HomeMy WebLinkAboutWQ0009477_Residual Annual Report 2018_20190222Cascades Tissue Group — North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA
cascades
Phone: (910) 895-4033 Fax: (910) 895-9887
www.cascades.com ' Info@cascades.com
Date: Feb 12 ,2019
To: State of North Carolina Department of Environment and Natural Resources
Division of Water Quality
Aquifer Protection Section
Land Application Unit InolnQ
512 N SalisburySt. rncn
Raleigh, North arolina 27604 RECifJV��'I N
1-919-807-6300 M 2 1 2010
Non-Dl5ct1 [9 From: Karen Bellamy-ORC and Preparer of 2018 Annual Report permittinguhit
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
805 Midway Road
Rockingham, NC 28379
1-910-895-4033 EXT 2280
1-910-895-1877 Fax
Karen Bellamv&Cascades.com
Permit # WQ0009477
Subject: Land Application Annual Report Cover Letter
Forms Included:
Cover Letter
Annual Land Application Certification Form DENR Form ACF
Letters from E. D. Black on Application
Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, If K Soil,
Dry Tons, Dry tons per Acre, Long and Latitudes
DENR Form DMSDF and Additional Supplemental
DENR Form RSSF
DENR Form RSSF-B
Lab Results
TCLP, Ignitability, Reactivity, & Corrosivity
DENR Form PVRF 503
Letter on Vector Reduction
Page 1 of 2
% Solids, Acres, Wet Tons,
Subject: Land Application Annual Report Cover Letter.
Cascades have 1 ORC and 1 Backup with Additional backup soon at the present time. Karen Bellamy ORC
and David Sheppard (just pasted test Dec still need to send form in on David) and Corey Wyand as
Backup.
Field Inspections where conducted, equipment calibration, PM work on equipment and backup ORC
performed required inspections for the year.
Corey Wyand and Karen Bellamy attended Rural Water Association Training in 2018 for our Continuing
Education Contact Hours.
Dr. Elwood Black continues to work closely with our land application Program.
Advanced Residuals had No incidents in 2018.
2018 has proven to be a challenging year with Hurricane Florence and all the additional rain.
We were able to stay in compliance of the 60 day spread time for 2018, but had to ask for an extension in
Jan 2019. Worst weather and field conditions , since I started in 1994. We have made progress in Jan and
hoping the weather will hold out
%, dvanced Residuals has worked hard to have a good program. Cascades and Advanced Residuals has
worked hard to make sure we have a good program that is Environmentally Friendly and also benefits the
farmers. We have gotten a lot of positive feedback from farmers. Duke Goodwin is the Project Manager for
Advanced Residuals project at Cascades. Mr. Goodwin has been a farmer for several years and also has
worked at the City of Rockingham WWTP, so he is very familiar with regulations. Duke Goodwin also
received his certification for Land Application in 2016 . Mr. Goodwin also received his continuing Ed hours
for 2018.
Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also
been removed from our permit, since levels have been extremely low for over 10 years.
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0009477
County:
Richmond
Year: 2018
Facility Name (as shown on permit): Cascades Tissue Group -North Carolina, a division of Cascades Holding US
Inc.
Land Application Operator: Karen V. Bellamy Phone: 910-895-4033 Ext 74280
Lan application of residuals as allowed by the permit occurred during the past calendar year?
Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites: 25824.13556
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land applica ' n permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. W11yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in
the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Karen V. Bellamy Environmental Manager
Permittee Nan}e and Title (type or print)
Signature
Duke C;oe
Date
Signature of Preparer* Date
of Land Applier
(if different from Permittee) (if different from Pennittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
E. D. Black
Land Treatment • By -Product Ulikzafion • Soil Remediation • Wetlands • Bioliltralion
February 5, 2019
Cascades Tissue Group
POB 578
Rockingham, NC 28380
Attention: Karen Bellamy - Technical Director
Dear Ms Bellamy:
From January 1, 2018 thru December 31, 2018, FiberClay was distributed only to
agricultural land. No farm field received FiberClay in a continuous year-to-year
application as defined by the North Carolina Department of Environmental Quality
respective to permit WQ0009477.
These statements are based on information reported by Advanced Residuals
Management.
Sincerely
F
Elwood Black, Ph.D. - Soils
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Month
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69
3518.5dQN 7945.171W
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35 4.271 N 79 49, 5X
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3, YF,NS,
YP4,YD-
Y1/201B
Grass
16
44.60%
448
35 24.877N 78 49.210E
2or0 rrtevmmseea Rd. T .NC 77511
K,NW,YF,
T/f/2018m
RC
YS NP
44.60%
29
a
35 25.734H 79 5R 048 W
Z010 04--- Rd.7 .Nc V571
K, YbK
3,NF,NS,
2/52018
Gross
NP D-3
44.60%
95
a
15 ]3.79 39.854 W
959N
7530 &.an Rd y NC 77341
K,NW,NF
]lr2�3wa
-
_
]S 27.538N T9 4tl.563w
1904M.ids. Or. me KC 2 T U I
—
35 26, 2B6ty 77,u.511 w _
740 Hillside DSe -rove NC 27341
Grass
,NS,NP,D-
6
44.60%
62
a
2112MIS
Grass
K, YW, YS,
NF, YP
44.60%
94
a
K,YW,NF,
YD-
N9M
2/121018 -
it18+1i 0,1•
JS Z6.596N 79 Aa.943W
Grass
3.NP.NS
44.60%
61
a
_
T8R Hillside r Sea rove NC 27341
— -
K,NW,NF
-
3/8/2018
—
Gross
NS,YP,Y
D
44.60%
_
34
a
15 2r.2Pry 79 39.076w
1964 Cedar Hili Rd. robins NC 27125
K,YW,NF,
YS,YP,D-
&12/2078
Grass
2
44.60%
65
121662"
1.
a
SS2H]i0 7915.752YV
19[I HIII�We. Dr. Sea rove. NC 27341
NOWK,NW,NF
Ep,
NS,NP,D
21122018
Grass
6
44.60%
20
a
35 30 U-P; 79 45949W
—
190 HiIIaide. Or. Sea rove. NC 27341
KYW-
3,NF,NS,
7/fY1015
35 27 951 N 79 44-739 W
-
051 BOC 1T85!r6H.(1�-B�Srffke�P" Gross
YP.D-3--
-
-
190 NkOsldu-13, Sea rove NC 27341
KYW,NF, '
NS, YP,N
0f9
35 27.725N 79 37.9JBW
- Grass
D 44.60%
12 _
1984 Cedar HIII Rd robins NC 27325
K,YW-
_._ _ _
3/1I20f8
3,NF,NS,
35
3525Jim :
Grass
tEiGress
YP-7 O-4
44.60%
105
. Robbins9.40
. Jim Rd. Robbins. NC 27325
NKNW,N
F,YS,NP,
3/7/201B
D
04.60%
65
75 16-663N 74 48.]85W
2365 Jlm kd Robbins NC 27325
KYWNF,
NS,NP,D-
3/7/20fB
Grass
4
44.60%
89
a
75 78-549N 79 46 17] W
2365 An Rd ReWilns NC 27325
KNW,NF
7H/7018
Gross
O
44.60%
13
�
35 22.466N 79 45750 W
ag
2010 Ok�mae Rd. Twv. Nc 27371
-
KYIN, YF
2H40111 73r
NS,YP,Y
35 25.580N 79 50.287W
2010 06—emee 12d- 7r NC 27371
Grass
D-2
44.60%
KNW,NF
2H/2018
,YP-
35 25.857N 79 49.659W
Grass
2 NS ND
44.60%
34
2010 nFeewemee vd Fro NC 27371
KNWNF
7H2r20lB
Grass
NSNPN
D
44.60%
20
-
a757fi614N
734d.820W
190H'i.id.Or. S1ar.NC 27341KYW,NF,
49!77
NS,YP,Y
V-33rN 74 42 408 W
Grass
D-3
44.60%
3f-
- �7l7f a3S
-
-
490 H!Il.Ide Of S1ar,NC 77341
KYW
-
5H5/201B
2,NF,NS,
35 32.944r1 79 39.BBBW j
Gross
P-2YD-3
44.60%. 81 '70.b70617
--
Tl
-a
PO Box 469 Se rave NC 27341
--
-
- i
KNW,NF
- --
,NS,YP,Y
SH8/2018
Gross
D-3
44.60%
37
353] i96N T442_24MN
a
127B8 R4inlr Lawrence Rd- Rohhln.-NC 27341
M1f1fh
5015. 78WO
2237.03788
EW—d _ 2018 i I So i i Tans M n,
4hnM Tans Fspnry Field Raln Acre. Ilse
June
Good
K,YW,NF,
fOn64017
Grass
NS.YP.d
44.50%
56
24 35 .578N 79 42.746 W
4803 S les Rd Slay HC37351
KNW,YF,
Nrr20r8
RC
YS.NP
44.50%
117
..
35 25134N 79 5004£ W
2010 OP9ewa—Rd.TroNC :15 r!
YKNW,N
P,ND,NS,
2N/20f8
RC
NF
44.50%It
f3
a
a5 7S a77N y9 J9.4T8W
2010 Okxer.emro Rd. 7 NC 22,371
K,YW-
3,NF,YS,
2/5/2018
Grass
NP D-3
44.50%
95
ag
35 3z.959N 79 3A.864 W
_
I., Erecr Rd Sea re�y,NC p73►1
K,YW-
2,NF,NS,
211212018
-
Grass
YP-2
44.50%
228
a
35 26. 9500N 79 39-OM W
190 rfllaida Dr. NC 27141
KYW,NS
,NF,NP,D-
blZr2m8
Grass
3
44.50%
94
a
35 25. MN 17,44.61W
190 "Insrdr. DI. Nq 27341
KYW-
2,YP-
7,YD-
2Y2612B18
Grass
1 NSYF
1 44.50%
B35
a
1530A89N7921.7B1W
558 So Ah Carbm bM Rd Sadord NC 27830
K,YW,NF,
3/6/2018
Grass
NS YP
44.50%
12
33 2722SN 79 37.938'W
104 Cedar HWI Rd robins YC 27325
KYWNF,
--
- -
NS,NP,D-
3.0e'J018
-
Grasa
3
44.50%
25 -
-
00
35 27.MdAY 79 38.133 W
1984 Cedar Hlll Ro robins NC 2:375
K,YP-
2,NW,NF,
3!7/2018
Grass
YS"
44.50%
221
a
3526.5714 79379/5W
2365 Jim Rd. Robbins, NC 27325
K,NW,NF
2/1/2018
Grass
NS NP
44.50%
9
a
3s 26.589N 79 60 2RTW
2C10 04eawamm Rd. rro . NC 27371
KNW,NP
ND,NS,N
2R�DT6
Grass
F
44.50%
11
a
35 26.049N 78 49.eSTY1
2v10
�TIPI�21111
KYW,NF,
Grass
YP,NS,Y
D
44.50%
34
N1l28T8.
3526A52 7941659W
2070 Dk� did. Tra . NC 27171
K,YW,NF,
YS,YP,Y
211L207B
Grass
D
44.50%
31
35 Y1331N 794L408W
190 HlElslde Or, Saw.NC 27347
a
a
a
Crwood 2"0 i7ores 7 ¢
,Ila Tana Fonyw Rain 7 K Arms Use
Juk Good
KYW-
5,NF,NS,
f0141Z017
Grass
YF-3D-6
39.40%
127
a
36 14,307N f0 2P480W
73805 81 tJah Rd. Qahfb—. NC 28r29 —
—
TONROIY
3514.231N 80 22.899 W
Grass
KYW,NF,
YS YP
39.40%
43
1
a
12805 nr L1rk Rd DA&bam NC 28129
K YW-
—
2,YF,NS,
TO/4/30Y7 _ _-
1514 f22N H023977W
47aY16 e& Z �
Grass
YP D4
39.40%
96 - -
--
a
128D5 ildl Rd. OWA NC 28129
KNW,YP-
4,YS,YD-
}014R017 --- —
Grass
5NF
39.40%
192
a
35 72.577N 80 24-128 W
w
1
T2805 iJck RY OaYsbora NC 28129
NK,NW,N
}r21"lOTB
Grass
FNSNP
39.40%
35
a
3d 329I2N 79 3A.461 W
iP030 E 1 Rd Se NL '1833H
KYKt
2,YP-
7,YD-
2�36rMfe
Grass
12,NSYF
39.40%
835
a
35 30.389N 79 21.701 W
556 South Carbonton Rd- Sanford,NC 27330
K,NW,YF,
Grass
YS,YP-
2 D4
39.40%
60
a
35 31.883N 79 21 46aW
"-;56 Souln_ Carbanton Rd. Sanford,NC 27330
K,NW, YF,
YS,YP-
2/26/2018
Grass
5.D-7
39,40%
328
' SSB South �arbanron 11d- Sanlerd,NC 27330
K,NW,NF
..
,YS-2,YP-
31}3lY078 -
Grass
4 D-6
39.40%
52
-
a`
36 26.335y 79 35.73yW
596 Mamas Rd. ROW" NC 27325
YK,YW-
2,NS,YF,
3/20/2018
Grass
YP
39.40%
56
] 5 27.377N 79 4R MW
947 Dan Rd Rabb—, NC,2732;
YK,NS,N
F,NW,NP,
3/20Y2o78
Grass
D
39.40%
28
f+..l
a .
]527.793N 7830.475W
947 Dan Rd Robbtna. NC 27325
K, YW, YP,
YS,YD,N
8/15/2078
35 34,444N 79 38.311 ri
Grass
F
39.40%
55
a
5908 Asb18 Lh. Se ove NC 27341
K YW,NP
6/15I2018
Grass
NSD.NF
39.40%
25
a
35 34.119rd 79 38.001 ri
5906 yalR Ln. 5 ova NC 27341
K YW,NF,
8/15/2078
Grass
YSNP
39.40%E26
]5 ] 7.548 79 37.711 ri
--
51M A&Wfi Ln- rays NC 27M1
—
—
KYW, YP,
2R[:/2018
Grass
NS.NF
39.40%
a
35 30.7d8N 79 23 5W
556 Soul Lafbo.Wn Rd- Saalotd NC 27338
77
39.40%
ad
39.40%
39.40%
a
up i 2018 1 1 Soll I T—a To
Lfvnfi Fleld Rain X 8c+e1 wer-ja Use
A yq Good
K,YW,NF,
lO/4l2017
Grass
YSYP
44.60%
43 a
x614.x31N 80 22899W
12"!; HJ Lick Rd. Dak Strom NC 18129
K,YW-
3W412tl17
-- —
Grass
2,YF,NS,
YP.D-4
1 44.60%
96 a
z5 r4.42xN ea 22.9x7w
12806 ft Lick Rd-Qakmerc NC 26 29
K,NW.NF
TOpY20i7
Grass
,NSNP
44.60%
e
35 14./ 1TX By T4.3sOW
IMS ft UCk ft. Oaksbwo MC 28 UP
K,NW,YP-
4,YS,YD-
1 017
Grass
5 NF
44.60%
132
35 12.577N 80 24. 198W
f2888 Slo Lkk Rd. 01*100tb NC 28129
NKNW,N
F,NS,NP,
TNrd T
RC
D
44.60%
6020
34 ]v.993M 79 t 2.885W
1927 Cerald Rd. Rewrand NC
NK, YW,N
112912018
RC
F. NS NP
44.60%
25 ag
34 27 491N 7911.727W
5338 Hwy 130 East Rowland NC 28393
NKYW,N
112912018 -
RC
F NS NP
44.60%
15
34 28.54 TN 7912.394 W
5211HY.Y 1 j0 Ea11 Rriwland.NC 20.193
NK,NW,N
F,NS,NP,
1129/P0f8
RC
D-2
44.60%
40 a
04 32.389N 7913.273W
5338 N 13o Fa Rowland NC 28393
NKNF,N
1R911W18 -
RC
WNSNP
44.60%
25 a
34 33.236N 79 13 432 w
5338 130=EZ
NK,NW,N
F,NS,N,Y
1128/2016
RC
DP
44.80%
9 a
3{ 307N 79573f
f30NK,NW,N
FNSNP,RC
YD-3
44.60%
i 51�6 H wy 1] Eax r Rolland. NC 28393
NK,NW,Y
-
F,NS,NP,
_
xlxR7018
_
RC
D-5
44.60%
59 a
9
-3439,0S�N 791x.8POW
75 Rd. Pi hei* NC 2072
NK,YW-
1,YFNS,
2/29/2016
29 a
RC
NP D-4
44.60%
3437,997N I9 P}_pBrW
75 0—Rd Pe b-hv, NC 383?2
—
NK,YW Y
F,NS,NP,
2/29/T016 _
RC
D-3
44.60%
76 -- : TMau
34 ]7 395N 79 iv.99aw
75 Gale Rd. Pemhorka NC 28372
—
NKNW,Y
FNS, P,
T128r2016
RC
2
44.60%
63
sT.7464 - a il
34 37.0*4N 79 U8.094 W
75 Gene Rd. Penmorke_ NC 28372
KNW,NF
NS,NP,D-
7/29/2016
RC
B
44.60%
75
a
34 40.714N 79 06.154W
75 Cene Rd. Pemborke NC 28372
NK,YW,N
F,NS,P,D-
2/29/2016
RC
3
44.60%
94
a
3s 45. TlBN 79 06,4�! W
75 G9 Rd NC 28372
NKNW,N
F,NS,NP,
2/29/2018
RC
D-2
44.60%
46 -
a�
34 42. g4 } N 79 00.778 W
75 Gene Rd 7�adwr NC 2837T
�
Nk,NW,N
F,NS,NP,
W29/2016
R7
YD-2
44.60%
30
a
24 4 f,73ar17906. 143W
75 Gene Rd Pemborkv NC 7a373
NK,YW,N
F,NS,NP,
2/29/2016
RC
D-3
44.60%
64
a
34 43.772N 70 06.49DW
TB Genv Rd. PM16v1 20372
NKNW,N
FNSNP,
f1ffi10
RC
D5
44.60%
36
a
34 38.029N 79 11.812W
75 4mla Rd- FambarimmCM72
NK YW,Y
7/3f 8
RC
FNS,NP,
D-2
44.80%
61aq
3439.M14N 7914.f03W
545 Burlei h Rd. NC 253? 7
NKNW,Y
F,NS,NP,
713112018
RC
D-2
44.60%
17
a
3410.007N lJ.853W
5 5: A RQ P.nebroke NC 28372
NK, YW,Y
7Rl1207a
F,NS,YP,
3438.531N79 s3.855W
RC
D-2
44.60%
57
54e P.urfel h Rd Pemhroke.NC 28372
NKNW,Y
7131R078 -CUAWMF —IV-
_
RC
F YS NP
44.60%
9
134,37 299N 7g 1T S44W
545 Burkmh Rd. Pembroke NC 28372
7/21ROT8
RC
NK,NW,Y
FYS NP
44.60%
10
34 ]7.99bN 7¢Y].f79W
545 Burlei N Rd. Pembroke NC 28372
NKNW,Y
FNSNP,
7l41f10T8
RC
D
44.6051
11
34 41.526N 79 15.970 W
545 Burlwah Rd. Prmbrake NC 20372
NK,NW,Y
Jl31l26T8
Grass
FNSNP
44.60%
8
34 38. S07N 7014.064 W
545 Durlel n Rd. F mbr ke NC 28372
NK,NW,N
!0/f8/2017
RC
F,NS,NP
44.60%
30
a
34 28.386N 79 ! 1.047W
1927 Gordd Rd. Roy ww.NC
NKNW,N
F,NS,YP,
10H8/2017
RC
D
44.60%
26
a
34 wykm 7a 11. 151W
1927 Gma d Rd Ro
NK,NW,N
10M8/2017
RC
FNSNP
44.60%
2T
3e 29.045N af1.S95W
192r Gerald Rd. RoMgrld NC
NK,YW,N
F,NS,YP,
10H8/2017
Grass
D-2
44.6u% 1
65
a
34 30,3"N 79 11.511 W
192T Gvra�d Rd- Rowland NC
NKNW,N
_
_
F,NS, YP,
10M8/2017 — =
34 31.128N 79 12.195 W
a
Grass
YD4
44.60%
83
a
1927 Geraid Rd. Rowland NC
I
NK,NW,N
10H8/2017 271B9Rn?+Sieger
pFe,-,d;rre I P5a3
34 :.:.321N 79 12.694W
19:7 Rowland NC
Gross
F,NS,NP,
YS
44.60%
85
_ --
NK, YW-
2,NF,NS,
10/18/2017
*e,
Gross
YP YD-2
44.60%
68
}4 30.757N 79 13.856W
f92 7 GmId Rd, Rowland NC
NK, YW,Y
_
F,NS,YP,
H!J/101B
RC
D-2
44.60%
74 Y9.074{4 *$1d6437�1
a
34 25 576i�
L640 Mai WtW fdC Y8382
.. —
NK,NW,N
8/3/2018
RC
F,NS NP
44.00%
10
a
34 iR2991J 79 T"930Y1
2648 Marlette NC 29362
'
NK,NW,N
FNS,NP,
RC
YD
44.80%
41
a
34 29209N 79 11.536w
3877E ham Rd Folr nt. NC 28340
NK,NW,N
FN$,YP,
8M7/2018
RC
YD
44.80%
28
a
3420MON7912.088W
3377 E R ham Rd.'eirrn; 0nr NC
ig
NK, YW,N
F,NS,NP,
8/22/2018
-
RC
YD
44.60%
52
34 44.861 N 79 9, 513W
1312 J 1. RP Manton NC 23384
NK,YW,N
P,NS,YD,
dY18ROT8
Grass
YF
44.60%
28
34 40.617N 70 4. W
t 374 "sr * Fwtv Rd =NC 28364
NK,NW,Y
P, YD, YS,
8l28lJOTd -
Grass
YF
44.60%
12 {1i7000
y{ jy,yY(W 79 !4"387W
--
406 Trmbar ❑ak Rd. wovAand NC
-
NK,YW,N
P,YD,NS,
8l2IMS
>♦ 39.0:0N 7H 14.273W
RC
YF
44.60%
12
1
a
—
- —
—
-
St
170 E4rcn Rd. Pamblok*NC 28372
NK,YWN
P,YD,NS,
8f79r1'!Y!d
RC
YF
44.60%
32
T. 1694
_
a
3439.970N 79 ti]27]W
170 Elmce Rd Pkmhroka NC 28372
NK, YW,Y
P-4,YD-
8/29/2018
RC
8 NS YF
44.60%
19
-it
34 38.955N 79 11.839W
170 Etarce Rd. 139mbmke,NC 28372
NK,YW,P
,Y0.
