WQ0018525_Residual Annual Report 2018_20190221

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0018525
SUBMITTAL DATED: 2/20/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address* Phone Number*
[e-mail] 3363121396
Project Information
Application Type*
r New
r Renewal
r Annual Report
Permit Type *
r Wastewater Irrigation
r Other Wastewater
• Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor
N/A
Permit Number*
WQ0018525
Reviewer*
Troy Doby
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Permittee* Steven M. Barnes
Facility Name * Barnes Environmental Waste and Hauling, Inc.
County* Carteret
Please provide comments/notes on your current submittal below.
Barnes Environmental Waste and Hauling, Inc. - 2018 Annual Report WQ0018525
Please attach all information required or requested for this submittal to be review here.
Barnes Environmental Waste and Hauling 2018
7.07MB
Annual Report - NCDEQ.pdf
Application Form Engineering Rans, Specifications, Calculations, Etc.)

For nein and modification permit applications, the paper copy is required to be subrmtted to the
Division- Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follmtLring=
• Application Farm
• All rulevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extra set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
T:di shall ae mailed to the followins aPrl-: s:
By pc­lal ser- lce:
Divisron o= % ater Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 2.7699-1613
By Courier/Special Delivery:
Division of Water Resources- Non -Discharge Branch
AZ Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Ralei NC 27604
For que€tions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdenr_gov or
Sonia Graves at 919.707.3657 or Sonia.Graves(apcdenr..
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/20/2019

2018 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Summerfield, North Carolina 27358
February 2019

willcox&mate
SOIL SOLUTIONS
February 20, 2019
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9th Floor, Office# 942WM
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2018 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling, Inc.
WMSS, Inc. Project No. 15-02 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental
Waste and Hauling, Inc. (Barnes Environmental Waste). WMSS compiled this report using
data gathered during the compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this land application
program please do not hesitate to contact Mr. Steve Barnes, with Barnes Environmental
Waste 252-241-5014 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosure(s)
cc Barnes Environmental Waste
Shared%WMSS Projects12015115-02 Barnes Environmental12018 Annual Report12018 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road 1 Summerfield, NC 273581 Rob 336.339.9128 or
Martin 336.312.13961 www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL. LAND APPLICATION CERTIFICATION FORM
WQ PC17nitU: WQ0018525 County: Carteret Year:
Facility Name (as shown on permit): Barnes Gnvironmeotal Waste and Iia
Land Application Operator:
Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
[•%1 Yes 0 No - If No, skip Part A, and Par( B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annheation Sununarv:
_ Total another of application fields in the erntit; 1 6
Total number of fields utilized for land application during the yearl 5
Total amount of dry tons applied during the year for all application sites: 31.07
Total number of acres utilized for land application during the year: 24.7
2018
Part B - Annual Compliance Statemen(:
Facility was compliant during calendar year 2018 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality, B Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pld of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. 1 105(a) or the Pollutant
Loading Rates in I SA NCAC 02T .I 105(b) (applicable to 40 CPR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality,
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
Specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I ain aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations,"
_ Steven M. Barnes, President , � n) u7y�nu .9-/c/ - /9
Permittee Name and Title (type Or print) Signature of Permittee [)ate
Signature of Prepare]-* m Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 5039 (r) and I SA NCAC 02T, 1 102 (26) DENR FORM ACF (12/2006)

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 8, 2018
Permit No. WQ0018525
Atlantic Station 0.80 % Solids
12.1 mH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
% x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
0.723
140,600.000
281.200
Phosphorus
0.263
12,640.000
25.280
Potassium
0.449
3,290.000
6.580
PAN injected)*
0.258
2,575.540
5.151
PAN surface)*
0.231
2,312.040
4.624
Ammonia Nitrogen
0.053
235.500
0.471
Calcium
3.558
38,491.000
76.982
Calcium Carbonate Eq,
---
---
---
Magnesium
2,491.000
4.982
Sodium
18,364.000
36.728
Sulfur
---
---
---
Nitrate N / Nitrite N
---
37.640
0.075
Barium
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
3,288.00
6.576
Arsenic
---
2.80
0.006
Cadmium
---
0.50
0.001
Chromium
--- 1
14.000
---
Copper
699.00
1.398
Lead
---
17.00
0.034
Mercury
---
0.13
0.000
Molybdenum
---
5.00
0.010
Nickel
---
11.00
0.022
Selenium
---
5.00
0.010
Zinc
---
997.00
1.994
Hnvironment I. Incorporated I OSA
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +- Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Annnonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

u a
1 .,., mr,i i]v I.1 ii licit-_ a;
Drinking Water ID: 31715
ATLANTIC STATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
ID#: 108 A
DATE COLLECTED: 11/08/18
DATE REPORTED : 12/12/18
i
-C
REVIEWEIf HYIi
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
Ahnnbnut, (dry wt. basis), mg/kg
3288
11/21/18
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
2.8
11/26/18
MTM
3113B-04
Calcium (dry wt, basis), mg/kg
38491
11/21/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
11/21/18
MTM
31138-04
Copper (dry wt. basis), mg/kg
699
11/21/18
LFJ
EPA200.7
Chromium, T.(dry wt, basis),mg/Icg
14
11/21/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
17
12/03/18
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
2491
Il/21/18
LFJ
EPA200.7
Mercury (dry wt, basis), mg/kg
0.13
11/27/18
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
Il
11/21/18
LFJ
EPA200.7
Potassium ((try wt. basis), mg/lig
3290
11/21/18
LFJ
EPA200.7
Selenium ((try wt. basis), nig/lig
<5.0
11/27/18
M'1 10
3113B-04
Sodium ((try wt. basis), mg/kg
18364
12/07/18
AKS
3111B-11
Zine ((try wt. basis), mg/kg
997
11/21/18
LET
EPA200.7
Total Solids, %
0.80
11/13/18
JMT
2540G-11
TKN (dry wt.), mg/kg
c 140600
11/21/18
DTL
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/Icg
c 235.5
11/14/18
TLH
350.1 R2-93
Phosphorus, T, (dry wt.), tug/kg
c 12640
11/13/18
DTL
365.4-74
Nitrate -Nitrite ((try wt.), mg/kg
c 37.64
11/13/18
TLH
353.2 112-93
Plant Available Nitrogen, mg/kg
42265
11/28/18
SEJ
Molybdenum (dry wt. basis), nig/kg
<5.0
11/21/18
LFJ
EPA200.7
ID#: 108 A
DATE COLLECTED: 11/08/18
DATE REPORTED : 12/12/18
i
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REVIEWEIf HYIi
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 12, 2018
Permit No. WQ0018525
Beacons Reach 1.09 % Solids
Invironmeni I R 554A
kDetcrmination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(MineralizationRate)(TKN-.AmmoniaN) i(0.5)(AmmoniaN)+NitrateN+Nitrite N=%PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

BEACON'S REACH I/POND (HYDROTECH)
ATTN: DON O'MARA
HYDROTECTI
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARMI.ETERS Sample Date Analyst Code
PH (not to be used for reporting)
7.9
01/12/18
JTH
450010-11
Aluminum, (dr), wt. basis), mg/kg
2605
01/18/18
LH'J
EPA200.7
Arsenic (dry wt. basis), mg/Icg
3.2
01/22/18
M'l i'bi
31130-04
Calcium (dry wt. basis), mg/kg
35831
01/24/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.6
01/19/18
MTrvl
3113B-04
Copper (dry wt. basis), mg/kg
1811
01/18/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/Icg
11
01/18/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
22
01/18/18
MTM
31138-04
Magnesium (dry wt. basis), mg/kg
15935
01/18/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.14
01/29/18
LFJ
EPA7471B
Nickel (dry wt. basis), mg/kg
Il
01/18/18
LFJ
EPA200,7
Potassium (dry wt. basis), mg/kg
3725
01/18/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/Icg
<5.0
01/17/18
MTM
3113I3-04
Sodium (dry wt. basis), mg/kg
14698
01/23/18
JMN
3111B-11
Zinc (dry wt. basis), mg/kg
1032
01/18/18
LFJ
EPA200.7
Total Solids, %
1.09
01/18/I8
KDS
2540631
TI(N (dry wt.), mg/kg
c 79920
02/05/18
NIE
351.2 R2-93
Ammonia Nitrogen (dry wt.),rag/kg
c 433.0
02/01/18
CMI,
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 17350
02/05/18
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 520.4
02/02/18
CLO
353.2 R2-93
Molybdenum ((try wt, basis), mg/kg
5
01/18/18
LFJ
EPA200.7
ID#: 554 A
DATE COLLECTED: 01/12/18
DATE REPORTED : 02/06/18
REVIEWED BY/-'-e----
Y: . - _
c Uncertified aacz. nj,R due. not offer me aqucouo ccs 14 ficac ion fos eh 1:, end l ytical procedure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: July 17, 2018
Permit No. W00018525
Cape Royal Dolphin 0.34 % Solids
7.15 nil
Parameter
%`
,.Mg/Kgl?ryWeigSt
10,000
Poands(J)ryTgn ..
M K `x 0:002
Nitrogen (TKN)
6.180
61,800.000
123.600
Phosphorus
0.028
282.000
0.564
Potassium
0.753
7,530.000
15.060
PAN injected)"
3.497
34,967.000
69.934
PAN surface'
3.366
33,662.000
_
67.324
Ammonia Nitrogen
0.261
2,610.000
5.220
Calcium
1.840
18,400.000
36.800
Calcium Carbonate Eq.
---
---
---
Magnesium
1,980.000
3.960
Sodium
---
47,400.000
94.800
Sulfur
---
---
---
Niu ate N / Nitrite N
---
14,600.000
_
29.200
Baritun
---
---
---
Chloride
---
---
---
Iron
---
'--
---
_
Aluminum
---
5,280.00
10.560
Arsenic
---
67.40
0.135
Cadmium
---
67.40
0.135
Chromium
---
135.000
---
copper
---
210.00
0.420
---
135.00
0.270
rcur
_
--
5.29
0.011
LLed
l bdenum
---
67.40
0.1kel
135.00
0.270
Selenium
--
67.40
0.135
Zinc
---
1,790.00
3.580
P.nvirochem 9 2018-06923
`Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Anunonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) +(0.5)(Amntonia N) + Nitrate N + Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Fortin Contract Services
Post Office Box 4188
Emerald Isle NC
Attention: Dan Fortin
Lab ID Sample ID:
18-17283 Site: Sludge
Test
Sludge Residuals
v ' rf
I -minaemtal
Date of Report: Jul 17, 2018
Customer PC #:
28594 Customer ID: 08100061
Report #: 2018-06923
Project ID: Cape Royal Sludge
Collect Date/Time Matrix Sampled by
5/2/2018 7:55 AM Solid/Sludge Client
Method Results Date Ana
Aluminum
EPA 200 7
5240 mg/kg
05/17/2018
Calciurn
EPA 200 7
18400 mg/kg
05/09/2018
Chromium
EPA 200 7
<1 35 mq/kq
05/17/2018
Copper
EPA 200 7
210 mg/kq
05/17/2018
Lead
EPA 200 7
<1 35 mg/kq
05/17/2018
Magnesium
EPA 2003
1980 mg/kg
0(3/09/2018
Nickel
EPA 200 7
<1 35 mg/kg
05/1712018
Potassium
EPA 200 7
7530 ing/lic
05/09/2018
Sodium
EPA 200 7
47400 rng/kg
05/11/2018
Zinc
EPA 200 7
1790 mq/1<,q
05/17/2018
Arsenic
EPA 200 8
<67.4 mg/kg
06/18/2018
Cadmium
EPA 200 8
<67.4 mg/kg
06/18/2018
Molybdenum
EPA 200 8
<67.4 mg/kg
06/18/2018
Selenium
EPA 200 8
<67.4 mg/kg
06/18/2018
Nitrate+Niti ite-Nitrogen
EPA 353 2
14600 mg/kg
05/10/2018
Total Solids (%)
SM 2540 8
0.34%
05/03/2018
PH
SM 4500 11 B
7.15 units
05/15/2018
Ammonia Nitrogen
SM 4500 NH3 C
2610 mg/kg
05/07/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
61800 mg/k,
q
05/07/2018
Total Phosphorus
SM 4500 P F
282 mg/kg
05/10/2018
Mercury
SW846 7471 B
<5.29 mg/kg
05/05/2018
Comment Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by: k4ik
All,
Repo,! i� 2018-06921 Page I Of I

