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WQ0034468_Residual Annual Report 2018_20190227
INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0034468 SUBMITTAL DATED: 2/21/2019 Project Contact Information Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Rob Willcox Email Address* Phone Number* rob@Wllcoxmabesoil.com 336-339-9128 Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0034468 Reviewer* Troy Doby Permittee* John Nichols Facility Name * Brunswick County Public Utilities County* Brunswick r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. 2018 CLASS A ANNUAL REPORT - Brunswick 75.12 MB County- WQ0034468-signed.pdf Application Forint Engineering Rans, Specifications, Calculations, Etc.) For nein and modification permit applications, the paper copy is required to be subrmtted to the Division- Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follmtLring= • Application Farm • All rulevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extra set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) T:di shall ae mailed to the followins aPrl-: s: By pclal ser- lce: Divisron o= % ater Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 2.7699-1613 By Courier/Special Delivery: Division of Water Resources- Non -Discharge Branch AZ Nathaniel Thornburg- 9th Floor, Office #942WN 512 N_ Salisbury St_ Ralei NC 27604 For que€tions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdenr_gov or Sonia Graves at 919.707.3657 or Sonia.Graves(apcdenr.. * I;W By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/21/2019 2018 ANNUAL REPORT BRUNSWICK COUNTY PUBLIC UTILITIES DISTRIBUTION OF CLASS A RESIDUALS NON -DISCHARGE PERMIT NO. WQ0034468 Prepared For: Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 February 2019 willcox&mabe SOI L SOLUTIONS February 21, 2019 N.C. Department of Environmental Quality Division of Water Resources - Non -Discharge Branch 512 North Salisbury Street, 9' Floor, Office # 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Branch Reference: 2018 ANNUAL REPORT Brunswick County Public Utilities Non -Discharge Permit No. WQ0034468 WMSS Project No. 15-04, Phase: 06 Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit for Brunswick County on behalf of Brunswick County. WMSS compiled this report using data provided by Brunswick County and BioGreen Services, Inc. This data includes: 1) Class A Annual Distribution and Marketing / Surface Disposal Certification and Summary Form, 2) Annual Residual Sampling Summary Form, 3) Annual Pathogen and Vector Attraction Reduction Form (503), and 4) Analytical Data. Brunswick County distributed a total of 835.88 Dry Tons of Biosolids under Permit No. WQ0034468 during the 2018 calendar year (West Brunswick Regional WWTP — 469.87 Dry Tons, and Northeast Brunswick WWTP — 366.01 Dry Tons). Based upon the dry tons distributed, both the West Brunswick Regional WWTP and Northeast Brunswick WWTP were in the monitoring frequency of once per quarter (4 times per year) as established in 40 CFR Part 503 and 15A NCAC 02T .1111. It should be noted that both facilities were in compliance with having analytical for 4 times per year, however the 4 samples for some of the required monitoring were not within each specific quarter. If there is any further information required or questions regarding this distribution program please do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations with Brunswick County Public Utilities at (910) 253-2485 or Rob Willcox with Willcox & Mabe Soil Solutions, PLLC at (336) 339-9128 for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Rob Willcox, L.S.S. Partner / Soil Scientist Enclosure(s) cc: Brunswick County Public Utilities Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 06 - 2018 Annual Report\2018 Annual Report\Class A\2018 CLASS A ANNUAL REPORT - Brunswick County.doc Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 NC DISTRIBUTION OF CLASS A RESIDUALS PERMIT NO. WQ0034468 WEST BRUNSWICK REGIONAL WWTP PERMIT NO. WQ0023693 NORTHEAST BRUNSWICK REGIONAL WWTP NPDES PERMIT NO. NCO086819 Mr. Donald Dixon, Deputy Director of Wastewater Operations Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 (910) 253-2485 2018 West Brunswick Regional WWTP Dry Tons - 469.87 2018 Northeast Brunswick Regional WWTP Dry Tons - 366.01 Total Dry Tons 835.88 2018 West Brunswick Regional WWTP Dry Metric Tons 426.17 2018 Northeast Brunswick Regional WWTP Dry Metric Tons 331.97 Total Dry Metric Tons 758.14 TABLE OF CONTENTS SECTION NO. TITLE Class A Distribution and Marketing / Surface Disposal Certification Summary Form Form DMSDF H Annual Residual Sampling Summary Form Form RSSF III Annual Pathogen and Vector Attraction Reduction Form (503 Rules) Form PVRF 503 N Lab Sheets Analytical Data Class A Distribution and Marketing / Surface Disposal Certification Summary Form FORM DMSDF A. 3 3 3 c a� N 3 z a a O a O F =. i ❑0� M v O N N N N N N N N N N N N N N N N N N N N N N N N � rn O 0 cid N O O C% 00 00 n 00 M t,- \D LKoo '� 00 O N ono "o n O r n M N %D 00 N Vim' 41 a ? � ' a Y T n 0 0 0 m m t� to, T N E E i z ar 8E 0 0 0 G7 W F°, 0 0. f N oo 00 w 00 n� n o N ono a .O n M {,� w; n `o M N N" W � � Q F O v I Q) � m 'E' 0 -z' N N � N Q � m *, v� w W A � A rA 01 dM` CMr OM� C7, CM C7,�� ca mM�M 0 0 0 N N 0 0 NNN 0 0 0 N 0 N 0 N 0 N 0 pG c d yNNN o u= C0. a o a aa a oo a a o a 0 a 0 a o a O a o a 0 00 y 3 3 3 3 3 3 3 3 3 3 3 3 L O w W � F Q .r V _ Q M CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0034468 FACILITY NAME: West Brunswick Regional WWTP PHONE: 910-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) 11 Distribution and Marketing (camnlete Parte A- and Rl Amendments) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 DENR FORM DMSDF (Supp) (12/2006) Part Ax: Part Bx: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Residual In Product Out Bulking Agent Volume (dry tons) Name(s) Intended use(s) January WQ0023693 3.86 Harvey Bell 3.86 Fertilizer February WQ0023693 6.18 E. Robinson 6.18 Fertilizer February WQ0023693 30.13 D. Clemmons 30.13 Fertilizer February WQ0023693 29.35 Clyde Galloway 29.35 Fertilizer March WQ0023693 16.99 Bennie Smith 16.99 Fertilizer March WQ0023693 25.49 BS Roberts 25.49 Fertilizer March WQ0023693 13.90 J. Tennant 13.90 Fertilizer May WQ0023693 3.59 Albert Hughes 3.59 Fertilizer July WQ0023693 7.22 Frank Galloway 7.22 Fertilizer August WQ0023693 19.02 Harvey Bell 19.02 Fertilizer August WQ0023693 51.16 L. Lewis 51.16 Fertilizer August WQ0023693 11.81 Pearly Vereen 11.81 Fertilizer September WQ0023693 5.90 A. Clemmons 5.90 Fertilizer October WQ0023693 59.33 Clyde Galloway 59.33 Fertilizer October WQ0023693 3.36 A. Clemmons 3.36 Fertilizer Totals: Annual (dry tons): 0 0 287.29 287.29 Amendments) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 DENR FORM DMSDF (Supp) (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0034468 FACILITY NAME: Northeast Brunswick Regional W WTP PHONE: 910-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb - Wastewater Superintendent FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) 0 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar vear? Yes n No 1-1 --im. if Nn aloin Hams e R r and .. r"f , f I,o] ,.., Month Part A*: Sources(s) (include NPDES # if applicable) Volume (dry tons) Amendment) Bulking Agent Residual In Product Out Part B*: Recipient Information Name(s) Volume (dry tons) Intended use(s) January February NCO086819 8.02 E. Robinson 8.02 Fertilizer March NCO086819 24.05 B. Smith 24.05 Fertilizer April May NCO086819 NCO086819 47.52 6.07 A. Clemmons B. Smith 47.52 6.07 Fertilizer Fertilizer June NCO086819 5.06 Tom Maultsby 5.06 Fertilizer July NCO086819 14.88 Tom Maultsby 14.88 Fertilizer August NCO086819 24.80 Harvey Bell 24.80 Fertilizer September NCO086819 397 Pearly Vereen 3.97 Fertilizer October NCO086819 78.02 A. Clemmons 78.02 Fertilizer November December Total from FORM DMSDF (sup) 0 0153.62 153.62 Totals: Annual (dry tons): 0 0 1 366.01 1 366.01 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit El Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No 0, If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 y fZ Signature of Pe ittee Date Signature of Preparer** (if different from Permittee) "Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102 (26) Date DENR FORM DMSDF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0034468 FACILITY NAME: Northeast Brunswick Regional WWTP PHONE: 910-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) 0 Distribution and Marketing (complete Parts A. and B) Part Ax: Part Bx: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Residual In Bulking Agent Product Out Names) Volume (dry Intended use(s) tons) February NCO086819 41.42 D. Clemmons 41.42 Fertilizer March NCO086819 8.02 J. Tennant 8.02 Fertilizer March NCO086819 5.35 Harvey Bell 5.35 Fertilizer May NCO086819 1.01 Albert Hughes 1.01 Fertilizer May NCO086819 5.06 L. Lewis 5.06 Fertilizer July NCO086819 2.98 Frank Galloway 2.98 Fertilizer August NC0486819 37.70 Pearly Vereen 37.70 Fertilizer September NCO086819 17.86 A. Clemmons 17.86 Fertilizer October NCO086819 34.22 Clyde Galloway 34.22 Fertilizer Totals: Annual (dry tons): 0 0 153.62 153.62 Amendment(s) used: Bulking Agent(s) used: ' If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) DENR FORM DMSDF (Supp) (12/2006) BRUNSWICK COUNTY ADMINISTRATION BRUNSWICK COUNTY GOVERNMENT CENTER DAVID R, SANDIFER COUNTY ADMINISTRATION BUILDING 30 GOVERNMENT CENTER DRIVE, N -F, MAILING AI]DUSS: BOLIVIA, NORTH CAROLINA 28422 TFUPHONF: (91.0) 253-2000 POST OmcF Box 249 (804) 442-7033 BOLIVIA, NOR'T'H CAROLINA 28422 FAx (910) 253-2022 July 30, 2018 Mr. William L. Pinnix, P.E. Director of Engineering Mr. John Nichols, P.E., Director of Public Utilities Re: County Signatory Authority Dear Mr. Pinnix and Mr. Nichols: You are hereby authorized to sign the following permit applications and certification related documents: • NCDEQ-PWSS Water Permit Applications • NCDEQ-DWQ Sewer Permit Applications • NCDEQ-DWQ FTSE -04/I6 Sewer Flow Tracking Applications • NCDOT Encroachment Permit Applications • County Letter (ref contractor's bond) required for the NCDOT Encroachment Permit • Partial and ! or Final Applicant's Certifications for Water Main Extensions • Partial and / or Final Applicant's Certifications for Sewer Main Extensions • NCDEMLR — Land Quality Sedimentation & Erosion Control Permit Applications (for County CIP projects) Please let me know if you have any questions. Sincerely, Ann B. Hardy County Manager Annual Residual Sampling Summary Form FORM RSSF ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WQ0034468 Brunswick County WQ0023693 WWTP Name: West Brunswick Regional WWTP Residual Analvsis Data Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. Parameter (mg/kg) Conc. Limit {mg/kg)a Sample or Composite Date 0 I /10118 09/28/ 18 10/03/18 11/14/18 Percent Solids {%) NA 2.85 3.31 2.42 4.13 Arsenic 75 17.20 14.90 19.80 12.40 Cadmium 85 17.20 14.90 19.80 12.40 Chromium NA 55.40 33.20 50.40 38.30 Copper 4,300 547.00 447.00 653.00 567.00 Lead 840 29.50 17.90 25.80 25.20 Mercury 57 1.09 1.03 1.28 5.76 Molybdenum 75 17.20 14.90 19.80 12.40 Nickel 420 32.40 19.60 29.30 21.30 Selenium 100 17.20 14.90 19.80 12.40 Zinc 7,500 2,060 1,600 2,310 2,420 Total Phosphorus NA 62,600 44,100 2,520 2,370 TKN NA 91,200 86,500 123,000 76,600 Ammonia -Nitrogen NA 707.00 50,300 72,000 39,200 Nitrate and Nitrite NA 95.10 0.60 469.00 214.00 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T _1102 (26) pbNR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analv.