WQ0011448_Residual Annual Report 2018_20190227

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0011448
SUBMITTAL DATED: 2/22/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address* Phone Number*
[e-mail] 2528839301
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0011448
Reviewer*
Troy Doby
Pe rmittee * Town of Snow Hill
Facility Name * Snow Hill WWTP
County* Greene
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
2018 Snow Hill Annual Report.pdf 2.37MB
Application Form Engineering Aans, Specifications, Calculations, Etc.)

For nein and modification permit applications, the paper copy is required to be subrrutted to the
Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic
applications have been received_ The paper copy shall include the follo-kAmig:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineenng plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Service:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigb_ NC 27699-1613
By CourieriSpecial Delivery:
Division of Water Resources- Non -Discharge Branch
Ag Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Raleigh,NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or
Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/22/2019

TOWN OF SNOW HILL
2018 ANNUAL LAND APPLICATION OF
RESIDUAL BIO -SOLIDS REPORT
CLASS B PROGRAM
WQ0011448
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
January 3, 2019
SOIL PLUS

SOIL PLUS
January 3, 2019
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2018 LAND APPLICATION ANNUAL REPORT
Town of Snow Hill "Class B" Program
NC Permit No.: WQ0011448
Soil Plus Project No. 200804.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Snow Hill on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The Town of Snow Hill conducted application events on permitted fields in Greene
County during 2018. A total of 42.99 Dry Tons or 293,700 gallons of permitted residual
bio -solids were land applied to permitted fields.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Town of Snow Hill (252-935-5994) for further
assistance.
Respectfully,
Drew Matthews, Soil Plus
Joe Roberts, Town of Snow Hill
Jason Smith, Granville Farms
P.O. Box 1396
Oxford, NC 27565
[phone]
dmatthews @s oilplus. net
www.soilplus.net

Town of Snow Hill
2018 Annual Land
Application of
Residual Bio -Solids
Report
WQ0011448
Snow Hill, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Analytical Data
TCLP
FIELD LOADING
SUMMARY FORM
Town of Snow Hill Farm
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
SOIL SAMPLES
Town of Snow Hill Farm

Town of Snow Hill
2018 Class B Annual Report
WQ Permit# WQ0011448
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber )FacilityName Land Application Operator County Phone Number
WQ0011448 Town of Snow Hill Granville Farms, Inc. Greene [phone]
Year: 2018
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. :also, If residuals were generated but not land applied, please attach an explanation on how the k El
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 1
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 42.99
Total number of acres utilizes for land application during the year: 11.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality 0 R
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15x1 NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit
S. All monitoring and reporting requirements in 15x1 NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received ftom the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediation.
11- Vegetative cover upas maintained and proper crop management was performed on each site receing residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals._
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowinLy violations."
(ArF 1 hofy-�M 1QAW V
Title e or print)
S' ature of Preparer* Date
(t different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15.x1. NCAC 02T .1102 (26)
Thursday, faivaq 3, 2019
Signature of Permittee
1-3-2019
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
Town of Snow Hill WWTP 293,700 42.99
Total 293,700 42.99
Thursday, January 3, 2019 Page 1 of 1

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Town of Snow Hill
2018 Class B Annual Report
WQ Permit# WQ0011448
Residual Sampling Summary Form
Field Loading Calculations
2018 Analytical
2018 TCLP

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AGMAN FIELD LOADING ESTIMATES
Facility Town of Snow Hill WWTP
Sampling Date 3/26/2018
% Solids 3.51
Mineralization Rate 0.3
Gallons per DT 6,832.14
pH 5.8
Sodium Absorpotion 0.99 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 38,200 lbs./1,000 gal 11.18
Ammonia Nitrogen (mg/Kg) 284.00 lbs./1,000 gal 0.08
Nitrate -Nitrite (mg/Kg) 3,080.00 lbs./1,000 gal 0.90
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 14,597 lbs./1,000 gal 4.27
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 14,739 lbs./1,000 gal 4.31
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.41
Phosphorus lbs./1,000 gal 5.65
Calcium lbs./1,000 gal 4.74
Magnesium lbs./1,000 gal 1.23
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
1.42
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.75
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
652.00
Copper lbs./1,000 gal
0.19
Lead (mg/Kg)
22.50
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.50
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
19.60
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
1.42
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
442.00
Zinc lbs./1,000 gal
0.13
RESIDUAL NITROGEN CALCULATION
23,603
Total 20,673 41.35
Total 20,778 41.56
Equations
1 st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TIflV
(mg/kg) (lbs/DT)
(m Y_-)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
38,200
14,597
29.19
23,603
38,200
14,739 29.48
23,461
23,603
3,540
7.08
20,063
23,461
3,519 7.04
19,942
20,063
1,505
3.01
18,558
19,942
1,496 2.99
18,446
18,558
696
1.39
17,862
18,446
692 1.38
17,755
17,862
335
0.67
17,527
17,755
333 0.67
17,422
Total 20,673 41.35
Total 20,778 41.56
Equations
1 st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

