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Home My WebLink AboutWQ0034513_Residual Annual Report 2018_20190227INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0034513 SUBMITTAL DATED: 2/21/2019 Project Contact Information Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Rob Willcox Email Address* Phone Number* rob@Wllcoxmabesoil.com 336-339-9128 Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0034513 Reviewer* Troy Doby Permittee* John Nichols Facility Name * Brunswick County Public Utilities County* Brunswick r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. 2018 CLASS B ANNUAL REPORT - Brunswick 7.1 MB County-WQ0034513-signed.pdf Application Forint Engineering Rans, Specifications, Calculations, Etc.) For nein and modification permit applications, the paper copy is required to be subrmtted to the Division- Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follmtLring= • Application Farm • All rulevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extra set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) T:di shall ae mailed to the followins aPrl-: s: By pclal ser- lce: Divisron o= % ater Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 2.7699-1613 By Courier/Special Delivery: Division of Water Resources- Non -Discharge Branch AZ Nathaniel Thornburg- 9th Floor, Office #942WN 512 N_ Salisbury St_ Ralei NC 27604 For que€tions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdenr_gov or Sonia Graves at 919.707.3657 or Sonia.Graves(apcdenr.. * I;W By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/21/2019 2018 ANNUAL REPORT BRUNSWICK COUNTY PUBLIC UTILITIES RESIDUALS LAND APPLICATION PROGRAM NON -DISCHARGE PERMIT #WQ0034513 Prepared For: Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 February 2019 willcox&mabe SOI L SOLUTIONS February 19, 2019 N.C. Department of Environmental Quality Division of Water Resources — Non -Discharge Branch 512 N. Salisbury Street, 9t' Floor, Office # 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Branch Reference: 2018 LAND APPLICATION ANNUAL REPORT Brunswick County Public Utilities Non -Discharge Permit No. WQ0034513 WMSS Project No. 15-04 Phase: 06 Non -Discharge Branch: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Brunswick County Public Utilities (Brunswick County). WMSS compiled this report using data gathered during the compliance year by Brunswick County and BioGreen Services, Inc. This data includes: 1) land application certification forms, 2) annual residual sampling summary forms, 3) annual pathogen and vector attraction reduction forms, 4) annual field summary forms and metals field loading summary forms, 5) lab sheets, and 6) soil analysis reports. Brunswick County land applied a total of 18.24 dry tons of biosolids under Permit No. WQ0034513 during the 2018 calendar year (Carolina Shores WWTP-10.19 dry tons, Ocean Isle Beach WWTP-2.73 dry tons, and Sea Trail WWTF-5.32 dry tons). If there is any further information required or questions regarding this annual report please do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations with Brunswick County at (910) 253-2485 or Rob Willcox with WMSS for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe Agronomist/Partner Enclosures Rob Willcox, L.S.S. Soil Scientist/Partner Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 06 - 2018 Annual Report\2018 Annual Report\Class B\2018 CLASS B ANNUAL REPORT - Brunswick County.doc Willcox & Mabe Soil Solutions, PLLC/7231B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com TABLE OF CONTENTS SECTION NO. TITLE Annual Land Application Certification Forms (Form ACF) II Annual Residual Sampling Summary Forms (Form RSSF) Annual Pathogen and Vector Attraction Reduction Forms (503 Rules) (Form PVRF 503) IV Annual Land Application Field Summary Forms and Annual Metals Field Loading Summary Forms (Form FSF and MFLSF) V Lab Sheets VI Soil Analysis Reports Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 RESIDUALS LAND APPLICATION PROGRAM CLASS B RESIDUALS PERMIT NO. WQ0034513 CAROLINA SHORES WWTP NPDES PERMIT NO. NCO044873 OCEAN ISLE BEACH WWTP PERMIT NO. WQ0006085 SEA TRAIL WWTF PERMIT NO. WQ0012748 Mr. Donald Dixon, Deputy Director of Wastewater Operations Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 (910) 253-2485 2018 Carolina Shores WWTP Dry Tons - 10.19 2018 Ocean Isle Beach WWTP Dry Tons - 2.73 2018 Sea Trail WWTF Dry Tons - 5.32 Total Dry Tons 18.24 2018 Carolina Shores WWTP Dry Metric Tons - 9.24 2018 Ocean Isle Beach WWTP Dry Metric Tons - 2.48 2018 Sea Trail WWTF Dry Metric Tons - 4.83 Total Dry Metric Tons 16.55 SECTION I ANNUAL LAND APPLICATION CERTIFICATION FORMS (Form ACF) ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 County: Facility Name (as shown on permit): Land Application Operator: Brunswick Year: 2018 Brunswick County Bio -Green Services, Inc. Phone: 336-940-4544 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary. Carolina Shores WWTP Total number of application fields in thepermit: 23 Total number of fields utilized for land application during the year: 5 Total amount of dry tons applied during the year for all application sites: 10.19 Total number of acres utilizes for land application during the year: 51.4 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. ❑r Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I 111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." John Nichols, Director of Public Utilities Permittee Name and Title (type or print) of Preparer* Carolina Shores of Permittee r- L Date Signature of Land Date Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 County: Brunswick Year: Facility Name (as shown on permit): Land Application Operator: Brunswick County 2018 Bio -Green Services, Inc. Phone: 336-940-4544 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes L1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals AvOication Summary: Ocean Isle Beach WWTP Total number of application fields in thepermit: 23 Total number of fields utilized for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 2.73 Total number of acres utilizes for land application during the year: 11.3 Part B_ -_Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant Loading Rates in 15A NCAC 02T.] 