-ds Data WQ0034468 Brunswick County WQ0023693 West Brunswick Regional WWTP Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." signature of Preparer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1 102 (26) Date DENR FORM RSSF - B (12/2006) Sample or Composite Date Parameter (mg/kg) 01/10/18 09/28/18 10/03/18 11/14/18 Aluminum 29,100 17,100 27,400 28,300 Calcium 30,600 24,900 37,800 1 44,300 Magnesium 4,630 4,170 5,700 8,980 pH 7.74 8.30 8.27 7.45 Potassium 6,110 5,500 8,550 7,380 Sodium 3,150 2,050 1 2,970 2,880 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." signature of Preparer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1 102 (26) Date DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WQ0034468 Brunswick County NCO086819 WWTP Name: Northeast Brunswick Regional WWTP Residual Analvsis Data Laboratory: I) 2) 3) 4) S) Environmental Chemists, Inc. Parameter (mg/kg) Cone. Limit (mg/kg)o Sample or Composite Date 01/10/18 03/28/18 07/26/18 11/01/18 Percent Solids (%) NA 4.93 3.73 3.66 5.05 Arsenic 75 10.80 13.50 13.50 10.70 Cadmium 85 10.80 13.50 13.50 10.70 Chromium NA 61.70 41.00 53.60 37.80 Copper 4,300 217.00 194.00 238.00 193.00 Lead 840 19.00 13.80 15.00 12.20 Mercury 57 0.446 0.429 0.519 0.396 Molybdenum 75 10.80 13.50 13.50 10.70 Nickel 420 34.10 25.50 30.90 23.80 Selenium 100 10.80 13.50 13.50 10.70 Zinc 7,500 1,220 1,060 997.00 956.00 Total Phosphorus NA 60,300 57,300 32,400 34,200 TKN NA 144,000 107,000 98,400 89,300 Ammonia -Nitrogen NA 46,200 65,800 52,600 40,600 Nitrate and Nitrite NA 91.40 5.83 201.00 152.00 " For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ignature of Preparer Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analvsis Data WQ0034468 Laboratory: Brunswick County Q 1 1 i 9 i_ J Northeast Brunswick Regional WWTP 3) 4) 5) Environmental Chemists, Inc. " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." signature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T - 1 102 (26) Date DENR FORM RSSF - B (12/2006) Sample or Composite Date Parameter (mg/kg) 01/10/18 03/28/18 07/26/18 11/01/18 Aluminum 6,090 6,380 8,060 656 Calcium 19,500 16,500 1 16,600 17,900 Magnesium 8,820 6.090 3,930 5,070 pH 7.29 7.41 7.36 8.05 Potassium 13,500 13,000 10,400 8,550 Sodium 1,830 1,820 1,730 1,630 " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." signature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T - 1 102 (26) Date DENR FORM RSSF - B (12/2006) Annual Pathogen and Vector Attraction Reduction Form - (503 Rules) FORM PVRF 503 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WWTP Name: West Brunswick Regional WWTP WQ Permit Number: NPDES Number: WQ0034468 WQ0023693 Monitoring Period: From 1/1/2018 To 3/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative l ❑ Alternative 2 ❑ Alternative 3 ❑ ❑ Alternative 4 ❑ Alternative 5 El Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Furtlrer Reduce Patl►ogens": Compost ❑ fleat Drying ❑ HeatTreatment ❑ 7`llemlophilic 0 Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative I ❑ Altemative 2 ❑ If applicable to alternative performed (Class 13 only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Conlpastin� El Aerobic l:)igestion ❑ Anaerobic Digestion ❑ _. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Alt. 9 (Injection) Allowable Level Pathogen Density � Y Number of Frequency Sample Analytical Parameter in Sludge Excee- deuces of Analysis Type Tech-nique Minimum Geo. Mean Maxirnu� Units 2 x 10 to the MPN 6th power per grarn of Fecal Coliform total solids C1"U 1000 tnpn per gram MPN/ of total solid (dry 7 7 8 0 Quarterly Grab SM9221 CE weight) Gram Salmonella bacteria 3 MPN per 4 grarns (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed - Alt, I erformed: Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) El lAlt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) D "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) 1-10-11-� Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1 102 (26) Date DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WWTP Name: West Brunswick Regional WWTP NPDFS Number: Monitoring Period: From 4/1/2018 To 6/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: WQ0034468 WQ0023693 Class A: Alternative 1 ❑ Alternative 2 ❑ 1 Alternative 3 ❑ ❑ Alternative 4 ❑ Alternative 5 El I Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 11'o 1'Drying, ElI-feat Treatment ❑ Thermophilic El Beta Ray ❑ Gramma Ray ❑ Pasteurization ❑ Class B: I Alternative 1 ❑ Allematrve 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Com posting ❑ jAerobic Digestion ❑ Anaerobic Digestion El- ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Alt_ 10 (Incorporation) Allowable Level Pathogen Density g y Number o Frequency Sample Analytical Parameter in Sludge g Excee- dentes of Analysis Type yp Teclr-ni ue Minimum Geo. Mean Maximum Units 2 x 10 to the MPN 6th power per grant of Fecal Coliform total solids CFU 1000 mpn per gram MPN/ of total solid (dry 45 46 46 0 Quarterly Grab SM9221 CE weight) Gram Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ All. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) El Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Dying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt_ 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name. West Brunswick Regional WWTP NPDCS Number: WQ0023693 Monitoring Period: From 7/1/201$ To 9/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ 1 Alternative 2 ❑ Alternative 3 ❑ ❑ Alternative 4 ❑ Altemative 5 ❑ Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ heat Drying ❑ Heat Treatment ❑ Thennophilic 0 Beta Ray ❑ Gamma Ray ❑ Pastetwization ❑ Class B: Alternative l L1Altcn]atn�c, � ❑ Y If applicable to alternative performed (CIass B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ I Alt. S (Drying - Unstable) If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Densis � Y Number o Gxcee- Frequency Sample Analytical Minimum Geo. Mean Maximum Units in Sludge deices of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per grain of Fecal Coliform total solids CFU 1000 mpn per gram MPN/ of total solid (dry 554 579 603 0 Quarterly Grab SM92210E, weight) Gram Salmonella bacteria:1 3 MPN per 4 grains (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.] (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) El JAIL 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. S (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) L7 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Narne and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Pcrmit Number: WQ0034468 WWTP Name: West Brunswick Regional WWTP Monitoring Period: From 10/1/2018 To NPDES Number: W00023693 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 ❑ ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ heat Drying ❑ I -neat `I`reatment ❑ Theriiophilic CI Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative I 0 Altemative 2 ❑ If applicable to alternative performed (Class B only) indicate "Prt>cess to Signilicailtly Reduce. Pathogens". Lime Stabilization ❑ Air Drying❑ Coni posting ❑ Aerobic Digestion ❑ Anaerobic Digestion - If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen DensityNum ef•o Excee- 1:'requency Sample Analytical Minimum Geo. Mean MaXiInLl Units in Sludge g dences of Analysis Type yp Tech-ni ue 9 2 x 10 to the MPN 6th power per gram of Decal Coliform total solids CF[J 1000 mpii per gram MPN/ of total solid (dry 61 64 67 0 Quarterly Grab SM922 € CE weight) Gram Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.] (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ 1Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date 'Preparer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T. 1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: NCO086819 Monitoring Period: From 1/1/2018 To 3/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ ❑ Alternative 4 ElAlternative 5 CD Alternative 6 11 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ heat Drying ❑ Ileat "treatment ❑ 'I'hemlophilic 0 Beta Ray ❑ Gamma Ray ❑ Pasterrr-izatiorr ❑ Class B: Alternative l ElAltenlative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Com posting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ Alt 7 (Drying - Stable) ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: ❑ Allowable Level Patho en Densit y Nunn er o frequency Sample Analytical Parameter� in Sludge Exeee- deuces of Analysis Type Tech-nique Minimum Geo. Mean Maximum Units 2 x 10 to the MPN 6th power per grain of Fecal Coliform total solids CPL 1000 mpn per grain MPN/ of total solid (dry 450 465 473 0 Quarterly Grab SM92210E weight) Grath Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) Q A]t. 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) D "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: Northeast Brunswick Regional WW`l'P NPI)ES Number: NCO086819 Monitoring Period: From 3/€12018 To 6/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Altemative 2 ❑ I Alternative 3 ❑ ❑ Alternative 4 ❑ Altemative 5 0 I Alternative 6 ❑ ❑ If applicable to alternative performed ((:lass A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying❑ Heat Treatment ❑ Thetinol}hilic CI Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Conn posting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: ❑ Allowable Level Pathogen Density Number oFrequency ❑ Sample Analytical Parameter i� Sludge g Excce- dentes of Analysis y Type Tech-ni ue q Minimum Geo. Mean MaximuE Units 2x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per grain MPN/ of total solid (dry 339 355 379 0 Quarterly Grab SM92210E weight) Gram Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) 0 Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) CD "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WWTP Name: Northeast Brunswick Regional WWTP WQ Permit Number: NPDCS Number: WQ0034468 NCO086819 Monitoring Period: From 7/1/2018 To 9/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 ❑ I Alternative 4 ❑ Alternative 5 ❑ Alten]ative 6 El If applicable to alternative pee forined ((,lass A only) indicate "Process to I'urtber lZeduce Pathogens": Compost ❑ 1 -feat Dying ❑ Heat Treatment ❑ Thennophilic CI Beta Ray ❑ Gamma Ray ❑ Past euricatlon ❑ Class B: Alternative I ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number Of ixece- ]l-equency of Analysis Sample 'Type Analytical Tecli-pique Minimum Geo. Mean Maximus Unitsdenccs Fecal Coliform 2 x 10 to the 6th power per grana of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 40 41 43 MPN/ Gram 0 Quarterly Grab SM9221C1' Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry Weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) [Q JAR. 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tian Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1102 (26) Date DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick Cminty WQ Permit Number: WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: Monitoring Period: From 10/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: WQ0034468 NCO086819 Class A: Altemative l El Altemative 2 ❑ 1 Alternative 3 ❑ ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce 11'atliogens": Compost ❑ bleat Drying ❑ Pleat Treatment ❑ 1 henliophllic ❑ ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative l ❑ Alternative 2 ❑ if applicable to alternative performed (Class 13 only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ lAerobic Digestion ❑ Anaerobic Digestion ❑ Alt. 9 (Injection) If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number oFrequency Excee- deuces of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximurnj Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 36 41 44 MPN/ Gram 0 Quarterly Grab SM92210E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grants total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) [Q I Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 1AIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Cl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been inet. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date SignatUre of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1 102 (26) Date DENR FORM PVRF 503 (12/2006) Lab Sheets ANALYTICAL DATA BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 10, 2018 West Brunswick Regional WWTP Mineralization Rate 0.30 2.85 % Solids 7.74 pl4 Permit No. WQ0034468 Nitrogen (TKN) 9.120 91,200.000 182.400 Phosphorus 6.260 62,600,000 125.200 Potassium 0,611 6,110.000 12.220 PAN (injected)* 2.795 27,950.000 55.900 PAN (surface)* 2.760 27,596.500 55.193 Ammonia Nitrogen 0.071 707.000 1.414 Calcium 3.060 30,600.000 61.200 Calcium Carbonate Eq. --- --- --- Magnesium --- 4,630.000 9.260 Sodium --- 3,150.000 6.300 Sulfur --- --- --- Nitrate N / Nitrite N --- 95.100 0.190 Barium --- --- --- SAR< Chloride --- --- --- 0 75 ]ron --- -- 1Ceiltng Conce>Is Aluminum --- 29,100.00 58.200 (MgIK) Arsenic --- 17.20 0.034 75 Cadmium --- 17.20 0.034 85 Chromium --- 55.40 0.111 --- Copper - 547.00 1.094 4,300 Lead --- 29.50 0.059 840 Mercury --- 1.090 0.002 57 Molybdenum --- 17.20 0.034 75 Nickel --- 32.40 0.065 420 Selenium --- 17.20 0.034 100 Zinc --- 2,060.00 4.120 7,500 Envirochem: 2018-00424 Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) -t- Ammonia N + Nitrate N -+ Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Chemists, Inc. << s a a (60 irldnlill 1h'n, lhtlll�ilzht�fi, NC.:1840; 911.3392.022—) Leib 910.392.442-1 I ar 7J(? J3uVN",0I tc7WI'! t�niuJ, Mo to a NC 27954 2;2.473.7,702 Lab �� � � ��" 1 ltiltttrl� ;fo,t IJi•;#nv,1r, jaci;xm�'ilJt '\C: 2,9540 ')1.03�i. 843 Ub l' Y•xx ANALYTICAL R CONSULT€NG CI4EMISTS itE'o';,:cttvirct�tmcnt,ii�lter,ls t,.