WQ0001026_Residual Annual Report 2018_20190301

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0001026
SUBMITTAL DATED: 2/25/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address* Phone Number*
[e-mail] 336-751-1441
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0001026
Reviewer*
Troy Doby
Permittee * Adam Waters
Facility Name * City of Washington
County* Beaufort
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Washington Annual Report - WQ0001026.pdf 2.88MB
Application Form Engineering Rans, Specifications, Calculations, Etc.)

For nein and modification permit applications, the paper copy is required to be subrrutted to the
Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic
applications have been received_ The paper copy shall include the follo-kAmig:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineenng plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Service:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigb_ NC 27699-1613
By CourieriSpecial Delivery:
Division of Water Resources- Non -Discharge Branch
Ag Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Raleigh,NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or
Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/25/2019

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026 County:
Facility Name (as shown on permit):
Land Application Operator:
Beaufort County, NC Year: 2018
City of Washington
EMA Resources Inc. Phone: _ 336-751-1441
Land application of residuals as allowed by the permit occurred during the past calendar year?
© Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annlication Summary!
Total number of application fields in the permit: 54
Total number of fields utilized for land application during the year: I
Total amount of dry tons applied during the year for all application sites: 108.93
Total number of acres utilizes for land application during the year: 65.5
rnit D - Hunua, v—umuiance matement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in ISA NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T, I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations." "� f
Adam Waters - Water Resources Superintendent w. -.G /2'Z
Permittee
Name and Title (type or. print) Signature of Permittee / Date
h.� Ze—' Z /22//S 2 e 4� — 2!5/2019
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual): 108.93
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series: GoA
65.5 Acres Permitted: 65.5 Site #:
BF210 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kp-, % Solids use Raw Percent #1:
. �•.
Com-
posite_
Date
..
2
3
141
1 51
1 61
1 71
1 81
L9J
110111
12
DT/Ac./
c
App'
Event
1.66
"
Arsenic
0.028
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Cadmiuml
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper 1
1.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.014
ChromiA
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Lead 1
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Nickel
0.055
Total Phos
phorusENEENEENEEN
-,M
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Selenium
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
141
1 51
1 61
1 71
1 81
L9J
110111
12
DT/Ac./
c
App'
Event
1.66
"
Arsenic
0.028
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Cadmiuml
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper 1
1.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.014
ChromiA
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Lead 1
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Nickel
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Selenium
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Zinc
1.949
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.949
L
98.782
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
98.782
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
ze- " 2/5/2019
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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Waypoiht
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 18-143-0200
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
is Yes
0 No
Number of coolers received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: randi Watson Date & Time: 5/23/2018 14:00:53
Page 5 of 6

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*ESC ANALYTICAL REPORT myESC
" May 03, 2018
EMA Resources
Sample Delivery Group:
Samples Received:
Project Number:
Description:
L988279
04/24/2018
Washington, NC
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: �✓
Cassandra Foster
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. When, applicable, sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.

TABLE OF CONTENTS ONE LAB, NATIONWIDE.
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
WASHINGTON WWTP L988279-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 82608
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
GI: Glossary of Terms
AL Accr i tatinon Lorations
Sc: Sample Chain of Custody
9
10
11
12
13
15
16
17
19
21
ACCOUNT: PROJECT: SDG: DATE[TIME: PAGE:
EMA Resources L988279 05/03/1815:02 2 of 21

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
WASHINGTON WWTP L988279-01 Waste
Collected by
Roy Whitaker
Collected date/time
04/23/1808:30
Received date/time
04/24/1808:45
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
!
Preparation by Method 1311
WG1102730
1 04/25/18 08:36
04/25/18 08:36
TM
Preparation by Method 1311
WG1102797
1 04/25/1813:13
04/25/1813:13
RT
Wet Chemistry by Method 9012 B
WG1103534
1 04/26/18 22:35
04/27/1810:08
KK
Wet Chemistry by Method 9034-90308
WG1103812
1 04/27/18 22:00
04/27/18 22:00
JLJ
Wet Chemistry by Method 9045D
WG1103282
1 04/26/1815:30
04/26/1817:00
ITB
a
Cn
Wet Chemistry by Method D93/1010A
WG1103090
1 04/26/1812:42
04/26/1812:42
TH
Mercury by Method 7470A
WG1103260
1 04/26/18 07:24
04/26/1810:58
ABL
Metals (ICP) by Method 6010D
WG1103269
1 04/26/18 07:51
04/26/1810:20
CCE
Sr
Volatile Organic Compounds (GC/MS) by Method 82608
WG1103327
1 04/26/1817:14
04/26/1817:14
RAS
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1104955
1 05/02/18 06:57
05/02/18 20:37
KLM
a
QC
Pesticides (GC) by Method 80818
WG1104746
1 04/29/18 22:37
05/01/1815:59
VKS
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
WG1104339
1 04/30/18 09:25
04/30/18 21:27
LA
AGI
9 —71
Sc
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L988279
05/03/1815:02
3 of 21

