.2 Lab/Pax
255-A Wilmington Highway Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@,envirot'imentaichexnists.com
Branch Residuals/Bob Branch
Date of Report: Apr 12, 2018
Customer PO #:
Customer ID: 15060009
Attention:
Report #: 2018-04464
Project ID: Wallace WWTP
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
03/29/2018
Chloroform
sw846 Method 8260/5030
<0.01 mg/L
03/29/2018
Methyl ethyl ketone
swe46 Method 82eo/sow
<0.05 mg/L
03/29/2018
Tetrachloroethylene
SW848 Meuvd e260/solo
<0.01 mg1L
03/29/2018
Trichloroethylene
Sw848 Method 8250/5030
<0.01 mglL
03/29/2018
Vinyl Chloride
SW848 Method 8200/5030
<0.01 mg/L
03/29/2018
RCE
Cyanide
EPA 335.4
<0.05 mg/kg
03/27/2018
Sulfide
SM 4500 s D
<0.1 mg/kg
03/26/2018
Reporting limit eievated due to matrix
interference.
Ignitability
SW 846 method 1010
X212 °F
03/27/2018
Sludge Residuals
Aluminum
EPA 200.7
10700 mg/kg
03/26/2018
Arsenic
EPAZ00.7
<30.4 mg/kg
03/30/2018
Cadmium
EPA 2007
<61.1 mg/kg
03/2612018
Calcium
EPA 200.7
27800 mg/kg
03/29/2018
Chromium
EPA 200.7
<61.1 mg/kg
03/26/2018
Copper
EPA 2001
904 mg/kg
03/26/2018
Lead
EPA 2007
67.1 mg/kg
03/26/2018
Magnesium
EPA 200.7
4820 mg/kg
03/2912018
Molybdenum
EPA 200.7
<30.4 mg/kg
03/30/2018
Nickel
EPA 200.7
<61.1 mg/kg
03/26/2018
Potassium
EPA 200.7
3530 mg/kg
03/29/2018
Selenium
EPA 200.7
<61.1 mg/kg
03/26/2018
Sodium
EPA 200.7
7490 mg/kg
03/29/2018
Zinc
EPA 200.7
1580 mg/kg
03/26/2018
Nitrate+Nitrite-Nitrogen
EPA 953.2
<1.20 mglkg
04/05/2016
Total Solids (°110)
SM 2540 s
1.67%
03/22/2018
pH
SM 4500 H e
6.96 units
04/06/2018
Ammonia Nitrogen
SM 4500 NH3 C
2100 mglkg
03/27/2018
Report#:: 2018-04484 Page 2 of 4

Environmental Chemists, Inc.
it 6602 Windmill Way, Wiirnington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28,540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@,,environmentalchcmists.com
Branch ResidualslBob Branch Date of Report: Apr 12, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2018-04464
Project ID: Wallace WWTP
Total Kjeldahl Nitrogen (TKN) 5M 4500 Org B 64600 mg/kg 0312212018
Total Phosphorus SM 4500 P F 30500 mg/kg 03/28/2018
Mercury Sw848 7471B 1.50 mg/kg 0312312018
TCI_P Metals
Arsenic
EPA 200.7
<1.0 mg/L
03131!2018
Barium
EPA 200.7
<1.0 mg/L
03/31/2018
Cadmium
EPA 200.7
<1.0 mg/L
03/31/2018
Chromium
EPA 200.7
<1.0 mg/L
03/31/2018
Lead
EPA 200.7
<1.0 mg/L
03/31/2018
Selenium
EPA 200.7
<1.0 mg/L
03/31/2018
Silver
EPA 200.7
<1,0 mg/L
03/31/2018
Mercury
EPA 245.1
<0.0020 mg/L
04/03/2018
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
18-11082 Site:1
3/21/2018 10:35 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
18-11083 Site:2
��LFfn-]
SM 9221C E MPN 24 hr 503
2.12% 03/22/2018
15567 MPN/g 03122/2018
Collect Date/Time Matrix Sampled by
3/21/2018 10:38 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 2.07% 03/22/2018
Fecal Density SM 92210 E MPN 24 hr 503 53141 MPNIg 03/22/2018
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
18-11084 Site: 3 3/21/2018 10:42 AM Water Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2,01% 03/22/2018
Fecal Density SM 9221C E MPN 24 hr 503 16418 MPN/g 03/22!2018
Report #:: 2018-04464 Page 3 of 4

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ANALYTICAL R CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manbeo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 lab/Fax
info a@environmentalchemists-com
Branch ResiduaWBob Branch Date of Report: Jun 13, 2018
Customer Pd #:
Customer ID: 15060009
Attention: Report #: 2018-07366
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-18343 Site: sludge 519/2018 10:16 AM Solid/Sludge Ralph Ezelle/Bradley Vann
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
10500 mg/kg
0610212018
Arsenic
EPA 2M.7
<20.1 mg/kg
06102/2018
Cadmium
EPA 200_7
<20.1 mglkg
06/02/2018
Calcium
EPA 200.7
24300 mg/kg
05/11/2018
Chromium
EPA 200.7
27.4 mg/kg
06/02/2018
Copper
EPA 200.7
859 mg/kg
06/0212018
Lead
EPA 200-7
62.2 mglkg
06/02/2018
Magnesium
EPA 200.7
2940 mg/kg
0511 1/2018
Nickel
EPA 200.7
<20.1 mg/kg
06/0212018
Potassium
EPA 200.7
3900 mg/kg
05111/2018
Selenium
EPA 200.7
<20.1 mglkg
06/02/2018
Sodium
EPA 200.7
4820 mglkg
0511112018
Zinc
EPA 200.7
1370 mg/kg
06/02/2018
Molybdenum
EPA MR
<20.1 mg/kg
06/05/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
792 mg/kg
05/21/2018
Total Solids
SM2U0 s
2.49%
05/10/2018
PH
SM4500"D
7.12 units
05/21/2018
Ammonia Nitrogen
SM 4500 NN3 c
3730 mg/kg
05/17/2018
Total Kjeldahl Nitrogen (TKN)
SM 46DO 0rg B
55400 mg/kg
05/17/2018
Total Phosphorus
SM 4500 P F
1550 mg/kg
05/17/2018
Mercury
SW846 74718
0.7230 mg/kg
05/31/2018
Report #:: 2018-07986 Pa x, i of a

MW
ay Wil
w
ENVIRONMENTAL CHEMISTS, INC OFFICE:
-022323E iAX910,M-4424
406
Analytical & Consulting Chemists
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Branch Residuale/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: 0_7
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT TO:
PHONEIFAX: 284.790 284.5073
ANALYSIS REQUESTED
COPY TO: Anthony Colon, Public Works
email: bdeangtownofwallace.aom
Sampled By; hr4dley Vghw► & 04&k Ezr,41 SAMPLE TYPE: I = Influent, E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Siudoe. Other:
Sample Identification
Collection
I
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a
E ; opp
Gl
t �
O
c W
s
21
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PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
Z
Z
c
a
0
Sludge
C P
X
nutrients/metals
39-1ff 10110
G G
1
C P
X
fecal dens' 1 %TS
5- 9. If lacy
G G
2
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X
fecal density/ %TS
5-9-12' ICIDq
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3
5-9-12 too &
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X
fecal density/ %TS
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4
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fecal density/ %TS
5'- 9- 11? 1008
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5-9-!$ 1010
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55 9-11? p!y
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G I G
Transfer Rellnquished Pr Dataffime Rec By: Dat&Mme
1- 51241V IDxla
2.
Temperature when Received: It.,3 Accepted: ejected: Resample Requested:
Delivered By: Received By: L_. �-Date: 3 "" Time: ! z -
TURNAROUND:

Envi7rochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 0 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail].
Branch Residuals/Bob Branch Date of Report: Oct 16, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2018-14714
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-37286 Site: sludge 9/512018 9:32 AM Solid/Sludge client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
9640 mg/kg
09/0912018
Arsenic
EPA 200.7
18.3 mg/kg
09/09/2018
'EPA -200,7
<18.3 mg/kg
09/09/2018
Calcium
EPA 200.7
24600 mg/kg
09/25/2018
Chromium
-EPA 200.7
54.0mglkg
09/09/2018
Copper
EPA 200.7
737 mg/kg
09/09/2018
Lead
EPA 200.7
98.6 mg/kg
09/09/2018
Magnesium
EPA 200.7
2830 mg/kg
09/25/2018
Molybdenum
EPA 200.7
<18.3 mg/kg
09/27/2018
Nickel
EPA 200.7
39.6 mg/kg
09/09=18
Potassium
EPA 200.7
3090 mg/kg
09/25/2018
Selenium
EPA 20D.7
<18.3 mg/kg
09/0912018
Sodium
EPA 200.7
3960 mg/kg
09/26/2018
Zm0 _ ......
EPA200.7
.131.0 mg*g .._.
--- . -09i'081201-8
Nitrate+Nitrite-Nitrogen
EPA 353.2
151 mg/kg
10/01/2018
Total Solids M
SM 2540 B
2.78%
09/06/2018
pH
sM 4500 H B
6.93 units
09127/2018
Ammonia Nitrogen
SM 4500 NH3 c
337 mglkg
10/15/2018
Analyzed outside of holding time.
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
47400 mg/kg
10/151/2018
Total Phosphorus
SM 4500 P F
22500 mglkg
09/26/2018
Mercury
SWO467471B
1.04 mg/kg
09/09/2018
Report#:: 2018-14714 Page 1 of 3

dm"!> ENVIRONMENTAL CHEMISTS, INC
Analytical &Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NO 28405
OFFICE: 910+392.0223 FAX 910-X2.4424
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: /17 ltf
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC i
PO NO:
PRESERVA
REPORT t,O: `.
PHONE/FAX: [phone]
ANALYSIS REOUESTED
COPY TO: jAnthany Colon, Public Works
email: [e-mail]
Salmoled By: tlor= LlAvj- d- S MPLE TYPE: I = Influent. E = Effluent. W = Welly ST o Stream. SO = Soil. SL = Siudae. Other:
Sample Identification{
Collection
a
:°
[7 o
s E
Q W
W Z
PRESERVA
ION
ANALYSIS REOUESTED
Date Time
Temp0
W
_
o
Sludge
P
i
X
nutrients/metals
9-5-119 09&P-
G G
1
P
3 }�!�
X
fecal densi I %TS
- S -N 0919
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2
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X
fecal density/ %TS
_t ,'lo
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'
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fecal density/ %TS
9 -.5-1$
G
4
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/
X
fecal density/ %TS
-5741? o m
G
5
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Lam -I
X
fecai density/ 0/6TS
- - i$ 09A"
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X
I
fecal density/ %TS
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7)
C1 I P
�$U'
}fit^I
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fecal densi / %TS
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i
Transfer Reli uiehed By: Datef ime By. Datelfime
1. 9-S .2oje
2.
Temperature when Received: Accepted: jected: RO.wmple Reg ed:
Delivered By: `'"! Receive4 By: Date:`v Time: 3 _