�ont Brunswick County Public Utilities Post Office Sox 249 Bolivia NC 28422 Attention: Donald Rixon Date of Report: Feb 07, 2018 Customer PO #: Customer ID: 08100011 Report #: 2018-00424 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01093 Site: Sludge 1/10/2018 11:08 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Chlordane SW 846 Method 80811313510 <0.05 mg/L 01/18/2018 Endrin SW 846 Method 8081B/3510 <0•0005 mg/L 01/18/2018 Heptachlor 5W 846 Method 8081B13510 <0,0005 mg/L 01/18/2018 Heptachlor epoxide 5W 846 Method 80818/3510 <0.0005 mg/L 01/18/2018 Lindane SW 846 Method 80BIB13510 <0.0005 mg/L 01/18/2018 Methoxychlor SW 846 Method 8081 B13510 <0.0005 mg/L 01/18/2018 Toxaphene -W 846 Method 8081 B11510 <0.05 mg/L 01/18/2018 1,4 -Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 2,4,5 -Trichlorophenol (TCLP) SW 846 method 827013510 <0•050mg/L 01/19/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8274/3510 <0.050 mg/L 01/19/2018 Cresol (TCLP) SW 846 method 8270/3510 0.066 mg/L 01/19/2018 Hexachloro-1,3-butadiene (TCLP) SW 846 method 827013510 <0.050mg1L 01/19/2018 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 m + p -Cresol (TCLP) SW 846 method 827013510 0.066 mg/L 01/19/2018 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 o -Cresol (TCLP) SW 846 method 8 27013 5 1 0 <0, 050 mq/L 01/19/2018 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/19/2018 Pyridine (TCLP) SW 846 method 627013510 <0.050 mg1L 01/19/2018 2,4,5 -TP SW846 Method 8151A <0.003 mg/L 01/18/2018 2,4-D SW846 Method 8151A <0.003 mg/L 01/18/2018 1,1-Dichloroethylene SW846 Method 826015030 <D•01 mg/L 01/17/2018 1,2-Dichlorcethane SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Benzene SW846 Method 8260/5030 <0.01 mg/L 01/1712018 Carbon Tetrachloride SW846 Method82G615030 <0.01 mg/L 01/17/2018 Report #:. 2018-00424 Page 3 of 6 { K y. n �c .eta. Chemists, t t;[l} 417incla�Iill 1V<� r, bti'iliiain< < �� �t c n i l n, \C �0i )I{T: { ( 2+I 11 910 3)2. 4' I -a\ fiowso.rtow-71 R(c ad \9 3teEec , NC ?7954 '152.473-9702 Lab /lax „,A Wilmington fii)'hwal, Jacksonville, NIC 2.�5.?4(1 , 9I0347.;?bk.31..aL�ll�a� ANALYTICAL & CONSULTlNC CHEMISTS i;:li> a ctrvu'(rni��c,]uilc11c911i:;�.ti.i:nr!1 Brunswick County Public Utilities Date of Report: Feb 07, 2018 <0.0347 mg/kg Post Office Box 249 Customer PO #: SM 4500 S D Bolivia NC 28422 Customer ID: 08100011 Ignitability Attention: Donald Dixon Report #: 2018-00424 01/19/2018 Sludge Residuals Project ID: West Brunswick Regional WWTP Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Chloroform SW846 Method 826015030 <0.01 mg/L 01/17/2018 Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L 01/17/2018 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Trichloroethylene SW846 Methoc 8260/5030 <0.01 mq/L 01/17/2018 Vinyl Chloride SW646 Method 826015030 <0.01 mg/L 01/17/2018 RCI Cyanide EPA 335.4 <0.0347 mg/kg 01/16/2018 Sulfide SM 4500 S D 0.08 mg/kg 01/22/2018 Ignitability SW 846 method 1010 X212 OF 01/19/2018 Sludge Residuals Aluminum EPA 200 7 29100 mg/kg 01/19/2018 Arsenic EPA 200.7 <17.2mg/kg 01/18/2018 Cadmium EPA 200.7 <17.2 mg/kg 01/1912018 Calcium EPA 200.7 30600 mg/kg 01/15/2018 Chromium EPA 2007 55.4 mg/kg 01/18/2018 Copper EPA 200.7 547 mg/kg 01/18/2018 Lead EPA 2D0.7 29.5 mg/kg 01/18/2018 Magnesium EPA 200.7 4630 mg/kg 01/15/2018 Molybdenum EPA 200.7 <17.2 nag/kg 01/18/2018 Nickel EPA 200.7 32.4 mg/kg 01/18/2018 Potassium EPA 200 7 6110 mg/kg 01/15/2018 Selenium EPA 200.7 <17.2 mg/kg 01/18/2018 Sodium UA 200.7 3150 mg/kg 01/15/2018 Zinc PPA 2007 2060 mg/kg 01/18/2018 Total Kjeldahl Nitrogen (TKN) EPA 351 2 91200 mg/kg 01/17/2018 Nitrate+Nitrite-Nitrogen EPA 363.2 95.1 mg/kg 01/16/2018 Total Solids {%) SM 2540 B 2..85% 01/11/2018 pH SM 4500 H B 7.74 units 01/18/2018 Ammonia Nitrogen SM 4500 NH3 c 707 mg/kg 01/21/2018 Report #:: 2018-30420 ����� ��� ���, Page 4 of 5 lidilvironmental Chemists Inc. NC `'8.405 � �i1O.39' U �.; [_ th cll�) �)? i•3'� I ,ia i #[1 bovvw town Road, Wlitc o, i\;C 279514 2,2 255 1 kltl[11in ;fcirt Cli ;lt..}}, inci onvillc, ti'C?.S EU gi{1.31%.5b ),� [_iii/I ax ANALYTICAL & CONSULTING CHEMISTS ill 7 riven ironment:iicix.J1ii t� cn3>> Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00424 Project ID: West Brunswick Regional WWTP Total Phosphorus SM 4500 P F 62600 mg/kg 01/18/2018 Mercury SW846 74716 1.09 mg/kg 01/15/2018 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 01/30/2018 Barium EPA 200.7 <1.Omg/L 01/28/2018 Cadmium EPA 200 7 <1.0 mg/L 01/28/2018 Chromium EPA 200.7 <1.Omg/L 01/28/2018 Lead EPA 200.7 <1.0 mg/L 01/28/2018 Selenium EPA 200.7 <1.Qmg/L 01/28/2018 Silver EPA 200.7 <1.0mg/L 01/28/2018 Mercury EPA 245.1 <0.0020 mg/L 01/22/2018 Comment: Suldge residuals, except phi, reported on a dry weight basis Reviewed by:`z Report V: 2018-00424_a,..,o.....w..�.�.,..«.�.�.,.�..d.�,.�..�.�..��...:.:�....,spa.�.,e.•,.,�..w,.,,.,�.�,..,.a...r�...�.,��..�..m Page 5of5 .�..�.., BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: September 28, 2018 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.31 % Solids 8.3 D1-1 Nitrogen (TKN) 8.650 86,500.000 173.000 Phosphorus 4.410 44,100.000 88.200 Potassium 0,550 5,500.000 11.000 PAN (injected)* 6.116 61,160.600 122.321 PAN (surface)' 3.601 36,010.600 72.021 Ammonia Nitrogen 5.030 50,300.000 100.600 Calcium 2.490 24,900.000 49.800 Calcium Carbonate Eq. --- --- Magnesium --- 4,170.000 8.340 Sodium --- 2,050.000 4.100 Sulfur --- --- --- Nitrate N / Nitrite N - - 0.600 0.001 Barium --- --- ---AR Chloride --- -- --=. 0.57 _<:.._...' Iron - --- --- Cel tltg is Aluminum --- 17,100.00 34.200 (MglKgj Arsenic --- 14.90 0.030 75 Cadmium --- 14.90 0.030 85 Chromium --- 33.20 0.066 --- Copper --- 447.00 0.894 4,300 Lead --- 17.90 0.036 840 Mercury --- 1.030 0.002 57 Molybdenum --- 14.90 0.030 75 Nickel --- 19.60 0.039 420 Selenium --- 14.90 0.030 100 Zinc --- 1,600.00 3.200 7,500 E'nvirochcm; 2018-15974 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application, (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, lnc. 710 i),ow,wilov.,11 Ro"'d, M1111eo, V. ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Date of Report: Oct 29, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-15974 Project ID: West Brunswick Regionaf WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-40329 Site, Sludge 9/28/2018 1:30 PM Solid/Sludge Matt Henry Test Method Results Date Analyzed Chlordane SW 846 Method 8081 B13510 <0.03 mg/L 10/08/2018 Endrin SW 846 Method 8081 B/3510 <0.0005 mg/L 10108/2018 Heptachlor SW 846 Method 8081B/3610 <0.0005mg/L 10/08/2018 Heptachlor epoxide SW 846 Method 5081 B/351 0 <0.0005 mg/L 10/08/2018 Lindane SW 846 Method 8081 W3510 <0.0005 mg/L 10/08/2018 Methoxychlor SW 846 Method 80811313510 <D.0005 mg/L 10/08/2018 Toxaphene SW846Method 6081B/3510 <0.05 mg/L 10/08/2018 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0, 050 mg/L 10/05/2018 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/05/2018 2,4,6-Trichlorophenol (TCLP) SW 646 method 827013510 <0.050 mg/L 10/05/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/05/2018 Cresol (TCLP) SW 846 method 8270/3510 0.094 mg/L 10/05/2018 Hexachloro-1,3-butadiene (TCLP) SW 846 method 827013510 <0.050mg/L 10/05/2018 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/05/2018 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/0512018 rn + p-Cresol (TCLP) SW 846 method 8270/3510 0.094 mg/L 10/05/2018 Nitrobenzene (TCLP) SW 846 method $27013510 <0.050mg/L 10105/2018 o-Cresol (TCLP) SVV 846 method 8270/3510 <0.050 mg/L 10/05/2018 Pentachlorophenol (TCLP) $W 846 method 827013510 <0.250 mg/L 10105/2018 Pyridine (TCLP) SW 846 method 6270/3510 <0.050 mq/L 10/0512018 2,4,5-TP SW846 Method 8151A <0.003 rng1L 10/10/2018 2,4-D SW846 Method 8151A <0, 003 mg/L 10/10/2018 1,1-Dichlorcethylene SVVW Method 826016030 < 0.01 mg/L 10120/2018 1,2-Dichloroethane SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Benzene SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Carbon Tetrachloride SW846 Method 8260/5030 < 0.01 mg/L 10/2012018 Repert it: 2018-15974 Page 1 of 3 RCI Cyanide Environmental Chemists, Inc. 10/15/2018 Sulfide SM 4500 s o Iii) i� ibV 6Y. 1't lY?'Jil Roa(l, %1,inleo, 11X 71)5.1 10/17/2018 lgnitability 5:, -A V\Cii1)1nw)i1 ligh va\, ill l;l: i�Hll`I)i�, AC .2iS540 910-34"', 1 ANALYTICAL. & CONSULTING CHEWST5 ni:;(ir;c:3' it r,1n} i ; iIi i] i3;i5tti. un SW 846 method 9045D Brunswick County Public Utilities Date of Report: Oct 29, 2018 Sludge Residuals Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 17100mglkg Attention: Donald Dixon Report #: 2018-15974 EPA 200.7 <14.9 mg/kg Project ID: West Brunswick Regional WWTP Chlorobenzene SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Chloroform SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Methyl ethyl ketone SW846 Method 826015030 < 0.05 mg/L 10/20/2018 Tetrachloroethylene SW846 Method 8260/5030 < 0.01 mg/L 10/20/2018 Trichloroethylene SW848 Method 826015030 < 0,01 mg/L 10/20/2018 Vinyl Chloride SW846 Method 826015030 < 0.01 mg/L 10/20/2018 RCI Cyanide EPA 335.4 <0.05 mg/kg 10/15/2018 Sulfide SM 4500 s o <0.10 mg/kg 10/17/2018 lgnitability SW 846 method 1010 >215 OF 10/15/2018 pH SW 846 method 9045D 8.30 units 10/08/2018 Sludge Residuals Aluminum EPA 200.7 17100mglkg 10/11/2018 Arsenic EPA 200.7 <14.9 mg/kg 10/0912018 Cadmium EPA 200 7 <14.9 mg/kg 10/09/2018 Calcium EPA 200 7 24900 mg/kg 10/10/2018 Chromium EPA 200.7 33.2 mg/kg 10/09/2018 Copper EPA 200.7 447 mg/kg 10/09/2018 Lead EPA 200.7 17.9 mg/kg 10/09/2018 Magnesium EPA 200.7 4170 mg/kg 10/10/2018 Molybdenum EPA 200.7 <14.9 mg/kg 10/16/2018 Mickel EPA 2001 19.6 mg/kg 10/09/2018 Potassium EPA 200.7 5500 mg/kg 10/11/2018 Selenium EPA 200.7 <14.9 mg/kg 10/09/2018 Sodium EPA 200.7 2050 mg/kg 10/11/2018 Zinc EPA 200.7 1600 mg/kg 10/09/2018 Nitrate+Nitrite-Nitrogen EPA 353,2 <0.60 mg/kg 10/09/2018 Total Solids (%) SM 2540 0 3.31% 10/02/2018 Ammonia Nitrogen SM 4500 NH3 C 50300 mg/kg 10/09/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 org s 86500 mg/kg 10/09/2018 Report # 2018.15974 «,a�.�v�� .�,..�,,...,..�...a..... Page 2 of 3 .�,..�Y,.�..�. E nvironinental. Chemists, Inc. .N( 18.41:7 il(1_;�?O?231..ab c,l�i.3i'?-142A 71 i 13_>t,_;ctrtut`i Ru d,:M,wfl(m, NE:: 275'i}; 2ri2.. _3.;'7i)7 -1.53- A Vv I rtiF) iun I'Ik"! tvar, iacksotIv llc, V "ti540 , 9 M.3•l1v Fay ANALYTICAL $ CONSULTING CHEMISTS Brunswick County Public Utilities Date of Report: Oct 29, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-15974 Project ID: West Brunswick Regional WWTP Total Phosphorus SM 4500 P F 44100 mg/kg 10/16/2018 Mercury SW846 74718 1.03 mg/kg 10/23/2018 TCLP Metals Arsenic GPA 200.7 <1.0 mg/L 10/09/2018 Barium EPA 200.7 X1.0 mg/L 10/05/2018 Cadmium EPA 200.7 <1,0mg/L 10/05/2018 Chromium EPA 200.7 <1.0 mg/L 10/05/2018 Lead EPA 200 7 <1.0 mg1L 10/05/2018 Selenium EPA 200 7 <1.0 mg/L 10/09/2018 Silver EPA 200.7 <1.0 mg/L 10/05/2018 Mercury EPA 245.1 <0.0002mg/L 10/10/2018 Comment: Reviewed by: Repor; p: 2018-15974 Page 3 of 3 COUNTY OF BRUNSWICKQJ�6 r West Brunswick Regional Laboratory Public utilities Department `� 235 Grey Water Road Wastewater Treatment Division Suppl NC 2$4Fi2 Y CIA 46��! Phone: 910-755-7921 Pax: 910-755-7927 Sample Collection and Cham of Custody Collected By: Matthew Henn Report No.: _ Samp#e Type: I = Influent, E = Effluent, W = Wel(, ST = Stream. SO = Soil Si = SlioriP ()thar Sample Identification West Brunswick Regional Collection Sample Type SL Composite Container or Grab (Plastic or Glass) C P Chlorine mglL ���!I � LAB 10 NUMBERINONE1 PRESERVATION ANALYSIS REQUESTED DATE TIME TEMP 45'C XRCl/RIIResiduals HCI IHZSO4 HNO3 THIO OTHER TC 9/28/2018 1:30 PM G G C P G G C P G G C P G G C P G G C P G G C P G (T— C C P G G C P G G C P G G C P G G ATTENTION: Samples submitted for analysis forAmmonia, TKN, Cyanide, Phenol and all Bacteriologicais must be dechlorinated to a 0.2 ppm at time of collection Transfer Relinquished By - 2 DatelTime Received By: Date/Time 'Temperature when Received. Accepted: Reiecled: esa "i eAu `ed. Delivered By: j r Comments: pH BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 3, 2018 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 2.42 % SoIids 8.27 nll Nitrogen (TKN) 12.300 123,000.000 246.000 Phosphorus 0.252 2,520.000 5.040 Potassium 0.855 8,550.000 17.100 PAN (injected)* 8.777 87,769.000 175.538 PAN (surface)* 5.177 51,769.000 103.538 Ammonia Nitrogen 7.200 72,000.000 144.000 Calcium 3.780 37,800.000 75.600 Calcium Carbonate Eq. --- --- --- Magnesium --- 5,700.000 11.400 Sodium --- 2,970.000 5.940 Sulfur --- --- Nitrate N / Nitrite N --- 469.000 0.938 Barium --- --- Chloride --- --- ]ron - - �81Illg COCeII;,', Aluminum - 27,400.00 54.800 Arsenic --- 19.80 0.040 75 Cadmium -- 19.80 0.040 85 Chromium --- 50.40 0.101 --- Copper --- 653.00 1.306 4,300 Lead --- 25.80 0.052 840 Mercury --- 1.280 0.003 57 Molybdenum --- 19.80 0.040 75 Nickel --- 29.30 0.059 420 Selenium --- 19.80 0.040 100 Zinc --- 2,310.00 4.620 7,500 E:nvirochem: 2018-16162 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization hate)(TKN-Ammonia N) + Ammonia N -t Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits for calculation purposes. Erivironniental Chemists, Ine, Ma €t N( 27W;-,' A V I T i I 1 1 1 i I 1) k).:11,7 ah?.' -J.0,?1 a>. ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Date of Report: Oct 26, 2018 Post Office Box 249 Customer PO #, Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-16162 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-40859 Site: Sludge 10/3/2018 11:42 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Chlordane SW 846 Method 80816/3510 <0,03mg/L 10/18/2018 Endrin SW 846 Method 8081813510 <0.0005mg/L 10/18/2018 Heptachlor SW 848 Method 8081 x/3510 <0.0005 mg/L 10/18/2018 Heptachlor epoxide SW 846 Method 8081813510 <0.0005 mg/L 10118/2018 Lindane SW 846 Method 8061613510 <0.0005 mg/L 10/18/2018 Methoxychlor SW 846 Method 808B/3510 <0.0005mg/L 10/18/2018 Toxaphene 9VV 846 Method 8081813510 <0.05 mg/L 10/18/2018 1,4-Dichlorobenzene (TCLP) SW 846 method 8270136 10 <0.050 mg/L 10/17/2018 2,4,5-Trichlorophenol (TCLP) SW 346 method 8276Y351 0 <0.050 mg/L 10/17/2018 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/17/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/17/2018 Cresol (TCLP) SW 846 method 8270!3510 0.111 mg/L 10/17/2018 Hexachloro-1,3-butadiene (TCLP) SW 846 method 6270/3510 <0.050 mg/L 10/1712018 Hexachlorobenzene (TCLP) SW 846 method 8270/3610 <0.050 mg/L 10117/2018 Hexachloroethane (TCLP) SW 846 in ethod 8270/3510 <0.050 mg/L 10/1712018 rn + p-Cresol (TCLP) SW 846 method 8270/3510 0.111 mg/L 10/17/2018 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/1712018 o-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 10/17/2018 Pentachlorophenol (TCLP) SW a46 method 827013510 <0.250mg/L 10/17/2018 Pyridine (TCLP) SW846 method 827013510 <0.D50 mq/L 10/17/2018 2,4,5-TP SN1846 Method 8151 A <0.003 mg/L 10/18/2018 2,4-D SW646 Method 6151A <0.003mg/L 10/1812018 1, 1 -DicNoroethylene $W845 Method 825015030 < 0.01 mg/L 10/20/2018 1,2-Dichloroethane SW846 Method 8260/5030 < 0.01 mg/L 10/20/2018 Benzene SW846 Method 626015030 < 0.01 mg/L 10/20/2018 Carbon Tetrachloride SW846 MPthod 8260,5030 < 0.01 mg/L 10/20/2018 Repu; t;V 20i8-16162 Page 3 of 5 . ;t;:ai'r�' s s Environmental Chenusts, Inc. e W 4 ,ti o10"' 1ti'illdri';ll 11�ti}'. VV;Imin g toil. ;N(. 1>84 i� Lal? �il0 3«._.-11 2 `. Ili! )w L'Ilow I1 l% $,1,)( VVi1in,,(on l f;l;) 1c1'sl)Iw I , AA ^. 510 -, 17 ]"'A i f ax ANA[YTICAL. & CONSULTING CHRIISTS :tf, r`em in,nni .nZ MIo ti�i .-.:int Brunswick County Public Utilities Date of Report: Oct 26, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-16162 Project ID: West Brunswick Regional WWTP Chlorobenzene SW846 Method 826015030 <0.01 mg/L 10/20/2018 Chloroform SW846 Method 8260/8030 < 0.01 mg/L 10/20/2018 Methyl ethyl ketone SW846 Method 8260/6030 < 0.05 mg/L 10/20/2018 Tetrachloroethylene SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Trichloroethylene -SW846 Method 6260/5630 < 0.01 mg/L 10/20/2018 Vinyl Chloride SW846 Method 8260/5030 < 0.01 mg/L 10120/2018 RCI Cyanide EPA 335.4 <0.05 mg/kq 10/15/2018 Sulfide SM 4500 S o <0.10 mg/kg 10/17/2018 lgnitability SW 846 method 1010 >215 OF 10/15/2018 pH SW 846 Method 9045D 8.27 units 10/10/2018 Sludge Residuals Aluminum EPA 260.7 27400 mg/kg 10/11/2018 Arsenic EPA 200 7 <19.8 mg/kg 10109/2018 Cadmium EPA 200.7 <19.8 mg/kg 10/09/2018 Calcium EPA 200 7 37800 mg/kg 10/10/2018 Chromium EPA 200 7 50.4 mg/kg 10/09/2018 Copper EPA 200.7 653 mg/kg 10/09/2018 Lead EPA 200.7 25.8 mg/kg 10/09/2018 Magnesium EPA 200.7 5700 mg/kg 10/10/2018 Molybdenum EPA 200.7 <19, 8 mg/kg 10/16/2018 Nickel EPA 200.7 29.3 mg/kg 10/09/2018 Potassium EPA 200 7 8550 mg/kg 10/12/2018 Selenium t=PA 200.7 <19.8 mg/kg 10/09/2018 Sodiums EPA 200.7 2970 mg/kg 10/12/2018 Zinc EPA 200.7 2310 mglkg 10/0912018 Nitrate+Nitrite-Nitrogen EPA 353.2 469 mg/kg 10/24/2018 Total Solids (%) SM 2540 B 2.42 % 10/05/2018 Ammonia Nitrogen SM 4500 NH3 C 72000 mg/kg 10/10/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 cis B 123000 mg/kg 10/10/2018 Repori 4.. 2018-76? 6'L..W,Tw«,�..,�„<.�...,,.,�..e.,m......,,rW.�., _,.�.,..,......�.,...�,,.,.�d..a...,.....,...,...�.....,.._,.,.._..,.,..,..w��„r--- - -------w-�.�,,... Pa9s 4 of 5 w.»�...,�.._. ` Y ° N?, -40 �•> �� E � Ix � ��i � � i 1Z<r3r! \t�t�lct� \_( ' �1i-I �',7,�t.', s i[l' i 3h I t� i A b1 1E ANALYMAI.. & CONSULTING i:HEMIS7"5 id;tilfrl;Cl ,A'EI'ivi;7`Clif.!I� Brunswick County Public Utilities Date of Report: Oct 26, 2018 Post Office Box 249 Customer PO #,- Bolivia :Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-16162 Project ID: West Brunswick Regional 11VWTP Total Phosphorus SM 4500 P r W 2520 mg/kg 10/19/2018 Mercury SW846 74718 1.28 mg/kg 10/10/2018 TCLP Metals Arsenic EPA 200 7 <1.0 mg/L 10/19/2018 Barium EPA 200.7 <1.0mg/L 10/19/2018 Cadmium EPA 200.7 <1.0mg/L 10/19/2018 Chromium EPA 200.7 <1.0mg/L 10/19/2018 Lead EPA 200 7 <1.0 mg/L 10/19/2018 Se€enium EPA 200 7 <1.0 mg/i_ 10/19/2018 Silver EPA 200 7 <1.0 mg/L 10/19/2018 Mercury _EPA 245 , <0.0002 mg/L 10/1712018 Lab Ill Sample ID: Collect Date/Time v Matrix _- Sampled by __ 18-40869A Site: Sludge 10/3/2018 11:42 AM Solid/Sludge Matt Henry Test _ Method µ Results Date Analyzed 1,1-Dichloroethylene 9W846 Method 8260/5030 <0.01 rng/L 10/20/2018 1,2-Dichloroethane SW846 Method826ol5o30 <0.01 mg/L 10/20/2018 Benzene SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Carbon Tetrachforide SW846 Method 8260/5030 < 0.01 mg/L 10/20/2018 Chlorobenzene SW846 Method 8260/5030 < 0.01 mg/L 10/20/2018 Chloroform SW646 Method 8260/5030 < 0.01 mg/L 10/20/2018 Methyl ethyl ketone SW848 Method 8260/5030 < 0 05 mg/L 10/20/2018 Tetrachloroethylene SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Trichloroethylene SW846 Method 8260/5030 < 0.01 mg/L 10/24/2018 Vinyl Chloride SW846 Method 826015030 < 0.01 mg/L 10/20/2018 Comment: Sludge residuals reported on a dry weight basis Reviewed by; ���� Retort # : 251 8-1 61 62 Page 5 of 5 COUNTY OF BRUNSWICK ws s West Brunswick Regional Laboratory Public Utilities Department 235 Grey Water Road Wastewater Treatment Division Supply, NC 28462 Phone: 910-755-7921 Fax: 910-755-7927 Sample Collection and Chain of Custody Collected By: Matthew Henry Repot? No Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Sail, SL = Sludpe Other: Sample Identification Collection Sample Type Compos Composite Container or Grab (Plastic or Glass) Chlorine mg/L LAB IQ NUMBER PRESERVATION ANALYSIS REQUESTED DATE TIME TEMP NONE HCI H,SOe €iNO, THIO OTHER SDNR Tank WBR 48"C SL P X Fecal Density 1013!2018 11:35 G SDNR Tank WBR 48'C SL P 0 X Fecal Density 10/312018 1136 G SDNR Tank WBR 48'C SL P D r_ X Fecal DensitySDNR 10/3/2018 11-37 G Tank WBR 48`C SL P D X Fecal Density 10/312018 11:38 G SDNR Tank WOR 48'C SL P 0 { X Fecal DenSity 10/312018 11:33 G SDNR Tank VVBR 48'C SL P D X Fecal Density 101312018 11:40 G SDNR Tank VJBR 48'C SL P 0 X Fecal Density 1013/2018 11,41 G SDNR Tank VIER { 48-C Si P a E I TCLPI RClrResaduais 1002018 11.42 G I I I I ATTENTTON: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and a{! BactenOiogicals [must be dechlorinated to < 0.2 ppm at time of Collection. Transfer Relinquishes! 13 : Date/Time y Received 8y: Date/Time 2 t Temperature when Received. �Aceepted Re ectett: ..:.,:� !— 1 ftesample Required, Delivered BY: r<- BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 14, 2018 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 4.13 % Solids 7.45 oll Nitrogen (TKN) 7.660 76,600.000 153.200 Phosphorus 0.237 2,370.000 4.740 Potassium 0.738 7,380.000 14.760 PAN (injected)* 5.063 50,634.000 101.268 PAN (surface)* 3.103 31,034.000 62.068 Ammonia Nitrogen 3.920 39,200.000 78.400 Calcium 4.430 44,300.000 88.600 Calcium Carbonate Eq. --- --- --- Magnesium --- 8,980.000 17.960 Sodium --- 2,880.000 5.760 Sulfur --- --- --- Nitrate N 1 Nitrite N --- 214.000 0.428 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Cei Ing,Concen . Aluminum - 28,300.00 56.600 Arsenic -- 12.40 0.025 75 Cadmium --- 12.40 0.025 85 Chromium --- 38.30 0.077 --- Copper --- 567.00 1.134 4,300 Lead --- 25.20 0.050 840 Mercury --- 5.760 0.012 57 Molybdenum --- 12.40 0.025 75 Nickel -- 21.30 0.043 420 Selenium - - 12.40 0.025 100 Zinc --- 2,420.00 4.840 7,500 L• nv irochem: 2018-18854 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. V4 a Environmental emists, Inc. 6602 4Vincliititl LMiv, Wilmington, N(' 25105 - 9)M.392.0)2:; Lab s 9!0392.$.I'J,4 Faux 710 Bmvye rtowrl Road, Nimitcu, AC 2'i954 252.473.5702 Lab/ Fax 255-A Mimington acksonviliu, N(' 24510 < 910.344 3M'3 i..-ab/Fax I)11 Uli7 C IPt' i ro[I inxlita]c ht nI ISt$. t. on -t Brunswick County Public Utilities bate of Report: Dec 17, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-18854 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-47751 Site: West Brunswick Regional 11/14/2018 8:15 AM Solid/Sludge Chris coddington WWTP Test ------Y - Method— ---- _ ^ M1 Results — Date Analyzed Sludge Residuals Aluminum FPA 200.7 28300 mg/kg 11/30/2018 Calcium EPA 2003 44300 mg/kg 11/29/2018 Magnesium EPA 200 7 8980 mg/kg 11/29/2018 Molybdenum FPA "0 7 <12.4 rrig/kg 12/09/2018 Potassium FPA 200 7 7380 mg/kq 11/29/2018 Sodium EPA 200 7 2880 mg/k. 11/29/2018 Zinc EPA 200 7 2420 mg/kq 11/30/2018 Arsenic EPA 200.8 <12A mg/kq 11/26/2018 Cadmium EPA 200.8 <12.4mg/kg 11/26/2018 Chromium EPA 200.8 38.3 mg/kg 11/26/2018 Copper CPA 200.5 567 mg/kg 11/26/2018 Lead EPA 200.8 25.2 mg/kg 11/26/2018 Nickel EPA 200.8 21.3mg/kg 11/2612018 Selenium EPA 200 a <12.4 mg/kg 11/26/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 214 mg/kg 12110/2018 Total Solids (%) SM 254013 4.13% 1211312018 pH SM 4500 H s 7.45 units 11/28/2018 Ammonia Nitrogen SM 4500 NH3 C 39200 mg/kq 11/27/2018 Total KjeldaM Nitrogen (TKN) SM 4500 org s 76600 mglkq 11/27/2018 Total Phosphorus SM 4500 P F 2370 mg/kg 12/07/2018 Mercury SW846 747113 5.76 mg/kg 11/26/2018 Comment: Sludge residuals, except pig, reported on a dry weight basis, pH reported on an as received basis.— Reviewed by: ,d1.�, { Report i♦:2018-18854 W,,.,.,,ww.,,..�..H�.....,�.e.,..�.�..�„_....�„�...d.._..w.....�,��,�,.�.��.,�..,.A..�._.....,�.,...�,.�.,.,..�.m..e.,....,.e_�»..,,.m.....w.�,..,�.....,w�.«a,..�„-_ Paae 2 of 2 � § Z § k D f 2 � � � k LL O$R � $ $ � ? ■ 0 \ UDR A /§ 3 { J \j } _ ) } Li & ` \ } {& } \� } / x x qW , \/ • \� �\ CL 3° &( 2� § o g , r ¥ /u F e \§ d \ / 2 / / BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 10, 2018 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 493 % Solids 7.29 PH Nitrogen (TKN) 14.400 144,000.000 288.000 Phosphorus 6.030 60,300.000 120.600 Potassium 1.150 11,500.000 23.000 PAN (injected)* 7.563 75,631.400 151.263 PAN (surface)* 5.253 52,531.400 105.063 Ammonia Nitrogen 4.620 46,200.000 92.400 Calciuria 1.950 19,500.000 39.000 Calcium Carbonate Eq. --- --- Magnesium --- 8,820.000 17.640 Sodium --- 1,830.000 3.660 Sulfur --- --- Nitrate N / Nitrite N --- 91.400 0.183 Barium Chloride --- --- --- --- --- --- Iro, Aluminum -- 6,090.00 12.180 '(Mg1K') Arsenic --- 10.80 0.022 75 Cadmium --- 10.80 0.022 85 Chromium -- 61.70 0.123 --- Copper -- 217.00 0.434 4,300 Lead --- 19.00 0.038 840 Mercury --- 0.446 0.001 57 Molybdenum --- 10.80 0.022 75 Nickel --- 34.10 0.068 420 Selenium --- 10.80 0.022 100 Zinc --- 1,220.00 2.440 7,500 Envirochem: 2018-00446 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N T % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) t- (0.5)(Ammonia N) + Nitrate N A- Nitrite N — % PAN Note: Constituents N.D. (Not Detected) or r detection limits are listed as detection limits for calculation purposes. envirochem ANALYTICAL, & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i n fo(t ie nvi ron men t a lchem i st s. com Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00446 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01149 Site: Sludge 1/10/2018 8:00 AM Solid/Sludge Client Test Method Results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.05 mg/L 01/1812018 Endrin SW 846 Method $081813510 <0.0005 mg/L 01/18/2018 Heptachlor SW 846 Method a081Br3510 <0,0005mg/L 01/18/2018 Heptachlor epoxide SW 846 Method 8081 B13510 <0.0005 mg/L 01/18/2018 Lindane SW 846 Method 8081B13510 <0.0005 mg/L 01/18/2018 Methoxychlor SW 846 Method 80818/3510 <0.0005 mg/L 01/18/2018 Toxaphene SW 846 Method 8081813510 <0.05 mg1L 01/18/2018 1,4 -Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,5 -Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4-Dinitrotoluene (TCLP) SW 845 method 8270/3510 <0.050 mg/L 01/19/2018 Cresol (TCLP) SW 846 method 8270/3510 2.09 mg/L 01/19/2018 Hexachloro-1,3-butadiene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 Hexachlorobenzene (TCLP) SW 846 method $27013510 <0,050 mg/L 01/19/2018 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 m + p -Cresol (TCLP) SW 846 method 827013510 2.09 mg/L 01/19/2018 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/19/2018 o -Cresol (TCLP) SW 845 method 82 7013 51 0 <0.050 mg/L 01/19/2018 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/19/2018 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/19/2018 2,4,5 -TP SW846 Method 8151A <0.003 mg/L 01/18/2018 2,4-1D SW846 Method 8151A <0.003 mg/L 01/18/2018 1,1-Dichloroethylene SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 1,2-Dichloroethane SW846 Method $26015030 <0.01 mg/L 01/17/2018 Benzene SW846 Method $260/5030 <0.01 mg/L 01/17/2018 Carbon Tetrachloride SW846 Method $26015030 <0.01 mg/L 01/17/2018 Reoort #:: 2018-00446 D.