Contact: C. Scott Carpenter
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 4
Report Date: 4/12/2018
Project: Snow Hill
Date Sample Rcvd: 3/26/2018
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
03261820 Sample:
Results
3.52 %
258 col/g dry wt
Snow Hill Grab
Analysis Date
3/28/18
3/26/18
Reporting Limit
0-100 %
258 col/g dry wt
3/26/2018
Method
SM 2540B
SM 9222D
Meritech Work Order #
03261821
Sample:
Snow Hill Grab
3/26/2018
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.51
%
3/28/18
0-100
%
SM 2540B
Ammonia, Nitrogen
<284
mg/kg
3/27/18
284
mg/kg
EPA 350.1
TKN
38,200
mg/kg
3/27/18
20
mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
3,080
mg/kg
3/28/18
391
mg/kg
EPA 353.2
Aluminum, total
6,840
mg/kg
4/2/18
2.50
mg/kg
EPA 200.7
Arsenic, total
<1.42
mg/kg
4/2/18
1.42
mg/kg
EPA 200.7
Cadmium, total
0.746
mg/kg
4/2/18
0.510
mg/kg
EPA 200.7
Calcium, total
16,200
mg/kg
4/2/18
10.0
mg/kg
EPA 200.7
Copper, total
652
mg/kg
4/2/18
1.00
mg/kg
EPA 200.7
Lead, total
22.5
mg/kg
4/2/18
5.56
mg/kg
EPA 200.7
Magnesium, total
4,200
mg/kg
4/2/18
10.0
mg/kg
EPA 200.7
Mercury, total
0.499
mg/kg
4/3/18
0.051
mg/kg
EPA 245.1
Molybdenum, total
1.93
mg/kg
4/2/18
4.63
mg/kg
EPA 2003
Nickel, total
19.6
mg/kg
4/2/18
2.0
mg/kg
EPA 2003
Phosphorus, total
19,300
mg/kg
4/2/18
2.00
mg/kg
EPA 200.7
Potassium, total
4,800
mg/kg
4/2/18
20.0
mg/kg
EPA 200.7
Selenium, total
<1.42
mg/kg
4/2/18
1.42
mg/kg
EPA 200.7
Sodium, total
2,930
mg/kg
4/2/18
20.0
mg/kg
EPA 2003
Zinc, total
442
mg/kg
4/2/18
0.500
mg/kg
EPA 2003
pH
5.8
S.U.
4/2/18
1.0 -14.0
S.U.
SM 4500 -HB
fi
I hereby certify that I have reviewed and approve these data. �F �-,�j�;��
Laboratory Representative
642 Tamco Road, Reidsville, Nort
h Carolina 27320
tel.[phone] fax.[phone]