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1 1 11 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources, 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." John Nichols, Director of Public Utilities Permittee Name and Title (type or print) of Permittee c -- Date Signature of Preparer* Ocean Isle Beach WWTP Date �ignature of Land AOHp r Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T ,1102 (26) DENR FORM ACF (12/2006) ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 County: Brunswick Year: 2018 Facility Name (as shown on permit): Brunswick County Land Application Operator: Bio -Green Services, Inc. Phone: 336-940-4544 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes L1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A -_Residuals Application Summary: Sea Trail WWTP Total number of application fields in the permit: 23 Total number of fields utilized for land application during the year: 4 Total amount of dry tons applied during the year for all application sites: 5.32 Total number of acres utilizes for land application during the year: 39.4 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .l 111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." John Nichols, Director of Public Utilities Permittee Name and Title (type or print) of Preparer* Sea Trail W WTP JZ_ A�/ Z 9 Sip,naNre of Vermittee .4 Date r Date Signature of Land �f //� Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) BRUNSWICK COUNTY .A.DMINISTRATION BRUNSWICK COUNTY GOVERNMENT CENTER DAVID R. SANDIFER COUNTY ADMINISTRATION BuiLDiNG 30 GOVERNMENT CENTER DuivE, N.E. MAILING Am)RFss: BOLIVIA, NORTH CAROLINA 284.22 TFLEPHONE (910)253-2000 POST OMCE Box 249 (800) 442-7033 BOLIVIA, NORTH CAROLINA 28422 FAX (910) 253-2022 July 30, 2018 Mr. William L. Pinnix, P.E. Director of Engineering Mr. John Nichols, P.E., Director of Public Utilities Re: County Signatory Authority Dear Mr. Pinnix and Mr. Nichols: You are hereby authorized to sign the following permit applications and certification related documents: • NCDEQ-PWSS Water Permit Applications • NCDEQ-DWQ Sewer Permit Applications • NCDEQ-DWQ FTSE -04/16 Sewer Flow Tracking Applications • NCDOT Encroachment Permit Applications • County Letter (ref contractor's bond) required for the NCDOT Encroachment Permit • Partial and / or Final Applicant's Certifications for Water Main Extensions • Partial and / or Final Applicant's Certifications for Sewer Main .Extensions • NCDEMLR — band Quality Sedimentation & Erosion Control Permit Applications (for County CIP projects) Please let me know if you have any questions. Sincerely, Ann B. Hardy County Manager SECTION II ANNUAL RESIDUAL SAMPLING SUMMARY FORMS (Form RSSF) E5 12k I l4 M d- M O C? r N M `i W) 4' w a E a F I Q 0 O U L N a �moo Q o "o C> �aC) n, �O NtiCi r --N d. r- n M N o0 N 0 (::) Q Q UbA 2� O0 2 n r-(-4 z Z Z 2 FS U U a� U E I M M d 0 .d E m r.� r M Q 0 a i Zn 0 0 N N r^I LL V) V) re O LL z 1,- d w c� Q a� O O U 0 00 o c> 0 OfJ U L} cc CL Q V] Zn 0 0 N N r^I LL V) V) re O LL z 1,- d F5 AWN 11 Q 0 ro 04 M c1' M O O N M 't r 'i V KA: 00 0 IS C] Q 0 r. i 0 0 U 0 v CL 0 DO C O o O M n N 4 Ono ono � N tiD d n v-)d1�1 t- Ln o d Q d d U bA z n oo 00 n z z z z O b Y n r O O A V] L U G O m s �.. d "C7 O Q C) O A z .� a- C6 o m :, ,, C1 U CJ o tii co L ,-. — 1— r—. �-- N m Wt kr� I O Z L O Get Mi M M O O Lr) 00 0 0 Q O III w r u c� Q a� O Q U 0 U 00 CD CD O U fl v, c3 M `� 3 M Q 0 i 00 N Q 0 r cd a H wI a Ca N N LL N N O LL z LLJ0 CCS a N_ N 0 F- iU Q Q -n rn M 0 a� x L) � L co Q y .Q i�. O S-. O u 00 oo o 0 0 o 0 0 0 0 0 0 C> 006 O h r r = Z 4 r- N r- r- r- Ln 2 Z o 0 2 Z A a--� y �A n Q N s p U O tr Q Q3 as N -I- E o s � Q z a Ca N N LL N N O LL z LLJ0 CCS a N_ N 0 F- iU Q Q -n rn M 0 a� x L) � L co R. 04 Cf) v-� d' M O 0 M. 00 n N 0 0 I Ow G.w z .* Q 0 0 U L Q C�d U? 00 � C? O O O N G7 O C? C� mU r cC4 .N O V] .* SECTION III ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS (503 RULES) (Form PVRF 503) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WWTP Name: Carolina Shores WWTP NPDES Number: Monitoring Period: From I /112018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: WQ0034513 NCO044873 Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alt. 2 (40 -day bench) ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ jAlt. 4 (Spec. O) uptake) If applicable to alternative. performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ 1-Ieat Treatment ❑ Thennophilic ❑ Alt. 6 (Alk. Stabilization Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 0 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Alt. 10 (incorporation) Air Drying❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Num er o Excee- dences Frequency of Analysis Sample Type Analytical Tech pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: AIt.I (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ jAlt. 4 (Spec. O) uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization [] Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Cl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Denise Harrison - Vice President (BioGreen) Prep rer Name and Ti le (type or print) r Signature of Preparer* Vat Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034513 WWTP Name: Ocean Isle WWTP NPDES Number: WQ0006085 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alt. 2 (40 -day bench) ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ JAIt. 4 (Spec. O, uptake) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑ Alt. 6 (Alk. Stabilization Beta Ray ❑ Gamina Ray ❑ Pasteurization ❑ Class B: Alternative 1 EI Alternative 2 ❑ If applicable to alternative performed (Class ll only) indicate "Process to Significantly Reduce Pathogeias": Lime Stabilization ❑ Air Drying.[] Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ I- If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Num Cr o Excee- dences Frequency of Analysis Sample Type Analytical Tech mnique Minimum Geo. Mean Maximum Units Fecal Coliforrn 2 x 10 to the 6th power per grain of total solids MPN CFU 1000 nnpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grains total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ JAIt. 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization C] Alt 7 (Drying; - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) D "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Denise Harrison - Vice President (BioGreen) Prepar ame and Title type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034513 WWTP Name: Sea Trail W WTF NPDES Number: WQ0012748 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ ❑ Alternative 4 ❑ Alternative S ❑ Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Alt. 5 (14 -Day Aerobic) Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative l 0 Alternative 2 ❑ - If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Cl Air Drying[] Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Num er o NExcee- deuces Frequency of Analysis Sample Type Analytical Tech -pique Minimurn Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per ,gram of total solids MPN CFD 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed; Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ jAlt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Q Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please cheep the appropriate statement) Cl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you cheep this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Denise Harrison - Vice President (BioGreen) Prepa e - Name and Tit e (type or print) Land Applier Name and Title (if applicable)(type or print) —4)9f c xex Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR fart 503.9(r) and 15A NCAC 2T.1 102 (26) DENR FORM FVRF 503 (12/2006) SECTION IV ANNUAL LAND APPLICATON FIELD SUMMARY FORMS ANNUAL METALS LOADING SUMMARY FORMS (Form FSF and MFLSF) N_ N S U ch AM 3F * * dE ^- N 1 m r vi '4-, � o0 O, R N U V p NrL N ro Q U O O ) O E U U O b O Q v cn rn r r z Q 0 0 0 0 tt �* z;r�.. 