— 4 „r z Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 f3owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax s 255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info drenvironmentatchemists.com Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention; Donald Dixon Date of Report: Feb 07, 2018 Customer PO #: Customer ID: 08100011 Report #: 2018-00446 Project ID: NE Brunswick Regional WWTP Chlorobenzene SW846 Method 6260/5030 <0.01 mg/L 01/17/2018 Chloroform SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Methyl ethyl ketone SW646 Method 8260/5030 <0.05 mg/L 01/17/2018 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Trichloroethylene SW846 Method 6260/5030 <0.01 mg/L 01/17/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 01/17/2018 Sludge Residuals Aluminum EPA 200.7 6090 mg/kg 01/19/2018 Arsenic EPA 200.7 <10.8 mg/kg 01118/2018 Cadmium EPA 200.7 <10.8 mg/kg 01/19/2018 Calcium EPA 200.7 19500 mg/kg 01/15/2018 Chromium EPA 200.7 61.7 mglkg 01/18/2018 Copper EPA 200.7 217 mg/kg 01/18/2018 Lead EPA 200.7 19.0 mg/kg 01/18/2018 Magnesium EPA 200.7 8820 mg/kg 01/15/2018 Molybdenum EPA 200.7 <10.8 mg/kg 01/18/2018 Nickel EPA 200.7 34.1 mglkg 01/18/2018 Potassium EPA 2007 11500 mg/kg 01/15/2018 Selenium EPA 2007 <10.8 mg/kg 01/18/2018 Sodium EPA 200.7 1830 mg/kg 01/15/2018 Zinc EPA 200.7 1220 mglkg 01/18/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 144000 mg/kg 01/18/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 91.4 mg/kg 01/16/2018 Total Solids (%) SM 2540 B 4,93% 01/11/2018 ply SM 4500 H B 7.29 units 01/18/2018 Ammonia Nitrogen SM 4500 NH3 C 46200 mg/kg 01/21/2018 Total Phosphorus SM 4500 P P 60300 mg/kg 01/19/2018 Mercury SW846 7471 B 0.4460 mg/kg 01/15/2018 TCLP Metals Arsenic BPA 200.7 <1.0 mg/L 01/22/2018 Report *: 2018-00446 b--- „ ,,, , N Environmental Chemists, Inc. a 6602 Windmill Wzly, Wilinington, NC 28105 9 9117.392.0223 Lab - 910.392.4424 Fax 710 C3nw'Qr-toia:n Road, MaInteo, IVC 27954 & 252.473.5702 Lab/Fax ShS: 255-A Wihningt(m I linhway, Jacksonville, NC 28540 6 91(1.347.58431 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infi�(ri;er7r ironri�cn[ t]clt�mist .i oi�� Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00446 Project ID: NB Brunswick Regional WWTP Barium EPA 200.7 <1.Omg/L 01/22/2018 Cadmium EPA 200.7 <1.0 mg/L 01/22/2018 Chromium EPA 200.7 <1.0 mg/L 01/22/2018 Lead EPA 200.7 <1.0 mg/L 01/22/2018 Selenium EPA 200.7 <1.0mg/L 01/22/2018 Silver EPA 200.7 <1.0 mg/L 01/22/2018 Mercury EPA 245.1 <0.0020 mg/L 01/22/2018 Comment: Suldge residuals, except pH reported on a dry weight basis. 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Gf H co v BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 28, 2018 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.73 % Solids 7.41 PH Nitrogen (TKN) 10.700 1 107,000.000 214.000 Phosphorus 5.730 57,300.000 114.600 Potassium 1.300 13,000.000 26.000 PAN (injected)* 7.817 78,165.830 156.332 PAN (surface)* 4.527 45,265.830 90.532 Ammonia Nitrogen 6.580 65,800.000 131.600 Calcium 1.650 16,500.000 33.000 Calcium Carbonate Eq. --- --- --- Magnesium --- 6,090.000 12.180 Sodium --- 1,820.000 3.640 Sulfur --- --- Nitrate N / Nitrite N --- 5.830 0.012 Barium --- --- --- Chloride --- --- --- Cron --- -- - Aluminum --- 6,380.00 12.760 Arsenic - - 13.50 0.027 Cadmium --- 13.50 0.027 Chromium --- 41.00 0.082 Copper --- 194.00 0.388 Lead --- 13.80 0.028 Mercury - - 0.429 0.001 Molybdenum - 13.50 0.027 Nickel --- 25.50 0.051 Selenium --- 13.50 0.027 Zinc --- 1,060.00 2.120 Env i rochem : 2018-04920 Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N A- Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N = Nitrite N = % PAN Note: Constituents \.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 75 85 4,301 840 57 75 420 100 7.501 Environmental Chemists, Inc. 6602 VVin(Imili Wav, bVilmington, N(-_)84055 - 91o.392.02D5 Lib ., 910 _'�92..: 424 Fax 710 13owsertown Koid, Mantoo, NC ''7954 - '52.473.,W02 Lab/Fax 2515-A Wilmington 1li��hway,)ar,� cun-illi�, NC: 285-10 , 910.347.5843 I.��IrJl tix 1111 U![f(CilS'IrC)pll31C13181Ch�F)Yljl5,Cg131 Brunswick County Public Utilities Date of Report: Apr 19, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-04920 Project ID: NEBR Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12249 Site: Sludge 3/28/2018 8:00 AM Solid/Sludge Test Method Results_ Date Analyzed Sludge Residuals Aluminum EPA 200.7 6380 mg/kg 03130/2018 Arsenic EPA 200'7 <13.5 mg/kg 03/30/2018 Cadmium EPA 200.7 <13.5 mglkg 03/30/2018 Calcium EPA 200.7 16500 mg/kg 04/11/2018 Chromium EPA 200.7 41.0 mg/kg 03/30/2018 Copper EPA 200.7 194 mg/kg 03/30/2018 Lead EPA 200 7 13.8 mglkg 03/3012018 Magnesium EPA 200.7 6090 mglkg 04/11/2018 Molybdenum EPA 200.7 <13.5 mg/kg 03/30/2018 Nickel EPA 200.7 25.5 mg/kg 03/30/2018 Potassium EPA 200 7 13000 mg/kg 04/11/2018 Selenium EPA 200 7 <13.5 mg/kg 03/30/2018 Sodium EPA 200.7 1820 mg/kg 04/11/2018 Zinc EPA 200.7 1060 mg/kg 03/30/2018 Nitrate+Nitrite-Nitrogen EPA as3.2 5.83 mg/kg 04118/2018 Total Solids {%j SM 2540 a 3.73% 03129/2018 pH SM 4500 H H 7.41 units 04/06/2018 Ammonia Nitrogen SM 4500 NH3 0 65800 mg/kg 04/05/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 Org 8 107000 mg/kg 04/06/2018 Total Phosphorus SM 4500 P E 57300 rng/kg 04/10/2018 Mercury SW846 74718 <0.429 mg/kg 04/10/2018 Comment: Sludge residuals, except pH, reported on a dry weight basis. Reviewed by: Report.Y;: 20i3-04920..,,Nw.�.,..e.�..,.,.,....,...,�,��.,,,....�.....,.m.,a......m...,.,.-...:.,.,d..o.�.,,..,.,�.,.........._.F....�...,.�..,.,.,,,as,..,.,�...,.,..�.,..•.,,�,,,,...A....�_,.�V.,,.<.............>.,s-,�....,...�.,�..' Page 1 Of tx.,..,.....,.v,,.,.,.. G E ME < zi LU cc z S: BaHj.() OlH.L If Z m 1�1 0 — I > HOVN II LI,1 W POSEN X -1314 u ir Ll a— U31RUMN D (319% f -I -)/BW ourioll4o (D JO d) C'32 Co mCL I m a. Jou!8JU03 0 Off$odwoo QdA eldweS Q C cr c (n G E ME BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 26, 2018 NE Brunswick Regional WW`I'P Permit No. WQ0034468 Mineralization Rate 0.30 3.66 % Solids 7.36 nH Nitrogen (TKN) 9.840 98,400.000 196.800 Phosphorus 3.240 32,400.000 64.800 Potassium 1.040 10,400.000 20.800 PAN (injected)* 6.654 66,541.000 133.082 PAN (surface)* 4.024 1 40,241.000 80.482 Ammonia Nitrogen 5.260 52,600.000 105.200 Calcium 1.660 16,600.000 33.200 Calcium Carbonate Eq. --- --- Magnesium --- 3,930.000 7.860 Sodium --- 1,730.000 3.460 Sulfur --- --- --- Nitrate N 1 Nitrite N -- 201.000 0.402 Barium Chloride --- -- --- --- --- --- SAR: Iron --- --- --- C91 109 CnAcen: Aluminum --- 8,060.00 16.120 Arsenic --- 13.50 0.027 75 Cadmium --- 13.50 0.027 85 Chromium --- 53.60 0.107 --- Copper --- 238.00 0.476 4,300 Lead --- 15.00 0.030 840 Mercury --- 0.519 0.001 57 Molybdenum --- 13,50 0.027 75 Nickel --- 30.90 0.062 420 Selenium -- 13.50 0.027 100 Zinc --- 997.00 1.994 7,500 l nvirochcm: 2018-12053 *Determination of Plant Available Nitrogen (PAN): Injected Application; (Mineralization Rate)(TKN-Ammonia N) d Ammonia N A- Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Amrnonia N) + Nitrate N + Nitrite N — % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. envirochem SM ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392,4.424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info[?environmentalclicmists.com Date of Report: Aug 15, 2018 Customer PO #: Customer ID: 08100011 Report #: 2018-12053 Project ID: NEER Lab ID Sample ID: BCPl1 Collect Date/Time Matrix Sampled by 18-30360 Site: NEER Effluent Grab 7126/2018 1:30 PM Solid/Sludge Tim Webb Test Method Results Date Analyzed /silver EPA 200.7 <93.5 mg/kg 08/07/2018 --Sludge Residuals .,Aluminum EPA 200.7 8060 mg/kg 08/07/2018 Arsenic EPA 2M.7 <13.5 mg/kg 08/07/2018 ,/Cadmium EPA 200.7 <13.5 mg/kg 08/07/2018 calcium EPA 200.7 16600 mg/kg 08/06/2098 ,-Chromium EPA 200.7 53.6 mg/kg 08/0712018 ✓Copper EPA 200.7 238 mg/kg 08/0712018 ✓Lead EPA 200.7 96.0 mg/kg 08/0712018 ,lagnesiurn EPA 200.7 3930 mg/kg 08/06/2018 VMolybdenum EPA 200.7 <13.5 mg/kg 08/07/2018 ,-Nickel EPA 200.7 30.9 mg/kg 08/07/2018 EPA 200.7 'frotassium 10400 mg/kg 08/06/2018 ,,-Selenium EPA 200.7 <13.5 mg/kg 08/07/2018 odium EPA 200.7 1730 mg/kg 08/03/2018 enc EPA 2007 997 mglkg 08/07/2018 ✓/Citrate+Nitrite-Nitrogen EPA 353.2 201 mg/kg 08/08/2018 ✓Total Solids (%) SM 2540 s 3.66% 07/27/2018 ,---pH SM 4500 H B 7.36 units 08/06/2018 Ammonia Nitrogen SM 4506 NH3 C 52600 mg/kg 07/30/2018 Aotal Kjeldahl Nitrogen (TKN) SM 4500 Org 8 98400 mg/kg 07/3012018 Jfotal Phosphorus SM 4500 P F 32400 mg/kg 08/06/2018 .,Mercury SWW7471B <0.619 mg/kg 08/05/2018 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ltow-, Report#:: 201 &12053 Pape 1 of 1 BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant. Date Sampled: November 1, 2018 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 5.05 % Solids 8.05 pH Nitrogen (TKN) 8.930 89,300.000 178.600 Phosphorus 3.420 34,200.000 68.400 Potassium 0.855 8,550.000 17.100 PAN (injected)` 5.536 55,362.000 110.724 PAN (surface)* 3.506 35,062.000 70.124 Ammonia Nitrogen 4.060 40,600.000 81.200 Calcium 1.790 17,900.000 35.800 Calcium Carbonate Eq. --- --- --- Magnesium --- 5,070.000 10.140 Sodium --- 1,610.000 3.220 Sulfur --- --- --- Nitrate N 1 Nitrite N --- 152.000 0.304 Barium --- --- -- SAR ; Chloride Iron --- --- --- Ceiling Conten Aluminum --- 656.00 1.312 '(MW -Kg) Arsenic --- 10.70 0.021 75 Cadmium --- 10.70 0.021 85 Chromium -- 37.80 0.076 --- Copper --- 193.00 0.386 4,300 Lead --- 12.20 0.024 840 Mercury --- 0.396 0.001 57 Molybdenum -- 10.70 0.021 75 Nickel --- 23.80 0.048 420 Selenium --- 10.70 0,021 100 Zinc --- 956.00 1.912 7,500 l: nvirochem: 2018-17963 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Arnmonia N) + Ammonia N -4- Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0,5)(Amrnonia N) + Nitrate N + Nitrite N — % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environ.me-ti-tal Chemists, Inc. p (601.,4'iruirrrlkJv`ay4'%)hnjn ikm,",, 2`ik+i% dI(�:9ril':3i c c � r, f � ,h 1 iif � i .�I l:.4 1'.lx 710 I Cr tie!'i'ut Yt 1Zwd, N4,into b, ( 2 71)5'1 2,-52.47151702 Loh/Fax � `say r;--14Nitn;ir�;;for{ Hif hr, ov, 1,t, k,:oiivillt„ AC. =S. 74} lair/Fax ANAL 'TICAL & CONSUOING CHEMISTS iia[i!'ri.;e:t,ircr n enE;t:chi Ertl t s.cnrro Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Glenn Walker Revised Report: Jan 04, 2019 Original Report Date: Dec 06, 2018 Report #: 2018-17963 Customer ID: 08100011 Project ID: NEBR Lab ID Sample ID: 18-45361 Site: Sludge Collect DatelTime 11/1/2018 11:01 AM Method Matrix Sampled by Solid/Sludge Client Results Date Analyzed Silver EPA 200.7 <10.7 mg/kg YW 11/05/2018 Total Solids (%) SM 2540 s 5.05% 11/06/2018 Ammonia Nitrogen SM 4500 NH3 C 40600 mg/kq 11/06/2018 Sludge Residuals Arsenic EPA 200.7 <10.7 mg/kg 11/05/2018 Cadmium EPA 200 7 <10.7 mg/kg 11/05/2018 Chromium EPA 200.7 37.8 mg/kg 11/05/2018 Copper EPA 200 7 193 mg/kg 11/05/2018 Lead EPA 200.7 12.2 mg/kg 11/05/2018 Molybdenum EPA 260.7 <10.7mglkg 12/04/2018 Nickel EPA 200.7 23.8 mg/kg 11/05/2018 Zinc EPA 200 7 956 mg/kg 11/05/2018 Selenium EPA 200 8 <10.7 mg/kg 11/23/2018 Nitrate+Nitrite-Nitrogen EPA 353 2 152 mg/kg 11/21/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 org n 89300 mg/kg 11/05/2018 Total Phosphorus SM 4500 P F 34200 mg/kg 11/19/2018 Mercury SM4E 74 71 B <0.396 mg/kg 11/04/2018 Report g'. 201817963.s.,.,..,.-,.,..�.w..,,�..._,.,...,.r.