8/29/2018
RC
2 NS YF
44.60%
28
a
34 37.906N 79 10.388W
M7 Cam= Rd. Pembroke NC 28372
NK,YW,N
P,NS,NF,
8l2A 101d
RC
YD
44.60%
1{
a
3{41.0 f2N 79 f3207W
170 04" Rd. Pomtlfekv NC 28372
NK,NW,N
P,NS,YD-
7lFrJ01a
Gross 8 RC
1 YF
44.60%
67
a
34 {O.T71N 79 T4,{f6aW
304 MC HWY 7101Aulcn.NC 28384
a
a
a
—
�
a
Ebmgo 1 2019 7vns oRa
dr Tons I Fr Flefd Rain K A —
Sept I Good
K,NW,NP
,YD,NS,N
1/5/2018
RC
F
46.10%
23 a
358.10PlaesanN8018.SO5W
3407 r Hill Church Rd. Marshwflm NC 24702
K,NW,NP
,ND,NS,N
1fL20le
RC
F
46.f0%
18
asr.9a3N aB fe.7e9w
5407 Prwsanr HM Church Rd. +farshv8/a NC p6102
KYW,NP
,YD-
T/Y3Ol8
RC
3,NS,NF
46.10%
33 e
$407 Pleasant f liN Chuleh lid AfarehVlNe NC T8l87
KNW,NF
,NS,NP,Y
1/5/2018
RC
D-3
46.10%
36 a
15 9.321N 80 14.721W
5407 P/easanr N!0 Church Rd. Alannvr8e NC p8r07
NKNW,N
129/2018 -
RC
F NS YP
46.10%
24 a
34 2&MWi 79 f0.051 W
r 583s fla 130 Farr R*$w&,?GCNC 28393
NK YW,N
L
F,NS,NP,
112912018 —0
RC
YD4
46.101
170
a
34 iY. P37N 79 9.676 W
5.338 H 130 Eaaf Rowland NC 28393
KYW-
2,YF,NS,
3/20/2018
Grass
YP
46.10%
56 a
75 p7.Ji7N 79 w.f97W
047 Dun Rd. Robbom.NC
NKYW-
2,NFNS
10/18/2017 -_
Grass
YP YD-2
46.10%
6s all
34 3f1.957A 79 13 058W
i9T7 Garafd Rd. Rowland N
NK YW,N
F,NS,NP,
0PV29/18
RC
YD-f0
46.10%
114 a
34 40.083N 79 7 649w
936 Gene', Rd Perna -A. NC 28372
-
NKNW,N
g•77,7018
8 air
3r 10. r J rN Is r 2 0rsw
Grass
FNS.NP
46.1036
3577 E R.o-J, am F.7—t. NC 28340
NKNW,N
FINS,NP,
8/17/2018
859M
RC
YD-3
46.10%
37
a
34 30344N 79 1 R 123 W
3577 E Ra nhem R0 Fahmownl 293"
KYW,YD-
S,NS,NF,
111912017
RC
NP
1 46.10%
73 a
]S l7.079N 6019.237w _
1434A MELnkn Rd. oaw M=o 11 2B129
NK,YW,N
P,YD-
e/29/201B
RC
2,NSYF
46.10%
19 a
34 37.872N 7912.582P7
170 £larce RO Pembroke NC 28372
NKYW,N
P,YD,NS,
812912018
3440.a03►r 7911.074Y4
RC
NF
46.10%
8 a
170 Elalce Re Pe bfbMa NC 28372
Nk,NW,N
P,NS,YD-
plaV7096
34 40. ! 7!N 7414.658 W
Grass B RC
2, YF
46.10%
67 a
3" NC 1iW1710 Azar lan.NG 2e3e4
NK YW,IV
P, D-3,
9/5/20f8
RC
NS_ NF
46.10%
39 ag
453 Arthur Rd, Rat Sprinas. NC 28377
NK, YW,N
P,YD,NS,
2P19/lO16
RC
NF
46.10%
49
a
3J 63.22JN 79 tlA905W
T5 Genv Rd- Pa bmke NL' 2a572
NK,YW-
2,NP,YD-
212912016
RC
ANS,NF
46.10%
83
a
3J 54.683N 79 f0-35Ew
75 Ornp Rd. P—D-ht,NC 28372
K,NW,NP
,YD-
9rr170f7
RC
3 YS NF
46.10%
34
a
35 9-308N 80 Y8,84PW
6408 Sr. Fm-fhP Rd- M—hwlh NO 78106
K,YW,NP
,YD,NS,N
9/2/2017
RC
F
46.10%
10
75 8-J93N 80 I9, r➢6 W
94w Sl, rhmplhy Rd, M[rY71Wlh NC 28106
K,NW,YP
,YD-
OfLw17
RC
3 MS. YF
46.10%
92
a
35 7.3B9N 80 19.62T W
a4" St TrMwh Rd. Marahwple NO 2a106
NKYW,N
P,YD-
9YV2017
RC
NS NF
46.10%
18
a
35 8 80ON 8.8 20.635W
8408 St TimothyRd. MarshvilM NC 28106
KNW,YP
-
YD-
9IV2017 -
RC
2 NS NF
46.10%
41 -
-
a
35 9.069N 60 17 483 W
8408 Sl Tf'mmrr • Rd. MarzF.v(Ilr NC 26 r06
K, YW,NP
,YD-
QM2017 1-ZT!
RC
3 NS NF
48.10%
46
a
l6 i f.76N 88 iy,370W
94M Sr. Trmwi8 Rd. 66rrahWo. NC 28Tp6
KNW,NP
YD,NS,N
➢1212017 4-4,
35 8 744N 80 r 7 475 W
RC
F
46.10%
41
ag
840E St To— Rd- Marshville, NO 28108
K,NW,NP
YD-
9/2/2017 ]Q3
RC
2.NS,NF
46.10%
25
_
35 8.299N IIO 15.231W
8408 St Tlmol!' Rd NC 29106
' -
-
KYW,YP,
9/2/2017 =
RC
YD-
7,NS,NF
a
75 S. 668N 8D 14_IfOw
46,10%
44
`
Sao St T., e,M Rd. Ma"hvi0e NO 73Y06
KYW,NP
YD,NS N
B/2/2017
RC
F
46.10%
30
1J-1rn1
-
75 [ 763N 8a 13 5S1 W
9408.Sr r; 90 • Kd Ma"Wr8a NC 281
K YW, YP,
YD-
VD2017
RC
2 NS NF
46.10%
15
354, 62dN 80 13 SY[yY
8408 Sf. 7fmof7i Rd. Marshville. NC 38106
K YW,YP,
YD,NS,N
9/2/2017
RC
F
46.10%
31
a5 17.39BN 80 : !.305 W
5408 S1 . omoth Rd. Marshville, NC 28106
-
K,NW,YP-
.
2,YD,NS,
9.O12617
RC
NF
46.10%
94
3912.672N 80 21.318W
8408 St. Timoth Rd. Marshville NO 28106
K, YW,NP
- 1
,YD,NS,N
9/2/2017
RC
F
46.10%
13
3612072N 8021.M6 W
_
"as Sd- Tlmoth Rd Afarsrfvill'. NC :8106
K W,NF,
9 1202017
RC
NS NP D
46.10%
B
a
35 17.35 80 20.920w
—thy Rd. MomhVille NC 28106
£laved 20ra -i i Tons
A1onM Tam I FwNW Field Raln runs cnm D Use
Oct Good
YK,YW-
2,NF,NS,
TRf20Ta
RC
NP D-2
43.60%
44
a
35 18.20-M 80 18.256 W
2➢7la Or A NC7 D01
K,NW,NP
,YD,NS,N
1/7J20S8
RC
F
43.6,
23
a
358.707N80 T� HW
$407 P1anaer AV➢Ch1 ft Rd. Manhri NC 28103
YK,YW-
$NP,YD-
lJ.y➢01H
RC
4 VS. YF
43.60%
45
aff
35 9.531N 80 14.145W
W07 P1ss.1'sn! ll07 Ch—h Rd. M—hW5. NC 2MV03
NK,YW,N
F,NS,NP,
fOMB/2017
RC
YD-2
43.60%
58aff
34 31.636N 79 12.281W
1021 Gera/d Rd. RQ1rWmd.NC
NK,NW,Y
F,NS,YP,
172arF91➢
RC
D4
43.60%
155
OIL
34 34.206N 79 5.151 W
WM N !30 fall Rowland NC MM
NK,
NW,NF,N
10M7R0l7
RC
S.NPYD
43.60%
43
a
34 49.6-17N 79 6.990 W
6274 0ld Lowwy Rd Shannon NC 28386
NK,YW,N
10/17/2017 3569
RC
FYS.NP
43.60% 1 48
a
34 49.215N 79
5274 OW cowy Rd. Sn4rr+ron NC 28386
_
1 a1l iRD17
RC
43.60%
43., 43
]f 49.6l5N i9 9. TB2 W
5274 DM I.wwv Rd Shmenumm NC 24396
NK,NF,Y
S,NS,NP,
10/17/2017
RC
YD-2
43.60%. 49
N¢772r
344➢.8 m7aa,l2fW
H274 Rd NC 2➢3➢6
NK,YW„
-
NFNS,N
10M7/2017 3572
RC
P
43.60%
45
a
34 48.949N 79 9.345W
527/ Gfd La Rd. Shannon NC 2838a
NK,YW,N
a!L➢70l8 3617
RC
FNSNP
43.60%
29
a
34 /J.941 N 79 5.➢SOW
110 h7sMcs Rd ftrubmle NC 20372
NK,YW,N
8/29/1018 3620
RC
FNSNP
43.60%
22
a
7J J7.➢97N 79 8.QP7 W
f 70 FLTe Rd Pembroke NC 20772
K,NW,NP
9/22017
8N 25 10.5/80 a3 17.9W
RC
NS,NF
43.60%
31
a
➢/08 St rr M Rd. Mmvh,Olk NC 28 NO
YK, YW,Y
P,YD-
9/22017 f-
RC
2 NS.NF
43.60%
17
a
35 5.9r 7N 30 13.899W
0408 St numm Ra ATarshville NC 2a109
K,NW,NP
,YD,YS,Y
9�7J20T7
RC
F
43.60%
16
a
35 /,53SN 80 7/, 663W
9408 S1. 7r-w Rd. Afarsf wAle NC 2610H
YK,YW,N
P,YD-
9/2/20f7
RC
3 NS NF
43.60%
20
a
35 77.70➢NJV l9,OM8W
a40 81, fkr ll Rd. MJrshrl8s MOO
vx,nu
2,YP,NS,
9/2/2017
RC
NF
43.60%
13
13512.234N
80 20.638 W
8408 St. TImothy Rd. Marshville, NC 28108
YK,YW,N
P,YD-
RC
2 YS YF
43.60%
21 a
3S 1 .153N f0 22.301W
6408 Sr 'nm rhv Rd Ya.hwn. NC 28100
YK,NW,N
P,YD-
RC
3,NS,NF
43.60%
24 a
a59. son 8D IY-go9w
mag $t Im-aft no M—hvl8e NC 281 OH
YK,NW,N
P, YD.
RC
3NS,NF
43.60%
61 a
35 9366N 90 ! 7. T09W
H408 Rt. Tx o Ad. A41f4T1wraA NC MP6
YK,NW,N
P,YD-
9/2/2017
RC
3 NS NF
43.60%
]2
35 13.466N 90 24.379W
0408 St
IN 6h.N
.--_..Ti.m....
YK,YW-
2,NP,YD,
9/2/2017
-
RC
YS NF
43.60%
28 a
35 f3."2N ao 3L.Iww
8408 St T'?MWhV Rd. NC �51P6
YK,NW,Y
P,YD-
10/2/2018
RC
2,NS,NF
43.60%
50 a
551.267R 80 }3.914 W
27}7R 2}eP¢�rlda�dNC281]`-
YK,YW iV
P, YD, YS,
IfA'2120 fil 13
—
3679
RC
NF
43.60%
10 a
- — - --
YK,NW,Y
1
P YD-
10/2/2018
.:
RC
2 NS NF
43.60%
13 a
95 7.DD7N 80 t3.378W
ESfi PiB flxMrad NC ae 137
YK, YW,N
P,YD,NS,
10/112018 a:lTJIIO
RC
NF
43.60%
14 a
as � fsrx 80 rs.163w
E3 17 Hwy;? Y9 PeachlarM NG a8l33
YK, YW,N
P, YD, YS,
RC
IF
43.60%
18 a
36 2,O11N $a 15.746W
2317 a1a Py4NVNld NC aa133
YK, YW,N
P,
YD,NS,N
101212018 - -
RC
F
43.60%
11
35 1-8B9N 80 }S69DW
23l7 R 2}8 Peachla A9C 28133
YK, YW,Y
P, YD, YS,
70R120ia
3690
RC
NF
43.60%
10 _73 !TAl156 au
i75 i ,r60N ti0 }3.iT2W
10263 WlriD"Rd kwwccd.NC 26t28
---
YK,YW,Y
P,YD,NS,
}07/2Ma 3691
RC
NF
j 43.60'/.
