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HomeMy WebLinkAboutWQ0009477_Residual Annual Report 2018_20190222Cascades Tissue Group — North Carolina A Division of Cascades Holding US Inc. 805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA cascades Phone: (910) 895-4033 Fax: (910) 895-9887 www.cascades.com ' Info@cascades.com Date: Feb 12 ,2019 To: State of North Carolina Department of Environment and Natural Resources Division of Water Quality Aquifer Protection Section Land Application Unit InolnQ 512 N SalisburySt. rncn Raleigh, North arolina 27604 RECifJV��'I N 1-919-807-6300 M 2 1 2010 Non-Dl5ct1 [9 From: Karen Bellamy-ORC and Preparer of 2018 Annual Report permittinguhit Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. 805 Midway Road Rockingham, NC 28379 1-910-895-4033 EXT 2280 1-910-895-1877 Fax Karen Bellamv&Cascades.com Permit # WQ0009477 Subject: Land Application Annual Report Cover Letter Forms Included: Cover Letter Annual Land Application Certification Form DENR Form ACF Letters from E. D. Black on Application Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, If K Soil, Dry Tons, Dry tons per Acre, Long and Latitudes DENR Form DMSDF and Additional Supplemental DENR Form RSSF DENR Form RSSF-B Lab Results TCLP, Ignitability, Reactivity, & Corrosivity DENR Form PVRF 503 Letter on Vector Reduction Page 1 of 2 % Solids, Acres, Wet Tons, Subject: Land Application Annual Report Cover Letter. Cascades have 1 ORC and 1 Backup with Additional backup soon at the present time. Karen Bellamy ORC and David Sheppard (just pasted test Dec still need to send form in on David) and Corey Wyand as Backup. Field Inspections where conducted, equipment calibration, PM work on equipment and backup ORC performed required inspections for the year. Corey Wyand and Karen Bellamy attended Rural Water Association Training in 2018 for our Continuing Education Contact Hours. Dr. Elwood Black continues to work closely with our land application Program. Advanced Residuals had No incidents in 2018. 2018 has proven to be a challenging year with Hurricane Florence and all the additional rain. We were able to stay in compliance of the 60 day spread time for 2018, but had to ask for an extension in Jan 2019. Worst weather and field conditions , since I started in 1994. We have made progress in Jan and hoping the weather will hold out %, dvanced Residuals has worked hard to have a good program. Cascades and Advanced Residuals has worked hard to make sure we have a good program that is Environmentally Friendly and also benefits the farmers. We have gotten a lot of positive feedback from farmers. Duke Goodwin is the Project Manager for Advanced Residuals project at Cascades. Mr. Goodwin has been a farmer for several years and also has worked at the City of Rockingham WWTP, so he is very familiar with regulations. Duke Goodwin also received his certification for Land Application in 2016 . Mr. Goodwin also received his continuing Ed hours for 2018. Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also been removed from our permit, since levels have been extremely low for over 10 years. ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0009477 County: Richmond Year: 2018 Facility Name (as shown on permit): Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Land Application Operator: Karen V. Bellamy Phone: 910-895-4033 Ext 74280 Lan application of residuals as allowed by the permit occurred during the past calendar year? Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summarv: Total number of application fields in thepermit: Total number of fields utilized for land application during the year: Total amount of dry tons applied during the year for all application sites: 25824.13556 Total number of acres utilizes for land application during the year: Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land applica ' n permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. W11yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Karen V. Bellamy Environmental Manager Permittee Nan}e and Title (type or print) Signature Duke C;oe Date Signature of Preparer* Date of Land Applier (if different from Permittee) (if different from Pennittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) E. D. Black Land Treatment • By -Product Ulikzafion • Soil Remediation • Wetlands • Bioliltralion February 5, 2019 Cascades Tissue Group POB 578 Rockingham, NC 28380 Attention: Karen Bellamy - Technical Director Dear Ms Bellamy: From January 1, 2018 thru December 31, 2018, FiberClay was distributed only to agricultural land. No farm field received FiberClay in a continuous year-to-year application as defined by the North Carolina Department of Environmental Quality respective to permit WQ0009477. These statements are based on information reported by Advanced Residuals Management. Sincerely F Elwood Black, Ph.D. - Soils lii� Efwovd 207E - -Sa0 Tana rwa fywm Tans Famrar Field _ Rain tlTa K Ar ri f Wen !D vl Use NK,YW,Y P,Y0. W2'7017 - RC 3NS.NF 42.5096 248 34 27.9MN 79 72.236W r927 e,prard Rd Rawfand, NC 2$3E9 34 49.029N 80 2.595 W 813 R.S. Salters Rd Chesterfield. NC 29709 _ 2301 Grass YK,NP,N W, YD,NS NF 42.50% 301470 a 12/5/2017 .18,554N 80 a.5l4W ArnonWevkd. Mi WHJI .NC 21107 }21dtE0l7 330A _ f Grass K,NW,NP ,YS.NF 42.50% 18 a � a 958N 80 7.850 W '- l nn-AvW.W Mww W9a Nc 26?0] 12narral7 - — 350-ITaN 79So. 9P8W Grass K,NW,NP YD,NS,N F 42.50% 130 a 7440 $tonll2Cp F Rd. Lnaev8la NC 28091 _ r=r[7R017 - 1•B96iC�Zy _ — — - - 34 �e.]saH Ba r.a75W Grass K,NW,NP NS,YD,N F 42.50% 47 a 91r4/2075 PC so. am HYd"ftro NC 28I70 35 2-863N a0 IFOW W RC K,NW,YD NSYFP 42.50% 20 40.42 f -UJ-M Ofi¢r 6EB aff 4723 Ansonvllle Rd. Marehville NC 9R71i'017 RC K, YW, YP, YD,YS,N F 42.50% i9 _ 3515 T74K 80 78 038ry r441 W Swropoton Rd. M., --d NC 28128 1/5/2018 35 8.179N M 79. 78b W RC K, YW,NP,N D.NS NF 42,50% 17 so 5407 Pleasant Hill Chruch Rd Marshville NC 28103 1/5/2018 35 3.799N BQ faS8f W RC K,YW- 2,YP,ND, NS.NF 42.50% 42 5407 Pleasant Hill Chruch Rd Marshville NC 28103 1lS'20r8 75 4.4aaN an 1 i 094W RC K, YW,NP ND,NS,N F 42.50% 28 U07 Pleasant Hill Chruch Rd. Marshville NC 28103 1/5/2018 35 5.032N at 7. S 78 lk STOP Pleasant Hill Chruch Rd MarahWfle, NC 28703 - 3i 29.114N 791s916iY RC K,NW,YP ,YD- 3 NS NF 42.50% 73 - Grass NK,YW,Y P- 2,ND,NS, NF 42.50% 58 a f0/18/2017 1927 Gerald Rd N9wQand NC 2a388 f0/f8/2017 1 RC NK, YW,N P, YD,NS, NF 42.50% 55 a 34 29.969N 7913.539W 1927 C Wd W Rowlwnd NC 2e382 rre9nbla RC NK, YW,Y P,YD- 2NSNF 42.5O% 27 ARM S1 Awa 34 29.B97N m 13,3saw - 5338 Hwo 138 East Rawlantl NC 28382 - a a a — a I E11re0d 2018 tons Tnns Moh1h TMa I Field Rain ACrea r Use Feb IGb.d K,NW,YP ,NS,ND,Y 9/2'2017 _ RC F 43.7011 39 a 35 9.607N 80 19.269W "a St 7ilnnth Rd. Marchv'H NC 28103 YK,YW,N F,NS,NP, 10/5/2017 3727 Grass i YD-2 1 43.70% 63as 34 50. 77TN 80 8.28x W 0210 RMSWqtl Mvlrcoe NG 26172 YK,NW,Y F,NS,YP, !0/5'Y017 3r28 Grass YO 43.70% 80 34 s>:793N 80 .227W - 6210 Plim Ad Mantua NC 28}}2 NK,NW,N F,NS,NP, 10/18/2017 - RC YD-2 43.70% 297 — 34 29.067N 79 12.953W }927 G—M Rd. RorNarM NC 28383 NK,NW,N P,NS,ND, 10/18/2017 N RC NF 43.70% 38 74 29.7}NN ,l I.1.1v9W }917 Gerald Rd. Rox mnd. NC 28383 NK,YW,N F,NS,NP, 10M8/2017 - 34 36.947N 7.9 14.840W RC D-3 43.70% }55 9927 Gva Ad. %*&nd NC mm K, YM 2,NF,NS, 11M/2017 Grass YP-2 D-3 43.705 95 34 63.8 N 7. 1"W 3N, 9'W Rd Maauae Sc 21U79 NK,YW,N F YS,NP, YD-5 43.701' 128 a920W F12.712 19 t 7 Old Baher Rd. Mar NC 283W K,YW- 3,NF,NS, 3,x1A Grass YP YD•2 43.70% }}8 H61.002NAD5.WSW Po Sox 56a Wadee6op NC 21170 NK,NW,N F,NS,NP, lOMilR017 RC D-5 43.70% 139 a 34 32 69711 79 1 }.791 W 7927 Gerald Rd Rowland NC 28382 — K,YW,NF, Tpauld _ RC NS NP 43.70% 21 a 35 9.246N 2'0 19 315W 9 $07 Pleasant Hill Chruch Rd. MarshNlle, NC 28103 K,YW,NF, 1/5/2018 RC NS NP 43.70% 17 a 36 i1.102N 8018.505 W U07 Pleasant Hill Chruch Rd Marshville, NC 28103 K,YW- 2,NFYS, YP-2,YD- 2H27T018 Grass N 43.70% 229 a 75 �9.50UN 79 39.489 W 190 Nndslde Ot. Srar HC 2734r K,YW,NF, NS,NP,D- 2M2R018 Grass 3 43.70% 94 a 35 26, 286k 79 44.53 r W 190 Ikllsldn Or. Sear NC 2734} K,YW 2/12/2018 _ 35 77.984N 79 46,010 W Grass 2,NFNS, iNP 43.70% 25 a f 80108sIde Or Star, NC 27741 trf 2/21YL018 — — - Grass 43.70% 25 a 34 55.76IN 80 10.8 } 2 W Emma I MT6 i i I SuR I Tans T e Monrh Toga F.—Field Rain K Arn s Use Mar Good K,YYK $NF,NS, Grass YP2 D-3 47.40% 95 a3453.606N 80 7.194W7001 flda4 d. Va NC 28379YK,NW,N pfl.M P,ND,YS, RC YF 41.40% 56 7b72193ka016739W1434a Md}.ester Rd Oakbw9.NC 26129K,YW,NP ,YO- _ RC 3 YS NF 41.40% 79 35 l3.355N 80 t6.}6pW 1 All" Mc�eater Rd Oakp9ro NC 2l1a YK,YW,Y P,YD,NS, 11H92017 RC NF 41.40% 34 .fr0w no 1.7 T028tlti18 a 15 14.291 N a0 1 7.%M W 14W Mcl."Mr Rd. O4kbola.NC 2,8129 - K,YW- 2,NP,YD- - 11/192017 RC 4 NS.NF 41.40% 4f a 35 15. r38N 80 18.923 W 1434a lit"atvr Rd. Oakbom NC 28729 K,YW, YP, YD,NS,N 11/19/2017 RC F 41.40% 37 a 3S 14.82N.- 70.fM7W 14348 Melesler Rd. O4 kbolo.NC 22129 YK,NW,Y P,YD- 11119/2077 RC 1 YS,NF 41.40% 110 a 35 1 S118N 811 2'L 941 W 14348 MnLeeler Rd O.M.re NC 28129 YK,YW- 4,NP,YD- 11lI92017 RC 2 NS NF 41.405 38 a 35 13.314N $0 21.663ri 14348 Mc4esun Rd. Oaht—O.NC 2612E K,NW,NF ,NS,NP,Y 11/142,111' b5 17-026N 80 lcw2W RC D-2 1 41.40% 22 -41850 Carrlkof Rd. A;bwnuwla NC 29IW 1 K,YW,YP- 3,YD- f1/O1M7 Grass Z YS NF 41.40% 45 35 2.343N 60 19-J02W 2823 Marshville Olive Branch Rd. Marshville, NC 21l103 K,YW,NF, 1227/2017 0 Grass NS YP 41.417 140an 2J 56.110N NO 6-8Y6W nQ 8pr 65$ Wmdasboro NC 26170 K,YW- 2, YF, YS, 11142018 _ 35 18 18YN 010 45.7733Y RC YP YD-6 41.40% 105 am 21fi57 Cerri'k,-Rd. AL"maNa NC 7800r K,NW,NF NS,NP� 1/42018 RC YD 41.40% 31 a.t 11 3b }B.074N 60 7T+-6J9W 1657 am Rd. AahrmJlhf NC 28001 - K,NW,NF NS,YP- _f'a2018 Grass 2.YD3 47.40% 64 be 75 1T 843N Be 75.6Y9W 93556}7N 21657 Camper Rd Albemarle, NC 28091 K,YW- 2,NF,YS, 1r5r2ara RC YPYD3 4f.40% 174 8018.951W 5407 Pleasant Hill Chruch Rd Mesh viW,, NC 26103 K YW,NF, YS,YP,Y 223201E Grass D-2 41.40% 54 ?i J8-813N BO 8 379 W Ma —dfu a Rd Morv9rl 220119 _ 2/23/2018 34 49.28MM9 Grass K,YW,NF, NS, YP,Y D 41.40% 25 a Ma 0-M, Rd. Af— 28119 2/23/2018 - - - Grass K,NW,YP NF YS 41.40% 20 34 50.470N 80 7.417W svi0e Rd- • Morvan 28119 34 52.482N 79 59.919 W 3112/2018 Grass NK,YW,Y P, YS NF 41.40% 62 i 1r.H;;: 11w• 145 Morvan..NC 2811p AW 3/12,2018 I NK,NW,N aQ 34 51.797N 80 0. 573W Grass P.NS NF 41.40% 7 _ 3H2r201B 19802 H �/5 kpryan NC 28518 34 51.590H 8Q }_040 W Grass NK,NW,N P,ND,NS, NF 41.40% 11 e f08021iw 145 Marren ,NC 2B119 3111/2018 0Grass 34 50.250N 80 1.481W 10802 Hw 145 lurrran .NC 28119 Nk,NW,N D,NS,NF, NP 41.40% 13 3+r3l2DTB — - 34 50.461N 801.557W Grass NK,YW- 2,NPYD- 2 NS NF 4f.40% 89 a 11204 NSW 14,9 Suu1n Atom*n NC 28119 1.]3Ej]�' _ 34 51.220N 80 7.108W 11 POf HWY 1f5 5au01 Mo—n NC 28119 3M3R01B Grass NK,YW,N P,ND, Y- 3SNF 41.40% 45 a - 3n3,2018 3/ 50, 804N /0 f.093 W Grass NK,YW- 2,NP,ND, YS-2NF 41.40% 105 a Tt2m HWY US$0ufh Af r MNC 28119 31}212d18 094'4: -�2.ggpyiy _ _ Grass NK YW N S ND NF 41.40% f0 — /0.5.+fg9. 48 1.91 a _ 34 49A67N 80 pJ�9yW _ �10002 Hw i4S M..rvan.N C 26i 19 a 3/23/2018 RC 8 Ha NK, YW,N F,NS,YP- ,YD 41.40% 35 4.581 N 79 f8.0f4W 948 GM-y !eland Rd. Ellerbe NC 28338 Month 5170.25000 2140.48350 E761wd 2018 1 Sou Tons 7 ddontn Tam F Field I Rain K A— K, 35 25.479N 79 44.696W - . Dr. Sea roe&, NC 97Mt K,NW, YP ,YD,NS,N 2rt3l2D18 Grass F 44.80% 18 Yi apA 76aL4 a 79 44.635W -' LMia Candor K,YW- 2,NS,NP, zr=olg SWOWn Grass NFD 44.80% 20 a 711 WhaN . Nabuns sK,NW,NF 2QT/2078 Grass D 44.80%a 79 WTrstl Rd. Ruhbina 7732j K,NW,NF 2/22/2018 m Grass NS,NP 44.80% 16 a 35 28.997N 79 39.472W W8 Nuv^n WhOM R0 Robbins NC 7.7325 K,NW,NF 2/22/2010 Grass NS,NP 44.80% 20 a 35 26.598N 79 39.413W 144 ,l on Wnnel Rd, Robbins NC .7125 K,NW,NF ,NS,YP,Y 3/6/2018 Grass D 44.8011 34 3527-217fa 7938.078W 1as 9l4 Cedar HA Rd -bin, NC 27325 K, YW,NF, Grass NS,YP,N D 44.80% 12 a 3,fr2618 75 27.37SN 79 37.938W 1984 Cedar Rill Rd. rohrns NC 21325 K,YWNF, A NP,D- 716litl18 Gress 3 44.80% 25 35 27.247N 79 38,076 W I Cod. Ni9 Rd. -Nm. NC 273p5 K,YW,NF, NS,NP,D- 3/7/2018 Grass 4 44.80% 69 3518.5dQN 7945.171W 2365 Jim Ro RnWns. NC 21325 NK,YW,N F,NS,YP, 03/23/18 Grass 8, RC YD-2 44.80% 31 a 35 4.271 N 79 49, 5X 948 G'a..v Island Rd Ellsrby NC 283M K,NW,NF 03/23N8 RC ,NP,YD,N S 44.80% 44 ME T. a ]5 4 974N 74 4B.193'4`d 948 Smay Island Rd. Elterbe,NC 28338 KNW,YD YS_ 122'YF'yp 4/5/2018 a iK - RC 44.80% 58 --numb," a, 25 10.444N 60 4.333 W 40445Mr lion ^.Porch Rd Norw d,NC 28128 - --- - - YKNW,Y P, YD, YS, 4WO18 L42 -- _ RC YF 44.80% 46 s d E 4 p50474 : a4 35 10.345N 801.H 72W 40ruE4N. 712, CNarrh Hd. No sd. NC MM � K,YW,NF, — NS,YP,N 411=018 Gr.s D 44.80% 40 aJ 35 23,485N 79 +8.305 W 21,13 Canny Cross CMwch Rt. AshbWv NC 27206 K,NW,YP ,ND,NS,N 4/23/2018 Gross F 44.809 3528.6KSN 78 37.814W 488 Lambert Rd Rahbdns . NC p7325 K,NW,NP ND,NS,N 4/23/2018 Grass F 44.8094 8 a 3525.567N 7944,636W 488 lanrmert Rd. Rnhhins,NC 27325 _ a a Elwcod 20T8 1 1 1runs M11�ntl1 Tgrra Farinur I Field j Rain K /leree Is7Cr Use may Good K,YW,NP ,NS,YD- 10/16/2017 Grass 3 NF 44.60% 58 a 35 26012N 79 38.385W 4807 Up- Rd Star NC 37756 K,YW- 3,NP, YD, 10/1612017 Grass NS NF 44.60% 42 a 35 2C012N 79 28.986W 4546 Woodlern Rd SeeerOve,NC 27341 K,YW- 2,NF,NS, 212212018 Nesa Grass NP YD4 44.60% 129 IIALMI 35 28.598N 79 3S.413vi -- 146 Wiliton wheel ad Robbins NC 27325 K,NW,YP 1/2/2018 Grass ,YD- 2-NS,NF 44.60% 25 1Jp7,t},i8aa 3s+11.4r5N r943 246W 4546 Woodlern Rd Sam —AC 7734} K,NW,NP rr2/2016 Grass .NS NF 44.60% 25 a 354d.TNN 7943.7{S W lute Wovdlern Rd. Ieve.NG 27341 K,YW- 4,NF,NS, ICL2018 Grass YP YD-5 44.60% a 3634.674N T939.8{.3W 7005p ErKI Rd 94 rvYv NC 28320 d2. K,NW,NF , YS, YP,Y 1/2/20f8 Grass D 44.80% a 79285}5W 3573.76 . 70060 Er wl Rd. Sr NC Z8220 K,YW- 3, YF,NS, YP4,YD- Y1/201B Grass 16 44.60% 448 35 24.877N 78 49.210E 2or0 rrtevmmseea Rd. T .NC 77511 K,NW,YF, T/f/2018m RC YS NP 44.60% 29 a 35 25.734H 79 5R 048 W Z010 04--- Rd.7 .Nc V571 K, YbK 3,NF,NS, 2/52018 Gross NP D-3 44.60% 95 a 15 ]3.79 39.854 W 959N 7530 &.an Rd y NC 77341 K,NW,NF ]lr2�3wa - _ ]S 27.538N T9 4tl.563w 1904M.ids. Or. me KC 2 T U I — 35 26, 2B6ty 77,u.511 w _ 740 Hillside DSe -rove NC 27341 Grass ,NS,NP,D- 6 44.60% 62 a 2112MIS Grass K, YW, YS, NF, YP 44.60% 94 a K,YW,NF, YD- N9M 2/121018 - it18+1i 0,1• JS Z6.596N 79 Aa.943W Grass 3.NP.NS 44.60% 61 a _ T8R Hillside r Sea rove NC 27341 — - K,NW,NF - 3/8/2018 — Gross NS,YP,Y D 44.60% _ 34 a 15 2r.2Pry 79 39.076w 1964 Cedar Hili Rd. robins NC 27125 K,YW,NF, YS,YP,D- &12/2078 Grass 2 44.60% 65 121662" 1. a SS2H]i0 7915.752YV 19[I HIII�We. Dr. Sea rove. NC 27341 NOWK,NW,NF Ep, NS,NP,D 21122018 Grass 6 44.60% 20 a 35 30 U-P; 79 45949W — 190 HiIIaide. Or. Sea rove. NC 27341 KYW- 3,NF,NS, 7/fY1015 35 27 951 N 79 44-739 W - 051 BOC 1T85!r6H.(1�-B�Srffke�P" Gross YP.D-3-- - - 190 NkOsldu-13, Sea rove NC 27341 KYW,NF, ' NS, YP,N 0f9 35 27.725N 79 37.9JBW - Grass D 44.60% 12 _ 1984 Cedar HIII Rd robins NC 27325 K,YW- _._ _ _ 3/1I20f8 3,NF,NS, 35 3525Jim : Grass tEiGress YP-7 O-4 44.60% 105 . Robbins9.40 . Jim Rd. Robbins. NC 27325 NKNW,N F,YS,NP, 3/7/201B D 04.60% 65 75 16-663N 74 48.]85W 2365 Jlm kd Robbins NC 27325 KYWNF, NS,NP,D- 3/7/20fB Grass 4 44.60% 89 a 75 78-549N 79 46 17] W 2365 An Rd ReWilns NC 27325 KNW,NF 7H/7018 Gross O 44.60% 13 � 35 22.466N 79 45750 W ag 2010 Ok�mae Rd. Twv. Nc 27371 - KYIN, YF 2H40111 73r NS,YP,Y 35 25.580N 79 50.287W 2010 06—emee 12d- 7r NC 27371 Grass D-2 44.60% KNW,NF 2H/2018 ,YP- 35 25.857N 79 49.659W Grass 2 NS ND 44.60% 34 2010 nFeewemee vd Fro NC 27371 KNWNF 7H2r20lB Grass NSNPN D 44.60% 20 - a757fi614N 734d.820W 190H'i.id.Or. S1ar.NC 27341KYW,NF, 49!77 NS,YP,Y V-33rN 74 42 408 W Grass D-3 44.60% 3f- - �7l7f a3S - - 490 H!Il.Ide Of S1ar,NC 77341 KYW - 5H5/201B 2,NF,NS, 35 32.944r1 79 39.BBBW j Gross P-2YD-3 44.60%. 81 '70.b70617 -- Tl -a PO Box 469 Se rave NC 27341 -- - - i KNW,NF - -- ,NS,YP,Y SH8/2018 Gross D-3 44.60% 37 353] i96N T442_24MN a 127B8 R4inlr Lawrence Rd- Rohhln.