��,....,..m,.-.,,..��w�,..a,.,�.,��.v.,,....,,..�..,�,..,.......,.,....,.,,.s,.e..�...._....�...,,a.n..�«..�,.»...,�...�....,,�.,....W...x..,�..,.P 3oa 4 of? .�..a.......�, Brunswick County Public Utilities Post Office Box 249 Bofivia NC 28422 Attention: Glenn Walker Lab ID Sample ID: 18-45361A Site: Sludge Test Aluminum Calcium Magnesium Potassium Sodium pH Comment Reviewed by: ��602 iv'Indo-?;!] VV„V. ��Iillttllr:.r Cft, N.'(_ 2"405 o 9i..iil; - y 1.0.'392 4424 1 ii 10 lic>t `n I: ROO.d, N(-'7� ! �-'A' a ;';"02 5 A 1�1haI}Zs'{� It Ci �;P;ti ��, <tChsi�I,�'i).lt, NC. 28:)4"} a 9:C)347.)8,3 I_ab!Pxx ait ii�l(2PdtA�3 Yi)!t [flBit! i? IC11 CfYI F>;E S.ti.4H11 Revised Report: Jan 04, 2019 PfL 0 V11" N� •���,,� SCS {, r iii���'��r,:",z�'' 08100011 �r�"� ,'�� 01/03/2019 8.05 units ANALY;'ICAL & CONSULTING CHCWSTS Brunswick County Public Utilities Post Office Box 249 Bofivia NC 28422 Attention: Glenn Walker Lab ID Sample ID: 18-45361A Site: Sludge Test Aluminum Calcium Magnesium Potassium Sodium pH Comment Reviewed by: ��602 iv'Indo-?;!] VV„V. ��Iillttllr:.r Cft, N.'(_ 2"405 o 9i..iil; - y 1.0.'392 4424 1 ii 10 lic>t `n I: ROO.d, N(-'7� ! �-'A' a ;';"02 5 A 1�1haI}Zs'{� It Ci �;P;ti ��, <tChsi�I,�'i).lt, NC. 28:)4"} a 9:C)347.)8,3 I_ab!Pxx ait ii�l(2PdtA�3 Yi)!t [flBit! i? IC11 CfYI F>;E S.ti.4H11 Revised Report: Jan 04, 2019 Original Report Cate: Dec 06, 2018 Report #: 2018-17963 Customer ID: 08100011 Project ID: NEBR 01/03/2019 Collect Date/Time Matrix 11/1/2018 11:01 AM Solid/Sludge Method EPA 200.7 EPA 206 7 EPA 200.7 FPA 200.7 EPA 200.7 SW 846 Melhoo 9045D Results reported on a dry weight basin Revised to Results Sampled by Client Date Analyzed 956 mg/kg 11/05/2018 17900 mg/kg 01/03/2019 5070 mg/kg 01/03/2019 8550 mg/kg 01/03/2019 1610 mg/kg 01/03/2019 8.05 units 01/04/2019 H, Al, Ca, Mg, K, NA per clientM�.�___________. Report k-: 2016-17M Page 2 of 2 31 ry 1 7S C7 a� „ C7 fi C7 G� C7 ti} C7 G7 C7 G7 C? �r \1 C 3 Composite C? or Grab G7 Gi Ht C7 G7 G7 [7 G7 O l7 C7 G7 !] C,i "fJ � "q� Contilner (p or G) ll HNO3 .�.j NAOI-1 fD n 57mp10 Ype Cry C7 a� C7 C} C7 fi C7 G� C7 ti} C7 G7 C7 G7 C? �r \1 C 3 Composite C? or Grab G7 Gi f7 C7 G7 G7 [7 G7 O l7 C7 G7 !] C,i "fJ � "q� Contilner (p or G) m Chlorine m�14 Ik LAB ID NUMBER M ~ .JS NONE M c tics, 4 H2SO4 m m ll HNO3 .�.j NAOI-1 D -I THO Z u OTHER .. C °�1 A Mr CD S M. :i L z z M z 9 i3 J t1 to 34 a C °�1 A Mr CD S M. :i L z z M z 9 i3 J West Brunswick WWTP WQ0034468 Class A - 1st Quarter 2018. Date Fecal Coliform MPN 2er ram Log 01/10/18 7 0.8451 01/10/18 7 0.8451 01/10/18 7 0,8451 01/10/18 7 0.8451 01/10/18 8 0.9031 01/10/18 7 0,8451 01/10/18 7 0.8451 Total 1 5.9737 Average 0.8534 Geometric Mean 7 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. ��y y X34 Wx Environmental Chemists, Inc. 6602 Windmill Vv�a, AC2810`i 910.3i 2.03 Lih 1 14 : �1#�3x f3�x,;ea�t�nvn f:;iui \�larll�t�, AL �ir).i3 'i2.�d73.,7p? €_ ab/I as �gx ?55 11 VV iInIi11g'(r7I lil'ii� i,', )tu.}:5ctttviIIL', NC 255'I0 , 910.,3,17,- }3 1, 1)/1�n-' ANALYTICAL. & CONSULTING CHEMISTS Ifllilri.',�Ei1'!I'JE1111C111aiCii;°mi;i..com Brunswick County Public utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO ##: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00424 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01078 Site: 1 1/10/2018 11:09 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.87% 01/11/2018 Fecal Density SM 922#C E MPN 24 hr 503 <7 MPN/g 01/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01083 Site: 2 1/10/2018 11:10 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM2540G 3,04% 01/11/2018 Fecal Density SM 9221C E MPN 24 hr 5o3 <7 MPN/g 01/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01084 Site: 3 1/10/2018 11:11 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.10% 01/11/2018 Fecal Density SM 9221 C E MPN 24 hr 503 <7 M PN/g 01/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01087 Site: 4 1/10/2018 11:12 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.86% 01/11/2018 Fecal Density SM 9221C E MPN 2411, 503 <7 MPN/g 01/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01088 Site: 5 1/10/2018 11:13 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.61% 01/11/2018 Fecal Density SM 9221C E MPN 24 hr 503 <8 MPN/g 01/11/2018 Reportk: 2018-00424 Page 1 of 5 '� ���j ✓' s ��e -� n ��� 0602 Windmill 11<<1��, VVilmiiz-;tota, N("2810 910.392.rl',?3 Lab 910.392.4424 I�,tx 710 Bovo ertmvt Road, .Mankeo, N(' 279",4 - 252. 73 5702 1 ab, ax ?.VA' ldInit1-Iola I Iiliw�;;tti, I,ac_I<4oiavdI e, \C. 28540 - 9!0 3-47.5843 LaI)/I ax ANALYTICAL. & CONSULTING CHEMISTS iri'o(u cnvirononcnIl tId loll] ist Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-00424 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-01089 Site: 6 1/10/2018 11:14 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) sM 2540 G 3.09% 01/11/2018 Fecal Density SM9221C E MPN 24 hr 503 <7 MPNlg 01/11/2018 Lab ID Sample ID: Collect Date[Time Matrix Sampled by 18-01090 Site: 7 1/10/2018 11:15 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.00% 01/11/2018 Fecal Density SM 92210 E MPN 24 hr 503 <7 MPN/g 01/11/2018 Report #:: 2018-64424 .d.K.� Page 2 of 5 I, - C14 % InL f \ I- 0 / U. � n C%4 20rqP- 2q § k N M kk\ a,Lnik \\/ƒ \ LJ z \ LU ) ƒ } / / \ 3 ( / x x xx x zz /f � } \ \ \ ~ \ � §3 {® CL a I CL CL I a� (L 3 ) \\ 0 0io 0 0 0 0 0 J( 2 e e e 2 a G m G ) Ky o 0 0 0 p o u / jLLJ / \ - � \ ƒ \ ( \ ( } \ } « t \ ) ®§ ®§ « ®§ « D R § § § § ) m e m e m m m West Brunswick WWTP WQ0034468 Class A - 2nd Quarter 2018 Date Fecal Coliform MPN per ram Log 04/04/18 46 1.6628 04/04/18 46 1.6628 04/04/18 46 1.6628 04/04/18 46 1.6628 04/04/18 45 1.6532 04/04/18 46 1.6628 04/04/18 46 1.6628 Total 11.6298 Average 1.6614 Geometric Mean 46 Fecal Coliform MPN / gram. Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. 4, Environmental Chemists, Inc. [i(02 Windmill ti,Vav, VVifin;ngton, NC- 23405 � 1)30-:192.0223 Lab , �110.392,4 321 Frsx IO t9knv',c!rt0v%n Road, NlvlWo, NV 27>5.4 _ 252,171.:57 1„ab/1=nx . ?:ii-:(1']ISl'llil,'iUft1.11gEilialr aCk�L)nvlll[s,�C.2hi4i) 7.55. ANALYTICAL & CONSULTING CHEMISTS ilEft ll; 'I1VS1'()11131 13121 I1'i1�1111 i�,40111 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Date of Report: Apr 18, 2018 Customer PO #: Customer ID: 08100011 Report #: 2018-05327 Project ID: SDNR Tank Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13183 Site: # 1 4/4/2018 11:11 AM Solid/Sludge Matthew Henry Test Solid/Sludge Matthew Henry Method Results Date Analyzed Total Solids (%) SM 2540 G - 3.95% 04/06/2018 Fecal Density SM 9221C E MPN 24 hr 503 Total Solids (%) SM 2540 G 3.95% 04/06/2018 Fecal Density 4/4/2018 11:14 AM SM 92210 E MPN 24 hr 503 <46 MPN/g 04/05/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-13184 Site: # 2 4/4/2018 11:12 AM Solid/Sludge Matthew Henry Test Lab ID Sample ID: Method Results Date Analyzed Total Soiids (%) SM 2540 G 3.98% 04/06/2018 Fecal Density SM 92210 E MPN 24 hr 503 —_ <46 MPN/g 04/05/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-13185 Site: # 3 4/4/2018 11:13 AM Solid/Sludge Matthew Henry Test —� Method_ Results Date Analyzed Total Solids (%) SM 2540 G - 3.95% 04/06/2018 Fecal Density SM 9221C E MPN 24 hr 503 <46 MPN/g 04/05/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13186 Site: # 4 4/4/2018 11:14 AM Solid/Sludge Matthew Henry Test.----- Method Results Date Analyzed Total Solids (%) SM 2540 G 3,98% 04/0612018 Fecal Density - SM 92210 E MPN 24 hr 503 <46 MPN/g 04/05/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13187 Site: # 5 4/4/2018 11:15 AM Solid/Sludge Matthew Henry Test--.._�_ ----- M�Method Results Date Analyzed Total Solids (%) SM 2540 G 4.00% 04/06/2018 Fecal Density SM 92210 E MPN 24 hr 5o3 <45 MPN/,q 04/05/2018 Report a.. 2018-05327 Page 1 of 2 Environmental Chemis s, Inc. 6002 Winds ti} Mw, 011 !392.02'-5 Lab . 9) J 92. i424 Fax 71013ows glows Road, 1�1,� leo NC 21,971"1 . 2,?,d7, ( Iib, 1 ax ; � � 13 :114'i1�a1i��l;tun iliz;���� �� 1�lchsoll� ills, N`C' 28.540 . 9 W 347.;35'4:3 ANALYTICAL & CONSULTING CNEWSTS �li);rt:c� it : iin3eEzl;E3ch{>in st,.cnEEr Brunswick County Public Utilities Date of Report: Apr 18, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-05327 Project ID: SDNR Tank Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13188 Site: # 6 4/4/2018 11:16 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Sdids (%) Fecal Density Lab ID Sample ID: 18-13189 Site: # 7 Test Total Soiids (%) Fecal Density SM 2540 G SM 92210 E MPN 24 hr 503 3.94% 04/06/2018 <46 MPNIg 04/05/2018 Collect Date/Time Matrix 4/4/2018 11:17 AM Solid/Sludge Method Results SM 2540 G SM 9221 G E MPN 24 hr 503 Comment: Reported on a dry weight basis. Reviewed by: Sampled by Matthew Henry Date Analyzed 3.99% 04/06/2018 <46 MPNIg 04/0512018 Report 9:"m2018`05327 Paqe 2 of 2 cn m O Cr0 fD n' C C Z tu w f�11 0 ami C7 n m ,.r C a � Z A m ZZ x x Z :EZ x Z :u :EZ xu � Z x tt W �u m ;u m m� m d;13 co w z w; W w co z v {. m s a a A A A .a. A b b OO O O O m m m m m m m m ID W N m 0 n W n W a W a W A W a W a W m ti m o o_ L� 0 G) 0 0 G) 0 U o v � Q � o "Cf i7 Cf "f7 "C] "tl CJ m_ v N Ci ro z �'C1 Du yob m C7 Z O z m _ n _ v QCl) m C _ z O w o z X X X X x X x s 0 O m 91 r. n m W n -fl N n [z Al o a n o CD n CD ( o CD J Z fmCD cn N N N m V] O cn m O Cr0 fD n' C C Z tu w f�11 0 ami C7 n m ,.r C a � Z A West Brunswick WWTP WQ0034468 Class A - 3rd Quarter 2018 Date Fecal Coliform MPN per ram Log 07/18/18 603 2.7803 07/18/18 576 2.7604 07/18/18 554 2.7435 07/18/18 572 2.7574 07/18/18 591 2.7716 07/18/18 574 2.7589 07/18/18 587 2.7686 'T'otal 1 19.3408 Average 2.7630 Geometric Mean 579 Fecal Coliform. MPN 1 gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. 4-1 1-linvironmental Chemists, Inc. 4rr,if 1,V: 1111 c I ? {J ?3 , t 1. 91 1) 2.1 1' i,�x r' -7 10 1 i N.4y111 Rr c1NIazttvo, NC 2795 1 i air �g .111it1nr, I JackStiiuvi;l,,'\C�?�')4ft ':0d3_347.1i8;�,I_ah?1:a>= ANALYTICAL CONSULTING C;M(=NsiS'TS iiEoi�rc i! �ir�a3171Cri%ti:at�nitSFs.it��'o1 Brunswick County Public Utilities Date of Report: Jul 23, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-11631 Project ID: SDNR Tank Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-29360 Site: 001 7/18/2018 10:31 AM Solid/Sludge Matt Henry Test ----v- --� Method Results Date Analyzed Total Solids (%) SM 2540 G 2.99% 07/19/2018 Fecal Density SM 9221C E MPN 24 hr 503 <603 MPNIg 07/19/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-29361 Site; 002 7/18/2018 10:32 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.13% 07/19/2018 eca# ' Density y .... N 24 hr 503 ..._.._SM 922121 C C E E MP y _......._ <576 MPNIg 07/19/2018 Lab ID Sample ID: __ Collect Date/Time _ . _ Matrix Sampled by 18-29362 Site: 003 7/18/2018 10:33 AM Solid/Sludge Matt Henry TestV T ^_ Method_ Results Date Analyzed Total Solids (%) SM 2540 G 3.25% 07/19/2018 Fecal Density SM 9221C E MPN 24 hr 503 <554 MPNIg 07/19/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-29363 Site: 004 7/18/2018 10:34 AM Solid/Sludge Matt Henry Test - - Method Results Date Analyzed Total Solids (%) SM 2540 G 3.15% 07/19/2018 Fecal Density .... SM 92210 E MPN 24 hr 503 �� <572 MPNIg 07/19/2018 Lab ID Sample ID:� Collect Date/Time � Matrix Sampled by 18-29364 Site: 005 7/18/2018 10:35 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.05% 07/19/2018 Fecal Density SM 9221C E MPN 24 hr 503 <591 MPN/g 07/19/2018 ftepor!#, 2016-1163•�.,n.�.W.,...a..,a....,,._.H..,....,.�.,,�,...m.�....�..,,,.,....,,�,...�,.w..,n..,,,:.�....��,...•-----...d.�,�v..,��,,.�..�,..�.,.�.�.�.,.,.,,,.q..,-..�.,....,... ,.�.�.�,,...�..x Page 1 of 2 y i �fir`rrr. p' q�x "Tr !�i tic,+ �i Itirs!dr! ft1 tV 1%,2 VVI 1 niiIol N C'r.10"; _ x,71ih 10 i_I2.I V.ix YI �I I. kmd, �hlilit'r;, '�C. 77�}741 �,��. 0•/�1�n.11��.I}� ANALYTICAL & CONSULTING CHH 1EST5 in><>:ir Ill iic.fil it oltil l . ti:itilicom Brunswick County Public Utilities Date of Report: Jul 23, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-11631 Project ID: SDNR Tank Lab ID Sample ID: Collect Date/Time Matrix Sampled by�� 18-29365 Site: 006 7/18/2018 10:36 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.14% 07/19/2018 Fecal Density SM 9221C E MPN 24 hr 503 X574 MPN/g 07/19/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by� 18-29366 Site: 007 7/18/2018 10:37 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.07% 07/19/2018 Fecal Density SM 9221C E MPN 24 hr 503 X587 MPN/g 07/19/2018 Comment: Results reported on a dry weight basis. Reviewed by: _� Rppws~„W2018-11�i31�,�.,.�,��.....,�.,..�,...,..,,,.,�..�,W.�_>.w._=,�..�.«..,.�,..����..�,,,,..,..,:..,.,.m,...�,.d.,.W�_�,..rH,...z_Page 2 of 2 e.�..............