NC0004944_Other Correspondence_20190212

tt Dewberr Dewberry Engineers Inc. 919.881.9939
y 2610 Wycliff Road,Suite 410 919.881.9923 fax
Raleigh,NC 27607 www.dewberry.com
February 12,2019 RECEIVED/DENR/DWR
NC Department of Environmental Quality—NPDES Complex Permitting Unit FER 15 2019
Attn:Sergei Chernikov,Engineer
Archdale Building Water Resources
512 N.Salisbury Street Permitting Section
Raleigh,NC 27699
RE:Edge Water Treating,LLC—NPDES Permit NC0004944-Total Nitrogen Limit
Dear Mr.Chernikov:
On behalf of our client,Edge Water Treating,Dewberry respectfully submits this letter to propose a total
nitrogen limit for the Edge Water Treating wastewater treatment plant located in Salisbury,NC(Salisbury
Facility). The Salisbury Facility discharges wastewater into the High Rock Lake watershed under NPDES
Permit NC0004944 and has recently submitted a NPDES permit modification request to modify the
permit from an Organic Chemical,Plastics and Synthetic Fiber(OCPSF)category 414 to Centralized
Waste Treatment category 437.Based on subsequent conversations with NC DEQ,it is our understanding
that NC DEQ intends to implement an effluent numerical total nitrogen(TN)limit within the modified
permit. NC DEQ indicated that a TN limit is required to freeze TN discharges at 2004 discharge levels
during the interim period prior to finalization of a formal nutrient strategy for High Rock Lake.We
understand High Rock Lake was added to the NC 3o3d list in 2004 for chlorophyll a and turbidity.
•
NC DEQ preliminarily suggested an effluent TN limit of 33.51b/d.NC DEQ indicated this limit is not
based on historical data from the Salisbury Facility but on the total nitrogen discharge of a similar OCPSF
facility. The similar facility has not been identified.As previously indicated,Edge Water Treating is very
concerned with the proposed limit as its basis is not well defined,and as the limit will have significant
implications on redevelopment of the site and its financial viability.Total nitrogen discharges from
OCPSF facilities can vary significantly depending on specific operations within the facility,the wastewater
treatment infrastructure utilized,and the operational strategy of the wastewater treatment plant.As the
proposed limit is not based on historical data from the Salisbury Facility,it is not representative of the
2004 discharges from the Salisbury facility and could be overly restrictive and inconsistent with the intent
to freeze discharges at 2004 levels.
At the time of our January 23,2019 meeting with NC DEQ,historical total nitrogen data from the
Salisbury Facility had not been identified.NC DEQ indicated that in the absence of site specific historical
data,NC DEQ would consider an alternate proposed limit to be based on effluent data from multiple other
OCPSF facilities,estimation/modeling of 2004 total nitrogen discharges from the Salisbury Facility,or a
combination of both.
To develop a proposed total nitrogen limit,Dewberry reviewed the following:
• Historical NC0004944 files retrieved from NC DEQ Central File archives
• Discharge data from four other OCPSF polyester fiber dischargers.
The files retrieved from archive contained limited historical total nitrogen data for the Salisbury Facility
which included the following:
• August 1992—July 1992:Once per month sample analyzed for total nitrogen
• January 2009—December 2009: Once per month sample analyzed for total nitrogen
Page 1 of 3

Copies of the files referenced above are provided in Attachment A.The 2009 samples were collected
immediately after the Salisbury Facility was sold from Invista to Performance Fibers;it is our
understanding that by 2009 Performance Fibers had significantly reduced staff and production
operations at the Salisbury Facility. As such,the 2009 data is not representative of 2004 discharge
conditions and is not used for this evaluation.The 1992/1993 data represents a time when the Salisbury
Facility was operating at full production capacity and is deemed the most representative to use in the
evaluation to estimate 2004 discharges.
An anaerobic treatment system(Celrobic®)for contaminated groundwater was operated at the Salisbury
Facility from approximately 1994—2004.The effluent from the Celrobic®system was discharged to the
Salisbury Facility's wastewater treatment plant(WWTP). The Operation Manual for this system was
obtained from the Salisbury Facility control room and excerpts are provided in Attachment B. The
Operation Manual indicated the system included an ammonia addition system to provide nutrients for the
anaerobic organisms. The Operation Manual instructed that ammonia be dosed to achieve an excess of •
3o mg/l in the anaerobic system effluent which was designed to operate at ioo,80o gallons per day. The
Operation Manual also indicated that biomass was wasted from the Celrobic®system to the WWTP.
Therefore the Celrobic®effluent would be expected to contain two primary forms of total nitrogen:
excess ammonia at 3o mg/land insoluble organic nitrogen from the wasted biomass.
As the Celrobic®system was not operational until 1994,the 1992/1993 data presented above would not
capture the total nitrogen discharges from the Celrobic®system. The Celrobic®system was operated
until 2004 and thus it is assumed to have been operated during the period the impairment was identified
in High Rock Lake.As such,it is valid to include nitrogen contributed from this system in this evaluation
if the intent is to freeze nitrogen dischargers at the time the impairment was identified. In addition,the
Consent Order(date October 4,2000)is still active and the Celrobic®system may be operated again in
the future if groundwater monitoring indicates additional remediation is required.Excerpts from the 2017
Annual Groundwater Report by CAN Holdings LLC are provided in Attachment D.
To estimate the total nitrogen effluent discharges attributable from the Celrobic®system,Dewberry
assumed the residual effluent ammonia would pass through the WWTP and the nitrogen present in the
waste sludge would be hydrolyzed in the WWTP and both would be discharged in the WWTP effluent.The
additional chemical oxygen demand load from the anaerobic effluent would result in additional sludge
generation at the WWTP and a portion of the nitrogen would be used by the WWTP to support that cell
growth.The calculations presented in Attachment B include an estimate of the sludge generated as a
result of the anaerobic system and subtracts the nitrogen that would report to that biomass.The model
calculations and supporting documentation are presented in Attachment B.The net total nitrogen impact
from operation of the Celrobic®system is calculated to be 117 Ib/d total nitrogen.
To estimate non-Celrobic®effluent total nitrogen discharges,the 1992/1993 data was utilized.The
average and maximum effluent total nitrogen from the 1992/1993 data was calculated to be 3.3 mg/I and
4.7 mg/1,respectively.As the peaking factor of 1.4 is relatively low and 50%of the data is above the
average,we propose to use the maximum value of 4.7 mg/I as representative of historical total nitrogen
discharges prior to operation of the Celrobic®anaerobic system.A concentration of 4.7 mg/1 at the
permitted flow rate of 2.305 MGD is an equivalent mass discharge of 90.4 lb/d.
The sum of the 9o.4 lb/d of historical total nitrogen and the 117 lb/d total nitrogen contributed by the
Celrobic®system result in an estimated 2004 effluent total nitrogen load of 207.4 lb/d. Therefore,we
propose a numerical total nitrogen permit limit of 207.41b/d.We propose once weekly
monitoring with an annual average limit,which is consistent with your email on December 14,2018.The
proposed 207.4 lb/d total nitrogen limit for the Salisbury Facility is the equivalent of 10.7 mg/l total
nitrogen at the maximum permitted flow rate of 2.305 MGD.
Dewberry Page 2 of 3

To support this evaluation,Dewberry researched the effluent total nitrogen discharge from similar OCPSF
facilities in order to evaluate if the proposed limit of 207.4 lb/d is reasonable for discharges from a
polyester fiber manufacturer.Our search focused on polyester fiber manufacturers with current or
historical direct discharge permits.Table 1 below summarizes the data obtained for four manufacturers in
NC.Excerpts from the supporting documentation is provided in Attachment C.This information was
obtained from NC DEQ's Laserfiche Document Management System but full copies can be provided upon
request.
Table 1.Total Nitro:en Dischar:e Data from Other Pol ester Manufacturers
Facility Name NPDES Description Source Total Nitrogen Data
DuraFibers NC0001899 Manufacturer of polyester 2016 NPDES Permit >6.9 mg/I*
(Moncure,NC) resin and fibers Renewal Application (*only ammonia data
was available)
DAK Americas NC0003719 Manufacturer of polyester 2016 NPDES Permit 8.9—27.4 mg/I
(Fayetteville,NC) chip Renewal Application
Celanese NC0004952 Manufacturer of polyester 2018 NPDES Permit 0.62 mg/I
(Shelby,NC) resins Renewal Application
Invista NC0001112 Manufacturer of polyester 2014 NPDES Permit 39.5 mg/I
(Wilmington,NC) polyols Renewal Application
The effluent total nitrogen data from other polyester manufacturers ranges from o.62—39.5 mg/1.The
wide range is likely due to difference in production operations and/or wastewater treatment operations at
the facilities.For example,the finishing chemistries for polyester varies by manufacturer.Finish
• chemistries,including those used at the Salisbury Facility,use urea as a carrier during the finishing
process.The average effluent flow rate from September 1992-August 1993 at the Salisbury Facility was
1.029 MGD(Attachment A).At this flow rate,the 2o7.4 lb/d translates to 24.1 mg/L.This concentration is
within the range of effluent TN concentrations observed at similar OCPSF facilities.Flow data from 1992-
1993 is used for this comparison as this time period is the closest to 2004 for which data was obtained
from NCDEQ electronic and archived files and was during a period when the facility was operating at a
production capacity similar to 2004.Diane Rodman with Central Files indicated that some historical
discharge monitoring reports including records from 2004 have been destroyed.
We appreciate your consideration.Please feel free to contact me at 919-424-3764 with any questions
regarding this matter.
Sincerely,
(VJ Leigh-Ann Dudley,PE
Project Manager
Cc: Julie Grzyb,NC DEQ
MariJon Owens,Edge Water Treating
Greg Coleman,Edge Water Treating
Ryan Ford,PE,Edge Water Treating
Tom McKittrick,Edge Water Treating
Katie Jones,PE,Dewberry
Dewberry Page 3 of 3