Contact: C. Scott Carpenter
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Report Date: 4/12/2018
Project: Snow Hill
Date Sample Rcvd: 3/26/2018
Meritech Work Order # 03261813 Sample: Snow Hill Grab 3/26/2018
1311- TCLP Metals
Parameter Results Analysis Date Det. Limit Reg. Limit Method
Arsenic <0.100 mg/L 4/2/2018 0.100 5.0 EPA 200.7
Barium 0.561 mg/L 4/2/2018 0.050 100.0 EPA 200.7
Cadmium <0.020 mg/L 4/2/2018 0.020 1.0 EPA 200.7
Chromium <0.050 mg/L 4/2/2018 0.050 5.0 EPA 200.7
Lead <0.100 mg/L 4/2/2018 0.100 5.0 EPA 200.7
Mercury <0.02 mg/L 4/3/2018 0.02 0.2 EPA 245.1
Selenium <0.100 mg/L 4/2/2018 0.100 1.0 EPA 200.7
Silver <0.050 mg/L 4/2/2018 0.050 5.0 EPA 200.7
TCLP Organics
Parameter Results Analysis Date Report
ing Limit Method
Volatiles 8260 Attached 4/3/2018 - 8260
em o. Attached 4/5/2018 8270
Other Tests
Parameter Results Analysis Date Reporting Limit Method
Cyanide, total <0.500 mg/kg 3/27/2018 0.500 mg/kg EPA 335.4
Sulfide <10.0 mg/kg 3/27/2018 10.0 mg/kg SW 846 9038
Ignitability >140 OF 4/2/2018 EPA 1030
Corrositivity (pH) 5.8 S.U. 4/2/2018 1.0 - 14.0 S.U. SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
«h
Page 2
Contact: C. Scott Carpenter Report Date: 4/12/2018
Client: Soil Plus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 3/26/2018
Meritech Work Order # 03261813 Sample: Snow Hill Grab 3/26/2018
1311- TCLP Pesticides & Herbicides
Pesticide - SW -846 8O81A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin
<0.002
mg/L
4/10-11/18
0.002
0.02
1
Chlordane
<0.003
mg/L
4/10-11/18
0.003
0.03
1
Toxaphene
<0.050
mg/L
4/10-11/18
0.050
0.5
1
Methoxychlor
<1.00
mg/L
4/10-11/18
1.00
10.0
1
Heptachlor
<0.0008
mg/L
4/10-11/18
0.0008
0.008
1
Lindane
<0.040
mg/L
4/10-11/18
0.040
0.4
1
Herbdes - SW -846 8151A
Parameter
Results
Analysis Date Det. Limit
Reg. Limit Dilution Factor
2,4-1)
<1.0 mg/L
4/10-11/18 1.0
10.0 1
2,4,5 -TP (Silvex)
<0.10 mg/L
4/10-11/18 0.10
1.0 1
Meritech Work Order #
03261814 Sample:
Snow Hill Grab
3/26/2018
Parameters
%Total Solids
Fecal Coliform (Sludge)
Results Analysis Date Reporting Limit Method
3.52
%
3/28/18
0-100
%
SM
2540B
<258
col/g dry wt
3/26/18
258
col/g dry wt
SM
9222D
Meritech Work Order #
642 Tamco Road, Reidsville, Nort
03261815 Sample:
Snow Hill Grab
3/26/2018
Parameters
Results
Analysis Date
Reporting Limit Method
% Total Solids
3.52 %
3/28/18
0-100 % SM 2540B
Fecal Coliform (Sludge)
258 col/g dry wt
3/26/18
142 col/g dry wt SM 9222D
h Carolina 27320
tel.[336)342-4748 fax.[phone]

MERITECH, INC.
Environmental Laboratories
Laboratory Certificate #165
Client: Soil Plus
Project: Snow Hill
Client Sample ID: Snow Hill
Sample Collection: 03/26/18
Meritech Sample ID: 03261813
1311 - TCLP Organics
Volaffies: SW -846 8260
Analysis: 04/03/18 Extracted: 03/28/18
Analyst: VWV
Parameter Result Units Det. Limit Ree. Limit Dilution Factor
Benzene
Parameter Result Units Det. Limit Ree. Limit Diluti
< 0.0100
mg/L
0.0100
5.00
10
Carbon Tetrachloride
<0,0100
mg/L
0.0100
5.00
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
12-Dichloroethane
<0,0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
<0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
<0,0200
mg/L
0.020
0.20
10
Semi -Volatiles: SW -846 8270
200
10
Nitrobenzene
<0.100
Analysis: 04/05/18
0.100
Extracted:
03/28/18
10
Pentachlorophenol
Analyst: CWL
mg/L
0.500
100
I hereby certify that I have reviewed and approve these data. Cj_'�
Laboratory Representative
642 Tamco Road *Reidsville, NC 27320
[phone] Ph * [phone] Fax
on Factor
1,4 -Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0:100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachtoroethane
<0.100
mg/L
0.100
3.00
10
o -cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5 -Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6 -Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. Cj_'�
Laboratory Representative
642 Tamco Road *Reidsville, NC 27320
[phone] Ph * [phone] Fax