Environmental Chemists, Inc.
6502 Windmill Way, Wilmington, NC 28405 • 91.0.392.0223 Lab • 910.392.4424 Fax
710 8owsertown Road, Manteo, NC 27954 • 2,52.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL. & CONSULTING CHEMISTS info(c enviroamentalchemists corn
Branch Residuals/Bob Branch Date of Report: Nov 17, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2018-17185
Project ID: Wallace WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
18.43409 Site: sludge 10/18/2018 11:17 AM Solid/Sludge Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
12800 mg/kg
10/25/2018
Arsenic-- -
EFA -2Q0 7........._.. _ .
-<20:2-nWkg
101261-2048
Cadmium
EPA 200.7
<20.2mglkg
10/25/2018
Calcium
EPA 200.7
29600 mg/kg
10/23/2018
Chromium
EPA 200.7
35.2 mg/kg
90125/2018
Copper
EPA 200.7
992 mg/kg
1 012 512 01 8
Lead
EPA 200.7
65.2 mglkg
10/25/2018
Magnesium
EPA 200.7
3200 mg/kg
10/23/2018
Molybdenum
EPA 200.7
020.2 mg/kg
10/2512018
Nickel
EPA 200,7
25.8 mg/kg
10/25/2018
Potassium
EPA 200.7
3330 mg/kg
10/23/2016
Selenium
EPA 200.7
<20.2mg/kg
10/25/2018
Sodium
EPA 240.7
4390 mg/kg
11/1412018
Zinc
EPA 200.7
1760 mgikg
10/25/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
159 mg/kg
11/0812018
Total Solids (%}
SM 2540 B
2.53%
1 01=01 8
pH
SM 4500 H B
7.36 units
1 012 512 0 1 8
Ammonia Nitrogen
SM 4500 NH3 C
3300 mg/kg
1012312018
Total Kieldahl Nitrogen (TKN)
SM 4500 org B
49400 mg/kg
10/22/2018
Total Phosphorus
SM 4500 P F
23900 mg/kg
11/02/2018
Mercury
SW8467471B
0.7910mg/kg
10/2312018
Report X: 2018-17185 Pane 1 of 3

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Dec 10 2018 01,25PM Kmberly G, Quinn 9102984977 page 7
5 -Dec -21518 15:14 911037701
91BZ93MI
Dec. 5.2018 10:06AM
Tom Of Warsaw p`�
No -5064 P. 2
_
EnvironMental Chemists, Inc.
6602 Wandm ' Way, Wgn'In8tay NC 28905 • 910.392AM isb +
910392.412` Pax
720 BuwsextOVA Road, Wnoo, NC 27954 . 752.475.5702 isb/Pax
255-A "I-ftft Higfiway, Jsc "Us, NC 280 • 910.347.5M
Ubtltax
ANALY11CAL a Co NSUmNe C11EMlM
into(��viicoprllAh�ahEmrlls.cpno
Town of 1ik saw
P.Q. Box 464
date of CRMO& OC102, 2018
Warsaw NC 28300
Cnelsinsr PO 8:
AllN&n: 80 tYGwmedin
C im. 01070029
R*pmt#i: 2018.16371
Projeet N): Swdpe
Lsb ID SarapEs ID; Wanoaw WWTP
Collect 08taITime IUW Sampled by
184g all: Sludge
8/1412016 10:45 AM SoiidlSWps Client
Test
iMslhod �
s
811udps RaNdeals
Aiurninum
EVA zoe r
8640 rr�AtQ
061171!019
Arsenic
EPA 2aaa
Cadmium
�2oai
<32.6""g0611812018
Caloi�m
s32.6 nnpJkQ
0l�i'181201 i3
Chromium
ePA 400.r
16100 m9llg
05115/2019
IEPv►2ca.r
<32.5 mak
01311512018
Capper
&AX0.7
Law
533m#ft06/181
IS
tlrlapriesivrn
lP11200.7
eAA i0C.7
`32.5 s
WAS/2018
��denum
EPA =742.5
1570 n7pik9
091116/2015
Nickel
liiglkp
08M 712018
Pota�oaium
OR 200.7
i 5 9
0511612016
8eldrdum
W zoo.:
Zr00
0811612015
���
EPA 20x.7
42.5
08118/2018
Zbe4030m9ft
EPA 200.7
08/1b/2018
Mercury
ePa 200.7
1Si0 ft
0611$12018
Nitrale+�Niiriis-Nilsen
� ao3.2
2.36 mUft
05/17/2018
T0181 SO& ("%)
sM pro B
311 m9ft06/2412018
PH
1A9 %
Mlft018
SMl50p H 0
3.44 ulllte
05122/2016
Ammonia Nftg�
aM4MNHsc
2300 mg(ka
DR10712016
Tobi Kjeldahl NLroom (TKN)
SM 4MOro a
Tobal Phan p hwua
sM X00 P F
40300 �
0911212018
14200 m01kp
Comment Rasiduele, swept pH, reportasd on a dry weight b"jL
0812212018
I
Reviewed by; �
f
now*, M4.1arl

Dec 10 2018 01:25PM Krnberly G Quinn 9102984977
5 -Dec -2818 15:14 9192937781
5.2018_10:06AM Tnwfl Of WarSaw
w
page 8
9182937781 -
No. 5064
p.3
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TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF WALLACE
TCLP DATA WAS PROVIDED FOR THE FOLLOWING ADDITIONAL FACILITIES:
TOWN OF KENANSVILLE

y i
■
ANALYTICAL & CONSULTING CHEMISTS
Town of Kenansville
PO Box 370
Kenansville NC 28349
Attention: Garry Benson
Lab ID Sample ID:
18-13011 Site: sludge
Environmental Chemists, Inc.
6602 Windmill Way, Wdmington, NC 28405 . 910.392.0223 Lab . 910.592.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab /Fax
[e-mail]
Date of Report: Apr 30, 20'18
Customer PO M
Customer ID: 09020018
Report #: 2018-05250
project ID: Sludge
Collect Date/Time Matrix Sampled by
414/2018 10:00 AM Solid/Sludge Client
Test Method Resuitc Date Analyzed
Chlordane
Endrin
Heptachlor
Heptachlor epoxide
Lindane
Methoxychlor
Toxaphene
1,4 -Dichlorobenzene (TCLP)
2,4,5 -Trichlorophenol (TCLP)
2;4,6 -Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p -Cresol (TCLP)
Nitrobenzene (TCLP)
o -Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5 TP
2,4-D
1,1-Dichloroethylene
1,2-Dichloroethane
Benzene
Carbon Tetrachloride
SW 846 Method 8081E4510
<0.03 mg1L
0411112018
SW 846 Method 8081M510
<0.0005 mg1L
04/11/2018
SW 848 Method 80811/3510
<0.0005 mg1L
0411112018
SW 846 Method 8081913510
<0.0005 mg/L
04/11/2018
SW 848 Method 1108 1 513 5 1 0
<0.0005 mg/L
04/11/2018
SW848Method808150510
<0.0006 mg/L
04/11/2018
SW 848 Method 80818/3510
<0.05 mg/L
04111/2018
SW 845 method 8270/3510
<0.050 mg/L
04/12/2018
SW 846 method 8270/5510
<0.050 mg/L
04/12/2018
sW 846 method 82 M510
<0.050 mg/l_
0411 212 0 1 8
SW 848 method 8270/3510
<0.050 mg/L
04/12/2018
SW s48 method 827013610
<0.050 mg/L
04112/2018
SW $4s method 8279540
<0.050 mg1L
04112/2018
SW 848 method 8270/3810
<0.050 mg1L
04/12/2018
SW 848 method 8270/3510
<0.050 mg1L
04/1212018
SW 848 method 827013 6 1 0
<0.050 mg/L
04/12/2018
sw a46 rmthod 8270/3510
<0.050 mg/L
04/12/2018
SW 848 method 527013 5 1 0
<0.050 mg/L
04/12/2018
SW 848 method 8270/9510
<0.250 mg/L
04/12/2018
SW 848 method 827013.510
<0.050 mg/L
04/12/2018
SW846 Method 8161A
<0.003 mg1L
04/17/2018
swe4s Method a161A
<0.003 mg/L
04/17/2018
$M40 Method 8280!6030
<0.01 mg/L
04/1312018
SW548Method UM5030
<0.01 mg1L
04/13/2018
SW848 Method 82015030
<0.01 mg/l_
04/13/2018
SW846 Method 82$015030 <0:01 mg/L
E-MAILED APR 3 0 7018
04/13/2018
Report #:; 2018-052.50 d` S 1,11 Page 1 of 3

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910392.4424 Rax
71013owsertown Road, Manteo, NC 27954 . 252.473.5702 Lab /lax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 tab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town of Kenansville
EPA 336A
Date of Report: Apr 30, 2018
4/1612018
PO Box 370
SM 4500 H 6
Customer PO M,
04106/2018
Kenansville NC
28349
Customer ID: 09020018
04116/2018
Attention: Garry Benson
matrix Interference.
Report M 2018-05250
Ignitability
SW 846 method 1010
Project ID: Sludge
04/24/2018
Chlorobenzene
SW846 Maud 6260/8030
<0.01 mg/L
04/1W018
Chloroform
8VM6 Method 626015030
<0.01 mg/L
04/13/2018
Methyl ethyl ketone
SW046 Method 8260/5030
<0.05 mg/L
04/13/2018
Tetrachloroethylene
SW646 Method 8200/5030
<0.01 mg1L
04/13/2018
Trichloroethylene
SVM46 Method 826015030
<0.01 mg/L
0411312018
Vinyl Chloride
SVd846 Method 8260/5030
<0.01 mg/L
04113/2018
RCI
Cyanide
EPA 336A
X0.05 mg/kg
4/1612018
pH
SM 4500 H 6
7.11 units
04106/2018
Sulfide
SM 4600 s o
<0.1 mgfkg
04116/2018
Reporting limit elevated due to
matrix Interference.
Ignitability
SW 846 method 1010
>212 OF
04/24/2018
Sludge Residuals
Aluminum
EPA 200.7
4450 mg/kg
04110/2018
Arsenic
EPA 200.7
<32.8mglkg
0411012018
Cadmium
EPA 2001
<32.8 mg/kg
04/1012018
Calcium
EPA 200.7
30500 mg/kg
04/1112018
Chromium
EPA 200.7
<32.8 mg/kg
04/10/2018
Copper
EPA 200.7
446 mg/kg
041/0/2018
Lead
EPA200.7
<32.8 mg/kg
04/1012018
Magnesium
EPA 200.7
2190 mg/kg
0411112018
Nickel
EPA 200.7
<32.8 mg/kg
04/10/2018
Potassium
EPA 200.7
3270mglkg
04111/2018
Selenium
EPA 200.7
<32.8 mg/kg
04/10/2018
Sodium
EPA 200.7
5890 mg/kg
04/1112018
Zinc
EPA200.7
743 mg/kg
0411012018
Molybdenum
FPA 200.8
<32.8mglkg
04/17/2018
Nitrate+Nltrite-Nitrogen
EPA 3532
34.3 mg/kg
04/1812018
Total Solids (%)
SM 2540 B
1.52%
04/06/2018
Ammonia Nitrogen
SM 4500 NHS C
912 mg/kg
04/11/2018
Report #:: 2018-05260 Page 2 of S

Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910392.01223 Lab , 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town of Kenansvllle
Date of Report: Apr 30, 2018
PO Box 370
Customer PO #:
Kenansville NC 28349
Customer ID: 09020018
Attention: Gary Benson
Report #: 2018-05250
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN)
SM 4500 org a
3850 mglkg
04/11/2018
Total Phosphorus
SM 4500 P F
20000 mglkg
04/16/2018
Mercury
SWO4674710
22.4 mg/kg
04110/2018
TCI..P Metals
Arsenic
EPA 2003
<1.0 mg1L
04/17/2018
Barium
EPA 200.7
<1.0 mg/L
04117/2018
Cadmium
EPA 200.7
<1.0 mg/L
04/20/2018
Chromium
EPA 200.7
X1.0 mg1L
04/17/2018
Lead
EPA 200.7
<1.0 mg/L
04/17/2018
Selenium
EPA 200.7
<1.0 mg1L
04/17/2018
Silver
EPA 200.7
<1.0 mg/L
04/17/2018
Mercury
EPA 245.1
<0.0020 mg/i_
04/11/2018
Comment: Sludge reported on a dry weight basis.
Reviewed by: _�"rLo
CQ WAY,
Report k- 2018-05250 Page 3 of 3