AttachmentA 0 9/15/9 3
COMPLIANCE EVALUATION ANALYSIS REPORT PAGE 1
PERMIT--NC0004944 PIPE--001 REPORT PERIOD: 9208-9307 LOC---E
FACILITY--HOECHST CELANESE - SALISBURY DESIGN FLOW-- 1.2000 CLASS--4
LOCATION--SALISBURY REGION/COUNTY--03 ROWAN
50050 00310 00530 31616 00010 00400 00600 00665
MONTH Q/MGD BOD RES/TSS FEC COLI TEMP PH TOTAL N PHOS-TOT
LIMIT F 1.2000 F 323.0 F 1000.0 NOL 9.0 6.0 NOL NOL
92/08 1.0933 110.06 123.6 75.2 27.45 8.5-7.1 2.590 2.9000
92/09 1.0486 90.23 9.8.2 56.8 25.30 8.1-7.2 4.670 3.1000
92/10 1.0581 60.74 105.9 35.9 17.93 9.2-7.3F 3.890 2.4000
92/11 1.0617 64.33 87.9 45.2 13.75 9.0-7.3F 2.350 2.0000
92/12 .9740 91.80 38.2 32.8 8.16 7.7-6.9 3.530 1.9000
93/01 1.0632 189.90 159.1 44.5 8.48 7.8-7.1 3.130 2.3000
93/02 .9484 219.60 214.4 96.7 8.17 7.7-7.0 2.510 2.5000
93/03 1.0225 265.32 219.2 56.7 10.80 7.6-6.9 2.980 2.0000
93/04 1.1914 211.13 255.9 44.0 17.50 7.6-7.0 3.420 2.0000
93/05 .9205 117.48 160.1 44.9 24.25 8.2-7.0 1.430 .6600
93/06 .9334 104.03 123.1 34.0 28.03 8.9-7.4 4.570 3.7000
93/07 1.0337 89.96 167.1 76.3 30.41 8.4-7.4 4.700 3.0000
:j
AVERAGE 1.0290 134.54 146.0 53.5 18.35 3.314 2.3716._;
MAXIMUM 1.5680 505.00 447.0 232.0 32.00 9.200 4.700 37000 ,'
MINIMUM .3650 24.00 15.0 23.0 6.00 6.900 1.430 .6600
UNIT MGD LBS/DAY LBS/DIY #/100ML DEG.0 SU MG/L ':JIG/L.=
-1
0

Attachment A
l
EFFLUENT page 1 of 2
:MIT NO: NC0004944 DISCHARGE NO: 001 MONTH JANUARY YEAR 2009
ri.C1LITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I PERSONS COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to: �2 /
DIVISION OF WATER QUALITY X �N , vo - v2-. /U� "
ATTENTION: CENTRAL FILES ( NATURE OF ORC DATE
P.O.BOX 29535 BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
50050 00310 00040 00530 00610 31616 00300 1042 01045 01055
D Opr. Opr. Fecal D
A Arrive Time ORC Flow GODS T Coliform Dissolvd Total A
T Time on on (41 pH S AMMONIA Oxygen Copper Iron Manganese T
E 2400 Site Site [ ]Inf 20C S NITROGEN Geometric (DO) E
clock [X]Eff Mean
# HRS HRS YIN MGD LBS/D UNITS LBS/D LBS/D #/100m1 Mg/1 Mg/I Mg/I Mg/1 #
.7.
i`31i#iEi?'i^iii' ''=::i:i�i ::^'-l:: E`::: [ iiii i := lilil! i , `...
2 0700 24 B 0.303 7.2 12.0 2
i i �
i'i ..•..: ;_i4 �'
2 �i�f'i'� il i5�'ii��'�i5i 5i�i1:`ii:i i�iiiii T`i ii�ii�i i 5 E:� ::
.:„f : i ' ;i i:i:M'i'Si:Mifi`;Tf:`•,'lii iiiiii ii iiii` : i
;i :;::;>.; iii ::i:is:',
4 0700 24 B 0.301 18 88 4
&!: 7DD'. .2q.: . 4.i, i.0"#I"bi.. ?i..i. .i.ii.ii.ii: .j. ' ik . ' i: . :4•Z . ` .• .:
0700 24 0 477 28 131 <0 40 0.038 0.34 0.091
::07il0:'.: . 24;:: i€i 0653€`: [`€.°i :€;€�:4 :.. :.....: < ::::rAat .:. .:.::: . :: ..:
0700 24 0.671 34 157 MI
El:.0760 :.iq? !:: . i09
10 0700 24 B 0.492 --_-- 10
Q700:�: 0k19'::i`E:21'::i: i''
12 0700 24 Y 0.380 7.2 12 112 1 12
1
.''13 0700::1 24 . Y.".;:0.355 i '1'24 ' 13[
14 0700 24 Y 0.330 7.0 112 14
BE .0706s WNW: 0 714:€i Ei']:6"'.i` .p`ii6(ii:iiy ...,.i:OM ..
16 0700 24 © 0.306 7.8 _-- 10.7 -__- 16
�g� 0700 24 m 0.286 12 33 -_ 1 1 _
g700::: 24:.:: i:0:21:4:.:.'.:;:.::ipii 21. 10.2
20 0700 24 0.232 0.35 20
'27 E'r:Q9:00". is 24:.:: `'0`igi . ;ii i`i :q:`i;s . is
® 0700 24 © 0.160 5 16 -_- ®
MN 0700 24 . 0.223 __---_ i 24 j
i` °I070iiii:'.W.:p:E:.0:r: .°0 2 ii - z
26... .. 2.......$.....q.2fiS'`E :::E�9'.E � EcE aE:Ei'.E: EEcB$E'.`Eli E:E:Er.:�`E E::::::::i:::.i'.::E..: `:; ;'; ''. -�..
26 0700 24 Y 0.325 8.0 20 11.3 26
27.. ..:. •
...{130 24. T.. .,.0.377 ...16 `: 541''.:: E:.'r403)1:: li'i `i;si i`:E' ' '. 27?
28 0700 24 Y 0.402' 7.6 11.4 28
29 .0740 .i OX611 21 ": • 34' `• _ :2.9
30 0700 24 111/11 0.284 7.6 _-_ 11 2 30
AVERAGE 0.346 17 67 0.80 17 11.1 0.038 0.34 0.091 AVG
MAXIMUM P.:i ::q.67i: :.'::3k':i: . R:Ei'•: : :!#S`r....: .1>74 •s1 . 12-8 .:: 0038 0.54 ::0.091.'. MAST
MINIMUM 0.160 5 '.0 16 <0.31 12 9.5 0.038 0.34 0.091 i MIN
C6M2IGRAB:t: :Gt714T'::l : .COXE': r`:CO4-.i .'GRAB GRAB'.::: ::COMIPi COMP .:COMP. :. i'
DAILY LIMIT NA 518 6-9 1043 46.00 400 5.0 DY
1401 1)t(V..Ii4if . '::` ::7a0S :.:201 ., 3$0 i3 .:::ii:]20q - 5 0....;::. . .3i4f3
DEM Form MR-1(12/931

Attachment A
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH JANUARY YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) . DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I I PERSON COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
DIVISION OF WATER QUALITY X
G
Rai'+-✓L-i
ATTENTION: CENTRAL FILES IGNATURE OF ORC) DATE
P.O.BOX 29535 BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
00076 00630 00600 00625 00665 _
0062o D
a Turbidity Nitrate+ Total Total Total A
T Nitrite Organic Kjeldahl Phosphorus T
Nitrogen Nitrogen Nitrogen (as P) E
(as N) (as N) (as N)
# NI'U mg/1 mg/1 me `, mg/1 #
i.: — 2
••
4
•: 4
6 14.8 0.043 1.6 1.6 0.22 .... ..... ............. .. .......... ....... 6
t..-
8 8
i iIEIii
14 9.4 14
:1
18 18
•
20 20
22
22
24 2
4
26
:2•�i:'�'`'°i:::;SiEi yi :6 :'i i_i?`yEi_i;; ;.;.;:;.?5:` : .. 4:: •..." 26
28 8.3 28
30
........-... 30
AVG 9.8 0.043 1.6 1.6 0.22 AVG
MAX: ..14.$ ::;'-._::;::< :'::.•::::.,:
....!);OS3:'. � .::�.fs:;.;:•: •s:I.6-:...�..1).22.::.;.:-. .........:.;_p...:i:i:i.p:;::�::��::-�:�.: :::.. :. P1i3AXi
MIN 6.7 0.043 _ 1.6 1.6 0.22 MIN
DY NA NA NA NA NA DY
OEM Form MR-t(12/93)

Attachment A
EFFLUENT page 1 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH FEBRUARY YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED J I PERS.() OLLECTING SAMPLES WST TRT OPRS
• Mail ORIGINAL and ONE COPY to: C�
DIVISION OF WATER QUALITY "/7•- 0 /
ATTENTION: CENTRAL FILES • - (SIGNATURE OF ORC) DATE
P.O.BOX 29535 BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
50050 00310 00040 00530 00610 31616 00300 1042 01045 01055 TGP38
D Opr. Opr. Fecal D
A Arrive Time ORC Flow GODS T Coliform Dissolvd Total - A
T Time on on ® pH S AMMONIA Oxygen Copper Iron Manganese CHRONIC T
E 2400 Site Site [ )Inf 20C S NITROGEN Geometric (DO) TOXICITY E
clock [X)Eff Mean
1/ HRS HRS YIN MGD LBS/D UNITS LBS/D LBS,'D 4/100m1 Mg/1 Mg/1 Mg/1 Mg/1 PA'34% #
:...........,.,.E.....O.i.6S .:.:.Y1.•. ,...: .- .< ,2i:. ....:::;.;:•`•E.E:E::::::°�::'s°- :::: .�: ' rrr.::::::::::::::E::a?:
2 0700 24 Y 0.178 7.7 11 9.9 PASS 2
3:....... ,.24......`ty.......0.2113:::::::1'�:::::::::::: :::�:::�::26:::::::[::::a3D:::::::::::::�:�::: :::::::::::;:::;::;:::: : ' :�: �::_'�' ::�:::::: : :.:•::.::.:::::.:::::-:-:::.:..•. .•
4 0700 24 Y 0.281 16 7.7 11.4 4
6 0700 24 Y 0.312 7.6 11.2 6
.-...U7flD.....,24... ..13......0.32a.
8 0700 24 B 0.328 38 8
10 0700 24 Y 0.303 13 33 0.30 10
....., .bfibD. ..2&.. ..�".....D.3�..;.•.,I3..-.�.....7,:&.............:.:.:.:.:::.:.:.:.:.:.:.:.::.:.:.:.:.:.:.:.::.::.::[D.S:-:.:.::.:::.::::.:::::::::::::::.:::::::::::::::;:::::::::;:::::::::::::::: ::t::::::::::l:t:':
12 0700 24 Y 0.346 14 38 12
_ 14 0700 24 B 0.398
14
.... .....
16 0700 24 Y 0.445 7.7 23 9.9 16
..:2?F=:::;::;•Y:;::::;O:ddYr._s::::3a':g;;:;::;:::`:-E,">�p`:SCi::: Odd: `. ,.
18 0700 24 Y 0.534 27 7.7 10.3 18
3'9 E 3 p 0?.0....24.......X`.•...�.0.S6d_......38.............•.•.•:.�:.:•71.:..,.:.,.:.:.:.;.:.;.:..:.:::.:.::::::�:::-:::::.:: ::: ::::::::::::::::::::::::: ::::::::::::::::�::'.a:["s[::: :;:;:;:p:::;::E1�E
20 0700 24 Y 0.523 7.6 10.4 20
>�I i
22 0700 24 N 0.411 51
22
5i'�i: i!: i:ii�i;iiiii=Pi
....... ...>5.:..,, .:...,..... .......• .;:22;:::::.�::::.70�7::..:..:::::-::::- ::•. .,.:: <: :: :33::
24 0700 24 B 0.361 24 42 0.39
24
26 0700 24 B 0.398 23 43 26
:......
28 0700 24 B 0.509 28
AVERAGE 03'3 21 41 0.37 18 10.4 0.025 022 0.061 PASS AVG
�` . ,..;.,,. .ft,566: 3R. 7� :�:?.�:�:�1:`:: :•`:'tt.48 .•2�:::;:: .;::r:ll4 '.�:AQ35., 02Z :: Oi163111 ,..P.ASS .. ..:-':`::NI��
MINIMUM 0.165 11 7.5 21 0.30 11 9.4 0.025 0.22 0.061 PASS MPV
COMP .:GR :iO W :•Gf3hlfi i :::: R: B .-:GR4B:- .'COMP.:` cl MP: (OMI>:. .::.
DAILY LIMIT NA 518 6-9 1043 46.00 400 5.0 DY
_......Iv10
DEM Form MR-I(12/93)