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within F -u----
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All radiochemical sample results for
solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet
weight was requested by the client. All Method and Batch Quality Control are within established RScriteria except where addressed in this case narrative, a non-conformance form or properly qualified
within the sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
El
RC
Cassandra Foster
Technical Service Representative
9Sc
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L988279 05J03/1815:02 4 of 21

WASHINGTON WWTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 04/23/18 08:30 L988279
Preparation by Method 1311
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
4/25/20181:13:21 PM
WG1102797
TCLP ZHE Extraction
4/25/2018 8:36:25 AM
WG1102730
Fluid 1
4/25/20181:13:21 PM
WG1102797
Initial pH 6.63
4/25/20181:13:21 PM
WG1102797
Final pH 4.72
4/25/20181:13:21 PM
WGI102797
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250
1
04/27/201810:08
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/kg
mg/kg
date /time
Reactive Sulfide 128
25.0
1
04/27/2018 22:00
Wet Chemistry by Method 9045D
Result Qualifier
Dilution
Analysis
Batch
Analyte su
date / time
Corrosivity by pH 6.92 T8
1
04/26/201817:00
Sample Narrative:
L988279-01 WGI103282: 6.92 at 21C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date/time
Ignitability DNI at 170
1
04/26/201812:42
Mercury by Method 7470A
Result Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date / time
Mercury ND
0.0100
0.20
1
04/26/201810:58
Metals (ICP) by Method 6010D
Result Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date / time
Arsenic ND
0.100
5
1
04/26/201810:20
Barium ND
0.100
100
1
04/26/201810:20
Cadmium ND
0.100
1
1
04/26/201810:20
Chromium ND
0.100
5
1
04/26/201810:20
Lead ND
0.100
5
1
04/26/201810:20
Selenium ND
0.100
1
1
04/26/201810:20
Silver ND
0.100
5
1
04/26/201810:20
Volatile Organic Compounds (GC/MS) by Method
8260B
Result Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date / time
Benzene ND
0.0500
0.50
1
04/26/201817:14
Carbon tetrachloride ND
0.0500
0.50
1
04/26/201817:14
Chlorobenzene ND
0.0500
100
1
04/26/201817:14
Chloroform ND
0.250
6
1
04/26/201817:14
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L988279 05/03/1815:02 5 of 21
e
Sc