ENVIRONMENTAL CHEMISTS, INC � nll miW9 FAMn 24
Analytical & Consulting Chemists NCDENR: DWC CERTIFICATION 9 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Town of Kenansviile
PROJECT NAME: Annual Sludge
REPORT NO: 05 2:7-0
ADDRESS:
CONTACT NAME: Garry Benson
PO NO:
REPORT TO:
PHONEIFAX,
CORY TO:
email:
Sampled Bv: SAMPLE TYPE: I = Influent. E = lEiflueaL W = Well. ST = Weam. SO = Soil. SL = Sludge, Other.
Temperature when Received: .j Accepted: _Rbjected:Resample Requested:
Delivered By: Received By., 11,.L L�--'�Date: - Time:
Full TCLP/RC11Nutdents/MeWs
WIN
Relinquished By.
Temperature when Received: .j Accepted: _Rbjected:Resample Requested:
Delivered By: Received By., 11,.L L�--'�Date: - Time:

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
770 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL& CONSULTING CHEMISTS [e-mail]
Branch ResidualslBob Branch Date of Report: Apr 12, 2018
Customer PO M
Customer ID: 15060009
Attention: Report M 2018-04464
Project ID: Wallace WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
18-11081 Site: sludge 3/21/2018 10:55 AM Solid/Sludge Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Chlordane
SW 846 Method 8 081 813 5 1 0
<0.02 mg/L
03/28/2018
Endrin
SW 846 Method 8 081 813 51 0
<0.0005 mg/L
03/28/2018
Heptachlor
SW 846 Method 80818/3510
<0.0005 mg/L
03128/2018
Heptachlor epoxide
SW 846 Method 80 81 813 51 0
<0.0005 mg1L
03/28/2018
Lindane
SW 846 Method 6081 819 51 0
<0.0005 mg/L
03/28/2018
Methoxychlor
Sw 646 Method 8081 813 61 0
<0.0005 mg/L
0312812018
Toxaphene
SW 846 Method 80818/3610
<0,05 mg/L
03/28/2018
1,4 -Dichlorobenzene (TCLP)
SW e46 method 827W3610
<0.050 mg1L
03/26/2018
2,4,5 -Trichlorophenol (TCLP)
SW 648 MEMOd 627D13510
<0.050 mg/L
0 3126/2 0 1 8
2,4,6 -Trichlorophenol (TCLP)
SW 846 method 6 27 019 5 1 0
<0.050 mg/L
03/26=18
2,4-Dinitrotoluene (TCLP)
SW 646 method 627D13510
<0.050 mg/L
03126/2018
Cresol (TCLP)
SW Me method 8270/3510
<0.050 mg/L
03/26/2018
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 6270/3510
<0.050 mg/L
03/26/2018
Hexachlorobenzene (TCLP)
SW 846 method 8270!3510
<0.050 mg/L
03/26/2018
Hexachloroethane (TCLP)
SW 8" method 8270!3510
<0.050 mg/L
03/26/2018
m + p -Cresol (TGLP)
SW 646 method 6270/3510
<0.050 mg/L
03/26/2018
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/26/2018
o -Cresol (TCLP)
SW 846 method 627019510
<0.050 mg/L
03/26/2018
Pentachlorophenol (TCLP)
SW 646 method 8270/3510
<0.250 mg/L
03/26/2018
Pyridine (TCLP)
SW 846 method 8270/3610
<0.050 mg/L
03/26/2018
2,4,5 -TP
SW846 Metrod 61s1A
<0.003 mg/L
03/2912018
2,4-D
SW846 Method 8151A
<0.003 mg/L
03/29/2018
1,1-Dichloroethylene
SW646 Method 62606o3o
<0.01 mg/L
03/29/2018
1,2-Dichloroethane
SWa46Method 826015030
<0.01 mg/L
03/29/2018
Benzene
WON Method 8280/5030
<0.01 mg/L
03/29/2018
Carbon Tetrachloride
SW846 Method 8280/5030
<0.01 mg/L
03/29/2018
Report #:: 2016-D4464 Page 1 of 4

-M"ql
Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wiimingtoin Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Apr 12, 2018
Customer PO #:
Customer ID: 15060009
Attention:
Report #: 2018-04464
Project ID: Wallace WWTP
Chlorobenzene
SW848 MetiW 8260/5030
<0.01 mg/L
03/29/2018
Chloroform
Swsa6 Method 826015030
<0.01 mg/L
03/29/2018
Methyl ethyl ketone
SW846 Method 8260/6030
<0.05 mg/L
03/29/2018
Tetrachloroethylene
sW848 Method 0260/5030
<0.01 mg/L
03/29/2018
Trichloroethylene
SW848 Method 8260/5030
<0.01 mg1L
03/29/2018
Vinyl Chloride
SW848 Method 8280/5030
<0.01 mg/L
03/29/2018
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
03/27/2018
Sulfide
sM 4500 s D
<0.1 mg/kg
03/26/2018
Reporting limit elevated due to matrix
interference.
Ignitability
SW 646 method 1010
X212 OF
03127/2018
Sludge Residuals
Aluminum
EPA 200.7
10700 mg/kg
03/26/2018
Arsenic
EPA 200.7
<30.4 mg/kg
03/30/2018
Cadmium
EPA 200.7
<61.1 mg/kg
03/26/2018
Calcium
EPA 200.7
27800 mg/kg
03/29/2018
Chromium
EPA 200.7
<61.1 mg/kg
03/26/2018
Copper
EPA 200.7
904 mg/kg
03/2612018
Lead
EPA 200.7
67.1 mg/kg
03/26/2018
Magnesium
EPA 200.7
4820 mg/kg
03/2912018
Molybdenum
EPA 200.7
<30A mg/kg
03/30/2018
Nickel
EPA200.7
<61.1 mg/kg
03/2612018
Potassium
EPA 200.7
3530 mg/kg
03/29/2018
Selenium
EPA 200.7
<61.1 mg/kg
03/26/2018
Sodium
EPA 200.7
7490 mg/kg
03/29/2018
Zinc
EPA 200.7
1580 mg/kg
03/26/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
<1.20mg/kg
04/05/2018
Total Solids (%)
SM 2540 B
1.67%
03/22/2018
pH
SM 4600 H B
6.96 units
04/06/2018
Ammonia Nitrogen
SM 4500 NH3 C
2100 mg/kg
03/27/2018
ReporW 2018404484 Page 2 of 4

Environmental Chemists, Inc.
■ a 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bnwsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a@environmentaichemismcom
Branch Residuals/Bob Branch Date of Report: Apr 12, 2018
Customer PO #:
Customer 10: 15060009
Attention: Report #: 2018-04464
Project ID: Wallace WWTP
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 64600 mg/kg 03/2212018
Total Phosphorus SM 4600 P F 30500 mg/kg 03/28/2018
Mercury SW945 74718 1.50 mg/kg 03/23/2018
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
03/31/2018
Barium
EPA 200.7
<1.0 mg/L
03/31/2018
Cadmium
EPA 200.7
<1.0 mg/L
03/31/2018
Chromium
EPA 200.7
<1.0mg/L
03/31/2018
Lead
EPA 200.7
<1.0 mg/L
03/31/2018
Selenium
EPA 200.7
<1.0 mg/L
03/3112018
Silver
EPA 200.7
<1.0 mg/L
03/31/2018
Mercury
EPA 245.1
<0.0020mg1L
04103/2018
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
18-11082 Site: 1
3/21/2018 10:35 AM Water Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2x40 B 2.12% 03/22/2018
Fecal Density SM 9221C E MPN 24 hr 503 15567 MPN1g 03/22/2018
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
18-11083 Site: 2 3/21/2018 10:38 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids M SM 2540 B 2.07% 03/2212018
Fecal Density SM 9221C E MPN 24 hr 503 53141 MPN/g 03/22/2018
Lab ID Sample ID: Collect DateITime Matrix Sampled by
18-11084 Site: 3 3/21/2018 10:42 AM Water Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%) sM 2540 B 2.01% 03/22/2018
Fecal Density SM 9221C E MPN 24 hr 503 16418 MPN/g 03/22/2018
Report ik: 2019-04464 Page 3 01`4

6-4 1lI
ENVIRONMENTAL CHEMISTSgw
, INC OFFICE: 910 4 2ayW�i1� Wilmington,
Analytical 8 Cansufting Chemists NCDENR: DWO CERTIFICATION* 94 NCDHHS: DLS CERTIFICATION #1 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Branch Realduals/Bob Branch
PROJECT NAME: SlugtWallace WWTP
REPORT NO: q T � q
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT TO:
PHONEIFAX: 284.7969 284.5073
COPY TO: Anthony Colon, Public Works
email: [e-mail]
Santnled Bv: c rr. A.. t &TKF NO% SAMPLE TYPE: I = Influeltt. E = Effluent, W = Well. ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
IL
a
liss
° v o'►
o w
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
yy5
Sludge
C P
f 0�
X
nutrients/metals h' '
G G
9
C P
1,
0
1
X
fecal density/°/6TS
-tg 1o3S
G G
2
C P
�163
x
fecal dens' I %TS
3•Ii-tv 1039
G G
3)
C P
r1 �
X
fecal density/ °/6TS
3 z -n? lbq;
G G
4
C P
•
��
X
fecal density/ %TS
"1-19 1n�S
G G
5
C P
X
fecal density/ %TS
31- 1D+f
G G
6)
C P
l�
X
fecal density/ °/6TS
3'11-1`4 105
G G
7
C P
110
X
fecal density/ %TS
3-�I-Ib� to
G G
C P
G G
_H
Transfer Relinquished By: Dame ved 13y: Detamme
1. 3-;1-xo�� ;3--2Z i 3:3a
2.
Temperature when Received: : v Rejected: Resample RegLwm :
Delivered By Received By: Date: 5_` Z Time:, g
Comments: TURNAROUND:

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Rose Hill, Town of Beulaville, Town of Warsaw, and Southwest Plantation meet
pathogen reduction and vector attraction reduction requirements through lime stabilization. The
Town of Wallace met pathogen reduction through fecal density and vector attraction reduction
through injection or incorporation
The forms for these facilities are marred appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Fadiity Nane: 2ple.SFarms A Cleaning WQ Permit Number: WQOg34998
WWTP Nam: Town of $aalawille VIWT.P ��.NPDES Number: NCOMWI8
w•I�YY�wwww�w
Monttorbig Period: From LIM2018 To 12/31/2018
Pathogen Reilection (13A NCAC 02T .111161- Please Indicate level schleved and alternative nerfarmel:
Clnse A: Alt A ) D
I Alt B Alk © C War MiQC3
Alt D n Priicr Test ©
Process to Fa*w Redwe PWwnmo
0
If ble alternative rlhrmeds A lite "Ptmcem >Per Rolm
©Hmt Dift El
Heat Treatpt D lilac fl
Bob -gay 11 Gamma D
Pasteauiul6n Q
Clan B: Alt. (1) Fecal De" Q
Alt. Process to SignifloandReduce PBdru
p
H to alternadvt Clem S oaW b db*te "Proem to
Linke Stabilization Elj
Aerabic Di ti+o�n
Anaerobic M
tion © n a' :;�,• e s fza ji ,:;i� ,y • ; a $ 4. �i - '
If ble to
alternative Performed(Claes A or Class B)m&ete the
fo madtnrin
dow
Parameter
A owable Leval
in Sludge
Padwip rr
DvtSty
F�coee-
F��
of AWY-4$
SampleUMtW
Typic
1'ecl3-
idmie
Geo. Mean
Urtrts
Fecal Coliform
2 x 1010 die
bib powar
per FM of
total solids
MPN
1000 mar: Per PM
of total solid (dry
wcl
Salmonella
(in lies of feel
COMM)
3 MM per 4 S ma
total solid (dry
. W&wx J%ku atiuvu j"EMUM a=P& 1'MOAM. vy 1 •ilv /) - rimm ARSUMM ==mauve
t.1(VS r+eduotiaar © Alt, 2 L4q-dM LowF.AIL 3 bench © t~ 4 (Spec, 0,:rptaloe) O
Alt. 5 14- Aet+abic) 13 Alt 6 (Alk, Staldlimf=7 - Stable) flAtt, 8 -Unstable) OAlt, 9 (lil#ectina) fl Alt 10 (hwapo ation) Qvector at4ractioa reduction alk n dives wore v arfm=W
CERTMCAT1ON STATEMENT (please cheek the appropriate statement)
® aI certify, under penalty of law, that the pathogen requirements in ISA NCAC 02T.1106 and the
vector attraction reductionairemerit in 15A NCAC 02T.1107 have been meta
"I certify, under penalty of law, that the pathegm requirements Im ISA NCAC 02T .1106 and the
0 vector attraction reduction requirement in 1SA NCAC 02T' .1107 have not been meta' Must note if
you check this statement attach an c*aaation why you have not met one or both of the
under my
With the system
designed to erasure that qualified personnel properly gather and evaluate the information and to determine
that the pathogen and vector attraction redwedon regairemenis have been met. I am aware that there are
signM cant penalties for false certification incladWS fine and imprisonment."
_
W. Stanle3r Miller, WWTP ORC
Prieparer Now and Tide (type or print)
S2,te -f "*/*
Signage of +
Land Applier Name and Title Cif alrglicab1gXg7e or print)
—.u'!f
Date ftnatury of Land Applier (if applicable) Date
*Preparw is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1 102 (26)
DENR FORM PvRF 0ZT (i2=M)

ANNUAL PATHOGEN AND VECTOR ATI'ItACTION REDUCTION FORM (02T Rules)
Fadllfy Name: Triple 3 Farms & Claae WQ Permit Number: Wp0U MB
WW rP Nwae: Town ofRoae Hill WWTF NPDES Number: NCOD56863
Monitoring Period: From 111/2018 To 1251/2018
Pathosen Reduction (15A NCAC 02T.1 1061 -Please ludteate I" achieved and Alternative nerformed:
Gose A: Alt. A timeltema
13 1 Alt B(Alk Treabnuat Q Alt. C CMq Tong 0
2 (40•day bench
A1t.D Prior T
O Woo= to Fnrdw Radom P
0
D
If affficabh to alteruative pwhnwd
PONA sad a �Prvcess to F�Ietllet naa
Alt. 6 (Asir. Stdift ien
IAIL10
Compost C3 HQat
C] Heat Trewwast fl '
'c I,
Beta Oe:ma:s Rav
M © � � ��
©
Closs B: Alt. 1 FeaalQ
Alt. (� Pfoccas to 3' t aatl R-1-06patboms
Na velar attraWan rodwtkm aitarnatim
U a 11eeb1v to Alts mnore
Clm B indkate "Proeese to Retlome
Stamlisati��t{../yam©
Air Ae[�c W
AA `�..��
r SMA'.
If a llcable to
alternative
Clam A or Cies tke
tnlloPwfua mo
dab:
Parameter
Allowable Level
in Su*
Pokogen Density
°
Fnq=My
ofAnalyais
Smaple
Teo1r
Wmumm
000.l fi=
im
Units
Fecal COMO=
2x 1010the
6th povwpr
per FM of
total solids
]w61sN
LTU
1040 MVnper V=
of total solid (dry
S dmoo Ila bacteria
(in lien of focal
coliform
3 baM por 4 gt�rw
tocol solid (dqr
+7.i�:LWjj.%if-I WRIkill D:TTI'VI- 7
Alt.1(Y3 rediutiam
©A1t.
2 (40•day bench
Alt. 3 (30,! bench)
(Spec. uptelca
D
Alt. 5 (14 -Day Aemblc
p
Alt. 6 (Asir. Stdift ien
IAIL10
®
Alt's . - Stable
Alt. S - i7mAable
3
t. 9 ectiorl
©
C3
Na velar attraWan rodwtkm aitarnatim
were
U KI'iF1UNF1U14 STATEMM T1' (please chi[ the appropriate statement)
® -I eerbily, ander penalty► of law, that the pathogen roqalremonts in ISA NCAC 02T .1106 and the
vector attraction reducfim reauirenaeat in ISA NCAC 02T.1107 have been met"
"I certify, Ander penalty of law, that the pathogen requirements In ISA NCAC 02T.1106 and the
13 vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met:' (Please note if
YOU check this statcumt attach an c:rplaMtlon why you have not met one or both of the
the
designed to ensure that qualified personnel properly gather and evaluafe the Informadon used to determine
that the pathogen and vector attra Aon reduction requirements have been met. I em aware that time are
significant penalties for false certillcation Including fine and imprisonment"
Mr. Carl Wheeler, WWTP ORC
Prepar r Name and Title (type or print) band Applier Name &W Title (if applicable)(type or print)
3iViAM of Prepares* Dab: Signahwe of Land Applier (if applicable) W slate
*Pry is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102 (26)
0ENNR FORM PVRF 02T (IMM)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Faciiity Nenw.- T IVe S Farms a Cleaning WQ Permit Number: W 0030998
WWTP Namw Souft" Plentabon_WWTp . _ NPDES Number. W00029501
Moultwfag Period From 1/1/2018 77 12/31/2018
© --i "MIN water penally of law, that the pathogen requiremeuta in 15A NCAC 02T .I106 and the
vector attraction reduction requiretneut In 15A NCAC 02T.1107 have been nat."
© "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T.1106 and the
vector attraction reduction requ remmt in ISA NCAC 92T.1107 have not been met:" (Please note if
you cheek tufa statement attach an explanadoo wlty you have not met one or both of the
_ ` `up'nuun au■ ueen mane under my dh*Won and supervlsioo In accordance wlih the rystem
designed to cusure that qualified personnelproperly gather and cMuate the information and to deteeroine
that the pathogen and vector attraction reductlen regnhMoats have been met: I am aware that there are
s[gni$eant penalties for fade eertlticado n including fine and ftnprisonment."
Mr. Sonny Sco ORC
PremwName or
tl type or print)
T yrt
Signature of
Land Appiier Name and Title Of epplicablc)(type or print)
Signature of Land Applier (ifappiicable) Date
•PMPS= Wde nW In 40 CFR Fart 303.9(r) and ISA NCAC 2T. i m (26)
DENR FORM PVRF 02-r (1212008)

ANNUAL PATSOGIW AND VLCrOKATTRACTION MMUCTKON Ft)P W 0903 Fes)
ftd&yNmm Ml a 8 Phar k Clm ft WQ Pmt �: bOLim
WWW Tamar" ww p �.._.�.... XPDu x=lb ex Ncoo2 7f?3
BK w I I pPiM Wj Pm Ulal To 14LOON
to
AgomdAft PdbnmDonft niumm Plrigaeaol+ $Alvis mow=
Puammete: ow. uwu �0°°6� afTYP AM
ztiok-
WN 1SX7 41MO Am idRN/ 0 OEM" Gob 9=
ftpww
Pend carom 0" clu
WDWVM
eft" a m 6W
o►am+orfr w j k"Wm
ATM UAMMUM (pWw sheep tbte fq�re>patate �aleet�q
� "P � ��' fQlt � . that the palhogoM regdre■m�a ftp � CRR �i3.33 a>!d tba v+ecbar
� 3+ed reatuiragte�th 40 C�8 S8Gi.331�a base met."
� "x � ■a�ax of 1aw� that tfre p�aparr �h11a 40 CRJt aqui � vaatar
m"mom be .0 cm W." m" aot wa Md." riot ft';ym cu*
thla abltemaat ait & an as barns ag east aye w beth
"M deter ba bm =& reeler mW dime do ud ewe ft aeeeordam wo fe Mtom
dwvnd to ease me guom peraoard p "aft paw sad e' SW& as hft=Wm am b Ahem se
that �e PoMesm w d vm ftr aamam raftedw regrdtaeWu lame lessee mat: Y m awm tW there an
*"=a peu ift offsw "mmun" w"ft !a Md :'
Mr. &a t K Dom V11WM OW Mr, Erin R font Yard Mft ORC
N4a�and - Qr )Laad A"HaX (if an "o or .
DW MoaftmofLad ApOw Qf �
'Iftopmfsd in4OCM%djo3"nd]SArlCr+CXr.1102C*
MR mw PVRF =(I="

A1UAL PATHOMN AND 'V®C lDR ATTRACTION RBDUMON F WM (503 Ries)
Fob Ramo Tapia 81 A
4nftJ n � `r n
ls To
A
LwW
ill g dp �111e1F1
2*10toeie 1 1
opm
Fact Co�li�brm PW %W� C�
atud ltw
(IoNmedat I 4d mmd(dq
,131 1 12,d44 f
fs—
WQPM=*Namdw= W OLtM
1 ice: NCQ
rrrur .�
TMW
mrAW&TiON0TATXmw eiwmk im �b
® `l M*, d(r1r,1M tide p@M - �b W # crR so= and do vector
Q 'R asr�lq►, radar PNOW 0110 , that &D POO" regdrmm@Kb in 40 CORMM oord dwvmtw
red�oetlea rega0r�eet he 40 COR x.33 lu�ve ssi ltieen tuet.�+ des lame iy�
thle ethehpggqmdln ggym hm matmet one dw be& *room
"'M men 1u baatt mmu m hx ooy door end arperv�3eat fn aeuordaaet with t1,e eAbeo
dsdpW to uwm that qui e1 proparly mer cad a daab thte aced to
dtM 9m aad ver attrsdit redeedm ngatraatb have bem dad, I am amm *at dwt an
dvm=* pmemm far fte owift m kdafts ihte me t oaML"
Mr. *0* )L. Dem. W M 4R(: Mr. Bde R jai t=d Om
ORC
Zw=
LidApp]3ar1�ema 'xYt1e Dw S ofr@ndAppHw(lfWplW") nde
*PRPM L ddlAW to 40 CFR Pet! 503.9(x) ad 1414 NCAC IT .1102 (?,6)
1W FORM PVW ma (12PJM)

ANNUAL PA,TROGZNAPM VICTOR ATTBACrM REDUClMff ICBM (W artier)
Fmft moue; ftk a Fkm A g!!!ft WQ p Abe *wl ali3om
WWTPN=m TbwnvfW 4=WWTP ASUP&M xcm2m
CXwri'ICATWN 3TATEMM (plots a &e gwrap rbte tq
M *1 cer ft, ■ Wk r poft edkrw, So Me pxbegr reqdmwb k 40 CMM32 32 wed der vnW
p "i cerft ander peadWatlowtthelthapoftopme rogubso hk 40 CYR MJ2 wed the vader
xftodko ndodim x et in 40 CllR +M 33 Lwre =t beam m"w (P ere aeRe H yn d aek
NO etaemwmt aleck a eaawtie■.tdty you bm est met One or beik acthe x+egptbrllum i
ddwmdmmdn has beet MR& vader Xly d ed Apert fit ftcmdmw witthe goom
decked tr man tket quluw permodpropeol POW aed evabute tie hdwns#m wed tr detarmbie
Ad the pesttopee quad *Um" nkdka req*mmob berm been ea. I an aware that tie ere
ftdOC tPM Mee IW Oft GKIEW010 hMhdb* AM ted. tenVr MORt#
Mr. M� � � ORC W. H& Land oRV
AN�� IIIIYw1
(Wx or purl) Lend Andw Nomme sand of Wk IMO)Oype cc
�-- Z
lkndmof pnpuwDo* ftwdmofL;@ndAppUw(lfWb")
hddhea in 40 CPR Plot 503J" mod ISAW,.W 2T.1 102 (26)
DEFIB FORM PVW 003 (IW M)