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Town of Snow Hill
2018 Class B Annual Report
WQ Permit# WQ0011448
Land Application Field Summary Form

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Town of Snow Hill
2018 Class B Annual Report
WQ Permit# WQ0011448
Pathogen & Vector Attraction Reduction Form
30 -Day Scale Bench Test
Fecal Coliform Geometric Mean

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Snow Hill WQ Permit Number: NVQ0011448
WWTP Name: Town of Snow Hill WWTI' NPEDS Number. NCO020842
Monitoring Period: 01/01/2018 to 12/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens":
"Class S" Alternative: Alternative 1
If applicable to alternative performed ("Class 6" only) indicate "Process to Further Reduce Pathogens":
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 258 258 258 U
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30 -day bench)
Not Applicable
Not Applicable
Frequency Sample Type
Crab Samplcs
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been suet."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Joe Roberts, ORC
Jason Smith VP
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
S'c
1-3-2019
S ature of Preparer* Date Signature of Land Applier (if applicable Date
i
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Wednesday, December 5, 2018

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
«h
Page 2
Contact: C. Scott Carpenter Report Date: 4/12/2018
Client: Soil Plus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 3/26/2018
Meritech Work Order # 03261813 Sample: Snow Hill Grab 3/26/2018
1311- TCLP Pesticides & Herbicides
Pesticide - SW -846 8O81A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin
<0.002
mg/L
4/10-11/18
0.002
0.02
1
Chlordane
<0.003
mg/L
4/10-11/18
0.003
0.03
1
Toxaphene
<0.050
mg/L
4/10-11/18
0.050
0.5
1
Methoxychlor
<1.00
mg/L
4/10-11/18
1.00
10.0
1
Heptachlor
<0.0008
mg/L
4/10-11/18
0.0008
0.008
1
Lindane
<0.040
mg/L
4/10-11/18
0.040
0.4
1
Herbdes - SW -846 8151A
Parameter
Results
Analysis Date Det. Limit
Reg. Limit Dilution Factor
2,4-1)
<1.0 mg/L
4/10-11/18 1.0
10.0 1
2,4,5 -TP (Silvex)
<0.10 mg/L
4/10-11/18 0.10
1.0 1
Meritech Work Order #
03261814 Sample:
Snow Hill Grab
3/26/2018
Parameters
%Total Solids
Fecal Coliform (Sludge)
Results Analysis Date Reporting Limit Method
3.52
%
3/28/18
0-100
%
SM
2540B
<258
col/g dry wt
3/26/18
258
col/g dry wt
SM
9222D
Meritech Work Order #
642 Tamco Road, Reidsville, Nort
03261815 Sample:
Snow Hill Grab
3/26/2018
Parameters
Results
Analysis Date
Reporting Limit Method
% Total Solids
3.52 %
3/28/18
0-100 % SM 2540B
Fecal Coliform (Sludge)
258 col/g dry wt
3/26/18
142 col/g dry wt SM 9222D
h Carolina 27320
tel.[336)342-4748 fax.[phone]