WASHINGTON WWTP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE
Collected date/time: 04/23/18 08:30 L988279
Volatile Organic Compounds (GC/MS) by Method 8260B
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte
mg/I
mg/I
mg/I
date / time
1,2-Dichloroethane
ND
0.0500
0.50
1 04/26/201817:14
1,1-Dichloroethene
ND
0.0500
0.70
1 04/26/201817:14
2-Butanone (MEK)
ND
0.500
200
1 04/26/201817:14
Tetrachloroethene
ND
0.0500
0.70
1 04/26/201817:14
Trichloroethene
ND
0.0500
0.50
1 04/26/201817:14
Vinyl chloride
ND
0.0500
0.20
1 04/26/201817:14
(S) Toluene -d8
109
80.0-120
120
04126/20181794
(S) Dibromofluoromethone
102
76.0-123
123
04/26/201817.•14
(S)a,o,o-Trifluorotoluene
99.0
80.0-120
120
04/26/20181714
(S) 4-Bromofluorobenzene
100
80.0-120
120
041261201817.14
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Analyte
Chlordane
Endrin
Heptachlor
Lindane
Methoxychlor
Toxaphene
(S) Decochlorobiphenyl
(S) Tetrachloro-m-xylene
Result
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5 -TP ISilvex)
ND
0.00200
1
1 05/02/2018 20:37
2,4-D
ND
0.00200
10
1 05/02/2018 20:37
(S) 2,4-Dichlorophenyl Acetic Acid
119
14.0-158
158
0510212018 20.37
Pesticides (GC) by Method 8081B
Analyte
Chlordane
Endrin
Heptachlor
Lindane
Methoxychlor
Toxaphene
(S) Decochlorobiphenyl
(S) Tetrachloro-m-xylene
Result
Qualifier RDL
Limit
mg/I
mg/I
mg/I
ND
0.00500
0.03
ND
0.00500
0.02
ND
0.00500
0.0080
ND
0.00500
0.40
ND
0.00500
10
ND
0.0100
0.50
70.0
10.0-144
144
72.8
10.0-135
135
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Dilution Analysis Batch
date / time
1 05/01/201815:59
1 05/01/201815:59
1 05/01/201815:59
1 05/01/201815:59
1 05/01/201815:59
1 05/01/201815:59 4I
05/01/201815:59
0510112018 15:59
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L988279 05/03/1815:02 6 of 21
Fc
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte
mg/I
mg/I
mg/I
date / time
1,4 -Dichlorobenzene
ND
0.100
7.50
1 04/30/2018 21:27
2,4-Dinitrotoluene
ND
0.100
0.13
1 04/30/2018 21:27
Hexachlorobenzene
ND
0.100
0.13
1 04/30/2018 21:27
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 04/30/2018 21:27
Hexachloroethane
ND
0.100
3
1 04/30/2018 21:27
Nitrobenzene
ND
0.100
2
1 04/30/2018 21:27
Pyridine
ND
0.100
5
1 04/30/2018 21:27
3&4 -Methyl Phenol
ND
J3 0.100
400
1 04/30/2018 21:27
2-Methylphenol
ND
J3 0.100
200
1 04/30/2018 21:27
Pentachlorophenol
ND
0.100
100
1 04/30/2018 21:27 (
2,4,5 -Trichlorophenol
ND
0.100
400
1 04/30/2018 21:27
2,4,6 -Trichlorophenol
ND
0.100
2
1 04/30/2018 21:27
(S) 2-Fluorophenol
49.9
10.0-120
120
04/30/2018 21:27-
(S) Phenol -d5
35.4
10.0-120
120
04/30/2018 21.27
(S) Nitrobenzene -d5
61.8
10.0-126
126
0413012018 2127
(S) 2-Fluorobiphenyl
70.7
22.0-127
127
0413012018 2127
(S) 2,4,6-Tribromophenol
83.6
10.0-153
153
0413012018 21.•27
(S)p-Terphenyi-dM
80.2
29.0-141
141
04130120182127
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L988279 05/03/1815:02 6 of 21
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GLOSSARY OF TERMS ONE LAB. NATIONWIDE 40
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
s
Ss
RDL
Reported Detection Limit.
Rec.
Recovery.
1174
RPD
Relative Percent Difference.
Cn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Fr
S
OY
Matrix Spike/Duplicate; used to evaluate anal tical efficienc b measurin recove Surro ates are not ex ected to be
Y Y 9 ry• 9 P
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
F
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
,..._ .._."'
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
e
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
SC
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L988279 05/03/1815:02 19 of 21

ACCREDITATIONS & LOCATIONS ONE LAE. NATIONWIDE.
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab
r
is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences.
Alabama 40660
Nebraska
NE -OS -15-05
SS
Alaska 17-026
Nevada
TN -03-2002-34
Arizona AZO612
Arkansas 88-0469
New Hampshire
New Jersey—NELAP
2975
TN002
Fnj
California 2932
New Mexico'
n/a
ND
Colorado TNO0003
Connecticut PH -0197
New York
North Carolina
11742
Env375
J r
Florida E87487
North Carolina'
DW21704
Georgia NELAP
Georgia' 923
North Carolina'
North Dakota
41
R-140
1QC1
Idaho TNO0003
Ohio—VAP
CL0069
Illinois 200008
Indiana C -TN -01
Oklahoma
Oregon
9915
TN200002
G
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Kentucky' a 90010
Rhode Island
South Carolina
LA000356
84004
a
Kentucky16
South Dakota
n/a
r
Louisiana A130792
Louisiana' LA180010
Tennessee"
Texas
2006
T 104704245-17-14
9
S C
Maine TN0002
Texas'
LA80152
— '� � RA
Maryland 324
Utah
TN00003
Massachusetts M-TN003
Vermont
VT2006
Michigan 9958
Virginia
460132
r T
Minnesota 047-999-395
Washington
C847
Mississippi TNO0003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2LA
CA \
\ �_..._..._
A2LA — ISO 17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2LA — ISO 17025' 1461.02
DOD
1461.01
r,
ICY
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ' Chemical/Microbiological 'Mold 'Wastewater
n/a Accreditation not applicable
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
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ACCOUNT:
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SDG:
DATE/TIME: PAGE:
EMA Resources
L988279 05/03/1815:02 20 of 21