23 a
351.37 80 12. T66 W
'10967 tA811ow Rd. Nonvgod NC 7812a
YK, YW,N
P, YD, YS,
1012l101d 3693
RC
NF
43.60%
129 a
352.874NMAS3t W
10967 Wlllme Ad- Norwood NC a8 t25
K,YW,NP
,YD-
11/9/2017
RC
3 NS NF
43.60%
59
1514-% N 8D 18.91LIW
R14a MCLgaus Rd. OaRbWO, NC 29129
K,YW,YP-
2, YD-
11/9Y2017
RC
3 NS NF
43.60%
84
15 15AWN 60 2D.104W
_
i4mil wkk 1lt M Rd, Gakbwm NC 25122
YK, YW,N
P,YD-
RC
3 YS YF
43.60%
33 29
35 16.223N 80 18.0921 W
1434a CL"iw Rd. GaAr6oro. NC 28129
l0.Y8l3017
34 32-11 "179 11.859W
RC
NK,YW,N
P,YD-
3.NS.NF
43,60%
51
a
i927A ald Rd Rowm"ONC
70nd/2017
RC
NK,YW-
2,NP,NS,
ND. YF
43.60%
56
e
3a 71.962E 79 8.4544+1
TO/18fi017
l927 Gerald Rd Rowfar3d.NC
34 31.432N 79 7.068 W
RC
NK, YW,Y
P,NS,NF,
YO
43.60%
43
a
Tr1n 912017
1927 G2rafd Rd RowlendX
34 31.568M 79 6d69 W
RC
NK, YW,
YP, YD,N
SNF
43.60%
52
a
ivn 8/20f7
1927 GNr.1d Rd Partied NC
?4 30.824N 79 12919 W
RC
NK,NW,N
F,NS,NP,
ND
43.60%
10
a
1927 4WWd Rd. R0N1and NC
10n W2017
_ -
RC
NW,NF,N
S,NP,YD-
3
43.60%
43
34 Jtl.MN 791-4.196W
19270 Al Rd. R.,W.ntl NC
11N/2017
—
RC
YK,YW-
2,YP-
3,YD-
6.N5 NF
43.60%
70
a
3515.342N 80 19.307W
14J44 Mclsskr Rd. OaRboro NC 28129
- -
I?Z?014P
RC
YK,YW-
2,YP, YS,
NF.D-4
43.60%
109
35 17.502N 60 14.064 W
29716 KafttmoA Dr. AMaOP NC 2a00r
w— SiB7.39000
2252.98204
2018 iSpit TOIIF Tana
MpnN Tp Farmer I Field Rain alL Aer.. Use
Nov Good
YK,YW,N
f/2/2018
RC
F NS YP
42.40%
15
a
9s }5 ar4waa ra.832W
29716 Dr. AAn—*r1q. NO J%Wl
Yk,YW,N
F,NS,NP,
11/16,2017
RC
D-5
42.40%
147
a
3517.214N 80 12.777W
36083 W—tam Rd. Nae7madv NC
NK, YW,Y
FNS,NP,
11H6/2017 3512
RC
YDS
42.40%
15
a
3516.159N 80 12.539 W
3EOa3 +snsten Rd. AADwmarle NC
NK, YW,Y
7Rtf10in
RC
FYSNP
42.40%
38
a
34 40.186N 79 13.915W
5a5 Di h Rd. FV.W ke. NC
NK, YW,Y
7131/2018 3546
RC
F YS NP
42.40%
49
a
34'39,532N 79 14.19E W
54S Bud.! Rd. P.mhrak.. NC
_
Nk,YW,Y
F,NS,NP,
7l31/20f8
Grass
YD
42.40%
11
ag
34 39,880N 77 e7 455W
5O 8wfei n Rd -em. mke NO
NK,NF,Y
W-
2,NS,NP,
10H7/2017
RC
YD
42.40%
}t
34 49.562N 795.622W
S27J Okf to—y Rd. Shannon NG 2aJSB
_
NK,NW,N
F,NS,NP,
fOH7/2017
RC
D•2
42.40%
48
34 40.744N 7$ 7.0s0W
U14 O!d La Rd S4MrNlen NC am$
NK,NF,Y
S,NS,NP,
10/17/2017
11~8 4 1'
RC
YD-2
42.40%
49
a
34 49,S18N 79
6274 old Lowory Rd. 54a 0 NC 23331
NK,YW,N
F,NS, YP,
aH 7r2018
RC
D-2
42.40%
70
a
iJ 29-880N 79 12A } 7 W
_
3577 E Ravnham Rd FafrmAwftit NC 783J0
_
NK,YW,N
F,NS,YP,
8H7/2018
RC
D
42.40%
45
aL46LU
a
34 29.70fN 7911.919W
3577 E Ra Ad FlHmnnl, NC 28340
NK,YW-
2,NF,NS,
8H7/T018 -
RC
YPD4
42.40%
90
a
34 29.97aN 79 f1 6ETW
3577 E Ra Ram Rd. Faffmnt. NC 78340
NK,NW,Y
F,NS,NP,
frd7/Z018
RC
YD-3
42.40%
29
34 39761N 79 r4.229 W
us Rud Rd. pmamhk NC
YK, YW,Y
1/2/1018 3642
RC
FYS YP
42.40%
400
a
35 17. f 9}N 80 15.918w
2Y718 Dr. Alewmatk NC 28001
NK, YW,Y
9/29/2019 3607 1
RC
F NS NP
42.40%.
29
aff
36,17 872N 7012.562 W
1711Bla Nd �ernhrvka NC
NK,YWN
8/29/2018 3616
RC
FNS NP
42.40%
13
a
34 43.387N 76 6.405W
170 Elarce Rd. Pembroke NC
YK,NW,Y
F, YS,NP,
NEW
!0l212018
RC
YD-2
42.40%
34
a
351.238N80 T3,a28w
2317 H 218 Peachland NC 28133
F `�I
NK,YW-
3,NF,NS,
1011112018
Grass
YP.YD4
42.40%
134
air
3/ N. 747W 79 8.44CW
1189 Wf; S ane t Rd. Frkn m! NC 28340
NK, YW,N
P,NS,NF,
fOMB/2017
3719
RC
YD
42.40%
le
a
9/ 2.7 020N 79 1 T.970 W
1927 Ge ydidol RawlnW NC 74Ja]
NK YW,N
P, YD,NS,
T0q Y7
3720
RC
NF
42.40%
f7
a
34 3I.1i2N 74 17-177W
Y927 OW10d Rd. R9w14ad. NC 2a383
"' NW
F,NS,NP,
7�M T1
RC
YD-3
42.40%
59
a
04 33. 11 IN 78 6.2fi0w
1927 Gerald Rd. Rowland NC 28383
NK, YW,N
F,NS,NP,
e/3/2ofe
RC
YO
42.40%
14
a
34 2e.086N 79 7.735W
2648 Manetra Marlena NC 283a2
_ -
NK,YW,N
RC
F,NS,YP,
YD-3
42.40%
20 s9 M
i 5o e
.12018
_
_
34 25.852N 79 7.896W
2648 Mz lelra WHO* NC 28362
_...
YK,YW,N
F,NS,NP,
fOr2r2016
_
MIN11.+971sat
RC
YD
42.40%
22
70.8a
a
351862 8015.SOHW
23T7R 278 Plash/and 71C 28733
NK, YW,N
3738
RC
P,YD,NS,
YF
42.40%
43 a
0729I018
_
34 J7.7/7N 7B 12.408W
170 E4r Rd. Pembrvkv NC
YK,YW,N
— - —
F,NS,NP,
37A7'
RC
YD
42.40%
19 a
35169T6N 8018.844W
2971611n1 ck Or AIb mark NC 28001
YK,YW,N
F, YS,YP,
12/2018
RC
YD-3
42.40%
38 a
3 16.162N 00 16.52d W
29776 No11 aro0k 0r. Alb —le NC 2W01
YK, YW,Y
11y70fe
RC
FNS.NP
42.40%
16 a
3515.71BN 80 18.711W
20716 Linn a.,.oa fi, R:nermarle. NC 7r001
Yk,YW,N
F,NS,NP,
1N/3018
- — -
35 � 7. d67N 8Fl i 1. r 5/ W
RC
D-5
42.40%
27 a
29716 Ivah Dr AibelnF/Ikl kC 28001
YK,YW,N
fy20T8
—
3 1s. a52N e0 18, 246 w
RC
FNSYP
42.40%
18 a
29718 ftHybmk Or Albormall¢ rr[_' : aeiR1
RC
K,YW,NF,
NS.NP
42.40%
17 a
f/Z70T8
35 15 VON 80 16.sa4 W
2971E 0r .Albermarfe NC 28001
ifibrook
_ -
Nk,NW,N
F,NS,NP,
11/9/201B
Firms
RC
YD-3
42.40%
134 4f..763N 79 7F 531W
343W. L. Moore Maxton NC JJ364
E12
NK, YF,
NW, NS,
34 42.213N 79 16.720 W
RC
NP YD-5
42.40%
a
343 W. L. Moore Maxton NC 28364
- 2815 rnru
Month F Held I Rain Ac Use
Dec Good
—.1
NK,NW,Y
F,NS, YP,
1/29/2018
RC
D4
42,00%
155
7d 34.M6N 798.1S1W
3338 N t30 Eau Rowland NC T8393
YK, YW,N
F,NYS,N
11r1617017
0
RC
PYD J
42.00%
59
3516.983N B0 12 W6 W
360a7 Weston Rd AltW.3de C
YK, YW,N
F,NS,NP,
11N6/2017
RC
D-5
42.04
147 a
3517.214N 80 12.777W
36083 Weston Rd Albemarle, NC
NK,NW,N
F,NS,NP,
f0/17/2017
-
RC
Yd
42.00%
Hall
34 49.637N 79 6.990 W
5274 DO Lo kd Shannon NC 28986
-
Nk,YW,N
20117R0f7
rr
3569
RC
FYSNP
42.00%
H a
74 49.215N 79 6.181W
5274 Old Lowe Rd. Shannon NC 28386
NK,YW,N
1O117/2017
3571
RC
F.YS.NP
42.00%
43 a
r
3f 49 i15N 79 r r n T.v
5274 O!d Loaxr.l Rd. Shannon NC 28386
NK, YW,N
10/17/2017
3572
RC
F NS NP
42.00%
45
3448.94 W 79 9.345 W
52 4 Old Lnwe Rd Shannon NC 2d.!2_h
NK,NW,N
F,NS,NP,
IM772P77
RC
YD-2
42.00%
46 a
3449.7441f 797MW
527A CM LDWWP Rd SADAronNC 28786
NK,YW,N
F,NS,NP,
T 7R0}7
RC
YD-2
42.00%
49 a
3449.518A 796.T2tW
74 00 L—y Rd, S NC 21.
NK,YW,N
fOff}128}7
3579
RC
F.YS.NP
42.00%
33
7447.623N?25,2 aW
5274 Oid lad. Shannon NC 2a3a8
NK,NW,N
10/17/2017
3580
RC
F NS NP
42.00%
50 a
34 47569N 79 5.637 W
5774 Ord La - no Shann9n NC woo
NK,YW,N
10H7/2017
RC
FYSNP
42.00%
69 846:200 a
_M.
- -- - - 34 49.067N 70 7.097W
5274 Old Lo Rd Shannon NC:83a5
Grass
NK,YW,N
F NS NP
42.0021
28 AIRML
10/17/2017
51.872N 79 9.795W
7 ow Rd Sbannon NL'I8786
NK,YW,N
F,NS,YP,
r On 712017
RC
YD-2
42.00%
50 a
34 ST.a43N 79 8.484 W
6274 OM L Rd. Shannon. Nc 28386
NK,NF,Y
W,NS, YP,
10/f7ra017
RC
YD
42.00%
5a a
34 AS 100W 79 8.404 W
52M Ofd Loyrory Rd. Sk"wMI NG 2BM
NK,YW,N
F,NS,YP,
8M7/2018
RC
D-2
42.00%
70
34 29.89011 79 12.411.W
3577 E Raynham Rd. Fairmont NC 28340
NK,YW
$NF,NS,
dli7 1d =
RC
YP
42.00%
90
a
34 29.978N 79 77.857 W
7577 F Ra am Rd. Fur ArC 28740
77
NK,NW,N
Nr3+2p77 3594
RC
FYS.NP
42.00%
524
aaa
34 29.881N 79 4355W
1372 N RK P"MhMAaNC28372
NK,YW,N
3617
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9
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3620
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.lafN
170 Ef9c4 Rd. Prkrok NC 2772
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4020
dW W
75 t] e9O ,s8dl
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ars
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129
_ 1 -
-
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1 i8 3744
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10/18M017
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32
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119
a
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10,23/2018
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87
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i0/T3/2018 3815
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14
a
7413.076N 7118.768 W
1384 School Rd- Framrarrl NC 2e340
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72/7/2018
RC
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20
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34 46.771N 79 12.231 W
441 McGaint Rd Maxton NC 28364
1217, 2018
-
— —
-
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f8
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12/7/2018
3823
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12/7/2018
3824
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113
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3832
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40
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3/2/2016
—
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12/27/2078
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12/27/2018
_— -
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864 fClrrlc Marlorr, NC 28364
ay
a
a
a
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): urface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
L$rDistribution and Nyarketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes C No ❑ -► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
WQ0009477
2142.53975
2142.53975
See Attached
2142.53975
Agricultural
February
WQ0009477
2081.19939
2081.19939
2081.19939
Agricultural
March
WQ0009477
2140.4835
2140.4835
2140.4835
Agricultural
April
WQ0009477
2304.76288
2304.76288
2304.76288
Agricultural
May
WQ0009477
2237.03788
2237.03788
2237.03788
Agricultural
June
WQ0009477
1983.74770
1983.74770
1983.74770
Agricultural
July
WQ0009477
2024.33654
2024.33654
2024.33654
Agricultural
August
WQ0009477
2565.88706
2565.88706
2565.88706
Agricultural
September
WQ0009477
1915.16918
1915.16918
1915.16918
Agricultural
October
WQ0009477
2252.98204
2252.98204
2252.98204
Agricultural
November
WQ0009477
2056.93424
2056.93424
1
2056.93424
Agricultural
December
WQ0009477
2119.05540
2119.05540
2119.05540
Agricultural
Total from FORM DMSDF (sup)
0
25824.13556 25824.13556
25824.13556
Totals: Annual (dry tons):
O'�824.13556
25824.13556
25824.13556
Amendment(s) used: Bulkin Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 1W Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
S gnature of Permittee 61�-
Date Signature ofPreparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (12/2006)
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only)
VDistribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
Jan
WQ0009477
171.36425
171.36425
Jamie Austin
171.36425
ag
WQ0009477
19.35875
19.35875
Kevin Baucom
19.35875
ag
WQ0009477
321.01950
321.01950
Dan Brooks
321.01950
ag
WQ0009477
90.90750
90.90750
Jody Dennis
90.90750
ag
WQ0009477
30.41300
30.41300
Mike Freeman
30.41300
ag
WQ0009477
50.09050
50.09050
Jimmy Gaddy
50.09050
ag
WQ0009477
10.65050
10.65050
Robbie Harrington
10.65050
ag
WQ0009477
128.88550
128.88550
Robert Kimrey
128.88550
ag
WQ0009477
51.10200
51.10200
Rex Oxendine
51.10200
ag
WQ0009477
1067.18775
1067.18775
Roger Oxendine
1067.18775
ag
WQ0009477
89.60275
89.60275
Glen Phiefer
89.60275
ag
WQ0009477
19.84325
19.84325
Lynn Thomas
19.84325
ag
WQ0009477
92.11450
92.11450
Vinson York
92.11450
ag
Feb
WQ0009477
49.12754
49.12754
Jamie Austin
49.12754
ag
WQ0009477
39.51791
39.51791
Kevin Baucom
39.51791
ag
WQ0009477
62.67891
62.67891
Jason Blackwelder
62.67891
ag
WQ0009477
163.32438
16332438
Fairly Drake
163.32438
ag
WQ0009477
235.62166
301.82716
159.86334
655.28587
413.95262
235.62166
301.82716
159.86334
655.28587
413.95262
Robbie Harrington
Jeff Long
Ozmer Lee Oxendine
Roger Oxendine
Wayne Saunders 1
235.62166
301.82716
159.86334
655.28587
413.95262
ag
ag
ag
a
WQ0009477
WQ0009477
WQ0009477
WQ0009477
ag
Totals:
Annual (dry tons):
0
4213.73914
4223.73914 4223.73914
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 7
DENR FORM DMSDF (Supp) (12/2006)
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT N: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
X niafrihnfinn and Mar4rfi- f -Wl Pads A and Rl
Part A":
Part Ba:
Month
Sources(s) (include NPDES 4 if
applicable)
Volume (dry tons)
Recipient Information
.Amendment) BuFkmtt Agent
Residual In
Product Out
Name(s)
Volume)
(dry tons
Intended use(s)
Mar
W00009477
161.71668
161.71668
Jamie Austin
161.71668
ag
W00009477
313.72092
313.72092
Bart Barbee
313.72092
a
W00009477
31.04172
31.04172
Dan Brooks
31.04172
ag
W00009477
422.51184
422.51184
Bruce Cuddy
422.51184
ag
W00009477
39.77712
39.77712
Fairly Drake
39.77712
ag
W00009477
148.89096
148.89096
Barrett Gaddy
148.89096
a
W00009477
304.95240
304,95240
Robbie Harrington
304.95240
ag
W00009477
147.23496
147.23496
Johnny Helms
147.23496
ag
W00009477
323.68590
323.68590
Lee's Farm
323.68590
ag
WQ0009477
192.34026
192.34026
Marshall Red Locklear
192.34026
ag
WQ0009477
54.61074
54.61074
Will Russell
54.61074
a
Apr
W00009477
229.39840
229.39840
DewightAtkins
229.39840
a
W00009477
623,54432
623.54432
Blue Q Ranch
623.54432
a
W00009477
356.03456
356,03456
Terry Freeman
356,03456
a
W00009477
145.77472
145.77472
Brandon Husse •
145.77472
ag
W00009477
76.40640
76.40640
Darrell Hussey
76.40640
a•
WQ0009477
20.50048
20.50048
Vance Lambert
20.50048
ag
W00009477
142,04736
142.04736
Franklin Lee
142.04736
a
W00009477
205.97248
205.97248
Lee's Farm
205.97248
a
WQ0009477
32,19776
32.19776
Ricardo Rodrizuez
32.19776
ag
ota s:
Annual (dry tons):
0
34:2.35998
3972.35998 3972.35998
....... ........... .........