AWWAL PATHOGEN AND VZCTOR ATTRAMOX M=CnDN Rider)
FddWF Nom;
WWTP Nast
men (40 CFR
lead
WQ>bimban WQQ000998
NPDFSNawberr XOOMM
��
CRRTiiRCATjON 8TA'!�' {p�E �keck the a�pra'prl�e e�
"I ew1}, udar rmidt df;awil that the pulpa nqdrmo& in 46 aM M.32 o d the Yectw
dkwd u ofttfin g2kgge ilk 46 CFR WX hm baso ret.„
p "1 yusaw>Pal* d bow,a"the mft in da tPt mn and the vachm
Ntrse" redidim re+pd<+rssst is 40CFR 500.n hors not b*m wwL" (Please sft if yew dmw&
- - ._fide obtmM mato& en uWamkdss why yea have nrt set ase or be& oiA id ih.)
'pM det Ub"as ho ban made oder my dWa dw and uWrwMtes in aeeor4mm wink So suss
darted % eo o n 60 qumMftd p mmmd preery 000 and +tiv bob the i&rnwdm pwd to deknW e
that t@ pdbWa ad ■ntw attr MM r*addm r*pkewmN bm hom met. Y an mmm that &m are
dpaillmtpemitlr tar the ardfl,maties bdwfp Hae a" '. V, I is
bk. Baw x De W WTP ORG W. Baia R Soft l and Applift O3MRC
grrr�ri..r�i ��
gVa ar pj N m»d (N�Y3Pe ar
2
all
ftwmofhwwmv Dae SkaMm oflAW AMMw afWlio")
*Pnp wb dob d 1n 90 CMPwt 50.9(c) ad 15ANCAC2T .110206)
DMFt FORMA PVRF W3 (I="

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Fsdlily N=fte: TTTTTTTO& S Fannia & Cleerrig - WQ Permit Number: X30999
lMrP Name: Taws of Wwuw STM NFDFB Nom: _ WQ0021903
Menhorian Period; From 1/1/2019 To/4131/2018
Pathown Reduction (15A NCAC 02T .11061- Pleme indicate levd addeved and alternative neriormed:
Class A:
Alt. A 13 1
Alt B Alk Twafto ntj p I
Alt. 70* Tesfin p
Alt. S 14-D4 Aeraobic
D Alt 6 Alk. Siabi W ionfl
AILD (No Prior LeaE3 I Preolaw W Furdu r Redneo Patomm
p
Alt. 9
ble to alteraatatve A 1mba:k "Proen to hunker Renee 1'11
.
C t ©
Heat Drying p
Host Twat p
Themaphlic
Be" 13
0.8mma Ray 13
PastwAizedon
Claw B:
AIL 1 Fatal Dcadly ©
Ala. Piss to $'
Raduce PWhams
appikable to al#remtiveraved CLtat H iadieatle "Frieve!! to
Rete Pa
'�:
Stabilization
El Air
- © Compoefisix
p jAmUop d
Alia rmbic RigggM
[3,
v:>'�4. '; ': ,T` '4 "` ;ta+,•-' r ,,r.
_ .
If !nMcaMe to alternative onfonned(Clan
Aar Class lets the
monitarin� data:
Paratnetsr
Allowable Level
m Sludge
Pathogen Density
Excex-
FrequcMey
of,Analym
Sample
Type
seem
[leo. Meatt
UnitsdMM
Fecal Coliform
2 x 14 to the
6th pouver
pargMM of
tow solids til]
000 n4m per trate
of total amid (dry
't
Salmonella becteds3
(inlieu o f w
col�
per4 ymns
toW solid (dry
I wicigbd
ai yr. - ir-!�iDLII :! 19 iI;,Il$-Y VkLW VIIYI W It, I Fi�i'I T 'r
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JAIL 4 .Ox Wtske D
Alt. S 14-D4 Aeraobic
D Alt 6 Alk. Siabi W ionfl
Alt 7 - Stable) D
Alk, S - i%sishle [3
Alt. 9
Att. io all E3
INo vector a*acfim redw ion a
wnaiives were pafirmed E3
CLrRTIFICATION $TATEIVIENT fpiease check the appropriate statement)
"I cerdfy, nuder penalty of law, that the pathogen requhm a wts in 15A NCAC 02T .1106 and the
vector attraction reduction Ott in 15A NCAC 02T.1107 have ban =V
0 "1 rarlify, under penally of law, that the pathogen regain #In IMA NCAC 02T .1104 and tate
vector attraction reduction requirement in 15A NCAC 02T .1107 )rave not been met." {Please note if
you check this statement attach an explanation why you have not met one or both of the
rrquiremimb.) -
"This determination has been made under my dlratim and snpervidion irnaccordance with the sy staan
dedgned to ew are that qualbiied persound properly Sather and evah ate the information used to determine
that the cogen and vector attraction reduction requirements have been met, I am aware that there are
sipfficawt penaltk! for fate cerlMeaGen Weluding tine and int- ire ment."
Mr. 2M NAM WWI? ORC
Name and Tide (type or paint) Land Appluw Name and Title (if applicableXtype or print)
S'affim of Prleparrt* u _ Date S4pmd re of Land Applier (if applicable) Date
O epa= is defunct in 40 CFR )tart 503.9(r) and 15A NCAC 2T _ 1142 (26)
DENR FORM PVRF 02T (1 212006)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Rose Hill, Town of Beulaville, Town of Warsaw, and Southwest Plantation meet
pathogen reduction and vector attraction reduction requirements through lime stabilization. The
Town of Wallace met pathogen reduction through fecal density and vector attraction reduction
through injection or incorporation.
Documentation of these activities are found in the following section.

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pH 0.00 - uauAll pH yrkret do* hm mefrs erepNhar oorneW.
p1{.,.wr+piir�wl Mr1r 6� impw�ura oorreoied
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score aoq mm` Lim StsbftofhiDoia tatim
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pt1 � ' aeerl pp1 +abs �rt haroe extern roeptreear ecnmyed
pH.sem pH mbar horn bare Mpffoov a mewd,
Ail kapuu==L4 aea io Cold",

Tr1ptes Farms HQO1116498
Southwest Plantation/Bear Trail Lime Stabilization Docomen lotion
F aciliy Nome � ... _ _ Mouth _ 018 --
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Appmd.re Use
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Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Mar -18
Environmental Chemists Inc
Lab #
7
Date Analyzed
Most Probable Number
per gram
Log
1
3/22/18
15,567
4.192
2
3/22/18
53,141
4.725
3
3/22/18
16,418
4.215
4
3/22/18
83,334
4.921
5
3/22/18
72,626
4.861
6
3/22/18
62,201
4.794
7
3/22/18
38,350
4.584
Total 32.292
Averagel 4.613
Most Probable Number / Gram 1 41,040 IFecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

r7 --"qql Environmental Chemists, Inc.
einvirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Pax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@,environmentalchcmists.cnm
Branch Residuals/Bob Branch Date of Report: Apr 12, 2018
Customer PO 0:
Customer ID: 15080009
Attention: Report 0: 2018-04464
Project 1D: Wallace WWTP
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 64600 mg/kg 03/22/2018
Total Phosphorus SM 4600 P F 30500 mglkg 03/28/2018
Mercury Sw848 7471B 1.50 mglkg 03/23/2018
TCLP Metals
Arsenic
EPA 200.7
0.0 mglL
03/31/2018
Barium
EPA 200.7
<1.0 mg/L
03/31/2018
Cadmium
EPA 200.7
<1.0 mg/L
03131/2018
Chromium
EPA 200.7
<1.0 mglL
03/31/2018
Lead
EPA 200.7
<1.0 mg1L
03131/2018
Selenium
EPA 200.7
<1.0 mg1L
03/31/2018
Silver
EPA 200.7
<1.0mgI1-
03/31/2018
Mercury
EPA 246.1
X0.0020 mg/L
04/03/201 B
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
18-11082 She:1
3121/2018 10:35 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2-12% 03/22/2018
Fecal Density SM 9221C E MPN 24 hr 503 15567 MPN1g 03/22/2018
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
18-11083 Site: 2 3/21/2018 10:38 AM Water Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (°10) SM 2540 B 2.07% 03/22/2018
Fecal Density SM 82210 E MPN 24 hr 503 53141 MPN/g 03/2212018
Lab ID Sample ID: Collect DateMme Matrix Sampled by
18-11084 Site: 3 3/21/2018 10:42 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.01% 03/22/2018
16418 MPNIg 03/22/2018
Report #:: 2018-04464 Pape 3 of 4

PP007 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowserknvn Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch Date of Report: Apr 12, 2018
Customer PO 0:
Customer ID: 15060009
Attention: Report #: 2018-04464
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-11085 Site: 4 3/21/2018 10:45 AM Water Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2.04% 03/22/2018
Fecal Density SM 92210 E MPN 24 hr 503 83334 MPN/g 03/22/2018
Lab ID Sample ID: Collect Datelrime Matrix Sampled by
18-11086 Site: 5 3/21/2018 10:48 AM Water Bradley Vann/Brent Dean
Test
Method
Results Date Analyzed
Total Solids (%) SM 2640 a 1.79% 03/22/2018
Fecal Density 5M 9221C E MPN 24 hr 508 72626 MPN/g 03/22/2018
Lab ID Sample ID: Collect DateMme Matrix Sampled by
18-11087 Site: 8 3121/2018 10:52 AM Water Bradley Vann/Brent Dean
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
1811088 Site:7
Method
SM 2540 9
SM 9221 C E MPN 24 hr 508
Results Date Analyzed
2.09% 03/22/2018
62201 MPN/g 03/22/2018
Collect Date/Time Matrix Sampled by
3/2112018 10:55 AM Water Bradley Vann/Brent Dean
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 8
SM 9221C E MPN 24 hr 503
2.06% 03/22/2018
38350 MPN/g 03/22/2018
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: _ PAkL0 Qz (NQ&
Report AV: 2018-04484 Page 4 of 4