' 9 Attachment A
f- L�
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH FEBRUARY YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I I PERSON CTING SAMPLE WST TRT OPRS
Mail ORIGINAL and ONE COPY to: p�
ATTN:CENTRAL FILES �� , — / D 9
DIV.OF ENVIRONMENTAL MANAGEME'T (SIGNATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 I 00600 00625 00665
D 00620
A Turbidity Nitrate+ Total Total Total A
T Nitrite Organic Iijeldahl Phosphorus 7'
Nitrogen Nitrogen Nitrogen (as P) E
_ (as N) (as N) (as N)
# NTU mgA mg,/1 mgA mg/1
2 2
4 ' 8.5
4
6
8 •
10 10
`I E
12 12
14 - .. 14
16 16
18 8.7 18
20 20
22 22
24 24
26
26
28 28
AVG 8.7 <0.020 0.76 0.91 0.19 AVG
MIN 8.2 <0.020 0.76 0.91 0.19 MIN
CIQi :`�iR..... .•:£(�2+4PE E: :: k UfNPE ,'`tCDtdiP: :'COMP .: E .t .... '. £'CrE.
DY NA NA NA• NA NA DY
:-:
DEM Fenn MR-I(12/93)

Attachment A
EFFLUENT
PDES PERMIT NO: NC0004944 page 1 o1
FACILITY E PERFORMAN�R DISCH.-ARGE GE ORY
001 MONTH MARCH
OPERATOR Iti RESPONSIBLE CHARGE ORC CLASS IIi , YEAR 2009
OPERATOR
LABORATORIES ( DAVID L.CASNER PHONE
( R--
PERFORMANCE FIBERS,INC.-SALISBURY GRADE IV PHONE(70 -6000
CHECK BOX IF ORC HAS CHANCED
PERSONS COLLECTING SAMPLESAVIS&FLOYD, INC..
Mail ORIGINAL and ONE COPY to: WST TRT OPTS
DIVISION OF WATER QUALITY ? 2
Al I ENTION: CENTRAL FILES /� y
P.O.BOX 29535 (SIGNATURE OF OR "/••U J
RALEIGH,NC 27626-0535 BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS DATE
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
-_�— 50050 00310 00040 00530 00610 31616 00300
. Opr. Opr.
III
1042 0104) 01055 —�
Arrive Time ORC Flow SODS Fecal
Time on on @ AMMONIA Coliform Dissolvd
2400 Site pH Tom!
clock Site [ ]In 20C NITROGEN Geometric Oxygen Copper Iron Manganese
© HRS (X)Eff (DO)
HRS ® MGD LBS/D Mean
LBS/D
:E:�'7AOt: .: ® LBS/D #/looml � ®®07E
24 � 1.048 �-�0 a 07 �� 0.:6i iiEi6E3 i:E1:;: iRiD` ' :f i0:'g`/:.-.:i a:14.:
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69
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* © 0.586 •
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0.418 IIII 0700 ..0. .. __-_�
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:07Oti . ___-___
.0700: ;:El 0700 MOM iE t(1 !AVERAGE .00575 _ ¢3 k. �___—_®
ltAVERAGE 94 ® r G
1.048 ' �� 0.020 0.27 4 ]
_ 0.349 _� ,1 32 :< _Atjv
COMI'/GR :: <0 58 ® 0114
co P 0.020 0.27 0.14 _a
DAILY LIMITVIIIMMINIMIME 104 COMP
f.? DAILY
Y`L[�I1 1043 46.00 400' CO11111 GOMP .:C
0�:..: :20).. s o
El"d
DEM Form MR-1(12/93)

Attachment A
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH MARCH YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS.INC.-SALISBURY CLASS III COUNTY ROWAN
OPER:4TOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE 1V PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I PERSONS_ OLLECTING SA P S WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES X ! Z_ ,/ )f- �C �n _ - /7- - 7
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF ORC) BATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665
D 00620 D
n Turbidity Nitrate+ Total Total Total A
r Nitrite Organic Kjeldahl Phosphorus T
E Nitrogen Nitrogen Nitrogen (as P) E
(as N) (as N) (as N)
# NTU mg/1 mg/I mg/I m #
2 2
4 12.5
8 8
10 10
12
12
14 14
16 16
18 11.7
18
20 20
22 22
�: 3i?'i:;�i::;:`;`.:;:':';�:�`>::::,p:?:_•::;:;:;:;:!:i:;:i.;...;!;.;.i.i.i:......_...,i::;:?::::::::>6:;:.:;:;:::`":'::`ia:i:iEE[i.;i.i.;:;;.l;s=.i[;.;:;p;:;:i�;::i::;>.:53;:;�5:�:f;`;:::;;i;SE:�:i;i:::::::.:.:::.::.:::::.:::.::i:::[.'..:_.
24 24
26 _ 26
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28 28:.
AVG 123 0085 13 1.7 0.26
AVG
'MAX`
MIN 11-:, 0.085 1.3 1.7 0.26 MIN
CIG' GRA3?:_ COMP :;:;:COMP;:;;;::;CJMF COMP • CI0.1
DY NA NA NA I NA II N4 DY
OEM Form MR-1 I12193)

Attachment A
t
j EFFLUENT
page 1 of l
PERMIT NO: NC0004944 DISCHARGE NO:
001 ITY NAME: PERFORMANCE FIBERS OPERATIONS INC.-SALISBURY CL ASSH II APRIL COUNTYYEAR 2009
Ur.,-ATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER ROWAN
CERTIFIED LABORATORIES GRADE I PHONE(704�36-6000
(1)PERFORMANCE FIBERS OPERATIONS INC (2)DAVIS& OLF YD, INC.
CHECK BOX IF ORC HAS CHANGED
PERSON ELECTING SAM
WST TRT OPRS
Mail ORIGINAL and ONE COPY to: /
DIVISION OF WATER QUALITY ( ! 1 n G �_�/C-
ATTENTION: CENTRAL FILES U C�
P.O.BOX 29535 (SIGNATURE OF ORC) DATE
BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27626-0535
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
-_10111— 50050 00310 00040 00530 00610 31616 00300 Opr. Opr. 1042 01045 01055 __ 1
Arrive Time ORC Flow Fecal
HODS Colifonn Dissolvd D
Time on on Total
AMMONIAA
2400 Site Site [ ]Inf 20C Oxygen Copper Iron Manganese
IIIIclock [Xj EffNITR�' Geometric (DO) T
Mean
in HRS HRS ® MOD LBS/D UNITS LBS/D LBS/D q/10D� Mg/1 E
6.4 .:i ` 0,50Mill Me MgQ __0
© 0700 m© 0.518 9 -
35
III
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II
112 __
0700 24 © 0.407 7.7 23 -_-
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MIN uOU'STEM Efvy3 ° 92 --_ __
In 0700 24 NM 400 37 v ti , 26
.:0i .:R,383E' 7 7 67 0 67 _ m El 0700 24 El0 368 25 61 yam°
AVERAGE _IMMI 0.41 N. 20 _-_111111E___ 30
IMY11Irtf =';= A 56a . 143 8 <0 0.10 n zp 0.12 ®MINIMUM 0.298 • 6.8 '3 0 96 22 7.6 <0 R10.i; 0 3e;.: 0 12`f;:: „'?:
,6i0:!GB i : 1.6 <0 010 0.30 0 12 -_®
— COh'j'� �1[r{}I4 ,:;;ass :COME CAMP;.`:.: :(') ..
DAILY LIMIT -® $ GRAB :lY(3rp C =
300 6-9 1043 46.00 400 ;0
(Q FI3[?lLtM17 _::2:30 :::E �fJ:. 20D v -_ DY
33Q .` a ilb.
DEM Form MR-I(12/93) �'iop

Attachment A
•
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH APRIL YEAR 2009
FACILITY NAME: - PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I I PERSONS COLLECTING SAM ES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
DIV.OF ENVIRONMENTAL MANAGEMENT G�
DEHNR (SIGNATURE OF ORC) DATE
P.O.BOX 29535 BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE,
00076 00630 00600 00625 00665
D 00620
A Turbidity Nitrate+ Total Total Total A
T Nitrite Organic Kjeldahl Phosphorus A
E Nitrogen Nitrogen Nitrogen (as P) T
(as N) (as N) (as N)
6 NTU tokil m
.. .. 8^ mg/1 mgQ
3 '
4 ....,. 3E:
6
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10
12
12
14
14
15
16
16
18
IS
20
• 19:;'
20
22 6.8
22
24
24
26
6
28
28
30
AVG 7.8 0.53 1.3 23 0.39 ,,..:
:kl LJF: 16 J !Eb;S i:[e: .;.;....5 .;.....::i'`•�3 0,39 AVG
MIN 4.4 0.53 1.3 2.3 0.39 3MN
CMP'E `POMP::
MIN
DY NA 1A NA NA NA • `C1Cs
+. DY
DEM Form MR-1(12/931