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: June 21, 2018
Permit No. WQ0018525
CC Sass 0.55 % Solids
Envirochem N 2018-06900
*Determination of Plant Available Nitrogen (PAN):
injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Amnnonia N) +Nitrate N -1- Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

Report #- 207808900 Page 1 of 1
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ANALYTICAL& CONSULTING CHEWFS
Mfh(a;cn, i I onnwilw Ulcm is IS.cow
Fortin Contract Services
Date of Report: Jun 21, 2018
Post Office Box 4188
Customer PO #:
Emerald Isle NC 28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2018-06900
Project ID: CCSASS Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
18-1722.4 Site: Sludge
5/2/2018 10:25 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
---
Sludge Residuals'
Aluminum
EPA 2003
2290 mg/kg
05/16/2018
Calcium
EPA 200.7
28400 mg/kg
05/09/2018
Chromium
EPA 200.7
<91.5 mg/kg
05/16/2018
Copper
EPA 200.7
704 mg/kg
05/16/2018
Lead
EPA 200.7
<91.5 mg/kg
05/17/2018
Magnesium
EPA 2001
8090 mg/kg
05/09/2018
Nickel
EPA 200.7
<91.2 mg/kg
05/17/20'18
Potassium
EPA 2007
14500 mg/kg
05/09/2018
Selenium
EPA 200.7
<91.5 mg/kg
05/17/2018
Sodium
EPA 200.7
33500 mg/kg
05/11/2018
Zinc
EPA 200.7
640 mg/kg
05/17/2018
Arsenic
EPA 2008
<18.4mg/kg
05/30/2018
Cadmium
EPA 200 8
<18.4 mg/kg
05/30/2018
Molybdenum
EPA 200.8
<18.4mg/kg
05/30/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
38.5 mg/kg
05/10/2018
Total Solids (%)
SM 2540 B
0.55%
05/03/2018
pH
SM 4500 H B
6.77 units
05/15/2018
Ammonia Nitrogen
SM 4500 NH3 c 8070 mg/kg
05/07/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 org
B 75300 mg/kg
05/07/2018
Total Phosphorus
SM 4500 P F
56000 mg/kg
05/10/2018
Mercury
Sw8467471B <3.27 mg/kg
05/05/2018
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received
basis.
75
Reviewed by:
V
Report #- 207808900 Page 1 of 1

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 15, 2018
Permit No. W00018525
Colony By The Sea 0.62 % Solids
12.28 pH (taken from time stabilization event)
Parameter
%
Mg/Kg Dry Weight
% x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002
Nitrogen (TKN)
4.693
46,930.000
93.860
Phosphorus
1.342
13,420.000
26.840
Potassium
0.541
5,411.000
10.822
PAN injected)*
1.436
14,360.450
28.721
PAN surface)*
1,417
14,166.500
28.333
Ammonia Nitrogen
0.039
38+900
0.776
Calcium
2.936
29,358.000
58.716
Calcium Carbonate Eq.
---
---
---
Magnesium
---
4,802.000
9.604
Sodium
---
17,741.000
35.482
Sulfur
---
---
---
Nitrate N /Nitrite N
---
9.920
0.020
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
2,693.00
5.386
Arsenic
---
2.50
0.005
Cadmium
---
1.00
0.002
Chromium
---
12.000
---
Copper
--- 1
224.00
0.448
Lead
---
9.40
0.019
Mercury
---
0.21
0.000
Molybdenum
---
5.00
0.010
Nickel
-
13.00
0.026
Selenium
---
5.00
0.010
Zinc
---
1,343.00
2.686
L.nvironment I N 616A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N -+ Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N)+ Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COLONY BY THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt, basis), mg/kg
2693
01/23/18
LEJ
EPA200.7
Arsenic ((try wt. basis), nig/kg
<2.5
01/25/18
MTM
31138-04
Calcium (dry wt. basis), mg/kg
29358
01/23/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.0
01/25/18
MTM
31138-04
Copper (dry wt. basis), mg/kg
224
01/23/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/Icg
12
01/23/18
LFJ
EPA200.7
Lead (dry weight basis), mg/Icg
9.4
01/23/18
MTM
31138-04
Magnesium (dry wt. basis), mg/kg
4802
01/23/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/lig
0.21
01/29/18
LFJ
EPA7471B
Mickel ((try at. basis), mg/hg
13
01/23/18
LFJ
EPA200.7
Potassium (dry wt. basis), mglkg
5411
01/23/18
LFJ
EPA200.7
Selmlium (dry wt. basis), 1119/lig
<5,0
01/24/18
M1T1
31138-04
Sodium (dry wt. basis), mg/kg
17741
01/24/18
J1IN
31118-11
Zinc (dry wt. basis), mg/kg
1343
01/23/18
LFJ
EPA200.7
Total Solids, %
0.62
01/18/18
KDS
2540C-11
TKN (dry wt.), nig/kg
c 46930
02/05/18
ME
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg
c 387.9
02/08/18
CML
350.1 R2-93
Phosphorus, T, (dry wt.), mg/kg
c 13420
02/05/18
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 9.92
02/13/18
NW,
353.2 R2-93
Plant Available Nitrogen, nig/kg
14166
02/14/18
SEJ
Molybdenum (dry wt, basis), nig/kg
<5.0
01/23/18
LEJ
EPA200.7
IDi#: 616 A
DATE COLLECTED: 07./15/18
DATE REPORTED : 02/14/18
REVIEWED BY:
C Uncer[1. fl I dnt1. DIM aoen uo.. offer non- _ ovo cartsfleneinn for eSio anuly C!cnl [)LOC edure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater'freatmentPlant
Date Sampled: January 2, 2018
Permit No. WO0018525
Dmrescaoe 1.44 % Solids
F.nvizonmcm 1 9 556 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) -1. (0.5)(Ammonia N) .1. Nitrate N f Nitrite N = % PAN
Notc: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
fm, calculation purposes.

DUNESCAPE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, ((fry wt. basis), mg/I(g
Arsenic (dry wt. basis), mg/kg
Calcium ((fry wt. basis), mg/kg
Cadmium ((fry wt, basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/1(g
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), nig/kg
Alercury (dry wt. basis), mg/I(g
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mg/1(g
Selcnlum (dry wt, basis), mg/1(g
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/1(g
Total Solids, cry
TKN ((try wt.), mg/kg
Ammonia Nitrogen (dry wL),mg/1:g
Phosphorus, T. (dry wt.), mg/lig
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date. Analyst Code
7.1 01/02/18 KMR 4500HI3-11
4470 01/18/18 LFJ EPA200.7
3.0 01/25/18 MTM 311313-04
48033 01/24/18 LFJ EPA200.7
L2 01/19/18 MTNi 3113B-04
1023 01/18/18 LFJ EPA200.7
16 01/18/18 LFJ EPA200.7
30 01/18/18 MTNI 3113B-04
12259 01/18/18 LFJ EPA200.7
0,21 01/19/18 JiMN EPA7471B
13 01/18/18 LFJ EPA200.7
2777 01/18/18 LFJ EPA200.7
<5.0 01/17/18 MTM 311333-04
9614 01/23/18 JMN 3111B-11.
1306 01/I8/18 LFJ EPA200.7
1.44 01/03/18 AKS 254OG-11
c 71200 01/19/18 CIA 351.2 R2-93
c 968.5 01/22/18 CLO 350.1 R2-93
c 17480 01/18/18 A1F 365.4.74
c 940.9 01/26/18 CML 353.2 R2-93
<5.0 01/18/I8 LFJ EPA200.7
ID#: 556 A
DATE COLLECTED: 01/02/18
DATE REPORTED : 01/30/18
REVIEWED BY: /—i`(y"/—
O Unen xtitild data. o'm do., .me o_iu. ., o., -uq ue,u, c. -...d fie,, Sw -oc thf. aoa yt iaal ,,..educe,

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 8, 2018
Permit No. WQ0018525
Eight 1/2 Marina 0.51 %Solids
12.2 uH (taken from time stabilization)
Parameter
%
Mg/Kg Dry Weight
% x 10,000)
Pounds/Dry Ton
(MgtKg z 0.002
Nitrogen(TKN)
2.438
41,100.000
82.200
Phos horns
0.244
16,330.000
32.660
Potassium
0.349
2,923.000
5.846
PAN (injected)*
0.740
7,397.776
14.796
PAN (surface)*
0.735
7,349.886
14.700
Ammonia Nitrogen
0.010
713.200
1.426
Calcium
45,084.000
90.168
Calcium Carbonate Eq.
---
---
---
Ma nesiunt
---
2,655.000
5.310
Sodium
---
9,461.000
18.922
Sulfur
---
---
---
Nitrate N / Nitrite N
---
17.930
0.036
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
4,589.00
9.178
Arsenic
4.50
0.009
Cadmium
---
1.30
0.003
Chromium
---
21.000
---
Co er
---
1,071.00
2.142
Lead
---
28.00
0.056
Mercury
---
0.17
0.000
Molybdenum
---
5.00
0.010
Nickel
---
9.00
0.018
Selenium---
5.00
0.010
Zinc
---
2,066.00
4.132
Environment I# 196A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Go ill ',,/ ll��G��;l'
zr _I /a E.
EIGHT & ONE-HALF MARINA VILLAGE
MR. DAN FORTIN
FORTIN CONTRACT
SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC
28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
Aluminum, (dry wt. basis), mg/Icg
4589
02/26/18
LFJ
EPA200.7
Arsenic ((try wt. basis), mg/kg
4.5
02/26/18
NIT IM
3113B-04
Calcium (dry wt. basis), mg/kg
45084
02/26/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.3
02/26/18
MTM
3113B-04
Copper (dry wt, basis), mg/kg
1071
02/26/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/Icg
21
02/26/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
28
02/23/18
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
2655
02/26/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.17
02/27/18
MTM
EPA7471B
Nickel (dry wt. basis), mg/lig
9
02/26/18
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
2923
02/26/18
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
02/22/18
NITM
3113B-04
Sodium (dry wt, basis), mg/kg
9461
02/26/18
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
2066
02/26/18
LFJ
EPA200.7
Total Solids, %
0.51
02/13/18
KAC
2540G-11
TKN ((try wt.), mg/Icg
c 41100
02/22/18
CML
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/lcg
c 713.2
03/06/18
MF
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 16330
02/22/18
DTI,
365.4-74
Nitrate -Nitrite (dry wt.), mg/lig
c 17.93
03/09/18
Mr
353.2 R2-93
Plant Available Nitrogen, mg/kg
16529
03/12/18
S
Molybdenum (dry wt, basis), mg/]cg
<5.0
02/26/18
L17.1
EPA200.7
ID#: 196 A
DATE COLLECTED: 02/08/18
DATE REPORTED : 03/13/18
REVIEWED BY:
C Uncarei"-od data. DWR d000 not o_.or non-aqu e o ua Corti -lcat ion Eo- thio analytical P=ocedur.e.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2018
Permit No. W00018525
Genesis Condos 1.36 % Solids
^'Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(J'KN-Anvnonia N) + (0.5)(Ammonia N) + Nitrate N Nitrite N = % PAN
Note: Constitu to is N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