Win
Way
NC
05
ngton
ENVIRONMENTAL CHEMISTS, INC �CE:9mI192410311FAtX910 *244 4
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDK"S: DLS CERTIFICATION # 37729 Info®environmentalchemists.00m
CInLLFCTIDN AND CHAIN OF CUSTODY
Client: Branch Residuala/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: f
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT TO:
PHONEIFAX: 284.7969 284.5073
COPY TO: Anthony Colon, Public Works
email: bdean@townofwallacecom
Samnled Rw 17,21r, RZ, i- &W A." SAMPLE TYPE: I = Influerrt. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other:
Sample Identification
Collection
CL
c
oa
I
o
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
'
C Pl�Sludge
��0
X
nutrientstmetals
3 -;J -/:?loss'
G G
1
X
fecal dens! / %TS
3-.21-19
G G
2
C P
1��$3
X
fecal densit I %TS
TV -1V jolt
G G
3
C P
11
1
1 X
feel densay/ %TS
"I -1s'? rp 3
G G
4
C P
•
o%�
X
fecal density/ %TS
3 -11 -Ig f ods
G G
5
C P
OIL'
I
X
I
fecal density/ %TS
3 -m- t? ImIr
G G
6)
C P
tail
X
fecal densi 1 %TS
(00
G G
7)
C P
X
fecal density/ °kTS
G G
C P
G G
Transfer Relinquished By. Dateliime Recgved By: Datamme
1. -ZZ 1330
2.
Temperature when Received: `'L V Accepted: V mejeema: mesampte nequenew
Delivered By: Received By: Date: '_3-Z'( Time: 1,54-9
Comments: TURNAROUND:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
May -18
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
5/10/18
12,644
4.102
2
5/10/18
4,075
3.610
3
5/10/18
8,551
3.932
4
5/10/18
4,167
3.620
5
5/10/18
5,344
3.728
6
5/10/18
12,453
4.095
7
5/10/18
1,661
3.220
Total 26.307
Averagel 3.758
Most Probable Number / Gram 1 5,731 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Environmental Chemists, Ince
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Dowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL_ & CONSULTING CHEMISTS iniaQenvironmentalchemists.com
Branch ResiduaWBob Branch Date of Report: Jun 13, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2018-07366
Project ID: Wallace WWTP
Lab ID Sample 1D: Collect Datefrime Matrix Sampled by
18-18344 Site:1 5/9/2018 10:02 AM Solid/Sludge Ralph Ezelle/Bradley Vann
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.61% 05/1012018
Fecal Density SM 9221C E MPN 24 hr 503 12644 MP Wg 05/1012018
Lab ID Sample ID: Collect DateMme Matrix Sampled by
18-18345 Site: 2 5/9/2016 10:04 AM Solid/Sludge Ralph Ezelle/Bradley Vann
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.70% 05/1012018
Fecal Density SM MI C E MPN 24 ttr 503 4075 MPN/g 05/1012018
Lab ID Sample ID: Collect Datefl'ime Matrix Sampled by
18-18346 Site: 3 519!2018 10:06 AM Solid/Sludge Ralph Ezelle/Bradiey Vann
Test Method Results Date Analyzed
Total Solids (%) SM 2W a 2.69% 05/10/2018
Fecal Density SM 9221C E MPN 24 hr 503 8551 MPWg 05/10/2018
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-18347 Site: 4 5/9/2018 10:08 AM Solid/Sludge Ralph Ezelle/Bradley Vann
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2,64% 05/1=018
Fecal Density SM 9221C E MPN 24 hr 503 4167 MPN/g 05/10/2018
Lab ID Sample ID: Collect Dateffime Matrix Sampled by
18-18348 Site: 5 5/9/2018 10:10 AM Solid/Sludge Ralph EzellelBradley Vann
Teat Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2640 G
SM 922tC E MPN 24 hr 503
2.62%
5344 MPNIg
05/10/2018
05/10/2018
Report#:: 2018-07396 Pop$ 2 of 3

41wel
ANALYTICAL & CONSULTING CHEMISTS
Branch Residua"ob Branch
Attention:
Lab ID Sample ID. -
18 -18349
D:18-18349 Site:6
Test
Total Solids (%)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ` 2.52-473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
Method
SM 2wa G
[e-mail]
Date of Report: Jun 13, 2018
Customer PO 0:
Customer ID: 15060009
Report 9: 2018-07366
Project ID: Wallace WWfP
Collect DatelTime Matrix Sampled by
5/9/2018 10.12 AM Solid/Sludge Ralph Ezetle/Bradley Vann
Results Date Analyzed
2.66% 0511012018
Fecal Density SM 6221 C E MPN 24 hr 503 12453 MPNIg 05/10/2018
Lab ID Sample lD: Collect Daterrime Matrix Sampled by
18-18350 Slt ., 7
5/9/2018 10:14 AM Solid/Sludge Ralph Ezelle/Bradley Vann
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
2.71% 05/10/2018
Fecal Density SM 6221C E MPN 24 hr 503 1661 MPN/g 05/1012018
Comment: Results, except pH, reported on a dry weight basis. pH repoftd on an as received basis.
Reviewed by: dI"
Report #:: 2048-07366
Pane 3 f9.1

405
ENVIRONMENTAL CHEMISTS, INC i"� E:910�FAX910. 24
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION * 37729 infoeenvlronmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: Branch Residuak0ob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: 0'7
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT TO:
PHONEIFAX: 284.7969 284.5073
ANALYSIS REQUESTED
COPY TO: Anthony Colon, Public Works
remail: [e-mail]
Sampled 13v: _lem-► j, _ lA Ezzadl SAMPLE TYPE: I = Influent% E = Effluent, W = Well. ST = Stream. SO = Soil. SL = Sludge. Other.
Sample Identification
P
Collections
A
a
1 -01 d o
� U.S�
t
fi E
c CC
1 i
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
w
i
�
S
�
Sludge
C P
X
nutrients/metals
5,4--1ir IV&
G G
1
C P
X
fecal dens' / 4/aTS
5- 9- If 1"'_%
act
G G
2
C P
X
fecal densi / °/6TS
54-!$ J004
G G
3)
s- 9-I S J0040
C P
X
fecal density/ 0/6TS
G G
4
C P
X
fecal densi 1 %TS
6'-9L1g' levy
G G
5
C P
X
fecal density/ %TS
5-y-10 1 v;o
G G
6
C P
I
X
Ifecal density/ %TS
5- 9 -If 1011
G G
7
C P
X
fecal density/ %TS
5= 9 lb' O1'(
G G
C P
G G
Transfer Relinqul DataMme
Roc ed By. Datarrime
D.2ro
2.
Temperature when Received: Accepted: ejected: Resample Requested:
Delivered By: Received By: �-�' Date: 5 % Time:
Comments: TURNAROUND:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Sep -18
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
916118
4,468
3.650
2
9/6/18
12,456
4.095
3
916118
8,481
3.928
4
9/6/18
3,560
3.551
5
9/6/18
8,305
3.919
6
9/6118
6,116
3.786
7
9/6/18
5,924
3.773
Totall 26.704
Averagel 3.815
Most Probable Number / Gram 1 6,529 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Eenviroehem]n
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.022.3 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab / Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab /Fax
infoC4qenvirottnten ialchemists.com
Branch Residuals/Bob Branch Date of Report: Oct 16, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report M 2018-14714
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
18-37288 Site: # 1 9/5/2018 9:18 AM Solid/Sludge client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.91% 09/06/2018
Fecal Density SM 82210 E MPN 24 hr 503 4468 MPW9 09/06/2018
Lab ID Sample ID:
18-37289 Site: #2
Collect Date/Time. _ Matrix Sarnuled by _ _..
9/5/2018 9:20 AM Solid/Sludge client
Test Method Results Date Analyzed
Total Solids (010)
Fecal Density
Lab ID Sample 1D:
18-37290 Site: #3
$M 2540 G
SM 9221C E MPN 24 hr 503
2.81% 09/06/2018
12456 MPN/9 09/06/2018
Collect Date/Time Matrix Sampled by
9/5/2018 9:22 AM Solid/Sludge client
Test Method Results Date Analyzed
Total Solids (0%) SM 2540 G 2.83% 09/06/2018
Fecal Density SM 92210 E MPN 24 hr 503 8481 MPN/g 09/06/2018
Lab 1D. _ .._ _ _ _ Sample ID-:._.._.._-- - __ __ _ Collect Dat -49 1100- -- Matrix_. - ___ __ Sampled by. --.-
18-37291
y._._-
18-37291 Site: # 4 9/5/2018 9:24 AM Solid/Sludge client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 c
3.09%
09/06/2018
Fecal Density
5M 9221C E MPN 24 hr 503
3560 MPN/g
09/06/2018
Lab ID Sample 1D:
Collect Date/Time
Matrix Sampled by
18-37292 Site: # 5
9/5/2018 9:26 AM
Solid/Sludge client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.89%
09/06/2018
Fecal Density
SM 9221C E MPN 24 hr 649
8305 MPN/g.
0910 6120 1 8
Report #:: 2oia-14714 Page 2 of 3

lV'11i'11)
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392,4424 Pax
710 Bowsertown Road, Manteo, NC 27954 - 752.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Oct 16, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2018-14714
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-37293 Site: # 6 9/5/2018 9:28 AM Solid/Sludge client
Test Method Results Date Analyzed
Total Solids {%) SM 2540 c 2.78% 09106!2018
Fecal Density SM 92210 E MPN 24 hr 503 6116 MPN1g 09/06/2018
Lab ID Sample ID: Collect DatelTime_ Matrix____ _SarWed-by-
18-37294 Site: # 7 9/5/2018 9:30 AM Solid/Sludge client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 c 2.87% 09/06/2018
Fecal Density SM 9221C E MPN 24 hr 503 5924 MPNIg 09/06/2018
Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by:
Report Ar:: 2018-14714 Page 3 o13

25405
dmbi�
ENVIRONMENTAL CHEMISTS, INC OFFICE6602 :
2-=FAiXngton910.39ay Wi, 4424
Malytical &Consulting Chemists NCDENR: DWQ CERTIFIPATION # 94 NCDHHS: OLS CERTIFICATION #37729 ; InfolanvironmentalehamleMcom
COLLECTION AND CHAIN OF CUSTODY
Client: Branch ResidualsBob Branch
PROJECTINAME: Sludge -Wallace WWTP
REPORT NO.-
O:ADDRESS:
ADDRESS:CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT 10:
PHONE/FAX, 284.7969 284.5073
ANALYSIS REOUEST•ED
COPY TO: jAnthony Colon, Public Works
email: bdeanOtownofwailace.com
SamDled Bv: v d- WAIA Azze It S PLE TYPE: I = Influent. E = Effluent. W = Wells ST = Stream. SO = Soil. SL = Sludae. Other -
Coll on
ther:
Sample Identificationw
Collection
m
o
Y
g
g In
PRESERVATION
ANALYSIS REOUEST•ED
Date Time
Tem
2
x
=
W
c
Sludge
P
; �"
X
1
nutrients/metals
9-5-11 'D919.
(U G
P
3
X
fecal densi / %TS
-S-tB 091.9
G
2)
P
j
X
fecal densit
G
3}
P
L
a
X
Ifecal densi / 96TS
G
4)
P
X
fecal densit l %TS
09.{
G
P
�L
X
fecal density[ °�T5
-5-18 o ;49
G
P
3
'
X
I
Ifecal densit ! °kTS
G Gari
7
C P
SW
X
fecal densit /°1°TS
9- 09
G G�
P
CG
G
i
Transfer Relinquished BY: Datelf ime RAceived By: DateMme
2.
I emperature wnen maceiveq: Accepted: ✓" acted: Resample R ed:
Delivered By: __�Recelve�d BY: Date: Time:
Comments: 1 j TU AROUND: '

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Oct -18
Fnvironmental Chemists. Inc
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
10/19/18
69
1.839
2
10/19/18
70
1.845
3
10/19/18
63
1.799,
4
10/19/18
66
1.820
5
10/19/18
66
1.820
6
10/19/18
65
1.813
7
10/19/18
68
1.833
Totall 12.768
Averagel 1.824
Most Probable Number / Gram 1 67 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