Attachment A EFFLUENT page 1 of 6 •e� 001 MONTH MAY YEAR 2009
NC0004944 DISCHARGE NO: CLASS III COUNTY ROWAN
NPDES PERMIT NO: N'-"�FI RS,INC -SALI D L.C GRADE IV PHONE[phone]
i FACILITY NAME: PERFORMA DAVID L.CASNER
i OPERATOR IN RESPONSIBLE CHARGE(ORC) WST TRT OPRS
LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD,
{ INC.CHECKIED LA PERSONS COLLECTING SAMPLES
•
CHECK BOX IF ORC HAS CHANGED �7 7-C,
Mail ORIGINAL and ONE COPY to: X i �' DATE
ATTN:CENTRAL FILES {SIGNATURE OF ORC)
DIV.OF ENVIRONMENTAL MANAGEMENT BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
DEHNR ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
P.O.BOX 29535
RALEIGH,NC 27626 0535
50050 00310 00040 00530 00610 31616 00300 01042 01045 01055 TGP38
D
A Arrive Time Fecal A
D Opr. Time ORC Flow BO• T Colitorm Dissolvd Total A
AMMONIA Oxygen Copper Iron Manganese CHRONIC
Time O° on ��DS pH S 20C S NITROGEN Geometric (DO) TOXICITY E
clockT
Site Site [ J In[XI Elf f
Mean Mel q
# HRS HRS YIN MGD LBS/D UNITS LBO) LBS/D #/100ml Mg/1 MO
0700 24 .:: ,Y :D 3S9 .
2 0700 24.. . B.,. •,0.343 •
....:.: :.:....,.;..•..,....•'$tEEi ESOE3iT2:.di ifi` i .iE.... ..
64 - , 4
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i:'.: 22 7.4 PASS
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14 0700 24 B 0.386 13
INTEINIIII 16
4 ' 704i:'ss24`.i::::::B:p: 6:.0 500 .
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16 0700 24 B 0.500 ¢8 : i1: = 18
17 :$7C)t1`. Ei24Eiii i'iE$ :ii 0,509.: 116 8.6 .--
18 0700 24 Y 0.466 7.4
`20.'€0700 4 I.Y:.; : 0.381.:::; 1a:::: -_ 8.5 � ...,..•.•.• .
20 0700 ..24....�Y., 0.388• 13 7.5
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7.1
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II
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24 0700 24 B 0.379 - 1:4:: 26
26:.;:8704':<•a:24E t::[ Y .. . a&gig 47 1.09 --...... ......:.:.:..:.:.:.:.:.:.:.:.:.
26 0700 24 Y . •0.437 1 i
�i E:i:i7` i:ii:'. iiiliE;ii i;i ii iii��ii"ii%
MIN
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28 0700 24 Y 0.574 .. 10 . ® :::i:ifD
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30 0700 24 N 0.549
30
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iiiMffn
i l.i Ei}YI!V1 ::'�4pi;i ;:9N;:i i:Q41 air 54 0.50 74 7.6 ;i AVG
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............. II.f�O ii:�i:e`.;`�i,�i:i `i:i:668 E:iE:;1:99E: :� MIN
M NIMUMi:i: 22 <0.010 0.044 0.092 PASS
MINIMUM10 i'' tkiP .i:: COMP G • -
isCi1P/�:: 'C>71?i: CtSt�Pi: QfPc$ i.CDxEP.- ' ' 400 SA �Y
46 0D
NA 300 6-9 1043 ... .. .. ...T�fO:
DAILY LIMIT •'
•
i 334.., 2a4E?::::::aa DD:: 5>D . '2
i:i cfvtL11i7}iL,YlI)v11T `�305:'i• ;� `.` S-4 i
DEM Form MR-I(12/93)

Attachment A
EFFLUENT Ma. ..--- page 6 of 6
/DES PERMIT NO:
NC0004944 DISCHARGE NO: 001 MONTH APRIi YEAR 2009
/AGILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS
L.CASNER C GRADE IV PHONE[phone] ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC)
CERTIFIED LABORATORIES PERFORMANCE FIBERS,INC.-SALISBURY (2)DAVIS&FLOYD, INC.
CHECK BOX IF ORC HAS CHANGED I I PERSONS nr r cCTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to: X �4-2 � / Q2
D :CENTRAL FILES SIGNATURE OF ORC) DATE
DIV.V.OF ENVIRONMENTAL MANAGEMENT BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.OO..DEHNR BOX 29535
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665 D
D 00620
A
A Turbidity Nitrate+• Total Total Total T
T Nitrite Organic Kjeldahl Phosphorus E
I o Nitrogen Nitrogen Nitrogen (as P)
(aa N) (u N) (as N) r!
hiNTU mgA mg/1 mg/1 mg/1 ::::i :.: iiii
':
m
2
2 :2;i:i
4 4
4 iii:iSii
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DCM Fnrm MF-1 n--')

Attachment A
EFFLUENT page l of 2
4PDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH JUNE YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS HI COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I I PERSON OLLECTING SAMPLES WST TRT OPRS
/7 /77( 7
lY��r_,�— �f e'2 ..
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
50050 00310 00040 00530 00610 31616 00300 01042 01045 01055
D Opr. Opr. Fecal D
A Arrive Time ORC Flow BOOS T Coliform Dissolvd Total A
T Time on on @ pH S AMMONIA Oxygen Copper Iron Manganese T
E 2400 Site Site j j Inf 20C S NITROGEN Geometric (DO) E
clock IX]Eff Mean
# HRS HRS Y/N MGD LBS/D UNITS LBS/D LBS/D #/100m1 Mg/I Mg/1 MO Mg/1
`:?•!i i�i''i is :: :'_ `:i'ii[iii siiiii iiii`i ii'i"r E[`i'`i ..
2 0700 24 _ Y 0.351 15 35 1.79 _ <0.010 0.64 0.11 2
4 0700 24 Y 0.276 12 39 4
:ES A700: 24..E::Y.. .:p:837, '7;2: .,,.,i'i.::�;-;•E.. ;I :;'p:,6 �. •.• :�.. .............. ..... ... ... ....... ..
6 0700 24 B 0.955 6
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8 0700 24 Y 0.857 7.8 32 7.2 8
10 0700 24 Y 0.581 24 7.6 6.7 10
12 0700 24 Y 0.850 8.5 5.8 12
'13 4700', .,29. .[N D:843' ';� t ? •, ..::..::.::::a:p:;:::'E E:::;:: .. ,
13'
14 0700 24 N 0.679 198 -
14
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16 0700 24 Y 0.738 37 197 2.28 16
18 0700 24 Y 0.798 47 246
18
79:
20 0700 24 N 0.622
20
2:1: ::A70U:E:;:24:;:;.:;i;8::;:::,:O:SQ7.;...::;:- ;:: ..:92..:.:..::.........:.:. .,.. _.... ,.
22 0700 24 Y 0.454 7.2 34 6.5 22
:i�:a'::iiiiii E[E:i;::i;is•:: `i`i i i i i?:i:E;fiiiE:i;iii. ;i:i;i;i;i'i;i:i`i i`i i.;`i ;iiii,t::[;[i.:::i.: . 5
::24 :f3704E o E E24's iYEEE�Eii0;399iE iiPSD:Eii.,.,...0.�3.............. ... ..... ........ ......... ......... ..... ...........
24 0700 24 Y 0.341 14 7.0 6.7 24
.::;•::;:;
26 0700 24 Y 0.298 6.9 6.3 26
':'-'1: 9700:; .... .... - ..... .. :a7�:
28 0700 24 N 0.370 46
28
29 ;Q70D' ;:40 . `; 61
30 0700 24 Y 0.326 14 65 0.76
AVERAGE 1 0.522 24 108 1.16 40 6.6 0.000 0.64 0.11 AVG
Y,AXI3�2t M •. G.953 A7 8.5. 24d 228 61 .. .; 72 .. 4010 ;;;,.().4;;;;;L .,02f 14Ak
MINIMUM 0.000 12 6.9 35 <0. 3 32 5 8 0 010 0 64 0 I 1 MN
c.OMPl ::: CG?�T :Cf3MP lt?B COa11P QMP GRA$ GILSB`: c 00IP. COMP ... _:COMP C G:
DAILY LIMIT NA 300 6-9 1043 46.00 400 5.0 I DY
:``'.h4f5N:2iL3f#1MIT: 2.3a5 154 6;9__ ...330, 25;00 206 SQ ... .i MO[
DEM Form MR-I(12/93)

Attachment A
EFFLUENT page 2 of 2
. PDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH JUNE YEAR 2008
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I PERS . ELECTING S.A ES WST TRT OPRS
Mail ORIGINAL and ONE COPY to: d/J
ATTN:CENTRAL FILES .�� j/�j} -
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNA RE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665
D - 00620 D
A Turbidity Nitrate+ Total Total Total A
T Nitrite Organic Kjeldahl Phosphorus T
E Nitrogen Nitrogen Nitrogen (as P) g
(as N) (as N) (as NJ
8 NTU mg/1 mg/I mg41 mg/I q
1 +1'Eii E::: .•9?E i�ii:..: :i3 i.::i:.!: :`:pi:::i+i:i:"E'`';:i:':i ii:ii:i;i:i:.::�i i:i i:i:•: .:..: :: !i.i:i:i.i i.!i.i:i:i;H i.i:.•::•............::.:`;i,;:p i;i;i;:i;i;i;::�;i:i5:. i;i;iii;ij-: iS;:':;i;
2•....
4 4
:i:SS's:iii:::iii: ?[;��l:i[P:: i�i�3 i' 55ii'S;i55ii::i;i:iE` i:i`iiii'`:i;i:ii::i i::::i:(iy:i[ci Eii:iE`iiE:i;i i;ipi;i;ipi!i`;??:i:;[i(ii ii:i':::::!i•i::; i;;;i;::;i.::!,:;:;i;i i;iE[iii:i;i!;.E;:;i;i;i�i;i;i;i i`:.:::.:::.::.`:.`:.
...., ...
10 14.2 • 10
12 12
14 14 .
16 16
IB 18
20 20
22 22
24 11.7 T.T ,
24..
26
26
27i
28
28
30
30
AVG 13.6 0.097 1.3 2.0 0.90 T., AVG
M.A3 14,9. 0!09? 1�a 20: 0 90 MAX
MIN 11.7 0.097 1.3 T 2.0 0.90 MIN
COMP .::COMP `.;664 _::_ ..
DY NA NA t NA NA NA DY
OEM Form MR-](121931