GENESIS CONDO ASSOCIATION(HYDROTECH
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), tug/kg
Arsenic ((try wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg1kg
Copper ((try wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry «t. basis), mg/kg
Potassium ((try wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen ((try wt,),mg/kg
Phosphorus, T. (dry wt.), mgikg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.3 01/17/18 JTH 4500HB-11
2625 02/09/18 LFJ EPA200.7
3.7 02/14/18 NITNI 311313.04
34438 02/09/18 LFJ EPA200.7
0.90 02/13/18 MTM 3113E.04
476 02/09/18 LFJ EPA200.7
12 02/09/18 LFJ EPA200.7
15 02/12/18 MTM 3113B-04
3818 02/09/18 LFJ EPA200.7
<0.02 02/12/18 LFJ EPA7471B
16 02/09/18 LFJ EPA200.7
4183 02/09/18 LFJ EPA200.7
<5.0 02/14/18 MT\4 311311-04
15946 02/09/18 LEJ EPA200.7
1048 02/09/18 LFJ EPA200.7
1.36 01/18/18 KDS 254OG-11
c 42940 02/05/18 MF 351,2 112-93
c 2906 02/19/18 CLO 350.1 R2-93
C 13850 02/05/18 DTL 365.4-74
c 16.73 02/13/18 MF 353.2 R2-93
<5.0 02/09/18 LFJ EPA200.7
ID#: 68 C
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/20/18
REVIEWED BY:
c tinwrtiFied data. OWR aoea r.o- off.r a...- - .oun crrtiflcac!o. for th!o analytical pr Occ?%Ira.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 12, 2018
Permit No. WQ0018525
Parameter % MglKg
Hampton Suites 1.52 % Solids
7.40 pH
Grvirorment I, Incorporated 551 A
°Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-.Ammonia N) 'IAmmonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N .i. Nitrite N % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
Jr Wetgtrt,
' ("/o x 10,. 6)
Poauds/Dry
Nitrogen (TKN)
6.822
68,220.000
136.440
Phosphorus
1.364
13,640,000
27.280
Potassium
0.331
3,312.000
6.624
PANinjected)"
2.048
20,479.696
40.959
PAN surface)*
2.047
20,473.356
40.947
Ammonia Nitrogen
0.001
12.680
0.025
Calcium
4.354
43,5_36.000
87.072
Calcium Carbonate Eq.
---_
_
Ma nesium
--
2,298.000
4.596
Sodium
---
18,985.000
_
37.970
Sulfur
---
---
---
Nitiate N / Nitrite N
4.820B---
0.010
arium
- -
---
_ _
--
Chloride
---
---
--
Iron---
Aluminum
-
1679.000
3.358
Arsenic
2.50
0.005
---
0.50 --- 0.50
0.001
Chromium
5.000
Cot ter --____--
---_-_-
_ 902.00
_
1.804
Lead
_--
4.20
0.008
Mercur
---
0.10
0.000
___
Molybdenum
---
_
5.00
_
0.010
Nickel
_
---
13.00
0.026
_
Selenium
---
5.00
0.010
Zinc
---
460.00
0.920
-
--1
Grvirorment I, Incorporated 551 A
°Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-.Ammonia N) 'IAmmonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N .i. Nitrite N % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

f
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HAMPTON INN (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PIi (not to be used for reporting)
Aluminum, (dry wt, basis), mg/kg
Arsenic (dry wt, basis), mg/Icg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/Icg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/Icg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry wt, basis), mg/hg
Sodium (dry wt. basis), mg/kg
'Linc ((try wt. basis), mg/Icg
Total Solids, %
TPN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/Icg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite ((try wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.4 01/12/18 JTII 45001IB-I1
1679 01/18/18 LEJ EPA200.7
<2.5 01/22/18 MTM 3113B-04
43536 01/24/18 LFJ EPA200.7
<0.5 01/19/18 MTh4 3113B-04
902 01/18/18 LFJ EPA200.7
5 01/18/18 LFJ EPA200.7
4.2 01/18/18 MTM 3113B-04
2298 01/18/18 LFJ EPA200.7
0.10 01/19/18 JMN EPA7471B
13 01/I8/18 LFJ EPA200,7
3312 01/18/18 LFJ EPA200,7
<5.0 01/17/18 MTM 311313-04
18985 01/23/18 JMN 3111B-11
460 01/18/18 LFJ EPA200.7
1.52 01118/18 KDS 2540G-11
c 68220 01/26/18 DL 351,2 R2.93
c 12.68 01/29/18 DTL 350.1 R2-93
c 13640 01/26/18 N4R 365.4.74
c 4.82 01/26/18 CMI, 353.2 R2-93
<5.0 01./18/18 LET EPA200.7
ID#: 551 A
DATE COLLECTED: 01/12/18
DATE REPORTED : 01/30/18
E
REVIEWED BY:
uncertitto0 data. I:WR Ccee no, o-_�_ ..c., -aqueous ce rt i E is at 0n Eos Chia analytics: [race Aure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 23, 2018
Permit No. WQ0018525
Island Beach 1.06 % Solids
Environment 1 9 564 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N � Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) .1, Nitrate N 1 Nitrite N = ON. PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

tri �1( ijI�,
Cz'R,ET WHIE, `r.I.C. 217258
ENVIRACON UTILITIES
C/O MR. STANLEY BUCK
1745 BELLGRADE-SWANSBORO ROAD
MAYSVILLE ,NC 28555
PARAMETERS
PH Piot to be used for reporting)
Ahimbioni, (dry wt. basis), mg/kg
Arsenic ((try wt. basis), nig/kg
Calcium (dry wt. basis), nig/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/Icg
Lead ((fry weight basis), nig/hg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium ((fry wt, basis), mg/kg
Sodium (dry wt, basis), ing/Icg
Ziac (dry wt. basis), nig/kg
Total Solids, %
TION (dry wt.), mg/kg
Ammonia Nitrogen (div wt.),nig/lig
Phosphorus, T. ((try wt.), nig/hg
Nitrate -Nitrite ((fry wt.), nrg/Icg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.4 08/23/18 HYIM 4500HB-11
4163 09/20/18 LFJ EPA200.7
<2.5 09/25/18 MTM 311313-04
56398 09/20/18 LPJ EPA200.7
0.65 09/21/18 MTM 3113B 04
1237 09/20/18 LFJ EPA200.7
11 09/20/18 LPJ EPA200.7
9.2 09/20/18 IVITM 311313-04
3709 09/20/18 LFJ EPA200.7
0.19 08/31/18 MTM EPA74716
12 09/20/18 LPJ EPA200.7
3654 09/20/18 LFJ EPA200.7
<5.0 09/27/18 Iv1TM 31L3B-04
8807 09/20/18 LFJ EPA200.7
853 09/20/18 LFJ EPA200.7
L06 08/23/18 JMS 2540G -II
c 33370 08/28/18 DTL 351.2 R2-93
c 939.1 09/11/18 BLD 350.1 R2-93
c 22670 08/28/18 CLO 365.4-74
c 4.91 08/28/18 TLA 353.2 R2-93
<5.0 09/20/18 LFT EPA200.7
ID#: 564 A
DATE COLLECTED: 08/23/18
DATE REPORTED : 10/11/18
c Jo=or;.if luaa data. U"v!R doss not oE2er nnnn _i ,,x c�n.!fira[So:: fcr Ch!s nn,.!yf!caj P=ecedure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 23, 2018
Permit No. WQ0018525
Mariners Point 0.60 % Solids
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(-I'KN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (so( Detected) or < detection limits are listed as detection limits
for calculation purposes.

,i j,t 1 Ilii I l
0N 0HIVL
1,4 CAW
MARINERS POINT
C/O MR. STANLEY BUCR
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAMETERS
PH (not to be used for reporting)
Alumhmm, (dry wt, basis), nig/1(g
Arsenic (dry wt. basis), nig/kg
Calcium (dry wt. basis), mg/I(g
Cadmium (dry wt, basis), mg/kg
Copper ((try wt. basis), mg/kg
Chromium, T.(dry wt. basis),ug/kg
head ((try weight basis), mg/kg
Magnesium ((try wt. basis), mg/kg
Mercury ((try wt. basis), mg/leg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt, basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), nag/1(g
Sodium Adsorption Ratio (talc)
Total Solids, %
TEN (dry wt.), mg/kg
Anmmonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/Icg
Nitrate Nitrite (dry wt.), mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.3
08/23/18
i-MNI 45001IB-11
3622
09/20/18
LFJ
EPA200.7
4.0
09/25/18
MTh!
3113B-04
62329
09/20/18
LFJ
EPA200.7
0.71
09/21/18
MTM
3113B-04
792
09/20/18
LFJ
EPA200.7
20
09/20/18
LFJ
EPA200.7
19
09/20/18
MTV/
3113B-04
4892
09/20/18
LRT
EPA200.7
0.15
08/31/18
hfPM
EPA747113
7
09/20/18
LFJ
EPA200.7
4675
09/20/18
LFJ
EPA200.7
<5.0
09/27/18
MTM
3113B-04
6641
09/20/18
LF,1
EPA200.7
3004
09/20/18
LFJ
EPA200.7
0.2
0.60
08/23/18
JMS
2540E -I1
c 25130
08/28/18
DTL
351.2 82-93
c 243.5
09/11/18
BLD
350.1 R2-93
c 14870
08/28/18
CLO
365.4-74
c 604.8
09/19/18
DTL
353.2 112-93
<5.0
09/20/18
LFJ
EPA200.7
ID#: 307
DATE COLLECTED: 08/23/18
DATE REPORT D t 10/11/18
REVIEWED BY:
e:lrcrtif-Ad d.t.. n4'A don!i I'll. offer non-uqu Co':I3 c, _rt:ficuti7n Eor thio .1,.91`fL1Ca1 procedure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2018
Permit No. W00018525
NC Aquarium at Pine 1.35 % Solids
Knoll Shores 12.25 PH (taken from time stabilization event)
Parameter
%
Mg/Kg Dry Weigbt
% x 10,000
Pounds/Dry Ton
(M K 0.002
Nitrogen (TKN)
3.797
37,970.000
75.940
Phosphorus
1.209
12,090.000
24.180
Potassium
0.650
6,503.000
13.006
PAN (injected)*
1.175
11,747.570
23.495
PAN (surface)*
1.150
11,497.070
22.994
Ammonia Nitrogen
0.050
501.000
1.002
Calcium
3.320
33,196.000
66.392
Calcium Carbonate Eq.
---
---
---
Magnesium
---
8,531.000
17.062
Sodium
---
79,773.000
159.546
Sulfur
---
---
---
Nitrate N / Nitrite N
---
5.870
0.012
Barium
---
---
---
Chloride
---
---
---
Iron
---
--
---
Aluminum
---
1,293.00
2.586
Arsenic
2.50
0.005
Cadmium
---
17.00
0.034
Chromium
---
15.000
---
Copper
---
413.00
0.826
Lead
---
42.00
0.084
Mercury
0.25
0.001
M01 bdenum
---
5.00
0.010
Nickel
---
17.00
0.034
Selenium
5.00
0.010
Zinc
---
787.00
1.574
Environment I N 444 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0,5)(Antmonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

','„ ,
i� �,Jlil.l��1) nl).1 _p u
I_ !'EENIIVILLE, N.C. 278,5-7085
NC AQUARIUM AT PINE KNOLL SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
1293
02/09/18
LF.J
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/14/18
MTM
3113B-04
Calcium (dry wt, basis), mg/kg
33196
02/09/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
17
02/13/18
MTM
3113B-04
Copper (dry wt. basis), mg/kg
413
02/09/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),nlg/kg
15
02/09/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
42
02/12/18
MTM
3113B-04
Magnesium (dry wt, basis), mg/kg
8531
02/09/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.25
02/12/18
LFJ
EPA7471B
Nickel (dry wt. basis), mg/kg
17
02/09/18
LFJ
EPA200.7
Potassium (dry wt. basis), nig/kg
6503
02/09/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/14/18
MTM
3113B-04
Sodium ((try wt. basis), mg/kg
79773
02/09/18
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
787
02/09/18
LFJ
EPA200.7
Total Solids, %
1.35
01/18/18
RDS
2540G-11
TKN (dry wt.), mg/kg
c 37970
02/05/18
MP
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 501.0
02/19/18
CLO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 12090
02/05/18
Du.
365.4-74
Nitrate -Nitrite ((try wt.), mg/kg
c 5.87
02/13/18
MF
353.2 112-93
Plant Available Nitrogen, mglkg
11497
02/20/18
SEJ
Molybdenum (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA200.7
FAX (252) 156 -
ID#: 444 A
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/20/18
REVIEWED BY:
c Uncortafiod data. C.dR dooa not offor non-agnooua Certification for ....rn analytical proocdurc.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 24, 2018
Permit No. W00003067
Ocean Bay Villas 0.30 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
% x 10,000)
Pounds/Dry Ton S
(Mg/kg. X'0.002)
Nitrogen (TKN)
4.083
40,830.000
81.660
Phos horns
1.361
13,610.000
27.220
Potassium
0.452
4,518.000
9.036
PAN injected)*
1.228
12,281.514
24.563
PAN surface)*
1.227
12,265.304
24.531
Ammonia Nitrogen
0.003
32.420
0.065
Calcium
5.108
51,083.000
102.166
Calcium Carbonate Eq.
---
---
--- _
Magnesium
---
3,849.000
7.698
Sodimn
---
13,181.000
26.362
Sulfur
---
---
Nitrate N / Nitrite N
---
9.820
0.020
barium
-'-
--
---
Chloride
---
---
Iron
---
---
---
Aluminum —-
---
4,928.00
9.856
Arsenic ------
-----
— 2.80
___--
0.006
Cadmium
---
1.20
_
0.002
Chromium --
---
-- —17.000
Copper
---
331.00
0.662
Lead
33.00
0.066
Mercur
---
0.30
0.001
Molybdenum
---
5.00
0.010
Nickel
_
15.00
0.030
Selenium
5.00
0.010
Zinc
---
1,264.00
2.528
fnvironmcnl I d 442 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) I Ammonia N i Nitrate N t Nitrite N % PAN
Surface Application:
(MineralizationRate)(TKN-AmmoniaN) 1(0.5)(AnnnoniaN)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation pm -poses.