-NC 27341 M1f1fh 5015. 78WO 2237.03788 EW—d _ 2018 i I So i i Tans M n, 4hnM Tans Fspnry Field Raln Acre. Ilse June Good K,YW,NF, fOn64017 Grass NS.YP.d 44.50% 56 24 35 .578N 79 42.746 W 4803 S les Rd Slay HC37351 KNW,YF, Nrr20r8 RC YS.NP 44.50% 117 .. 35 25134N 79 5004£ W 2010 OP9ewa—Rd.TroNC :15 r! YKNW,N P,ND,NS, 2N/20f8 RC NF 44.50%It f3 a a5 7S a77N y9 J9.4T8W 2010 Okxer.emro Rd. 7 NC 22,371 K,YW- 3,NF,YS, 2/5/2018 Grass NP D-3 44.50% 95 ag 35 3z.959N 79 3A.864 W _ I., Erecr Rd Sea re�y,NC p73►1 K,YW- 2,NF,NS, 211212018 - Grass YP-2 44.50% 228 a 35 26. 9500N 79 39-OM W 190 rfllaida Dr. NC 27141 KYW,NS ,NF,NP,D- blZr2m8 Grass 3 44.50% 94 a 35 25. MN 17,44.61W 190 "Insrdr. DI. Nq 27341 KYW- 2,YP- 7,YD- 2Y2612B18 Grass 1 NSYF 1 44.50% B35 a 1530A89N7921.7B1W 558 So Ah Carbm bM Rd Sadord NC 27830 K,YW,NF, 3/6/2018 Grass NS YP 44.50% 12 33 2722SN 79 37.938'W 104 Cedar HWI Rd robins YC 27325 KYWNF, -- - - NS,NP,D- 3.0e'J018 - Grasa 3 44.50% 25 - - 00 35 27.MdAY 79 38.133 W 1984 Cedar Hlll Ro robins NC 2:375 K,YP- 2,NW,NF, 3!7/2018 Grass YS" 44.50% 221 a 3526.5714 79379/5W 2365 Jim Rd. Robbins, NC 27325 K,NW,NF 2/1/2018 Grass NS NP 44.50% 9 a 3s 26.589N 79 60 2RTW 2C10 04eawamm Rd. rro . NC 27371 KNW,NP ND,NS,N 2R�DT6 Grass F 44.50% 11 a 35 26.049N 78 49.eSTY1 2v10 �TIPI�21111 KYW,NF, Grass YP,NS,Y D 44.50% 34 N1l28T8. 3526A52 7941659W 2070 Dk� did. Tra . NC 27171 K,YW,NF, YS,YP,Y 211L207B Grass D 44.50% 31 35 Y1331N 794L408W 190 HlElslde Or, Saw.NC 27347 a a a Crwood 2"0 i7ores 7 ¢ ,Ila Tana Fonyw Rain 7 K Arms Use Juk Good KYW- 5,NF,NS, f0141Z017 Grass YF-3D-6 39.40% 127 a 36 14,307N f0 2P480W 73805 81 tJah Rd. Qahfb—. NC 28r29 — — TONROIY 3514.231N 80 22.899 W Grass KYW,NF, YS YP 39.40% 43 1 a 12805 nr L1rk Rd DA&bam NC 28129 K YW- — 2,YF,NS, TO/4/30Y7 _ _- 1514 f22N H023977W 47aY16 e& Z � Grass YP D4 39.40% 96 - - -- a 128D5 ildl Rd. OWA NC 28129 KNW,YP- 4,YS,YD- }014R017 --- — Grass 5NF 39.40% 192 a 35 72.577N 80 24-128 W w 1 T2805 iJck RY OaYsbora NC 28129 NK,NW,N }r21"lOTB Grass FNSNP 39.40% 35 a 3d 329I2N 79 3A.461 W iP030 E 1 Rd Se NL '1833H KYKt 2,YP- 7,YD- 2�36rMfe Grass 12,NSYF 39.40% 835 a 35 30.389N 79 21.701 W 556 South Carbonton Rd- Sanford,NC 27330 K,NW,YF, Grass YS,YP- 2 D4 39.40% 60 a 35 31.883N 79 21 46aW "-;56 Souln_ Carbanton Rd. Sanford,NC 27330 K,NW, YF, YS,YP- 2/26/2018 Grass 5.D-7 39,40% 328 ' SSB South �arbanron 11d- Sanlerd,NC 27330 K,NW,NF .. ,YS-2,YP- 31}3lY078 - Grass 4 D-6 39.40% 52 - a` 36 26.335y 79 35.73yW 596 Mamas Rd. ROW" NC 27325 YK,YW- 2,NS,YF, 3/20/2018 Grass YP 39.40% 56 ] 5 27.377N 79 4R MW 947 Dan Rd Rabb—, NC,2732; YK,NS,N F,NW,NP, 3/20Y2o78 Grass D 39.40% 28 f+..l a . ]527.793N 7830.475W 947 Dan Rd Robbtna. NC 27325 K, YW, YP, YS,YD,N 8/15/2078 35 34,444N 79 38.311 ri Grass F 39.40% 55 a 5908 Asb18 Lh. Se ove NC 27341 K YW,NP 6/15I2018 Grass NSD.NF 39.40% 25 a 35 34.119rd 79 38.001 ri 5906 yalR Ln. 5 ova NC 27341 K YW,NF, 8/15/2078 Grass YSNP 39.40%E26 ]5 ] 7.548 79 37.711 ri -- 51M A&Wfi Ln- rays NC 27M1 — — KYW, YP, 2R[:/2018 Grass NS.NF 39.40% a 35 30.7d8N 79 23 5W 556 Soul Lafbo.Wn Rd- Saalotd NC 27338 77 39.40% ad 39.40% 39.40% a up i 2018 1 1 Soll I T—a To Lfvnfi Fleld Rain X 8c+e1 wer-ja Use A yq Good K,YW,NF, lO/4l2017 Grass YSYP 44.60% 43 a x614.x31N 80 22899W 12"!; HJ Lick Rd. Dak Strom NC 18129 K,YW- 3W412tl17 -- — Grass 2,YF,NS, YP.D-4 1 44.60% 96 a z5 r4.42xN ea 22.9x7w 12806 ft Lick Rd-Qakmerc NC 26 29 K,NW.NF TOpY20i7 Grass ,NSNP 44.60% e 35 14./ 1TX By T4.3sOW IMS ft UCk ft. Oaksbwo MC 28 UP K,NW,YP- 4,YS,YD- 1 017 Grass 5 NF 44.60% 132 35 12.577N 80 24. 198W f2888 Slo Lkk Rd. 01*100tb NC 28129 NKNW,N F,NS,NP, TNrd T RC D 44.60% 6020 34 ]v.993M 79 t 2.885W 1927 Cerald Rd. Rewrand NC NK, YW,N 112912018 RC F. NS NP 44.60% 25 ag 34 27 491N 7911.727W 5338 Hwy 130 East Rowland NC 28393 NKYW,N 112912018 - RC F NS NP 44.60% 15 34 28.54 TN 7912.394 W 5211HY.Y 1 j0 Ea11 Rriwland.NC 20.193 NK,NW,N F,NS,NP, 1129/P0f8 RC D-2 44.60% 40 a 04 32.389N 7913.273W 5338 N 13o Fa Rowland NC 28393 NKNF,N 1R911W18 - RC WNSNP 44.60% 25 a 34 33.236N 79 13 432 w 5338 130=EZ NK,NW,N F,NS,N,Y 1128/2016 RC DP 44.80% 9 a 3{ 307N 79573f f30NK,NW,N FNSNP,RC YD-3 44.60% i 51�6 H wy 1] Eax r Rolland. NC 28393 NK,NW,Y - F,NS,NP, _ xlxR7018 _ RC D-5 44.60% 59 a 9 -3439,0S�N 791x.8POW 75 Rd. Pi hei* NC 2072 NK,YW- 1,YFNS, 2/29/2016 29 a RC NP D-4 44.60% 3437,997N I9 P}_pBrW 75 0—Rd Pe b-hv, NC 383?2 — NK,YW Y F,NS,NP, 2/29/T016 _ RC D-3 44.60% 76 -- : TMau 34 ]7 395N 79 iv.99aw 75 Gale Rd. Pemhorka NC 28372 — NKNW,Y FNS, P, T128r2016 RC 2 44.60% 63 sT.7464 - a il 34 37.0*4N 79 U8.094 W 75 Gene Rd. Penmorke_ NC 28372 KNW,NF NS,NP,D- 7/29/2016 RC B 44.60% 75 a 34 40.714N 79 06.154W 75 Cene Rd. Pemborke NC 28372 NK,YW,N F,NS,P,D- 2/29/2016 RC 3 44.60% 94 a 3s 45. TlBN 79 06,4�! W 75 G9 Rd NC 28372 NKNW,N F,NS,NP, 2/29/2018 RC D-2 44.60% 46 - a� 34 42. g4 } N 79 00.778 W 75 Gene Rd 7�adwr NC 2837T � Nk,NW,N F,NS,NP, W29/2016 R7 YD-2 44.60% 30 a 24 4 f,73ar17906. 143W 75 Gene Rd Pemborkv NC 7a373 NK,YW,N F,NS,NP, 2/29/2016 RC D-3 44.60% 64 a 34 43.772N 70 06.49DW TB Genv Rd. PM16v1 20372 NKNW,N FNSNP, f1ffi10 RC D5 44.60% 36 a 34 38.029N 79 11.812W 75 4mla Rd- FambarimmCM72 NK YW,Y 7/3f 8 RC FNS,NP, D-2 44.80% 61aq 3439.M14N 7914.f03W 545 Burlei h Rd. NC 253? 7 NKNW,Y F,NS,NP, 713112018 RC D-2 44.60% 17 a 3410.007N lJ.853W 5 5: A RQ P.nebroke NC 28372 NK, YW,Y 7Rl1207a F,NS,YP, 3438.531N79 s3.855W RC D-2 44.60% 57 54e P.urfel h Rd Pemhroke.NC 28372 NKNW,Y 7131R078 -CUAWMF —IV- _ RC F YS NP 44.60% 9 134,37 299N 7g 1T S44W 545 Burkmh Rd. Pembroke NC 28372 7/21ROT8 RC NK,NW,Y FYS NP 44.60% 10 34 ]7.99bN 7¢Y].f79W 545 Burlei N Rd. Pembroke NC 28372 NKNW,Y FNSNP, 7l41f10T8 RC D 44.6051 11 34 41.526N 79 15.970 W 545 Burlwah Rd. Prmbrake NC 20372 NK,NW,Y Jl31l26T8 Grass FNSNP 44.60% 8 34 38. S07N 7014.064 W 545 Durlel n Rd. F mbr ke NC 28372 NK,NW,N !0/f8/2017 RC F,NS,NP 44.60% 30 a 34 28.386N 79 ! 1.047W 1927 Gordd Rd. Roy ww.NC NKNW,N F,NS,YP, 10H8/2017 RC D 44.60% 26 a 34 wykm 7a 11. 151W 1927 Gma d Rd Ro NK,NW,N 10M8/2017 RC FNSNP 44.60% 2T 3e 29.045N af1.S95W 192r Gerald Rd. RoMgrld NC NK,YW,N F,NS,YP, 10H8/2017 Grass D-2 44.6u% 1 65 a 34 30,3"N 79 11.511 W 192T Gvra�d Rd- Rowland NC NKNW,N _ _ F,NS, YP, 10M8/2017 — = 34 31.128N 79 12.195 W a Grass YD4 44.60% 83 a 1927 Geraid Rd. Rowland NC I NK,NW,N 10H8/2017 271B9Rn?+Sieger pFe,-,d;rre I P5a3 34 :.:.321N 79 12.694W 19:7 Rowland NC Gross F,NS,NP, YS 44.60% 85 _ -- NK, YW- 2,NF,NS, 10/18/2017 *e, Gross YP YD-2 44.60% 68 }4 30.757N 79 13.856W f92 7 GmId Rd, Rowland NC NK, YW,Y _ F,NS,YP, H!J/101B RC D-2 44.60% 74 Y9.074{4 *$1d6437�1 a 34 25 576i� L640 Mai WtW fdC Y8382 .. — NK,NW,N 8/3/2018 RC F,NS NP 44.00% 10 a 34 iR2991J 79 T"930Y1 2648 Marlette NC 29362 ' NK,NW,N FNS,NP, RC YD 44.80% 41 a 34 29209N 79 11.536w 3877E ham Rd Folr nt. NC 28340 NK,NW,N FN$,YP, 8M7/2018 RC YD 44.80% 28 a 3420MON7912.088W 3377 E R ham Rd.'eirrn; 0nr NC ig NK, YW,N F,NS,NP, 8/22/2018 - RC YD 44.60% 52 34 44.861 N 79 9, 513W 1312 J 1. RP Manton NC 23384 NK,YW,N P,NS,YD, dY18ROT8 Grass YF 44.60% 28 34 40.617N 70 4. W t 374 "sr * Fwtv Rd =NC 28364 NK,NW,Y P, YD, YS, 8l28lJOTd - Grass YF 44.60% 12 {1i7000 y{ jy,yY(W 79 !4"387W -- 406 Trmbar ❑ak Rd. wovAand NC - NK,YW,N P,YD,NS, 8l2IMS >♦ 39.0:0N 7H 14.273W RC YF 44.60% 12 1 a — - — — - St 170 E4rcn Rd. Pamblok*NC 28372 NK,YWN P,YD,NS, 8f79r1'!Y!d RC YF 44.60% 32 T. 1694 _ a 3439.970N 79 ti]27]W 170 Elmce Rd Pkmhroka NC 28372 NK, YW,Y P-4,YD- 8/29/2018 RC 8 NS YF 44.60% 19 -it 34 38.955N 79 11.839W 170 Etarce Rd. 139mbmke,NC 28372 NK,YW,P ,Y0. 8/29/2018 RC 2 NS YF 44.60% 28 a 34 37.906N 79 10.388W M7 Cam= Rd. Pembroke NC 28372 NK,YW,N P,NS,NF, 8l2A 101d RC YD 44.60% 1{ a 3{41.0 f2N 79 f3207W 170 04" Rd. Pomtlfekv NC 28372 NK,NW,N P,NS,YD- 7lFrJ01a Gross 8 RC 1 YF 44.60% 67 a 34 {O.T71N 79 T4,{f6aW 304 MC HWY 7101Aulcn.NC 28384 a a a — � a Ebmgo 1 2019 7vns oRa dr Tons I Fr Flefd Rain K A — Sept I Good K,NW,NP ,YD,NS,N 1/5/2018 RC F 46.10% 23 a 358.10PlaesanN8018.SO5W 3407 r Hill Church Rd. Marshwflm NC 24702 K,NW,NP ,ND,NS,N 1fL20le RC F 46.f0% 18 asr.9a3N aB fe.7e9w 5407 Prwsanr HM Church Rd. +farshv8/a NC p6102 KYW,NP ,YD- T/Y3Ol8 RC 3,NS,NF 46.10% 33 e $407 Pleasant f liN Chuleh lid AfarehVlNe NC T8l87 KNW,NF ,NS,NP,Y 1/5/2018 RC D-3 46.10% 36 a 15 9.321N 80 14.721W 5407 P/easanr N!0 Church Rd. Alannvr8e NC p8r07 NKNW,N 129/2018 - RC F NS YP 46.10% 24 a 34 2&MWi 79 f0.051 W r 583s fla 130 Farr R*$w&,?GCNC 28393 NK YW,N L F,NS,NP, 112912018 —0 RC YD4 46.101 170 a 34 iY. P37N 79 9.676 W 5.338 H 130 Eaaf Rowland NC 28393 KYW- 2,YF,NS, 3/20/2018 Grass YP 46.10% 56 a 75 p7.Ji7N 79 w.f97W 047 Dun Rd. Robbom.NC NKYW- 2,NFNS 10/18/2017 -_ Grass YP YD-2 46.10% 6s all 34 3f1.957A 79 13 058W i9T7 Garafd Rd. Rowland N NK YW,N F,NS,NP, 0PV29/18 RC YD-f0 46.10% 114 a 34 40.083N 79 7 649w 936 Gene', Rd Perna -A. NC 28372 - NKNW,N g•77,7018 8 air 3r 10. r J rN Is r 2 0rsw Grass FNS.NP 46.1036 3577 E R.o-J, am F.7—t. NC 28340 NKNW,N FINS,NP, 8/17/2018 859M RC YD-3 46.10% 37 a 34 30344N 79 1 R 123 W 3577 E Ra nhem R0 Fahmownl 293" KYW,YD- S,NS,NF, 111912017 RC NP 1 46.10% 73 a ]S l7.079N 6019.237w _ 1434A MELnkn Rd. oaw M=o 11 2B129 NK,YW,N P,YD- e/29/201B RC 2,NSYF 46.10% 19 a 34 37.872N 7912.582P7 170 £larce RO Pembroke NC 28372 NKYW,N P,YD,NS, 812912018 3440.a03►r 7911.074Y4 RC NF 46.10% 8 a 170 Elalce Re Pe bfbMa NC 28372 Nk,NW,N P,NS,YD- plaV7096 34 40. ! 7!N 7414.658 W Grass B RC 2, YF 46.10% 67 a 3" NC 1iW1710 Azar lan.NG 2e3e4 NK YW,IV P, D-3, 9/5/20f8 RC NS_ NF 46.10% 39 ag 453 Arthur Rd, Rat Sprinas. NC 28377 NK, YW,N P,YD,NS, 2P19/lO16 RC NF 46.10% 49 a 3J 63.22JN 79 tlA905W T5 Genv Rd- Pa bmke NL' 2a572 NK,YW- 2,NP,YD- 212912016 RC ANS,NF 46.10% 83 a 3J 54.683N 79 f0-35Ew 75 Ornp Rd. P—D-ht,NC 28372 K,NW,NP ,YD- 9rr170f7 RC 3 YS NF 46.10% 34 a 35 9-308N 80 Y8,84PW 6408 Sr. Fm-fhP Rd- M—hwlh NO 78106 K,YW,NP ,YD,NS,N 9/2/2017 RC F 46.10% 10 75 8-J93N 80 I9, r➢6 W 94w Sl, rhmplhy Rd, M[rY71Wlh NC 28106 K,NW,YP ,YD- OfLw17 RC 3 MS. YF 46.10% 92 a 35 7.3B9N 80 19.62T W a4" St TrMwh Rd. Marahwple NO 2a106 NKYW,N P,YD- 9YV2017 RC NS NF 46.10% 18 a 35 8 80ON 8.8 20.635W 8408 St TimothyRd. MarshvilM NC 28106 KNW,YP - YD- 9IV2017 - RC 2 NS NF 46.10% 41 - - a 35 9.069N 60 17 483 W 8408 Sl Tf'mmrr • Rd. MarzF.v(Ilr NC 26 r06 K, YW,NP ,YD- QM2017 1-ZT! RC 3 NS NF 48.10% 46 a l6 i f.76N 88 iy,370W 94M Sr. Trmwi8 Rd. 66rrahWo. NC 28Tp6 KNW,NP YD,NS,N ➢1212017 4-4, 35 8 744N 80 r 7 475 W RC F 46.10% 41 ag 840E St To— Rd- Marshville, NO 28108 K,NW,NP YD- 9/2/2017 ]Q3 RC 2.NS,NF 46.10% 25 _ 35 8.299N IIO 15.231W 8408 St Tlmol!' Rd NC 29106 ' - - KYW,YP, 9/2/2017 = RC YD- 7,NS,NF a 75 S. 668N 8D 14_IfOw 46,10% 44 ` Sao St T., e,M Rd. Ma"hvi0e NO 73Y06 KYW,NP YD,NS N B/2/2017 RC F 46.10% 30 1J-1rn1 - 75 [ 763N 8a 13 5S1 W 9408.Sr r; 90 • Kd Ma"Wr8a NC 281 K YW, YP, YD- VD2017 RC 2 NS NF 46.10% 15 354, 62dN 80 13 SY[yY 8408 Sf. 7fmof7i Rd. Marshville. NC 38106 K YW,YP, YD,NS,N 9/2/2017 RC F 46.10% 31 a5 17.39BN 80 : !.305 W 5408 S1 . omoth Rd. Marshville, NC 28106 - K,NW,YP- . 2,YD,NS, 9.O12617 RC NF 46.10% 94 3912.672N 80 21.318W 8408 St. Timoth Rd. Marshville NO 28106 K, YW,NP - 1 ,YD,NS,N 9/2/2017 RC F 46.10% 13 3612072N 8021.M6 W _ "as Sd- Tlmoth Rd Afarsrfvill'. NC :8106 K W,NF, 9 1202017 RC NS NP D 46.10% B a 35 17.35 80 20.920w —thy Rd. MomhVille NC 28106 £laved 20ra -i i Tons A1onM Tam I FwNW Field Raln runs cnm D Use Oct Good YK,YW- 2,NF,NS, TRf20Ta RC NP D-2 43.60% 44 a 35 18.20-M 80 18.256 W 2➢7la Or A NC7 D01 K,NW,NP ,YD,NS,N 1/7J20S8 RC F 43.6, 23 a 358.707N80 T� HW $407 P1anaer AV➢Ch1 ft Rd. Manhri NC 28103 YK,YW- $NP,YD- lJ.y➢01H RC 4 VS. YF 43.60% 45 aff 35 9.531N 80 14.145W W07 P1ss.1'sn! ll07 Ch—h Rd. M—hW5. NC 2MV03 NK,YW,N F,NS,NP, fOMB/2017 RC YD-2 43.60% 58aff 34 31.636N 79 12.281W 1021 Gera/d Rd. RQ1rWmd.NC NK,NW,Y F,NS,YP, 172arF91➢ RC D4 43.60% 155 OIL 34 34.206N 79 5.151 W WM N !30 fall Rowland NC MM NK, NW,NF,N 10M7R0l7 RC S.NPYD 43.60% 43 a 34 49.6-17N 79 6.990 W 6274 0ld Lowwy Rd Shannon NC 28386 NK,YW,N 10/17/2017 3569 RC FYS.NP 43.60% 1 48 a 34 49.215N 79 5274 OW cowy Rd. Sn4rr+ron NC 28386 _ 1 a1l iRD17 RC 43.60% 43., 43 ]f 49.6l5N i9 9. TB2 W 5274 DM I.wwv Rd Shmenumm NC 24396 NK,NF,Y S,NS,NP, 10/17/2017 RC YD-2 43.60%. 49 N¢772r 344➢.8 m7aa,l2fW H274 Rd NC 2➢3➢6 NK,YW„ - NFNS,N 10M7/2017 3572 RC P 43.60% 45 a 34 48.949N 79 9.345W 527/ Gfd La Rd. Shannon NC 2838a NK,YW,N a!L➢70l8 3617 RC FNSNP 43.60% 29 a 34 /J.941 N 79 5.➢SOW 110 h7sMcs Rd ftrubmle NC 20372 NK,YW,N 8/29/1018 3620 RC FNSNP 43.60% 22 a 7J J7.➢97N 79 8.QP7 W f 70 FLTe Rd Pembroke NC 20772 K,NW,NP 9/22017 8N 25 10.5/80 a3 17.9W RC NS,NF 43.60% 31 a ➢/08 St rr M Rd. Mmvh,Olk NC 28 NO YK, YW,Y P,YD- 9/22017 f- RC 2 NS.NF 43.60% 17 a 35 5.9r 7N 30 13.899W 0408 St numm Ra ATarshville NC 2a109 K,NW,NP ,YD,YS,Y 9�7J20T7 RC F 43.60% 16 a 35 /,53SN 80 7/, 663W 9408 S1. 7r-w Rd. Afarsf wAle NC 2610H YK,YW,N P,YD- 9/2/20f7 RC 3 NS NF 43.60% 20 a 35 77.70➢NJV l9,OM8W a40 81, fkr ll Rd. MJrshrl8s MOO vx,nu 2,YP,NS, 9/2/2017 RC NF 43.60% 13 13512.234N 80 20.638 W 8408 St. TImothy Rd. Marshville, NC 28108 YK,YW,N P,YD- RC 2 YS YF 43.60% 21 a 3S 1 .153N f0 22.301W 6408 Sr 'nm rhv Rd Ya.hwn. NC 28100 YK,NW,N P,YD- RC 3,NS,NF 43.60% 24 a a59. son 8D IY-go9w mag $t Im-aft no M—hvl8e NC 281 OH YK,NW,N P, YD. RC 3NS,NF 43.60% 61 a 35 9366N 90 ! 7. T09W H408 Rt. Tx o Ad. A41f4T1wraA NC MP6 YK,NW,N P,YD- 9/2/2017 RC 3 NS NF 43.60% ]2 35 13.466N 90 24.379W 0408 St IN 6h.N .--_..Ti.m.... YK,YW- 2,NP,YD, 9/2/2017 - RC YS NF 43.60% 28 a 35 f3."2N ao 3L.Iww 8408 St T'?MWhV Rd. NC �51P6 YK,NW,Y P,YD- 10/2/2018 RC 2,NS,NF 43.60% 50 a 551.267R 80 }3.914 W 27}7R 2}eP¢�rlda�dNC281]`- YK,YW iV P, YD, YS, IfA'2120 fil 13 — 3679 RC NF 43.60% 10 a - — - -- YK,NW,Y 1 P YD- 10/2/2018 .: RC 2 NS NF 43.60% 13 a 95 7.DD7N 80 t3.378W ESfi PiB flxMrad NC ae 137 YK, YW,N P,YD,NS, 10/112018 a:lTJIIO RC NF 43.60% 14 a as � fsrx 80 rs.163w E3 17 Hwy;? Y9 PeachlarM NG a8l33 YK, YW,N P, YD, YS, RC IF 43.60% 18 a 36 2,O11N $a 15.746W 2317 a1a Py4NVNld NC aa133 YK, YW,N P, YD,NS,N 101212018 - - RC F 43.60% 11 35 1-8B9N 80 }S69DW 23l7 R 2}8 Peachla A9C 28133 YK, YW,Y P, YD, YS, 70R120ia 3690 RC NF 43.60% 10 _73 !TAl156 au i75 i ,r60N ti0 }3.iT2W 10263 WlriD"Rd kwwccd.NC 26t28 --- YK,YW,Y P,YD,NS, }07/2Ma 3691 RC NF j 43.60'/. 23 a 351.37 80 12. T66 W '10967 tA811ow Rd. Nonvgod NC 7812a YK, YW,N P, YD, YS, 1012l101d 3693 RC NF 43.60% 129 a 352.874NMAS3t W 10967 Wlllme Ad- Norwood NC a8 t25 K,YW,NP ,YD- 11/9/2017 RC 3 NS NF 43.60% 59 1514-% N 8D 18.91LIW R14a MCLgaus Rd. OaRbWO, NC 29129 K,YW,YP- 2, YD- 11/9Y2017 RC 3 NS NF 43.60% 84 15 15AWN 60 2D.104W _ i4mil wkk 1lt M Rd, Gakbwm NC 25122 YK, YW,N P,YD- RC 3 YS YF 43.60% 33 29 35 16.223N 80 18.0921 W 1434a CL"iw Rd. GaAr6oro. NC 28129 l0.Y8l3017 34 32-11 "179 11.859W RC NK,YW,N P,YD- 3.NS.NF 43,60% 51 a i927A ald Rd Rowm"ONC 70nd/2017 RC NK,YW- 2,NP,NS, ND. YF 43.60% 56 e 3a 71.962E 79 8.4544+1 TO/18fi017 l927 Gerald Rd Rowfar3d.NC 34 31.432N 79 7.068 W RC NK, YW,Y P,NS,NF, YO 43.60% 43 a Tr1n 912017 1927 G2rafd Rd RowlendX 34 31.568M 79 6d69 W RC NK, YW, YP, YD,N SNF 43.60% 52 a ivn 8/20f7 1927 GNr.1d Rd Partied NC ?4 30.824N 79 12919 W RC NK,NW,N F,NS,NP, ND 43.60% 10 a 1927 4WWd Rd. R0N1and NC 10n W2017 _ - RC NW,NF,N S,NP,YD- 3 43.60% 43 34 Jtl.MN 791-4.196W 19270 Al Rd. R.,W.ntl NC 11N/2017 — RC YK,YW- 2,YP- 3,YD- 6.N5 NF 43.60% 70 a 3515.342N 80 19.307W 14J44 Mclsskr Rd. OaRboro NC 28129 - - I?Z?014P RC YK,YW- 2,YP, YS, NF.D-4 43.60% 109 35 17.502N 60 14.064 W 29716 KafttmoA Dr. AMaOP NC 2a00r w— SiB7.39000 2252.98204 2018 iSpit TOIIF Tana MpnN Tp Farmer I Field Rain alL Aer.. Use Nov Good YK,YW,N f/2/2018 RC F NS YP 42.40% 15 a 9s }5 ar4waa ra.832W 29716 Dr. AAn—*r1q. NO J%Wl Yk,YW,N F,NS,NP, 11/16,2017 RC D-5 42.40% 147 a 3517.214N 80 12.777W 36083 W—tam Rd. Nae7madv NC NK, YW,Y FNS,NP, 11H6/2017 3512 RC YDS 42.40% 15 a 3516.159N 80 12.539 W 3EOa3 +snsten Rd. AADwmarle NC NK, YW,Y 7Rtf10in RC FYSNP 42.40% 38 a 34 40.186N 79 13.915W 5a5 Di h Rd. FV.W ke. NC NK, YW,Y 7131/2018 3546 RC F YS NP 42.40% 49 a 34'39,532N 79 14.19E W 54S Bud.! Rd. P.mhrak.. NC _ Nk,YW,Y F,NS,NP, 7l31/20f8 Grass YD 42.40% 11 ag 34 39,880N 77 e7 455W 5O 8wfei n Rd -em. mke NO NK,NF,Y W- 2,NS,NP, 10H7/2017 RC YD 42.40% }t 34 49.562N 795.622W S27J Okf to—y Rd. Shannon NG 2aJSB _ NK,NW,N F,NS,NP, fOH7/2017 RC D•2 42.40% 48 34 40.744N 7$ 7.0s0W U14 O!d La Rd S4MrNlen NC am$ NK,NF,Y S,NS,NP, 10/17/2017 11~8 4 1' RC YD-2 42.40% 49 a 34 49,S18N 79 6274 old Lowory Rd. 54a 0 NC 23331 NK,YW,N F,NS, YP, aH 7r2018 RC D-2 42.40% 70 a iJ 29-880N 79 12A } 7 W _ 3577 E Ravnham Rd FafrmAwftit NC 783J0 _ NK,YW,N F,NS,YP, 8H7/2018 RC D 42.40% 45 aL46LU a 34 29.70fN 7911.919W 3577 E Ra Ad FlHmnnl, NC 28340 NK,YW- 2,NF,NS, 8H7/T018 - RC YPD4 42.40% 90 a 34 29.97aN 79 f1 6ETW 3577 E Ra Ram Rd. Faffmnt. NC 78340 NK,NW,Y F,NS,NP, frd7/Z018 RC YD-3 42.40% 29 34 39761N 79 r4.229 W us Rud Rd. pmamhk NC YK, YW,Y 1/2/1018 3642 RC FYS YP 42.40% 400 a 35 17. f 9}N 80 15.918w 2Y718 Dr. Alewmatk NC 28001 NK, YW,Y 9/29/2019 3607 1 RC F NS NP 42.40%. 