•
Attachment A
EFFLUENT page 1 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH JULY YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED ( I PERSON COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES Q / -Z)
DIV.OF ENVIRONMENTAL MANAGEMENT CA
IGNATURE OP ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
50050 00310 00040 00530 00610 31616 00300 01042 01045 01055
D Opr. Opr. Fecal
A Arrive Time ORC Flow GODS A
T Coliform Dissolvd Total A
T Time on on @ pH S AMMONIA Oxygen Copper Iron Manganese T
E 2400 Site Site ( J Inf 20C S NITROGEN Geometric (DO)
clock I XI Eff Mean
# HRS HRS Y/N MGD LBS/D UNITS LBS/D LBS/D #/100m1 Mg/1 Mg/1 Mg/1 Mg/1 #
.. :`:� ;::�:`i;:Q3:;:�'::;Y•;:p:::.::'s!s..:,..E.::::::,:::'::-:�:;`'�:'''i`i':p``i�'�i :E: E:::`j��
2 0700 24 Y 0.304 13 35
. 3 ;;8700 .s[2IiE ' > ; ;;ii; :s:;7i ;;i;; `:.:.:..:.:.:.:.. 2
63 .... .................:.::.:.:.:.:.:....:::: :: :; ;:4
4 0700 24 B 0.278 '
4
6 0700 24 Y 0 7.7
- 248 23 6.6
:::?;E:'- 70Z1�`'s:[2 ::;a:E;i,'..:..O`�3�:':;;;;:8;;;;.:i;i::%i:i:i:: :i;. .i,::: ::: isi'i "[ ::.:.::: .:':.:.:.-. 6
Y . 9;;;;; .....: ,.,.2b ..:::::.6 62 ;;;:41010. : .B. .64
p U;14.: : 8'8 0700 24 Y 0.266 11 7.9
67
8
10 0700 24 Y 0:328 7.9 6.8 E,4'.,
- .I:Y::t1706 24::: _:EG 3bG. l0
12 0700 24 B 0.388
;;:13:E ii0704 :;::'24i:s.::t:Y:;;;;, ... ;;;:;;;:;;;:;E;i.H;[; 1.: ; ;i:i 12
74
14 0700 24 Y 0.501 25 142 <0.42
14
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16 0700 24 Y 0.419 21
105 16
IT .;n'lAD.` � .Y ,�''0385':.'.:?: :`?.2`:-' . :•: ,
18 0700 24 B 0.330 ?:17
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20 0700 24 B 0.287 7.5 .30
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22 0700 24 B 0.293 12 7.2 �'' .,.:: ........ ...:.:........:: .. ...
6.5
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24 0700 24 B 0.336 7.3 - ..-: ...- :.:.24
6.3
........
26 0700 24 N 0.303 61
27 07DOi:;'.t2{:`E 'f¢EY::E '4:�02:: :: 1:E 26
28 0700 24 Y 0.318 8
; 45 0.66
29 a74Q': 24 r.. Y .
0:338 i:& 7:2 ;
z
8
30 0700 24 Y 0.337 8 51
9
31 &T40` 2# " $ O'S25 T.I i 30
£l '
AVERAGE 0331 13 1111111 E2 0.52 32 6.4 0000 0.69 014
f ' MAJCi>fE1M fr501 i 8:3 42 (1.81.... 10. 6$ .:. I .<O
AVG
:0 1D 0:69 414 MAX'MINIMUM 0.239 6 7.0 26 <0.42 22 5.9 <0.010 0.69 0.14
CO'vip..1GR B:: CQN1' CG!tE GRAB. ':: Dh#': MIN
.�C3ti4p ,.:. GR,aB GRtiB..= Colv(p �
DAILY LIMIT NA 300 6-9 1043 46.00 400 5 0 COA F P
DY
)`: -MONTFILY E:1MIT 730fi: i50 6:9 3a0 23;00 �A0 .:: SA
I'1
DENT Form MR-1(12/53)

Attachment A
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH JULY YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I PERSONS COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
DIV.OF ENVIRONMENTAL MANAGEMENT ( NA RE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535 r
00076 00630 00600 00625 00665
00620 D
A Turbidity Nitrate+ Total Total Total A
Nitrite Organic Kjeldahl Phosphorus T
E Nitrogen Nitrogen Nitrogen (as P) E
(as N) (as N) (as N)
# NTU m .. m R mgfl m fl
2
4 4.
6;[5`.: "i i'-�i`ii'i'i'ii;iiii`iiiEiE?iiii.i�ii[`i.'.i ii i i 5t'Si.55f i:.:::..:.::......::::.::::::......::::::....:.[?::.:!:.:.:.:;:.:.:.;5 is�:i:i i'S5i 5i'.:.:a:!::: ?: ::::::P •;:;:;:.,.:.::.;.;.;.;.
6
6
8 8.3 0.12 1.7 2.0 0.81 8
"i`5�
10 10
12 12
3.
14
... ' ..... 14..
16
c •.. 16
7•^
20
20
22 14.0 22
24
26
26
28 28
30 2q.
30
.AVG. 107 0.12 17 1 20 081
AVG
•MrlX' •i• • .:ice 12 7?::;•'' ::'::•• •S- ;.
MIN 8.3 0.12 1.7 2.0 0.81
CMG;; :GFA18' C(3 .... COMP .... Cf1lvA. C(TMp
MIN
DY NA NA NA NA NA ` DY
.M0 i N•A, ... ..NA,;: :.1~i4- .�.,:,.:AtA. ;..:.:i NA..... ....: ...-.I ii I I t ,JI
DEM Form MR-)(12/03)

Attachment A
EFFLUENT page 1 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH AUGUST YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I I P LLECTING SAMP S WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES X
DIV.OF ENVIRONMENTAL MANAGEMENT • (SIGNATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
50050 00310 00040 00530 00610 l 31616 00300 01042 01045 01055 TGP3B
D Opr. Opr. Fecal D
A Arrive Time ORC Flow GODS T Coliform Dissolvd Total A
T Time on on ® pH S AMMONIA Oxygen Copper Iron Manganese CHRONIC T
E 2400 Site Site [ 1 Inf 20C S NITROGEN Geometric (DO) TOXICITY E
clock [XI Eff Mean
# HRS HRS Y/N MGD LBS/D UNITS LBS/D LBS/D #/100m1 Mg/1 Me Mg/I Mg/I P/F34% #
.:.:;E3:::''�306- �;:?E;i::i::i:: �:::::i s '::EE;::::;i;:;:;ibi;'•;:;i6E E�i;:;:EE:iEEi:iiii;�::::::::::: ::::i:::'•::i::::::;:•::;::::::�::::2:i:i:i::;�::;::::;:;::i;:;:;i:;i';:;
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2 0700 24 B 0.336 50 2
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4 0700 24 Y 0.314 10 81 <0.26 <0.010 0.53 0.13 4
6 0700 24 Y 0.334 14 92 6
8 0700 24 N 0.278 8
giAria : s;
0 0700 24 Y 0.259 7.1 28 6.4 10
12 0700 24 Y 0.297 10 7.1 6.0 12
::98::::�7DD.::...24:•:•::.:..Y:.;..:.:D.31�a......:::5.... ............:.:a7..........:.:........ ....:::::::::::::�:�::::::;:::::'::::::;::;:::::::::::s:::::::::::::::;......,.,.•...:...... ..:..:. ....... 13:
14 0700 24 Y 0.342 7.1 6.4 14
16 0700 24 B 0.419 • 77 16
.:::::.::::.:.:..:::::::;:::::.:::._.::........:......:.........;...17:;
18 0700 24 Y 0.337 11 70 <0.28 18
....................................... ...... .T..
20 0700 24 Y 0.354 15 62 20
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22 0700 24 N 0.405 22
:W ;
24 0700 I 24 Y 0.608 7.3 116 6.4 24
• i
.87 :::�:�• :::�::::�:�:• :0:412::::::::?6:::: ::::::::::::::::::::::t28:::::::::::�0;37::::: ;:;:;:;:;:;:;:;:;:;::;:;:;:;:;:;:;:;:;:;;:::;:;:;:;:;:;:::;::;:;:;:;:;:;:;:;:;::;:;:;:;:;:;:;:::;:::�:�:::�:�::::::::::�:�::::33::
26 0700 24 Y 4 0.574 24 7.4 6.6 26
28 0700 24 B 0.448 7.1 6.5 28
39E�:f{700�E:::2A::S i::�$E'+`:0:385 S;t E;2;S;EEE:E; ::EE:pi�Es:E E�i E;f;E;E;i;i::�s:�:;::E�2E6,i;ip:;::::.:�.,�_.�...._.....�....... .......:.:............:.............................•...,.;�.......•.24. I
30 0700 24 B 0.364 49 30
`31:;::b7D4;:E 24 E B Q;SQ'?•r.:r•:rrr':�:7:2:::<.::�:�:�:�:�:�::�:::�:::�• :. 5� b6 '>' E?:�:
AVERAGE 0.377 14 JIM 73 0.00 41 6.4 6.000 0.53 ( 0.13 FAIL AVG
MAX
MINIMUM 0.243 5 7.1 45 <0.22 22 6.0 <0.010 0.53 0.13 FAIL MIN
P.:::::;.•.... ::.:GEL
E:::€:•COIgiP1.h3�.f,8': �a�lstl: `•COh3P. � �1t�'s>i.s::£t�t+I ...>wc�(I'::;:::4RSa8�� 13... . �iP<....�Q.�: .CY?h�tE-' :.:.: ::.:::...emu
DAILY LIMIT NA 300 6-9 1043 46.00 400 5.0 DY
i `,;.1
`•<`htY7!iTHLY�;1toIIT �:�2305':':::LSYi:. 5-9'a::':`330.. ;23:03'i�Ei?�i:_.3 0.... :....4.,...., � ....... ..............�., ... ,.,:...: ..:::: 1�.
DEM Form MR-I(12/93)

Attachment A
EFFLUEN
T page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH AUGUST YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED 1 PERS LLLEE)CLING SAMP VVST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
X
DIV.OF ENVIRONMENTAL MANAGEMENT (SI ATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665
D 00620 D
A Turbidity Nitrate+ Total Total Total A
7 Nitrite Organic Kjeldahl Phosphorus T
E Nitrogen Nitrogen Nitrogen (as 1') E
(as N) (as N) (as N) _
# NTU m ll mg/I me. m6/1
2
2
4
4
::��...........:....::::.:.:.:.......!i�i`i'•i�i�i�"•i�';`;i;��i�i�ii��0`i�5i;i5itii7Q:ii?i:i:i:[�i�i ',iiii[i;iii i`i`Jtti'i�i iii i?i=i"iSii:i iiiE:i�::.:i::;�ii;;?ii�> i�i�[�i[t�3 i��.�:;i;ii�i:i�"':.
6
6
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8
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12 12.8 12
14
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23
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AVG 13.8 • 0079 2.0 2.0 070 AVG
:MAX:
MIN 12 0.079 2.0 2.0 0.70 MIN
c�G• "GRAi•2:' :i.E.CC3h4P :: •: . ::CaG'�
DY NA NA NA NA NA I DY
:140 A. bq N-4 N.A :: � ? fy[p:i
DEM Form MR-1(12M3)
1