i
:ii ill;�lix-s!i) i' 1i,, ',;'0 (f,
t 1RIEENvU-E, N.C,',27835-7085
C&P ENTERPRISES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
ijl
PAX (252) 7E6 C633
ID#: 442 A
DATE COLLECTED: 01/24/18
DATE REPORTED : 02/28/18
REVIEWED BY:�`
e Vnc nr ti f.iod data. DWR dopa not o. -er non-aqu nous ecrtif 1e aion Cor thio analytical nro cc avre.
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PH (not to be used for reporting)
7.1
01/24/18
JTH
450OBB-11
Aluminum, (dry wt. basis), mg/kg
4928
02/20/18
LPJ
EPA200.7
Arsenic ((try wt. basis), mg/kg
2.8
02/21/18
MTM
3113B-04
Calcium ((try wt. basis), mg/kg
51083
02/20/18
LFJ
EPA200,7
Cadmium (dry wt. basis), mg/kg
1.2
02/20/18
MTM
3113B-04
Copper (dry wt. basis), mg/kg
331
02/20/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
17
02/20/18
L.PJ
EPA200.7
Lead ((try weight basis), mg/kg
33
02/19/18
MTM
3113B-04
Magnesium ((try ict. basis), mg/kg
3849
02/20/18
LEJ
EPA200.7
Mercury (chy wt, basis), mg/lig
0.30
02/12/18
LFJ
EPA7471B
Nickel ((try wt. basis), mg/kg
15
02/20/18
LPJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4518
02/20/18
LFJ
EPA200.7
Selenium ((try wt. basis), mg/lig
<5.0
02/22/18
MTM
311313-04
Sodium (dry wt. basis), mg/kg
13181
02/20/18
LPJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1264
02/20/18
LFJ
EPA200.7
Sodium Adsorption Ratio (cafe)
0.5
Total Solids, %
0.30
01/25/18
MAR
2540G-1.1
TKN (dry wt.), mg/kg
c 40830
02/16/18
CLO
351.2 112-93
Ammonia Nitrogen ((try wt.),mg/lig
c 32.42
02/20/18
CML
3501 R2-93
Phosphorus, T. (dry wt.), mg/lig
c 13610
02/16/18
CMI,
365.4-74
Nitrate -Nitrite (dry wt.), mg/ki;
e 9.82
02/21/18
CLO
353.2 112-93
A4olybdenum (dry wt. basis), mg/lig
<5.0
02/20/18
LFJ
EPA200.7
PAX (252) 7E6 C633
ID#: 442 A
DATE COLLECTED: 01/24/18
DATE REPORTED : 02/28/18
REVIEWED BY:�`
e Vnc nr ti f.iod data. DWR dopa not o. -er non-aqu nous ecrtif 1e aion Cor thio analytical nro cc avre.

BARNES ENVIRONMENTAL. WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2018
Permit No. W00018525
Ocean Club 0.36 % Solids
12.05 nH (taken from lime stabilization event)
2.022
IlPotassium 1 0.7161 7.155.0001 14.31011
12.490
nia Nitrogen
0.025 246.100
0.492
n
4.523 45,227.000
90.454
n Carbonate Eq.
--- ---
---
duni
-- 5,209.000
10.418
Aluminum
14,522.000
29.044
M /K
_—
Arsenic
--- 2.50
N / Niuite N
--- 6.860
0.014
13arium
---
---
SAR
Chloride
1.03
_
---
CeilingConcen.'
Aluminum
--- - —_--- 1.622.00
-- 3.244
M /K
_—
Arsenic
--- 2.50
0.005
75
Cadmium
_
--- 0.75
_
0.002
85
Chromium
--- 7.000
---
...
•--
FCOer
368.00
0.736
4,300
Lead
--- 9.60
0.019
840
Mercui
0.38
0.001
_ 57
_
Mol bdenum
_
5.00
_
0.010
75
Nickel
-- 9.00
0.018
420
Selenium
5.00
0.010
100
Zinc
--- 1,735.00 1
3.470
7,500
11 I I �I
Environment I N 404 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N i- Nitrate N -+ Nitrite N = % PAN
Surface Application:
(MincralizationRate)(TKN-AmmoniaN) I (0.5)(AmnnoniaN) I Nitrate N+ Nitrite NN %PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

?.t). BOX i'085, 1140^,Ki'j!=0Nj'i
OCEAN CLUB
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
t AXI [phone]
ID#: 404 A
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/20/18
REVIEWED BY:�
.. Oncer¢iflcb data. DWZ door not offer non-aquoonn cortifir.atlon for th}n analyt5cal procaduro.
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
Alumumm, (dry wt, basis), mg/lig
1622
02/09/18
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/14/18
MTA1
3113B-04
Calcium (dry wt. basis), mg/kg
45227
02/09/18
Lrl
EPA200.7
Cadmium ((try wt. basis), mg/kg
0.75
02/13/18
MTM
31138-04
Copper (dry wt. basis), mg/kg
368
02/09/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
7
02/09/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
9.6
02/12/18
MTM
311313-04
Magnesium (dry wt. basis), mg/lig
5209
02/09/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/Icg
0.38
02/12/18
LFJ
EPA7471B
Nickel (dry wt. basis), mg/kg
9
02/09/18
LFJ
EPA200.7
Potassium (dry wt, basis), mg/kg
7155
02/09/18
LFJ
EPA200.7
Selenium ((try wt. basis), mg/kg
<5.0
02/14/18
MTM
3113B-04
Sodium ((try at. basis), mg/kg
14522
02/09/18
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1735
02/09/18
LFJ
EPA200.7
Total Solids, %
0.36
01/18/18
IRDS
25406-11
TKN (dry wt.), mg/lig
c 20220
02/05/18
MF
351.2 82-93
Ammonia Nitrogen (dry wt.),mg/kg
c 246.1
02/19/18
CLO
350.1 R2-93
Phosphorus, T. ((try wt.), mg/kg
c 19881
02/05/18
DTL
36.5.4-74
Nitrate -Nitrite ((try wt.), mg/kg
c 6.86
02/13/18
NfF
353.2 112-93
Plant Available Nitrogen, mg/Icg
6122
02/20/18
SEJ
Molybdenum (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA200.7
t AXI [phone]
ID#: 404 A
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/20/18
REVIEWED BY:�
.. Oncer¢iflcb data. DWZ door not offer non-aquoonn cortifir.atlon for th}n analyt5cal procaduro.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual'Pype: Wastewater Treatment Plant
Date Sampled: January 16, 2018
Permit No. W00018525
Oceans Condominiums 0.85 % Solids
7.6 nH
Parameter
'O!o .Mg/Kg Dry height
O,UQO)
Poundsl,Ury Toa
. (M /Kg z
NiGogen (TKN)
0.330 52,120.000
104.240
Phos horns
0.266 9,932.000
19.864
Potassium
0.504 6,435.000
12.870
PANinjected)"
0.119 1,186.300
_
2.373
PAN surface)*
O. 105 1,051.800
2.104
Ammonia Nitrogen
0.027 1,598.000
_
3.196
Calcium
5.876 21,532.000
43.064
Calcium Carbonate Eq.
--- ---
---
Mamiesium
0.418 3,912.000
7.824
Sodium
--- 19,609.000
39.218
Sulfur
--- ------
Nittate N / Nitrite N
--- 8.900
0.018
_
Barium
--- ---
--
Chloride
_
--- ---
---
Iron
Iron
--- ---
_
--
Aluminum
--- 2,302.00
4.604
Arsenic
_
2.50
0.005
Cadmium
--- 0.96
0.002
Chromiunn ---_--
-- -----_ 7.000
---
Co et
--- 541.00
1.082
Lead
--- 15.00
0.030
Mercer _
--- _ 0.26
0.001
M01 bdenum
--- 6.00
0.012
_
Nickel
--- 11.00
0.022
Selenium
-- 5.00
0.010
Linc
--- 1.044.00
2.088
Environment 1 ft 566 A
*Determination of Plant Available Nitrogen (PAN):
injected Application:
(Mineralization Rate)(i'KN-Ammonia N) -t- Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-AmmoniaN) i (0.5)(AmmoniaN)+Nitrate N; NitriteN=%PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

OCEANS CONDOMINIUMS (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/Icg
Cadmium ((try wt_ basis), mg/Icg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead ((try weight basis), mg/k-1
Magnesium (dry wt, basis), mg/Icg
Mercury (dry wt. basis), mg/hg
Nickel (dry wt. basis), mg/Icg
Polassium (dry wt, basis), mg/kg
Selenium (dry wt. basis), mg/hg
Sodium ((try wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids,
TKN ((try wt.), tng/kg
Ammonia Nitrogen ((try w0,111111/kIl
Phosphorus, T. ((try wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum ((try wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.6 01/16/18 JTH 4500HII-11
2302 01/23/18 LhJ EPA200.7
<2.5 01/25/18 NYPM 3113B-04
21532 01/23/18 LRJ EPA200.7
0.96 01/25/18 M'I'NI 3113B-04
541 01/23/18 LPJ EPA200.7
7 01/23/18 LPJ EPA200.7
15 01/23/18 MTNI 3113B-04
3912 01/23/18 LhJ EPA200.7
0,26 01%29/18 LPJ EPA747113
11 01/23/18 LPJ EPA200.7
6435 01/23/18 LPJ EPA200.7
<5.0 01/24/18 NITNI 3113E-04
19609 07/24/18 JMN 31111341
1044 01/23/18 LPJ EP.A200.7
0.85 01/18/18 KDS 7,540G-11
c 52120 02/05/18 MP 351.2 R2-93
c 1598 02/08/18 CML 350.1 R2-93
c 9932 02/05/18 DTL 365.4-74
c 8.90 02/13/18 MP 353.2 R2-93
6 01/23/18 LPJ EPA200.7
Ill#: 566 A
DATE COLLECTED: 01/16/18
DATE REPORTED : 02/14/18
REVIEWED BY:
c Onrcrc i''ietl tlaca. Dtvl ..o_n Ooc offer ron . ouo c¢ictfic st l on oChia anav Yeic+3 r=a C sdu Sc

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 12, 2018
Permit No. W00018525
Ocean Terrace 1.79 % Solids
8.3 pIl
Parameter
°/q " Mg I{g Dry Weight,
Pounds/Dry Ton ,
(Mg/Kg'•x 9.002)
Nitrogen (TI<N)
6.037 60,370.000
120.740
Phosphorus
1.759 17,590.000
35.180
Potassium
0.271 2,707.000
5.414
PAN (injected)"
1.815 18,154.422
36.309
PAN (Surrface v
1.815 18,148.842
36.298
Ammonia Nitrogen
0.001 11.160
0.022
Calcium
_
5.214 52,144.000
104.288
Calcium Carbonate Bch_
_- ---
Ma nesium
-- 2,637.000
5.274
Sodium
--- 13.930.000
27.860
Sulfur
---
Nitrate N / Nitrite N
_
--- 35.610
0.071
Barium
-- -----
Chloride
--
--- ---
-------------
---
--
6'011
------
--- ---
--
Aluminum
--- 4703.000
9.406
Arsenic
_
4.70
0.009
Cadmium ---
_
--- 1.40
------ 0.003
Chromium
-- 20.000
--
---
Coper-----__-_----_-
Copper
--- ----
- t ,1 17.00
---- 2.234
Lead
_ _
37.00
_
0.074
mercury_
--- _-----_- 0.48
- -- 0.001
Mol bdenun
5.00
0.010
Nickel
--- 12.00
0.024
Selenium
_ _
- 5.00
_
0.010
zinc
--- 2,392.00
4.784
[nvironment 19 557 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N -1 Nitrite N = % PAN
Surface Application:
(Mineralization Rale)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N - % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation Purposes.