4t, z;-, x* o c C o ,n z Qztt n o 4t N n N :rtt Q O O O0, Opp O O 0 074t.vl a� ClQ Gd � ,n G. z c01 - z O N N a r ry r� p z goo Q Ln It C, M- f•T. C!1 C O q, 00 n0IN 00. Inkn l_ WN N cz p o Q o o In M 0 c O O Q U � O C7 C7 kn In In n N n N Q U y O O O O C, d V V V V p O p ?; '^ v ^ n N O O O N00 Q N 3 3 U ol N L o oc M N M QuO UO O O O, n C o 0 o p o p o o- oc `o c N o O n C n p o p rl)�, 00 �A o 00 c� IN � G Q Q O N ••••• --• O C7 C O O Q O M M O O C5 C O C p p Q p 0 0 O O O Q a 0 o vV 00 �o 14 cid n U � � R O p o n N Ov o 0 0 0? nl �.•.• Q � � `t M N � _S CC y v U _ p V� U LIJUON m S ai F G fGG^ .10 OIL(] Q F Q U •O ri per. I Q ti F -x- m 0 0 N L iry U - L2 2 0 LU 0 ANNUAL METALS FIELD LOADING SUMMARY FORM` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 72.12 Permit #: WQ0034513 Predominant Soil Series: Lynchburg; -Ly Operator: Al Hughes Owner: Guy A. Hughes Etals Acres Used:1 1.3 Acres Permitted: 11.3 Site th NC -BIZ -AH Field #: 3 .................. Residual Analysis Data (Heavy Metals and Total Phosphorus usemg/kg, % Solids use Raw Percent #): Sample or Com- posite Date ' 1 2 3, A 5 1/10118 6 1110118 7 1110118 _a1 9 10 11 : i 1/10/18 %Solids 1 0.63 0.64 0.68 1 0.64 Arsenic 47.3 46.3 72.1 46.3 Cadmium < 78.7 77 72.1 77 Chromium � n 78.7 77 72.1 77 Copper 235 242 551 0.2418 0.1689 242 Lead 0.0838 78.7 77 72.1 0 0 0 0.0229 77 Mercury 0 0 0 0 2.7 2.66 2.5 0 0 0 0 2.66 Molyb- denum 0.0183 0 0 0 47.3 46.3 72.1 ,hroniiun 0 0 0 46.3 Nickel 0.026 0.0183 0 1 78.7 77 72.1 0.0952 Copper 0 0 77 Selenium 0.1136 0.0817 0.1396 0 78.7 77 72.1 0.0406 0.3756 Lead 0 77 Zinc 0 0.0381 0.026 0.0183 684 736 1,150 0 0.0129 0.0952 Mercury 736 'Dotal Phos- porus 0 0 1 0.0013 0.0009 20,400 31;000 57,800 0 0 0.0004 1 0.0033 31,000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): w _7 qj 5j 6 7 8� 3; 10� 11 12 < � n o' 0.2418 0.1689 0.1267 0.0838 Arsenic 0 0 0 0 0.0229 0.0156 0.0183 0 0 0 0 0.0078 0.0645 Cadmium 0 0 0 0 0.0381 0.026 0.0183 0 0 0 0 0.0129 0.0952 ,hroniiun 0 0 0 0 0.0381 0.026 0.0183 0 0 0 0 0.0129 0.0952 Copper 0 0 0 0 0.1136 0.0817 0.1396 0 0 0 0 0.0406 0.3756 Lead 0 0 0 0 0.0381 0.026 0.0183 0 1 0 0 0 0.0129 0.0952 Mercury 0 0 0 0 1 0.0013 0.0009 0.0006 0 0 0 0 0.0004 1 0.0033 Molyb- 0 0 0 0 0.0229 0.0156 0.0183 0 0 0 0 0.0078 0.0645 denum Nickel 0 0 0 0 0.0381 0.026 0.0183 0 0 0 0 0.0129 0.0952 Sclel,iuni 0 0 0 0 0.0381 0.026 0.0183 0 0 0 0 0.0129 0.0952 Zinc 0 0 0 0 0.3308 0.2486 0.2914 0 0 0 0 0.1234 0.9942 'total Phos- 0 0 0 0 9.8654 10.472 14.647 0 0 0 0 5.1956 40.179 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, includ'n the possibilit f fines and imprisonment for knowing violations" r Sig;natEu•e of Land Applier Date K See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) r - O M I IN ME Fes., a� or M W" ni N v 0 O (A O LL cc z LW 0 N M I � I V, 'o � 1 W 1 Ci O ' :: I N R N U N _ cis d U U n z a o o n o 0 0 0� o z �L M Q z G a a 0 a G7 C C�� O z N all M •C z OO M C7 'ci'' � �n � N Cc, K] M M M ryry n • O� a 0 �� c�-U v o 0 0 � c W d # o M a N o 0 CID 0 CD �° 0© c`Dv n w `' ¢ d v v vCL 0 o c or C r 3 3 U O Ir I co C- CA C CA CIOI c U ono � p M 'D O It I I I I I I O V1 p 4 C3 [/� O N C O O O O O O O C O� C, O O y., O Of1i c0 C C g C O 0 a O a O O O a O In m M cp �f' a O O �L` 'C% Q, V' M M O N O Q G O a O O ^^ © Q O O a C O O O O O O C O C Q Q Q Q C Q rs O � It CIO U c� oc • U TI � O � � O O C Lam. � U n M M cz fl cd ra LIJUOIN xo o1vu O ° v 0 O (A O LL cc z LW 0 ANNUAL METALS FIELD LOADING SUMMARY FORM'S Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Permit #: WQ0034513 Operator: Clyde Galloway Owner: Acres Used: 6.4 Acres Permitted: 6.4 Total Dry Tons Applied (Annual): 67.07 Predominant Soil Series: Goldsboro-GoA Clyde Galloway Site #: NC -BR -CG Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date -.� -2 1/10/18 3--' i ��.; _6_l ? -8J 9.j 40 1/10/18 11 1110/18 12, Solids -s q 0.64 0.64 0.68 A1•senic 46.3 46.3 72.1 Cadmium 77 f, 77 72.1 Chromium 77 o' 0.2982 77 72.1 Copper 0.1355 242 Arsenic 0 0.0276 0 0 242 551 0 bead 0 77 0.0208 0 0.0609 Cadmium 0 0.0459 0 77 72.1 0 Mercury 0 2.66 0.0209 0.0208 0 0.0876 'hr0miUn 0 0.0459 2.66 2.5 0 Molyb- denum 0 46.3 0 0.0209 0.0208 0 0.0876 Copper 0 46.3 72.1 0 Nickel 0 77 0 0 0.0656 0.1587 0 0.3686 1.,ead 77 72.1 0 Selenium 0 77 0 0 0 0.0209 0.0208 0 0.0876 77 72.1 0.0016 Zinc 0 736 0 0 0 0 0.0007 0.0007 0 736 1,150 Total Phos- horus 31,000 31,000 57,800 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incl"g g the possibility of fines and imprisonment for knowing violations" J (10 Si nature of Land App ier Date * See bottom of FSI' Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (512003) 4 5 61 71 8 1 _.. 9 16 ] 11 : 12 i -s q M 'V V C f, o' 0.2982 0.1355 0.144 Arsenic 0 0.0276 0 0 0 0 0 0 0 0.0125 0.0208 0 0.0609 Cadmium 0 0.0459 0 0 0 0 0 0 0 0.0209 0.0208 0 0.0876 'hr0miUn 0 0.0459 0 0 0 0 0 0 0 0.0209 0.0208 0 0.0876 Copper 0 0.1443 0 0 0 0 0 0 0 0.0656 0.1587 0 0.3686 1.,ead 0 0.0459 0 0 0 0 0 0 0 0.0209 0.0208 0 0.0876 Mercury 0 0.0016 0 0 0 0 0 0 0 0.0007 0.0007 0 0.003 Molyb- 0 0.0276 0 0 0 0 0 0 0 0.0125 0.0208 0 0.0609 denum Nickel 0 0.0459 0 0 0 0 0 0 0 0.0209 0.0208 0 0.0876 Selenium 0 0.0459 0 0 0 0 0 0 0 0.0209 0.0208 0 0.0876 Zinc 0 0.439 0 0 0 0 0 0 0 0.1995 0.3312 0 0.9696 Total Phos- 0 18.488 0 0 0 0 0 0 0 8.401 16.646 0 43.536 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incl"g g the possibility of fines and imprisonment for knowing violations" J (10 Si nature of Land App ier Date * See bottom of FSI' Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (512003) Cl) r� m r L O a L d L U d SM m 0 0 N u LL (A LL 2 Of Q Ll - a ui LLJ 0 N M 7' V1 �c n 1 00 c " U a Cd ria o U N da U U U U d 4t � Q z o c O o o °C yr o 0 0 0 c z rn Q N 16 Q 4 N U C3 n o L z z N I C� • w In O ItM M O 00 kn �- N N N F" o 0 0 N O z N N n 0 Cl It �t M O O n O N N N � vit- U U O O V VN b C7 C� C/a U C G V U N C d d N O M ry ✓> N N n V� U C O C O O 00Ln C n n n O n O n Q Ol 0� n O O O O C O O O O O v1 N C O n O O O n Q n Q M C 10 M 0 0 o a o ri o o a o 0 0 o c� o Q :b �r o0 U U Nrq "� n n n O O C O O O O N y •� � „..a .