M���... FIBERS,li•.. ViD L CA�,� • � w a`�
PERFOR ANCE DA INC. SpI i
eE�11T`Q4 GE(OR� FIBERS, lNG SAMPLES
LITY vAp1EESPONSIBLE CHAR (t)FERFORh1ANCE PERSONS COLLECT .-A U
ERATOR IN BORATORIES CHANGED r DATE ,
FIEp La C HAS CHA :.
ERTt FOR �' H1S REPORT iS ,LEDGE•
t Ow
HECK IGI d ONE COPY to: l►GNA URE OF ORE,I CERTIFY THAT
OF MY KN
Mal ORIGINALF1LEg G1 MENT gY THIS TESIG ND COMPLETE TO TH _-
ATTN:CENTRA wIMENTAL MpNA ACCURATE A moss DIV.OFRA EI ENVIRO 01042
Ot045
00300
DEHNR 35 oobt0 CHRONIC
P.O.BOX 2NC 21626 0535 00040 00530 Fall Total Manganese p;30lvd ToxlctTY
RpLE 01111110, . 50050 0o3t0 Colitorm Copper -©
Oxl gen �OW
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0n 1 1 lnf LBSlD #Il00ml -v
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DAILY LIMIT � TSB`'
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DEM Form MR-t(12193)

Attachment A ggpTEMBEK an^"
001 MONTH ROWAN
DISCHARGE NO: —CLASS III COUNTY
LANCE FIBERS,44 SALISBURY GRADE IV PHONE[phone]
SIT NO: DAYID I CASNER
/OPERA PER: PERFORMANCE INC. •
OPERAT'Y NAME: WST TRT OPRS
CEERATOR L BORATO IES CHAR I)PERFORMANCER PERSONS COLLECTING SAMPLES
(I) FIBERS,INC.-SAI,ISBUR
�� CERTIFIED LABORATORIES � 0/
CHECK BOX IF ORC HAS CHANGED
, J� DATE
f Mail ORIGINAL and ONE COPY to: (SIGNA CRE OF ORC)
DEDIVAN CENTRAL FILES BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O BOFX
ENVIRONMENTAL MANAGEMENT ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DEHNR �illi II _-
P.O.EOX ,2 NC ______
RMI , 27626 30 _
00600 00625 00665
_ 00016 00630 c0620
Turbidity Nitrate+ Total Total Total
Nitrite Organic Kjeldabl $•hosphorus
Nitrogen Nitrogen (as P) __
Nitrogen _ __- :...,:::.
as N (e�� m -_ ___©
worniumwommumumimmumummousomm
MI_ 0.15 _________11111111111111111111111111
SYM _
In :. _______
® 111
WiE , MA' " Wil
__ 14
�� _____11111111111111111111111111111111101
MIN
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lrIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIInl
1111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111
IIIIIIIIIIIIIIIIINIIIIIIIIIIIIIIIIIIIIIIIIIINIIIIIIIIINIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIHIIIIIIIEDI
IISIIIIIIIIIIIIIIIIIIIIIINIIIIIIIIIIIIIIIIIINIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIEII
,11111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111113
SOIM �_�"""'r�°1
E 10.3 0.15 .... OSIMMEN O60 : _______ GLG-
W�5 �;':�:Q:1 :::: : IIIIIIIIIIIIIIIIIIIIIIIMISS
IIY
EMMIMMIMMENNSMy
�ies°..Bi
DEM Form MR-1(12A3)

Attachment A
EFFLUENT page 1 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH OCTOBER YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I I PERSONS COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES 7 �� ��� /7 d
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNA RE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH.NC 27626-0535
50050 00310 00040 00530 00610 31616 00300 01042 01045 01055 TIIP3B
D Opr. Opr. Fecal D
A Arrive Time ORC Flow BODS T Coliform Dissolvd Total A
T Time on on (a) pH S AMMONIA Oxygen Copper Iron Manganese CHRONIC T
E 2400 Site Site I I Inf 20C S NITROGEN Geometric (DO) TOXJCITY E
clock I XI Eff Mean
N FIRS HRS V/N MGD LBS/D UNITS LBS/D LBS/D N/100mI Mg/I Mg/I Mg/I Mg/I CI)Value% N
I 01(0 .:..:.1#.. .:.Y. : 0.36S: . :: ....:i: 5 .:
2 0700 24 Y 0.330 7.3
87
2
3:::� U?OD :: 24 •...N ..:0 320 .;: : :.
- 4 0700 24 B 0.327 55 4
c
6 0700 24 1 0.373 6 47:.. 1.75 <0.010 6
0 U 03G9 0.0775
7aa ,O70E).: 29 -:: .':Y U:;}$7 a 8 .74.<: ., .:.,:.i i
8 0700 24 Y 0.334 6 42
:> i179 24 ;Y
10 0700 24 B 0.307
10
":I:I :;049Fk'.:;:24 . :..I3 ...a':31;p, :::: 3?1..: ..
12 0700 24 Y 0.329 7.3 44 8.5 12
:1:3.`i%;A7017...• i:24:...$..iV..: 9.3,14 . ?:: ...:: : 25:> : 491:
14 0700 24 Y 0.379 3 7.3 8.6 _
14
16 0700 24 B 0.426 7.3 9.0 16
:11';>?.4I713tf: . .. : ig:4 :1i:.i. ::':::.:;y;: :i;:::;>i*i i,: `#:'.i;::` •i:=:i:r::<:'';i'.W.: /'.. ..: ,- ...... , :. ..:.:.. 17.
18 0700 24 N 0.334 17
18
I9 41700 .. :24. .,;.;IS 0.290 ;:, :73::<. . .. . ...: . ..; .:24.... . -..JOt : ,:
20 0700 24 Y 0.258 4 11 <0 22
31.::.1)700 ::.::24.. x.. a; :' 2 .
22 0700 24 Y 0.206 2 5 22
5.2. 070fl. ,;:4 :Y 0 2Q7. .':,,... .; 7II.:.i 2
24 0700 24 B 0.253
0:.:i:.OTS)ty.-..:. 24 - 0 373!. ... .......
26 0700 24 Y 0.289 7.9
22 9.2 20
27 `: 4)700 . ;:24 Y: it3N0 3.-. 19. -.o.3
28 0700 24 Y 0.557 5 8.0 9.0
28
?9" `074f0 . .:;2$ ::Y 41.5B8 ' 5 v; 5... 34: ,:
�. . : _ . 2r
30 0700 24 Y 0.54 I 8 2 9 2
fii;�::1:0 . '24 . ;Q.:IiE: SSS 30
AVERAGE 0354 5 111111, 30 067 32 91 0000 0.369 1 00775 68 AVG
1ti3AX`If‘40lv3.;' 0 i$3 fl :' 8,.2 :il M8 1 75 : 44- k10 9 `:' 0 0100,>:
MINIMUM 0.206 2 0 5 <0 22 22 8.2 0 01n0 0.369 0 O.75 >C 8 MIN`
:COv1PORAB .; CY31�T: L'OMk GRAB.;; COMP; COMIy: GRAB ' ._ � ,'CrRA33 COA3z' ;' t"'lltvli?; CO*:1B Cf){v1P :.:;;. £1G
DAILY LIMIT NA 300 6-9 1043 I 46.00 400 5.0 DY
: 1(>NITIuLY.1,1MIT 2 365: 154 : 4....: ME1...;I -.: 3R :<._ . :.34;t -8
DEM Form MR-I(12/93)

Attachment A
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH OCTOBER YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY DAVID L.CASNER CLASS III ARADE IV COUUNT(704)636-6 ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC)
CERTIFIED LABORATORIES (I)PERFORMANCE FIBERS,INC.-S" LISBURY
PERSONS COLLECTING SAMPLES WST TRT OPRS
CHECK BOX IF ORC HAS CHANGED i
Mail ORIGINAL and ONE COPY to: X nv c/�_ r� /C /'/ ()
DI ,-;- 7
V.
O CENTRAL.FILES SIGNATURE OF ORC) DATE
DIV.OF ENVIRONMENTAL MANAGEMENT BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P OBR ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
P.O.BOX 29535
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665 p
I) I alem A
A Turbidity Nitrate+ Total Total Total T
T Nitrite Organic Kjeldahl 'hosphorus
E Nitrogen Nitrogen Nitrogen (as P)
(as N) (as N) (as N)II NTU mg/I mg./1g
m fl mg/1 ..........._............:. :. ::::::.::.::::;o:c:......::;:; i::F E::::;;::::;;;;9;?::;;:;;>:SiGi:<i;�:::2Y::iS:i:r c::<a
•
........................2
-•::::.: : : : .;:;:;:;:::r: i'iiE:is :•i ''•:...i:< `.:i
•
•
•
•
•
•
•
•
•
4 ...::. ... ...
1111_ <002W 0330 0695 0617 --___-_-- .., "._ .. •
•
6?A _. a
14
15..
16
16
18
.._..................::...:::::,:::.:.: .:::;:;:»:::.::::::o:i5::: > ::%':;i;'?3i:<?;i.'$;its:> irr#i::i'%;!i:33;:(i y:ii i%iYi<;ji?18 '
18 ....... .. • • ... .. ........
20 20
. ..:i.... • 1.
23,. • 390 22
•
22 ,.:....:. :.:...::.::....:. .. .. .,.........
24
Z3:::::L:Yi:::?s;::i:�� i;i%;:ii^,:<:r;:i::':::Y.:2::;;::;>:;:::::.>::>::c:::•xo:�:�:�;:�:�r:r.::;:r..;:.:::::::::::.�:.:........
..................,.:::.�:::::::.:::::::.: r;:.;:;.>.:::.::;:;;:L;:;:;x;5;52:?S:'ct F.'s i 5;'i::% i i'.i[[ii.i i::i•'ii iii;i+'4...... % =`<'4:
24 .. .. ._.._.
.. .:::::;:.;>::>::::>::• :::::;:;;:i::SS: `i:i `:i: i•:i2':iiii:ii;::ii:i:::ivi'r3E: i>iSii'i;;`'ii:i;R:>::i;::;:::;;::;::::i:%::::.':::.:;.;.:::•;>;.:. .:. .::..............:.
•
•
26 26
:
30
30
0
AVG
AVG 5.75 0 0330 0895 0617
:0 i..1/ .:6: .-:
1
® 3,90 <0.0200 . 0.330 0.895 0.617 .. .. .
( L}::. GP.AI3 L'OMl c-oiw • CDLdP COA4P
DY 1 NA NA NA NA NA h33
N4:':F ItiA h4 .. :::
o L11 rnrm MR•1 112.93)