OCEAN TERRACE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, ((ry wt, basis), mg/kg
Arsenic (dry wt, basis), mg/itg
Calcium ((try wt. basis), mg/kg
Cadmium (dry wt, basis), ung/kg
Copper ((try wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/Itg
Lead (dry weight basis), mg/kg
.Magnesium ((try wt, basis), mg/kg
Mercury (dry wt. basis), mg/hg
Nickel (dry wt, basis), mg/kg
Potassium (duy wt. basis), mg/kg
Selenium (dry NO. basis), mg/kg
Sodium (dry wt, basis), me/kg
Zinc (dry wt. basis), mg/lip
Total solids, %
TICK ((try wt.), mg/ltg
Ammonia Nitrogen ((fry wt.),mg/kg
Phosphorus, 'r. ((try wt.), mg/hg
Nihate-Ni0ito (dry wt.), mglkg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis m0hod
Sample Date Analyst Code
8.3 01/12/18 JTH 450ORB-11
4703
01/18/78
LET
EPA200.7
4.7
01/22/18
MTN4
311313-04
52144
01/24/18
LFJ
EPA200.7
1.4
01/19/18
NCI;M
3113E-04
1117
01/18/18
LFJ
EPA200.7
20
01/18/18
LFJ
EPA200.7
37
01/18/18
MTM
311313-04
2637
01/18/18
LFJ
EPA200.7
0.48
01/29/18
LFJ
EPA747111
12
01/18/18
LFJ
EPA200.7
2707
01/18/13
LFJ
EPA200.7
<5.0
01/17/18
M1'M
3113B-04
13930
01/23/18
JM`N'
3111B-11
2392
01/18/18
LFJ
EPA200.7
1.79
01/18/18
KDS
2540G-11
c 60370
02/05/18
MF
351.2 R2-93
c 11.16
01/29/18
DTI.
350.1 R2-93
c 17590
02/05/18
DTL
365.4-74
c 35.61
02/13/18
MF
353.2 722.93
<5.0
01/18/IS
LPJ
EPA200.7
ID#: 557 A
DATE COLLECTED: 01/12/18
DATE REPORTED : 02/14/18
a
REVTRWED BY:
C (fjc,rti, and r-'zt.a. Part dOOl ..0[ OY!er non-nyueeoc -evti. E1 ca c' -Oa EOr ^_hiu an IycI ,,I DcOeadu:.e.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 15, 2018
Permit No. W00018525
Pebble Beach 3.05 % Solids
7 pll
Parameter
°/q
M 1Kg Dry LVeIght,
(% x 10,000
-Ppttnds/Dry `<'on ,
(iVL K x 0.002)"
Nitrogen (TKN)
7.123
71,230.000
142.460
Phos horns
1.202
12,020.000
24.040
Potassium
0.246
2,455.000
4.910
PAN (iti ected)
2.467
2,464.097
_
4.928
PAN surface)"
2.231
2,435.542
4.871
Ammonia Nitrogen
0.470
4,704.000
9.408
Calcium
2.340
23,397.000
46.794
Calcium Carbonate E
---
---
---
Ma nesium
6,936.000
13.872
Sodium
---
4,079.000
8.158
Sulfur
---
---
---
Nitrate
4.940
0.010
Barium
---
---
---
Chloride
---
---
roll
--
--
---
Aluminwn_
---
2,688.000
—
5.376
Arsenic
---
_
2.50
_
0.005
Cadmium - -
---
0.96
_
0.002
Chromium
---
8.000
copper
---
503.00
1.006
—
Lead
-----------
— - 17.00
— — 0.034
_
Mercury
---
0.08
0.000
Ntol bdenum
--- 1
5.00
---- 0.010
__ _-
Nickel
10.00
0.020
Selenium
---
5.00
0.010
_
zinc
---
1,108.00
2.216
linvironmem 1 N 287A
-Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Ratc)(T KN -Ammonia N) + Ammonia N + Nitrate N -, Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +- Nitrite N - % PAN
Note: Corstitaents N.D. (Not Detecte(I) or <detection limits arc listed as detection iimits
for calculation purposes.

ii ��,liN
1
PEBBLE BEACH (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used For reporting)
Ahunimmn, ((try wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry at. basis), mg/kg
Copper (dry wt. basis), mg/Iig
Chromium, 'r,(dry wt. basis),mg/lig
Lead (dry weight basis), mg/hg
Magnesium (dry wt. basis), mg/kg
N4ercury (dry wt. basis), mg/lig
Nickel (dry wt, basis), mg/lig
Potassium ((fry wt. basis), mg/lig
Selenium (dry wt. basis), mg/lig
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids, %
TKN ((fry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/lag
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/lig
Plant Available Nitrogen, mg/kg
Molybdenum ((ry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.0 01/16/18 JTII 4500HB-I1
2688 01/23/18 LFJ EPA200.7
<2.5 01/25/18 NrrM 3113B-04
23397 01/23/18 LFJ EPA200.7
0.96 01/25/18 M1'M 3113B-04
503 01/23/18 LFJ EPA200.7
8 01/23/18 LFJ EPA200.7
17 01/23/18 MTM 311313-04
6936 01/23/18 LFJ EPA200.7
0.08 01/29/18 LFJ EPA747113
10 01/23/18 LFJ EPA200.7
2455 01/23/18 LFJ EPA200.7
<5.0 01/24/18 MTM 3113B-04
4079 01/24/18 JMN 311113-11
1108 01/23/18 LFJ EPA200.7
3.05 01/18/18 I<DS 2540G-11
c 71230 02/05/18 MF 351.2 82-93
c 4704 02/08/18 CML 350.1 R2-93
c 12020 02/05/18 D'PL 365.4-74
c 4.94 02/13/18 MF 353.2 R2.93
22315 02/14/18 StJ
<5.0 01/23/18 LFJ EPA200.7
ID##: 287 A
DATE COLLECTED: 01/15/18
DATE REPORTED : 02/14/18
REVIEWED BY:
v Gncezei;aed 1u11, p'd8 deco ..ol: oetar non-aqe eo us ce<<:.f 1c[,e So:� fo= eLitl .+c ilC 0.cu1 pzo<^duce.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: ,January 19, 2018
Permit No. W00018525
Peppertree 0.67 % Solids
12.3 pli (taken from lime stabilization event)
Parameter
%i
Mg/Kg Ary Weight
" % x 70,000
Founds/Dry Ton
M x 0.002
Nitrogen (TKN)
3.394
33,940.000
67.880
Phosphorus
0.964
9,635.000
19.270
Potassium
0.253
2,534.000
5.068
PAN (injected)*
1.070
10,697.560
21.395
PAN surface)*
1.033
10,330.710
20.661
Ammonia Nitrogen
0.073
733.700
1.467
Calcium
4.231
42,308.000
84.616
Calcium Carbonate Eq.
---
--Ma
nesium
Magnesium
---
2,523.000
5.046
Sodium
---
6,862.000
13.724
Sulfur
---
---
---
Nitrate N/NitriteN
---
1.970
0.004
Barium
---
---
---
Chloride
---
---
lion
---
---
---
Aluminum
---
3,505.000
7.010
Arsenic
---
2.50
0.005
Cadmium
---
1.10
0.002
Chromium
---
13.000
---
Co er
---
482.00
0.964
Lead
---
8.00
0.016
Mercury
---
0.27
0.001
Molybdenum
---
5.00
0.010
Nickel
---
11.00
0.022
Selenium
---
5.00
0.010
Zinc
---
1,302.00
2.604
Environment 1 N 129 C
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ani nonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

P>✓ URTAVE RE80RTO
ATTN: ;), A. DAN FOMIP
P.O... EO.X 1Q88
ATIANTIC 81✓ACLI ,NC 28512
ID#t 129 C
DATE CO'LL4CTEnt. 01/19/18,
DkWE REPORTED 't 02/20/18
REVI>tip ED BYs _
c Uni,3s CP.l'iotl data: DWI? Ocoa not cutis, nam-uqutitiyp aerciTL.PnLlan [oq tl{ia ondly G}dnl psoc u:furo.
Sludge
Analysts
Method
PARAKETERS
sample
Date :Analyst
Cade
A)gmioum, (dry. ;ivi. basis), ;mgliq
3505
02/09/18
LYJ
) I?A2tIQ,7
Arso do (cloy wt. basiu)t mg/49
<2,5
02/14/18.
MTM
31131.144
G,illcium (dry avt, basis), �nglkg
42366
02/04/18
LPJ
MPA200,7
Cn(bmlmn,(dry rvt, bosfs),'mg/lcg.
1:7
02/13%18
MTM
3100,04
coppery (dry wt, basis), virg/Icg
482
02/09/18
LFJ
EPA200,7
Clurorrliam, T.(dvy Avl, basis);nig/hg
13
02109/18;
LIN
I�P'A200.7
Lead (Jry weight ;basis), u10%
8,0
,02112118
MTM
711313.04
Mngneslurn .(dry rot. ,basis), m911%
2523
620/1s
Lw
EPA200,7
Nlorcary (Ory w6 basis), mg/lig
0;27
02/12118.
LM
tPA7471T1
Nickel ((Iry wt, basis),, mg/f(g
i1
02/09/-18
LFJ
rRA200,7
Potussluna (dry wt, basis), mg/ttg.
2534
02/09/18
LPJ
RPAMM
Selenium_ (dry wt, basis), nog/lcg
<.50
02/14/18
MTM
311313,-04
Sodium (dry wt. imsfs), ang/I(g
G862
02/0?/l8
LITJ
EPA200;7
Ziac (dry w1, basis), nigAg
1302
02(09118
LIU
EPA200,7
Total S4,llds, %
'0,67
01/23/18
MA18
2540G -1I
TI{N (dry'wi.), nig/kg'
c 33240
02105118
MF
351;2122.93
Ammonla:Nipogeu (drrd(,),mglt(g
c 7.33,7
02119/18.
CLD
'350,1 82.93
Phosphorus, T. (ary wtJ, mglltg
c X9$35
02/05/18
DTL
365.474
NitrateaNfirltc (dry wt), mg/Ug
c.I,97
02/13/18
MF
353.2:'R2-93
i'laat'Mailable Nitrs gent, -lhg/lig
:13651
02/20118
SPT
Nfolybdcuurn (dry 1".. basis), ling/lig
<5,0-
02109!18
LTJ
lePA200.7
ID#t 129 C
DATE CO'LL4CTEnt. 01/19/18,
DkWE REPORTED 't 02/20/18
REVI>tip ED BYs _
c Uni,3s CP.l'iotl data: DWI? Ocoa not cutis, nam-uqutitiyp aerciTL.PnLlan [oq tl{ia ondly G}dnl psoc u:furo.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALVSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 25, 2018
Permit No. WQ0018525
Pine Knoll Townes 2.15 % Solids
^Determinatimt of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N - Nitrite N =_ % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N - Nitrite N = 9'0 PAN
Note: Constituents N.D. (Not Detected) or < detection limits arc listed as detection limits
for calculation purposes.