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 1/1/2018 To 12/31/2018
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment)❑ 1 Alt. C (Prior Testing)"FJ
Alt.D (No Prior Test) LlProcess to Further Reduce Pathogeng
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Therinophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1) Fecal Density 21 Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Com )ostia ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑ `
. .... .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
umer oFrequency
Excee-
dente
of Analysis
Sample
Type
Analytical
Tech-nique
inimU
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
15464
26840
44828
MPN/g
0
Quarterly
G
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
vector Attracuon xceuuction ki:)A i-iuAu uz i .tiu-i) - riease tnutcate alternative pertormea:
Alt.I (VS reduction) Rl JAIt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) R1 jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) El Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ElAit. 10 (Incorporation) [3No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
R1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
A.,� 2/11/A
Signature of Preparer* Date
Brent Collins; Director of Technical Services
Land Applier Name and Title(if(if applicable)(type or print)
Z 4� 2/5/2019
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 419/2018
Location #
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
27272.7
23367.7
31724.1
15463.9
26896.6
Log
4.4357
4.3686
4.5014
4.1893
4.4297
26621.2 4.4252
44827.6 4.6515
Geometric Means/g
Total Dry Solids
A&ri-) �,
Signature

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January 2018 Average
AVG.
2018 Average
R.S. 1 & 2 R.S. 3 R.S. 4
74.97% 75.76% 75.51%
75.41%
1st Quarter
VS in
0.7239
February 2018 Average
VS out
0.6122
R.S. 1 & 2 1 R.S. 3 R.S. 4
VSFR=
0.3979
74.91% 1 75.23% 1 74.84%
74.99%
March 2018 Average
2nd Quarter
R.S. 1 & 2 R.S. 3 R.S. 4
VS in
0.7239
75.27% 75.58% 1 77.40%
76.08%
VS out
0.6122
VSFR=
0.3979
April 2018 Average
PR.S. 1 & 2 R.S. 3 R.S. 4
74.59% 75.10% 1 74.86%
74.85%
3rd Quarter
VS in
0.7239
May 2018 Average
VS out
0.6122
R.S. 1 & 2 R.S. 3 R.S. 4
VSFR=
0.3979
73.10% 73.91% 73.14%
73.38%
June 2018 Average
4th Quarter
PR.S. 1 & 2 R.S. 3 R.S. 4
1
VS in
0.7239
70.48% 71.63% 1 70.01%
70.71%
VS out
0.6122
VSFR=
0.3979
July 2018 Average
PR.S. 1 & 2 R.S. 3 R.S. 4
67.51% 68.20% 70.79%
68.83%
August 2018 Average
R.S. 1 & 2 R.S. 3 R.S. 4
67.91% 69.58% 69.94%
69.14%
September 2018 Average
E6R.S. 1 & 2 R.S. 3 R.S. 4
66.91% 1 68.09% 1 72.21% 69.07%
October 2018 Average
R.S. 1 & 21 R.S. 3 R.S. 4
67.00% 1 69.54% 69.11% 68.55%
November 2018 Average
PR.S. 1 & 2 R.S. 3 R.S. 4
70.32% 75.00% 71.69% 72.34%
December 2018 Average
R.S. 1 & 2 1 R.S. 3 R.S. 4
72.54% 1 75.66% 1 77.86% 75.35%
72.39%

EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
Reported:
For:
Comments:
Analytical Results
11/02/2018
1210712018
WASHINGTON
ANALY TiCAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
181102-16-01 30 Day Benchscale Washington <1 % EPA625-R-92/0 11/02/2018 WC
WWTP
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Analytical Results
EMA Resources, Inc.
Mocksville, NC 27028
Sample ID: 181102-16-01
For: Washington WWTP
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
Week 1 2.31 1.07 0.4625
Week 2 2.05 0.97 0.4748
Week 3 1.86 0.86 0.4613
Week 4 1.79 0.83 0.4619
Week 5 1.55 0.75 0.4849
Volatile Solids Reduction: 0.4625- 0.4849x 100 =<l%
0.4625 - (0.4625 X 0.4849)
Respectfully submitted,
Dena Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
DW Cert. #37755

Condition of Receipt
Sample Number 181102-16-01 Temp on Arrival: 3.3
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

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