Attachment A
EFFLUENT page 1 of 2
, PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH NOVEMBER YEAR 2009
-ILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
PERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED 1 PERSONS COLLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to: �2�� ''
ATTN:CENTRAL FILES X �ir �ti J, qo.�--- ��-�D 'C J
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNA RE OF CRC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
50050 J 00310 00040 00530 _ 00610 31616 00300 01042 01045 01055 TGP3B
D Opr. Opr. Fecal D
A Arrive Time ORC Flow BOD5 T Coliform Dissolvd Total A
T Time on on @ PH S AMMONIA Oxygen Copper Iron Manganese CHRONIC T
E 2400 Site Site I I Inf 20C S NITROGEN Geometric (DO) TOXICITY E
clock I XI Eff Mean _
8 HRS HRS Y/N MGD LBS/D UNITS LBS/D LBS/D a/100ml Mg/1 Mg/I Mg/1 Mg/1 P/F34% 8
1 0700 : 24 N 0.851 43:: I.
2 0700 24 Y 0.860 7.6 50 9.3 PASS 2
3 0700 24' . 'Y' 0.744 6 68 <0.62 _ <0:MOO 0.214 0.0409 3
4 0700 24 Y 0.604 5 7.7 9.7 4
5 0700 24 ' Y 0.503 ' 4 25 5
6 0700 24 Y 0.431 7.5 9.4 6
7 0700 . 24 B 0.377 7
8 0700 24 B 0.346 23 8
9' 0700 . 24 B 0.325 7.3 23 10.1 9
10 0700 24 Y 0.391 3 23 <0.33 10
11 0700 24 Y 0.846 7 7.3 10.0 11
12 0700 24 Y 1.156 10 67 12
13 0700 -24 Y 1.174 7.5 9.8 13
14 0700 24 N 1.003 14
15 0700 24 N . . 0.796 40 15
16 0700 24 Y 0.640 7.5 54 9.8 _ 16
17 0700 24 Y 0.540 9 32 '<0.45 17
18 0700 24 Y 0.492 8 7.5 9.8 18
19 0700 24 Y 0.457. 8 . 27 19
' 20 0700 24 Y 0.422 7.1 9.6 20
21 0700 24 B 0.386 _ 21
22 0700 24 B 0.385 19 <0.32 22
,
23 0700. 24 B 0.477 7.3 22 10.5 23
24 0700 24 B 0507 8 30 24
25 0700 24 B 0.487 8 7.5 9.8 1 25
26 0700 24 B 0.451 8 23 _ 26
27 0700 24 B 0.408 7.5 - 10.0 _ 27
28 0700 24 N 0.349 _ _ 28
29 0700 24 N 0.306 IS 29
30 0700 24 Y 0.288 7.4 21 10.1 30
AVERAGE 0.567 7 "MIN 33 0.00 31 9.8 _ 0.000 0214 0.0409 PASS 1 4VG
MAXIMUM 1.174 10 7.7 63 <0.62 50 10.5 <0.0100 0.214 0.0409 PASS MAX
MINIMUM 0.288 3 7.1 15 <0.32 21 9.3 <0.0100 1 0.214 0.0409 PASS MIN
COMP!GRAB CONT. COMP GRAB COMP COMP. GRAB GRAB COMP. COMP. COMP. COMP. C/G
DAILY LIMIT ( NA 518 6-9 1043 46.00 400 5.0 DY
MONTHLY LIMIT I 2.305 201 6-9 330 23.00 200 ' 5.0 MO
DEM Form MR-1(12/93)

✓ . �,; s Attachment A
,
EFFLUENT page 2 of 2
DES PERM"i'NO: NC0004944 DISCHARGE NO: 001 MONTH NOVEMBER YEAR 2009
�1ANCE FIBERS,INC.-SALiSBIJRY CLASS III COUNTY ROWAN
ACILITY NAME: PERFOR. E ORC) DAVID L.CASNER GRADE IV PHONE[phone]
.OPERATOR IN RESPONSIBLE CHARG
i CERTIFIED LABORATORIES (I)PERFORM1IANCE FIBERS,INC.-SALISBURY
t` ('HECK BOX IF ORC HAS CHANGED PERSONS C LECTING SAMPLES W'ST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
�I ' a
i-. DATE�4 '
D1V.OF ENVIRONENTAL ,aNAGEtiiENT SIGNA RE OF ORC)
DEIINR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665
U I 00620
A Turbidity Nitrate+ Total Total Total D
T Nitrite Organic Kjeldahl Phosphorus A
E Nitrogen Nitrogen Nitrogen (as P) T
(as N) (as N) (as N) E
# NTU mg/I mg/i mg/I mg/I
2 I
2
3 0.0741 1.09 1.09 0.330
4 4.90 3
5 4
6
7 6
8
8
10 9
I1 3.80 .. 10
12 _ ij
13. - 12
' !4
14 14
— .
16 15
17 - 16
18 5.30 17
19 18
20 19
T _
21 20
22 21.
23 4.10' 22
24
25 23
24
26 25
27 - _ — _ 26
28 27
29 — 28
30 29
30
AVG 4.53 0.0741 1.09 1.09 0.330 _
MAX 5.30 0.0741' 1.09 1.09 0.330 AVG
t MAX
MIN 3.80 0.0741 1-09 1 1.09 0.330 _
C/G GRAB COMP COMP ' COMP COMP
— 1 . MIN
DY NA NA NA . NA NA CO
MO NA NA NA NA NA I DY
MO +
DEM Form MR-I(12/93)

Attachment A
EFFLUENT page 1 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH DECEMBER YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS III COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I ' PERSONS OLLECTING SAMPLES WST TRT OPRS
MailORIGINAL and ONE COPY to:
ATT / /�/
ATTN:CENTRAL FILES �/ I/ //?—"/0
DIV.OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
50050 00310 00040 00530 00610 31616 00300 01042 01045 01055
D Opr. Opr. Fecal
A Arrive Time ORC Flow BODS D
T Coliform Dissolvd Total A
T Time on on @ pH S AMMONIA Oxygen Copper Iron Manganese T
E 2400 Site Site [ ]Inf 20C S NITROGEN Geometric (DO)
clock 1 Xi Eff E
Meao
# FIRS FIRS YIN MGD LBS/D UNITS LBS/D LBS/D #/100ml Mg/I Mg/I Mg/I Mg/I #
i` ':':n70bs `i' :i ii'i•`..`>:_:'[:'"i[i:i i:i( i:i[i[i:iii: i; ,;::5•:•.:: :::::: ...::::::;:::::•: -:.;.;.:.;._:... •.-......_.,,....,.•
.. . ... d..... .......:..... c;.;.:.;.;.;.,:.::::::: :;:;:;::::�: ::::;::;`;:::[::?:::MiX 5i Si;::iiii'S '`•:.EE'i ff:f
2 0700 24 Y 0.410 10 7.7
::: i;::€0011: ::24€:;:;: is Vi641:€::::ia::::::i: i:::: . :: :i :;:::.::.:.:::::::;:;:,:::.:.:.::.;.;.,..:.;.,.................................:.,.;. .:;;.._......_................ 2
4 0700 24 Y 0.621 7.3 " "'
:::;::•:-•.:.:.;.: ... In s
i3:S i:4700iE('''24':`':.'B;:i E:E0811ir E i:: :i:i:``i':?.;,: ,,?,!:;c: :: ::: :: : :.:•.:.::
4
6 0700 24 B 0.483 24
i i .. 5.i.E...E : 6r............... :: : i E;i'7 i /0 `ii s 4 :B": 0'#li i. ?:.iai ...:. :i ..:::: d :iiE.(:i:::; :,: ` :i ;1-'i?: i: i ii i : >8 0700 24 Y 0 401 7 20 <0.33 <0.0100 0.110 0.0476
8.
:::9 ::0001:i:'•i2di i:::i:Y:c ::0 56Ti :::'::::::::::::::::: ::: .;.:.;
10 0700 24 Y 0.602 10 30
i':F°I:I!::'ky0ii 'sE24::ii :: i: •':c' :'?
' •', ..:;.:.:::[iii:i:; "' i `i'i 555i ' :.::: .-. 10
12 0700 24 N 0.475
::1H1::iA700 i'`:'I:2d: ::::;l l::i : i,.463iT:iiEi:!E:::::i;::E_:E:::i::::i:;::: ;.•..............:.:.:.:....•.•.-.........,..:,:. ...:..:. ::10:.....,.;:;:;: :.:.:.;.-:.;.;.;......:'i,F i......-.-.........,..... 12
14 0700 ::r.:..: :::14::
24 B 0 472 7.7
�� 14
:1ii :t ......::i.'I:;:E ;1 :;:::E0:451�f•i: 'i:[: ::E:E:lif::�S:::1:i E::i:i::::::•':• .....::::::::::::::::':.:::::::::.:;:.:.::.:-:.:.:...:.:.:. ...............- . . .... .. l
16 0700 24 Y 0.419 7 • 7.8 .:.:...:::: ::::76::
:'1'l;E.07AO a::24 r ..t`E 0 3$4:: =i•iiiii i r;; i 20. 6;E:::: ::.:E::. :.:............ .. : :;::::.:-..:i":::::::;,9.8 16
!7
...�..�v ....:...:.:..:.:.:..... ......�;;;�;�;•;�;:;:;.;;:: �f:i:i�:�i:i;: ::;ii?iLj iii:!;i;i::::i[i: :ii:ii i?i ii-:,i:18 0700 24 Y 0.459 _..i8.0
':19' si#700`:';' ; .'• ^::Iii:: ::?::::::: : ::::::
::::: ::::: :':: :::.::•.: ::• : :.:.:. 104.....:.............. .-........ ... IS
::::20iP
20 0700 24 B 0.537 27 <0.45
E;21E `$7l)0`%!14.Ci:;EE'-YPEi E;:0 i.'!:i:i :`';i ,: 79..[:
0
22 0700 24 Y 0.468 12 EEii:i:
: iE ::t17b11i'c:Ei i1i'i'.i:i1i'':::0:402::::::::i:iii: : :::: ::::::::::::::::::::: :::::::::::::::::::::::::::::::::::::::::::;:; ;:•:.:::::•: 22
24 0700 24 B 0.366 6 24-.. •:::::.::::::::::::: . :;
18 24
26 0700 24 N 0.689 `'``;
.. O.k6.:f::2a:€: :::1its:: is€U:¢ :i: ::::::::::::::.:::::::::::::::: .::: :
:::::::::::,:;:;:;:,:;;:: :::.;.;.:.;..;,.,.;.:.; ::::;:. :::;:::.,..;.:.::.;.;.:.;.:.:....................... -......
26
28 0700 24 B 0.533 7.9
::29:::E0700`z`:24 B: 0,431,E! b.':. is::: i :r::: ::25.;.;..E i.0 8 ii :::':`i 1iEiEi:ii .:':E::Ei:f.. :... .
.........•:..:...:::.:?:;.,:i.!I •: .:: :;: ...::.:.,.:....... 28
19:
30 0700 24 B 0.372 6 7.4 9.3
91' {I?0Q # il;' ::E$: �353.......................................................... - 30
AVERAGE 0.485 8 '3G
24 0�� '3 �1C 0.000 0.110 0.0476 AVG
i:iv[A0GJM 4689k 14 ;g_3 is' 37 6 85 24: s 2
1- D 01tN1 O IiI f20iti 6 :::`:MiO.C:
MINIMUM 0.286 4 ^ 7.3 14 <0 24 21 9.3 <0 0100 0.110 0.0476
• . O1�1P.7Glt II3`:. COtv'I� CO'vtP: •::;i : Ri4 42 .':::L'•di3.4: :: • •hll? GR tB .•; P:.Ali eifii P :COMI'i..: Cif,O .:.;. MIN
64
DAILY LIMIT NA 518 6-9 1043 45.00 400
5.0 DY
::$40ii*il:'1IIvi1:T E 4: 'E..`.201:'',.'•�;:: 6-9;i i a3p c E:`29;66.:: :: : i a00"::.'' i;::::3:A
DEM Form MR-1(12/93)