PINE KNOLL TOWNES (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/Icg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/I<g
Cadmium (dry wt, basis), mg/Icg
Copper (dry wt. basis), mg/Icg
Chromium, T.(dry wt, basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt, basis), mg/Icg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/Icg
Selenium (dr) wt. basis), mg/Icg
Sodium (dry wi. basis), mgilcg
Zinc (dry wt. basis), mg/Icg
Total Solids, %
TKN (dry w(.), Ing/k-1n
Anuonia Nitrogen (dry et.),mg/hg
Phosphorus, T. (dry wt), mg/Icg
Nitrate Nitrite (dry wt.), mg/kg
Molybdenum (diy. wt, basis), mg/kg
Sludge
Analysis
Method
Sample
Date
Analyst
Code
7.4
01/25/18
J'I5d
4500111M 1
4030
02/20/18
LFJ
EPA200.7
2,6
02/21/18
MTNI
311313-04
45608
02/20/18
LFJ
EPA200.7
0.99
02/20/18
MTM
311313-04
874
02/20/18
LFJ
EPA200.7
17
02/20/18
LFJ
EPA200.7
17
02/19/18
NITNl
311313.04
2550
02/20/18
LFJ
EPA200.7
0.25
02/21/18
MTM
EPA747133
12
02/20/18
LFJ
EPA200.7
1896
02/20/18
LFJ
EPA200.7
<5.0
02/22/18
MTNI
3113B-04
10104
02/20/18
LFJ
EPA200.7
2723
02/20/18
LFJ
EPA200.7
2.15
01/25/18
MAR
2540G-11
c 53370
02/20/18
,14F
351.2 122-93
c 178.8
02/20/18
CML,
350,1 R2-93
c 20480
02/20/18
D'I'L
365.4-74
c 3.00
02/21/18
CLO
353.2 R2:93
<5.0
02/20/18
LFJ
EI'A200.7
ID#: 558 A
DATE COLLECTED: 01/25/18
DATE REPORTED : 02/28/18
c ., no o c 121 o I1,ta, moa aoe.0 not oz. eee con-agv3ouS c[- rtErlce^von for ¢hts er.aly -loa: pcocectu ra.

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13ARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual'rype: Wastewater Treatment Plant
Date Sampled: January 17, 2018
Permit No. WQ0018525
Point Emerald Villas 0.40 % Solids
8.2 pH
Parameter
%q
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton ".
(Mg/Kg` x 0.002)
Niuogen (TKN)
5.254
44,820.000
89.640
phosphorus
1.482
12,270.000
24,540
Potassium --
0.273
2,794.000---
5.588
PAN in'ected)"
1.612
16,123.000
32.246
PAN surface)*
1.595
15,952.500
31.905
Ammonia Nitrogen
0.034
105.400
0.211
Calcium
4.028
23,343.000
46.686
Calcium Carbonate Et .
---
---
---
Magnesium
2,057.000
4.114
Sodium
---
28,403.000
_
56.806
sulfur
---
---
--- -
-Nitrate N / Nitrite N
---
_
123.200_
0.246
Barium
---
---
Chloride
---
---
---
h'on
---
---
---
Aluminum
---
6,748.00
13.496
_
Arsenic
---
2.50
0.005
Cadmium
---
1.20
0.002
Chromium
---
23.000
---
Copper ---
---
_-- 781.00
1.562
Lead
---
92.00
92.00
0.184
Mercur
_
-
0.61
0.001
Mol bdenum
---
5.00
0.010
Nickel
---
14.00
0.028
Selenium
5.00
0.010
Zinc
---
2,707.00
5.414
Fnvironrnent 1 a 348 A
*Determination of Plant Available Nitrogen (PAN):
injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nio-ate N 1 Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N)+ Nihate N + Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

o
I ji
Willi n� L�i1I�II , l;0 ,i..J
G? EEN`dlLLE NX121c35-7085
POINT EMERALD VILLAS (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH, Units
8.2
02/06/18
KDS
4500HB-11
Aluminum, ((try wt. basis), mg/lig
6748
02/09/18
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/14/18
MTM
311313-04
Calcium (dry wt. basis), mg/kg
23343
02/09/18
LrJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.2
02/13/18
MTNI
31138-04
Copper (dry wt. basis), mg/kg
781
02/09/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/I(g
23
02/09/18
LEJ
EPA200.7
Lead (dry weight basis), mg/kg
92
02/12/18
MTM
311313-04
Magnesium (dry wt. basis), mg/kg
2057
02/09/18
LrJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.61
02/12/18
LFJ
EPA7471B
Nickel (dry wt. basis), mg/kg
14
02/09/18
LFJ
EPA200.7
Potassium ((try wt. basis), mg/kg
2794
02/09/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/14/18
MTM
3113B-04
Sodium ((try wt, basis), nig/lig
28403
02/09/18
LFJ
EPA200.7
Zinc (dry wt. basis), mg/1(g
2707
02/09/18
LFJ
EPA200.7
Total Solids, %
0.40
01/18/18
KDS
2540G-11
TKN (dry wt.), mglkg
c 44820
02/05/18
MF
351.2 R2-93
Annuonia Nitrogen ((fry wt.),mg/kg
c 105.4
02/19/18
CLO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 12270
02/05/18
DTL
365,4-74
Nitrate -Nitrite (dry wt.), rng/1(g
c 123.2
02/13/18
MF
353.2 R2-93
Molybdenum ((fry wt. basis), mg/1(g
<5.0
02/09/18
LFJ
EPA200.7
1"2)
ID#: 348 A
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/20/18
REVIEWED BY: %
c 4nc er::f iad data. Dll3 doe, not offer non-aqueovo ce.rti ficatior. for thio analytical piccedu:e.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: June 21, 2018
Permit No. WQ0018525
Queens Cour 0.24 % Solids
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)( I(N-Ammonia N) + Ammonia N + Nitrate N a- Nitrite N — % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation proposes.

Environmental Chemists, Inc.
!; f
(.602 Windmill Vviy, Wilmington, N( .4405 ° 9103/20)23 La I, ° 910.392.4 124 Fax
710 Bowsertomi Road, Manlco, NC 279' ;1 ° 252.173 5702 1 ab/pax
255-A Wilmington I lighway; lar r;onvill", W 2SW ° 910.347.;843 1.abj Fax
ANALYTICAL & CONSULTING CHEMISTS inli�(<gcnviro0nunuilchemisis.com
Fortin Contract Services
Date of Report: Jun 21, 2018
Post Office Box 4188
Customer PO #:
Emerald Isle NC 28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2018-06910
Calcium
Project ID: Queens Court
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
18-17240 Site: Sludge
5/2/2018 9:22 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
3150 mg/kg
05/16/2018
Calcium
EPA 200.7
24700 mg/kg
05/09/2018
Chromium
EPA 200.7
<190mg/kg
05/16/2018
Copper
EPA 200.7
408 mg/kg
05/16/2018
Lead
EPA 200.7
<190 mg/kg
05/17/2018
Magnesium
EPA 2001
7250 mg/kg
05/09/2018
Nickel
EPA 200.7
<190mg/kg
05/17/2018
Potassium
EPA 200.7
21100 mg/kg
05/09/2018
Sodium
EPA 2001
68800 mg/kg
05/11/2018
Zinc
EPA 200.7
2140 mg/kg
05/17/2018
Arsenic
EPA 200E
<3T9 mg/kg
05/30/2018
Cadmium
EPA 200.8
<37.9 mg/kg
05/30/2018
Molybdenum
EPA 2009
<37.9 mg/kg
05/30/2018
Selenium
EPA 200.8
<37.9 mg/kg
05/30/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
38.9 mg/kg
05/10/2018
Total Solids (%)
SM 2540 8
0.24%
05/03/2018
pH
SM4500H8
6.84 units
05/15/2018
Ammonia Nitrogen
SM 4500 NH3 C
1230 mg/kg
05/07/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 org o
131000 mg/kg
05/07/2018
Total Phosphorus
SM 4500 P F
30700 mg/kg
05/10/2018
Mercury
Sw54674710
<7.08 mg/kg
05/05/2018
Comment: Sludge residuals, except
pH, reported on a dry weight basis.
pH reported on an as received basis.
Reviewed by:
Report #. 2018.03910 Page i of 1

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13ARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 16, 2018
Permit No. W00018525
Sands Villas 2.71 %Solids
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N 9- Nitrate N � Nitrite N = % PAN
Surface Application:
(Mineralization Rate)("PKN-.Ammonia N) + (0.5)(Ammonia N) -I Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Defected) or < detection limits are listed as detection limits
for calculation purposes.

11111l 1pil ����� iLt��)�.'l(j) il,
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G N'IVI_L N.C. 27858
SANDS VILLA (HYDROTECH)
DON O'MARA
HYDRO'TECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
ID#: 559
DATE COLLECTED: 01/16/18
DATE REPORTED : 02/14/18
REVIEWED BY:
ur:ce rt J. f iad data. DWR d.eI not a. fer mn- vqueeuu —al;l f. ca c i cr. Co- this .,aalytieal g: oc ¢dare.
Sludge
Analysis
Method
PARAME9'ERS
Sample
Date Analyst
Code
PIl (not to be used for reporting)
7.4
01/16/18
JTH
45001IB-11
Aluminum, (dry wt, basis), mg/Icg
4309
01/23/18
LFJ
EPA200.7
Arsenic (dry wt, basis), mg/kg
<2.5
01/25/18
MTM
311313-04
Calcium (dry wt. basis), mg/kg
44850
01/23/18
LFJ
EPA200.7
Cadmium (dry wt, basis), mg/kg
0.98
01/25/18
rwrM
31138-04
Copper (dry wt. basis), mg/kg
325
01123/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),nig/Icg
15
01/23/18
LF.I
EPA200.7
Lead (dry weight basis), mg/kg
11
01/23/18
M1'M
3113B-04
Magnesium (dry wt. basis), mg/Icg
3798
01/23/18
LFJ
FPA200.7
Mercury (dry wt. basis), mg/kg
0.31
01/29/18
LFJ
EPA747113
Nickel (dry wt. basis), mg/kg
12
01/23/18
LFJ
EPA200.7
Potassium (dry wt, basis), mglkg
2077
01/23/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/24/18
M'PNf
3113B-04
Sodium (dry wt. basis), mg/kg
5048
01/24/18
AIN
3111B-11
Zinc ((try wt. basis), mg/lig
1187
01/23/18
LFJ
EPA200.7
Total Solids, %
2.71
01/18/18
KDS
2540G -1I
THIN (dry wt.), mg/kg
c 53070
02/05/18
MF
351.2 122-93
Ammonia Nitrogen (dry wt.),nng/Icg
c 1717
02/08/18
CNLi,
350.1 R2-93
Phosphorus, T. (dry wt.), mg/Icg
c 13210
02/05/18
DTL
365.4-74
Nitrate -Nitrite (dry wt.), nig/kg
e 3.90
02/13/18
MF
353.2 IU -93
Molybdenum (dry wt. basis), mg/lig
<5.0
01/23/18
LFJ
EPA200.7
ID#: 559
DATE COLLECTED: 01/16/18
DATE REPORTED : 02/14/18
REVIEWED BY:
ur:ce rt J. f iad data. DWR d.eI not a. fer mn- vqueeuu —al;l f. ca c i cr. Co- this .,aalytieal g: oc ¢dare.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2018
Permit No. WO0018525
Sea Isle Plantation 0.33 % Solids
12.25 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
'(% x 10,000)
Pounds/Dry Ton
(Mglkg x 0.002
Nitrogen (TKN)
1.917
36,290.000
72.580
Phosphorus
0.675
9,091.000
18.182
Potassium
0.452
6,261.000
12.522
PAN injected)*
0.581
5,810.088
11.620
PAN surface)*
0.577
5,771.268
11.543
Ammonia Nitrogen
0.008
1,552.000
3.104
Calcium
4.831
25,493.000
50.986
Calcium Carbonate Eq,
---
---
---
Magnesium
---
3,300.000
6.600
Sodium
-
31,191.000
62.382
Sulfur
---
---
Nitrate N / Nitrite N
---
5.940
0.012
Barimn
---
---
Chloride
---
---
Iron
---
---
Aluminum
---
1,554.00
3.108
Arsenic
---
2.50
0.005
Cadmium
---
0.82
0.002
Chromium
---
9.000
---
Copper
122.00
0.244
Lead
---
27.00
0.054
Mercury
---
0.02
0.000
Molybdenum
---
5.00
0.010
Nickel
---
11.00
0.022
Selenium
5.00
0.010
Zinc
---
667.00
1.334
Environment 1 N 96A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Antmonia N) + Nitrate N Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