�. �_ `C1 � it O O U U c/ Ln z E-+dUaa.a.. m 0 0 N u LL (A LL 2 Of Q Ll - a ui LLJ 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 31.96 Permit #: WQ0034513 Predominant Soil Series: Goldsboro-GoA Operator: Clyde Galloway Owner: Clyde Galloway Acres Used: 11,5 Acres Permitted: 11.5 Site #: NC -BR -CG Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com - posite Date '- 2 3 A 5 6 1/10/18 7 1110118 8 9; 1D i 11 12 Solids � O• 0.64 0.68 Arsenic n 46.3 72.1 Cadmium D 777 72.1 ChrorniL1117 o' 7 ! I 72.1 0.1508 0.1245 Copper Arsenic 242 551 0 0 0 0.014 0.018 Lead 0 0 0 0 0.0319 77 72.1 0 0 0 0 0.0232 Mercury 0 0 0 0 0 2.66 2.5 0 0 0 0 0 Molyb- denum 0.018 0 0 0 0 46.3 72.1 Copper 0 0 0 0 Nickel 0.073 0.1372 0 0 0 77 72.1 0.2102 Lead 0 0 0 Selenium 0 0.0232 0.018 1 0 77 72.1 0 0.0412 Mercury 0 0 Zinc 0 0 0.0008 0.0006 0 736 1,150 0 0 1 0.0014 Molyb- 0 "Total Phos- bonds 0 0 0 0.014 0.018 31,000 57,800 0 0 0 0.0319 denum Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I awn aware that there are significant penalties for submitting false information, incl i g the possibility of rues and imprisonment for knowing violations" _ 41 Signature of Land Applier Date * See bottom of f SF Foran for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) 1 2 3i 4 5 S3 7 8_i 91 40j it 12 � O• n D o' 0.1508 0.1245 Arsenic 0 0 0 0 0 0.014 0.018 0 0 0 0 0 0.0319 Cadmium 0 0 0 0 0 0.0232 0.018 0 0 0 0 0 0.0412 Clit•omiuni 0 0 0 0 0 0.0232 0.018 0 0 0 0 0 0.0412 Copper 0 0 0 0 0 0.073 0.1372 0 0 0 0 0 0.2102 Lead 0 0 0 0 0 0.0232 0.018 0 0 1 0 0 0 0.0412 Mercury 0 0 0 0 0 0.0008 0.0006 0 0 0 0 0 1 0.0014 Molyb- 0 0 0 0 0 0.014 0.018 0 0 0 0 0 0.0319 denum Nickel 0 0 0 0 0 0.0232 0.018 0 0 0 0 0 0.0412 Selenium 0 0 0 0 0 0.0232 0.018 0 0 0 0 0 0.0412 Zinc 0 0 0 0 0 0.222 0.2864 0 0 0 0 0 0.5083 "Total Phos- 0 0 0 0 0 9.3496 14.392 0 0 0 0 0 23.742 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I awn aware that there are significant penalties for submitting false information, incl i g the possibility of rues and imprisonment for knowing violations" _ 41 Signature of Land Applier Date * See bottom of f SF Foran for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) x- � ae � -- N M �f- v -i � n oo � O -• �,� V] O U ^ N p CL n y w O O o Q N N 2 O O�� O C C O C n n n z C o � *F "4ta:VL q q g q q O O d G O R v - R. N N z o N Z oo n n o0 0 X ri VS O d d o0 O CIO N O C > N O O n O x o 0 0 0 0 0 • � � � � � On -� i ^fl C � rU L- Ca n n n ^p + ^ O v to tn q 00 O U] O U Q v v U N omo LL, c o 0 N N 6 Cd Y- � O G1. 00 00 n O O B� Ul C C C n n O O O OC::) C ^ C C q q q Q C. 0 0 0 o c� ri o c� o 0 o c o o ri Q O p o o Q< r7 Vi > CL p ' IN 00 10 OILLIJUO M v s G ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual:): 28.97 Permit #: WQ0034513 Predominant Soil Series: Goldsboro-GoA Operator: Harvey Bell Owner: Joyce Brown Acres Used: 10.2 Acres Permitted: 10.2 Site #: NC -BR -I -IB Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent 9): Sample or Com- posite Date -J 2 3 1/10/18 4; 1110118 5j -611 7, 6� 91 10 11 12 Solids 0.64 0.68 Arsenic 4 n -= 46.3 72.1 Cadmium 77 72.1 Chromium 77 72.1 0.0994 0.1501 Copper 242 551 Arsenic 0 0 0.0092 0.0216 0 0 0 Lead 0 0 77 72.1 0.0308 Cadmium 0 0 0.0153 0.0216 0 0 Mercury 0 0 2.66 2.5 0 0.037 Chl'OlniUff 0 0 0.0153 0.0216 0 Molyb- denum 0 0 46.3 72.1 0 0 0.037 Copper 0 0 0.0481 0.1654 Nickel 0 0 77 72.1 0 0 0 0.2135 Lead 0 0 0.0153 Selenium 0 0 77 72.1 0 0 0 0 0.037 Mcrculy 0 0 'Linc 0.0008 0 736 1,150 0 0 0 0 0 0.0013 Molyb- 0 Total Phos- porus 0.0092 0.0216 31,000 57,800 0 0 0 0 0 0 0.0308 denum Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu g the possibility of fi es and imprisonment for knowing violations" .��.,IV `r!. I Signature o Land Applier Da e x See bottom of FSF form for helpful instructions for this MFLSF Form and the mathematically linked FSF form DENR FORM FSF (5/2003) 1j 2i 3 -- . 4f 5 6� 7, 6� 8� 10i 11� 12� 4 n -= 0.0994 0.1501 Arsenic 0 0 0.0092 0.0216 0 0 0 0 0 0 0 0 0.0308 Cadmium 0 0 0.0153 0.0216 0 0 0 0 0 0 0 0 0.037 Chl'OlniUff 0 0 0.0153 0.0216 0 0 0 0 0 0 0 0 0.037 Copper 0 0 0.0481 0.1654 0 0 0 0 0 0 0 0 0.2135 Lead 0 0 0.0153 0.0216 0 0 0 0 0 0 0 0 0.037 Mcrculy 0 0 0.0005 0.0008 0 0 0 0 0 0 0 0 0.0013 Molyb- 0 0 0.0092 0.0216 0 0 0 0 0 0 0 0 0.0308 denum Nickel 0 0 0.0153 0.0216 0 0 0 0 0 0 0 0 0.037 Selenium 0 0 0.0153 0.0216 0 0 0 0 0 0 0 0 0.037 Zinc 0 0 0.1463 0.3452 0 0 0 0 0 0 0 0 0.4915 Total Phos- 0 0 6.1628 17.352 0 0 0 0 0 0 0 0 23.514 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu g the possibility of fi es and imprisonment for knowing violations" .��.,IV `r!. I Signature o Land Applier Da e x See bottom of FSF form for helpful instructions for this MFLSF Form and the mathematically linked FSF form DENR FORM FSF (5/2003) M P* d N rig w U d N x •x• -� •x• N M � {n �p n co � c ^ � � U o nz� 03 ri o U � � N zit Q Q Y � ZP- 0. N O O O O Q M N n N N m ot Z z Cl� M E cd A O N Gam', r � •� 2 0 - N N �� •- � r o o rLn M M Q C4 n n n Q C] Q i C N ,�„ O ,�,. r•1 M. M M O � � n] O O O aF Ca o '� O b 0 0 Q U Q O O .O" r U N ta..+i w C> N d �' o �a�•p � Uo N N © O c 00 M rte. d O MM O G1. v y, o0 O O Cl O o C- c Q c C> o O N o C o Ca c C o CD 0 of 0 00 0 I:r CQ ¢ O O U O O O Q O C) 'n O O O O O O O G Q O O O � 0 c000a0000000 000 -o w U O O O O O C Q ""C. n oc xo DIB(] d U si u 0 n ANNUAL, METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 17.55 Permit #: WQ0034513 Predominant Soil Series: Lynchburg -Ly Operator: Pearly Vereen Owner: Pearly Vereen Acres Used: 12 Acres Permitted: 12 Site #: NC -BR -PV Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Rare Percent #): Sample or Cotn- posite Date --3-I 2 3 4 5 6 7 A.1 I/10/18 9 10 ii 12 Solids 0.64 Arsenic 46.3 Cadmium 77 Chromium o' 77 0.1512 Copper Arsenic 0 0 242 0 0 0 0 Lead 0 0 0 0 0.014 Cadmium 0 77 0 0 0 0 Mercury 0.0233 0 0 0 0 0.0233 'hromlu 2.66 0 0 0 0 Molyb- denum 0 0.0233 0 0 0 0 0.0233 46.3 0 0 0 0 Nickel 0 0 0.0732 0 0 0 0 77 Lead 0 0 0 Selenium 0 0 0 0.0233 0 0 0 77 0.0233 Mercury 0 0 Zinc 0 0 0 0 0.0008 0 0 736 0 0.0008 Molyb- 0 Total Phos- porus 0 0 0 0 0 0.014 0 31,000 0 0 0.014 denum Annual Heavy Metal Field Loadings (Calculated in lbs/acre): C f 2 3i 4 5 8 71 8 9 10 11, 12] o' 0.1512 Arsenic 0 0 0 0 0 0 0 0.014 0 0 0 0 0.014 Cadmium 0 0 0 0 0 0 0 0.0233 0 0 0 0 0.0233 'hromlu 0 0 0 0 0 0 0 0.0233 0 0 0 0 0.0233 Copper 0 0 0 0 0 0 0 0.0732 0 0 0 0 0.0732 Lead 0 0 0 0 0 0 0 0.0233 0 0 0 0 0.0233 Mercury 0 0 0 0 0 0 0 0.0008 0 0 0 0 0.0008 Molyb- 0 0 0 0 0 0 0 0.014 0 0 0 0 0.014 denum Nickel 0 0 0 0 0 0 0 0.0233 0 0 0 0 0.0233 Selenium 0 0 0 0 0 0 0 0.0233 0 0 0 0 0.0233 Linc 0 0 0 0 0 0 0 0.2226 0 0 0 0 0.2226 Total Phos- 0 0 0 0 0 0 0 9.3744 0 0 0 0 9.3744 phorus 9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incl di g the possibility of fines and imprisonment for knowing violations" s� 4 4--� 4 Signature of Land Applier Date x See hottom of FSF Form for helpful instructions for this M!<LSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) SECTION V LAB SHEETS BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type. Wastewater Treatment Plant Date Sampled: January 10, 2018 Carolina Shores WWTP Permit No. WQ0034513 Mineraiization Rarc 0.30 0.64 % Solids 7.01 pH Nitrogen (TKN) 8.230 82,300.000 164.600 Phosphorus 3.100 31,000.000 62.000 Potassium 0.611 6,1 10.000 12.220 PAN (injected)* 2.882 28,815.000 57.630 PAN (surface)* 2.724 27,240.000 54.480 Anunonia Nitrogen 0.315 3,150.000 6,300 Calcium 3.640 36,400.000 72.800 Calcium Carbonate Eq. --- --- Magnesium --- 3,440.000 6.880 Sodium --- 7,910.000 15.820 Sulfur --- --- --- Nitrate N / Nitrite N --- 1,920.000 3.840 Barium --- --- Chloride -__ --- Iron --- --- - Ceding Concen,' Aluminum -- 3,140.00 6.280 :Iglfg3 Arsenic --- 46.30 0.093 75 Cadmium --- 77.00 0.154 85 Chromium --- 77.00 0.154 --- Copper --- 242.00 0.484 4,300 Lead - - 77.00 0.154 840 Mercury --- 2.66 0,005 57 Molybdenum --- 46.30 0.093 75 Nickel --- 77.00 0.154 420 Selenium --- 77.00 0.154_1 100 Zinc --- 736.00 1.472 1 7,500 lnvirochern: 2018-00427 *Determination of Plant Available nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N 7 Nitrite N W. % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) .�. (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note; Constituents N.D. (Not Detected) or < detection lirrtits are listed as detection limits for calculation purposes. n won �hem a s a � Asp �.� ��: h �'� 0/i h�¢•�( �" s E s' s �y"�i :�I;if? 51' ll�.'!i!il X1',1\, i1ii11111i'`i I LL �r7 tl.�� )IE- ii1' {i�� i..<kl� Jif?..',`).�.•$�.'�� i -i\ "A°ii tt np; on Iir,hwav, J ick of . kilC, L abi - \ ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Revised Report: Mar 07, 2018 Original Report Date: Feb 20, 2018 Report #: 2018-00427 Customer ID: 08100011 Project ID: Carolina Shores Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01086 Site: 1/10/2018 9:30 AM Solid/Sludge Aaron Hewett Test Method Results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.05 mg/L 01/18/2018 Endrin SW 846 Method 80818/3510 <0.0005 mg/L 01/18/2018 Heptachlor SW 846 Method 80818135 10 <0.0005 mg/L 01/18/2018 Heptachlor epoxide SW 846 Method 80811313510 <0.0005 mg/L 01/18/2018 Lindane SW 846 Method 60818/3514 <0.0005 mg/L 01/18/2018 Methoxychlor SW 846 Method 80818/3510 <0.0005 mg/L 01/18/2018 Toxaphene SW 846 Method 80818/3510 <0.05 mg/L 01/18/2018 1,4 -Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 2,4,5 -Trichlorophenol (TCLP) SW 845 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 8270!3510 <0.050 mg/L 01/19/2018 2,4-Dinitrotoluene (TCLP) SW 846 mefhod 8270/3510 <0.050 mg/L 01/19/2018 Cresol (TCLP) SW 846 method 827013510 <0,050 mg/L 01/19/2018 Hexachloro-1,3-butadiene (TCLP) SW 84G method 8270/3510 <0.050 mg/L 01/19/2018 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mglL 01/19/2018 m + p -Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 o -Cresol (TCLP) SW846 method 6270/3510 <0.050 mg/L 01/19/2018 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/19/2018 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,5 -TP SW846 Method 8151A <0.003 mg/L 01/18/2018 2,4-D SW646 Method 8151A <0.003 mg/L 01/18/2018 1,1-Dichloroethylene SW646 Method 826015030 <0.01 mg1L 01/17/2018 112-Dichioroethane SW846Method 626015030 <0.01 mg/1- 01/17/2018 Benzene SW846 Method 8260/6030 <0.01 mg/L 01/1712018 Carbon Tetrachloride SW846 Method 82.60!5030 <0.01 mg/L 01/17/2018 Report tR 2418-04427 �,,.a�..•...e.,,..,�,T,...�........r....w..W,,. ---„d.....,n.,_.r,,...,_a....a.,..,.v�...,.,.mb,,,e.=,c..�.,_,.�..�»m...,F.......,...�.....e.,..�H...,N.,.a.... Page i o}.3 �2 'im, mi .).vironrnental Chemists, Ince F fq + 'W `� t 3 ', t11 1 1 )lj;t, ti \C' �jl 1 <?t?1 i9'? +!'' �"S l il) W --�✓ti - _ =,)`��u'�,� ` I �� :: ?�� 1rVtl3�3i.:fc,�^ :ul:�tinc,Ilc. NC �nys'cy_ - �- ANALYTICAL & COMSULrINGCHEMISTS i>t:i);=rCiititmntr,Ct11.11 l?itl7E fs.c'7171 Brunswick County Public Utilities Post Office Box 249 Bofivia NC 28422 Attention: Donald Dixon Revised Report: Mar 07, 2018 Original Report Date: Feb 20, 2018 Report #: 2018-00427 Customer ID: 08100011 Project ID: Carolina Shores Chlorobenzene SW846 Method 826015030 <0.01 mg/L 01/17/2018 Chloroform SW646 Method 8260!5030 <0.01 mg/L 01/17/2018 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 01/1712018 Tetrachloroethylene SW846 Method 8260/503D <0.01 mg/L 01/17/2018 Trichloroethylene SW846 Method 826015030 <0.01 mg/L 01/17/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 01/1712018 RCI EPA 200 7 <46.3 mg/kg 02/16/2018 Cyanide EPA 335.4 <0.0160 mg/kg 01/16/2018 pH SM 4500 H 8 7.01 units 01/18/2018 Sulfide SM 4500 S o <0.0321 mg/kg 01/22/2018 Ignitability SW 846 melnod 1010 >212 °F 01/19/2018 Sludge Residuals EPA 200.7 7910 mg/kg 01/15/2018 Aluminum EPA 200 7 3140 mg/kg 01/18/2018 Arsenic EPA 200.7 <46.3mglkg 02/16/2018 Reanalyzed 2.16-18 EPA 353.2 1920 mg/kg 01/16/2018 Cadmium EPA 200 7 <77.0 mg/kg 01/28/2018 Calcium EPA 200 7 36400 mg/kg 01/15/2018 Chromium EPA 200 7 <77.0 mg/kg 01/18/2018 Copper EPA 200.7 242 mg/kg 01/18/2018 Lead EPA 200.7 <77.0 mg/kg 01/18/2018 Magnesium EPA 200 7 3440 mg/kg 01/15/2018 Molybdenum EPA 200 7 <46.3 mg/kg 02/16/2018 Reanalyzed 2-16-18 Nickel EPA 200.7 <77.0 mg/kg 01/18/2018 Potassium EPA 200.7 6110 mg/kg 01/15/2018 Selenium EPA 200 7 <77.0 mg/kg 01/18/2018 Sodium EPA 200.7 7910 mg/kg 01/15/2018 Zinc EPA 2007 736 mg/kg 01/18/2018 Total Kjeldahl Nitrogen (TKN) EPA 351 2 82300 mg/kg 01/17/2018 Nitrate4-Nitrite-Nitrogen EPA 353.2 1920 mg/kg 01/16/2018 ReFoi�i:a...2Dsa..0o4z7�.,...9w.w��...��_,..y.,:,..<.�,_.,�,._,.,_-�--.,�..,.�....a..�,..,..w._.�..,�,��,..�...,,..,.�..wa.,�.,...�.�..�.�.a,�._.,.�..._.,..,..sM,,.�,.....n.e.�......,..�...,.u,.� Pane. 2 of 3 z� li. ii 1 c°:t 11 11'c>l 2 1[ nCc t, �[ 1 1 �. 