29 aff 36,17 872N 7012.562 W 1711Bla Nd �ernhrvka NC NK,YWN 8/29/2018 3616 RC FNS NP 42.40% 13 a 34 43.387N 76 6.405W 170 Elarce Rd. Pembroke NC YK,NW,Y F, YS,NP, NEW !0l212018 RC YD-2 42.40% 34 a 351.238N80 T3,a28w 2317 H 218 Peachland NC 28133 F `�I NK,YW- 3,NF,NS, 1011112018 Grass YP.YD4 42.40% 134 air 3/ N. 747W 79 8.44CW 1189 Wf; S ane t Rd. Frkn m! NC 28340 NK, YW,N P,NS,NF, fOMB/2017 3719 RC YD 42.40% le a 9/ 2.7 020N 79 1 T.970 W 1927 Ge ydidol RawlnW NC 74Ja] NK YW,N P, YD,NS, T0q Y7 3720 RC NF 42.40% f7 a 34 3I.1i2N 74 17-177W Y927 OW10d Rd. R9w14ad. NC 2a383 "' NW F,NS,NP, 7�M T1 RC YD-3 42.40% 59 a 04 33. 11 IN 78 6.2fi0w 1927 Gerald Rd. Rowland NC 28383 NK, YW,N F,NS,NP, e/3/2ofe RC YO 42.40% 14 a 34 2e.086N 79 7.735W 2648 Manetra Marlena NC 283a2 _ - NK,YW,N RC F,NS,YP, YD-3 42.40% 20 s9 M i 5o e .12018 _ _ 34 25.852N 79 7.896W 2648 Mz lelra WHO* NC 28362 _... YK,YW,N F,NS,NP, fOr2r2016 _ MIN11.+971sat RC YD 42.40% 22 70.8a a 351862 8015.SOHW 23T7R 278 Plash/and 71C 28733 NK, YW,N 3738 RC P,YD,NS, YF 42.40% 43 a 0729I018 _ 34 J7.7/7N 7B 12.408W 170 E4r Rd. Pembrvkv NC YK,YW,N — - — F,NS,NP, 37A7' RC YD 42.40% 19 a 35169T6N 8018.844W 2971611n1 ck Or AIb mark NC 28001 YK,YW,N F, YS,YP, 12/2018 RC YD-3 42.40% 38 a 3 16.162N 00 16.52d W 29776 No11 aro0k 0r. Alb —le NC 2W01 YK, YW,Y 11y70fe RC FNS.NP 42.40% 16 a 3515.71BN 80 18.711W 20716 Linn a.,.oa fi, R:nermarle. NC 7r001 Yk,YW,N F,NS,NP, 1N/3018 - — - 35 � 7. d67N 8Fl i 1. r 5/ W RC D-5 42.40% 27 a 29716 Ivah Dr AibelnF/Ikl kC 28001 YK,YW,N fy20T8 — 3 1s. a52N e0 18, 246 w RC FNSYP 42.40% 18 a 29718 ftHybmk Or Albormall¢ rr[_' : aeiR1 RC K,YW,NF, NS.NP 42.40% 17 a f/Z70T8 35 15 VON 80 16.sa4 W 2971E 0r .Albermarfe NC 28001 ifibrook _ - Nk,NW,N F,NS,NP, 11/9/201B Firms RC YD-3 42.40% 134 4f..763N 79 7F 531W 343W. L. Moore Maxton NC JJ364 E12 NK, YF, NW, NS, 34 42.213N 79 16.720 W RC NP YD-5 42.40% a 343 W. L. Moore Maxton NC 28364 - 2815 rnru Month F Held I Rain Ac Use Dec Good —.1 NK,NW,Y F,NS, YP, 1/29/2018 RC D4 42,00% 155 7d 34.M6N 798.1S1W 3338 N t30 Eau Rowland NC T8393 YK, YW,N F,NYS,N 11r1617017 0 RC PYD J 42.00% 59 3516.983N B0 12 W6 W 360a7 Weston Rd AltW.3de C YK, YW,N F,NS,NP, 11N6/2017 RC D-5 42.04 147 a 3517.214N 80 12.777W 36083 Weston Rd Albemarle, NC NK,NW,N F,NS,NP, f0/17/2017 - RC Yd 42.00% Hall 34 49.637N 79 6.990 W 5274 DO Lo kd Shannon NC 28986 - Nk,YW,N 20117R0f7 rr 3569 RC FYSNP 42.00% H a 74 49.215N 79 6.181W 5274 Old Lowe Rd. Shannon NC 28386 NK,YW,N 1O117/2017 3571 RC F.YS.NP 42.00% 43 a r 3f 49 i15N 79 r r n T.v 5274 O!d Loaxr.l Rd. Shannon NC 28386 NK, YW,N 10/17/2017 3572 RC F NS NP 42.00% 45 3448.94 W 79 9.345 W 52 4 Old Lnwe Rd Shannon NC 2d.!2_h NK,NW,N F,NS,NP, IM772P77 RC YD-2 42.00% 46 a 3449.7441f 797MW 527A CM LDWWP Rd SADAronNC 28786 NK,YW,N F,NS,NP, T 7R0}7 RC YD-2 42.00% 49 a 3449.518A 796.T2tW 74 00 L—y Rd, S NC 21. NK,YW,N fOff}128}7 3579 RC F.YS.NP 42.00% 33 7447.623N?25,2 aW 5274 Oid lad. Shannon NC 2a3a8 NK,NW,N 10/17/2017 3580 RC F NS NP 42.00% 50 a 34 47569N 79 5.637 W 5774 Ord La - no Shann9n NC woo NK,YW,N 10H7/2017 RC FYSNP 42.00% 69 846:200 a _M. - -- - - 34 49.067N 70 7.097W 5274 Old Lo Rd Shannon NC:83a5 Grass NK,YW,N F NS NP 42.0021 28 AIRML 10/17/2017 51.872N 79 9.795W 7 ow Rd Sbannon NL'I8786 NK,YW,N F,NS,YP, r On 712017 RC YD-2 42.00% 50 a 34 ST.a43N 79 8.484 W 6274 OM L Rd. Shannon. Nc 28386 NK,NF,Y W,NS, YP, 10/f7ra017 RC YD 42.00% 5a a 34 AS 100W 79 8.404 W 52M Ofd Loyrory Rd. Sk"wMI NG 2BM NK,YW,N F,NS,YP, 8M7/2018 RC D-2 42.00% 70 34 29.89011 79 12.411.W 3577 E Raynham Rd. Fairmont NC 28340 NK,YW $NF,NS, dli7 1d = RC YP 42.00% 90 a 34 29.978N 79 77.857 W 7577 F Ra am Rd. Fur ArC 28740 77 NK,NW,N Nr3+2p77 3594 RC FYS.NP 42.00% 524 aaa 34 29.881N 79 4355W 1372 N RK P"MhMAaNC28372 NK,YW,N 3617 8B7R/R289/l/222D00T17' 88 RC FNSNP 4200% 9 34 44.9410 7 S}.9a }7YEaa Rd.. POihr9Me NC28772 NK,YW,N 3620 RC FNS 42.00% N479N7d.027W .lafN 170 Ef9c4 Rd. Prkrok NC 2772 YK,NW,Y 364 2 RC FYSYP 42.00% 4020 dW W 75 t] e9O ,s8dl 29710 W MOOR A. AM 10 NC 2801 YKYWN , P,YD,YS 101212018 7 RC NF 42.00%;23 35 1.3e0Ar Biz i.R333 W 23T7Nw 2r8 Peachfarrd NC 28s93 YK, YW,Y P,YD,YS, !0/2/2018 3690 RC NF 42.00% ars ,is i,780N a6 r3, T 12W f 0967 Nhllow Rd. Norwoed.NC 23129 W, YK, YY P,YD,NS, f0/2/2018 3691 RC NF 42.00% 74, pR a 3S }.378N 88 12.766 W 10963 W71ow Rd.Nur—djiC20125 YK,YW,N P,YD,YS, f077l20t8 3693 RC NF 42.00% 129 _ 1 - - a 75 2A74N 80.15.363 W f09YG1 w+ll-... Rd. Narw .NC 28128 NK, YW,N P,YD,YS, 1 i8 3744 RC NP 42.00% 39 - - - a 74 33.726N 79 Jr. low 12d4 Schaal Nd f NC 2834tl K,YW,NP , YD,NS,N 17272dra 3773 RC F 42.00% 85 3S 1 R MOP fl0 2T 870 W 2070e MoRomot Dr. AMarmada MC 2Mtt1 NK,NW,N F,NS,NP, 10/18M017 RC YD3 42.00% 32 34 2OL467N 79 14.743 W 7927 Ga ld Rd. Rowfand.NC NK, YW,N F,NS,NP, IWIR 017 RC YD-3 42.00% 119 a 34 Md.46SN 79 15.163 W 1927 C w&W PA lowlmd Nc NK,NW,N F,NS,NP, 10,23/2018 RC YD3 42.00% 87 3i 32.i72N 7i d.2BTW V164 Sr7mol Rd. FalmrorrL NC 28340 NK,YW,Y P. YD, YS, i0/T3/2018 3815 RC NF 42.00% 14 a 7413.076N 7118.768 W 1384 School Rd- Framrarrl NC 2e340 NK,YW,N t2Rr2vra Grass FNSNP 42.00% 10 7a 46.706N 7919.747,,V 44r McWainf Rd Martin NC ie364 NK,YW,N 72/7/2018 RC FNSNP 42.00% 20 a 34 46.771N 79 12.231 W 441 McGaint Rd Maxton NC 28364 1217, 2018 - — — - RC NKNF,Y S,NS,NP, Y0.3 42.00% 21 34 44.790N 78 fa. 666 W f7/7/pp}d "I aieGRlrlf Rd Naxfpn 38361 3448.2MM 7818.820W Grass NK,YW,N KNPNF 42.00% f8 a 4*1 MNiamt Rd Nat! NC 28364 12/7/2018 3823 RC Nk,YW,N P, YD,NS, NF 42.00% 55 a 343 19 2.387W 562 Pavevroed Rd. F i—f NC Ta2dO 12/7/2018 3824 RC NK YW,Y P,YD,YS, YF 42.00% 30 a. 34 32.304N 792.782W el3p�201d 563 Pk—..__d Rd. Falmont NC 28340 34 43.85411 791 SAW W 3830 RC NK,YW,N P,YS,YD, NF 42.00% 130 a 13C C Rd. Pembrofn NC 29372 3/7l301b 3831 RC NK,NW,N F,NS,NP, YD 42,00% 113 a 34 46.1d rN 7816.r9w 2702 Pras7Pa Rd Maxtom NC 28364 31212018 3832 RC W, NKYN P,NS, YD, NF 42.00% 40 34 43'.302N 78 i5.947W 2702 Preston Rd. Maxton NC 28364 3/2/2016 — 3839 RC NKYW,N P,YS,NF, YD 42.00% 73 I34 a4.5P4N 79 f7.624 W 2707 Presto.'?d Marton ,VC 283F4 .,Awao16 .. .. ..... ... .._.. 3841 RC NKNW,Y P,NS,ND' YF 42.00% 32 —-TYr,83 5T..108d a 34 45.79.1Y 7919.44W 2702 Preston Rd. Marton NC 28364 3f712018 3843 RC P,ND,YD, NF 42.00•/ 50 d a 54 /S,O T5N ]9 114y 1 W Pl3017019 7707 P—e Rd Upwm NC 2 344 34 4a, OIN 79 6.2-M W 3849 RC 8 Grass NKNP,Y W,YF,YS, YD 42.00% 118 - ® a 7 zlI7D l8 731 Gx ft. P4mbrokv NC 28377 34 49,799N 79 22 MW 3866 RC Nk,YW,N P,NS, YD, NF 42.00% 42 12/27/2078 171 ENlwn Dr, Mqwm Nc 28364 34 49.v7I�' 19 7v 8e0 W 3867 RC NK,YW,N P,NS,YD, YF 42.00% 58 a 179 Elmore t=a Maxton. Nc 28364 12/27/2018 _— - 34 47.447N 79 19.a73 W 3873 RC 8 Gress NK,YW,N P NS NF 42.00% 24 a 864 fClrrlc Marlorr, NC 28364 ay a a a CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): urface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) L$rDistribution and Nyarketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes C No ❑ -► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January WQ0009477 2142.53975 2142.53975 See Attached 2142.53975 Agricultural February WQ0009477 2081.19939 2081.19939 2081.19939 Agricultural March WQ0009477 2140.4835 2140.4835 2140.4835 Agricultural April WQ0009477 2304.76288 2304.76288 2304.76288 Agricultural May WQ0009477 2237.03788 2237.03788 2237.03788 Agricultural June WQ0009477 1983.74770 1983.74770 1983.74770 Agricultural July WQ0009477 2024.33654 2024.33654 2024.33654 Agricultural August WQ0009477 2565.88706 2565.88706 2565.88706 Agricultural September WQ0009477 1915.16918 1915.16918 1915.16918 Agricultural October WQ0009477 2252.98204 2252.98204 2252.98204 Agricultural November WQ0009477 2056.93424 2056.93424 1 2056.93424 Agricultural December WQ0009477 2119.05540 2119.05540 2119.05540 Agricultural Total from FORM DMSDF (sup) 0 25824.13556 25824.13556 25824.13556 Totals: Annual (dry tons): O'�824.13556 25824.13556 25824.13556 Amendment(s) used: Bulkin Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit 1W Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." S gnature of Permittee 61�- Date Signature ofPreparer** (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM DMSDF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only) VDistribution and Marketing (complete Parts A, and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Jan WQ0009477 171.36425 171.36425 Jamie Austin 171.36425 ag WQ0009477 19.35875 19.35875 Kevin Baucom 19.35875 ag WQ0009477 321.01950 321.01950 Dan Brooks 321.01950 ag WQ0009477 90.90750 90.90750 Jody Dennis 90.90750 ag WQ0009477 30.41300 30.41300 Mike Freeman 30.41300 ag WQ0009477 50.09050 50.09050 Jimmy Gaddy 50.09050 ag WQ0009477 10.65050 10.65050 Robbie Harrington 10.65050 ag WQ0009477 128.88550 128.88550 Robert Kimrey 128.88550 ag WQ0009477 51.10200 51.10200 Rex Oxendine 51.10200 ag WQ0009477 1067.18775 1067.18775 Roger Oxendine 1067.18775 ag WQ0009477 89.60275 89.60275 Glen Phiefer 89.60275 ag WQ0009477 19.84325 19.84325 Lynn Thomas 19.84325 ag WQ0009477 92.11450 92.11450 Vinson York 92.11450 ag Feb WQ0009477 49.12754 49.12754 Jamie Austin 49.12754 ag WQ0009477 39.51791 39.51791 Kevin Baucom 39.51791 ag WQ0009477 62.67891 62.67891 Jason Blackwelder 62.67891 ag WQ0009477 163.32438 16332438 Fairly Drake 163.32438 ag WQ0009477 235.62166 301.82716 159.86334 655.28587 413.95262 235.62166 301.82716 159.86334 655.28587 413.95262 Robbie Harrington Jeff Long Ozmer Lee Oxendine Roger Oxendine Wayne Saunders 1 235.62166 301.82716 159.86334 655.28587 413.95262 ag ag ag a WQ0009477 WQ0009477 WQ0009477 WQ0009477 ag Totals: Annual (dry tons): 0 4213.73914 4223.73914 4223.73914 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 7 DENR FORM DMSDF (Supp) (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT N: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X niafrihnfinn and Mar4rfi- f -Wl Pads A and Rl Part A": Part Ba: Month Sources(s) (include NPDES 4 if applicable) Volume (dry tons) Recipient Information .Amendment) BuFkmtt Agent Residual In Product Out Name(s) Volume) (dry tons Intended use(s) Mar W00009477 161.71668 161.71668 Jamie Austin 161.71668 ag W00009477 313.72092 313.72092 Bart Barbee 313.72092 a W00009477 31.04172 31.04172 Dan Brooks 31.04172 ag W00009477 422.51184 422.51184 Bruce Cuddy 422.51184 ag W00009477 39.77712 39.77712 Fairly Drake 39.77712 ag W00009477 148.89096 148.89096 Barrett Gaddy 148.89096 a W00009477 304.95240 304,95240 Robbie Harrington 304.95240 ag W00009477 147.23496 147.23496 Johnny Helms 147.23496 ag W00009477 323.68590 323.68590 Lee's Farm 323.68590 ag WQ0009477 192.34026 192.34026 Marshall Red Locklear 192.34026 ag WQ0009477 54.61074 54.61074 Will Russell 54.61074 a Apr W00009477 229.39840 229.39840 DewightAtkins 229.39840 a W00009477 623,54432 623.54432 Blue Q Ranch 623.54432 a W00009477 356.03456 356,03456 Terry Freeman 356,03456 a W00009477 145.77472 145.77472 Brandon Husse • 145.77472 ag W00009477 76.40640 76.40640 Darrell Hussey 76.40640 a• WQ0009477 20.50048 20.50048 Vance Lambert 20.50048 ag W00009477 142,04736 142.04736 Franklin Lee 142.04736 a W00009477 205.97248 205.97248 Lee's Farm 205.97248 a WQ0009477 32,19776 32.19776 Ricardo Rodrizuez 32.19776 ag ota s: Annual (dry tons): 0 34:2.35998 3972.35998 3972.35998 ....... ........... ......... - Amendment(s) used: Bulking Agent(s) used: u more space is requrrea, attacn aaanronal mtormation sheets (FURM DMSDF (supp)): Total Number of Form DMSDF (Supp)�_ 7 1 2140.4835 1831.87648 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketing (complete Parts A, and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) April continued WQ0009477 101.54816 1 101.54816 Will Russell 101.54816 ag WQ0009477 252.90944 252.90944 Wayne Saunders 252.90944 ag WQ0009477 53.73760 53.73760 Duane Strider 53.73760 ag WQ0009477 64.69120 64.69120 Terry Williams 64.69120 ag Ma►• W00009477 74.82542 74.82542 Dewight Atkins 74.82542 ag WQ0009477 182.36494 182.36494 Bernard Beck 182.36494 ag WQ0009477 458.86710 458.86710 Blue Q Ranch 458.86710 ag WQ0009477 61.27148 61.27148 D lon Chriscoe 61.27148 ag WQ0009477 165.39018 165.39018 Wayne Chriscoe 165.39018 ag W00009477 126.97174 126.97174 Charles Deaton 126.97174 ag WQ0009477 199.79462 199.79462 Terry Freeman 199.79462 ag WQ0009477 42.65990 42.65990 Brandon Hussey 42.65990 a WQ0009477 31.3761 31.3761 Darrell Hussey 31.3761 a WQ0009477 544.62844 544.62844 Wayne Saunders 544.62844 ag WQ0009477 348.88796 348.88796 Terry Williams 348.88796 a Totals: Annual (dry tons): 0 2709.92428 2709.92428 : 270Q.92428 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7 472.88640 2237.03788 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT 0: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month', "Source(s)" and "Residual In" columns only) X nistrihntinn and Mnrkrtinn lromnlntn Pnrfs A. and R\ _ PartA*: PartB*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Mended use(s) Jun* W00009477 1157.20915 1157.20915 B&F Farms 1157.20915 ag W00009477 72.51275 72.51275 Blue Q Ranch 72.51275 ag WQ0009477 10.48420 10.48420 Charles Deaton 10.48420 a W00009477 43.62335 43.62335 Terry Freeman 43,62335 ag W00009477 21.45790 21.45790 Darrell Hussey 21.45790 ag W00009477 125.10285 125.10285 Wayne Saunders 125.10285 ag W00009477 553.35750 553.35750 Terry Williams 553.35750 ag Julv W00009477 124.17698 124.17698 Max Asbill 124.17698 ag WQ0009477 1147.82444 1147.82444 B&FFarms 1147.82444 ag W00009477 44.22256 44.22256 Bernard Beck 44.22256 a W00009477 64.01318 64.01318 James Dunlap 64,01318 ag W00009477 69.01304 69.01304 Gilbert Keys 69,01304 a W00009477 575.08634 575.08634 Tony Smith 575.08634 ag Totals: Annual (dry toes): 0 4008 0842 4008 0842 401,80842 Amendment(s) used: Bulking Agent(s) used: 1t more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)1 7 1983.74770 2024.33654 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT 9: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X nictrihnlinn and Markrtina lrmml . P-t. A and Rl Part A•: Part B": Month Sources(s) (include NPDES 4 if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Aug WQ0009477 11.05188 11.05188 1 John Cummings 11.05188 ag W00009477 42,61084 42.61084 Kenwin Cummings 42.61084 a W00009477 830,48322 830.48322 Lacy Cummings 830.48322 a WQ0009477 2070778 20.70778 William Cummings 20.70778 a W00009477 62,83248 62,83248 Wilber Harris 62,83248 ag W00009477 109.047 109.047 Richard Hays 109.047 ag WQ0009477 82,1755 82.1755 Sean Hunt 82.1755 ag W00009477 185.11676 185.11676 Lycurous Lowery 185.11676 ag W00009477 189.3493 189.3493 Rex Oxendine 189.3493 ag W00009477 704,92976 704,92976 Roger Oxendine 704.92976 ag W00009477 118.18554 118.18554 Jessie Oxendine 118.18554 a W00009477 209.397 209.397 Tony Smith 209.397 ag Se it W00009477 123,96751 