, 11
C-V4�U"Q
SEA ISLE PLANTATION
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry -wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (thy wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt, basis),mg/lig
Lead (dry weight basis), mg/lig
Magnesium (dry wt. basis), mg/lig
Mercury (dry wt. basis), mg/lig
Nickel (dry wt. basis), nig/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry w(, basis), mg/lig
Sodium (dry wt. basis), nig/kg
Zinc (dry wt. basis), mg/kg
Total Solids,
TKN (dry wt.), mg/lig
Ammonia Nitrogen ((try wt.),mg/kg
Phosphorus, 1'. (dry wt.), mg/lig
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
1554 01/23/18 LFJ EPA200.7
<2.5 01/25/18 MTM 3113B-04
25493 01/23/18 LFJ EPA200.7
0.82 01/25/18 MINI 3113B-04
122 01/23/18 LFJ EPA200.7
9 01/23/18 LFJ EPA200.7
27 01/23/18 M'FNi 3113B-04
3300 01/23/18 LFJ EPA200.7
<0.02 02/12/18 LFJ EPA7471B
11 01/23/18 LFJ EPA200.7
6261 01/23/18 LFJ EPA200.7
<5.0 01/24/18 MTM 3113B-04
31191 01/24/18 JMN 3111B-11
667 01/23/18 LFJ EPA200.7
0.33 01/18/18 KDS 254OG-11
c 36290 02/05/18 MF 351.2 R2-93
c 1552 02/19/18 CLO 350.1 R2.93
C 9091 02/05/18 DTL 365.4-74
c 5.94 02/13/18 MF 353.2 82.93
11203 02/21/18 SE.1
<5.0 01/23/18 LFJ EPA200.7
ID#: 96 A
DATE COLLECTED: 01/17/18
DATE REPORTED : 02/21/18
REVIEWED BY:
c Uncertified data. DWR doeo not offor non-aqueouo certification for thio anal7ticul procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 29, 2018
Permit No. WO0018525
Sea Surav 2.49 % Solids
6.7 ull
Parameter
%Mglh g Dry �4�ight
'j%,x 0,400)
Pounds/Dry Tou,
(MglKg x 9 002) ;,
Nitrogen (TKN)
2.885 42,550.000
85.100
Phosphorus
0.416 15,730.000
31.460
Potassium
0.100 3,575.000
7.150
PAN in'ected)`
0.889 8.887.150
17.774
_
PAN surface *
0.873 8,728.150
17.456
Ammonia Nitrogen
0.032 3,141.000
6.282
_
Calcium
3.890 48,546.000
97.092
Calcium Carbonate B
--- ---
---
Magnesium
3.480.000
_
6.960
Sodium
_
- 3,398.000
6.796
Sulfur
--- ---
Nitrate N /Nitrite N
--- 8.950
0.018
Barium
---
-
_
Chloride
--- ---
---
Iron
--- ---
---
Aluminum----
---- 2,942.00
5.884
Arsenic
_ 2.50
Cadmium
--- 0.63
_0.005
— - 0.001
_
Chromium
--- 10.000
_ _
PCo . er
--- 1,056.00
-�� 2.112
____
Lead
__
--- 11.00
0.022
Mercury
0.17
0,000
Molybdenum
--- 5.00
0.010
Nickel
14.00
0.028
SCIen IUnt
5.00
0.010
Zinc
--- 977.00
1.954
Environment I K 560
'Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rale)(TKN-Ammonia N) , Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) * Nitrate N + Nitrite N = %b PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

.'� ,a 1�� �
1.11 'P'1o)11'1o(6)I Ce i'e
SEA SPRAY (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
ID#: 560
DATE COLLECTED: 01/29/18
DATE REPORTED : 02/28/18
REVIEWED BY:��
.. UnC ertif.icd data. MOR eoe3 not of Fer no.. aque:oun c.Z t_f icat ion :or tSis un :ytrcul jarOCA dura.
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PH (not to be used for reporting)
6.7
01/30/18
JTH
450OH13-IL
Aluminum, ((try wt. basis), mg/lig
2942
02/20/18
LFJ
EPA200.7
Arsenic ((try wt. basis), mg/kg
<2.5
02/21/18
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
48546
02/20/18
LFJ
CPA200.7
Cadmium (dry wt. basis), mg/lig
0.63
02/20/18
MTM
3113B-04
Copper ((try wt. basis), mg/kg
1056
02/20/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
10
02/20/18
LFJ
EPA200.7
L,cad (dry weight basis-), mg/kg
11
02/19/18
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
3480
02/20/18
LFJ
EPA20047
Mercury (dry wt. basis), mg/kg
0.17
02/21/18
M1'M
EPA7471B
Nickel (dry wt. basis), 1119/Icg
14
02/20/18
LEJ
EPA200.7
Potassium (dry wt4 basis), mg/kg
3575
02/20/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/22/18
MTM
311313-04
Sodium (dry wt, basis), mg/kg
3398
02/20/18
LFJ
EPA200.7
Zinc ((try wt. basis), mg/Icg
977
02/20/18
LFJ
EI'A200.7
Total Solids, %
2.49
02/01/18
KAC
2540G1 I
TKN (dry wt.), mg/lig
c 42550
02/22/18
CML
351.2 R2-93
Ammonia Nitrogen ((Try wt.),mg/Icg
c 3141
02/20/18
CML
350.1 R2-93
Phosphorus, T, (dry wt.), mg/kg
c 15730
02/22/18
DTL
365.4-74
Nitrate -Nitrite (dry wt.), urg/kg
c 8.95
02/21/18
CLO
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
02/20/18
LFJ
EPA200.7
ID#: 560
DATE COLLECTED: 01/29/18
DATE REPORTED : 02/28/18
REVIEWED BY:��
.. UnC ertif.icd data. MOR eoe3 not of Fer no.. aque:oun c.Z t_f icat ion :or tSis un :ytrcul jarOCA dura.

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BARNES ENVIRONMENTAL. WASTE
LAND APPLICATION PROGRAM
RCSIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 31, 2018
Permit No. W00018525
Sound Of The Sea 1.66 % Solids
7.3 PH
3 ram
g/1�g Qrv, 'eight Pougi#slDry TdA
Nitrogen (TKN)
2.885
46,900.000 93.800
Phos horns
0.416
20,100.000 40.200
Potassium
0.100
2,885.000 5.770
PAN injected)`
0.888
_
8,881.140 17.762
PAN surface)*
0.872
8,722.140 17.444
AmntoniaNitiogen
0.032
1,625.000 3.250
_
Calcium
3.890
_
33,202.000 66.404
Calcium Carbonate Eq.
---
---
Ma_gnesiunt
---
10,353.000 20.706
Sodium
6,150.000 12.300
Sulfur
- --
- --- ---
Nitrate N"/ NiUite N
---
2.940 0.006
---
[larium
---
---
Chloride
_
---
---
_
Cron
---
- --- --
Aluminum
---
_
5,038.00 10.076
Arsenic
--
2.50 0.005
Cadmium
_
---
_
1.50 0.003
_
Chromium
16.000
Co er _
---
------_—__ 2,825.00 —_ -- 5.650
Lead
---
96.00 0.192
Mercur
---
0.21 0.000
'Molybdenum
---
_
5.00 0.010
_
Nickel
13.00 0.026
Selenium
5.00 0.010
Zinc
---
_
2,159.00 4.318
Environmem 1 S 561
"Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Ratc)(TKN-Ammonia N) + Ammonia N . Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N) = Nitrate N + Nitrite N % PAN
Note: Constituents N.D. (Not Detected) or <delection limits are listed as detection limits
for calculation purposes.

SOUND OF THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, ((try wt. basis), mg/kg
Arsenic (dry wt. basis), mg/1(g
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium ((try wt, basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/1(g
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/1(g
Sodium (dr ;y w(. basis), mg/kg
Zinc ((try wt. basis), nrglkg
Total Solids, %
TKN ((try wt.), nig/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T, (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), nig/I(g
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date .Analyst Code
7.3 02/01/18 JTH 45001 -11
5033 02/26/18 LFJ EPA200.7
2.5 02/26/18 MTM 311313-04
33202 02/26/18 LFJ EPA200.7
1.5 02/26/18 MTM 3113B-04
2825 02/26/18 LFJ EPA200.7
16 02/26/18 LFJ EPA200.7
96 02/23/18 MTM 311313-04
10353 02/26/18 LFJ EPA200.7
0.21 02/21/18 NITi11 EPA7471B
13 02/26/18 LFJ EPA200.7
2885 02/26/18 LFJ EPA200.7
<5.0 02/22/18 MTM 3113B-04
6150 02/26/18 LFJ EP.A200.7
2159 02/26/18 LFJ EPA200.7
1.66 02/06/18 AKS 2540G-11
c 46900 02/22/18 CML 351.2 R2-93
c 1625 03/06/18 MF 350.1 R2-93
c 20100 02/22/18 DTC, 365.4-74
c 2.94 02/23/18 MP 353.2 R2-93
5 02/26/13 LFJ EPA200.7
ID#: 561
DATE COLLECTED: 01/31/18
DATE REPORTED : 03/08/18
REVIEWED BY;
c Unce rti f: cd dd-a. JWR do ...- o-.r_r -ac(aeoae cert if l cbt'i w: .or Lhid and lytiaul Frnc educe.

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I3ARNLS LNVIRONMLNTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 25, 2018
Permit No. WO0018525
Southwinds Condontiniams 1.64 %Solids
Inrironmeni 1 i; 562 B
Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N -t Nitrite N = % PAN
Surface Application:
(Mineralization Rale)(FK'N-Ammonia N) + (0.5)(Ammonia N) + 1`iitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

SOUTHWINDS (HYDRO'PECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), rug/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg/Icg
Chromium, T.(dry wt, basis),mg/Icg
Lead (dry weight basis), mg/kg
Nlagnesimn (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/Icg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt, basis), mg/Icg
Total Solids, %
'PI{N (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg,
Phosphorus, T. (dry wt.), mg/lig
Nitrate -Nitrite (dry wt.), mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.1 01/25/18 J'rH 4500HB-11.
4283 02/20/18 LFJ EPA200.7
<2.5 02/21/18 NIT N1 3113B-04
63451 02/20/18 LFJ EPA200.7
0.50 02/22/18 MTM 311311-04
967 02/20/18 LFJ EPA200.7
12 02/20/18 LFJ EPA200,7
15 02/19/18 MTM 311313-04
3188 02/20/18 LFJ EPA200.7
0.23 02/12/18 LF.1 LPA747111
9 02/20/18 LFJ EPA200.7
2809 02/20/18 LFJ EPA200.7
<5.0 02/22/18 MTM 311313-04
4058 02/20/18 LB.L EPA200.7
1593 02/20/18 LFJ EPA200.7
1.64 01/25/18 MAR 254OG-11
c 65980 02/20/18 MF 351.2 R2-93
c 15.63 02/20/18 CML 350.1 132-93
c 17230 02/20/18 DTI, 365,4-74
c 56.64 02/21/18 CLQ 353.2 R2-93
<5.0 02/20/18 LFJ EPA200.7
TD#: 562 B
DATE COLLECTED: 01/25/18
DA'Z'E REPORTED : 02/28/18
REVIEWED BY: ,
UncoYti fled da a. DWR cues r0[ offer non-aque0is certi EJ c aC ion fo:: t:, .te analytical procedure.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual'Pype: Wastewater Treatment Plant
Date Sampled: January 25, 2018
Permit No. WQ0018525
Summer Winds 2.54 %Solids
Environment 1 4 1 19A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)('rKN-Ammonia N) ' Ammonia N -� Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) , Nitrate N+ Nitrite N = %PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

SUMMERWINDS HOA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARANIFFERS
PH blot to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt, basis), mg/lig
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
A4ercury (dry avt. basis), ntg/lig
Nickel (dry wi. basis), mg/kg
Potassium (dry wt. basis), mg/lig
Selenium (dry wt. basis), mg/lag
Sodium (dry wt. basis), mg/lig
Zinc (dry wt. basis), mgdkg
Total Solids, %
TION (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. ((try wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt, basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.4 01/25/18 JTH 4500HB-11
3291 02/20/18 LFJ EPA200.7
<2.5 02/21/18 MTM 3113B-04
52829 02/20/18 LFJ EPA200.7
0.85 02/20/18 MTM 3113E-04
623 02/20/18 LFJ EPA200.7
8 02/20/18 LFJ EPA200.7
14 02/19/18 MTM 3113B-04
5249 02/20/18 LFJ EPA200.7
0.13 02/12/18 LFJ EPA7471B
12 02/20/18 LPJ EPA200.7
2960 02/20/18 LFJ EPA200.7
<5.0 02/22/18 MTM 3113B-04
10635 02/20/18 LFJ EPA200.7
3122 02/20/18 LFJ EPA200.7
2.54 01/25/18 iYIAR 2540G-11
c 46110 02/16/18 CLO 351.2 R2-93
c 1760 02/20/18 CML 350.1 82-93
c 15750 02/16/18 CML 365.4-74
c 3.94 02/21/18 CLO 353.2 R2-93
5 02/20/18 LFJ EPA200.7
ID#: 119 A
DATE COLLECTED: 01/25/18
DATE REPORTED : 02/28/18
REVIEWED BY: _
Unce•_tificd Seta. Ines uoo» not nP.[er voi.-I'o eou3 ce_c if ica!; ion for r.114 analytical Proc�du:'e.