111 x Wiils?,�.r,fi�i� ANALYTr,AL ONSULTNG CHEF, ISIS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Revised Report: Mar 07, 2018 Original Report Date: Feb 20, 2018 Report #: 2018-00427 Customer ID: 08100011 Project ID: Carolina Shores Total Solids (%) SM 2540 s 0.64% _ 01/11/2018 Ammonia Nitrogen SM 4500 NH3 c 3150 mg/kg 01/21/2018 Total Phosphorus SM 4500 P F 31000 mg/kg 01/18/2018 Mercury SW8467471[3 <2.66 mg/kg 01/15/2018 TCLP Metals Arsenic EPA 2007 <1.0mg/L 01/22/2018 Barium EPA 200 7 <1.0 mq/L 01/22/2018 Cadmium EPA 2007 <1.0mg/L 01/22/2018 Chromium EPA 200.7 <1.0 mg/L 01/22/2018 Lead EPA 200.7 <1.0 mg/L 01/22/2018 Selenium EPA 2007 <1.0mg/L 01/22/2018 Silver EPA 200.7 <1.0 mg/L 01/22/2018 Mercury`— -- EPA 245 <0.0020 mg/L 01/22/2018_Y Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01086A Site: 1/10/2018 9:30 AM Solid/Sludge Aaron Hewett Test Method Results Date Analyzed Ammonia Nitrogen sin 4,500 NI13 c rnq/kq Total Kjeldahl Nitrogen (TKN) sto 4500 org a _ mg/kg Comment: Siudge residuals reported on a dry weight basis. Revised due to NH3 calculation error. Reviewed by: Report u� 2018-00�:27 Page 3 of BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled, January 10, 2018 Ocean Isle Beach WWTP Permit No. WQ0034513 Mineralization Rate 0.30 0.63 % Solids 6.57 pH Par�rneter to Mg/Kg dry We�g�i Pou�tds,�31t� Nitrogen (TKN) 7,680 76,800.000 153.600 Phosphorus 2,040 20,400.000 40.800 Potassium 0.746 7,460.000 14.920 PAN (injected)* 2.660 26,599.000 53.198 PAN (surface)* 2.420 24,199.000 48.398 Ammonia Nitrogen 0.480 4,800.000 9.600 Calcium 1.300 13,000.000 26.000 Calcium Carbonate Eq. --- --- --- Magnesiurn --- 5,320.000 10.640 Sodium --- 17,900.000 35.800 Sulfur --- --- --- Nitrate N 1 Nitrite N --- 199.000 0.398 Barium --- --- Chloride --- Iron --- --- ---eai[g Aluminum - 3,020.00 6.040 Arsenic --- 47.30 0.095 75 Cadmium --- 78.70 0.157 85 Chromium --- 78.70 0.157 --- Copper -- 235.00 0.470 4,300 Lead --- 78.70 0.157 840 Mercury --- 2,700 0.005 57 Molybdenum --- 47,30 0.095 75 Nickel --- 78.70 0.157 420 Selenium --- 78.70 0.157 100 Zinc -- 684.00 1.368 7,500 F iwi rochcm : 2018-00451 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Ratc)(TKN-Ammonia N) + Ammonia N 1- Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N a Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. re"novirochem 6 ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/);ax 255-A Wilmington Highway, Jacksonville, NC 28540 4 910.347.5843 Lab/Pax info(a_�cnvironnlen take lieinist>.com Date of Report: Feb 20, 2018 Customer PO #: Customer ID: 08100011 Report #: 2018-00451 Project ID: Ocean Isle Beach Lab ID Sample ID: 18-01154 Site: Sludge Test Collect DatelTime 1/10/2018 9:53 AM Method Matrix Sampled by Solid/Sludge Scott Leonard Results Date Analyzed Chlordane SW 846 Method 8081B)3510 <0.05 mg/L 01/18/2018 Endrin SW 846 Method 8081613510 <0, 0005 mg/L 01118/2018 Heptachlor SW 846 Method 8081 B13510 <0.0005 mg/L 01/1812018 Heptachlor epoxide SW 846 Method 80816/3510 <0.0005 mg/L 01/18/2018 Lindane SW 846 Method 8081813510 <0.0005 mg/L 01/18/2018 Methoxychlor SW 846 Method 80816/3510 <0.0005 mg/L 01118/2018 Toxaphene SW 846 Method 8081 B/3510 <0.05 mg/L 01/18/2018 1,4-pichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,5 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 01/19/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8 2 7 0135 1 0 <0.050 mg/L 01/19/2018 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 Hexachloroethane (TCLP) SW 848 method 8270!3510 <0.050 mg/L 01/19/2018 m + p -Cresol (TCLP) SW 646 method 6270/3510 <0.050 mg/L 01/19/2018 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 o -Cresol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 01/19/2018 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/19/2018 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,5 -TP SW846 Method 8151A <0.003 mg/L 01/18/2018 2,4-D SW846 Method 8151A <0.003 mg/L 01/18/2018 1,1-Dichloroethylene SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 01/2612018 Benzene SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 Report C 2018-00451 Page 1 of 3 t ANALYTICAL & CONSULTING., CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Environmental Chemists, Inc, 6602 Windmill Way, Wiliningtan, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax 710 Bowsertown Road, Mantco, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 285.10 • 910.347.5843 tab/Fax it' foCa`em,ironmentaIcheniists.com Date of Report: Feb 20, 2018 Customer PO #: Customer ID: 08100011 Report #,- 2018-00451 Project ID: Ocean Isle Beach Chlorobenzene SW846 Method 8260!5030 <0,01 mg/L 01/26/2018 Chloroform SW846 Method 826015030 <0.01 mg/L 01126/2018 Methyl ethyl ketone SWa46 Method 6260/5030 <0.05 mg/L 01/26/2018 Tetrachloroethylene SW846 Method 8260/5030 <0 01 mg/L 01/26/2018 Trichloroethylene $w$46 Method $26015030 <0,01 mg/L 01/26/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 RCI EPA 200.7 <47.3 mg/kg 01/18/2018 Cyanide EPA 3354 <0.025 mglkg 01/22/2018 pH SM 4500 H B 6.57 units 01/23/2018 Sulfide SM 4.500 S D <0.05 mg/kg 01/22/2018 Ignitability SW 846 method 1010 >212 OF 02/02/2018 Sludge Residuals EPA 200.7 684 mg/kg 01/18/2018 Aluminum EPA 200.7 3020 mg/kg 01/18/2018 Arsenic Reanalyzed 2-16-18 EPA 200.7 <47.3 mg/kg 01118!2018 Cadmium EPA 200.7 <78.7 mg/kg 01/19/2018 Calcium EPA 200.7 13000 mg/kg 01/15/2018 Chromium EPA 200.7 <78.7 mg/kg 01/18/2018 Copper EPA 200.7 235 mg/kg 01/18/2018 Lead EPA 200.7 <78.7 mg/kg 01/18/2018 Magnesium EPA 200 7 5320 mg/kg 01/15/2018 Molybdenum Reanalyzed 2-16-18 EPA 200.7 <47.3 mg/kg 01/18/2018 Nickel EPA 200.7 <78.7mglkg 01/18/2018 Potassium EPA 200.7 7460 mg/kg 01/15/2018 Selenium EPA 200.7 <78.7mg/kg 01/18/2018 Sodium EPA 2007 17900 mg/kg 01/15/2018 Zinc EPA 200.7 684 mg/kg 01/18/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 76800 mg/kg 01/18/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 199 mg/kg 01/16/2018 Report M: 2 01 8-0 04 5 1 Page 2 of 3 9: 2018-00461 W Y Page 3 of 3 Environmental Chemists, Inc. a uqo. 6602- Wi nd nli I I W�l y, VVil ill 4 ngton, NC 28-105 4 910.:392.€)223 Lab , 910.392,44".NFax, 71013o�%F,,ci-totviiRoacl,vii)iito.�),NC-27954 2:5'?. A 73.5702 '..