-
Amendment(s) used:
Bulking Agent(s)
used:
u more space is requrrea, attacn aaanronal mtormation sheets (FURM DMSDF (supp)): Total Number of Form DMSDF (Supp)�_ 7 1
2140.4835
1831.87648
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
X Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
April continued
WQ0009477
101.54816
1 101.54816
Will Russell
101.54816
ag
WQ0009477
252.90944
252.90944
Wayne Saunders
252.90944
ag
WQ0009477
53.73760
53.73760
Duane Strider
53.73760
ag
WQ0009477
64.69120
64.69120
Terry Williams
64.69120
ag
Ma►•
W00009477
74.82542
74.82542
Dewight Atkins
74.82542
ag
WQ0009477
182.36494
182.36494
Bernard Beck
182.36494
ag
WQ0009477
458.86710
458.86710
Blue Q Ranch
458.86710
ag
WQ0009477
61.27148
61.27148
D lon Chriscoe
61.27148
ag
WQ0009477
165.39018
165.39018
Wayne Chriscoe
165.39018
ag
W00009477
126.97174
126.97174
Charles Deaton
126.97174
ag
WQ0009477
199.79462
199.79462
Terry Freeman
199.79462
ag
WQ0009477
42.65990
42.65990
Brandon Hussey
42.65990
a
WQ0009477
31.3761
31.3761
Darrell Hussey
31.3761
a
WQ0009477
544.62844
544.62844
Wayne Saunders
544.62844
ag
WQ0009477
348.88796
348.88796
Terry Williams
348.88796
a
Totals:
Annual (dry tons):
0
2709.92428
2709.92428 : 270Q.92428
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7
472.88640
2237.03788
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT 0: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month', "Source(s)" and "Residual In" columns only)
X nistrihntinn and Mnrkrtinn lromnlntn Pnrfs A. and R\
_ PartA*:
PartB*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Mended use(s)
Jun*
W00009477
1157.20915
1157.20915
B&F Farms
1157.20915
ag
W00009477
72.51275
72.51275
Blue Q Ranch
72.51275
ag
WQ0009477
10.48420
10.48420
Charles Deaton
10.48420
a
W00009477
43.62335
43.62335
Terry Freeman
43,62335
ag
W00009477
21.45790
21.45790
Darrell Hussey
21.45790
ag
W00009477
125.10285
125.10285
Wayne Saunders
125.10285
ag
W00009477
553.35750
553.35750
Terry Williams
553.35750
ag
Julv
W00009477
124.17698
124.17698
Max Asbill
124.17698
ag
WQ0009477
1147.82444
1147.82444
B&FFarms
1147.82444
ag
W00009477
44.22256
44.22256
Bernard Beck
44.22256
a
W00009477
64.01318
64.01318
James Dunlap
64,01318
ag
W00009477
69.01304
69.01304
Gilbert Keys
69,01304
a
W00009477
575.08634
575.08634
Tony Smith
575.08634
ag
Totals:
Annual (dry toes):
0
4008 0842
4008 0842 401,80842
Amendment(s) used:
Bulking Agent(s)
used:
1t more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)1 7
1983.74770
2024.33654
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT 9: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
X nictrihnlinn and Markrtina lrmml . P-t. A and Rl
Part A•:
Part B":
Month
Sources(s) (include NPDES 4 if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
Aug
WQ0009477
11.05188
11.05188
1 John Cummings
11.05188
ag
W00009477
42,61084
42.61084
Kenwin Cummings
42.61084
a
W00009477
830,48322
830.48322
Lacy Cummings
830.48322
a
WQ0009477
2070778
20.70778
William Cummings
20.70778
a
W00009477
62,83248
62,83248
Wilber Harris
62,83248
ag
W00009477
109.047
109.047
Richard Hays
109.047
ag
WQ0009477
82,1755
82.1755
Sean Hunt
82.1755
ag
W00009477
185.11676
185.11676
Lycurous Lowery
185.11676
ag
W00009477
189.3493
189.3493
Rex Oxendine
189.3493
ag
W00009477
704,92976
704,92976
Roger Oxendine
704.92976
ag
W00009477
118.18554
118.18554
Jessie Oxendine
118.18554
a
W00009477
209.397
209.397
Tony Smith
209.397
ag
Se it
W00009477
123,96751
123.96751
Jamie Austin
123.96751
ag
W00009477
766.9657
766.9657
KevinBaucom
766.9657
ag
W00009477
95.21955
9521955
John Cummings
9521955
ag
WQ0009477
146.13239
146,13239
Lacy Cummings
146.13239
a
W00009477
4148613
43.48613
James Dunlap
43.48613
ag
WQ0009477
91.49006
91.49006
Sean Hunt
91,49006
ag
W00009477
104.09841
104.09841
Lee Farms
104.09841
ag
WQ0009477
154.76231
154,76231
Terry Locklear
154,76231
ag
W00009477
66.07974
66.07974
Eddie Moore Brother Ag
66.07974
ag
WQ0009477
22.74113
22.74113
Jessie Oxendine
22.74113
ag
W00009477
275.93616
275.93616
Rex Oxendine
275.93616
ag
W00009477
24.29009
24.29009
Roger Oxendine
2429009
ag
Totals:
Annual (dry teas):
0
4481 0562
1 4481 0562 4-191 ,i62
Amendment(s) used:
Bulking Agent(s) used:
' If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)�
2565.88706 _-
1915.16918 IK;
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT if: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc
PHONE: 910-895-4033 7428C COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
X Distribution and Marketing (complete Parts A- and Rl
Part A*:
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume
(dry tons)
Intendeduse(s)
Oct
W00009477
61.9992
61.9992
Jamie Austin
61.9992
a
W00009477
33T49016
337.49016
KevinBaucom
337.49016
ag
W00009477
133.00616 11
133.00616
Jeff Griffin
133.00616
a
W00009477
322.93648
322.93648
Lee Fang
322.93648
ag
W00009477
65.3782
65.3782
Jessie Oxendine
65.3782
a
W00009477
19T83936
197.83936
Rex Oxendine
197.83936
ag
W00009477
398.08108
398.08108
Roger Oxendine
398,08108
a
WQ0009477
297.93624
297.93624
Mike Presslar
297.93624
ag
W00009477
206.79916
206.79916
David Underwood
206.79916
ag
W00009477
231.51600
231.51600
Robert Wilkins
231.516001
a
Nov
W00009477
210.1768
210.1768
Ronnie Bralock
210.1768
ag
W00009477
96.65504
96,65504
JeffGriffm
96.65504
ag
W00009477
96.03176
96.03176
Richard Hays
96.03176
a
W00009477
253.74704
253.74704
Sean Hunt
253.74704
ag
W00009477
270.18552
270.18552
L&R Moore Fangs
270.18552
a
W00009477
112.20312
112.203121
Wendell Locklear
112.20312
ag
W00009477
243.43536
243.435361
L curous Lowery
243.43536
ag
W00009477
108.23024
108.23024
Jessie Oxendine
108.23024
a
W00009477
102.34936
102.34936
Roger Oxendine
102.34936
ag
WQ0009477
241.92168
241.92168
David Underwood
241.92168
ag
W00009477
226.72128
226.72128
Mike Willoughby
226.72128
ag
W00009477
95.27704
95.97704
Robert Wilkins
95.27704
ag
Totals.
Annual (dry tons):
0
430991628
430991628-...-.:'.'.':':':':':'::':'::::::: 43095-1628
'-. ...........
Amendment(s) used.
Bulking Agent(s)
used:
it more space is required, attach additional mtormation sheets (FUKM DMSL)F (supp)): Total Number of Form DMSDF (Supp)1 7 1
2252.98204
2056.93424 -
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
X Distribution and Markefinv (comnlete Parts A. and R)
Part A*:
Part B*•
Month
Sources(s) (include NPDES # if applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended
use(s)
Dec-18
W00009477
41,1894
41.1894
Ronnie Bralock
41.1894
ag
W00009477
105.8778
105.8778
Adam Collins
105,8778
ag
W00009477
158.62980
158,62980
Aundra Hunt
158.62980
a
W00009477
20.9622
20.9622
Sean Hunt
20.9622
ag
W00009477
32.08380
32.08380
Daniel Locklear
32.08380
ag
WQ0009477
595.8876
595.8876
Lee Grady LavcEry
595.8876
ag
W00009477
146.1894
146.1894
Phillip Locklear
146.1894
ag
WQ0009477
83.23980
83.23980
Jimmy McMillan
83.23980
W00009477
20.37000
20.37000
Jessie Oxendine
20.37000
ag
W00009477
10.72680
10.72680
Rex Oxendine
10.72680
ag
W00009477
210.21000
210,21000
Roger Oxendine
210.21000
ag
W00009477
63.24360
63.24360
Ronald Stickland
63.24360
ag
W00009477
133.63980
133.63980
David Underwood
133.63980
a
W00009477
453.73440
453.73440
Robert Wilkins
453.73440
ag
W00009477
10.74780
10.74780
Jeff Griffin
10.74780
a
W00009477
32.32320
32.32320
Mike Preslar
32.32320
ag
Totals:
Annual (dry tons}:
0
2119 05540
2119.05540 : j; j j; ;< ; . : }; : }; ; }; ; 2119.0554
Amendment(s) used:
Bulking Agent(s)
used:
It more space is required, attach additional mtormation sheets (F(JRM DMSDF (supp)): Total Number of Form DMSDF (Supp)1 7 J
2119.M.4
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0009477 Laboratory: 1) Pace Analytical Services LLC.
Cascades Tissue Group -North Carolina a
Facility Name: division of Cascades Holdings US Inc. 2) Waypoint Analytical
Residual Source WQ # or WQ0009477 3) Summit
NPDES #: 4)
WWTP Name: 5)
Residual Analvsis Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
(m 4/k )a
Sample or Composite Date
01/03/18
02/14/18
03/12/18
04/05/18
05/08/18
06/12/18
07/11/18
& Retest
07/31/18
08/6/18
09/06/18
10/09/18
11/08/18
12/06/18
Percent Solids (%)
NA
42.50
1 43.7
41.40%
44.8
44.6
44.5
39.4
44.6
46.1
43.6
42.4
42
Arsenic
75
1
0.87
0.89
0.81
0.95
0.79
1.1
1
0.05 1
1
0.87
0.84
Cadmium
85
Not
Permit
Required -
Copper
4,300
21.1
24.5
20.5
22
19.9
18.4
20.9
18.9
14.5
22.7
16.5
37
Chromium
NA
Not
Permit
Required
Lead
840
Not
Permit
Required
Mercury
57
Not
Permit
Required
Molybdenum
75
Not
Permit
Required
Nickel
420
4.7
1.1
1.7 1.20
1.2
2.6
2.1
1.1
1.6
2.10
2.1
1.4
Selenium
100
Not
Permit
Required
Zinc
7,500
72.9
64.7
58.8
97.1
60.3
92
134
102
297
118
166
75.2
Total Phosphorus
NA
Not
Permit
Required
TKN
NA
1600
1680
1530
1630
1300
2080
1660
1120
1410
1800
1520
782
Ammonia -Nitrogen
NA
22.6
22.9
24.2
15.3
22
15.4
20.6
18.1
21.3
19.8
21.4
23.3
Nitrate and Nitrite
NA
4.7
4.6
4.8
4.5
1 4.4
4.4
5.1
4.5
4.3
4.4
4.7
4.7
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties p4tbinittin false infoamation, including the possibility of fines and imprisonment for knowing violations."
C
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00009477 Laboratory: 1) Pace Analytical Services, LLC
Cascades Tissue Group -North Carolina, a Wa oint Analytical
Facility Name: division of Cascades Holding US Inc. 2)
Residual Source WQ0009477 3) Summit
NPDES # or WQ#: 4)
WWTP Name: 5)
Residual Analvsis Data
Sam ile or C mposite Date
Parameter
(mg/kg)
01/03/18
02/14/18
03/12/18
04/05/18
05/08/18
06/12/18
07/11/18
& Retest
07/31 /18
08/06/18
09/06/18
10/09/18
11/08/18
12/06/18
Pan Cal
480
504
459
489
390
624
498
336
423
540
456
235
Aluminum
Not
Permit
Re uired
Carbon/Nitrogen Ratio
160
140
180
140
387.3
210
180
150
66
92
59
27
Calcium Carbonate
Equivalency
Not
Permit
Required
PH
7.1
7.9
7.4
8.4
7.70
7.6
7.7
7.1
8.3
7.1
7.4
7.4
Magnesium
1510
1620
1630
1240
1570
1360
1580
1630
1400
1650
1460
1740
Sodium
Not
Permit
Required
Potassium
Not
Permit
Required
Calcium
171000
189000
167000
150000
187000
211000
158000
168000
179000
157000
160000
185000
Ignitablilty- Summit
08/28/18
ND
Reactivity Summit
08/28/18
ND
Corrosivity Summit
08/28/18
7.1
Total Nitrogen
1600
1680
1530
1630
1300
2080
1660
1120
1410
1800
1520
782
TOC
289000
272000
323000
293000
306000
318000
311000
275000
312000
310000
306000
290000
Volatile Solids
496700
467500
555300
503100
526300
546500
535300
473800
536200
534000
527000
498000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
si4ulies for submitting fai info cation, including the possibility of fines and imprisonment for knowing violations."
r * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)
.0001
PaceAnalyfical
..pacelaft corn
March 02, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92369117
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on January 09, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
A revised report is being submitted on 3/2/18 to include a corrected PAN calculation.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
od*c
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 18
1
PaceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92369117
Sample: Monthly Sludge Lab ID: 92369117001 Collected: 01/03/18 13:40 Received: 01/09/18 09:43 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND mg/kg 2.0
1.0
1
01/11/18 08:45
01/15/18 12:33
7440-38-2
Calcium
171000 mg/kg 200
99.8
10
01/11/18 08:45
01/15/18 12:37
7440-70-2
Copper
21.1 mg/kg 1.0
0.50
1
01/11/18 08:45
01/15/18 12:33
7440-50-8
Magnesium
1510 mg/kg 20.0
0.50
1
01/11/18 08:45
01/15/18 12:33
7439-95-4
Nickel
4.7 mg/kg 1.0
0.50
1
01/11/18 08:45
01/15/18 12:33
7440-02-0
Zinc
72.9 mg/kg 2.0
1.0
1
01/11/18 08:45
01/15/18 12:33
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
42.5 % 0.000010
1
01/09/18 17:21
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
57.5 % 0.10
0.10
1
01/10/18 11:24
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.1 Std. Units 0.10
0.10
1
01/11/18 13:23
I Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
480 mg/kg 0.12
0.12
1
01/23/1814:48
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1600 mg/kg 40.0
20.0
1
01/23/1815:15
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 22.6
22.6
1
01/1811814:02
7664-41-7 R1
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
1600 mg/kg 118
58.9
1
01/23/18 03:41
7727-37-9 M1
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 4.7
4.7
1
01/23/18 03:21
M1
Nitrogen, Nitrite
ND mg/kg 2.4
2.4
1
01/23/18 03:21
Nitrogen, NO2 plus NO3
ND mg/kg 4.7
4.7
1
01/23/18 03:21
M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18
Page: 1 of 1
Report Number: 18-010-0208
■
Account Number: 05734(2) 7621 Whitepine Road, Richmond, VA 23237
Submitted By: Angela Baioni Waypoint
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Monthly Sludge/92369117001
ANGELA BAIONI
9800 KINCEY AVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OFANALYSIS
Lab Number: 58006
Sample Id : Monthly Sludge/92369117001
Date Sampled: 1/3/2018 13:40:00
Date Received: 01/10/2018 00:00
Date Reported: 01/16/2018
Total Solids *
43.30
433000
100.0
R D
01/10/2018 13:30
SM-2540G
Moisture *
56.69
100.0
R D
01/10/2018 13:30
SM-2540G
Total Kjeldahl Nitrogen
0.18
1800
50.0
R D
01/11/2018 09:00
SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
44.80
448000
2500
R D
01/11/2018 13:15
AOAC 955.01
Total Volatile Solids
49.67
496700
100.0
R D
01/10/2018 13:30
SM-2540G
C/N RATIO *
160
1
01/10/2018 13:30
CALCULATION
Carbon (TOC) *
28.90
289000
100
01/10/2018 13:30
CALCULATION
Comments:
NC CERT#257, SC CERT#9300 7001
ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Ot,re•: -)as and letters are for the exclusive and confidential use of cur Gieats, and may not be rrp oduced in whole or p nor may any r ference be made
tot' ork, the results, orlhe company in ary advertising, news release, .:, r- erpuhlic announc+:ra . Ys without obta,! g our pr.Y.., :i-i authorizaiian.