123.96751 Jamie Austin 123.96751 ag W00009477 766.9657 766.9657 KevinBaucom 766.9657 ag W00009477 95.21955 9521955 John Cummings 9521955 ag WQ0009477 146.13239 146,13239 Lacy Cummings 146.13239 a W00009477 4148613 43.48613 James Dunlap 43.48613 ag WQ0009477 91.49006 91.49006 Sean Hunt 91,49006 ag W00009477 104.09841 104.09841 Lee Farms 104.09841 ag WQ0009477 154.76231 154,76231 Terry Locklear 154,76231 ag W00009477 66.07974 66.07974 Eddie Moore Brother Ag 66.07974 ag WQ0009477 22.74113 22.74113 Jessie Oxendine 22.74113 ag W00009477 275.93616 275.93616 Rex Oxendine 275.93616 ag W00009477 24.29009 24.29009 Roger Oxendine 2429009 ag Totals: Annual (dry teas): 0 4481 0562 1 4481 0562 4-191 ,i62 Amendment(s) used: Bulking Agent(s) used: ' If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)� 2565.88706 _- 1915.16918 IK; CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT if: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc PHONE: 910-895-4033 7428C COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketing (complete Parts A- and Rl Part A*: Part B*• Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intendeduse(s) Oct W00009477 61.9992 61.9992 Jamie Austin 61.9992 a W00009477 33T49016 337.49016 KevinBaucom 337.49016 ag W00009477 133.00616 11 133.00616 Jeff Griffin 133.00616 a W00009477 322.93648 322.93648 Lee Fang 322.93648 ag W00009477 65.3782 65.3782 Jessie Oxendine 65.3782 a W00009477 19T83936 197.83936 Rex Oxendine 197.83936 ag W00009477 398.08108 398.08108 Roger Oxendine 398,08108 a WQ0009477 297.93624 297.93624 Mike Presslar 297.93624 ag W00009477 206.79916 206.79916 David Underwood 206.79916 ag W00009477 231.51600 231.51600 Robert Wilkins 231.516001 a Nov W00009477 210.1768 210.1768 Ronnie Bralock 210.1768 ag W00009477 96.65504 96,65504 JeffGriffm 96.65504 ag W00009477 96.03176 96.03176 Richard Hays 96.03176 a W00009477 253.74704 253.74704 Sean Hunt 253.74704 ag W00009477 270.18552 270.18552 L&R Moore Fangs 270.18552 a W00009477 112.20312 112.203121 Wendell Locklear 112.20312 ag W00009477 243.43536 243.435361 L curous Lowery 243.43536 ag W00009477 108.23024 108.23024 Jessie Oxendine 108.23024 a W00009477 102.34936 102.34936 Roger Oxendine 102.34936 ag WQ0009477 241.92168 241.92168 David Underwood 241.92168 ag W00009477 226.72128 226.72128 Mike Willoughby 226.72128 ag W00009477 95.27704 95.97704 Robert Wilkins 95.27704 ag Totals. Annual (dry tons): 0 430991628 430991628-...-.:'.'.':':':':':'::':'::::::: 43095-1628 '-. ........... Amendment(s) used. Bulking Agent(s) used: it more space is required, attach additional mtormation sheets (FUKM DMSL)F (supp)): Total Number of Form DMSDF (Supp)1 7 1 2252.98204 2056.93424 - CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Markefinv (comnlete Parts A. and R) Part A*: Part B*• Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Dec-18 W00009477 41,1894 41.1894 Ronnie Bralock 41.1894 ag W00009477 105.8778 105.8778 Adam Collins 105,8778 ag W00009477 158.62980 158,62980 Aundra Hunt 158.62980 a W00009477 20.9622 20.9622 Sean Hunt 20.9622 ag W00009477 32.08380 32.08380 Daniel Locklear 32.08380 ag WQ0009477 595.8876 595.8876 Lee Grady LavcEry 595.8876 ag W00009477 146.1894 146.1894 Phillip Locklear 146.1894 ag WQ0009477 83.23980 83.23980 Jimmy McMillan 83.23980 W00009477 20.37000 20.37000 Jessie Oxendine 20.37000 ag W00009477 10.72680 10.72680 Rex Oxendine 10.72680 ag W00009477 210.21000 210,21000 Roger Oxendine 210.21000 ag W00009477 63.24360 63.24360 Ronald Stickland 63.24360 ag W00009477 133.63980 133.63980 David Underwood 133.63980 a W00009477 453.73440 453.73440 Robert Wilkins 453.73440 ag W00009477 10.74780 10.74780 Jeff Griffin 10.74780 a W00009477 32.32320 32.32320 Mike Preslar 32.32320 ag Totals: Annual (dry tons}: 0 2119 05540 2119.05540 : j; j j; ;< ; . : }; : }; ; }; ; 2119.0554 Amendment(s) used: Bulking Agent(s) used: It more space is required, attach additional mtormation sheets (F(JRM DMSDF (supp)): Total Number of Form DMSDF (Supp)1 7 J 2119.M.4 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0009477 Laboratory: 1) Pace Analytical Services LLC. Cascades Tissue Group -North Carolina a Facility Name: division of Cascades Holdings US Inc. 2) Waypoint Analytical Residual Source WQ # or WQ0009477 3) Summit NPDES #: 4) WWTP Name: 5) Residual Analvsis Data Parameter (mg/kg) Ceiling Conc. Limit (m 4/k )a Sample or Composite Date 01/03/18 02/14/18 03/12/18 04/05/18 05/08/18 06/12/18 07/11/18 & Retest 07/31/18 08/6/18 09/06/18 10/09/18 11/08/18 12/06/18 Percent Solids (%) NA 42.50 1 43.7 41.40% 44.8 44.6 44.5 39.4 44.6 46.1 43.6 42.4 42 Arsenic 75 1 0.87 0.89 0.81 0.95 0.79 1.1 1 0.05 1 1 0.87 0.84 Cadmium 85 Not Permit Required - Copper 4,300 21.1 24.5 20.5 22 19.9 18.4 20.9 18.9 14.5 22.7 16.5 37 Chromium NA Not Permit Required Lead 840 Not Permit Required Mercury 57 Not Permit Required Molybdenum 75 Not Permit Required Nickel 420 4.7 1.1 1.7 1.20 1.2 2.6 2.1 1.1 1.6 2.10 2.1 1.4 Selenium 100 Not Permit Required Zinc 7,500 72.9 64.7 58.8 97.1 60.3 92 134 102 297 118 166 75.2 Total Phosphorus NA Not Permit Required TKN NA 1600 1680 1530 1630 1300 2080 1660 1120 1410 1800 1520 782 Ammonia -Nitrogen NA 22.6 22.9 24.2 15.3 22 15.4 20.6 18.1 21.3 19.8 21.4 23.3 Nitrate and Nitrite NA 4.7 4.6 4.8 4.5 1 4.4 4.4 5.1 4.5 4.3 4.4 4.7 4.7 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties p4tbinittin false infoamation, including the possibility of fines and imprisonment for knowing violations." C Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00009477 Laboratory: 1) Pace Analytical Services, LLC Cascades Tissue Group -North Carolina, a Wa oint Analytical Facility Name: division of Cascades Holding US Inc. 2) Residual Source WQ0009477 3) Summit NPDES # or WQ#: 4) WWTP Name: 5) Residual Analvsis Data Sam ile or C mposite Date Parameter (mg/kg) 01/03/18 02/14/18 03/12/18 04/05/18 05/08/18 06/12/18 07/11/18 & Retest 07/31 /18 08/06/18 09/06/18 10/09/18 11/08/18 12/06/18 Pan Cal 480 504 459 489 390 624 498 336 423 540 456 235 Aluminum Not Permit Re uired Carbon/Nitrogen Ratio 160 140 180 140 387.3 210 180 150 66 92 59 27 Calcium Carbonate Equivalency Not Permit Required PH 7.1 7.9 7.4 8.4 7.70 7.6 7.7 7.1 8.3 7.1 7.4 7.4 Magnesium 1510 1620 1630 1240 1570 1360 1580 1630 1400 1650 1460 1740 Sodium Not Permit Required Potassium Not Permit Required Calcium 171000 189000 167000 150000 187000 211000 158000 168000 179000 157000 160000 185000 Ignitablilty- Summit 08/28/18 ND Reactivity Summit 08/28/18 ND Corrosivity Summit 08/28/18 7.1 Total Nitrogen 1600 1680 1530 1630 1300 2080 1660 1120 1410 1800 1520 782 TOC 289000 272000 323000 293000 306000 318000 311000 275000 312000 310000 306000 290000 Volatile Solids 496700 467500 555300 503100 526300 546500 535300 473800 536200 534000 527000 498000 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are si4ulies for submitting fai info cation, including the possibility of fines and imprisonment for knowing violations." r * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) .0001 PaceAnalyfical ..pacelaft corn March 02, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92369117 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on January 09, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. A revised report is being submitted on 3/2/18 to include a corrected PAN calculation. If you have any questions concerning this report, please feel free to contact me. Sincerely, od*c Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 1 PaceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92369117 Sample: Monthly Sludge Lab ID: 92369117001 Collected: 01/03/18 13:40 Received: 01/09/18 09:43 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic ND mg/kg 2.0 1.0 1 01/11/18 08:45 01/15/18 12:33 7440-38-2 Calcium 171000 mg/kg 200 99.8 10 01/11/18 08:45 01/15/18 12:37 7440-70-2 Copper 21.1 mg/kg 1.0 0.50 1 01/11/18 08:45 01/15/18 12:33 7440-50-8 Magnesium 1510 mg/kg 20.0 0.50 1 01/11/18 08:45 01/15/18 12:33 7439-95-4 Nickel 4.7 mg/kg 1.0 0.50 1 01/11/18 08:45 01/15/18 12:33 7440-02-0 Zinc 72.9 mg/kg 2.0 1.0 1 01/11/18 08:45 01/15/18 12:33 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 42.5 % 0.000010 1 01/09/18 17:21 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 57.5 % 0.10 0.10 1 01/10/18 11:24 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.1 Std. Units 0.10 0.10 1 01/11/18 13:23 I Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 480 mg/kg 0.12 0.12 1 01/23/1814:48 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1600 mg/kg 40.0 20.0 1 01/23/1815:15 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 22.6 22.6 1 01/1811814:02 7664-41-7 R1 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1600 mg/kg 118 58.9 1 01/23/18 03:41 7727-37-9 M1 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 4.7 4.7 1 01/23/18 03:21 M1 Nitrogen, Nitrite ND mg/kg 2.4 2.4 1 01/23/18 03:21 Nitrogen, NO2 plus NO3 ND mg/kg 4.7 4.7 1 01/23/18 03:21 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 Page: 1 of 1 Report Number: 18-010-0208 ■ Account Number: 05734(2) 7621 Whitepine Road, Richmond, VA 23237 Submitted By: Angela Baioni Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Monthly Sludge/92369117001 ANGELA BAIONI 9800 KINCEY AVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OFANALYSIS Lab Number: 58006 Sample Id : Monthly Sludge/92369117001 Date Sampled: 1/3/2018 13:40:00 Date Received: 01/10/2018 00:00 Date Reported: 01/16/2018 Total Solids * 43.30 433000 100.0 R D 01/10/2018 13:30 SM-2540G Moisture * 56.69 100.0 R D 01/10/2018 13:30 SM-2540G Total Kjeldahl Nitrogen 0.18 1800 50.0 R D 01/11/2018 09:00 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 44.80 448000 2500 R D 01/11/2018 13:15 AOAC 955.01 Total Volatile Solids 49.67 496700 100.0 R D 01/10/2018 13:30 SM-2540G C/N RATIO * 160 1 01/10/2018 13:30 CALCULATION Carbon (TOC) * 28.90 289000 100 01/10/2018 13:30 CALCULATION Comments: NC CERT#257, SC CERT#9300 7001 ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ot,re•: -)as and letters are for the exclusive and confidential use of cur Gieats, and may not be rrp oduced in whole or p nor may any r ference be made tot' ork, the results, orlhe company in ary advertising, news release, .:, r- erpuhlic announc+:ra . Ys without obta,! ­g our pr.Y.., :i-i authorizaiian. 0 Pauric McGroary Agronomist YacleAnaljdical www.pacelabs.com March 01, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92373556 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 aWnalytica!® www.pacawbs.com f ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92373556 Sample: Monthly Sludge Lab ID: 92373556001 Collected: 02/14/18 15:35 Received: 02/15/18 10:30 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic ND mg/kg 1.7 0.87 1 02/20/18 01:15 02/23/18 01:56 7440-38-2 Calcium 189000 mg/kg 346 173 20 02/20/18 01:15 02/23/18 15:37 7440-70-2 Copper 24.5 mg/kg 0.87 0.43 1 02/20/18 01:15 02/23/18 01:56 7440-50-8 Magnesium 1620 mg/kg 17.3 0.43 1 02/20/18 01:15 02/23/18 01:56 7439-95-4 Nickel 1.1 mg/kg 0.87 0.43 1 02/20/18 01:15 02/23/18 01:56 7440-02-0 Zinc 64.7 mg/kg 1.7 0.87 1 02/20/18 01:15 02/23/18 01:56 7440-66-6 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 43.7 % 0.000010 1 02/15/18 17:13 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 56.3 % 0.10 0.10 1 02/16/18 10:59 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.9 Std. Units 0.10 0.10 1 02/16/18 13:40 Plant Available Nitrogen Analytical Method: SM 2710E Plant Available Nitrogen 504 mg/kg 0.12 0.12 1 03101/1816:01 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1680 mg/kg 40.0 20.0 1 02128/1817:11 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 22.9 22.9 1 02/24/18 14:50 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1680 mg/kg 87.9 44.0 1 02/16/18 17:24 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 4.6 4.6 1 02/27/18 22:59 Nitrogen, Nitrite ND mg/kg 2.3 2.3 1 02/27/18 22:59 Nitrogen, NO2 plus NO3 ND mg/kg 4.6 4.6 1 02/27/18 22:59 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/01/2018 04:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17 Page: 1 of 1 Report Number: 18-047-0201 Account Number: 05734 Waypointe-r ANALYTICAL Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Sludge/92373556001 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Date Sampled: 2/14/2018 15:35:00 Lab Number: 58644 Date Received: 02/16/2018 00:00 Sample Id : Sludge/92373556001 Date Reported: 02/23/2018 PARAMETER RESULT - maim RESULT QUANTITATION Total Solids " 43.74 437400 100.0 R D 02/16/2018 15:15 SM-254OG Moisture' 56.25 100.0 R D 02/16/2018 15:15 SM-2540G Total Kjeldahl Nitrogen 0.20 1990 50.0 R D 02/19/2018 08:40 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 45.80 458000 2500 R D 02/21/2018 12:30 AOAC 955.01 Total Volatile Solids 46.75 467500 100.0 R D 02/16/2018 15:15 SM-2540G C/N RATIO * 140 0 02/16/2018 15:15 CALCULATION Carbon (TOC) * 27.20 272000 100 02/16/2018 15:15 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Od re:•orrs and letters are fa the exclusive and confidential use of our clients, and may not be reproduced irs whole orpan, normay any reference be made ?WI: to tD;wcrk, tho results, Of the company in any advertising, neu-s mleas ar, d )vr Public announcements o mhout obtaorung our prior w.i+4on 'wlhonzation. 0 Pauric McGroary V Agronomist ,PaceAnalyfical www..pa&abs.com March 23, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92376666 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, ,1� Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 PMAnalj cal www.paceiabs.corn ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92376666 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92376666001 Collected: 03/12/18 15:05 Received: 03/13/18 09:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050 Arsenic ND mg/kg 1.8 0.89 1 03/14/1813:50 03/17/1819:04 7440-38-2 Calcium 167000 mg/kg 355 178 20 03/14/18 13:50 03/20/18 02:47 7440-70-2 Copper 20.5 mg/kg 0.89 0.44 1 03/14/1813:50 03/17/1819:04 7440-50-8 Magnesium 1630 mg/kg 17.8 0.44 1 03/14/1813:50 03/17/1819:04 7439-95-4 Nickel 1.7 mg/kg 0.89 0.44 1 03/14/1813:50 03/17/1819:04 7440-02-0 Zinc 58.8 mg/kg 1.8 0.89 1 03/14/1813:50 03/17/1819:04 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 41.4 % 0.000010 1 03/13/18 17:13 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 58.6 % 0.10 0.10 1 03/14/18 10:41 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.4 Std. Units 0.10 0.10 1 03/15/18 14:15 (Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 459 mg/kg 0.12 0.12 1 03/23/18 15:52 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1530 mg/kg 40.0 20.0 1 03/23/1815:43 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 24.2 24.2 1 03/21/18 16:37 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1530 mg/kg 92.9 46.4 1 03/22/18 13:37 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 4.8 4.8 1 03/15/18 03:22 Nitrogen, Nitrite ND mg/kg 2.4 2.4 1 03/15/18 03:22 Nitrogen, NO2 plus NO3 ND mg/kg 4.8 4.8 1 03/15/18 03:22 Date: 03/23/2018 03:53 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 17 Page: 1 of 1 Report Number: 18-074-0207 ' Account Number: 05734���a �� M 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Monthly Sludge/92376666001 ANGELA BAIONI 9800 KINCEY AVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Date Sampled: 3/12/2018 15:05:00 Lab Number: 59212 Date Received: 03/15/2018 00:00 Sample Id : Monthly Sludge/92376666001 Date Reported: 03/22/2018 PARAMETER RESULT RESULT QUANTITATION LIMIT ANALYSIS ANALYST ., •. Total Solids " 41.86 418600 100.0 R D 03/15/2018 15:15 SM-254OG Moisture * 58.13 100.0 R D 03/15/2018 15:15 SM-2540G Total Kjeldahl Nitrogen 0.18 1790 50.0 R D 03/16/2018 09:00 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 38.50 385000 2500 R D 03/19/2018 13:00 AOAC 955.01 Total Volatile Solids 55.53 555300 100.0 R D 03/15/2018 15:15 SM-254OG C/N RATIO * 180 0 03/15/2018 15:15 CALCULATION Carbon (TOC) * 32.30 323000 100 03/15/2018 15:15 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. �,ri4` G¢orv�r/ Or �rv,,.ons and letters ore for the exclusive and confidenti,U as- of our crier fs, and may rat be nr duced in whola :: in. nor may any ie.