-)702 Lah./Fax 2,-�5� A Wilmington Ffiso ,�hwIN, )acknville, NC 28540 � 910.347-5843 Lab Tax ANALYTICAL & CONSULTING CHEMISTS 7 Brunswick County Public Utilities Date of Report: Feb 20, 2018 Post Office Box 249 Customer PO #,. Bolivia NC 28422 Customer 10: 08100011 Attention: Donald Dixon Report #: 2018-00451 Project ID: Ocean Isle Beach Total Solids (%) SM 2540 8 0,63% 01111/2018 Ammonia Nitrogen SM 4500 NH3 C 4800 mg/kg 01/2112018 Total Phosphorus SM 4500 P F 20400 mg/kg 01/18/2018 Mercury SW846 747 18 <2,70 mg/kg 01/15/2018 TCLP Metals Arsenic EPA 2001 <1.0 mg/L 01/22/2018 Barium EPA 200.7 <1.0 mg/L 01/22/2018 Cadmium EPA 20D 7 <1.0 mg/L 01/22/2018 Chromium EPA 200.7 <1.0 mg/L 01/2212018 Lead EPA 2001 <1.0 mg/L 01/22/2018 Selenium EPA 200.7 <1.0 mg/L 01/22/2018 Silver EPA 200.7 <1.0 mg/L 01/22/2018 Mercury EPA 245.1 <0.0020mg/L 01/22/2018 Comment: Suldge residuals reported on a dry weight basis. Reviewed by: 9: 2018-00461 W Y Page 3 of 3 d o� 'v_ Ym /Q.I♦�� Y4� � w�/y W _ ro 46 1 .i N N Ca 'A Ca a � A y sl— LAB FD NUMBER IE � d o � y Sample �. Type Composite or Q Grab Container (PorG) Chlorine_ mg/L w C NONE 10 HCL H280, Cp MN03 C NUOR TEUO QTHT?R r:} V o� ro � W _ ro 46 1 .i N N Ca 'A Ca a � (f y n LAB FD NUMBER IE � d o � y Sample �. Type Composite or Q Grab Container (PorG) Chlorine_ mg/L w C NONE 10 HCL H280, Cp MN03 C NUOR TEUO QTHT?R r:} V o� W 46 1 .i N N Ca 'A Ca a � (f y BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 10, 2018 Sea Trail WWTN+ Permit No. WQ0034513 Mineralization Rate 0.30 0.68 % Solids 7.62 pH Lnvircchem: 2018-00448 xDetermination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N r Nitrite N = % PAN Surface Application: (Mineralization lZate)(TKN-Ammonia N) + (0,5)(Ammonia N) + Nitrate N W Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 4U11D Nitrogen (TKN) 16.600 166,000.000 332,000 Phosphorus 5.780 57,800,000 115.600 Potassium 0.659 6,590.000 13.180 PAN (injected)* 6.871 68,708.000 137.416 PAN (surface)* 6.649 66,488.000 132.976 Ammonia Nitrogen 0.444 4,440.000 8.880 Calcium 9.090 90,900,000 181.800 Calcium Carbonate Fq. --- --- Magnesium -- 5,000.000 10.000 Sodium --- 13,200.000 26.400 Sulfur --- --- Nitrate N 1 Nitrite N --- 15,800.000 31.600 Barium Chloride --- --- --- --- SAR Iron Aluminum --- 8,310.00 16.620 „hI Arsenic --- 72.10 0,144 75 Cadmium --- 72.10 0.144 85 Chromium --- 72.10 0.144 --- Copper - - 551.00 1.102 4,300 Lead --- 72,10 0.144 840 Mercury --- 2.500 OM5 57 Molybdenum --- 72.10 0,144 75 Nickel --- 72.10 0.144 420 Selenium --- 72.10 0.144 100 Zinc --- 1,150.00 2.300 7,500 Lnvircchem: 2018-00448 xDetermination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N r Nitrite N = % PAN Surface Application: (Mineralization lZate)(TKN-Ammonia N) + (0,5)(Ammonia N) + Nitrate N W Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. €x � y g,Environmental Chemists, Inc. ` tt10;�7"�~' a, <, r v, ;,fir s ��`•, IN- W1,11,111,111,40 [h-<I r, 1 sal ,-irlk to N( ioL, t)10 '92 f 7 ? i L 11r 1" r 11.1 I }lvsi rt x !1 I« Iii t E !!7lc c) �( ) 1 7. ?i (I' i 7h i r ax a 3 ; :i 2.)5--A 1�'1'i1!1)i11Igt�7i'i f der !7t�� 14, 1�7<"k_.ii,.� Ill(, NC 285 1) )1.0.>4'7.58,1 , [ ,[b §=�tx ANALYTICAL & CONSULTING CHEMISTS 1171[);il,en4lr;l:ilt3C 11(81�t1caYlltil�,Ct1f71 Brunswick County Public Utilities Date of Report: Feb 06, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer 1D: 08100011 Attention: Donald Dixon Report #: 2018-00448 Project ID: Sea Trail Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01151 Site: Sludge 1/10/2018 8:43 AM Solid/Sludge C. HumpHrey Test Method Results Date Analyzed Chlordane SW 646 Method 8o818/3510 <0.05 mg/L 01/18/2018 Endrin SW 846 Method 8081#313510 <0.0005 mg/L 01/18/2018 Heptachlor SW 846 Method 6081813510 <0.0005 mg/L 01/18/2018 Heptachlor epoxide SW 846 Method 8081B13510 <0,0005 rmg/L 01/18/2018 Lindane SW 846 Method 8081613510 <Q,0005 mg/L 01/18/2018 Methoxychlor SW 846 Method 8081 81351 0 <0.0005 mg/L 01/18/2018 Toxaphene SW 846 Method 80818/3510 <0.05 mg/L 01/18/2018 1,4 -Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 2,4,5 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Hexachloro-1,3-butadiene (TCLP) SW846rnethod827013510 <0.050mg/L 01/19/2018 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Hexachloroethane (TCLP) SW 546 method 8270/3510 <0.050 mg/L 01/19/2018 m + p -Cresol (TCLP) SW 848 method 8270/3510 <0.050 mg/L 01119/2018 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 o -Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2098 Pentachlorophenol (TCLP) SW 846 method 8270!3510 <0.250 mq/L 01/19/2018 Pyridine (TCLP) SW 848 method 827013510 <0.050 mg/L 01/19/2018 2,4,5 -TP SW846 Method 6151A <0.003 mg/L 01/18/2018 2,4-D SW846 Method 8151A <0.003 mg/L 01/18/2018 1,1-Dichloroethylene SW846 Method 826015030 <0.01 mg/L 01/26/2018 1,2-Dichloroethane SW846 Method 826015030 <Q,01 mq/L 01/26/2018 Benzene SW846 Method 8260!5030 <0.01 mg/L 01/26/2018 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 Report u 2018-00448 Pace 1 of 3 nnvia Chemists,Aal onmei ('60, Winch/-,iIi t!E'�t}'. Wilmillot n 2840' 9 3914l' 1 5 - Il 1f) Nowa ,(,itlwn ko,id 1f<:tt€ rt NC_ -27,93-1 -. 25' 'i ', (3? -a3 , f,.X < '. A 1ti'ilt lilt Fi,i Ili 11�� ;� J,ii k5rt11ti�i11u, �� ,.218 4i.) ff 910.'347. 4, . i643,1 -ab; ANALYTICAL & CONSULTING CHEMISTS lit; r;c;;r it y;1'tt tttalcl:e;; ist .cc ;tt Brunswick County Public Utilities Date of Report: Feb 06, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00448 Project ID: Sea Trail Chlorobenzene SW846 Method 526015030 <0.01 mg/L 01/26/2018 Chloroform SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L 01/26/2018 Tetrachloroethylene SW846 Method 826015030 <0.01 mq/L 01/26/2018 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 01/26/2018 RCI Cyanide EPA 335.4 <0.025 mg/kg 01/22/2018 pH SM 4500 H B 7.62 units 01/23/2018 Sulfide SM 4500 s o <0.05 mg/kg 01/22/2018 Ignitability sW 846 method 1010 7212 °F 02/02/2018 Sludge Residuals Aluminum EPA 200 7 8310 mg/kg 01/1812018 Arsenic FPA 200.7 <72.1 mg/kg 01/18/2018 Cadmium EPA 200 7 <72.1 mg/kg 01/19/2018 Calcium EPA 200-7 90900 mg/kg 01/16/2018 Chromium EPA 200.7 <72.1 mg/kg 01/18/2018 Copper EPA 2003 551 mg/kg 01/18/2018 Lead EPA 200 7 <72.1 mg/kg 01/18/2018 Magnesium EPA 200.7 5000 mg/kg 01/16/2018 Molybdenum EPA 200.7 <72.1 mg/kg 01/18/2018 Nickel EPA 200.7 <72.1 mg/kg 01/18/2018 Potassium EPA 200.7 6590 mg/kg 01/24/2018 Selenium EPA 200 7 <72.1 mg/kg 01/1812018 Sodium EPA 200.7 13200 mg/kg 01/24/2018 Zinc EPA 200.7 1150 mg/kg 01/19/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 166000 mg/kg 01/18/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 15800 mg/kg 01/16/2018 Tota! Solids (%) SM 2540 s 0.68% 01/11/2018 Ammonia Nitrogen SM 4500 NH3 C 4440 mg/kg 01/21/2018 Report #:: 2015-00448 Paqe 2 of 3 -Environmental Chemists, Inc. 4 }y, 'in Vi NK. 241C'. gl!)392-322.3 L�Ai �rfT "710 3 3:x,5. ��c� i, R,)ad, ,A ? %0;�' ?� :4�3.-'ii )`l L„t',i Fax rt. 1< t;t; z \C i r 52. ".3i -A 1AVi1:11in ton % av„ Jack�o will NC 211'3=311 c11t}.. 1%,)8 i'i d1 1) /FaX ANALY'1"iCAL & CONSULTING CHEMISTS ifnr�r �i;�uon3uc�ruuicl:en�i�ts.coi3� Brunswick County Public Utilities Date of Report: Feb 06, 2018 Post Office Box 249 Customer PO M Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Hixon Report #: 2018-00448 Project ID: Sea Trai# Total Phosphorus SM 4500 P F 57800 mg/kg 01/19/2018 Mercury SM467471B <2.50 mg/kg 01/15/2018 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 01/22/2018 Barium EPA 200 7 <1.0 mq/L 01/22/2018 Cadmium EPA 200.7 <1,0mg/L 01/22/2018 Chromium EPA 200.7 <1.0 mg/L 01/22/2018 Lead EPA 200 7 <1.0 mg/L 01/22/2018 Selenium EPA 200.7 <1,O mg/L 01/22/2018 Silver EPA 200.7 <1.0 mg/L 01/22/2018 Mercury EPA 245.1 <0.0020 mg/L 01/22/2018 Comment: Sludge residuals reported on a dry weight basis Reviewed by: Report#:: 2018-00440.,�,.A�..d..