0
Pauric McGroary
Agronomist
YacleAnaljdical
www.pacelabs.com
March 01, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92373556
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 17
aWnalytica!®
www.pacawbs.com
f
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92373556
Sample: Monthly Sludge Lab ID: 92373556001 Collected: 02/14/18 15:35 Received: 02/15/18 10:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND mg/kg 1.7
0.87
1
02/20/18 01:15
02/23/18 01:56
7440-38-2
Calcium
189000 mg/kg 346
173
20
02/20/18 01:15
02/23/18 15:37
7440-70-2
Copper
24.5 mg/kg 0.87
0.43
1
02/20/18 01:15
02/23/18 01:56
7440-50-8
Magnesium
1620 mg/kg 17.3
0.43
1
02/20/18 01:15
02/23/18 01:56
7439-95-4
Nickel
1.1 mg/kg 0.87
0.43
1
02/20/18 01:15
02/23/18 01:56
7440-02-0
Zinc
64.7 mg/kg 1.7
0.87
1
02/20/18 01:15
02/23/18 01:56
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
43.7 % 0.000010
1
02/15/18 17:13
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
56.3 % 0.10
0.10
1
02/16/18 10:59
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.9 Std. Units 0.10
0.10
1
02/16/18 13:40
Plant Available Nitrogen
Analytical Method: SM 2710E
Plant Available Nitrogen
504 mg/kg 0.12
0.12
1
03101/1816:01
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1680 mg/kg 40.0
20.0
1
02128/1817:11
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 22.9
22.9
1
02/24/18 14:50
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
1680 mg/kg 87.9
44.0
1
02/16/18 17:24
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 4.6
4.6
1
02/27/18 22:59
Nitrogen, Nitrite
ND mg/kg 2.3
2.3
1
02/27/18 22:59
Nitrogen, NO2 plus NO3
ND mg/kg 4.6
4.6
1
02/27/18 22:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/01/2018 04:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17
Page: 1 of 1
Report Number: 18-047-0201
Account Number: 05734
Waypointe-r
ANALYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni)
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project : Sludge/92373556001
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS
Date Sampled: 2/14/2018 15:35:00
Lab Number: 58644
Date Received: 02/16/2018 00:00
Sample Id : Sludge/92373556001
Date Reported: 02/23/2018
PARAMETER
RESULT
- maim
RESULT
QUANTITATION
Total Solids "
43.74
437400
100.0
R D
02/16/2018 15:15 SM-254OG
Moisture'
56.25
100.0
R D
02/16/2018 15:15 SM-2540G
Total Kjeldahl Nitrogen
0.20
1990
50.0
R D
02/19/2018 08:40 SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
45.80
458000
2500
R D
02/21/2018 12:30 AOAC 955.01
Total Volatile Solids
46.75
467500
100.0
R D
02/16/2018 15:15 SM-2540G
C/N RATIO *
140
0
02/16/2018 15:15 CALCULATION
Carbon (TOC) *
27.20
272000
100
02/16/2018 15:15 CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Od re:•orrs and letters are fa the exclusive and confidential use of our clients, and may not be reproduced irs whole orpan, normay any reference be made
?WI:
to tD;wcrk, tho results, Of the company in any advertising, neu-s mleas ar, d )vr Public announcements o mhout obtaorung our prior w.i+4on 'wlhonzation.
0
Pauric McGroary
V
Agronomist
,PaceAnalyfical
www..pa&abs.com
March 23, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92376666
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
,1�
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 17
PMAnalj cal
www.paceiabs.corn
ANALYTICAL RESULTS
Project: Sludge
Pace Project No.: 92376666
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: Monthly Sludge Lab ID: 92376666001 Collected: 03/12/18 15:05 Received: 03/13/18 09:44 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010 Preparation Method: EPA3050
Arsenic
ND mg/kg 1.8
0.89
1
03/14/1813:50
03/17/1819:04
7440-38-2
Calcium
167000 mg/kg 355
178
20
03/14/18 13:50
03/20/18 02:47
7440-70-2
Copper
20.5 mg/kg 0.89
0.44
1
03/14/1813:50
03/17/1819:04
7440-50-8
Magnesium
1630 mg/kg 17.8
0.44
1
03/14/1813:50
03/17/1819:04
7439-95-4
Nickel
1.7 mg/kg 0.89
0.44
1
03/14/1813:50
03/17/1819:04
7440-02-0
Zinc
58.8 mg/kg 1.8
0.89
1
03/14/1813:50
03/17/1819:04
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
41.4 % 0.000010
1
03/13/18 17:13
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
58.6 % 0.10
0.10
1
03/14/18 10:41
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.4 Std. Units 0.10
0.10
1
03/15/18 14:15
(Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
459 mg/kg 0.12
0.12
1
03/23/18 15:52
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1530 mg/kg 40.0
20.0
1
03/23/1815:43
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev
2.0
Nitrogen, Ammonia
ND mg/kg 24.2
24.2
1
03/21/18 16:37
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
1530 mg/kg 92.9
46.4
1
03/22/18 13:37
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 4.8
4.8
1
03/15/18 03:22
Nitrogen, Nitrite
ND mg/kg 2.4
2.4
1
03/15/18 03:22
Nitrogen, NO2 plus NO3
ND mg/kg 4.8
4.8
1
03/15/18 03:22
Date: 03/23/2018 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 17
Page: 1 of 1
Report Number: 18-074-0207 '
Account Number: 05734���a �� M 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Monthly Sludge/92376666001
ANGELA BAIONI
9800 KINCEY AVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS
Date Sampled: 3/12/2018 15:05:00
Lab Number: 59212
Date Received: 03/15/2018 00:00
Sample Id : Monthly Sludge/92376666001
Date Reported: 03/22/2018
PARAMETER
RESULT
RESULT
QUANTITATION LIMIT
ANALYSIS
ANALYST
., •.
Total Solids "
41.86
418600
100.0
R D
03/15/2018 15:15 SM-254OG
Moisture *
58.13
100.0
R D
03/15/2018 15:15 SM-2540G
Total Kjeldahl Nitrogen
0.18
1790
50.0
R D
03/16/2018 09:00 SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
38.50
385000
2500
R D
03/19/2018 13:00 AOAC 955.01
Total Volatile Solids
55.53
555300
100.0
R D
03/15/2018 15:15 SM-254OG
C/N RATIO *
180
0
03/15/2018 15:15 CALCULATION
Carbon (TOC) *
32.30
323000
100
03/15/2018 15:15 CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
�,ri4` G¢orv�r/
Or �rv,,.ons and letters ore for the exclusive and confidenti,U as- of our crier fs, and may rat be nr duced in whola :: in. nor may any ie.•`erernce be ma.+e p
is HI; wo,h, the results, or the company in arty ad;erfisiup, ti-ws n-wase, ort4rw. r oblk: mnnrunccments without on -"Iraq our prior AWtc rl at,
0
Pauric McGroary
Agronomist
axAnalj cal
www.pacelabs.com
t
April 18, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92379782
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on April 05, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
01 L qrn thou o�{
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 17
r �
AJceAnalX cal
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92379782
Sample: Monthly Sludge Lab ID: 92379782001 Collected: 04/05/18 09:00 Received: 04/05/18 11:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND mg/kg 1.6
0.81
1
04/06/18 21:50
04/09/18 19:22
7440-38-2
Calcium
150000 mg/kg 162
80.8
10
04/06/18 21:50
04/10/18 14:54
7440-70-2
Copper
22.0 mg/kg 0.81
0.40
1
04/06/18 21:50
04/09/18 19:22
7440-50-8
Magnesium
1240 mg/kg 16.2
0.40
1
04/06/18 21:50
04/09/18 19:22
7439-95-4
Nickel
1.2 mg/kg 0.81
0.40
1
04/06/18 21:50
04/09/18 19:22
7440-02-0
Zinc
97.1 mg/kg 1.6
0.81
1
04/06/18 21:50
04/09/18 19:22
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
44.8 % 0.000010
1
04/05/18 17:53
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
55.2 % 0.10
0.10
1
04/06/18 10:44
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.4 Std. Units 0.10
0.10
1
04/06/18 12:03
)Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
489 mg/kg 0.12
0.12
1
04/18/18 17:12
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1630 mg/kg 40.0
20.0
1
04/18/1816:57
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 15.3
15.3
1
04/17/18 14:43
7664-41-7 R1
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
1630 mg/kg 101
50.7
1
04/11/18 13:13
7727-37-9
363.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 4.5
4.5
1
04/11/18 23:19
Nitrogen, Nitrite
ND mg/kg 2.2
2.2
1
04/11/18 23:19
Nitrogen, NO2 plus NO3
ND mg/kg 4.5
4.5
1
04/11/18 23:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04118/2018 05:14 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17
Page: 1 of 1
Report Number: 18-100-0207 '
Account Number: 05734���� �� 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92379782001
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
Lab Number: 59610
Sample Id : Sludge-92379782001
REPORT OF ANALYSIS Date Sampled: 4/5/2018 09:00:00
Date Received: 04/10/2018 00:00
Date Reported: 04/17/2018
ANALYST
Total Solids `
44.58
445800
100.0
JM
04/10/2018 15:00
SM-2540G
Moisture'`
55.41
100.0
JM
04/10/2018 15:00
SM-254OG
Total Kjeldahl Nitrogen
0.21
2110
50.0
R D
04/11/2018 08:30
SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
43.10
431000
2500
R D
04/13/2018 12:15
AOAC 955.01
Total Volatile Solids
50.31
503100
100.0
JM
04/10/2018 15:00
SM-2540G
C/N RATIO "
140
0
04/10/2018 15:00
CALCULATION
Carbon (TOC) *
29.30
293000
100
04/10/2018 15:00
CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
v �qw
0
60,1nrcits and fetters are for the exclusive an:9 confideii:iai use of our ciier?is, and may no be reproducei! in wnoie or part, normay any reference be made
to 0 woik, the results, or the company in any advertising, news release, or other p.rhlic announceme,)ts without obtaining ow'p ror wd1tun authorization.
0
JPauric McGroary
Agronomist
VIC
aceAnalyiical
www.pacelabs.mn
May 21, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92383860
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C +1 . '-�=N'
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 19
10? /4
FaceAnalytica!
..pacetabsxom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92383860
Sample: Monthly Sludge
Lab ID: 92383860001 Collected:
05/08/18
07:25
Received: 05/08118 10:19 Matrix: Solid
Results reported on a "dry weight'
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Arsenic
ND mg/kg 1.9
0.95
1
05/19/18 16:00
05/20/18 20:20
7440-38-2
Calcium
187000 mg/kg 190
95.1
10
05119/1816:00
05/2111815:41
7440-70-2 M6
Copper
19.9 mg/kg 0.95
0.48
1
05/19/18 16:00
05/20/18 20:20
7440-50-8
Magnesium
1570 mg/kg 19.0
0.48
1
05/19/18 16:00
05/20/18 20:20
7439-95-4
Nickel
1.2 mg/kg 0.95
0.48
1
05/19/18 16:00
05/20/18 20:20
7440-02-0
Zinc
60.3 mg/kg 1.9
0.95
1
05/19/18 16:00
05/20/18 20:20
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
44.6 % 0.000010
1
05/09/18 15:21
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
55.4 % 0.10
0.10
1
05/10/18 10:59
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.7 Std. Units 0.10
0.10
1
05/11/18 03:12
H1
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
390 mg/kg 0.12
0.12
1
05/17/18 16:40
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1300 mg/kg 40.0
20.0
1
05/17/1816:47
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 22.0
22.0
1
05/1511814:47
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
1300 mg/kg 66.0
33.0
1
05/16/18 01:57
7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 4.4
4.4
1
05/16/18 21:35
Nitrogen, Nitrite
ND mg/kg 2.2
2.2
1
05/16/18 21:35
Nitrogen, NO2 plus NO3
ND mg/kg 4.4
4.4
1
05/16/18 21:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2018 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19
Report Number: 18-130-0201
• a.
Account Number: 05734�point,,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92383860001
ANGELA BAIONI
9800 KINCEYAVENU=
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS
Lab Number: 60605
Sample Id : Sludge-92383860001
Date Sampled: 5/8/2018 07:25:00
Date Received: 05/10/2018 00:00
Date Reported: 05/18/2018
Total Solids *
44.06
440600
100.0
R D
05/10/2018 14:30
SM-2540G
Moisture *
55.93
100.0
R D
05/10/2018 14:30
SM-2540G
Total Kjeldahl Nitrogen
0.18
1790
50.0
JM
05/11/2018 08:30
SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
40.90
409000
2500
R D
05/15/2018 10:30
AOAC 955.01
Total Volatile Solids
52.63
526300
100.0
R D
05/10/2018 14:30
SM-2540G
C/N RATIO *
387.3
0
05/10/2018 14:30
CALCULATION
Carbon (TOC) *
30.60
306000
100
05/10/2018 14:30
CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not
to the work, the results, or the company in any advertising, . -- release, or other public am
Pofie. P 101*vr
Pauric McGroary
Page 18 of 19
Agronomist
Page 2 ,i 3
YaxAnalytical"
�
/
1 www.pacelabs.cw
June 25, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92388134
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on June 12, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a.Qt0��1
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21
I
PaceAnalj cal
www.pacelabs.eom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92388134
Sample: Monthly Sludge
Lab ID: 92388134001 Collected:
06/12/18
07:30
Received: 06/12/18 10:17 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Arsenic
ND mg/kg 1.6
0.79
1
06/13/18 10:25
06/14/18 23:49 7440-38-2
Calcium
211000 mg/kg 317
158
20
06/13/18 10:25
06/15/1817:11 7440-70-2
Copper
18.4 mg/kg 0.79
0.40
1
06/13/18 10:25
06/14/18 23:49 7440-50-8
Magnesium
1360 mg/kg 15.8
0.40
1
06/13/18 10:25
06/14/18 23:49 7439-95-4
Nickel
2.6 mg/kg 0.79
0.40
1
06/13/18 10:25
06/14/18 23:49 7440-02-0
Zinc
92.0 mg/kg 1.6
0.79
1
06/1311810:25
06/15/1812:05 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G
Total Solids
44.5 % 0.000010
1
06/12/18 17:00
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
55.5 % 0.10
0.10
1
06/13/18 10:27
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.6 Std. Units 0.10
0.10
1
06/14/18 08:08
�PlantAvailable Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
624 mg/kg 0.12
0.12
1
06/25/18 11:38 N2
Total Nitrogen Calculation
Analytical Method: TKN+NC3+NO2 Calculation
Nitrogen
2080 mg/kg 40.0
20.0
1
06/21/18 20:03 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 15.4
15A
1
06/18/1815:08 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
2080 mg/kg 77.5
38.8
1
06/16/18 02:31 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2
Nitrogen, Nitrate
ND mg/kg 4.4
4.4
1
06/16/18 02:35
Nitrogen, Nitrite
ND mg/kg 2.2
2.2
1
06/16/18 02:35
Nitrogen, NO2 plus NO3
ND mg/kg 4.4
4.4
1
06/16/18 02:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/25/2018 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 21
Report Number: 18-164-0204
Account Number: 05734 Waypoint-(Z-1
ANALYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project: 92388134001
ANGELA BAIONI
9800 KINCEY AVENUE
SUITE 100
HUNTERSVILLE , NC 28078
Lab Number: 61167
Sample Id : 92388134001
Total Solids'
Moisture "
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
C/N RATIO "
Carbon (TOC)'
Comments:
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 6/12/2018 07:30:00
Date Received: 06/13/2018 00:00
Date Reported: 06/18/2018
44.26
442600
100.0
R D
06/13/2018 12:30
SM-254OG
55.73
100.0
R D
06/13/2018 12:30
SM-254OG
0.15
1490
50.0
R D
06/14/2018 08:30
SM-4500-NH3C-TKN
39.20
392000
2500
R D
06/15/2018 08:30
AOAC 955.01
54.65
546500
100.0
R D
06/13/2018 12:30
SM-254OG
210
0
06/13/2018 12:30
CALCULATION
31.80
318000
100
06/13/2018 12:30
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and
to the wi.dk, the results, or the company in any advertising,
pwir- #1V 60° r
Pauric McGroary
Agronomist Page 19 of 21
Page 3 _)1
PaceAnalytical
www.pacelabs.com
July 26, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92391776
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on July 12, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless' otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 20
PaceAnalytical
www.pacelabs.com
August 13, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
RE: Project: Sludge TN resample
Pace Project No.: 92393883
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C. Page 1 of 14
aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sludge
Pace Project No.: 92391776
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: Monthly Sludge
Lab ID: 92391776001
Collected:
07/11/18 08:00
Received: 07/12/18 11:59 Matrix: Solid
Results reported on a "dry welght7 basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units
Limit
MDL DF
Prepared
Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Arsenic
ND mg/kg
2.2
1.1 1
07/13/18 10:30
07/16/18 00:55 7440-38-2
Calcium
I 158000 mglkg
437
219 20
07/13/18 10:30
07/16/18 22:39 7440-70-2
Copper
20.9 mg/kg
1.1
0.55 1
07113/18 10:30
07/16/18 00:55 7440-50-8
Magnesium
1580 mg/kg
21.9
0.55 1
07/13/18 10:30
07/16/18 00:55 7439-95-4
Nickel
2.1 mg/kg
1.1
0.55 1
07/13/18 10:30
07/16/18 00:55 7440-02-0
Zinc
134 mg/kg
2.2
1.1 1
07/13/18 10:30
07/16/18 00:55 7440-66-6
2540G Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
39.4 %, 0.000010
i
Percent Moisture I
Analytical Method: ASTM D2974-87
Percent Moisture
60.6 % 0.10 0.10
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
7.7 Std. Units 0.10 0.10
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Plant Available Nitrogen pwe9 ' -
r •
11300 . mg/kg 0.12 0.12
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
I�w
28800 mg/kg 40.0 20.0
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Nitrogen, Ammonia 42Ct-0$4-11
13400 mg/kg 497 497
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total !'�t`!�!'f'�C"
28800 mglkg 3620 1810
363.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3 Ae4ttq,
ND mg/kg 5.1 5.1
Nitrogen, Nitrate
ND mg/kg 5.1 5.1
Nitrogen, Nitrite
ND mg/kg 2.5 2.5
1
07/13/18 14:19
1
07/16/18 09:17
1
07/1611815:50 H1
1
07/26/1819:47 N2
1
07/25/1814:22 7727-37-9
20
07/19/18 03:00 7664-41-7
100
07/18/18 05:54 7727-37-9
1
07/20/18 21:15
1
07/20/18 21:15 14797-55-8
1
07/20/18 21:15 14797-65-0
Se-e Xow t 6
wC Slrt .