•`erernce be ma.+e p is HI; wo,h, the results, or the company in arty ad;erfisiup, ti-ws n-wase, ort4rw. r oblk: mnnrunccments without on -"Iraq our prior AWtc rl at, 0 Pauric McGroary Agronomist axAnalj cal www.pacelabs.com t April 18, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92379782 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on April 05, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, 01 L qrn thou o�{ Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 r � AJceAnalX cal www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92379782 Sample: Monthly Sludge Lab ID: 92379782001 Collected: 04/05/18 09:00 Received: 04/05/18 11:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic ND mg/kg 1.6 0.81 1 04/06/18 21:50 04/09/18 19:22 7440-38-2 Calcium 150000 mg/kg 162 80.8 10 04/06/18 21:50 04/10/18 14:54 7440-70-2 Copper 22.0 mg/kg 0.81 0.40 1 04/06/18 21:50 04/09/18 19:22 7440-50-8 Magnesium 1240 mg/kg 16.2 0.40 1 04/06/18 21:50 04/09/18 19:22 7439-95-4 Nickel 1.2 mg/kg 0.81 0.40 1 04/06/18 21:50 04/09/18 19:22 7440-02-0 Zinc 97.1 mg/kg 1.6 0.81 1 04/06/18 21:50 04/09/18 19:22 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 44.8 % 0.000010 1 04/05/18 17:53 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 55.2 % 0.10 0.10 1 04/06/18 10:44 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 8.4 Std. Units 0.10 0.10 1 04/06/18 12:03 )Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 489 mg/kg 0.12 0.12 1 04/18/18 17:12 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1630 mg/kg 40.0 20.0 1 04/18/1816:57 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 15.3 15.3 1 04/17/18 14:43 7664-41-7 R1 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1630 mg/kg 101 50.7 1 04/11/18 13:13 7727-37-9 363.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 4.5 4.5 1 04/11/18 23:19 Nitrogen, Nitrite ND mg/kg 2.2 2.2 1 04/11/18 23:19 Nitrogen, NO2 plus NO3 ND mg/kg 4.5 4.5 1 04/11/18 23:19 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04118/2018 05:14 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17 Page: 1 of 1 Report Number: 18-100-0207 ' Account Number: 05734���� �� 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92379782001 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 Lab Number: 59610 Sample Id : Sludge-92379782001 REPORT OF ANALYSIS Date Sampled: 4/5/2018 09:00:00 Date Received: 04/10/2018 00:00 Date Reported: 04/17/2018 ANALYST Total Solids ` 44.58 445800 100.0 JM 04/10/2018 15:00 SM-2540G Moisture'` 55.41 100.0 JM 04/10/2018 15:00 SM-254OG Total Kjeldahl Nitrogen 0.21 2110 50.0 R D 04/11/2018 08:30 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 43.10 431000 2500 R D 04/13/2018 12:15 AOAC 955.01 Total Volatile Solids 50.31 503100 100.0 JM 04/10/2018 15:00 SM-2540G C/N RATIO " 140 0 04/10/2018 15:00 CALCULATION Carbon (TOC) * 29.30 293000 100 04/10/2018 15:00 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. v �qw 0 60,1nrcits and fetters are for the exclusive an:9 confideii:iai use of our ciier?is, and may no be reproducei! in wnoie or part, normay any reference be made to 0 woik, the results, or the company in any advertising, news release, or other p.rhlic announceme,)ts without obtaining ow'p ror wd1tun authorization. 0 JPauric McGroary Agronomist VIC aceAnalyiical www.pacelabs.mn May 21, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92383860 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, C +1 . '-�=N' Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 10? /4 FaceAnalytica! ..pacetabsxom ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92383860 Sample: Monthly Sludge Lab ID: 92383860001 Collected: 05/08/18 07:25 Received: 05/08118 10:19 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic ND mg/kg 1.9 0.95 1 05/19/18 16:00 05/20/18 20:20 7440-38-2 Calcium 187000 mg/kg 190 95.1 10 05119/1816:00 05/2111815:41 7440-70-2 M6 Copper 19.9 mg/kg 0.95 0.48 1 05/19/18 16:00 05/20/18 20:20 7440-50-8 Magnesium 1570 mg/kg 19.0 0.48 1 05/19/18 16:00 05/20/18 20:20 7439-95-4 Nickel 1.2 mg/kg 0.95 0.48 1 05/19/18 16:00 05/20/18 20:20 7440-02-0 Zinc 60.3 mg/kg 1.9 0.95 1 05/19/18 16:00 05/20/18 20:20 7440-66-6 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 44.6 % 0.000010 1 05/09/18 15:21 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 55.4 % 0.10 0.10 1 05/10/18 10:59 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.7 Std. Units 0.10 0.10 1 05/11/18 03:12 H1 Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 390 mg/kg 0.12 0.12 1 05/17/18 16:40 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1300 mg/kg 40.0 20.0 1 05/17/1816:47 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 22.0 22.0 1 05/1511814:47 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1300 mg/kg 66.0 33.0 1 05/16/18 01:57 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 4.4 4.4 1 05/16/18 21:35 Nitrogen, Nitrite ND mg/kg 2.2 2.2 1 05/16/18 21:35 Nitrogen, NO2 plus NO3 ND mg/kg 4.4 4.4 1 05/16/18 21:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2018 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19 Report Number: 18-130-0201 • a. Account Number: 05734�point,, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92383860001 ANGELA BAIONI 9800 KINCEYAVENU= SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Lab Number: 60605 Sample Id : Sludge-92383860001 Date Sampled: 5/8/2018 07:25:00 Date Received: 05/10/2018 00:00 Date Reported: 05/18/2018 Total Solids * 44.06 440600 100.0 R D 05/10/2018 14:30 SM-2540G Moisture * 55.93 100.0 R D 05/10/2018 14:30 SM-2540G Total Kjeldahl Nitrogen 0.18 1790 50.0 JM 05/11/2018 08:30 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 40.90 409000 2500 R D 05/15/2018 10:30 AOAC 955.01 Total Volatile Solids 52.63 526300 100.0 R D 05/10/2018 14:30 SM-2540G C/N RATIO * 387.3 0 05/10/2018 14:30 CALCULATION Carbon (TOC) * 30.60 306000 100 05/10/2018 14:30 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not to the work, the results, or the company in any advertising, . -- release, or other public am Pofie. P 101*vr Pauric McGroary Page 18 of 19 Agronomist Page 2 ,i 3 YaxAnalytical" � / 1 www.pacelabs.cw June 25, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92388134 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on June 12, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, a.Qt0��1 Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 I PaceAnalj cal www.pacelabs.eom ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92388134 Sample: Monthly Sludge Lab ID: 92388134001 Collected: 06/12/18 07:30 Received: 06/12/18 10:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic ND mg/kg 1.6 0.79 1 06/13/18 10:25 06/14/18 23:49 7440-38-2 Calcium 211000 mg/kg 317 158 20 06/13/18 10:25 06/15/1817:11 7440-70-2 Copper 18.4 mg/kg 0.79 0.40 1 06/13/18 10:25 06/14/18 23:49 7440-50-8 Magnesium 1360 mg/kg 15.8 0.40 1 06/13/18 10:25 06/14/18 23:49 7439-95-4 Nickel 2.6 mg/kg 0.79 0.40 1 06/13/18 10:25 06/14/18 23:49 7440-02-0 Zinc 92.0 mg/kg 1.6 0.79 1 06/1311810:25 06/15/1812:05 7440-66-6 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 44.5 % 0.000010 1 06/12/18 17:00 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 55.5 % 0.10 0.10 1 06/13/18 10:27 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.6 Std. Units 0.10 0.10 1 06/14/18 08:08 �PlantAvailable Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 624 mg/kg 0.12 0.12 1 06/25/18 11:38 N2 Total Nitrogen Calculation Analytical Method: TKN+NC3+NO2 Calculation Nitrogen 2080 mg/kg 40.0 20.0 1 06/21/18 20:03 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen, Ammonia ND mg/kg 15.4 15A 1 06/18/1815:08 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 2080 mg/kg 77.5 38.8 1 06/16/18 02:31 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrate ND mg/kg 4.4 4.4 1 06/16/18 02:35 Nitrogen, Nitrite ND mg/kg 2.2 2.2 1 06/16/18 02:35 Nitrogen, NO2 plus NO3 ND mg/kg 4.4 4.4 1 06/16/18 02:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2018 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Report Number: 18-164-0204 Account Number: 05734 Waypoint-(Z-1 ANALYTICAL Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project: 92388134001 ANGELA BAIONI 9800 KINCEY AVENUE SUITE 100 HUNTERSVILLE , NC 28078 Lab Number: 61167 Sample Id : 92388134001 Total Solids' Moisture " Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO " Carbon (TOC)' Comments: REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 6/12/2018 07:30:00 Date Received: 06/13/2018 00:00 Date Reported: 06/18/2018 44.26 442600 100.0 R D 06/13/2018 12:30 SM-254OG 55.73 100.0 R D 06/13/2018 12:30 SM-254OG 0.15 1490 50.0 R D 06/14/2018 08:30 SM-4500-NH3C-TKN 39.20 392000 2500 R D 06/15/2018 08:30 AOAC 955.01 54.65 546500 100.0 R D 06/13/2018 12:30 SM-254OG 210 0 06/13/2018 12:30 CALCULATION 31.80 318000 100 06/13/2018 12:30 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and to the wi.dk, the results, or the company in any advertising, pwir- #1V 60° r Pauric McGroary Agronomist Page 19 of 21 Page 3 _)1 PaceAnalytical www.pacelabs.com July 26, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92391776 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on July 12, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless' otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 PaceAnalytical www.pacelabs.com August 13, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 RE: Project: Sludge TN resample Pace Project No.: 92393883 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 1 of 14 aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92391776 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92391776001 Collected: 07/11/18 08:00 Received: 07/12/18 11:59 Matrix: Solid Results reported on a "dry welght7 basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050B Arsenic ND mg/kg 2.2 1.1 1 07/13/18 10:30 07/16/18 00:55 7440-38-2 Calcium I 158000 mglkg 437 219 20 07/13/18 10:30 07/16/18 22:39 7440-70-2 Copper 20.9 mg/kg 1.1 0.55 1 07113/18 10:30 07/16/18 00:55 7440-50-8 Magnesium 1580 mg/kg 21.9 0.55 1 07/13/18 10:30 07/16/18 00:55 7439-95-4 Nickel 2.1 mg/kg 1.1 0.55 1 07/13/18 10:30 07/16/18 00:55 7440-02-0 Zinc 134 mg/kg 2.2 1.1 1 07/13/18 10:30 07/16/18 00:55 7440-66-6 2540G Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 39.4 %, 0.000010 i Percent Moisture I Analytical Method: ASTM D2974-87 Percent Moisture 60.6 % 0.10 0.10 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 7.7 Std. Units 0.10 0.10 Plant Available Nitrogen Analytical Method: SM 271 OB-2011 Plant Available Nitrogen pwe9 ' - r • 11300 . mg/kg 0.12 0.12 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen I�w 28800 mg/kg 40.0 20.0 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia 42Ct-0$4-11 13400 mg/kg 497 497 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total !'�t`!�!'f'�C" 28800 mglkg 3620 1810 363.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 Ae4ttq, ND mg/kg 5.1 5.1 Nitrogen, Nitrate ND mg/kg 5.1 5.1 Nitrogen, Nitrite ND mg/kg 2.5 2.5 1 07/13/18 14:19 1 07/16/18 09:17 1 07/1611815:50 H1 1 07/26/1819:47 N2 1 07/25/1814:22 7727-37-9 20 07/19/18 03:00 7664-41-7 100 07/18/18 05:54 7727-37-9 1 07/20/18 21:15 1 07/20/18 21:15 14797-55-8 1 07/20/18 21:15 14797-65-0 Se-e Xow t 6 wC Slrt . REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2018 07:51 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 4W00/1 PaceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge TN resample Pace Project No.: 92393883 Sample: Monthly Sludge Lab ID: 92393883001 Collected: 07/31/18 06:18 Received: 07/31/18 09:39 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Percent Moisture Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 )Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 08/13/2018 05:17 PM Analytical Method: ASTM D2974-87 55.1 % 0.10 0.10 1 07/31/1817:50 Analytical Method: SM 271 OB-2011 498 mg/kg 0.12 0.12 1 08/1311817:11 N2 Analytical Method: TKN+NO3+NO2 Calculation 1660 mg/kg 40.0 20.0 1 08/09/18 20:36 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 20.6 20.6 1 08/02/18 09:58 08/02/18 12:33 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1660 mg/kg 106 53.0 1 08/06/18 11:26 08/07/18 03:44 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.4 4.4 1 08/07/1811:07 08/07/1816:52 ND mg/kg 4.4 4.4 1 08/07/1811:07 08/07/1816:52 14797-55-8 ND mg/kg 2.2 2.2 1 08/07/1811:07 08/07/1816:52 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 14 Report Number: 18-198-0201 Account Number: 05734 Waypoint-(D ANALYTICAL Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : 92391776 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Lab Number: 61741 Sample Id : Monthly Sludge 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/11/2018 08:00:00 Date Received: 07/17/2018 00:00 Date Reported: 07/20/2018 Total Solids * 39.25 392500 100.0 JM 07/17/2018 15:30 SM-2540G Moisture * 60.74 100.0 JM 07/17/2018 15:30 SM-2540G Total Kjeldahl Nitrogen 0.17 1730 50.0 R D 07/18/2018 09:00 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 2.94 29400 2500 R D 07/19/2018 14:02 AOAC 955.01 Total Volatile Solids 53.53 535300 100.0 JM 07/17/2018 15:30 SM-254OG C/N RATIO * 180 0 07/17/2018 15:30 CALCULATION Carbon (TOC) * 31.10 311000 100 07/17/2018 15:30 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prim written authorization. Pauric McGroary Page 18 of 20 Agronomist Page 2 of 4 00001 FaceAnaljftal Wmpawabs.com September 05, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92394750 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. A revised report is being submitted on 9/5/18 to include a revised subcontract laboratory report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 1 of 21 -0 aceAnalytical' www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92394750 Sample: Monthly Sludge Lab ID: 92394760001 Collected: 08/06/18 15:15 Received: 08/07/18 10:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 09/05/2018 04:15 PM Analytical Method: EPA 6010D Preparation Method: EPA 3050E ND mg/kg 2.1 1.0 1 08/08/18 10:13 08/10/18 01:33 7440-38-2 168000 mg/kg 208 104 10 08/08/18 10:13 08/11/18 20:19 7440-70-2 18.9 mg/kg 1.0 0.52 1 08/08/18 10:13 08/10/18 01:33 7440-50-8 1630 mg/kg 20.8 0.52 1 08/08/18 10:13 08/10/18 01:33 7439-95-4 1.1 mg/kg 1.0 0.52 1 08/08/18 10:13 08/10/18 01:33 7440-02-0 102 mg/kg 2.1 1.0 1 08/08/18 10:13 08/10/18 01:33 7440-66-6 Analytical Method: SM 254OG-2011 44.6 % 0.000010 1 08/07/1817:31 Analytical Method: ASTM D2974-87 55.4 % 0.10 0.10 1 08/07/1817:28 Analytical Method: EPA 9045D 7.1 Sid. Units 0.10 0.10 1 08/13/18 12:23 Analytical Method: SM 271OB-2011 336 mg/kg 0.12 0.12 1 08122/1817:36 Analytical Method: TKN+NO3+NO2 Calculation 1120 mg/kg 40.0 20.0 1 08/22/1817:41 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 18.1 18.1 1 08/10/1812:59 08/1011817:03 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1120 mg/kg 83.1 41.6 1 08/21/18 01:46 08/22/18 01:40 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.5 4.5 1 08/17/1810:49 08/17/1814:05 ND mg/kg 4.5 4.5 1 08/17/1810:49 08/17/1814:05 14797-55-8 ND mg/kg 2.2 2.2 1 08/17/1810:49 0811711814:05 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H1 N2 Page 6 of 21 Report Number: 18-221-0204 Account Number: 05734 r Waypoint' ANALYTICAL Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 Lab Number: 62217 Sample Id : Monthly Sludge Project : 92394750 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 8/6/2018 15:15:00 Date Received: 08/09/2018 00:00 Date Reported: 09/05/2018 Total Solids * 44.40 444000 100.0 R D 08/31/2018 14:30 SM-2540G Moisture * 55.60 100.0 R D 08/31/2018 14:30 SM-2540G Total Kjeldahl Nitrogen 0.19 1870 50.0 R D 08/10/2018 08:30 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 27.60 276000 2500 R D 08/14/2018 10:30 AOAC 955.01 Total Volatile Solids 47.38 473800 100.0 R D 08/31/2018 14:30 SM-2540G C/N RATIO * 150 0 08/10/2018 08:30 CALCULATION Carbon (TOC) * 27.50 275000 100 08/31/2018 14:30 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining Pauric McGroary Agronomist Page 2 PaceAna1j cal www.pacelabs.com September 19, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92398534 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on September 06, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, a, W1. Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 �aceAnafj4ical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92398534 Sample: Monthly Sludge Lab ID: 92398534001 Collected: 09/06/18 07:40 Received: 09/06/18 08:17 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C ,Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 360.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 09/19/2018 04:36 PM Analytical Method: EPA 601 OD Preparation Method: EPA 3050B ND mg/kg 1.9 0.95 1 09/10/18 13:34 09/12/18 06:35 7440-38-2 179000 mg/kg 380 190 20 09/10/18 13:34 09/12/18 21:38 7440-70-2 14.5 mg/kg 0.95 0.48 1 09/10/18 13:34 09/12/18 06:35 7440-50-8 1400 mg/kg 19.0 0.48 1 09/10/18 13:34 09/12/18 06:35 7439-95-4 1.6 mg/kg 0.95 0.48 1 09/10/18 13:34 09/12/18 06:35 7440-02-0 297 mg/kg 1.9 0.95 1 09/10/18 13:34 09/12/18 06:35 7440-66-6 Analytical Method: SM 254OG-2011 46.1 % 0.000010 1 09/06/1817:45 Analytical Method: ASTM D2974-87 53.9 % 0.10 0.10 1 09/06/1817:36 Analytical Method: EPA 9045D 8.3 Std. Units 0.10 0.10 1 09/09/18 11:43 Analytical Method: SM 271OB-2011 423 mg/kg 0.12 0.12 1 09/19/18 09:02 Analytical Method: TKN+NO3+NO2 Calculation 1410 mg/kg 40.0 20.0 1 09/14/1815:39 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 21.3 21.3 1 09/11/1810:03 09/12/1814:30 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1410 mg/kg 90.3 45.2 1 09/12/18 02:26 09/13/18 07:32 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.3 4.3 1 09/07/18 01:00 09/07/18 04:34 ND mg/kg 4.3 4.3 1 09/07/18 01:00 09/07/18 04:34 14797-55-8 ND mg/kg 2.2 2.2 1 09/07/18 01:00 09/07/18 04:34 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H6 N2 Page 5 of 21 Report Number: 18-254-0206 Account Number: 05734 W 7621 Whitepine Road, Richmond, VA 23237 Waypoint Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. pwic- im` 6ewr Our reports and letters are for the exclusive and confidential use of our clients, and may not be .rrl+ r:,r:r, 14,c -Ihvre I +arr r,i I be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or otherpublic annuren.,rrrirrid;; cuft:rout nit uu r 4.ue.r r+rrr„ ,�y0r" Agronomist Page 18 of 21 Page 2 1 aceAnalj cal" www.pacelabs.com October 31, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92402749 Pace Analytical Services, LLC 6701 Conference Drive Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on October 09, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. Raleigh, NC 27607 (919)834-4984 A revised report is being submitted on 10/31/18 to revise the total nitrogen calculation. It was input incorrectly. If you have any questions concerning this report, please feel free to contact me. Sincerely, o-q�,' Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pagel of 22 aceAnalytical® r www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92402749 Sample: Monthly Sludge Lab ID: 92402749001 Collected: 10/09/18 07:30 Received: 10/09118 09:40 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 10/31/2018 10:01 AM Analytical Method: EPA 601OD Preparation Method: EPA 3050B ND mg/kg 2.0 1.0 1 10/11/1810:23 10/12/1815:59 7440-38-2 157000 mg/kg 205 102 10 10/11/1810:23 10/15/1812:19 7440-70-2 22.7 mg/kg 1.0 0.51 1 10/11/1810:23 10/12/1815:59 7440-50-8 1650 mg/kg 20.5 0.51 1 10111/1810:23 10/12/1815:59 7439-95-4 2.1 mg/kg 1.0 0.51 1 10111/1810:23 10112/1815:59 7440-02-0 118 mg/kg 2.0 1.0 1 10/11/1810:23 10/12/1815:59 7440-66-6 Analytical Method: SM 2540G-2011 43.6 % 0.000010 1 10/09/1817:39 Analytical Method: ASTM D2974-87 56.4 % 0.10 0.10 1 10/09/1817:37 Analytical Method: EPA 9045D 7.1 Std. Units 0.10 0.10 1 10/16/18 11:21 Analytical Method: SM 271OB-2011 540 mg/kg 0.12 0.12 1 10/22/1815:13 N2 Analytical Method: TKN+NO3+NO2 Calculation 1800 mg/kg 40.0 20.0 1 10122/1817:07 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 19.8 19.8 1 10/16/1814:29 10/1711814:18 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1800 mg/kg 115 57.4 1 10/14/18 14:41 10/16/18 01:29 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.4 4.4 1 10117/18 14:33 10/18/18 00:09 H1 ND mg/kg 4.4 4.4 1 10/17/18 14:33 10/18/18 00:09 14797-55-8 H1 ND mg/kg 2.2 2.2 1 10/17/18 14:33 10/18/18 00:09 14797-65-0 H1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 22 Report Number: 18-284-0203 Account Number: 05734 ����� �� 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92402749001 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Date Sampled: 10/9/2018 07:30:00 Date Received: 10/11/2018 00:00 Date Reported: 10/22/2018 Lab Number: 63122 Sample Id : 92402749001 Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: 43.10 431000 100.3 CJR 10/17/201815:59 SM-2540G 56.90 100.3 CJR 10/17/201815:59 SM-254OG 0.34 3360 250 CLP 10/19/201810:00 SM-4500-NH3C-TKN 24.90 249000 1000 DXT 10/19/2018 14:20 AOAC 955.01 53.40 534000 100.3 CJR 10/18/201816:39 SM-254OG 92 0 10/17/201815:59 CALCULATION 31.00 310000 100 10/18/201816:39 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not: to the work, the results, or the company in any advertising, news release, or other public am PaW« m` G06,'•' Pauric McGroary Agronomist Page 20 of 22 Page 3 of '-• .'T PaceAnalytical www..pacelabs.com :r November 26, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92406635 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sarah Graham for Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 /5a'oeAna1j6ca1" www..pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92406635 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92406635001 Collected: 11/08/18 08:05 Received: 11/08/18 08:32 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 360.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 11/26/2018 11:50 AM Analytical Method: EPA 601OD Preparation Method: EPA3050B ND mg/kg 1.7 0.87 1 11/09/18 12:22 11/10/18 04:02 7440-38-2 160000 mg/kg 173 86.7 10 11/09/18 12:22 11/10/18 20:28 7440-70-2 16.5 mg/kg 0.87 0.43 1 11/09/18 12:22 11/10/18 04:02 7440-50-8 1460 mg/kg 17.3 0.43 1 11/09/18 12:22 11/10/18 04:02 7439-95-4 2.1 mg/kg 0.87 0.43 1 11/09/18 12:22 11/10/18 04:02 7440-02-0 166 mg/kg 1.7 0.87 1 11/09/18 12:22 11/10/18 04:02 7440-66-6 Analytical Method: SM 2540G-2011 42.4 % 0.000010 1 11/08/1818:17 Analytical Method: ASTM D2974-87 57.6 % 0.10 0.10 1 11/08/1818:11 Analytical Method: EPA 9045D 7.4 Sid. Units 0.10 0.10 1 11/12/18 12:12 Analytical Method: SM 271 OB-2011 456 mg/kg 0.12 0.12 1 11/20/1814:44 Analytical Method: TKN+NO3+NO2 Calculation 1520 mg/kg 40.0 20.0 1 11/19/18 09:54 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 21.4 21.4 1 11111/1811:23 11/13/1813:34 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1620 mg/kg 94.3 47.1 1 11/14/18 01:17 11/14/18 13:16 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.7 4.7 1 11/09/18 02:38 11/09/18 13:15 ND mg/kg 4.7 4.7 1 11/09/18 02:38 11/09/18 13:15 14797-55-8 ND mg/kg 2.3 2.3 1 11/09/18 02:38 11/09/18 13:15 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H3 N2 Page 5 of 21 Report Number: 18-317-0206 Account Number: 05734 ���1110 ON � �� M 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge - 92406635001 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 Lab Number: 63522 Sample Id : Sludge - 92406635001 Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: REPORT OF ANALYSIS Date Sampled: 11/8/2018 08:05:00 Date Received: 11/13/2018 00:00 Date Reported: 11 /21 /2018 kESULT RESULT QUANTITATION Ak METHOD 43.30 433000 100.0 CJR 11/15/201815:30 SM-2540G 56.70 100.0 CJR 11/15/201815:30 SM-2540G 0.52 5220 250 CLP 11/19/201813:30 SM-4500-NH3C-TKN 36.20 362000 1000 DXT 11/19/2018 11:30 AOAC 955.01 52.70 527000 100.0 CJR 11/15/201815:30 SM-2540G 59 0 11/15/201815:30 CALCULATION 30.60 306000 100 11/15/201815:30 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in vm*- o 1kin rror ur.iy :viy ii.ftur uck 1Kv nimka to the work, the results, or the company in any advertising, news release, or other public announcements m1hrnit onroreriin rx+rp+ni;: ovrirwwi �utlii5l+l.rlrerrl. par« it G� Pauric McGroary Page 19 of 21 Agronomist Page 3 of 5 aceAnaljd cal www.pacelabs.com December 21, 2018 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92409891 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, a, q, fU Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 �- aceAnalj cal www..pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92409891 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92409891001 Collected: 12/06/18 07:55 Received: 12/06/18 10:55 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 12/21/2018 05:08 PM Analytical Method: EPA 601OD Preparation Method: EPA3050B ND mg/kg 1.7 0.84 1 12/14/18 09:37 12/16/18 20:41 7440-38-2 185000 mg/kg 838 419 50 12/14/18 09:37 12/17/18 13:44 7440-70-2 37.0 mg/kg 0.84 0.42 1 12/14/18 09:37 12/16/18 20:41 7440-50-8 1740 mg/kg 16.8 0.42 1 12/14/18 09:37 12/16/18 20:41 7439-95-4 1.4 mg/kg 0.84 0.42 1 12/14/18 09:37 12/16/18 20:41 7440-02-0 76.2 mg/kg 1.7 0.84 1 12/14/18 09:37 12/16/18 20:41 7440-66-6 Analytical Method: SM 2540G-2011 42.0 % 0.000010 1 12/06/1818:14 Analytical Method: ASTM D2974-87 58.0 % 0.10 0.10 1 12/06/1818:06 Analytical Method: EPA 9045D 7.4 Std. Units 0.10 0.10 1 12/13/18 07:10 Analytical Method: SM 271 OB-2011 235 mg/kg 0.12 0.12 1 12/21/1811:47 Analytical Method: TKN+NO3+NO2 Calculation 782 mg/kg 40.0 20.0 1 12/21/1811:30 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 23.3 23.3 1 12/11/1816:21 12/12/1814:53 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 782 mg/kg 99.2 49.6 1 12/16/18 10:07 12/20/18 01:46 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.7 4.7 1 12/07/18 01:56 12/07/18 04:25 ND mg/kg 4.7 4.7 1 12/07/18 01:56 12/07/18 04:25 14797-55-8 ND mg/kg 2.3 2.3 1 12/07/18 01:56 12/07/18 04:25 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Wt: H3 N2 Page 5 of 21 Report Number: 18-346-0201 ON Account Number: 05734 ���� ��.M 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge - 92409891 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Date Sampled: 12/6/2018 07:55:00 Lab Number: 63900 Date Received: 12/12/2018 00:00 Sample Id : Sludge - 92409891 Date Reported: 12/21/2018 PARAMETER RESULT RESULT QUANTITATION ;��+a►!� Total Solids * 43.20 432000 100.0 CJR 12/14/2018 13:57 SM-2540G Moisture * 56.80 100.0 CJR 12/14/2018 13:57 SM-2540G Total Kjeldahl Nitrogen 1.09 10900 250 CLP 12/19/2018 15:30 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 51.40 514000 1000 DXT 12/17/2018 14:50 AOAC 955.01 Total Volatile Solids 49.80 498000 100.0 CJR 12/14/2018 13:57 SM-2540G C/N RATIO * 27 0 12/14/2018 13:57 CALCULATION Carbon (TOC) * 29.00 290000 100 12/14/2018 13:57 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, it ;i •ri :, ?•1. 41-1�11 . r - ,1i ;rJj' to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. porza mW 60wr Pauric McGroary Page 19 of 21 Agronomist Page 3 of 5 ff]SUMMIAt ENVinL"M EN'A_TECHNOE04=1F.S.1NC AnsNtic�i �:�bc+�atc�rles September 17, 2018 Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htti�:llwww.settek.com Karen Bellamy Cascades Tissue Group - North Carolina Inc 805 Midway Road Rockingham, NC 28379 TEL: 910-895-4033 FAX: 910-895-9887 RE: Sludge Dear Karen Bellamy: Order No.: 18081887 Summit Environmental Technologies, Inc. received 1 sample(s) on 8/31/2018 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, �Ie Holly Florea Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon OH200001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 28 Summit Environmental Technologies, Inc. Case Narrative SUMMIi. 3310 Win St. ENVt OMMEN-t4L TECHNGEOGIF$,M Cuyahoga Falls, Ohio44223 WO#: 18081887 TEL: (330) 253-8211 FAX. (330) 253-4489 Date 9/1 81887 Website: hJt ://www.seuek.com CLIENT: Cascades Tissue Group - North Carolina Inc Project: Sludge WorkOrder Narrative: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 18081887-OOIA SVOC-BNA_TCLP(8270D): Possible low bias in the associated samples for 1,4- Dichlorobenzene and Hexachloroethane due to low recovery in the LCS. 18081887-OOIA TCLP-SVOC-HERB_TCLP(8151): Surrogate recovery unable to be reliably evaluated due to dilution; Sample diluted due to matrix; Reporting Limits adjusted accordingly. Analytical Sequence QC Notes: CCV 40ng 58-341 SVOC-MSTR_S(8270): The CCV (Batch R88555) exhibited high recovery for many analytes; associated samples are ND for all analytes of interest. Original Page 2 of 28 SUMM11 , Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htw.-11Www.settek.com CLIENT: Cascades Tissue Group - North Carolina Inc Project: Sludge Case Narrative WO#: 18081887 Date: 9/17/2018 CCV 40ng S8-341 SVOC-MSTR_S(8270): The CCV (Batch R88555) exhibited low recovery for Hexachlorocyclopentadiene, Hexachlorocyclopentadiene is not a selected analyte in the associated data. LCS-33748 SVOC-BNA_TCLP(8270): LCS-33748(R88555) exhibited low recovery for 1,4- Dichlorobenzene and Hexachloroethane. Possible low bias in the associated samples for 1,4- Dichlorobenzene and Hexachloroethane. PEST CCV 50OPPB svoc-CPEST_npw(8081): The CCV (Batch R88630) exhibited low recovery for Methoxychlor. Possible low bias for Methoxychlor in the associated samples. MB-33731 tclp-svoc-CPEST_TCLP(8081): Possible low bias for Methoxychlor due to low recovery in the CCV. 8151 CCV 500 ug/ svoc-herb_npw(8151): 8151 CCV (Batch R88676) exhibits high recoveries for all analytes except low for MCPA and MCPP. All samples are ND. LCS-33790 TCLP-SVOC-HERB_TCLP(8151): The LCS (Batch 33790/R88676) exhibited high recovery for 2,4-D. The associated samples are ND for 2,4-D. 8151 CCV 500 ug/ svoc-herb_npw(8151): 8151 CCV (Batch R88676) exhibits high recoveries for all analytes except low for MCPA and MCPP. All samples are ND. TCLP BLK 9-5-18 TCLP-SVOC-HERB_TCLP(8151): the TCLP Method Blank exhibtied high recovery for Surrogate: DCAA. The Blank is ND for all analytes of interest. Original Page 3 of 28 Sumrff ENVI'r10WEN7A_ TECMNpt OGIr-3, INC Xlns+ytleal Labomfartet Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httrr:1Avww.settek.com CLIENT: Cascades Tissue Group - North Carolina Inc Project: Sludge Lab SamplelD Client Sample ID 18081887-001 Sludge Tag No Date Collected 8/28/2018 6.15.00 AM Workorder Sample Summary WO#: 18081887 17-Sep-18 Date Received Matrix 8/31/2018 7:55:00 PM Solid Page 4 of 28 Summit Environmental Technologies, Inc. WO#: 18081887 SUMMI : 3310 Win St. EP#Vii GNWENTA_ TECHNGt 0GIFS, INC Cuyahoga Falls, Ohio 44223 Date Reported: 9/17/2018 TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Cascades Tissue Group - North Carolina I Website: htti,://www.settek.com Address: 805 Midway Road Rockingham NC 28379 Received: 8/31 /2018 Project#: Sludge TCLP Metals Analysis (SW1311/6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 8/28/2018 TCLP Arsenic(As) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Barium(Ba) 5.00 ND mg/L Solid EPA 6010 1 100 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Cadmium(Cd) 0.100 ND mg/L Solid EPA 6010 1 1.00 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Chromium(Cr) 0.200 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Lead(Pb) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Selenium(Se) 0.0500 ND mg/L Solid EPA 6010 1 1.00 9/6/2018 KMO D Sludge 001 8/28/2018 TCLP Silver(Ag) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO D TCLP Mercury Analysis (SW1311/7470) Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 8/28/2018 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470 A 1 0.200 9/7/2018 DNS TCLP Pesticides Analysis (SW1311/8081) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 8/28/2018 Chlordane, total 0.0200 ND mg/L Solid EPA 8081 B 10 0.0300 9/12/2018 RIS Sludge 001 8/28/2018 Toxaphene 0.200 ND mg/L Solid EPA 8081 B 10 0.500 9/12/2018 RIS Sludge 001 8/28/2018 Endrin 0.00200 ND mg/L Solid EPA 8081 B 10 0.0200 9/12/2018 RIS Sludge 001 8/28/2018 gamma-BHC 0.00200 ND mg/L Solid EPA 8081 B 10 0.400 9/12/2018 RIS Sludge 001 8/28/2018 Heptachlor 0.00200 ND mg/L Solid EPA 8081 B 10 0.00800 9/12/2018 RIS Sludge 001 8/28/2018 Heptachlor epoxide 0.00200 ND mg/L Solid EPA 8081 B 10 0.00800 9/12/2018 RIS Sludge 001 8/28/2018 Methoxychlor 0.00200 ND mg/L Solid EPA 8081 B 10 10.0 9/12/2018 RIS Sludge 001 8/28/2018 Surr:TCMX 10-119 55.7 %Rec Solid EPA 8081B 10 9/12/2018 RIS Sludge 001 8/28/2018 Surr: DCB 10-119 79.5 %Rec Solid EPA 8081B 10 9/12/2018 RIS TCLP Herbicides Analysis (SW1311/8151) Client ID# Lab H)# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 8/28/2018 2,4-D 10.0 ND mg/L Solid EPA 8151 A 10 10.0 9/13/2018 MES Sludge 001 8/28/2018 2,4,5-TP 5.00 ND mg/L Solid EPA 8151 A 10 1.00 9/13/2018 MES Sludge 001 8/28/2018 Surr: DCAA 20-140 334 %Rec Solid EPA 8151 A 10 9/13/2018 MES Page 5 of 28 EN%'!n0N,VEN7A-TECHNOL001:3, W Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: ht+r,://www.settek.com WO#: 18081887 Date Reported: 9/17/2018 Company: Cascades Tissue Group - North Carolina I Address: 805 Midway Road Rockingham NC 28379 Received: 8/31/2018 Project#: Sludge TCLP Volatiles Analysis Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 8/28/2018 1,1-Dichloroethene 0.0500 ND mg/L Solid EPA 8260 B 10 0.700 9/6/2018 MES Sludge 001 8/28/2018 1,2-Dichloroethane 0.0500 ND mg/L Solid EPA 8260 B 10 0.500 9/6/2018 MES Sludge 001 8/28/2018 MEK 0.250 0.558 mg/L Solid EPA 8260 B 10 200 9/6/2018 MES Sludge 001 8/28/2018 Benzene 0.0500 ND mg/L Solid EPA 8260 B 10 0.500 9/6/2018 MES Sludge 001 8/28/2018 Carbon tetrachloride 0.0500 ND mg/L Solid EPA 8260 B 10 0.500 9/6/2018 MES Sludge 001 8/28/2018 Chlorobenzene 0.0500 ND mg/L Solid EPA 8260 B 10 100 9/6/2018 MES Sludge 001 8/28/2018 Chloroform 0.0500 ND mg/L Solid EPA 8260 B 10 6.00 9/6/2018 MES Sludge 001 8/28/2018 Tetrachloroethene 0.0500 ND mg/L Solid EPA 8260 B 10 0.700 9/6/2018 MES Sludge 001 8/28/2018 Trichloroethene 0.0500 ND mg/L Solid EPA 8260 B 10 0.500 9/6/2018 MES Sludge 001 8/28/2018 Vinyl chloride 0.0200 ND mg/L Solid EPA 8260 B 10 0.200 9/6/2018 MES Sludge 001 8/28/2018 Surr: 4- 70-130 98.8 %Rec Solid EPA 8260 B 10 9/6/2018 MES Bromofluorobenzene Sludge 001 8/28/2018 Surr: 70-130 109 %Rec Solid EPA 8260 B 10 9/6/2018 MES Dibromofluoromethane edge 001 8/28/2018 Surr: Toluene-d8 70-130 104 %Rec Solid EPA 8260 B 10 9/6/2018 MES Page 6 of 28 I Client ID# Summit Environmental Technologies, Inc. WO#: - 3310 Win St. ENV,F ONIIVEN-A-' TECHNOL:OOrS, INC, Cuyahoga Falls, Ohio 44223 Date Reported: TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Website: htt,,://www.settek.com Address: Received: Project#: TCLP Semi-Volatiles Analysis (SW1311/8270) Lab ID# Collected Analyte Rep Lmt Result Units Matrix 18081887 9/1712018 Cascades Tissue Group - North Carolina I 805 Midway Road Rockingham NC 28379 8/31/2018 Sludge Method DF RegLv1 Run Analyst Sludge 001 8/28/2018 1,4-Dichlorobenzene 0.0800 ND mg/L Solid EPA 8270 2 7.50 9/10/2018 BJH D Sludge 001 8/28/2018 2,4,5-Trichlorophenol 0.200 ND mg/L Solid EPA 8270 2 400 9/10/2018 BJH D Sludge 001 8/28/2018 2,4,6-Trichlorophenol 0.200 ND mg/L Solid EPA 8270 2 2.00 9/10/2018 BJH D Sludge 001 8/28/2018 2,4-Dinitrotoluene 0.0400 ND mg/L Solid EPA 8270 2 0.130 9/10/2018 BJH D Sludge 001 8/28/2018 o-Cresol 0.200 ND mg/L Solid EPA 8270 2 9/10/2018 BJH D Sludge 001 8/28/2018 m/p-Cresol(s) 0.200 ND mg/L Solid EPA 8270 2 9/10/2018 BJH D Sludge 001 8/28/2018 Cresols, Total 4.00 ND mg/L Solid EPA 8270 2 200 9/10/2018 BJH D Sludge 001 8/28/2018 Hexachloro-1,3- 0.0160 ND mg/L Solid EPA 8270 2 0.500 9/10/2018 BJH butadiene D .fudge 001 8/28/2018 Hexachlorobenzene 0.0400 ND mg/L Solid EPA 8270 2 0.130 9/10/2018 BJH D Sludge 001 8/28/2018 Hexachloroethane 0.0800 ND mg/L Solid EPA 8270 2 3.00 9/10/2018 BJH D Sludge 001 8/28/2018 Nitrobenzene 0.0800 ND mg/L Solid EPA 8270 2 2.00 9/10/2018 BJH D Sludge 001 8/28/2018 Pentachlorophenol 0.200 ND mg/L Solid EPA 8270 2 100 9/10/2018 BJH D Sludge 001 8/28/2018 Pyridine 0.200 ND mg/L Solid EPA 8270 2 5.00 9/10/2018 BJH D Sludge 001 8/28/2018 Sum 2-Fluorophenol 10-109 26.0 %Rec Solid EPA 8270 2 9/10/2018 BJH D Sludge 001 8/28/2018 Surr: Phenol-d6 10-109 27.0 %Rec Solid EPA 8270 2 9/10/2018 BJH D Sludge 001 8/28/2018 Surr: Nitrobenzene- 19-120 42.3 %Rec Solid EPA 8270 2 9/10/2018 BJH d5 D Sludge 001 8/28/2018 Surr: 2,4,6- 10-120 31.1 %Rec Solid EPA 8270 2 9/10/2018 BJH Tribromophenol D Sludge 001 8/28/2018 Surr: 2- 22-117 45.4 %Rec Solid EPA 8270 2 9/10/2018 BJH Fluorobiphenyl D Sludge 001 8/28/2018 Surr: p-Terphenyl- 34-116 84.8 %Rec Solid EPA 8270 2 9/10/2018 BJH d14 D Page 7 of 28 Summit Environmental Technologies, Inc. Analytical Report SUMMOT 3310Win St. ENVOOM'TENva, TECHNt L OGISS, INC. Cuyahoga Falls, Ohio 44223 (consolidated) TEL: (330) 253-8211 FAX: (330) 253-4485 WO#: 18081887 Website: jUp://www.settek.com Date Reported: 9/17/2018 CLIENT: Cascades Tissue Group - North Carolina Inc Collection Date: 8/28/2018 6:15:00 AM Project: Sludge Lab ID: 18081887-001 Matrix: SOLID Client Sample ID Sludge Analyses Result PQL Qual Units DF Date Analyzed RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2)-SOLID Cyanide, Reactive ND 0.500 mg/Kg 1 9/6/2018 1:05:00 PM RCI-SOLID-WI IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW-846: 1030) Ignitability non-flammable 1 9/6/2018 2:30:00 PM RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: VVK PH (SW9045D) pH 7.1 s.u.@22.3C 1 9/5/2018 11:56:44 AM RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 9/6/2018 1:05:00 PM Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response ND Not Detected PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode Original Page 8 of 28 sul"Mur-- Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT llvt+liti}Np�1C Fd71L rrotiaut7!( ;cc tit Cuyahoga Falls, Ohio 44223 WO#: 18081887 .. .. TEL: (330) 253-8211 FAX. (330) 253-4489 Website: htt;):Ilwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33728 'ample ID mb-33728 SampType: MBLK TestCode: tclp-voc-mstr Units: mg/L Prep Date: 9/5/2018 RunNo: 88459 client ID: PBS Batch ID: 33728 TestNo: SW8260B SW1311M Analysis Date: 9/612018 SegNo: 1723507 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene ND 0.0500 1,2-Dichloroethane ND 0.0500 MEK ND 0.250 Benzene ND 0.0500 Carbon tetrachloride ND 0.0500 Chlorobenzene ND 0,0500 Chloroform ND 0.0500 Tetrachloroethene ND 0.0500 Trichloroethene ND 0.0500 Vinyl chloride ND 0.0200 Surr: 4-Bromofluorobenzene 474 Surr: Dibromofluoromethane 538 Surr: Toluene-d8 522 500.0 94.8 70 130 500.0 108 70 130 500.0 104 70 130 'ample ID Ics 13782/13818 SampType: LCS TestCode: tclp-voc-MST Units: mg/L Prep Date: RunNo: 88459 ;lient ID: LCSS Batch ID: 33728 TestNo: SW8260B SW1311M Analysis Date: 9/6/2018 SegNo: 1723515 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.0190 0.00500 1,2-Dichloroethane 0.0190 0.00500 MEK 0.0922 0.0250 Benzene 0.0187 0.00500 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds 0.0200 0 94.9 79.4 0.0200 0 94.9 73.6 0.100 0 92.2 55.1 0.0200 0 93.7 73.1 B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit 131 137 163 132 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 9 of 28 ' Summit Environmental Technologies, Inc. QC SUMMARY REPORT S U M M of 3310 Win St. F-XV100NhtENTAL TECTI N01 0-31r%, N% Cuyahoga Falls, Ohio 44223 WO#: 18081887 Antr/srticat L8bOrattrrt6s TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httn://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33728 iample ID Ics 13782113818 SampType: LCS TestCode: tclp-voc-MST Units: mg/L Prep Date: RunNo: 88459 client ID: LCSS Batch ID: 33728 TestNo: SW8260B SW1311M Analysis Date: 9/6/2018 SegNo: 1723515 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Carbon tetrachloride 0.0192 0.00500 0.0200 0 96.1 63.7 139 Chlorobenzene 0.0190 0.00500 0.0200 0 95.0 72.3 139 Chloroform 0.0190 0.00500 0.0200 0 94.8 79.3 129 Tetrachloroethene 0.0189 0.00500 0.0200 0 94.5 56.2 187 Trichloroethene 0.0178 0.00500 0.0200 0 89.1 64.1 138 Vinyl chloride 0.0249 0.00200 0.0200 0 124 22.1 147 Surr: 4-Bromofluorobenzene 50.6 50.00 101 80.4 126 Surr: Dibromofluorom ethane 52.9 50.00 106 70.3 125 Surr: Toluene-d8 51.3 50.00 103 82 117 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 28 Summit Environmental Technologies, Inc. SUMM161- 3310 Win St. QC SUMMARY REPORT VKA(l1t0NldEtdTAL TEt:1IN01 OGICS, lo' Cuyahoga Falls, Ohio 44223 • ..�- ••. TEL: (330) 253-8211 FAX:(330) 253-4489 WO#: 18081887 Website: httu://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33744 Sample ID MB-33744 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 9/7/2018 RunNo: 88486 Client ID: PBS Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 9/7/2018 SegNo: 1724470 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 0.00200 Sample ID LCS-33744 SampType: LCS TestCode: HG TCLP(74 Units: PPM Prep Date: 9/7/2018 RunNo: 88486 Client ID: LCSS Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 91712018 SegNo: 1724471 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00406 0.00200 0.00400 0 102 80 120 Sample ID 18081785-007AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 91712018 RunNo: 88486 Client ID: Batch= Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 9/712018 SegNo: 1724478 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00639 0.00200 0.00400 0.00160 120 75 125 0.00656 2.63 20 Sample ID 18081785-007AMS SampType: MS TestCode: HG_TCLP(74 Units: PPM Prep Date: 9/7/2018 RunNo: 88486 Client ID: BatchQC Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 9/7/2018 SegNo: 1724494 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00656 0.00200 0.00400 0.00160 124 75 Qualifiers: * Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds PL Permit Limit 125 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 11 of 28 uSm MI-1 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT EN0it-)Nh104TAL TEC1lN01 tltt•.F5, '•' Cuyahoga Falls, Ohio 44223 WO#: 18081887 TEI,: (330) 253-8211 FAX.- (330) 253-4489 Website: httu.11www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33744 Sample ID 18081785-007AMS SampType: MS TestCode: HG TCLPl74 Units: PPM Prep Date: 9/7/2018 RunNo: 88486 Client ID: BatchQC Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 9/7/2018 SegNo: 1724494 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 28 SUMMI'. Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT Li44+11t }NP�1CNiAL is"I 741Ut7I f}y,IcS •, - Cuyahoga Falls, Ohio 44223 W04: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httl,r://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33790 Sample ID MB-33790 SampType: MBLK TestCode: TCLPSVOC- Units: mg/L Prep Date: 911012018 RunNo: 88710 Client ID: PBS Batch ID: 33790 TestNo: SW8161A SW8151A Analysis Date: 9/1312018 SegNo: 1733066 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 1.00 0 0 d 2,4,5-TP ND 0.500 0 0 d Surr: DCAA 333 500.0 66.5 20 140 m Sample ID LCS-33790 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 9/10/2018 RunNo: 88710 Client ID: LCSS Batch ID: 33790 TestNo: SW8151A SW8151A Analysis Date: 9/13/2018 SegNo: 1733067 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 1.00 0.500 0 125 62.6 125 2,4,5-TP ND 0.500 0.500 0 95.3 52.5 128 Surr: DCAA 532 500.0 106 20 140 Sample ID 18081870-001AMS SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 9/10/2018 RunNo: 88710 Client ID: BatchQC Batch ID: 33790 TestNo: SW8151A SW8151A Analysis Date: 9/13/2018 SegNo: 1733077 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D 2,4,5-TP Surr: DCAA ND 10.0 ND 5.00 1170 0.500 0 149 37 105 0.500 0 106 38 106 500.0 233 20 140 S S Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 28 sum'M101 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT EIv4t11tt7Nli1E1J7ltL riC]EQJ(71 CF✓aiF"i, n i. Cuyahoga Falls, Ohio 44223 WO#: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htty://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33790 >ample ID 18081870-001AMSD SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: 911012018 RunNo: 88710 ;lient ID: BatchQC Batch ID: 33790 TestNo: SW8151A SW8151A Analysis Date: 9/13/2018 SegNo: 1733082 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 10.0 0.500 0 142 37 105 0 0 30 RS 2,4,5-TP ND 5.00 0.500 0 95.0 38 106 0 0 30 Surr: DCAA 1090 500.0 217 20 140 0 S Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 14 of 28 to , Summit Environmental Technologies, Inc. 3310 Win St. QC, MA Y REPORT SUMMARY EN4fli4a"1,N!d[NTAL TCCi1tiNol l4F; r ; N Cuyahoga Falls, Ohio 44223 WO#: 18081887 ,4.nry° !cat TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: brtf,:Ilwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33790 Sample ID MB-33790 SampType: MBLK TestCode: TCLPSVOC- Units: mg/L Prep Date: 9/1012018 RunNo: 88676 Client ID: PBS Batch ID: 33790 TestNo: SW8161A SW8151A Analysis Date: 9/12/2018 SegNo: 1731414 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 1.00 0 0 2,4,5-TP ND 0.500 0 0 Surr: DCAA 357 500.0 71.5 20 140 Sample ID LCS-33790 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 9/10/2018 RunNo: 88676 Client ID: LCSS Batch ID: 33790 TestNo: SW8151A SW8161A Analysis Date: 9/12/2018 SegNo: 1731416 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 2,4-D ND 1.00 0.500 0 125 62.6 125 S 2,4,5-TP ND 0.500 0.500 0 90.0 52.5 128 Surr: DCAA 487 500.0 97.3 20 140 Sample ID 18081870-001AMS SampType: MS TestCode: TCLPSVOC- Units: mg/L Prep Date: 9110/2018 RunNo: 88676 Client ID: BatchQC Batch ID: 33790 TestNo: SW8161A SW8151A Analysis Date: 911212018 SegNo: 1731416 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 10.0 5.00 0 44.3 37 105 2,4,5-TP ND 5.00 5.00 0 10.3 38 106 S Surr: DCAA 1250 5000 25.0 20 140 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H MC Holding times for preparation or analysis exceeded Value is below Minimum Compound Limit. J Analyte detected below quantitation limits ND Not Detected M O Manual Integration used to determine RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 28 �J m M 111 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT EJK%fl1t(]NtdEt4TAL I_r nvrli i MrS;, I.r Cuyahoga Falls, Ohio 44223 W04: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-4489 Wehsite: htto•/fwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: 33790 sample ID 18081870-001AMSD SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: 9/10/2018 RunNo: 88676 ;lient ID: BatchQC Batch ID: 33790 TestNo: SW8151A 5W8151A Analysis Date: 9/12/2018 SegNo: 1731417 lnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 10.0 5.00 0 30.5 37 105 0 0 30 RS 2,4,5-TP ND 5.00 5.00 0 9.25 38 106 0 0 30 S Surr: DCAA 879 5000 17.6 20 140 0 S Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 16 of 28 1=Wni S U M M I Summit Environmental Technologies, St. Inc. 3310 Win St QC SUMMARY REPORT E6tVIOONtotENTAL 3EC.O+N01 (1GiFS, '•• Cuyahoga Falls, Ohio 44223 WO#: 18081887 M TEL: (330) 253-8211 FAX: (330) 253-4489 Website: httn://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88403 Sample ID LCS-R88403 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@22.2C Prep Date: RunNo: 88403 Client ID: LCSW Batch ID: R88403 TestNo: SW9045D Analysis Date: 9/512018 SegNo: 1722113 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] pH 7.0 7.0 0 100 98.6 101.4 Sample ID CHECK 7 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@22.1C