Contact: C. Scott Carpenter
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 3
Report Date: 4/12/2018
Project: Snow Hill
Date Sample Rcvd: 3/26/2018
Meritech Work Order # 03261816 Sample: Snow Hill Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 3.52 % 3/28/18 0-100 %
Fecal Coliform (Sludge) 258 col/g dry wt 3/26/18 258 col/g dry wt
Meritech Work Order # 03261817
Parameters
Results
Sample: Snow Hill Grab
Analysis Date Reporting Limit
3/26/2018
Method
SM 2540B
SM 9222D
3/26/2018
Method
%Total Solids
3.52
%
3/28/18
0-100 % SM 2540B
Fecal Coliform (Sludge)
258
col/g dry wt
3/26/18
258 col/g dry wt SM 9222D
Meritech Work Order #
03261818
Sample:
Snow Hill Grab
3/26/2018
Parameters Results Analysis Date Renortin Lg imit Method
%Total Solids
3.52
%
3/28/18
0-100 % SM 2540B
Fecal Coliform (Sludge)
<258
col/g dry wt
3/26/18
258 col/g dry wt SM9222D
Meritech Work Order #
03261819
Sample:
Snow Hill Grab
3/26/2018
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.52 %
3/28/18
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<258 col/g dry wt
3/26/18
258 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: C. Scott Carpenter
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 4
Report Date: 4/12/2018
Project: Snow Hill
Date Sample Rcvd: 3/26/2018
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
03261820 Sample:
Results
3.52 %
258 col/g dry wt
Snow Hill Grab
Analysis Date
3/28/18
3/26/18
Reporting Limit
0-100 %
258 col/g dry wt
3/26/2018
Method
SM 2540B
SM 9222D
Meritech Work Order #
03261821
Sample:
Snow Hill Grab
3/26/2018
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.51
%
3/28/18
0-100
%
SM 2540B
Ammonia, Nitrogen
<284
mg/kg
3/27/18
284
mg/kg
EPA 350.1
TKN
38,200
mg/kg
3/27/18
20
mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
3,080
mg/kg
3/28/18
391
mg/kg
EPA 353.2
Aluminum, total
6,840
mg/kg
4/2/18
2.50
mg/kg
EPA 200.7
Arsenic, total
<1.42
mg/kg
4/2/18
1.42
mg/kg
EPA 200.7
Cadmium, total
0.746
mg/kg
4/2/18
0.510
mg/kg
EPA 200.7
Calcium, total
16,200
mg/kg
4/2/18
10.0
mg/kg
EPA 200.7
Copper, total
652
mg/kg
4/2/18
1.00
mg/kg
EPA 200.7
Lead, total
22.5
mg/kg
4/2/18
5.56
mg/kg
EPA 200.7
Magnesium, total
4,200
mg/kg
4/2/18
10.0
mg/kg
EPA 200.7
Mercury, total
0.499
mg/kg
4/3/18
0.051
mg/kg
EPA 245.1
Molybdenum, total
1.93
mg/kg
4/2/18
4.63
mg/kg
EPA 2003
Nickel, total
19.6
mg/kg
4/2/18
2.0
mg/kg
EPA 2003
Phosphorus, total
19,300
mg/kg
4/2/18
2.00
mg/kg
EPA 200.7
Potassium, total
4,800
mg/kg
4/2/18
20.0
mg/kg
EPA 200.7
Selenium, total
<1.42
mg/kg
4/2/18
1.42
mg/kg
EPA 200.7
Sodium, total
2,930
mg/kg
4/2/18
20.0
mg/kg
EPA 2003
Zinc, total
442
mg/kg
4/2/18
0.500
mg/kg
EPA 2003
pH
5.8
S.U.
4/2/18
1.0 -14.0
S.U.
SM 4500 -HB
fi
I hereby certify that I have reviewed and approve these data. �F �-,�j�;��
Laboratory Representative
642 Tamco Road, Reidsville, Nort
h Carolina 27320
tel.[phone] fax.[phone]

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P�
U F;Z
PROM PT•ACCU RATE -PC LIACLE
LABORATORIES, INC
%V %V.PARLA85.00.Nl
REPORT OF ANALYSES
Attn: SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS STREET
GREENVILLE, NC 27858 -
PROJECT NAME: MAR 18
DATE: 05/10/18
SAMPLE NUMBER- 131103 SAMPLE ID- SNCW HILL SAMPLE MATRIX- SO
DATE SAMPLED- 03/26/18 TIME SAMPLED- 0900
DATE RECEIVED- 03/27/18 SAMPLER- DM RECEIVED BY- DJ
TIME RECEIVED- 0955 DELIVERED BY- UPS TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 03/27/18 1400 RE ATTACHED
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, N('28241-1483
Phone: [phone] • Fax: [phone]

RbLF;Z
PROM PT-ACCURATr-• R E L. I A B LE
LA13ORA-r0P- ESQ INC
WWW. PARLASS . COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Start: End:
TS )
0.2458
0.1538
TS%
1.77%
1.78%
VS
0.1661
0.1015
VS%
67.58%
65.99%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0119612
0.0117503
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0057393
0.0060546
FSVR Mass Balance
1.75%
FSVR (Van Kleeck)
1.75%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 *Charlotte, NC 282414483
Phone: [phone] a Fax: [phone]