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/26/2018 07:51 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 20
4W00/1
PaceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge TN resample
Pace Project No.: 92393883
Sample: Monthly Sludge Lab ID: 92393883001 Collected: 07/31/18 06:18 Received: 07/31/18 09:39 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Percent Moisture
Percent Moisture
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
)Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 08/13/2018 05:17 PM
Analytical Method: ASTM D2974-87
55.1 % 0.10 0.10
1 07/31/1817:50
Analytical Method: SM 271 OB-2011
498 mg/kg 0.12 0.12
1 08/1311817:11 N2
Analytical Method: TKN+NO3+NO2 Calculation
1660 mg/kg 40.0 20.0
1 08/09/18 20:36 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 20.6 20.6
1 08/02/18 09:58 08/02/18 12:33 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
1660 mg/kg 106 53.0
1 08/06/18 11:26 08/07/18 03:44 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.4 4.4
1 08/07/1811:07 08/07/1816:52
ND mg/kg 4.4 4.4
1 08/07/1811:07 08/07/1816:52 14797-55-8
ND mg/kg 2.2 2.2
1 08/07/1811:07 08/07/1816:52 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 14
Report Number: 18-198-0201
Account Number: 05734 Waypoint-(D
ANALYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : 92391776
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS
Lab Number: 61741
Sample Id : Monthly Sludge
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 7/11/2018 08:00:00
Date Received: 07/17/2018 00:00
Date Reported: 07/20/2018
Total Solids *
39.25
392500
100.0
JM
07/17/2018 15:30
SM-2540G
Moisture *
60.74
100.0
JM
07/17/2018 15:30
SM-2540G
Total Kjeldahl Nitrogen
0.17
1730
50.0
R D
07/18/2018 09:00
SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
2.94
29400
2500
R D
07/19/2018 14:02
AOAC 955.01
Total Volatile Solids
53.53
535300
100.0
JM
07/17/2018 15:30
SM-254OG
C/N RATIO *
180
0
07/17/2018 15:30
CALCULATION
Carbon (TOC) *
31.10
311000
100
07/17/2018 15:30
CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prim written authorization.
Pauric McGroary
Page 18 of 20
Agronomist
Page 2 of 4
00001
FaceAnaljftal
Wmpawabs.com
September 05, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92394750
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2018. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
A revised report is being submitted on 9/5/18 to include a revised subcontract laboratory report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C. Page 1 of 21
-0 aceAnalytical'
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92394750
Sample: Monthly Sludge Lab ID: 92394760001 Collected: 08/06/18 15:15 Received: 08/07/18 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Calcium
Copper
Magnesium
Nickel
Zinc
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 09/05/2018 04:15 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3050E
ND
mg/kg
2.1
1.0
1
08/08/18 10:13
08/10/18 01:33
7440-38-2
168000
mg/kg
208
104
10
08/08/18 10:13
08/11/18 20:19
7440-70-2
18.9
mg/kg
1.0
0.52
1
08/08/18 10:13
08/10/18 01:33
7440-50-8
1630
mg/kg
20.8
0.52
1
08/08/18 10:13
08/10/18 01:33
7439-95-4
1.1
mg/kg
1.0
0.52
1
08/08/18 10:13
08/10/18 01:33
7440-02-0
102
mg/kg
2.1
1.0
1
08/08/18 10:13
08/10/18 01:33
7440-66-6
Analytical Method: SM 254OG-2011
44.6 % 0.000010 1 08/07/1817:31
Analytical Method: ASTM D2974-87
55.4 % 0.10 0.10 1 08/07/1817:28
Analytical Method: EPA 9045D
7.1 Sid. Units 0.10 0.10 1 08/13/18 12:23
Analytical Method: SM 271OB-2011
336 mg/kg 0.12 0.12
1 08122/1817:36
Analytical Method: TKN+NO3+NO2 Calculation
1120 mg/kg 40.0 20.0
1 08/22/1817:41 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 18.1 18.1
1 08/10/1812:59 08/1011817:03 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
1120 mg/kg 83.1 41.6
1 08/21/18 01:46 08/22/18 01:40 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.5 4.5
1 08/17/1810:49 08/17/1814:05
ND mg/kg 4.5 4.5
1 08/17/1810:49 08/17/1814:05 14797-55-8
ND mg/kg 2.2 2.2
1 08/17/1810:49 0811711814:05 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H1
N2
Page 6 of 21
Report Number: 18-221-0204
Account Number: 05734
r
Waypoint'
ANALYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni)
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
Lab Number: 62217
Sample Id : Monthly Sludge
Project : 92394750
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 8/6/2018 15:15:00
Date Received: 08/09/2018 00:00
Date Reported: 09/05/2018
Total Solids *
44.40
444000
100.0
R D
08/31/2018 14:30
SM-2540G
Moisture *
55.60
100.0
R D
08/31/2018 14:30
SM-2540G
Total Kjeldahl Nitrogen
0.19
1870
50.0
R D
08/10/2018 08:30
SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
27.60
276000
2500
R D
08/14/2018 10:30
AOAC 955.01
Total Volatile Solids
47.38
473800
100.0
R D
08/31/2018 14:30
SM-2540G
C/N RATIO *
150
0
08/10/2018 08:30
CALCULATION
Carbon (TOC) *
27.50
275000
100
08/31/2018 14:30
CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part,
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining
Pauric McGroary
Agronomist
Page 2
PaceAna1j cal
www.pacelabs.com
September 19, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92398534
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on September 06, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a, W1.
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21
�aceAnafj4ical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92398534
Sample: Monthly Sludge Lab ID: 92398534001 Collected: 09/06/18 07:40 Received: 09/06/18 08:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Calcium
Copper
Magnesium
Nickel
Zinc
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
,Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
360.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 09/19/2018 04:36 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
ND
mg/kg
1.9
0.95
1
09/10/18 13:34
09/12/18 06:35
7440-38-2
179000
mg/kg
380
190
20
09/10/18 13:34
09/12/18 21:38
7440-70-2
14.5
mg/kg
0.95
0.48
1
09/10/18 13:34
09/12/18 06:35
7440-50-8
1400
mg/kg
19.0
0.48
1
09/10/18 13:34
09/12/18 06:35
7439-95-4
1.6
mg/kg
0.95
0.48
1
09/10/18 13:34
09/12/18 06:35
7440-02-0
297
mg/kg
1.9
0.95
1
09/10/18 13:34
09/12/18 06:35
7440-66-6
Analytical Method: SM 254OG-2011
46.1 % 0.000010 1 09/06/1817:45
Analytical Method: ASTM D2974-87
53.9 % 0.10 0.10 1 09/06/1817:36
Analytical Method: EPA 9045D
8.3 Std. Units 0.10 0.10 1 09/09/18 11:43
Analytical Method: SM 271OB-2011
423 mg/kg 0.12 0.12
1 09/19/18 09:02
Analytical Method: TKN+NO3+NO2 Calculation
1410 mg/kg 40.0 20.0
1 09/14/1815:39 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 21.3 21.3
1 09/11/1810:03 09/12/1814:30 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
1410 mg/kg 90.3 45.2
1 09/12/18 02:26 09/13/18 07:32 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.3 4.3
1 09/07/18 01:00 09/07/18 04:34
ND mg/kg 4.3 4.3
1 09/07/18 01:00 09/07/18 04:34 14797-55-8
ND mg/kg 2.2 2.2
1 09/07/18 01:00 09/07/18 04:34 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H6
N2
Page 5 of 21
Report Number: 18-254-0206
Account Number: 05734
W
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
pwic- im` 6ewr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be .rrl+ r:,r:r, 14,c -Ihvre I +arr r,i I be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or otherpublic annuren.,rrrirrid;; cuft:rout nit uu r 4.ue.r r+rrr„ ,�y0r" Agronomist Page 18 of 21
Page 2 1
aceAnalj cal"
www.pacelabs.com
October 31, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92402749
Pace Analytical Services, LLC
6701 Conference Drive
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on October 09, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Raleigh, NC 27607
(919)834-4984
A revised report is being submitted on 10/31/18 to revise the total nitrogen calculation. It was input
incorrectly.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
o-q�,'
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Pagel of 22
aceAnalytical®
r www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Sludge
Pace Project No.: 92402749
Sample: Monthly Sludge Lab ID: 92402749001 Collected: 10/09/18 07:30 Received: 10/09118 09:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Calcium
Copper
Magnesium
Nickel
Zinc
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 10/31/2018 10:01 AM
Analytical Method: EPA 601OD Preparation Method: EPA 3050B
ND
mg/kg
2.0
1.0
1
10/11/1810:23
10/12/1815:59
7440-38-2
157000
mg/kg
205
102
10
10/11/1810:23
10/15/1812:19
7440-70-2
22.7
mg/kg
1.0
0.51
1
10/11/1810:23
10/12/1815:59
7440-50-8
1650
mg/kg
20.5
0.51
1
10111/1810:23
10/12/1815:59
7439-95-4
2.1
mg/kg
1.0
0.51
1
10111/1810:23
10112/1815:59
7440-02-0
118
mg/kg
2.0
1.0
1
10/11/1810:23
10/12/1815:59
7440-66-6
Analytical
Method: SM 2540G-2011
43.6
%
0.000010
1
10/09/1817:39
Analytical Method: ASTM D2974-87
56.4 % 0.10 0.10
1 10/09/1817:37
Analytical Method: EPA 9045D
7.1 Std. Units 0.10 0.10
1 10/16/18 11:21
Analytical Method: SM 271OB-2011
540 mg/kg 0.12 0.12
1 10/22/1815:13
N2
Analytical Method: TKN+NO3+NO2 Calculation
1800 mg/kg 40.0 20.0
1 10122/1817:07 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 19.8 19.8
1 10/16/1814:29 10/1711814:18 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
1800 mg/kg 115 57.4
1 10/14/18 14:41 10/16/18 01:29 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.4 4.4
1 10117/18 14:33 10/18/18 00:09
H1
ND mg/kg 4.4 4.4
1 10/17/18 14:33 10/18/18 00:09 14797-55-8
H1
ND mg/kg 2.2 2.2
1 10/17/18 14:33 10/18/18 00:09 14797-65-0
H1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 22
Report Number: 18-284-0203
Account Number: 05734 ����� �� 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge-92402749001
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS Date Sampled: 10/9/2018 07:30:00
Date Received: 10/11/2018 00:00
Date Reported: 10/22/2018
Lab Number: 63122
Sample Id : 92402749001
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
C/N RATIO *
Carbon (TOC)
Comments:
43.10
431000
100.3
CJR
10/17/201815:59
SM-2540G
56.90
100.3
CJR
10/17/201815:59
SM-254OG
0.34
3360
250
CLP
10/19/201810:00
SM-4500-NH3C-TKN
24.90
249000
1000
DXT
10/19/2018 14:20
AOAC 955.01
53.40
534000
100.3
CJR
10/18/201816:39
SM-254OG
92
0
10/17/201815:59
CALCULATION
31.00
310000
100
10/18/201816:39
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not:
to the work, the results, or the company in any advertising, news release, or other public am
PaW« m` G06,'•'
Pauric McGroary
Agronomist Page 20 of 22
Page 3 of '-•
.'T
PaceAnalytical
www..pacelabs.com
:r
November 26, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92406635
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21
/5a'oeAna1j6ca1"
www..pacelabs.com
ANALYTICAL RESULTS
Project: Sludge
Pace Project No.: 92406635
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: Monthly Sludge Lab ID: 92406635001 Collected: 11/08/18 08:05 Received: 11/08/18 08:32 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Calcium
Copper
Magnesium
Nickel
Zinc
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
360.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 11/26/2018 11:50 AM
Analytical Method: EPA 601OD Preparation Method: EPA3050B
ND
mg/kg
1.7
0.87
1
11/09/18 12:22
11/10/18 04:02
7440-38-2
160000
mg/kg
173
86.7
10
11/09/18 12:22
11/10/18 20:28
7440-70-2
16.5
mg/kg
0.87
0.43
1
11/09/18 12:22
11/10/18 04:02
7440-50-8
1460
mg/kg
17.3
0.43
1
11/09/18 12:22
11/10/18 04:02
7439-95-4
2.1
mg/kg
0.87
0.43
1
11/09/18 12:22
11/10/18 04:02
7440-02-0
166
mg/kg
1.7
0.87
1
11/09/18 12:22
11/10/18 04:02
7440-66-6
Analytical Method: SM 2540G-2011
42.4 % 0.000010 1 11/08/1818:17
Analytical Method: ASTM D2974-87
57.6 % 0.10 0.10 1 11/08/1818:11
Analytical Method: EPA 9045D
7.4 Sid. Units 0.10 0.10
1 11/12/18 12:12
Analytical Method: SM 271 OB-2011
456 mg/kg 0.12 0.12
1 11/20/1814:44
Analytical Method: TKN+NO3+NO2 Calculation
1520 mg/kg 40.0 20.0
1 11/19/18 09:54 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 21.4 21.4
1 11111/1811:23 11/13/1813:34 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
1620 mg/kg 94.3 47.1
1 11/14/18 01:17 11/14/18 13:16 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.7 4.7
1 11/09/18 02:38 11/09/18 13:15
ND mg/kg 4.7 4.7
1 11/09/18 02:38 11/09/18 13:15 14797-55-8
ND mg/kg 2.3 2.3
1 11/09/18 02:38 11/09/18 13:15 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
N2
Page 5 of 21
Report Number: 18-317-0206
Account Number: 05734 ���1110 ON
� �� M 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge - 92406635001
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
Lab Number: 63522
Sample Id : Sludge - 92406635001
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
C/N RATIO *
Carbon (TOC)
Comments:
REPORT OF ANALYSIS
Date Sampled: 11/8/2018 08:05:00
Date Received: 11/13/2018 00:00
Date Reported: 11 /21 /2018
kESULT
RESULT
QUANTITATION
Ak
METHOD
43.30
433000
100.0
CJR
11/15/201815:30 SM-2540G
56.70
100.0
CJR
11/15/201815:30 SM-2540G
0.52
5220
250
CLP
11/19/201813:30 SM-4500-NH3C-TKN
36.20
362000
1000
DXT
11/19/2018 11:30 AOAC 955.01
52.70
527000
100.0
CJR
11/15/201815:30 SM-2540G
59
0
11/15/201815:30 CALCULATION
30.60
306000
100
11/15/201815:30 CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in vm*- o 1kin rror ur.iy :viy ii.ftur uck 1Kv nimka
to the work, the results, or the company in any advertising, news release, or other public announcements m1hrnit onroreriin rx+rp+ni;: ovrirwwi �utlii5l+l.rlrerrl.
par« it G�
Pauric McGroary
Page 19 of 21
Agronomist
Page 3 of 5
aceAnaljd cal
www.pacelabs.com
December 21, 2018
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92409891
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2018.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a, q, fU
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21
�- aceAnalj cal
www..pacelabs.com
ANALYTICAL RESULTS
Project: Sludge
Pace Project No.: 92409891
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: Monthly Sludge Lab ID: 92409891001 Collected: 12/06/18 07:55 Received: 12/06/18 10:55 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Arsenic
Calcium
Copper
Magnesium
Nickel
Zinc
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 12/21/2018 05:08 PM
Analytical Method: EPA 601OD Preparation Method: EPA3050B
ND mg/kg 1.7
0.84
1
12/14/18 09:37
12/16/18 20:41
7440-38-2
185000 mg/kg 838
419
50
12/14/18 09:37
12/17/18 13:44
7440-70-2
37.0 mg/kg 0.84
0.42
1
12/14/18 09:37
12/16/18 20:41
7440-50-8
1740 mg/kg 16.8
0.42
1
12/14/18 09:37
12/16/18 20:41
7439-95-4
1.4 mg/kg 0.84
0.42
1
12/14/18 09:37
12/16/18 20:41
7440-02-0
76.2 mg/kg 1.7
0.84
1
12/14/18 09:37
12/16/18 20:41
7440-66-6
Analytical Method: SM 2540G-2011
42.0 % 0.000010
1
12/06/1818:14
Analytical Method: ASTM D2974-87
58.0 % 0.10
0.10
1
12/06/1818:06
Analytical Method: EPA 9045D
7.4 Std. Units 0.10
0.10
1
12/13/18 07:10
Analytical Method: SM 271 OB-2011
235 mg/kg 0.12
0.12
1
12/21/1811:47
Analytical Method: TKN+NO3+NO2 Calculation
782 mg/kg 40.0
20.0
1
12/21/1811:30
7727-37-9
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
ND mg/kg 23.3
23.3
1
12/11/1816:21
12/12/1814:53
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
782 mg/kg 99.2
49.6
1
12/16/18 10:07
12/20/18 01:46
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 4.7
4.7
1
12/07/18 01:56
12/07/18 04:25
ND mg/kg 4.7
4.7
1
12/07/18 01:56
12/07/18 04:25
14797-55-8
ND mg/kg 2.3
2.3
1
12/07/18 01:56
12/07/18 04:25
14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Wt:
H3
N2
Page 5 of 21
Report Number: 18-346-0201
ON
Account Number: 05734 ���� ��.M 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge - 92409891
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
REPORT OF ANALYSIS
Date Sampled: 12/6/2018 07:55:00
Lab Number: 63900
Date Received: 12/12/2018 00:00
Sample Id : Sludge - 92409891
Date Reported: 12/21/2018
PARAMETER
RESULT
RESULT QUANTITATION
;��+a►!�
Total Solids *
43.20
432000
100.0
CJR
12/14/2018 13:57 SM-2540G
Moisture *
56.80
100.0
CJR
12/14/2018 13:57 SM-2540G
Total Kjeldahl Nitrogen
1.09
10900
250
CLP
12/19/2018 15:30 SM-4500-NH3C-TKN
Calcium Carbonate Equivalent
51.40
514000
1000
DXT
12/17/2018 14:50 AOAC 955.01
Total Volatile Solids
49.80
498000
100.0
CJR
12/14/2018 13:57 SM-2540G
C/N RATIO *
27
0
12/14/2018 13:57 CALCULATION
Carbon (TOC) *
29.00
290000
100
12/14/2018 13:57 CALCULATION
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, it ;i •ri :, ?•1. 41-1�11 . r - ,1i ;rJj'
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
porza mW 60wr
Pauric McGroary
Page 19 of 21
Agronomist
Page 3 of 5
ff]SUMMIAt
ENVinL"M EN'A_TECHNOE04=1F.S.1NC
AnsNtic�i �:�bc+�atc�rles
September 17, 2018
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htti�:llwww.settek.com
Karen Bellamy
Cascades Tissue Group - North Carolina Inc
805 Midway Road
Rockingham, NC 28379
TEL: 910-895-4033
FAX: 910-895-9887
RE: Sludge
Dear Karen Bellamy:
Order No.: 18081887
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/31/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
�Ie
Holly Florea
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH200001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 28
Summit Environmental Technologies, Inc. Case Narrative
SUMMIi. 3310 Win St.