Prep Date: RunNo: 88403 Client ID: LCSW Batch ID: R88403 TestNo: SW9045D Analysis Date: 9/5/2018 SegNo: 1722132 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual pH 7.0 7.0 0 101 98.6 101.4 Qualifiers: * Value exceeds Maximum Contaminant Level, H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 17 of 28 S,ITSummit Environmental Technologies, Inc. 3310WinSt. QC SUMMARY REPORT EF,'ktlltONIAE14TAL ir.CiiNOt,kl ; I,, Nr, Cuyahoga Falls, Ohio 44223 WO#: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto:llwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88429 Ignitability 7.08 7.240 0 97.8 70 130 Ignitability ; not propagate 0 0 20 Sample ID 18081886-001ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: BatchQC Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722773 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability not propagate 0 0 20 Sample ID 18081887-001ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: Sludge Batch ID: R88429 TestNo: SW1030 Analysis Date: 91612018 SegNo: 1722775 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability non-flammable Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected PL Permit Limit 0 0 20 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 18 of 28 sumown Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT Eh4"IikN6�1�1dTALfieYt7t7tc3Cir, 'ry Cuyahoga Falls, Ohio 44223 WO#: 18081887 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: httn:1Avww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88429 Sample ID 18081887-001ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: Sludge Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722775 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sample ID 18090063-004ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: Batch= Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722777 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability ; not propagate 0 0 20 Sample ID 18090063-004ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: BatchQC Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722778 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability not propagate 0 0 20 Sample ID 18090063-005ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 Client ID: Batch= Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722780 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability ; not propagate 0 0 20 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 28 SUMMINI Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT h1�111JNh1CNT1tL rt rt#tt71 [i .If ;, Ns, Cuyahoga Falls, Ohio 44223 WO#: 18081887 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: htta://immsettek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88429 Sample ID 18090063-005ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429 .',lient ID: Batch= Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722781 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Ignitability ; not propagate 0 0 20 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 20 of 28 S umiw1� Summit Environmental Technologies, Inc.r--Zirdou 3310WinSt. QC SUMMARY REPORT "00] F.FIt�IC?th11d1dTal. rEG)t.N(7tC C,iF, Cuyahoga Falls, Ohio 44223 WO#: 18081887 r1, TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hgg:llwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88479 Sample ID MB-R88479 SampType: MBLK TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 88479 Client ID: PBS Batch ID: R88479 TestNo: SW9014 Analysis Date: 9/6/2018 SegNo: 1724355 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive ND 0.500 Sample ID LCS-R88479 SampType: LCS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 88479 Client ID: LCSS Batch ID: R88479 TestNo: SW9014 Analysis Date: 9/612018 SegNo: 1724366 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 9.66 0.500 10.00 0 96.6 85 110 Sample ID RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mglKg Prep Date: RunNo: 88479 Client ID: BatchQC Batch ID: R88479 TestNo: SW9014 Analysis Date: 9/6/2018 SegNo: 1724358 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 0.552 0.500 0.5000 0 110 50 150 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 28 sumra1 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT C 01ti7Nt004TAL rCCC++Hn1 cta ". Hr. Cuyahoga Falls, Ohio 44223 WO#: 18081887 Anitty+ticat Labwatorles TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htte:1Avww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge SatchID: R88490 Sample ID MB-R88490 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 88490 Client ID: PBW Batch ID: R88490 TestNo: SW9034 Analysis Date: 9/6/2018 SegNo: 1724579 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive ND 25.0 Sample ID LCS-R88490 SampType: LCS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 88490 Client ID: LCSW Batch ID: R88490 TestNo: SW9034 Analysis Date: 916/2018 SegNo: 1724580 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Sulfide, Reactive 4630 25.0 4800 0 96.5 85 115 Sample ID 18090063-002AMS SampType: MS TestCode: Sulf[de,React Units: mg1L Prep Date: RunNo: 88490 Client ID: BatchQC Batch ID: R88490 TestNo: SW9034 Analysis Date: 9/6/2018 SegNo: 1724582 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 4610 25.0 4800 0 96.0 75 125 W NOTES: Sample was received not meeting proper temperature requirements. Sample ID 18090063-002AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 88490 Client ID: BatchQC Batch ID: R88490 TestNo: SW9034 Analysis Date: 9/6/2018 SegNo: 1724583 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 22 of 28 SUMMIMI Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT EPWIlcaSNIAENTtlt_ Ti:T:iiNO[L G2r!;, Nr: Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 18081887 Website: htty:llwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge BatchID: R88490 'ample ID 18090063-002AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 88490 ;lient ID: BatchQC Batch ID: R88490 TestNo: SW9034 Analysis Date: 9/6/2018 SegNo: 1724583 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 4720 25.0 4800 0 98.3 75 125 4610 2.36 30 W NOTES: Sample was received not meeting proper temperature requirements. Qualifiers: * Value exceeds Maximum Contaminant Level, H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 23 of 28 Summit Environmental Technologies, In SUMM 3310 Win Qualifiers and Acronyms j ENVItIOP4"IEN'A�-TECHNOLtr)GIf INC Cuyahoga Falls, Ohio 442: WO#: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-442 Website: ht0.-11Www.settek.co Date: 9/17/2018 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+), R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 24 of 28 S 'T Summit Environmental Technologies, Inc. DATES REPORT 3310 Win St. l:NtV111ONi404TAL TE-CHN01 0017 :„ Nr Cuyahoga Falls, Ohio 44223 "Btor�es WO#: 18081887 TEL: (330) 253-8211 FAX.- (330) 253-4485 Website: hgE://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc Project: Sludge Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date 18081887-OOIA Sludge 8/28/2018 6:15:00 AM Solid Ignitability of Solids (SW-846: 1030) 9/6/2018 2:30:00 PM pH (SW9045D) 9/5/2018 11:56:44 AM Reactive Cyanide (9014/7.3.3.2)-Solid 9/6/2018 1:05:00 PM Reactive Sulfide (9034)/73.4.2 9/6/2018 1:05:00 PM TCLP Herbicides Analysis (SW1311/89/5/2018 6:00:00 PM 9/10/2018 11:45:00 AM 9/13/2018 8:14:00 PM TCLP Herbicides Analysis (SW1311/89/5/2018 6:00:00 PM 9/12/2018 9:22:00 PM TCLP Mercury Analysis (SW 1311/7479/5/2018 6:00:00 PM 9/7/2018 10:00:00 AM 9/7/2018 2:31:00 PM TCLP Mercury Analysis (SW 1311/7479/5/2018 6:00:00 PM 9/7/2018 10:00:00 AM 9/7/2018 2:31:00 PM TCLP Metals Analysis (SW 1311/6010 9/5/2018 6:00:00 PM 9/6/2018 12:15:00 PM 9/6/2018 7:24:00 PM TCLP Pesticides Analysis (SW1311/8(9/5/2018 6:00:00 PM 9/6/2018 10:15:00 AM 9/12/2018 1:45:00 AM TCLP Semi-Volatiles Analysis 9/5/2018 6:00:00 PM 9/7/2018 11:30:00 AM 9110/2018 7:41:00 PM (SW 1311 /8270) TCLP Volatiles Analysis 9/5/2018 6:00:00 PM 9/6/2018 8:04:00 PM Original Page 25 of 28 SUMM111- Summit Environmental Technologies, Inc. Accreditation Program 3310 Win St. Anal tes Report ENVIRO+rNIEN'AL TECMN01OMFS, 11YC Cuyahoga Falls, Ohio44223 Y p 4J16f)4l-tt0 t.ubrrtgtort+ I TEL: (330) 253-8211 FAX.- (330) 253-4485 WO#: 18081887 Website: http://www.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc State: NW Project: Sludge Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 18081887-OOIA Solid Ignitability of Solids (SW-846: 1030) Ignitability A Solid pH (SW9045D) Hydrogen Ion (pH) A Solid Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive 11 Solid Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive 11 Solid TCLP Herbicides Analysis (SW1311/8151) 2,4,5-TP A Solid TCLP Herbicides Analysis (SWI311/8151) 2,4-D A Solid TCLP Herbicides Analysis (SWI311/8151) DCAA A Solid TCLP Mercury Analysis (SW1311/7470) Mercury A Solid TCLP Metals Analysis (SW1311/6010) Arsenic A Solid TCLP Metals Analysis (SW1311/6010) Barium A Solid TCLP Metals Analysis (SW1311/6010) Cadmium A Solid TCLP Metals Analysis (SW1311/6010) Chromium A Solid TCLP Metals Analysis (SW1311/6010) Lead A Solid TCLP Metals Analysis (SW1311/6010) Selenium A Solid TCLP Metals Analysis (SW1311/6010) Silver A Solid TCLP Pesticides Analysis (SW1311/8081) 2Z.3:3 4,4 ,5,5',6,6'- A Decachlornbiphernyl Solid TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Solid TCLP Pesticides Analysis (SW1311/8081) Endrin A Solid TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A Solid TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Solid TCLP Pesticides Analysis (SW1311/8081) Tetrachloro-m-xylene A Solid TCLP Pesticides Analysis (SW1311/8081) Toxaphene A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Tribromophenol A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorobiphenyl A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorophenol A Key Key NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Page 1 of 2 Original #1 0 T Summit Environmental Technologies, Inc. Accreditation Program 3310 Win St. Anal te5 Report ENVIFiONr.tEN-tt_TECHNGI7CIf_S, INC; Cuyahoga Falls, Ohio44223 Y p ro5rtfi TEL: (330) 253-8211 FAX: (330) 253-4485 WO#: 18081887 Website: htt :Ilwww.settek.com 17-Sep-18 Client: Cascades Tissue Group - North Carolina Inc State: NW Project: Sludge Program Name: NC WW SCM Sample ID Matrix Test Name Analyte Status 18081887-OOIA Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Methylphenol A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A Solid TCLP Semi-Volatiles Analysis (SWI311/8270) Cresols, Total A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A Solid TCLP Semi-Volatiles Analysis (SWI311/8270) Hexachloroethane A Solid TCLP Semi-Volatiles Analysis (SWI311/8270) Nitrobenzene A Solid TCLP Semi-Volatiles Analysis (SWI311/8270) Nitrobenzene-d5 A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Phenol-& A Solid TCLP Semi-Volatiles Analysis (SWI311/8270) p-Terphenyl-d14 A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A Solid TCLP Volatiles Analysis 1,1-Dichloroethene A Solid TCLP Volatiles Analysis 1,2-Dichloroethane A Solid TCLP Volatiles Analysis 2-Butanone A Solid TCLP Volatiles Analysis 4-QTomolluorobcrizme A Solid TCLP Volatiles Analysis Benzene A Solid TCLP Volatiles Analysis Carbon tetrachloride A Solid TCLP Volatiles Analysis Chlorobenzene A Solid TCLP Volatiles Analysis Chloroform A Solid TCLP Volatiles Analysis Dibromofluoromethane A Solid TCLP Volatiles Analysis Tetrachloroethene A Solid TCLP Volatiles Analysis Toluene-d8 A Solid TCLP Volatiles Analysis Trichloroethene A Solid TCLP Volatiles Analysis Vinyl chloride A Key Key NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Page 2 of 2 Original #1 n1 nii il■ g?e Rv% 1 i lliMltT 0910; 1 -i ."1f E SUMMIT Analysis Request / Chum of Custody LN-41ROMMLNTAt TECt#NOk r.M-S. INC h'r ulitntii E nl'a[trttitrenhrl Ic,clurulcr rtti Inc, i.1y41.miv �3$O Wki Slre+l C.WYONVO iatis. ONO 4422.3 •Ytn_� sr._nf rn Pace 1 of t Page 1 of 1 Summit Environmental Technologies, Inc. mom 1 -1 3310 Win St. ENIVAON,VE147A_TECH NCILO IF$,IN Cuyahoga Falls, Ohio44223 Sample Log -In Check List du; TEL: (330) 253-8211 FAX. (330) 253-4489 Website: htq!:11www.settek.com Client Name: CAS-NC-28379 Work Order Number: 18081887 RcptNo: 1 Logged by: Jacqueline Rasile Completed By: Jacqueline Rasile Reviewed By: Brian J. Fackelman Chain of Custod 1. Is Chain of Custody complete? 2. How was the sample delivered? Loq In 3. Coolers are present? 8/3112018 7:55:00 PM 8/31/2018 10:01:54 PM 9/5/2018 10:52:47 AM 4. Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? No. Seal Date: 5. Was an attempt made to cool the samples? 6. Were all samples received at a temperature of >0° C to 6.0°C 7, Sample(s) in proper container(s)? 8. Sufficient sample volume for indicated test(s)? 9. Are samples (except VOA and ONG) properly preserved? 10. Was preservative added to bottles? 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? 12. Were any sample containers received broken? 13. Does paperwork match bottle labels? (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? 15. Is it clear what analyses were requested? 16. Were all holding times able to be met? (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes W] Summit Yes ❑�/ Yes d❑ Yes ❑ Signed By: Yes d❑ Yes ❑d Yes d❑ Yes d❑ Yes Yes ❑ Yes ❑ Yes ❑ Yes ❑d �.ik•Fk.7i, 1�1.ra •6',�r, No ❑ Not Present ❑ No ❑ NA ❑ No ❑ No ❑ Not Present ❑d No ❑ NA ❑ No ❑ NA ❑ No ❑ No ❑ No ❑ No NA ❑ No ❑ No VOA Vials ❑� No ❑� No ❑ Yes ❑d No ❑ Yes ❑ No ❑d Yes ❑�/ No ❑ Yes ❑ No ❑ NA W Person Notified: Date By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 18. Additional remarks: Cllient may need contacted on what TCLP is needed, logged full per past. Cooler Information Cooler No I Temp °C Condition I Seal Intact 1 Seal No Seal Date Signed B 1 13.5 Goodl Not Present' Page 28 of 28 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Cascades Tissue Group -North Carolina, a division of WQ0009477 Cascades Holding US Inc. WQ Permit Number: WWTP Name: NPDES Number: `Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alterative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray❑ Gamma Ray ❑ Pasteurization ❑ - . ........ ' Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Ai Drying❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ .I - ..... ................................_........_......................... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g l um ber o Excee- dences Frequency of Analysis le SampTech- Type na ytica Minimuir Geo. Mean Maxim u Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN N/A N/A CFU N/A N/A 1000 mpn per gram of total solid (dry weight) N/A N/A ,Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) N/A/ N/A Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) or "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector Nattraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Karen V. Bellamy Environmental Manager Duke Goodwin Project Manager Preps r Name /and! Tit e (type or print) Land Ter �n and Title (if applicable)(type or p in-71 �w (/ -Z/SM Signature of Preparer Date Signature of`i.and Applier (if applicable) ate *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) (W Cascades Date: Feb 12, 2019 Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc. 805 Midway Road, Post Office Box 578 Rockingham, NC 28380 USA Phone: (910) 895-4033 Fax: (910) 895-9887 From: Karen Bellamy Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Po Box 578 805 Midway Rd. Rockingham, NC 28380 Phone 1-910-895-4033-Ext 2280 Fax 1-910-895-9887 Email: Karen _Bellam @Cascades.com Permit: WQ0009477 Subject: Fecal Testing Cascades Material is a lime material, so we don't perform vector reduction. Should your office have any question please contact me at the above numbers or email. Karen V. Bellamy Environmental Manager Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.