PAR
RROMAT•ACCURAT E•R£LIABLE
LABORATORIES, INC
WWW.PARLABS.COM
Collected
D. 0.
Crucible
Tare Wt (g}
Sample Wt +
Tare Wt (g)
Liquid Sludge Wt
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wt
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Tel °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 Day Bench Scale Extended Aeration Test
1/AR nntinn i Parr'At7t Vnlatila Snlirl5 Radurtinn
CLIENT NAME:
SAMPLE ID:
SAMPLE #:
START DATE:
END DATE:
As Received Day 0
03127/18 03/29118
Day 7 Day 14 Day 21 Day 28
04/05/18 04112/18 04119/18 04126/18
22.1780
4.71
5.39
5.87
6.11
6.20
X13
X3
X17
X4
X2
X13
21.8715
21.5786
21.2166
20.3667
25.0630
21.8704
30.2095
35.4652
30.1442
28.9813
32.7661
30.5085
8.3380
13.8866
8.9276
8.6146
7.7031
8.6381
106
106
106
106
106
106
03/27/18 14:00
03/29/18 09:15
04/05/18 09:20
04/12/18 10A5
04/19/18 01
04/26/18 10:00
03/28/18 15:00
03/30/18 09:00
04/06/18 10:00
04/13/18 10:30
04/20/18 09:10
04/27/18 11:15
22.1780
21.8244
21.3764
20.5183
25.1978
22.0242
0.3065
0.2458
0.1598
0.1516
0.1348
0.1538
lv.
0.0797
0.0520
0.0494
0.0456
0.0523
Sludge at End of Test
550
550
550
550
550
T5
03/30/18 11:50
04/06/18 13:40
04/13/18 14:00
04/20/18 12:10
04/27/18 14:40
03/30/18 13:00
04/06/18 14:45
04/13/18 15:15
04/20/18 13:00
04/27/18 15:50
Yt Mass Fraction of Volatile Solids in Liquid (Feed)
21.6583
21.2686
20.4161
25.1086
21.9227
Sludge at End of Test
0.1661
0.1078
0.1022
0.0892
0.1015
3.68%
1.77%
1.79%
1.76%
1.75%
1.78%
Sludge at End of Test
67.58%
67.46%
67.41%
66.17%
65.99%
Yt Mass Fraction of Volatile Solids in Liquid (Feed)
Yb Mass Fraction of Volatile Solids in Liquid (Bottom]
Sludge at Start of Test
0.0119612
Sludge at End of Test
0.0117503
Xf Mass Fraction of Fixed Solids In Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids In Liquid (Bottom)
at Start of Test
0.0057393
Sludge at End of Test
0.0060546
TS )
0.2458
T5
0.1538
VS
0.1661
VS
0.1015
Volatile Fraction In: 0.38181
P.U. Box 411483 • Charlotte, NC 28141-1483
Phone: [phone] Fax: [phone]
Volatile Fraction Out: 1 0.37073

RAR
LA BORA TORIES. INC.
www.parlabs.com
Shipping:
2217 Graham Park Drive
Char[otte, NC 28273
CHAIN OF CUSTOD Y
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custndv document for acceptance by PAR Laboratories, Inc. and the North
r—lina rlanmrtmant of r—irnnmantal er m Natal Raa—r—
Company Name (billing)
Comments! Special Instructions
Soil Plus
Preserv.
Set Up
Data/Time
Email or fax results to
Analyses
Requested
Address
PO Box 1396
[e-mail]
X
[phone] Fax
3 f .Z� Ir
City, state Et zip code
Oxford, NC 27565
Only Send bill to
address shown
Point of Contact & Telephone Number
Scott Carpenter, [phone]
Sample
Taken By: SIGNATURE11LA PRINTED NAME Drew Matthews
ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO
Sample Type: ow VM GWMW HW Soil other x
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No x Teflon Liner/Zero Headspace: Yes No We x
IL Residual Chlorine checked at time of sampling IY1Nj: N Dechlorination Necessary IYINI: N
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Data/Time
Collection
Dateirime
Analyses
Requested
Snow Hill
X
3 f .Z� Ir
30 -Day Scale Bench Test
Rslinq>:j���Dartefff Ree®ivad b patelTlme
3ZC�Jr 7 45
Relinquished by: DatefTime. Received by: Daterrime
* C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW—Hazardous Waste

Town of Snow Hill
2018 Class B Annual Report
WQ Permit# WQ0011448
Soil Samples

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