4 0 106
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 91.0.392.4424 Fax
710 Rowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info Tivironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Nov 17, 2018
Customer PO #:
Customer ID: 15060009
Attention: Report M 2018-17185
Project ID: Wallace WWTP
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
18-43410 Site: # 1 10/18/2018 11:10 AM Solid/Sludge Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Total Solids {%)
SM 2540 G
2.61%
10/22/2018
Fecal Density
SM 9221C P MPN 24 hr 509
<69 MPN/g 10/19/2018
Lab ID Sample ID
Collect Datefrime
Matrix
Sampled by
18-43411 Site: # 2
10/18/2018 11:11 AM
Solid/Sludge
Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 c
2.59%
10/22/2018
Fecal Density
SM 9221c E MPN 24 hr 5D3
<70 MPN/g 10/19/2018
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
18-43412 Site: # 3
10/18/2018 11:12 AM
Solid/Sludge
Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.89%
10/2=018
Fecal Density
SM 92210 E MPN V hr 5D3
<63 MPN1g 10/1912018
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
18-43413 Site: # 4
10/18/2018 11:13 AM
Solid/Sludge
Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.73%
1 012212 0 1 8
Fecal Density
SM 9221C E MPN 24 hr 503
<66 MPN/g 10/19/2018
Lab ID Sample ID:
Collect Date/Time
Matrix
Sampled by
18-43414 Site: # 5
10/18/2018 11:14 AM
Solid/Sludge
Bradley Vann/Brent Dean
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.74%
10/22/2018
Fecal Density
SM 9221C E MPN 24 hr 603
<66 MPN/g 10/1912018
Report 11:: 201 B-17185 Page 2 of 3

Lx�v ro h ni
ANALYTICAL a CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Dowsertown Road, Mantec, NC 27954 • 252A73.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28544 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 17, 2018
Customer PO #:
Customer ID: 15060009
Report #: 2018-17185
Project ID: Wallace WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
18.43415 Site: # 6
10/18/2018 11:15 AM Solid/Sludge Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
2.78% 10122/2018
Fecal Density SM 92210 E MPN 24 hr 503 <65 MPN/g 10/19/2018
Lab^iD Sample ID Collect Date/Time Matrix Sampled by
18-43416 Site: # 7 10/18/2018 11:16 AM Solid/Sludge Bradley VannlBrent Dean
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
2.66% 10/22/2018
Fecal Density SM 92210 E MPN 24 hr 503 <68 MPN1g 1011912018
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: ' -Ick-
Report #:: 2018-17185 Page 3 013

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS,. INC
NCDENR: DWQ CEFMFICATION # 94 NCDHHS: OLS CERTIFICATION #.37M
COLLECTION AND CHAIN OF CUSTODY
6602 Windml11 Way Wilmington, NC 28405
OFFICE: 910-0223 FAX [phone]
info®environmentaichemiats.com
SSC. / -q-12r
Client: Branch Residuals/Bob Branch
PROJE NAME: Slud e-Walinoe WWTP
REPORT NO:
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
PRESERVATION
REPORT TO:
PHONEIFAX: 284.7969 284.5073
ANALYSIS REQUESTED
COPY T15: AnthonyColon, Public Works
email: [e-mail]
Sameled Rv: .v .." , kAMPLE TYPE: I = Influent. E i Effluent Wim Well. ST = Stream. SO = Soil. SL = Sluclue. Other:
Sample Identiflcation
Collectionm
E
n
o f os
v
n
m$
s
PRESERVATION
ANALYSIS REQUESTED
Date Time
Tem
g
120
Sludge
C P
fV
X
nutrients/metals
4t4r
G G
7
D -i -,S 1110
C P
a !0
X
fecal dens! /°/6TS
44&-6
I G G
2)
Jp-I JJ
C P
�
X
fecal dens' I %TS
G G
3)
Jl
C P
Z
X
fecal density/ %TS
+��'
G G
4)
C P
X
fecal density/ 9/oTS
G G
5)
C
X
fecal densit I %TS
y
G G
6
16-(J,4jr 11 1r
C P
Z
X
fecal density/ %TS
G G
7)
10 .
C P
t
X
fecal dens! / %TS
!G G
C P
G G
Transfer RellnquisW By. Daterrime ived By: Datemme
t. 0
2.
Temperature when
Delivered By: Received
Comments:
—d9

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SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Rose Hill, the Town of Beulaville, the Town of Warsaw and Southwest Plantation met
pathogen reduction and vector attraction reduction requirements through lime stabilization. The soil
pH will continue to be raised through the continued application of lime stabilized biosolids to these
application fields.

WrowgV06 By
Grower: Triple S Farms
Farm: Triple 5 Farm
Area: 115.8 acres
Sampling Overview
Master Soil Book
2018
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy 11/09/18 09:07 AM
Beulaville, NC 28518
910-298-3660

®r."I POWArto MY
Grnwpr: Triple S Farms Farm: Triple S Farm
Sample ID Map Book
Farm Sample ID Map
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy 11/09/18 09:03 AM
Beulaville, NC 28518
910-298-3660

'Location .:Grower farm .,Field Area
Dixie Chemical - Beulaville Triple S Farms Triple 5 Farm Field 1 32.85 acres
Master Soil Book
iCentrold
34.908716, -78.012548
Min Max:
Ca
591
5093
R
0.69
3.5
Fe
648
804
P1
45.0
611
10
13.0
32.0
51
27.0
71.0
Cui
68.0
1199
MnI
25.0
910
Zn1
122
3097
pH
4.5
63
bpH
7.0
7.8
CEC
4.2
14.6
%K
0,53
3.1
%Mg
4.5
9.4
%ca
351
89.3
%H
4.2
52.4
AC
0.68
4.3
HM
0.27
2.9
Avg
3271
2.1
720
371
19.9
44.5
755
61.6
1559
5.7
7.6
10.4
1.1
6.2
74.9
17.8
115
0.89
Sample Date: 2018-11-06
Soil Lab: Waters NCDA
a
:B
'Mn(
CEC
'%K
Mg
:%Ca
%H
ID
)bs/ac
- lbs/ac
PI
lbs/ac
K11
;SI
;Cul
Znl
pH
bpH
:%
-
:meq
- --
-%
1
591
0.69
736
45.0
25.0
27.0
68.0
25.0
122
4.9
7.5
4.2
3.1
9.4
35.1
52.4
2.2
1.7
2
3233
13
724
276
17.0
43.0
757
50.0
1079
5.9
7.8
9.7
0.90
55
83.3
10.3
1.0
0.51
3
4138
2.1
695
411
16.0
49.0
1084
62.0
2502
6.0
7.8
12.2
0.69
6.3
84.8
8. 2
1.1
0.50
4
4939
3.0
709
498
15.0
71.0
1052
56.0
1596
6.2
7.7
14.6
0.53
5.3
84.6
9.6
1.3
0.46
5
1557
1.2
648
154
23.0
39.0
343
53.0
601
4.5
7.0
8.8
1.3
8.4
44.5
45.7
4.3
2.9
6
2179
1.1
786
287
17.0
33.0
558
59,0
883
5.5
7-13
6.9
1.3
5.9
78.5
14.4
1.1
0.63
7
2302
2.1
804
312
13.0
37.0
616
56.0
1001
5.5
7.6
7.8
0.84
4.5
74.1
20.6
1.6
1.0
a
3441
2.5
777
397
32.0
66.0
768
65.0
1331
5.9
7.7
10.8
1.5
5.5
80.0
13.0
1.4
0.54
9
4460
3.0
719
577
21.0
47.0
1005
81.0
2434
6.0
7.7
13.2
0.84
5.4
84.6
9.1
1.1
0.27
10
5093
3.5
665
611
20.0
44.0
1199
78.0
3097
6.3
7.8
14.3
0.71
5.8
89.3
4.2
0.68
0.39
11
4050
3,0
659
512
20.0
34.0
850
93.0
2500
6.2
7.8
12,0
0.86
6.1
84.7
8.4
1.1
0.89
Dixie Chemical - Beulaville
1060 S. NC 41 & III Hwy 11/09/18 09:07 AM
Beulaville, NC 28518
910-298-3660

Powatrm Ay '� w•y
Location ;Grower 'Farm
Dixie Chemical - Beulaville Triple 5 Farms Triple S Farm
Master Soil Book
Field Area
',Centroid
Field 2 9.06 acres
34.912564, -78.013934
Min Max
Avg
Ca
2298 3293
2777
B
1.9 2.6
2.2
Fe
B49 865
858
PI
221 300
246
K1
12.0 21.0
15.4
51
37.0 58.0
43.8
Cul
563 604
583
Mnl
37.0 68.0
46.2
Znl
6B7 1083
881
pH
5.8 6.0
5.9
bpH
7.5 7.8
7.7
CEC
6.8 10.7
8.9
%K
0.59 1.2
0.91
%Mg
4.7 7,5
6.0
%Ca
76.7 B4.1
78.6
%H
8.8 16.9
14.6
AC
0.68 1.8
1.4
HM
0.35 0.68
0.51
Sample Date: 2018-11-06
Soil Lab: Waters NCDA
Ifl
Ea
s
;fie
P1
$1
:Cul
°MnI
Znl
pH
tpldl
CES
-4alF
s
96Mg
'%Ca
%H
AC
HM
d%
lbs/ac
-Ibslae
;lbslae
:..
,IFI
;_ .
meq+meq.
12
2997
2.6
849
300
21.0
37.0
604
68.0
1083
6.0
7.7
9.7
1.1
7.5
77.0
14.4
1.4
0.46
13
2684
2.2
865
240
16.0
42.0
584
43.0
1075
5.8
7.7
8.8
0.97
6.4
76.7
16.0
1.4
0.68
14
2298
1.9
854
230
16.0
39.0
563
46.0
792
6.0
7.8
6.8
1.2
6.0
84.1
8.8
0.68
0.35
15
2611
2.1
859
221
12.0
43.0
573
37.0
687
5.9
7.7
8.4
0.73
4.7
77.8
16.7
1.5
0.44
16
3293
2.3
865
239
12.0
58.0
593
37.0
767
5.9
7.5
10.7
0.59
5.2
77.3
16.9
1.8
0.65
Dixie Chemical - Beulavilie
1060 S. NC 41 & 111 Hwy 11/09/18 09:07 AM
Beulaville, NC 28518
910-298-3660

IM
revel*$ B9
iocation [Grower Farm field ;Area
Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 4 5.49 acres
Ca
B
Fe
PI
KI
SI
Cul
Mni
Znl
pH
bpH
CEC
%K
%Mg
%Ca
%H
AC
HM
Master Soil Book
,Centroid
34.913876,-78.019044
Min PSa
681
1116
0.61
1.1
501
872
83.0
102
84.0
149
21.0
31.0
97.0
173
21.0
25.0
142
293
5.9
6.0
7.3
7.8
3.4
6.8
11.0
12.7
10.2
12.9
40.8
50.6
23.8
38.0
0.76
2.6
0.49
0.90
Avg
898
0.84
686
92.5
116
26.0
135
23.0
218
6.0
7.6
5.1
11.8
11.6
45.7
30.9
1.7
0.69
Sample Date: 2018-11-06
Soil Lab: Waters NCDA
a a
C@G
%nK `%Mg' %C.a '/6H
AC
HM
�f
,IQdbs/ac. 16slae Pbsfac-......T..
,cul Mnl 7nl
� E
I>pK
meq
4/p ° % t %
`meq
24 1116 1.1 872
102 149
31.0
173 25.0 293
5.9
7.3 6.8
.
11.0 10.2 40.8 38.0
2.6
0.90
25 681 0.61 '501
83.0 84.0
21,0
97.0 21.0 142
6.0
7.8 3.4
12.7 12.9 SO 6 23 S
U.16
0.49
Dixie Chemical - Beulaville
1060 S. NC 41 6111 Hwy 11/09/18 09:07 AM
Beulaville, NC 28518
910-298-3660