ENVt OMMEN-t4L TECHNGEOGIF$,M Cuyahoga Falls, Ohio44223 WO#: 18081887
TEL: (330) 253-8211 FAX. (330) 253-4489 Date 9/1 81887
Website: hJt ://www.seuek.com
CLIENT: Cascades Tissue Group - North Carolina Inc
Project: Sludge
WorkOrder Narrative:
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt
Form, and other applicable forms as necessary. All documents contain the Summit Environmental
Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
18081887-OOIA SVOC-BNA_TCLP(8270D): Possible low bias in the associated samples for 1,4-
Dichlorobenzene and Hexachloroethane due to low recovery in the LCS.
18081887-OOIA TCLP-SVOC-HERB_TCLP(8151): Surrogate recovery unable to be reliably evaluated
due to dilution; Sample diluted due to matrix; Reporting Limits adjusted accordingly.
Analytical Sequence QC Notes:
CCV 40ng 58-341 SVOC-MSTR_S(8270): The CCV (Batch R88555) exhibited high recovery for
many analytes; associated samples are ND for all analytes of interest.
Original
Page 2 of 28
SUMM11
,
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htw.-11Www.settek.com
CLIENT: Cascades Tissue Group - North Carolina Inc
Project: Sludge
Case Narrative
WO#: 18081887
Date: 9/17/2018
CCV 40ng S8-341 SVOC-MSTR_S(8270): The CCV (Batch R88555) exhibited low recovery for
Hexachlorocyclopentadiene, Hexachlorocyclopentadiene is not a selected analyte in the associated data.
LCS-33748 SVOC-BNA_TCLP(8270): LCS-33748(R88555) exhibited low recovery for 1,4-
Dichlorobenzene and Hexachloroethane. Possible low bias in the associated samples for 1,4-
Dichlorobenzene and Hexachloroethane.
PEST CCV 50OPPB svoc-CPEST_npw(8081): The CCV (Batch R88630) exhibited low recovery for
Methoxychlor. Possible low bias for Methoxychlor in the associated samples.
MB-33731 tclp-svoc-CPEST_TCLP(8081): Possible low bias for Methoxychlor due to low recovery in
the CCV.
8151 CCV 500 ug/ svoc-herb_npw(8151): 8151 CCV (Batch R88676) exhibits high recoveries for all
analytes except low for MCPA and MCPP. All samples are ND.
LCS-33790 TCLP-SVOC-HERB_TCLP(8151): The LCS (Batch 33790/R88676) exhibited high
recovery for 2,4-D. The associated samples are ND for 2,4-D.
8151 CCV 500 ug/ svoc-herb_npw(8151): 8151 CCV (Batch R88676) exhibits high recoveries for all
analytes except low for MCPA and MCPP. All samples are ND.
TCLP BLK 9-5-18 TCLP-SVOC-HERB_TCLP(8151): the TCLP Method Blank exhibtied high
recovery for Surrogate: DCAA. The Blank is ND for all analytes of interest.
Original
Page 3 of 28
Sumrff
ENVI'r10WEN7A_ TECMNpt OGIr-3, INC
Xlns+ytleal Labomfartet
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httrr:1Avww.settek.com
CLIENT: Cascades Tissue Group - North Carolina Inc
Project: Sludge
Lab SamplelD Client Sample ID
18081887-001 Sludge
Tag No Date Collected
8/28/2018 6.15.00 AM
Workorder
Sample Summary
WO#: 18081887
17-Sep-18
Date Received Matrix
8/31/2018 7:55:00 PM Solid
Page 4 of 28
Summit Environmental Technologies, Inc. WO#: 18081887
SUMMI : 3310 Win St.
EP#Vii GNWENTA_ TECHNGt 0GIFS, INC Cuyahoga Falls, Ohio 44223 Date Reported: 9/17/2018
TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Cascades Tissue Group - North Carolina I
Website: htti,://www.settek.com Address: 805 Midway Road
Rockingham NC 28379
Received: 8/31 /2018
Project#: Sludge
TCLP Metals Analysis (SW1311/6010)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge 001 8/28/2018 TCLP Arsenic(As) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Barium(Ba) 5.00 ND mg/L Solid EPA 6010 1 100 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Cadmium(Cd) 0.100 ND mg/L Solid EPA 6010 1 1.00 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Chromium(Cr) 0.200 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Lead(Pb) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Selenium(Se) 0.0500 ND mg/L Solid EPA 6010 1 1.00 9/6/2018 KMO
D
Sludge 001 8/28/2018 TCLP Silver(Ag) 0.500 ND mg/L Solid EPA 6010 1 5.00 9/6/2018 KMO
D
TCLP Mercury Analysis (SW1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
Sludge 001 8/28/2018 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470 A 1 0.200 9/7/2018 DNS
TCLP Pesticides Analysis (SW1311/8081)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge
001
8/28/2018 Chlordane, total
0.0200
ND mg/L
Solid
EPA 8081 B
10
0.0300
9/12/2018
RIS
Sludge
001
8/28/2018 Toxaphene
0.200
ND mg/L
Solid
EPA 8081 B
10
0.500
9/12/2018
RIS
Sludge
001
8/28/2018 Endrin
0.00200
ND mg/L
Solid
EPA 8081 B
10
0.0200
9/12/2018
RIS
Sludge
001
8/28/2018 gamma-BHC
0.00200
ND mg/L
Solid
EPA 8081 B
10
0.400
9/12/2018
RIS
Sludge
001
8/28/2018 Heptachlor
0.00200
ND mg/L
Solid
EPA 8081 B
10
0.00800
9/12/2018
RIS
Sludge
001
8/28/2018 Heptachlor epoxide
0.00200
ND mg/L
Solid
EPA 8081 B
10
0.00800
9/12/2018
RIS
Sludge
001
8/28/2018 Methoxychlor
0.00200
ND mg/L
Solid
EPA 8081 B
10
10.0
9/12/2018
RIS
Sludge
001
8/28/2018 Surr:TCMX
10-119
55.7 %Rec
Solid
EPA 8081B
10
9/12/2018
RIS
Sludge
001
8/28/2018 Surr: DCB
10-119
79.5 %Rec
Solid
EPA 8081B
10
9/12/2018
RIS
TCLP Herbicides Analysis (SW1311/8151)
Client ID#
Lab H)# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl Run
Analyst
Sludge
001 8/28/2018 2,4-D
10.0 ND mg/L
Solid
EPA 8151 A
10
10.0 9/13/2018
MES
Sludge
001 8/28/2018 2,4,5-TP
5.00 ND mg/L
Solid
EPA 8151 A
10
1.00 9/13/2018
MES
Sludge
001 8/28/2018 Surr: DCAA
20-140 334 %Rec
Solid
EPA 8151 A
10
9/13/2018
MES
Page 5 of 28
EN%'!n0N,VEN7A-TECHNOL001:3, W
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: ht+r,://www.settek.com
WO#:
18081887
Date Reported:
9/17/2018
Company:
Cascades Tissue Group - North Carolina I
Address:
805 Midway Road
Rockingham NC 28379
Received:
8/31/2018
Project#:
Sludge
TCLP Volatiles Analysis
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge
001
8/28/2018 1,1-Dichloroethene
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.700
9/6/2018
MES
Sludge
001
8/28/2018 1,2-Dichloroethane
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.500
9/6/2018
MES
Sludge
001
8/28/2018 MEK
0.250
0.558 mg/L
Solid
EPA 8260 B
10
200
9/6/2018
MES
Sludge
001
8/28/2018 Benzene
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.500
9/6/2018
MES
Sludge
001
8/28/2018 Carbon tetrachloride
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.500
9/6/2018
MES
Sludge
001
8/28/2018 Chlorobenzene
0.0500
ND mg/L
Solid
EPA 8260 B
10
100
9/6/2018
MES
Sludge
001
8/28/2018 Chloroform
0.0500
ND mg/L
Solid
EPA 8260 B
10
6.00
9/6/2018
MES
Sludge
001
8/28/2018 Tetrachloroethene
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.700
9/6/2018
MES
Sludge
001
8/28/2018 Trichloroethene
0.0500
ND mg/L
Solid
EPA 8260 B
10
0.500
9/6/2018
MES
Sludge
001
8/28/2018 Vinyl chloride
0.0200
ND mg/L
Solid
EPA 8260 B
10
0.200
9/6/2018
MES
Sludge
001
8/28/2018 Surr: 4-
70-130
98.8 %Rec
Solid
EPA 8260 B
10
9/6/2018
MES
Bromofluorobenzene
Sludge
001
8/28/2018 Surr:
70-130
109 %Rec
Solid
EPA 8260 B
10
9/6/2018
MES
Dibromofluoromethane
edge
001
8/28/2018 Surr: Toluene-d8
70-130
104 %Rec
Solid
EPA 8260 B
10
9/6/2018
MES
Page 6 of 28
I
Client ID#
Summit Environmental Technologies, Inc. WO#:
- 3310 Win St.
ENV,F ONIIVEN-A-' TECHNOL:OOrS, INC, Cuyahoga Falls, Ohio 44223 Date Reported:
TEL: (330) 253-8211 FAX.- (330) 253-4489 Company:
Website: htt,,://www.settek.com Address:
Received:
Project#:
TCLP Semi-Volatiles Analysis (SW1311/8270)
Lab ID# Collected Analyte Rep Lmt Result Units Matrix
18081887
9/1712018
Cascades Tissue Group - North Carolina I
805 Midway Road
Rockingham NC 28379
8/31/2018
Sludge
Method DF RegLv1 Run Analyst
Sludge
001
8/28/2018 1,4-Dichlorobenzene
0.0800
ND mg/L
Solid
EPA 8270
2
7.50
9/10/2018
BJH
D
Sludge
001
8/28/2018 2,4,5-Trichlorophenol
0.200
ND mg/L
Solid
EPA 8270
2
400
9/10/2018
BJH
D
Sludge
001
8/28/2018 2,4,6-Trichlorophenol
0.200
ND mg/L
Solid
EPA 8270
2
2.00
9/10/2018
BJH
D
Sludge
001
8/28/2018 2,4-Dinitrotoluene
0.0400
ND mg/L
Solid
EPA 8270
2
0.130
9/10/2018
BJH
D
Sludge
001
8/28/2018 o-Cresol
0.200
ND mg/L
Solid
EPA 8270
2
9/10/2018
BJH
D
Sludge
001
8/28/2018 m/p-Cresol(s)
0.200
ND mg/L
Solid
EPA 8270
2
9/10/2018
BJH
D
Sludge
001
8/28/2018 Cresols, Total
4.00
ND mg/L
Solid
EPA 8270
2
200
9/10/2018
BJH
D
Sludge
001
8/28/2018 Hexachloro-1,3-
0.0160
ND mg/L
Solid
EPA 8270
2
0.500
9/10/2018
BJH
butadiene
D
.fudge
001
8/28/2018 Hexachlorobenzene
0.0400
ND mg/L
Solid
EPA 8270
2
0.130
9/10/2018
BJH
D
Sludge
001
8/28/2018 Hexachloroethane
0.0800
ND mg/L
Solid
EPA 8270
2
3.00
9/10/2018
BJH
D
Sludge
001
8/28/2018 Nitrobenzene
0.0800
ND mg/L
Solid
EPA 8270
2
2.00
9/10/2018
BJH
D
Sludge
001
8/28/2018 Pentachlorophenol
0.200
ND mg/L
Solid
EPA 8270
2
100
9/10/2018
BJH
D
Sludge
001
8/28/2018 Pyridine
0.200
ND mg/L
Solid
EPA 8270
2
5.00
9/10/2018
BJH
D
Sludge
001
8/28/2018 Sum 2-Fluorophenol 10-109
26.0 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
D
Sludge
001
8/28/2018 Surr: Phenol-d6
10-109
27.0 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
D
Sludge
001
8/28/2018 Surr: Nitrobenzene-
19-120
42.3 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
d5
D
Sludge
001
8/28/2018 Surr: 2,4,6-
10-120
31.1 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
Tribromophenol
D
Sludge
001
8/28/2018 Surr: 2-
22-117
45.4 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
Fluorobiphenyl
D
Sludge
001
8/28/2018 Surr: p-Terphenyl-
34-116
84.8 %Rec
Solid
EPA 8270
2
9/10/2018
BJH
d14
D
Page 7 of 28
Summit Environmental Technologies, Inc. Analytical Report
SUMMOT 3310Win St.
ENVOOM'TENva, TECHNt L OGISS, INC. Cuyahoga Falls, Ohio 44223 (consolidated)
TEL: (330) 253-8211 FAX: (330) 253-4485 WO#: 18081887
Website: jUp://www.settek.com Date Reported: 9/17/2018
CLIENT: Cascades Tissue Group - North Carolina Inc Collection Date: 8/28/2018 6:15:00 AM
Project: Sludge
Lab ID: 18081887-001 Matrix: SOLID
Client Sample ID Sludge
Analyses Result PQL Qual Units DF Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg 1
9/6/2018 1:05:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
9/6/2018 2:30:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: VVK
PH (SW9045D)
pH 7.1
s.u.@22.3C 1
9/5/2018 11:56:44 AM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
9/6/2018 1:05:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 8 of 28
sul"Mur--
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
llvt+liti}Np�1C Fd71L rrotiaut7!( ;cc tit
Cuyahoga Falls, Ohio 44223
WO#: 18081887
.. ..
TEL: (330) 253-8211 FAX. (330) 253-4489
Website: htt;):Ilwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33728
'ample ID mb-33728
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 9/5/2018
RunNo: 88459
client ID: PBS
Batch ID: 33728
TestNo: SW8260B SW1311M
Analysis Date: 9/612018
SegNo: 1723507
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0,0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
474
Surr: Dibromofluoromethane
538
Surr: Toluene-d8
522
500.0 94.8 70 130
500.0 108 70 130
500.0 104 70 130
'ample ID Ics 13782/13818
SampType: LCS
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 88459
;lient ID: LCSS
Batch ID: 33728
TestNo: SW8260B SW1311M
Analysis Date: 9/6/2018
SegNo: 1723515
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0190 0.00500
1,2-Dichloroethane
0.0190 0.00500
MEK
0.0922 0.0250
Benzene
0.0187 0.00500
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
P
Second column confirmation exceeds
0.0200 0 94.9
79.4
0.0200 0 94.9
73.6
0.100 0 92.2
55.1
0.0200 0 93.7
73.1
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
131
137
163
132
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 9 of 28
' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
S U M M of 3310 Win St.
F-XV100NhtENTAL TECTI N01 0-31r%, N% Cuyahoga Falls, Ohio 44223
WO#: 18081887
Antr/srticat L8bOrattrrt6s TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httn://www.settek.com 17-Sep-18
Client: Cascades Tissue Group - North Carolina Inc
Project: Sludge
BatchID: 33728
iample ID Ics 13782113818
SampType: LCS
TestCode: tclp-voc-MST Units: mg/L
Prep Date:
RunNo: 88459
client ID: LCSS
Batch ID: 33728
TestNo: SW8260B SW1311M
Analysis Date: 9/6/2018
SegNo: 1723515
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.0192
0.00500
0.0200
0
96.1
63.7
139
Chlorobenzene
0.0190
0.00500
0.0200
0
95.0
72.3
139
Chloroform
0.0190
0.00500
0.0200
0
94.8
79.3
129
Tetrachloroethene
0.0189
0.00500
0.0200
0
94.5
56.2
187
Trichloroethene
0.0178
0.00500
0.0200
0
89.1
64.1
138
Vinyl chloride
0.0249
0.00200
0.0200
0
124
22.1
147
Surr: 4-Bromofluorobenzene
50.6
50.00
101
80.4
126
Surr: Dibromofluorom ethane
52.9
50.00
106
70.3
125
Surr: Toluene-d8
51.3
50.00
103
82
117
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 28
Summit Environmental Technologies, Inc.
SUMM161- 3310 Win St.
QC SUMMARY REPORT
VKA(l1t0NldEtdTAL TEt:1IN01 OGICS, lo'
Cuyahoga Falls, Ohio 44223
• ..�- ••. TEL: (330) 253-8211 FAX:(330) 253-4489
WO#: 18081887
Website: httu://www.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID:
33744
Sample ID
MB-33744 SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date:
9/7/2018
RunNo: 88486
Client ID:
PBS Batch ID: 33744
TestNo: SW7470A SW7470A
Analysis Date:
9/7/2018
SegNo: 1724470
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND
0.00200
Sample ID
LCS-33744 SampType: LCS
TestCode: HG TCLP(74 Units: PPM
Prep Date:
9/7/2018
RunNo: 88486
Client ID:
LCSS Batch ID: 33744
TestNo: SW7470A SW7470A
Analysis Date:
91712018
SegNo: 1724471
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00406
0.00200 0.00400 0
102 80
120
Sample ID 18081785-007AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 91712018
RunNo: 88486
Client ID: Batch=
Batch ID: 33744
TestNo: SW7470A SW7470A
Analysis Date: 9/712018
SegNo: 1724478
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00639 0.00200 0.00400 0.00160 120 75 125 0.00656 2.63 20
Sample ID 18081785-007AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 9/7/2018
RunNo: 88486
Client ID: BatchQC
Batch ID: 33744
TestNo: SW7470A SW7470A
Analysis Date: 9/7/2018
SegNo: 1724494
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00656 0.00200 0.00400 0.00160 124 75
Qualifiers: * Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
125
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 11 of 28
uSm MI-1
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EN0it-)Nh104TAL TEC1lN01 tltt•.F5, '•'
Cuyahoga Falls, Ohio 44223
WO#: 18081887
TEI,: (330) 253-8211 FAX.- (330) 253-4489
Website: httu.11www.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33744
Sample ID 18081785-007AMS SampType: MS TestCode: HG TCLPl74 Units: PPM Prep Date: 9/7/2018 RunNo: 88486
Client ID: BatchQC Batch ID: 33744 TestNo: SW7470A SW7470A Analysis Date: 9/7/2018 SegNo: 1724494
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 28
SUMMI'.