� fD CD D n O n CD a- a a an CD 0 a G1 0 Q. 0 O c N 0 C. l< O m 0 z n w Q CD 0 C �tD 0 Q7 V IF 03 CD I'T C y L^ C /Cl) (/i d f/) cn t7 0 O co O C!> O (n 4 O W A CU Z 'n S Z W W W Z* W Z x1 W z i1 W x 7J xa z v x x x F x � � O• m F � a o O O co O C7 m O O O p O O O (D Q OJ W N W 0�0 Q� O] m T w 0 N m � 0 0 G) G? Gi G7 G) G) 0 g v N Q - a w ro z c cW M o -� •-�` �Jy `may � ..Sl � °z y t \ cry m Lk" ' 0 ? m M p o co m x � o w o z X x x x x x x s a O 2 m m m 'n m n ;o O O C7 q Ci 4 O w O m D p z co m O n O n CD a- a a an CD 0 a G1 0 Q. 0 O c N 0 C. l< O m 0 z n w Q CD 0 C �tD 0 Q7 V IF 03 CD I'T C y L^ C /Cl) West Brunswick WWTP WQ0034468 Class A - 4th Quarter 2018 Date Fecal Coliform MPN per ram Log 10/03/18 65 1.8129 10/03/18 63 1.7993 10/03/18 63 1.7993 10/03/18 67 1.8261 10/03/18 61 1.7853 10/03/18 65 1.8129 10/03/18 63 1.7993 Total 1 12.6353 Average I 1.8050 Geometric Mean 64 Fecal Coliform MPN / grain Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction. requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. � 'fit 284,,:i Mai P(:o, NV 27954 -i �)_�; 25,5.-A 5'�'11n;@;t $�Li)!1 "�i��fl 11'lb. l2i['.ksonvil°l , NC '2Zi 40 ANALYTICAL & CONSUIXI NG CMEWSTS � ruirr.e t it'i>; i3tcn{t i E c� ,i,l ., c ;:• Brunswick County Public Utilities Date of Report: Oct 26, 2018 Post Office Box 249 10/05/2018 10/04/2018 Customer PO #: Bolivia NC 28422 Matrix Sampled by Customer ID: 08100011 Attention: Donald Dixon 10/3/2018 11:38 AM Report #; 2018-16162 -Te5t Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-40849 Site: SDNR Tank 1 10/3/2018 11:35 AM Solid/Sludge Matt Henry Test_ Method Results Date Analyzed Fecal Density Sri 92210 E MPN 24 hr 503 _ Total Solids {%) SM 2546 G 2.77% 10/05/2018 Fecal Density SM 9221C E MPN 24 hf 543 <65 MPN/g 10/04/2018 Lab ID Sample ID: 10/3/2018 11:39 AM Collect Date/Time Matrix Sampled by 18-40853 Site: SDNR Tank 2 Test 10/3/2018 11:36 AM Solid/Sludge Matt Henry Test ---_ _ Method --__ ^- — Results Date Analyzed Total Solids (%) SM 2540 G 2,88% 10/05/2018 Fecal Density SM 9221C E, MPN 24 hr 503 <63 MPN/g 10/04/2018 Lab ID Sample ID: --_ Collect DatetTime LL Matrix Sampled by�—� ~ 18-40854 Site: SDNR Tank 3 10/3/2018 11:37 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (°1°) Fecal Density SM 2540 G SM 92210 E MPN 24 hr 503 2.90% <63 MPN/g 10/05/2018 10/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by _ 18-40855 Site: SDNR Tank 4 10/3/2018 11:38 AM Solid/Sludge Matt Henry -Te5t Method Results Date Analyzed Total Solids (°1°) SM 2540 G 2.69% 10/05/2018 Fecal Density Sri 92210 E MPN 24 hr 503 <67 MPN/g 10/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-40856 Site: SDNR Tank 5 10/3/2018 11:39 AM Solid/Sludge Matt Henry Test Meth od--� Results ___---.__---Date Analyzed Total Solids (%) Siva 2546 G 2.97% 10/05/2018 Fecal Densrty SM 9221C E MPN 24 hr503 <61 MPN/g 10/04/2018 Report #y�.2016-16162 �,.,.,�,�,.._,,,.m.,.,,�..�,.a.r..�v�.-w.,�.�,o.,.u...�.,,,�.T �. �_.,,.e..,..�,.�..<..�_..,�.,,.....,...nw..�.�..,�®.o..,N,w..�,.�.�..,�a�,...N.�,.,•_,,.�,..�.,-n,.>..�., �.. Page 1 of 5 Eiivironmental Chemists,, Inc. W 2S7 9 91;l 3 2 -A W; I i \C ANALYTfCAL & CONSOUING CHEMISTS .. ....... _77'7' Brunswick County Public Utilities Date of Report: Oct 26, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-16162 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: ry Collect Date/Time Matrix Sampled by 18-40857 Site: SDNR Tank 6 10/3/2018 11:40 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids SM 2540 G 2.80% 10/05/2018 Fecal Density SM 9221C E MPN 24 hr 503 <65MPN/g 10104/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-40858 Site: SDNR Tank 7 10/3/2018 11:41 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.90% 10/05/2018 Fecal Density SM 92210 E MPN 2n hr 503 <63 MPN/g 10/04/2018 Report P: 20',8-116162 Page 2 of 5 NF Brunswick WWTP WQ0034468 Class A - 1 st Quarter 2018 Date Fecal Coliform MPN per Tram Log 01/31/18 473 2.6749 01/31/18 468 2.6702 01/31/18 473 2.6749 01/31/18 450 2.6532 01/31/18 470 2.6721 01/31/18 461 2.6637 01/31/18 458 2.6609 Total 1 18.6698 Average 2.6671 Geometric Mean 465 Fecal Coliform MPN 1 gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 Teets a portion of Class A - Alternative 5 Pathogen Reduction requirement. "A �n.vironmen.tal Chemists, Inc® 6K12 Wi cmill May, Wilmington, tan vC 28405910-392,0223 a� e 910.392.4-124 Fax ( o 7 710 [3ow sertowr� Road,i �� � r �Lab/F, Mai. tur, NC 27)5l 2.2.I7_ .5/Uti x 255-A Wilmington Highway, Jacksonville, NC 28540 $ 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS irtfb(i Cllviroitm0ratarlchoil tists.coIII Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Glenn Walker Report #: 2018-01498 Project ID: NEBR Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03707 Site: # 1 1/31/2018 10:10 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2640 G 4.23% 02/02/2018 Fecal Density SM 92210 E MPN 24 hr 5o3 <473 MPN/g 02/01/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-03708 Site: # 2 1/31/2018 10:14 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4,28% 02/02/2018 Fecal Density SM 9221C E MPN 24 hr 503 <468 MPN/g 02/01/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-033709 Site; # 3 1/31/2018 10:16 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.23% 02/02/2018 Fecal Density SM 9221 C E MPN 24 hr 503 <473 MPN/g 02/01/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03710 Site: # 4 1/31/2018 10:20 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.45% 02/02/2018 Fecal Density SM 9221C E MPN 24 hr 503 <450 MPNIg 02/01/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03711 Site: # 5 1/31/2018 10:24 AM Solid/Sludge Randy Burngarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.26% 02/02/2018 Fecal Density SM 9221C E MPN 24 hr 503 <470 MPN/g 02/01/2018 Report #:: 2018-01498 Pape 1 of 2 Environmental Chemists, Inc. 6602 Windmill Way, VVilmington, NC 28405 ° 910.392.0223 1,1b ° 910.392.4429 Fax 710 Bowserlown Road, Manteo, NC 27954 m 252.=173.5702 Lab/Fax 255-A Wilmineton Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/lax n f0@XIIvirotuzaerl talChCIl1iSLS.cnIII Brunswick County Public Utilities Date of Report: Feb 07, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Glenn Walker Report #: 2018-01498 Project ID: NEBR Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03712 Site: # 6 1/31/2018 10:28 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.34% 02/02/2018 Fecal Density SM 9221C E MPN 24 hr 503 <461 MPN/g 02/01/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03713 Site: # 7 1/31/2018 10;32 AM Solid/Sludge Randy Bumgarner Test Method Results Date Analyzed Total Solids (%) SM 2540 G Fecal Density SM 9221 C E MPN 24 hr 503 Comment: Results reported on a dry weight basis. Reviewed by: &nlola 4.37% 02/02/2018 <458 MPN/g 02/01/2018 Report #:; 2018.01498 panty � M o 4 N vE .z a in C W E F- j _C U. � N a d mNO r= m `� J U) q �r c w w O► Z w Q LL R. z © m w OC 4 0. S c. cr N tE H9HiO o 7• V? o 0IH.4 > W 0 U 3 7 LL O I^ HOVN Z - _ c `tet X CONK LC z Q O LLJ Z z o 'a~ W 4OSM O LLE U Litw J Q C a /p6� V d O z OU >x c�L (� —�._-. o CC z -1OH v> Z z- W � 3NON .j u u u3sv v 'u " v at avi r U 3 vsur aulaoly� � � .3 O a Baa s�uo) I � � r C7 B; C7 C'3 CL (D a_ U` Q w � z O 1 Z 47 C W E F- d J U) q �r Z It tE H9HiO 7• H z 0IH.4 7 I^ HOVN `tet X CONK LC 11Lit 'a~ W 4OSM w � y -1OH { � 3NON u u u3sv v v at avi 3 vsur aulaoly� � � a ti� Baa s�uo) I � C7 B; C7 C'3 CL (D a_ U` � 1 � geAD [ co U C� U U. U U C7 U C'3 C? 0 � a�lsodw0� addl �\ aldweSCL T v N G ac ' Pr, fa .. I^ .i CL f K d E r N z O 1 Z 47 NE Brunswick WWTP WQ0034468 Class A - 2nd Quarter 2018 Date Fecal Coliform MPN 2er ram Log 11/07/18 364 2.5611 11/07/18 339 2.5302 11/07/18 379 2.5786 11/07/18 360 2.5563 11/07/18 347 2.5403 11/07/18 343 2.5353 11/07/18 358 2.5539 Total 1 17.8557 Average 2.550$ Geometric Mean 355 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. L Y.'• Invironmental Chemists, Inc. I ih 90) iW_2.-4,'24 1-:i\ 10 Bow "ol.tl i i 11ll;l(1 NIoi3 tuC) V 2i 1) ] # "• .). }2.47" C;7 {i'I i Iighwav, Jack.,nnvilko, NC 135.10 m 910,., }7.5843 Lalli:Fax ANALYTICAL CONSULTING CHEMISTS nksu;e;i�ici?iwon [,IlchemBts.k:o�l� Brunswick County Public Utilities Date of Report: Nov 11, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer 1D: 08100011 Attention: Glenn Walker Report #: 2018-18357 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-46415 Site: # 1 11/7/2018 10:12 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4,95% 11/0812018 Fecal Density SM 9221C E MPN 24 hr 503 <364 MPN/g 11/08/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-46416 Site: # 2 11/7/2018 10:16 AM Solid/Sfudge Client Test Method Results Date Analyzed Total Solids (%) SM2540G 5,31 % 11/08/2018 Fecal Density SM 9221C E MPN 24 hr 503 <339 MPN/g 11/08/2018 Lab ID Sample ID: Collect Date/Time Matrix r Sampled by _ 18-46417 Site: # 3 11/7/2018 10:20 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.76% 11/08/2018 Fecal Density SM 8221C E MPN 24 hr 503 <379 MPN/g 11/08/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-46418 Site: # 4 11/7/2018 10:24 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 5.00% 11/08/2018 Fecal Density SM 92210 s MPN 24 hr 303 <360 MPN/g 11/08/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-46419 Site: # 5 11/7/2018 10:28 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 5.20% 11/08/2018 Fecal Density SM 9221C E MPN 24 hr 503 <347 MPN/g 11/08/2018 Report #: 2018.18357 �..����,• �----^ Page i of 2 Environmental Chemists, Inc. v U k 7 i i ai[1_ l�tr«Ih'li� ti�s1YE[�Sal� _ 1)10."4112.0223) ilir >� 2hict�7A.1) I lt\ Z,i,\inic)\C270th t� �s. >a`✓ ? i3 -A V\:1i711k.141,on I1- );'hwa%i , �1C�yl1FZL'1.1��, N( 285-110 ANALYTICAL & CONSULTING CHEMISTS nlcx;rt,�,tt is'i ti]rett!<El 'hettti?t �itttt Brunswick County Public Utilities Date of Report: Nov 11, 2018 Post Office Box 249 Customer PQ #: Bolivia NC 28422 Customer ID: 08100011 Attention: Glenn Walker Report #: 2018-18357 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-46420 Site: # 6 11/7/2018 10:32 AM Solid/Sludge Client `Gest Total Solids (%) Fecal Density Lab ID Sample ID: 1846421 Site: # 7 Test Total Solids (%) Fecal Density Comment: Reviewed by: Method Results Date Analyzed SM 2540 G 5.25% 11/08/2018 SM 9221C E M P N 24 hr 503 <343 MPNIg 11/0812018 Collect DatelTime Matrix Sampled by 11/7/2018 10:36 AM Solid/Sludge Client Method SM 2540 G SM 9221C E MP 24 hr 503 Results reported on y qry weight basis. Results 5.03% <358 MPNIg Date Analyzed 11108/2018 11/08/2018 Report #:: 2018-18357 MI N Page 2 of 2 � Iy M w 7—N (7 N Q10 Z 0 M 0 0 M 0 T � o Z® t- 0 Z 0 ® p � T� > M 9 z MV ^y g Sa ' - !� t1 cn j v as PS I d M GC lr( GC e o a n M C a � sp V`: �., Semple Type 4 Composite or Grob Container Gi -0 `0 -0 -0 Ca} D ,f) -u fi7 'O G) -0 (P or G) t C7 Chlorine mg/L 3 LAB ID NUMBER NONE i HC. M =: H2304 M M HH03 m C n p { NADH ..� THIO Z X KY, t:C 'C OTHER 1 �. > z _ A � m N M f• M w 7—N (7 N Q10 Z 0 M 0 0 M 0 T � o Z® t- 0 Z 0 ® p � T� > M 9 z MV ^y g Sa ' - !� cn j v as PS Q10 Z 0 M 0 V p � MV ^y g Sa ' - !� m � as PS NE Brunswick WWTP WQ0034468 Class A - 3rd Quarter 2018 Date Fecal Coliform MPN per rain Log 11/14/18 41 1.6128 11/14/18 43 1.6335 11/14/18 40 1.6021 11/14/18 42 1.6232 11/14/18 42 1.6232 11/14/18 41 I.6128 11/14/18 41 1.6128 Total 1 11.3204 Average I.6172 Geometric Mean 41 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion. of Class A - Alternative 5 Pathogen Reduction requirement. Environmental Chemists, Inc. 6602 %,VrdmI1 9 1 o.3,1.0 -1,12A ]�,lx JZnc)d, Nlanteo, NC 27954 25'A73).-)7(.)2 1-11,/Fax, 2"3 -'i -A Y, � lack-onviil(,, 285-10 910 ,. 47.: 84") Llb/Fxx ANALYTIC A[ &CONSULTING CHEMISTS Brunswick County Public Utilities Date of Report: Nov 16, 2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Donald Dixon Report #: 2018-18859 Project ID: NEER Lab ID Sample [D: Collect Date/Time Matrix Sampled by 18-47765 Site: 001 11/14/2018 8:20 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.47% 11/15/2018 Fecal Density SFA 92216 E MPN 24 hr 503 <41 MPN/g 11/1512018 Lab ID Sample ID: Collect DatefTime Matrix Sampled by 18-A7766 Site: 002 11/14/2018 8:23 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SPA 2540 G 4.26% 11/15/2018 Fecal Density SM 02210 E MPN 24 Iv 103 <43 MPN/g 11/15/2018 .. 1-- 1., ....... ... ... . .......... .. ......... ..... . . .. ......... .. Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-47767 Site: 003 11114/2018 8:26 AM SoW/Sludge Client Test Method Results Date Analyzed ---- - ----- - Total Solids N W 2540 G 4,52% 11/15/2018 Fecal Density SM 9221c E MPN 24 hr 501 <40 MPN/g 11/15/2018 ........... Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-47768 Site: 004 11114/2018 8:29 AM Solid/Sludge Client Test Method Results Date Analyzed . ........ . . ........ ...... Total Solids SM 2540 G 4.36% 11/15/2018 Fecal Density SM 92210 E MPN 24 hr 501, <42 MPNIq 11/15/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-47769 Site: 005 11/14/2018 8:32 AM Solid/Sludge Client 'Test Method Results Date Analyzed Total Solids SM 2540 G 4.37% 11115/2018 Fecal Density SM 92210 E MPN 24 lir 50a <42 MPN/g 11/15/2018 Environmental Chemlists,'Ine,, 41't3v, �Ni?n) NC ')�4 6 , 4 +."3<:l. 2 2 a, I7D'.392.,+ 2r kl\ Nlnfo), NC. 27954 r,2A —,37€)' 1 I) :,i x, ANAI-YflCAL & CONSULTING CHEMISTS Brunswick County Public Utilities Date of Report: Nov '16,2018 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer 10: 08100011 Attention: Donald Dixon Report #, 2018-18859 Project ID; NEER Lab ID Sample ID: Collect Date[Time Matrix Sampled by 18-47770 Site: 006 11/14/2018 8-134 AM Solid/Sludge Client Test - -,- . ----------- Method Results Date Analyzed ----------- Total Solids (%) SM 2W G 4.46% 11/1512018 Fecal Density SM 9221 C F. WN 24 hr 503 ......... ........ . <41 MPN/g 11/15/2018 Lab 10 Sample ID: -- ------- Collect Date/Time Matrix Sampled by 18A7771 Site: 007 11/14/2018 8:37 AM Solid/Sludge Client .Test, ........lMet# oclResults ........ ....... Date Analyzed Total Solids (%) SM 2540 G 4.41 % 11/15/2018 Fecal Density SM 92210 E WN 24 hr 503 <41 MPN/q 11/15/2018 Comment Results reported on a dry weight basis Reviewed by.- Repoit 4 2018. 18859 Pane 2 of 2 LO O N O V rn v Z co ui o rn 75;�L E LL U ' N m V U. . wo 40 L.J z z F W Q V ZLU 0 00 >WON. Z LU rr� U z Z W E I.- 0 0 m as w z D O rcz cc D CD >, CD Q ; E © U m n � D 0 " z J.. II ' �u HAH10 � T II Z OIN-L 1 NQ H07N `Sr � SONH II w WVOSZH- ai ci y � l0H 3N0N I I LI if38Wf'>;N ED (it @V- 3 y II 'V5w aullOND t u .. (9 ao di aau;etuoo �J C"i U U' C7 U U C7 O U [L 0 0.. 0 j L gero [ ao U..C'31U`(7U U 3U UC�UU` 0 (DU{i atlsodwo0 \U i I ed i oldweg ca SIR C C O C � O � � V � i1 } CiL C tJ G r ri t E I.- 0 0 m as w z D O rcz cc D CD >, CD Q ; E © U NE Brunswick WWTP WQ0034468 Class A - 4th Quarter 2018 Date Fecal Coliform MPN per ram Log 11/28/18 43 1.6335 11/28/18 40 1.6021 11/28/18 41 1.6128 11/28/18 43 1.6335 11/28/18 42 1.6232 11/28/18 44 1.6435 11/28/18 36 1.5563 Total 11.3048 Average I 1.61 SO Geometric Mean 41 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Glenn Walker Lab ID Sample ID: NEBR 18-49636 Site: # 1 Test Total Solids (% Fecal Density Lab ID Sample ID: NEER 1849638 Site: # 2 Test Total Solids (%) Fecal Density Lab ID Sample ID: NEER 18-49639 Site: # 3 Test Total Solids (%) Fecal Density Lab ID Sample ID: NEBR 18-49640 Site: # 4 Test Environmental Chemists, Inc. 6)02 Windmill 1V<1y, Wilmirl fi>n, �C' 28� L15 910.392.0223 l,ab a 91031)2A424Fax 710 13mv,,(?rtown Rc)ac , IManteo, W 27954 . 2;52,173. 5702 l.&/Pax 25.5-A Wilmin�;ion Highway, jacksonvillc, IAC 28540 F 910.347.5843 Lab; Fax environ men ulkA Ills SLs.CO Ill Date of Report: Jan 03, 2019 Customer PO #: Customer ID: 08100011 Report #: 2018-19628 Project ID: NEER Collect Date/Time Matrix 11/28/2018 8:05 AM Solid/Sludge Method Results SM 2540 G SM 9221C E MPN 24 hr 503 Collect Date/Time 11/28/2018 8:08 AM Method SM 2540 G SM 92210 E MPN 24 hr 503 Collect Date/Time 11/28/2018 8:11 AM Method SM 2540 G SM 9221 C E MPN 24 hr 503 Collect DatelTime 11/28/2018 8:14 AM Method Sampled by Client Date Analyzed 4.19% 12/03/2018 <43 MPN/g 11/29/2018 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 4.50% 12/03/2018 <40 MPN/g 11/29/2018 Matrix Sampled by Solid/Sludge Client Results Date Anaivzec 4.46% 12/03/2018 <41 MPNIg 11/29/2018 Matrix Sampled by So€id/Sludge Client Results Date Analvzed Total Solids (%) SM 2540 G 4,24% 12/03/2018 Fecal Density SM 9221C E MPN 24 hr 503 <43 MPNIg 11/29/2018 Lab ID Sample ID: NEBR Collect Date/Time Matrix Sampled by 18-49641 Site: # 5 11/28/2018 8:17 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.29% 12103/2018 Fecal Density SM 92210 E MPN 24 hr 503 <42 MPNIg 11/29/2018 Report #:. 2018,19625 Page 3 of 2 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Glenn Walker Lab ID Sample ID: NEER 18-49642 Site: # 6 Test Total Solids (%) Fecal Density Lab ID Sample ID: NEER 18-49643 Site: # 7 Test EnvironmentalChemists, Inc. 6602 LVindntill kNay, LVilriington, NC 28405 . 91.0.392.0223 Lab t 97 0'.392.1424 Fx, 710 13ovv wrtc)vvn Road, Manteo, NC 27954 , 252.473.5702 1,nb!Fax 255--,,1 LVOniington T iigl�v��,}y, {acksojtville, N(' 285.40 r =9103417,5843 l-.ah/lax illi)!{„C Ii4'I roonlen ta1clkCnTISt S.Con) Date of Report: Jan 03, 2019 Customer PO #: Customer ID: 08100011 Report #: 2018-19628 Project ID: NEER Collect DatelTime 11/28/2018 8:19 AM Method SM 2540 G $M 9221 C E MPN 24 hr 503 Collect DatelTime 11/28/2018 8:22 AM Method Matrix Sampled by Solid/Sludge Client Results Date Analyzed 4,16% 12/03/2018 <44 MPN/g 11/29/2018 Matrix Sampled by Solid/Sludge Client Results Date Analyzed Total Solids (%) SM 2640 e 5.12% 12/03/2018 Fecal Density SM 9221C E MPN 24 W 503 <36 MPN/g 11/29/2018 Lab ID Sample ID: NEER Collect DatelTime Matrix Sampled by 18-49644 Site: NEBR Sludge 11/28/2018 8:30 AM Solid/Sludge Client Test Method Results Date Analyzed RCI Cyanide EPA 335.4 <0.05 mg/kg 12/10/2018 Sulfide SM 4500 S D <0.1 mg/kg 12/10/2018 Ignitability SW 846 method 1010 >215'F 12/31/2018 pH SW 846 Method 9046D 8.25 units 12/26/2018 Comment; Results reported on a dry weight basis. Reviewed by: - _ (C�!3 ,� �- _�-. ,4,� Report C 2018-19628 Page 2 of 2 yam. ... aa[aie;uq� ID IL L7 Cl C`3 m C7 4 C"1 t] C7 it '� "• (5 aklsnduio� County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory fi,wh Curolm" 1.U$oralll'1 Comfir[mon ;Yumbe, N('(9)901 ;Urns leRo:�x, La'+.Cvlxn7 u:: PO3ax 249 231 G,7 WaterHc^A1 rd[gH>: nr 91di-755-'1421 3aoiieia, \'[.' 23.52` tiup�riy, '`i.' 2S4ti'_ l:ax 91U-?cc.T727 ttejw}li Dale. 12.1:00-1018 LACffi1v S—WUIKF_F'!3C Sa.[ 1),11 1-1 dtt West Brunswick l Wrty Day Bench Beginning: 1/10/2018 Reduction of Vector Atiraction (<15% is considered passing) Regional Digestor Scale Test Ending' 21912018 as Required to Meet Option 3 7.40% WWTP BPA f508 13(b)(3)) PASS SDNR J i r Anna leRoux, Laboratory Supervisor County of Brunswick Public Utilities (XD West Brunswick Regional Facility Laboratory Noah Carolina 1-rrhrralru.v ('erlifirobt h Number" A'CM90.3 Anna lcRoux Lab Supaw�g VO Wx 249 235 (ircy W:jw Rmvi Tekplconc. 910.755-7921 lkwlivi-, N(' 28422 Supply, hC24G2 pax: 910'!55-7927 Repmi Dasc 77 -May -2018-2018 qac# 1 4>tinrnle "i'vac savil2le 118(c 'i"cst.dz A —ft hcett e'salts West Brunswick Thirty Day Bench Beginning: 413/2018 Reduction of Vector Attraction (e15% is considered passing) Regional Digestor Scala Test Ending: 5/312018 as Required to Meet Option 3 8.22% VvvvTP EPA j503.33(b)(3)] PASS SDNR (End of Repor3) ,` Certified by:✓`.;r Y:r ::, .. . 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Anna IeRoux, Laboratory Supervisor County of Brunswick Public Utilities Wast Brunswick Regional Facility Laboratory XmIllCrv,Amur.ahr,rnlnn N000.103 Ar:r.;, kRnux, 1.zh Su}+crvaor Mi 13r,x ?49 :175 (;irn� N�at� Kc�.�a i\^f<;ilicre hl t}.755.7t171 'SupplyAC 28.4(2 Vax 4}x'755'1927 .v.,.-..._._..._..._.._.o�� T s9 --.gid Rcpt}r( D;A(c 7t)-AUg�_2018 L-4 61 i t1v West Brunswick Regional WWTP SDNR "Sae. tiamp—] e -A —af C camd ORI —ts Thirty Day Bench Beginning: 7/18/2018 Reduction of Verlor Attraction (<15%n is considered passing) Digestor Scala Test Ending: 8/17/2018 as Required to Meet Option 3 1,94% EPA [503.33(b)(3)] PASS (:eljiiiecl try' [ ;f,,,;1,./.r... �� [�-•:"�-` - .... � Anna feRoux, Laboratory Supervisor (XD County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory NorrlrC.urvlirral.�rhoralary(.'errfc'ariunA'rrmhrr:' N(bU�13 Anna 1eRuux, l,ab SuMe isnr PO 13ox 249 235 Grey lYaicr Ruud 'fele enc; 910-755-7921 Bohvia, NC 28422 Sully, NC 28462 Fax: 910-755-7927 Rclxxt Bale: 7 -Nov -2018 ' c Ii it c'Mmak-PaLtst` bi 4 e t eti West Brunswick Thirty Day Bench Beginning: 10/3/2018 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 1112!2098 as Required to Meet Option 3 5.23% WWTP EPA [503.33(b)(3)j PASS 511N R Certified by: Anna leRoux, Laboratory Supervisor (ED County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory Narlh C.'nralbrn 1�bnrntor� CerYifrcalian Number: NCO0903 Anna JcRovx, Lab Supervisor I'() Dox 249 235 Grey Walu Road Tclgbone: 920-755.7921 BI)Nvi;� NC 25422 Supply, N(.29462 Fmx: 910-755-7927 Rcporf Date; 22-Pcb-2018 Eadfim jj 5t &_ Mcf, hod licse�lts Northeast Brunswick Thirty Day Bench Beginning: 1/23/2018 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test fi=nding: 2122/2018 as Required to Meet Option 3 10,00% WWTP EPA (503.33(b)(3)) PASS Post Tank End of Re orI Certified by: Anna leRoux, Laboratory Supervisor COnnty of Brunswick Public Utilities a. West Brunswick Regional Facility Laboratory North Cnrolinp l �rboralary C.'or� ferrlios NetnrLvr: NC0090.3 Anna lckoux, Jab Supervisor I'O Box 249 235 Gr7 i «'ntcr Road Tckphonc: 910,755-7921 glcr E x!i%;l;rniyaa,rsct l30iviu NO 25422 Supply, NC 294621 :uc: 910= 75 5-7_0 27 Repotl Date: 11-1)ec-201 S i+r�clll Sri Ic 1' a ,"81 Ic rite ' 'est & illetl ,Ad Northeast �—�---�--I-- ffic is Regional Thirty Day Bench Beginning: 11/7/2018 Reduction of Vector Attraction (r15% is considered passing) WV4TP Digestor Scale Test Ending: 12/7/2018 as Required to Meet Option 3 9.58% EPA [503.33(b)(3)] PASS SDNR End of Report) Certified by: Anna IeRoux. Laboratory Supervisor r.Vrr VlVrcl......V.L rVr 4U..... 8'1!!!...". "V'vvJVJ Anna IcRoux, Lab Supervisor PO 13ox 2A9 215 Cwey Water Road Telephone: 910.755.7921 Bolivia, NC 28422Supply, NC 28462 Pax: 910.755.7927 Report Daw 17 -Dec -2018 EHOUX Northeast Brunswick Thirty Day Bench Beginnial 11114/2M Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 12/14/2018 as Required to Meet Option 3 3.59% WWVTP EPA [503.33(b)(3)) PASS SDNR end — Re rt Certified by; '�LP. Y"' Brian Blanton, Laboratory Technician County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory Nor'l+Carolina LaboralmyC'v ijicalimtNumber: NCO0903 Anna IeRom, Lab Srptrvisor PO Box 249 235 Corey Wator Road Telephone 910-755.7921 ;ti�Ec,i whlviic g.ng� Bolivia, NC 28422 Supply, NC 28462 Fax: 910.7554927 Report Date: 20 -Dec -2018 Facility, Northeast Brunswick Thirty Clay Bench Beginning 1112012018 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 12/2012018 as Required to Meet Option 3 <1.0 TP EPA [503.33(b)(3)) PASS SD's R End of fie ort Certified by: Brian Blanton, Laboratory Technician s 8 i i 8 8 i 8 t i 8 = i s 8 3 3 2 C a 3 � m a I B B 8 8 s s 3 3 a s A 8 R m a i i E E 9 s =i i E i S Si 1 a i S � E i i R S = R s ' ^Nn � O IO r Cr V1 E �1 Ei F 3 � 3 i i E iE i 8 { 8 S � E i E E E S I i i E a E 3 S i i n ti i S S Z i f i E j 3 i i i 9 i g 4 E A MS LL I Q ^Nn � O IO r Cr V1 �1 U U Ci J '0I o 135Ln y y �C 7 tU N C O 0 W m E Z r W in LO w C�9 O m a 0 v OD n N I m a i i B i B s i Ei f i 8 i s = s 3 z i c i c i i i s 3 3 s l .j U U Ci J '0I o 135Ln y y �C 7 tU N C O 0 W m E Z r W in LO w C�9 O m a 0 v OD n N I m a m v CL S 8 8 = S i i i i s ' QS S fi n S n° 7 i i i 8 S 8 8 S S� S r� 3 3 s';+• S 7� I m v CL a B �i Q8 } i S i $ S+ 8 S 3 --9 Q12 si --9 i Q12 i a ! a E EE a s E g � E B I E i 4 � tL S a 8. $ E s � 5 E a 8 ti 3 i i i � 3 a ! fi a a w v w m m Z m m � I m Q a' CD ( (� r �J\ +n m 0 M [7 N N N � o N h LJ i i i a C> 0 c iD 00 N i a N Y a C S� a � bQ 9 8 'x 1 8 8 t i S i 8 8 i I i i i `a i s ?s i S i R 8 R a' CD ( (� r �J\ +n m 0 M [7 N N N � o N h LJ M a C> 0 c iD 00 N E N Y C S� a � bQ 9 v a �c i i B 8 8 3 i 5 S 7 i s R S R R �c a 0 L A C W t r M M O 0) in CD O �D r O `7 00 r LL N u7 0 rn M N EL9 N CN N a M N V v w 0 N 'M a 0 0 IR co G N N ■ 0 z Y cc F cc ' R }y}ys N CL m E 3:9 1 `7 Ed m a 8 S � S B a ! i 8 F s 3 F T i E ` a 0 L A C W t r M M O 0) in CD O �D r O `7 00 r LL N u7 0 rn M N EL9 N CN N a M N V v w 0 N 'M a 0 0 IR co G N N ■ 0 z Y cc F cc ' R }y}ys N CL m E 3:9 1 `7 Ed m a LJ T- m 0 n M m 0 rn m LL �i O V O N cn vi r: N d m N V V m N CV I IL o m O N O m m a � s 8 8 i s � s Q8 A S 7 8 i �L 8 c S .s a � S S R R LJ T- m 0 n M m 0 rn m LL �i O V O N cn vi r: N d m N V V m N CV I IL o m O N O m m a f i m N 00 (� J to N i i a' c s 0) T � 4V 4 v r LL m t Q LO t i a � u7 N M O V r Z co N 0) 0 N f r M ✓ � Il ri V a CCl Cn a a N O Z z � N 3 � N E d E z O_ V S 1 8 ; fi L E t i E s i S s= o m N 00 (� J to N o a' c K m 0) T � 4V 4 v r LL m t Q LO C O L � a � u7 N M O V r a co N 0) 0 N rS C W r M ✓ O � Il ri V CCl Cn C� v N O Z � N 3 � N E d E z O_ V S Q� bc) .............. . 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