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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 6, 2018
Permit No. WO0024756
The Grove WWTP 0.24 % Solids
7.2 uH
Environment 1 N 549 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N i- Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) 1- (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
Nitrogen (TKN)
5.800
58,000.000
116.000
Phos horns
2.067
_
20,670.000
41.340
Potassium
1.116
11,159.000
_
22.318
jected ^
1.779
17,794.260
_
35.589
urface *
r
1.752
17_,519.010
_
35.038
ia Nitrogen
0.055
550.500
I.10I
3.556_
35,559.000
71.118
Calcium Carbonate F...
---
--
_
--
Ma nesiurn
---
4,803.000
9.606
Sodium
---
44,089.000
_
88.178
Sulfur —
------
----'.
Nitrate N / Nitrite N
_
--
8.910
0.018
Barium
Chloride
--
--
---
---
---
BAR
IF,
trop
Aluminum __--
— ---
--- -- 2346.000
4.692
Arsenic
---
2.50
0.005
_ 75
Cadmium___
— ---------_---"--"
0.79
_
0.002
85
--_
Chromium-
--_—__--11._000
copperr
_—_
128.00
__---
0.256
4,300
Lead
---
7.70
_
0.015
840
Mercm ,
_
0.26
_
0.001
57
Molybdenum
_
_
5.00
0.010
75
_
Nickel
---
11.00
0.022
420
Selenium_
---
5.00
0.010
100
Zinc
597.00
1.194
7,500
Environment 1 N 549 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N i- Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) 1- (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

( mw0ff@lmHgM % hm
THE GROVE WWTP (HYDROTECH)
ATTNi DON O-MARA
HYDROTECH
P,O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETliRS
Pit (not to be used for reporting)
Aluminum, (dry w(. basis), mg/hg
Arsenic (dry }vl, basis), mg/Icg
Calcium (dry wt. basis), mg/l(g
Cachnhnn (dry w(, basis), mglkg
Copper (dry wt, basis), mg/hg
Chromium, T.(dvy rvl, basls),ntg/kg
Lead (dry weight basis), mg&g
Magnesium (dry wk basis), mg/kg
Mercury (dry wt, basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt, basis), mg/1%
Selenium (dry wl, basis), mg/Icg
Sodh:m (dry wt. basis), mg/kg
Zh:c (dry wL basis), mg'
/kg
Total Solids, 0/0
TKN (dry wt.), mg/Icg
Ammonia Nil rogeu Wry wt.),mg/kg
Phosphorus, T. (dry NY(.), mg/Icg
Nitrate-Nilthe (dry w(.), mgfltg
Molybdenum (dry evi. basis), mgli(g
Sludge
Analysis
Method
Sample
Date
Analyst
Code
7.2
02/06/18
JTH
45001-113.11
2346
02/26/18
LFJ
CPA200.7
<2.5
02/26/18
MTM
311313-04
35559
02/26/18
LFJ
GPA200.7
0.79
02/26/18
MTM
3113B.04
128
02/26/18
I VJ
CPA200.7
11
02/26/18
LFJ
BPA200.7
7.7
02/23/18
MTM
31138-04
4803
02/26/18
LPJ
GPA2K7
0.26
02121/18
MTM
El'A7471B
11.
02/26/18
LFJ
GPA200.7
11159
02/26/18
LCJ
EPA200,7
<5,0
02/22/18
MT1M
311313.04
44089
02/26/18
LPJ
LPA200,7
597
02/26/18
LFJ
CPA200.7
0.24
02/07/18
MAR
2,540G-11
c 58000
02/22/18
CML
351.2 R2-91
c 550.5
03/06/18
MP
350.1 122.93
c 20670
02/22/18
DTL
365.4-74
c 8.91
03/01/18
DT).,
353,2 R2-93
<5,0
02/26/18
LFJ
LPA200,7
IDQ: 549 A
DATE COLLECTED1 02/06/18
DATE REPORTED : 03/08/18
REVIEWED BY:
c ana9aGt G I o dut.o. e, Aoeu noe of Eu: nen aquewe cor.ti Eiaotiun [ox ,;hAn unnlyo]aa1 Vruuu dvzc.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 23, 2018
Permit No. WQOO18525
Whaler Inn 0.43 %Solids
7.3 pH
I�ai•ameter
°Xo � , ,it?gJKgDr�'�'YetgLt
1Pou�tls7Dty' !'On , y
Nitrogen (TKN)
1.601
25,540.000
51.080
0.397
16,880.000
33.760
IPliosphorus
potassium
0.399
4,054.000
8.108
PAN injected)*
0.502
5,015.170
10.030
PAN surface)*
0.487
4,870.170
9.740
Ammonia Nitrogen
0.029
67.730
0.135
Calcium
5.591
65,245.000
130.490
Calcium Carbonate Eq.
---
---
---
Ma nesium
3,810.000
7.620
Sodium
76,392.000
152.784
Sulfur
---
---
---
Nitrate N / Nitrite N
---
7.970
0.016
Barium
---
---
---
Chloride
---
---
---
11011
---
--- -
---
Aluminum
---
2,579.00
_
5.158
_
Arsenic
---
2.50
_
0.005
Cadmium
---
0.55
0.001
Chromium
---
7.000
---
Copper
530.00
1.060
Lead
---
7.30
0.015
,.Mercury_
---
0.15
0.000
Molybdenum
---
5.00
0.010
Nickel
6.00
0.012
Selenium
5.00
0.010
Zinc
---
829.00
1.658
Environment 1 d 70A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Nlineralization Rate)(TKN-Ammonia N) I- (0.5)(Ammonia N) -t- Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

THE WHALER INN
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/lig
Calcium ((try wt. basis), mg/Icg
Cadmium (dry wt, basis), mg/lig
Copper (dry wt. basis), mg/Icg
Chromium, T.(dry wt. basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium ((try wt. basis), mg/kg
N4ercury (dry wt. basis), nig/hg
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium ((try wt, basis), mg/kg
Sodium ((try wt. basis), mg/kg
Zinc (dry wt. basis), mg/Icg
Total Solids, %
TKN ((try wt.), mg/kg
Ammonia Nitrogen ((try wt.),mg/Icg
Phosphorus, T. (dry wt.), nig/lig
Nitrate-Nihite (dry wt.), nig/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), nig/lig
Sludge Analysis Method
Sample Date Analyst Code
7.3 08/23/18 HNIM 4500IM-11
2579 09/20/18 LFJ EPA200.7
<2.5 09/25/18 MTM 3113B-04
65245 09/20/18 LFJ EPA200.7
0.55 09/21/18 MTM 3113B-04
530 09/20/18 LFJ EPA200.7
7 09/20/18 LFJ EPA200.7
7.3 09/20/18 MTM 311311-04
3810 09/20/18 LFJ EPA200.7
0.15 08/31/18 MTM EPA7471B
6 09/20/18 LFJ EPA200.7
4054 09/20/18 LFJ EPA200.7
<5.0 09/27/18 NfCM 3113B-04
76392 09/20/18 LFJ EPA200.7
829 09/20/18 LFJ EPA200.7
0.43 08/23/18 JMS 254OG-11
c 25540 08/28/18 DTL 351.2 R2-93
c 67.73 09/11/18 BLD 350.1 R2-93
c 16880 08/28/18 CLO 365.4-74
c 7.97 09/19/18 DTL 353.2 112-93
5136 09/19/18 SEJ
<5.0 09/20/18 LFJ EPA200.7
ID#: 70 A
DATE COLLECTED: 08/23/18
DATE REPORTED : 10/11/18
r\ r
�L
REVIEWER BY:t)
e kj1<orCi fi ed dot I. DWR tleen :,oC offer n.n-<ogl,00uo corti f iCdl 1411 foz Cilie a:j a i y C1 C o pro e a d'J=e.

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PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION DORM (02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number: W00018525
WWTP Name: SEC ATTACHED LIST NPDES Nmnber: SPEATTACHED
Monitoring Period: Front I/I/2018 110 12/31/2018
Pathogen Reduction (15A NCAC 021'.1106) - Please indicate level achieved and alternative performed:
Class A:
A (timehem >) E] I Alt B (Alk Treattzzenti) p Alt. C (Prior Testin . 0
JAIt. 2 (40 -day bench) L]
Alt. 3 (30 -day bench) ❑ JAIt. 4 (Spec. 02 uptake)
_Alt.
Alt.D (Ano Prior Test) E7 Process to Further Reduce Patho en>s E7
Alt. 5 (14 -Day Aerobic)
If applicable to alternative performed (Class A only) indicate "Process to Farther Reduce Pathogens":
Compost ❑
1lcat Drying 0
ileal 1'reatmeat ❑ Thermo zlulic Cl
Beta RaZ 0
Gamma Ray t
Pasteurization
_Class B:
JAIt. (1) Pccal Density T-1
Alt. (2) Process to Significantly Reduce Pathogens O
If applicable to alternative performed (Class B only) indicate "Process to Significantly e( lice Pathogens":
Limo Stabilization E Air Drying U Com hosting Cd Aerobic Digestion Ll
Anaerobic Digestion Ll
If applicable to alternative perforined (Class A or Class B) complete the following
monitorin data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
Excee-
Frequency
of Analysis
sample
Type
na y ica
Tech-
MinimUll
Geo. Mean
MaXiM1,1111
Units
Fecal Coliform
2 x 10 to the
Gth power
per gram of
total solids
MPN
CPU
1000 mph per gram
oftotalsolid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grains
total solid (dry
wei hY
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt.] (VS reduction)
E]
JAIt. 2 (40 -day bench) L]
Alt. 3 (30 -day bench) ❑ JAIt. 4 (Spec. 02 uptake)
CI
Alt. 5 (14 -Day Aerobic)
❑
Alt. 6 (Alk. Stabilization Ll
IAR 7 (Drying - Stable) Cl JAR. 8 (Drying - Unstable,)
D
AIt. 9 (Injection)
0
All. 10 (Incorporation) LJ
INo vector attraction reduction alternatives were perforated
LI
CERTIIjICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02'1'.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you clieck this statement attach an explanation why you have not met oa(. or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate tine information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes, President _
Preparer NameandTitle (type or print) Land Applier Name and Title (if appiicable)(type or print)
1
Signature of Preparer" Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CPR Part 503.9(x) and 15A NCAC 2T.1 102 (26)
DENR FORM PVRF 02T (1212006)

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2018 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit # WQ 0018525
RESIDUALS APPLICATION
Totals jLjL.70_JL549,000_jj 31.0711
Total Gallons 549,000
W WTP - Metric Tons 28.18
2018 APPLICATION
SUMMARY
FARM NAME
I APPL
DATE
FIELD
NO.
I ACRES
USED
TOTAL
WW -GALS.
TOTAL
WW -DT
PAN (lbs/ac)
Crop 1 Crop 2
Will Turner
2018
1
6.20
66,500
3.85
15.18
0.00
Site WT
2018
2
5.00
114,000
6.12
28.44
11.30
2018
3
8.00
122,500
5.05
10.47
0.57
2018
5
2.60
94,500
5.79
48.07
34.47
2018
6
2.90
151,500
10.26
71.48
15.39
It -
Totals jLjL.70_JL549,000_jj 31.0711
Total Gallons 549,000
W WTP - Metric Tons 28.18

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SOIL ANALYSIS REPORTS

All residual sources land applied by Barnes Environmental Waste and Hauling, Inc. (Barnes
Environmental) during the 2018 calendar year were lime stabilized to meet Pathogen and Vector
Attraction Reduction monitoring. Therefore lime additions are continually applied to the fields
throughout the year through land application.
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist

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