4P ahAO0
POWOTCd NY
lvOrafiOn ;Grower Farm Field .:Area
Dixce ChernIcal - Beulaville Triple S Farms Triple S Farm Field 5 13.56 acres
Ca
B
Fe
PI
Ki
51
Cul
Mnl
Zni
pH
bpH
CEC
%K
%Mg
%Ca
%H
AC
HM
Master Soil Book
Centroid.��
Soil Lab: Waters NCDA
34.91382, -78.016318
Mine
["i` r
Avg'.
2038
6)L
2501
1.2
2.3
1.7
749
839
802
188
282
216
21.0
48,0
36.2
40.0
50.0
44.4
300
515
396
34.0
46.0
37.0
502
1031
779
5.6
5.9
5.7
7.6
7.8
7.7
6.6
10.6
8.6
1.3
2.5
2.1
6,7
8.2
7.2
74.3
75.9
75.3
13.8
17.6
15.3
1.0
1.6
1.3
0.61
1.2
0.79
Sample Date: 2018-11-06
Soil Lab: Waters NCDA
.1
'te
a
'E3
t
lel
!.w
V, nI
H
pH
-A
lC
°�Mg';
°�a d I
%Pf
C
SIM
ID
Jbs�acla
'bs�aeI
Eli
6___....
meq.
�o.
26
2622
1.2
. ;.
805
215
-.*
43.0
40.0
_
300
37.0
848
5.7
7.7
8.7 2.5
8.2
75.5
13.8
1.2
1.2
27
2756
1.7
749
206
39.0
47.0
359
46.0
502
5.9
7.7
9.1 2.2
7.0
15,5
15.3
1.4
0.64
28
3221
2.3
794
282
48.0
45.0
515
34.0
1031
5.9
7.6
10.6 2.3
6.7
75.9
15.1
1.6
0.77
29
.2366
1.8
839
.189
21.0
50.0
409
34.0
612
5.6
7.7
8.0 1.3
6.8
74.3
17.6
1.4
0.77
30
2038
1.8
825
188
30.0
40.0
398
34.0
904
5.6
7.8
6.8 2.3
7.5
75.5
14.8
1.0
0.61
Dixie Chemical - Beulaville
10605. NC 41&111 Hwy
Beulaville, NC 28518
910-298-3660
11/09/18 09:07 AM

Location Grower :'Farm field
Dixie Chemical - Beulaville Triple S Farms Triple S Farm Field 9
Area
12.38 acres
Sample Date: 20I8-11-06 Soil Lab: Waters NCDA
Ca
Fe
P1
KI
51
Cul
Mn1
Zn1
pH
bpH
CEC
%K
%Mg
%Ca
%H
AC
HM
Master Soil Book
;Centrold
34,904472,-78.010869
Nn
Max
1642
2093
0.84
I'l
512
691
153
237
135
187
28.0
32.0
224
314
31.0
53.0
IB4
258
519
6.2
7.5
7.8
7.0
8.8
U
11.6
110
17.8
50.9
59.1
14.2
24.6
0.92
2.0
0.82
1.1
Alig;.'-
1796
0.96
598
184
158
29.7
262
40.3
231
6.0
7.6
B.0
10.0
15.7
56.1
18.2
1.4
0.98
Dixie Chemical - Beulaville
1060 S. NC 41 & III Hwy 11/09118 09,07 AM
Beulaville, NC 28518
910-298-3660
Ca
B fe P1
'KI
51
11cut
Wl
2n)
0
pH
CEC
%K
9/,,Mg
%Ca
j%H
jAC " OM
:ID
bs/abs/ac
,lbs/air
J -lbs/ac
-meq
%
eq
1%
37
2093
0.96 591 163
153
28.0
224
37.0
184
6,2
7.7
8.8
8.7
16.3
59.1
15.8
1.3
1.1
38
1642
.1.1 691 153
135
29-0
314
31.0
252
6.0
7.8
7.0
9.6
17.8
58.3
14.2
'0.92
O.B2
39
1654
0.84 512 237
187
32.0
248
53.0
258
5.9
7.5
8.1
11,6
13.0
50.9
24.6
2.0
1.1
Dixie Chemical - Beulaville
1060 S. NC 41 & III Hwy 11/09118 09,07 AM
Beulaville, NC 28518
910-298-3660

2018 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2018 APPLICATION SUMMARY
Farmer
Tract
/Site
Field
Acres
Date
Spread
Gallons *
Dry Tons
/ Acre Dry Tons
Crop
Source
1119
PAN
(lbs/ac)
Eric Smith
1
1
34.2
Jan -18
85,000
0.14 4.89
Small Grain
Beulaville WWTP
67.22
Feb -18
12,600
0.03 1.16
Small Grain
Southwest Plantation
Mar -18
137,000
0.25 8.51
Small Grain
Warsaw WWTP
Mar -18
107,100
0.22 7.46
Small Grain
Wallace WWTP
May -18
90,000
0.15 5.18
Bermudagrass
Beulaville WWTP
May -18
12,727
0.03 1.17
Bermudagrass
Southwest Plantation
Jun -18
138,000
0.25 8.57
Bermudagrass
Warsaw WWTP
Aug -18
264,600
0.90 30.67
Bermudagrass
Wallace WWTP
Dec -18
59,400
0.18 6.27
Small Grain
Wallace WWTP
2
8.48
Jul -18
275,838
3.77 31.98
Bermudagrass
Wallace WWTP
110.16
4
4.14
Jun -18
36,000
1.10 4.56
Soybeans (Double Croppec
Rose Hill WWTP
33.35
5
11.2
Oct -18
12,600
0.10 1.16
Small Grain
Southwest Plantation
33.15
Oct -18
j 169,600
0.87 9.76
Small Grain
Beulaville WWTP
9
8.93
Mar -18
1 182,700
1.42 12.72
1 Millet
Wallace WWTP
59.42
Fields Applied to: 5 66.95
Total
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Town of Rose Hill
Southwest Plantation
Town of Wallace
Town of Warsaw
Gallons
1315831165
c
Metric
Dry Tons Tons
134.07 121.89
Permit Limit Dry Tons
NA
344,600
19.83 18.03
38
0
0.00 0.00
80
0
0.00 0.00
38
36,000
4.56 4.15
38
379927
3.50 3.18
5
889,638
89.10 81.00
330
2759000
17.09 15.53
38
Branch Residuals Soils, LLC Confidential 2/12/2019 Page 1

2018 APPLICATION CONDITION SUMMARIES

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Beulaville WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 1.38
Residual Report No.: B2018 1-18 Crop: Small Grain
Date
Field No. Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/24/18
1
42,000
Moist
Cool, Cloudy
0.00
1/25/18
1
43,000
Moist
Cool, Clear
0.00
Total Gallons
85,000

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Beulaville WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 1.38
Residual Report No.: B2018 1-18 Crop: Bermudagrass
Date
Field No. Subfield
Gallons
Soil Weather
Conditions Conditions
Prev. 24 Hour
Rainfall
5111118
1
90,000
Moist Hot, Clear
0.00
Total Gallons
90,000

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Beulaville WWTP
Farmer: Eric Smith Acres: 11.2
Site/Tract: 1 Application Method: Surface
Field: 5 Percent Solids: 1.38
Residual Report No.: B2018 1-18 Crop: Small Grain
Date
Wield No. Subfield Gallons
Soil
Conditions
Weather Prev. 24 Hour
Conditions Rainfall
10/31/18
5 75,600
Dry
Warm, Clear 0.00
1111118
5 94,000
Moist
Warm, Clear 0.00
Total Gallons
169,600

Triple S Farms
Rose Hill, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Rose Hill WWTP
Farmer: Eric Smith Acres: 4.14
Site/Tract: 1 Application Method: Surface
Field: 4 Percent Solids: 3.04
Residual Report No.: RH2O18 1-18 Crop: Soybeans (Double Cropped - Manured)
Date
Field No.
Subfield Gallons
Soil Weather
Conditions Conditions
Prev. 24 Hour
Rainfall
6/28/18
4
36,000
Moist Hot, Clear
0.00
Total Gallons
36,000

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Southwest Plantation
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 2.21
Residual Report No.: SWP 2018 1-18 Crop: Small Grain
Date Field No. Subfield Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
217118 1 12,600
Moist
Warm, Cloudy
0.21
Total Gallons 12,600

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Southwest Plantation
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 2.21
Residual Report No.: SWP 2018 1-18 Crop: sermudagrass
Date
Field No. Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5114118
1
12,727
Dry
Hot, Clear
0.00
Total Gallons
12,727

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Southwest Plantation
Farmer: Eric Smith Acres: 11.2
Site/Tract: 1 Application Method: Surface
Field: 5 Percent Solids: 2.21
Residual Report No.: SWP 2018 1-18 Crop: Small Grain
Date
Field No.
Subfield Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/17/18
5
12,600
Moist
Warm, Cloudy
0.00
Total Gallons
12,600

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2018
Wallace WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: injected
Field: 1 Percent Solids: 1.67
Residual Report No.: W1,2018 1-18 Crop: Small Grain
Date
3/5/18
Field No.
1
Subfield
Gallons
75,600
Soil
Conditions
Dry
Weather
Conditions
Warm, Clear
Prev. 24 Hour
Rainfall
0.00
3115/18
1
31,500
Moist
Warm, Clear
0.00
Total Gallons
107,100

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2018
Wallace WWTP
Farmer: Eric Smith Acres: 8.93
Site/Tract: 1 Application Method: Injected
Field: 9 Percent Solids: 1.67
Residual Report No.: WL2018 1-18 Crop: Millet
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/28/18
9
81,900
Dry
Warm, Clear
0.00
3129118
9
100,800
Dry
Warm, Clear
0.00
Total Gallons
182,700

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2018
Wallace WWTP
Farmer: Eric Smith Acres: 8.48
Site/Tract: 1 Application Method: Injected
Field: 2 Percent Solids: 2.78
Residual Report No.: WL2018 3-18 Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/12/18
2
98,420
Moist
Hot, Cloudy
0.00
7/13/18
2
92,780
Dry
Hot, Clear
0.00
7/15/18
2
72,120
Dry
Hot, Clear
0.00
7/16/18
2
12,518
Dry
Hot, Clear
0.00
Total Gallons
275,838

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2018
Wallace WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Injected
Field: 1 Percent Solids: 2.78
Residual Report No.: WL2018 3-18 Crop: Bennudagmss
Soil Weather Prev. 24 Hour
Date Field No. Subfield Gallons Conditions Conditions Rainfall
8/29/18
1
75,600
Dry
Hot, Clear
0,00
8/30/18
1
94,500
Dry
Hot, Clear
0.00
8/31/18
1
94,500
Dry
Hot, Clear
0.00
Total Gallons
264,600

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2018
Wallace WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Injected
Field: 1 Percent Solids: 2.53
Residual Report No.: WL2018 4-18 Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/6/18
1
54,000
Dry
Cool, Clear
0.00
1219/18
1
5,400
Dry
Cool, Clear
0.00
Total Gallons
59,400

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Warsaw WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 1.49
Residual Report No.: WR2018 1-18 Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/1/18
1
137,000
Moist
Cool, Clear
0.00
Total Gallons
137,000

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2018
Warsaw WWTP
Farmer: Eric Smith Acres: 34.2
Site/Tract: 1 Application Method: Surface
Field: 1 Percent Solids: 1.49
Residual Report No.: WR2018 1-18 Crop: Bmnudagrass
Date
Field No.
Subfield
Gallons Soil Weather
Conditions Conditions
Prev. 24 Hour
Rainfall
6/13/18
1
138,000 Moist Warm, Cloudy
0.01
Total Gallons
138,000