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Li44+11t }NP�1CNiAL is"I 741Ut7I f}y,IcS •, -
Cuyahoga Falls, Ohio 44223
W04: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httl,r://www.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33790
Sample ID MB-33790
SampType: MBLK
TestCode: TCLPSVOC- Units: mg/L
Prep Date: 911012018
RunNo: 88710
Client ID: PBS
Batch ID: 33790
TestNo: SW8161A SW8151A
Analysis Date: 9/1312018
SegNo: 1733066
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00
0 0
d
2,4,5-TP
ND 0.500
0 0
d
Surr: DCAA
333 500.0
66.5 20 140
m
Sample ID LCS-33790
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/10/2018
RunNo: 88710
Client ID: LCSS
Batch ID: 33790
TestNo: SW8151A SW8151A
Analysis Date: 9/13/2018
SegNo: 1733067
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 125
62.6
125
2,4,5-TP
ND
0.500 0.500
0 95.3
52.5
128
Surr: DCAA
532
500.0
106
20
140
Sample ID 18081870-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/10/2018
RunNo: 88710
Client ID: BatchQC
Batch ID: 33790
TestNo: SW8151A SW8151A
Analysis Date: 9/13/2018
SegNo: 1733077
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: DCAA
ND 10.0
ND 5.00
1170
0.500 0 149 37 105
0.500 0 106 38 106
500.0 233 20 140
S
S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 28
sum'M101
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EIv4t11tt7Nli1E1J7ltL riC]EQJ(71 CF✓aiF"i, n i.
Cuyahoga Falls, Ohio 44223
WO#: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htty://www.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33790
>ample ID 18081870-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 911012018
RunNo: 88710
;lient ID: BatchQC
Batch ID: 33790
TestNo: SW8151A SW8151A
Analysis Date: 9/13/2018
SegNo: 1733082
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 10.0 0.500 0 142 37 105 0 0 30 RS
2,4,5-TP ND 5.00 0.500 0 95.0 38 106 0 0 30
Surr: DCAA 1090 500.0 217 20 140 0 S
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 14 of 28
to ,
Summit Environmental Technologies, Inc.
3310 Win St.
QC,
MA Y REPORT
SUMMARY
EN4fli4a"1,N!d[NTAL TCCi1tiNol l4F; r ; N
Cuyahoga Falls, Ohio 44223
WO#: 18081887
,4.nry° !cat
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: brtf,:Ilwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33790
Sample ID MB-33790
SampType: MBLK
TestCode: TCLPSVOC- Units: mg/L
Prep Date: 9/1012018
RunNo: 88676
Client ID: PBS
Batch ID: 33790
TestNo: SW8161A SW8151A
Analysis Date: 9/12/2018
SegNo: 1731414
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 357 500.0 71.5 20 140
Sample ID LCS-33790
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/10/2018
RunNo: 88676
Client ID: LCSS
Batch ID: 33790
TestNo: SW8151A SW8161A
Analysis Date: 9/12/2018
SegNo: 1731416
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
ND
1.00 0.500
0 125
62.6
125 S
2,4,5-TP
ND
0.500 0.500
0 90.0
52.5
128
Surr: DCAA
487
500.0
97.3
20
140
Sample ID 18081870-001AMS
SampType: MS
TestCode: TCLPSVOC- Units: mg/L
Prep Date: 9110/2018
RunNo: 88676
Client ID: BatchQC
Batch ID: 33790
TestNo: SW8161A SW8151A
Analysis Date: 911212018
SegNo: 1731416
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 10.0
5.00 0 44.3 37
105
2,4,5-TP
ND 5.00
5.00 0 10.3 38
106
S
Surr: DCAA
1250
5000 25.0 20
140
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
MC
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
J Analyte detected below quantitation limits
ND Not Detected
M
O
Manual Integration used to determine
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 28
�J m M 111
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EJK%fl1t(]NtdEt4TAL I_r nvrli i MrS;, I.r
Cuyahoga Falls, Ohio 44223
W04: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-4489
Wehsite: htto•/fwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: 33790
sample ID 18081870-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/10/2018
RunNo: 88676
;lient ID: BatchQC
Batch ID: 33790
TestNo: SW8151A 5W8151A
Analysis Date: 9/12/2018
SegNo: 1731417
lnalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 10.0 5.00 0 30.5 37 105 0 0 30 RS
2,4,5-TP ND 5.00 5.00 0 9.25 38 106 0 0 30 S
Surr: DCAA 879 5000 17.6 20 140 0 S
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 16 of 28
1=Wni
S U M M I
Summit Environmental Technologies, St. Inc.
3310 Win St
QC SUMMARY REPORT
E6tVIOONtotENTAL 3EC.O+N01 (1GiFS, '••
Cuyahoga Falls, Ohio 44223
WO#: 18081887
M
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: httn://www.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88403
Sample ID LCS-R88403
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@22.2C
Prep Date:
RunNo: 88403
Client ID: LCSW
Batch ID: R88403
TestNo: SW9045D
Analysis Date: 9/512018
SegNo: 1722113
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 100 98.6 101.4
Sample ID CHECK 7
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@22.1C
Prep Date:
RunNo: 88403
Client ID: LCSW
Batch ID: R88403
TestNo: SW9045D
Analysis Date: 9/5/2018
SegNo: 1722132
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Qualifiers: * Value exceeds Maximum Contaminant Level,
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 17 of 28
S,ITSummit
Environmental Technologies, Inc.
3310WinSt.
QC SUMMARY REPORT
EF,'ktlltONIAE14TAL ir.CiiNOt,kl ; I,, Nr,
Cuyahoga Falls, Ohio 44223
WO#: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htto:llwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88429
Ignitability 7.08 7.240 0 97.8 70 130
Ignitability ; not propagate 0 0 20
Sample ID 18081886-001ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 88429
Client ID: BatchQC Batch ID: R88429 TestNo: SW1030 Analysis Date: 9/6/2018 SegNo: 1722773
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability not propagate 0 0 20
Sample ID 18081887-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 88429
Client ID: Sludge
Batch ID: R88429
TestNo:
SW1030
Analysis Date: 91612018
SegNo: 1722775
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0 0 20
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 18 of 28
sumown
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Eh4"IikN6�1�1dTALfieYt7t7tc3Cir, 'ry
Cuyahoga Falls, Ohio 44223
WO#: 18081887
TEL: (330) 253-8211 FAX. (330) 253-4489
Website: httn:1Avww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88429
Sample ID 18081887-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 88429
Client ID: Sludge
Batch ID: R88429
TestNo: SW1030
Analysis Date: 9/6/2018
SegNo: 1722775
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 18090063-004ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 88429
Client ID: Batch=
Batch ID: R88429
TestNo: SW1030
Analysis Date: 9/6/2018
SegNo: 1722777
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability ; not propagate 0 0 20
Sample ID 18090063-004ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 88429
Client ID: BatchQC
Batch ID: R88429
TestNo: SW1030
Analysis Date: 9/6/2018
SegNo: 1722778
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability not propagate 0 0 20
Sample ID 18090063-005ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 88429
Client ID: Batch=
Batch ID: R88429
TestNo: SW1030
Analysis Date: 9/6/2018
SegNo: 1722780
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability ; not propagate 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 28
SUMMINI
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
h1�111JNh1CNT1tL rt rt#tt71 [i .If ;, Ns,
Cuyahoga Falls, Ohio 44223
WO#: 18081887
TEL: (330) 253-8211 FAX. (330) 253-4489
Website: htta://immsettek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88429
Sample ID 18090063-005ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 88429
.',lient ID: Batch=
Batch ID: R88429
TestNo: SW1030
Analysis Date: 9/6/2018
SegNo: 1722781
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
; not propagate
0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 20 of 28
S umiw1�
Summit Environmental Technologies, Inc.r--Zirdou
3310WinSt.
QC SUMMARY REPORT
"00]
F.FIt�IC?th11d1dTal. rEG)t.N(7tC C,iF,
Cuyahoga Falls, Ohio 44223
WO#: 18081887
r1,
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: hgg:llwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88479
Sample ID MB-R88479
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 88479
Client ID: PBS
Batch ID: R88479
TestNo: SW9014
Analysis Date: 9/6/2018
SegNo: 1724355
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R88479
SampType: LCS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 88479
Client ID: LCSS
Batch ID: R88479
TestNo: SW9014
Analysis Date: 9/612018
SegNo: 1724366
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.66 0.500 10.00 0 96.6 85 110
Sample ID RLCheck
SampType: RLC
TestCode: Cyanide,Rea Units: mglKg
Prep Date:
RunNo: 88479
Client ID: BatchQC
Batch ID: R88479
TestNo: SW9014
Analysis Date: 9/6/2018
SegNo: 1724358
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
0.552 0.500 0.5000 0 110 50 150
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 28
sumra1
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
C 01ti7Nt004TAL rCCC++Hn1 cta ". Hr.
Cuyahoga Falls, Ohio 44223
WO#: 18081887
Anitty+ticat Labwatorles
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htte:1Avww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
SatchID: R88490
Sample ID MB-R88490 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 88490
Client ID: PBW Batch ID: R88490 TestNo: SW9034 Analysis Date: 9/6/2018 SegNo: 1724579
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R88490
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 88490
Client ID: LCSW
Batch ID: R88490
TestNo: SW9034
Analysis Date: 916/2018
SegNo: 1724580
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4630 25.0 4800 0 96.5 85 115
Sample ID 18090063-002AMS
SampType: MS
TestCode: Sulf[de,React Units: mg1L
Prep Date:
RunNo: 88490
Client ID: BatchQC
Batch ID: R88490
TestNo: SW9034
Analysis Date: 9/6/2018
SegNo: 1724582
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4610 25.0 4800 0 96.0 75 125 W
NOTES:
Sample was received not meeting proper temperature requirements.
Sample ID 18090063-002AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 88490
Client ID: BatchQC
Batch ID: R88490
TestNo: SW9034
Analysis Date: 9/6/2018
SegNo: 1724583
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 22 of 28
SUMMIMI
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EPWIlcaSNIAENTtlt_ Ti:T:iiNO[L G2r!;, Nr:
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 18081887
Website: htty:llwww.settek.com
17-Sep-18
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Sludge
BatchID: R88490
'ample ID 18090063-002AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 88490
;lient ID: BatchQC
Batch ID: R88490
TestNo: SW9034
Analysis Date: 9/6/2018
SegNo: 1724583
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4720 25.0 4800 0 98.3 75 125 4610 2.36 30 W
NOTES:
Sample was received not meeting proper temperature requirements.
Qualifiers: * Value exceeds Maximum Contaminant Level,
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 28
Summit Environmental Technologies, In SUMM 3310 Win Qualifiers and Acronyms
j
ENVItIOP4"IEN'A�-TECHNOLtr)GIf INC Cuyahoga Falls, Ohio 442: WO#: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-442
Website: ht0.-11Www.settek.co Date: 9/17/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+),
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 24 of 28
S 'T Summit Environmental Technologies, Inc. DATES REPORT
3310 Win St.
l:NtV111ONi404TAL TE-CHN01 0017 :„ Nr Cuyahoga Falls, Ohio 44223
"Btor�es WO#: 18081887
TEL: (330) 253-8211 FAX.- (330) 253-4485
Website: hgE://www.settek.com 17-Sep-18
Client: Cascades Tissue Group - North Carolina Inc
Project: Sludge
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
18081887-OOIA Sludge 8/28/2018 6:15:00 AM Solid Ignitability of Solids (SW-846: 1030)
9/6/2018 2:30:00 PM
pH (SW9045D)
9/5/2018 11:56:44 AM
Reactive Cyanide (9014/7.3.3.2)-Solid
9/6/2018 1:05:00 PM
Reactive Sulfide (9034)/73.4.2
9/6/2018 1:05:00 PM
TCLP Herbicides Analysis (SW1311/89/5/2018 6:00:00 PM
9/10/2018 11:45:00 AM
9/13/2018 8:14:00 PM
TCLP Herbicides Analysis (SW1311/89/5/2018 6:00:00 PM
9/12/2018 9:22:00 PM
TCLP Mercury Analysis (SW 1311/7479/5/2018 6:00:00 PM
9/7/2018 10:00:00 AM
9/7/2018 2:31:00 PM
TCLP Mercury Analysis (SW 1311/7479/5/2018 6:00:00 PM
9/7/2018 10:00:00 AM
9/7/2018 2:31:00 PM
TCLP Metals Analysis (SW 1311/6010 9/5/2018 6:00:00 PM
9/6/2018 12:15:00 PM
9/6/2018 7:24:00 PM
TCLP Pesticides Analysis (SW1311/8(9/5/2018 6:00:00 PM
9/6/2018 10:15:00 AM
9/12/2018 1:45:00 AM
TCLP Semi-Volatiles Analysis 9/5/2018 6:00:00 PM
9/7/2018 11:30:00 AM
9110/2018 7:41:00 PM
(SW 1311 /8270)
TCLP Volatiles Analysis
9/5/2018 6:00:00 PM
9/6/2018 8:04:00 PM
Original
Page 25 of 28
SUMM111-
Summit Environmental Technologies, Inc. Accreditation Program
3310 Win St. Anal tes Report
ENVIRO+rNIEN'AL TECMN01OMFS, 11YC Cuyahoga Falls, Ohio44223 Y p
4J16f)4l-tt0 t.ubrrtgtort+ I TEL: (330) 253-8211 FAX.- (330) 253-4485 WO#: 18081887
Website: http://www.settek.com 17-Sep-18
Client: Cascades Tissue Group - North Carolina Inc State: NW
Project: Sludge Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
18081887-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
11
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
11
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Solid
TCLP Herbicides Analysis (SWI311/8151)
2,4-D
A
Solid
TCLP Herbicides Analysis (SWI311/8151)
DCAA
A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
2Z.3:3 4,4 ,5,5',6,6'-
A
Decachlornbiphernyl
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Key Key
NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Page 1 of 2
Original #1
0
T Summit Environmental Technologies, Inc. Accreditation Program
3310 Win St. Anal te5 Report
ENVIFiONr.tEN-tt_TECHNGI7CIf_S, INC; Cuyahoga Falls, Ohio44223 Y p
ro5rtfi TEL: (330) 253-8211 FAX: (330) 253-4485 WO#: 18081887
Website: htt :Ilwww.settek.com 17-Sep-18
Client: Cascades Tissue Group - North Carolina Inc State: NW
Project: Sludge Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
18081887-OOIA Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
Nitrobenzene-d5
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-&
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
p-Terphenyl-d14
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
4-QTomolluorobcrizme
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Dibromofluoromethane
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Toluene-d8
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Key Key
NC_WW_SCM A Accredited NC_WW_SCM U Unavailable
Page 2 of 2
Original #1
n1 nii il■ g?e Rv% 1
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E SUMMIT Analysis Request / Chum of Custody
LN-41ROMMLNTAt TECt#NOk r.M-S. INC h'r ulitntii E nl'a[trttitrenhrl Ic,clurulcr rtti Inc, i.1y41.miv
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Page 1 of 1
Summit Environmental Technologies, Inc.
mom 1 -1 3310 Win St.
ENIVAON,VE147A_TECH NCILO IF$,IN Cuyahoga Falls, Ohio44223 Sample Log -In Check List
du; TEL: (330) 253-8211 FAX. (330) 253-4489
Website: htq!:11www.settek.com
Client Name: CAS-NC-28379 Work Order Number: 18081887 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Brian J. Fackelman
Chain of Custod
1. Is Chain of Custody complete?
2. How was the sample delivered?
Loq In
3. Coolers are present?
8/3112018 7:55:00 PM
8/31/2018 10:01:54 PM
9/5/2018 10:52:47 AM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes W]
Summit
Yes ❑�/
Yes d❑
Yes ❑
Signed By:
Yes d❑
Yes ❑d
Yes d❑
Yes d❑
Yes
Yes ❑
Yes ❑
Yes ❑
Yes ❑d
�.ik•Fk.7i,
1�1.ra •6',�r,
No ❑ Not Present ❑
No ❑ NA ❑
No ❑
No ❑ Not Present ❑d
No ❑ NA ❑
No ❑ NA ❑
No ❑
No ❑
No ❑
No NA ❑
No ❑ No VOA Vials ❑�
No ❑�
No ❑
Yes ❑d No ❑
Yes ❑ No ❑d
Yes ❑�/ No ❑
Yes ❑
No ❑ NA W
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cllient may need contacted on what TCLP is needed, logged full per past.
Cooler Information
Cooler No I Temp °C Condition I Seal Intact 1 Seal No Seal Date Signed B
1 13.5 Goodl Not Present'
Page 28 of 28
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Cascades Tissue Group -North Carolina, a division of WQ0009477
Cascades Holding US Inc. WQ Permit Number:
WWTP Name:
NPDES Number:
`Monitoring Period: From 1/1/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑ Alterative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑
Alternative 6
...........
If applicable to alternative performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray❑
Gamma Ray ❑
Pasteurization ❑
- . ........
'
Class B:
Alternative 1 ❑
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑
Ai Drying❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
.I -
..... ................................_........_.........................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
l um ber o
Excee-
dences
Frequency
of Analysis
le
SampTech-
Type
na ytica
Minimuir
Geo. Mean
Maxim u
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
N/A
N/A
CFU
N/A
N/A
1000 mpn per gram
of total solid (dry
weight)
N/A
N/A
,Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
N/A/
N/A
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
jAlt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
or "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
Nattraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Karen V. Bellamy Environmental Manager Duke Goodwin Project Manager
Preps r Name
/and! Tit e (type or print) Land Ter �n and Title (if applicable)(type or p in-71
�w (/ -Z/SM
Signature of Preparer Date Signature of`i.and Applier (if applicable) ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)
(W
Cascades
Date: Feb 12, 2019
Cascades Tissue Group - North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, Post Office Box 578
Rockingham, NC 28380 USA
Phone: (910) 895-4033 Fax: (910) 895-9887
From: Karen Bellamy
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
Po Box 578 805 Midway Rd.
Rockingham, NC 28380
Phone 1-910-895-4033-Ext 2280
Fax 1-910-895-9887
Email: Karen _Bellam @Cascades.com
Permit: WQ0009477
Subject: Fecal Testing
Cascades Material is a lime material, so we don't perform vector reduction.
Should your office have any question please contact me at the above numbers or email.
Karen V. Bellamy
Environmental Manager
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.