�..,....�.�,,..�..,,�..,�...�,.....�...,,.,�.,,�.4.......��...�..,,n,.,,4.�_,.u....nv...�.ti..F,�.ww..,...�._wM",..,.,.�.,,.a.".W,.�..�"w.�,,.�,.,,...,,.�..-,,...�,.,,a,..�..�.. Pane 3 of 3 Z r= LL. t1F E 3 w 0 Le fi "Suw.- MR)AININN SOMI#Dft Inr Timm 19 'IR -romp Time _Q S - C4 . . ... ............ . . JU043PS" MorojosS. 10C. t -o ..... .. .. ................A . . ... ..... ... ..... . ........ pis rmo .. ..... .. . .......... ... I%otqr Ph Test ' / - 11 0 /C- -i-ernp c!wrenjod IiJT'it 411" U A, "az*w.,, $9343PN" Sorolow, INIc. W P- -1-, 0 " C) P- � t t--,- ,,__...... --,- Airoyimm Odkwo;: 39 o o o . . ... . . . . . . . . . . . . . .. . . . . . . I'mpmulro Owwod fix 095OL'. / 4� . . . ....... Irmp "A'I ..... . .. .......... ...... . .... . r . ...... ,24 Ifoor.111'est fjr2l V R 1,\ � C. .......... TOO. .... . . )roarw .. ...... ...... . .... . - ,24 MigrPh ' too Cod( ShldAa 0 WWTP . ......... ... 1-9 ............ A14j". ,-)Piro )-eq T imp c ow� 2.8 omp . ..... .... vim" County T *at. AMM6� *wvkmw4 Inc. ci e- � -�_Q V-,-, Cl , L' ........ . .. .. ... WWM Ap Tim . . ......... ......... . low'. , )f)eRw. . . . . . . . . . . imp Cocromfm ph Y- ."..1.....` ..... ... ........... -low 0 9 'Tompmary orm� A ........... . .......... -S T .. .... ... .................. AMO 09 Pk. . ........... I�Itm Ll 'Appixon"to wimp" (#Anlow� IWL or,, �q ............ ............ T 0. romp, ... . .... . ... . . . . . . . . . . . . . . . . .. . . . . . . . . . . ,2 Owir 71.1tv, 0 . ...... ... . -rmp (,,*orrft—*w Ph - - I *1111W W - 0 q ... ............ ... ... ... .. I ............. How Ph Tent, 17 NJ,P I =V L "Slowh wo^wm owsomo Am'. cf—)A (5 -r D f, c'I -e- 5 t 0 k,-- ............ ............ ... Tim ......... .. ........... . ..... ft.#mr Flo 'up.w. ... ... ...... . .. ......... . ............. 24 Uoqr.jPh Tewt, e cl Cop Sludge Source: [ IN, n__0 L _j �. s + STP Permit #: IV C- L4� 7 ` � Approximate Gallons: Date J 0 Time 5` Operator ft f'e Ph 1,59 Temperature Corrected Ph o, Temp--!(, - b C, V) , . 6 r r T Dade � -oi Time 0 S� Operator je Ph `), Temp `9, 9- - - __ Temperature Corrected Ph . 1-i 3 Date � C) ,_P I,0j Time 0 9 as- Operator YA14ew Ph - �.-i.►� b' Temperature Corrected Ph a rsck County Lime Stabilization Ph Test Results. Hagler: B10 -GREEN Services, Ince Sludge Source: WWTP Permit #e /V C O .Approximate Gallows: 3,11 1�0 Inftial Ph "Test Date Time 0 9 L � Operator—�� Ph ) ._, ' Temp_ja\_J_�� Temperature Corrected Ph Aa, Date . 1 ? 4 Time 0 _ S Operator�e ph—) � Temp Temperature Corrected Ph 24 Hour Ph Test Date J Time V Operators r1 Ph Temperature Corrected Ph Slugs Sm= .. i h Ph Test o-5 -iy - JLL+ ,..t `damp' F&MpiUM,BMW.'E-�- 4�'''JF�°� n� 24 Hour Fb Test 'rime .-LM opwator i f /1191 Wjtr`s 110 (� IM Wom so rffi�lorllyz WWTP _ _ --- _ y_ . M: ��. - raw� Temp a. M 0 ,3-.8_20$ 'ems a AC 2• R metes_ e� T Y- 4�. a _2 �pt rme I Em Lb"O SUbiln jah #40ow"', 004mm ....... ... 2 rib .. .................... ... . .. ...... .. .. 24,Roiwr.rh ..... .. ... - loco� wwlp.p 2111 L 1 row, - Te -f c� ogna—lid �7 _dam A. p �iPh m g- % -Z w LOOS ftbifkgUM ph Tnt Rmulft Hadw. ma'asom s kF4�aq m V-',- — -- - �, A wwrP � -, -, a.-4- A _- ume -kw T" M. – - -2, &—. C*,mmmmm- opallm-f.el 4:0 ---------- ,Rhtr IVB ow, mm ACA-IV4"6-1-11-6 -re A. ]Brunswick County BIO -GREEN Sludge Source: WWTP Permit #. - 127.Approximate Gallons: (0 Initial Ph Test Date ja � LIPp e._ 9 L 4,5_ Operator Ph CZ -t3 Temp Temperature Corrected Ph1 -1-19 I k Date _jrj- A rBme_lqCQ_ Operator t - Ph Temp Temperature Corrected Ph � . � SECTION VI SOIL ANALYSIS REPORTS a C: m c a m z cv 0 "2 z _ y ,o CF) N } q 0 C Z LL 0. W O z m Ci O p m z 0 O dl .. � a c N c C,4 Lci C 3 v U N (n O U 0 CO m -0 (, N Q O Z N _T C b G Ul N Cl) 3 0— Orn C (D N .O m C v U U Nr -Z r 67 a' N N C L m aN E G o mn tm m M Q ri C CO N Y mCD � U U m m N gc N 0 O O CL � N r � � 3 E z o 0 LLI ii C U M z L `= c0 di C) d O Z i C) ILOO LO N CC Q R _ N O (7 N C J C O V M o CD — co d CL a' ... o R EE p C C V Uf O m Z = CL N O p 0 -0 C w m U u m 2 CD o E E U Q o j L) 0 N Q �+ ■ iny C A O .J m CO 0 4. V\ U o E o C — c*>w o Cn V cd O 44,%f'1111 /��, kfr 3 `q' T Q o z /q INVA fn ` J a C: m c a m ID c2 I ILL p' j.•' G. N O N Ol N d T 13 � a r � N E O = r N O N O Q O T .A U N Q V x X X _, O a C1 O f6 N a s N N x 'p [6 N N N E O N -O U N -0 _ T f.5 U L N [�6 '- U — S] 2] OT p — — N X '"' 7 9 O O X (D .EE. O N N N O '�' [Q/J O M02 -0 U U C N O N L c.i (9 (6 f6 f�6 N .V C d d i-. O L> C W W N N fIJ LU 0) 0) m t] X U D 0 U .p U U f6 lO f0 f6 O 2 tt3 W O O= .0) U N x O f6 O X U3 O O C C (if ,.. Q .- O) = L L Q fU O 'Yi O-o o o U U O Q Q O_ o E E 2i 2 E C 0 C Q U O. d N N ii �N G c N rN z a a - n o Z a s M C7 OQ T ammu�ciw��c a c��zzzocnai�NN L u m oc CD o} w 0 o a� s a ,� m N �... m O O d L O w aul I C T7 n O U m f- O C7 W o c C O A 4 0 0 c r m L o C7 m p O w L N {� TS N {n =_ 'L7 O LO� L C O 4q 7 Cr tm 7 d (1)x E O C N C@ 0O 'cn +4 QS -p tTf Q. C N V' U; Q y rn c 3: m Lo o E �. (D0 Q_�' = m oA oZ co O en 7- Q) cn _ U) p — iC L% v cn O_ i co E w E E M N .Q o ro o Q v a U) a c y c a m c _ a E o �' a� U) 'q `° N N m ro O ro m cw m a> ro E ro i O W) of 07 O ai Z rn �a b1 o Q N E u)ro C W. C� Cl Q- VJ = C C � o T N M f/3 N L C "Cy M 014 � (n QI LO 7- 0 'C m a E Ca `� a� w o m � of a, o o Q °o c D _ c �.o , mom, W y o E j m' o c`5 W p �1 C .w- CO to C 03 �. W U O ai 0 E scn c ro , c O o c r ai N E v o as o o c .� (DO I 5 E @ !Z u1 -d o E a •d o O C Zf o a) m U) L p m E w "0 Q o w as E m ui o p O fl E a o 0 o is m E m E c E cs U ¢oi N (D 0L1 d o Q = Q. 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R U � O �' C N O -� N � � � � � O O � O ON C N N SU .� m N U w tlJ OO N ,Q O O .r � N i.. n — V ID a Y o c w A co o �s t� v v o v c43 o a)O M iS1 x�-. U° O O .� .-- C "C f[5 W r7 O N � 7 CL U_ � rOy) V N -R tY:7 0� �� 0O p O a) c "CS M— 7 'C 0 N Q la c u) C N _.. C C) O C O 7 S 6 0 0,., C L1 D 2 a) ITf N U .r � 4-- T 3 a) of "-• U w C7) a) > U _ ur C r E O U WCO a) O _C X �.. m COi .0 ro Y �r mar L a 7 U) a) 'M U Z c m O E m J w O l l r . N LL c c vO (� (6 0 ro O a� L. C c t. a) � Ci E o E"" N All Biosolids sources land applied by BioGreen Services, Inc. (BioGreen) during the 2018 calendar year were lime stabilized to meet Pathogen and Vector Attraction Reduction monitoring. Therefore, lime additions are being made to fields applied to through land application.