Attachment A
EFFLUENT page 2 of 2
NPDES PERMIT NO: NC0004944 DISCHARGE NO: 001 MONTH DECEMBER YEAR 2009
FACILITY NAME: PERFORMANCE FIBERS,INC.-SALISBURY CLASS HI COUNTY ROWAN
OPERATOR IN RESPONSIBLE CHARGE(ORC) DAVID L.CASNER GRADE IV PHONE[phone]
CERTIFIED LABORATORIES (1)PERFORMANCE FIBERS,INC.-SALISBURY
CHECK BOX IF ORC HAS CHANGED I I PERSONS LLECTING SAMPLES WST TRT OPRS
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES X �—/ �D
DIV.OF ENVIRONMENTAL MANAGEMENT . (SIGNATURE OF ORC) DATE
DEHNR BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS
P.O.BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH,NC 27626-0535
00076 00630 00600 00625 00665
00620
D
A Turbidity Nitrate+ Total Total Total
A
T Nitrite Organic Kjeldahl Phosphorus T
E Nitrogen Nitrogen Nitrogen (as P) E
(as N) (as N) (as N)
# NTU roA nag/1 m /I ro
2 3.48
2
4
:. ..:. 4
5::::::: ::::::::::::::::::•:•:E:::'::::::;:::: :::::: ::: • ............::: :.;.:.;.;....;.;.;.;.;.;...................... ...-.... ........
6
6
NM
0.0516 1.02 1.02 0.265 miinmalm
10
IE i;M====M : •
• EMEMEMM• 012
14
.;..1................................. 14
16 2.90
16
18
:;:; ... ... 18
19:`:i...•................ ['i 5i:::`i:i:i`i i:;:i:':!:i::5i:iii;..: (:,i `i::;:[:;:
20
20
•. _1.:..,...Z<SQ:.:.::.:.:.:.:���:.:�: :.:.;.:..,.�.;.;i;i;iir:�:':::�::�E�:`•i:;:;:
22
2
23: :: ..... 2
24 ::�3
25 :.;.;.: • 24
�..�.�.. .............�.�::.:::;:.:-:�;•;;•; :[:.:: �:�:�:•:�:�:...�...�.�.�....:=:�[�ri gQ:>i�5?::i::is<:::::asi:i i::7
26 5
26
28 .. ... 27
,.,.,...
2A;:; i:i:i i::;:;::i ii3i?:" :'.:. :::::::::::::i'::_`!!;i[ p:p:;:.::E'i sG: :..........[:i f`.........::::::':::::.:::::::::.:.:.;,.:.: 28
• ;
30 3.00 - 24;:
31
30
3i •
® 2 96 0.0516 1.02 02 0.265 _-_EEO
MAC 48. 00515 ti02 102 0 2G3 •
MIN 2.50 0.0516 1.02 • 1.02 0.265 ME
?MIN
DY NA NA NA NA NA
DY
DRM l orm MR-I 112/93)

Attachment B
Calculation of Total Nitrogen Contributed by Anaerobic Pretreatment System
Edgewater Treating
NC0004944
Parameter Value Units I Notes/Source
Anaerobic Treatment System
COD Loading to Anaerobic Influent 25,000 J Ib/d Per 1994 Operating Manual this is design and normal loading rate(page 1-9,Table 1-2)
Flow through Anaerobic System 0.10 'MGD Per 1994 Operating Manual this is design and normal flow rate(page 1-9,Table 1-2)
Estimate Yield 0.04 lb VSS/lb COD/d Per Metcalf&Eddy page 634 and typical of anaerobic systems
Sludge Yield 1000 lb VSS/d Calculated(Yield x COD Loading)
Nitrogen Composition of Sludge 12.2% Metcalf&Eddy Section 7-3 p.565,Nutrients Required for Cell Growth
Dewberry assumes anaerobic thermophilic sludge would not thrive in downstream aerobic process and
TN Load from Anaerobic Sludge 122 Ib/d would be hydrolyzed to soluble organic nitrogen.Hydrolysis is expected to occur because the aeration
basin was operating at approximately 25 day SRT.
Residual Ammonia in Anaerobic Effluent 30 mg/I Per 1994 Operating Manual page 11-10 ammonia was dosed to achieve this residual
TN Load from Residual Ammonia 25 Ib/d Calculated
TN Load to WWTP Total from Anaerobic 147 lb/d Calculated,Sum of anaerobic sludge load and residual ammonia load
Impact of WWTP TN From Celrobic
WWTP Additional Influent COD from Anaerobic 2500 Ib/d Authorization to Construct documentation in Archive File indicates 90%COD removal in Anaerobic.
Yield 0.1 lb VSS/lb COD/d Assumed based on professional experience with aerations basins operating at higher SRTs.
Nitrogen Composition of Sludge 12.2% Metcalf&Eddy Section 7-3 p.565,Nutrients Required for Cell Growth
Additional Nitrogen to Sludge from Celrobic 31 Ib/d Sludge wasting is the only mechanism for removing nitrogen from the system.
Net Nitrogen Gain from Anaerobic 117 Ib/d Calculated(Nitrogen Contributed-Nitrogen to Sludge'
Acronyms
COD:chemical oxygen demand
lb/d:pounds per day
MGD:million gallons per day •
mg/I:milligrams per liter
SRT:solids retention time
TN:total nitrogen
VSS:volatile suspended solids
References
Metcalf&Eddy,Inc.(2003).Wastewater Engineering Treatment and Reuse(4th ed.).New York,NY:McGraw-Hill
Celrobic Wastewater Treatment Operating Manual developed by Raytheon Engineers and Constructors.February 1994.
2/7/2019 9??• Dewberry

Excerpt of pages from 1994 Operating Manual for Anaerobic Treatment System. Entire document can be provided
upon request.
Raytheon Attachment B Celrobic' Wastewater Treatment Operating Manual
Engineers 8.Oonstn�cio�s Hoechst Celanese Corporation
A Ccrioaidadon d Badger and UFBC Salisbury, NC
1. Type, Location, and Purpose of Facility
The facility will Celrobic high rate anaerobicgroundwater
a ty ilbea g g
treatment plant, located at the Hoechst Celanese facility at Salisbury,
NC. The unit is designed to treat groundwater containing ethylene
glycol from the plant site. Two trains of treatment (two 50% capacity
filters) are incorporated into the system to allow for future use of one
train in the treatment of plant effluent. The unit is designed to treat
25,000 lb/day of soluble biodegradable COD. Pilot testing carried out
on the plant site (Badger Project No. BD-7241) indicated that the water
is highly treatable.
2. Filter Feed
The initial substrate (feed) for this system will be groundwater
containing ethylene glycol from the Salisbury site. The average COD
concentration of the water is expected to be 29,750 mg/I. The water
has been identified by Hoechst Celanese as non-toxic and non-
hazardous.
Two operating cases have been defined. The normal case of 100,800
gal/day (35 gpm per filter) which is the initial planned pumping rate for
wells in the plant groundwater field. At the design COD concentration
of 29,750 mg/I, this stream contains 25,000 lb/day of COD.
The hydraulic design case has been fixed at the flowrate at which the
heat required to heat the feed is equal to the heat generated by burning
the off gas generated at the design organic load. This feedrate is 85
gpm per filter (122,400 gal/day).
Hoechst Celanese Corporation February 1994 Page 1-8

Attachment B
Celrobice" Wastewater Treatment Operating Manual
Hoechst Celanese Corporation
A Ccnso&dsticn d Badger and UEBC Salisbury, NC
Table I-2
Summary of Design Cases
Total Flow Normal Case Normal Case Hydraulic
(both filters (per filter) Design Case
combined) (both filters)
Total Flow (gal/day) 100,800 50,400 244,800
Total Flow (gpm) 70 35 170
COD Concentration (mg/I) 29,750 29,750 14,700
COD Load (lb/day) 25,000 12,500 30,000
Specific Gravity 1.0 1.0 1.0
Temperature 58 °F 58 °F 58 °F
3. Filter (MT-102 A/B)
The filter sizes are based on the normal organic (COD) load rate at an
applied specific organic load based on the results of the pilot test
results. The required packed volume for the total organic load has been
divided in half to create two 50% capacity filters.
Hoechst Celanese Corporation February 1994 Page 1-9

Attachment B
Rapboom Ce!rabic' Wastewater Treatment Operating Manual
�h�eer=g pia Hoechst Celanese Corporation
A CansoIdakti fialgef and MAC Salisbury, NC
Table 1-3
Filter Design Criteria
Specific Organic Load 0.7 lb COD/ft3/day
Required Packed Volume 35,715 ft(total)
17,858 ft3 (per filter)
Filter Size 27.5 ft diameter
(each filter) 40 ft high
Operating pH range 6.8 to 7.5
Recycle ratio 5:1 minimum (20:1 at initial conditions)
Upflow Velocity 9.6 - 17.7 ft/hr
Temperature 98 °F
Pressure 8" WC Normal
2" WC Minimum
14" WC Maximum
Materials Carbon Steel with internal epoxy coating
The filters are insulated for heat conservation.
Hoechst Celanese Corporation February 1994 Page 1-16

Raytheon . . . . Celrobie Wastewater Treatment Operating Manual
g Hoechst Celanese Corporation
A Consoldation of Badger and UE&C Salisbury, NC
Figure II-1
Equalization Flow Control
GA-102A 1iEo 1 i o
TO
// ' FILTER
j j %, : %%jam/ 7
AMMONIA % %/%,w.:, MT 102A
MT1Q1 '
FT
v v v -+ MICRO- FI 110 FY
NUTRIENTS t12 i 1108
PHOSPHOR! Fl s Q I' FY n
ACID 113 11 1� 110A
9' 1 '
ed
A
3 61\ FI (F-7Y..
AMMONIA 11 17 1 17A
I
MICRO- FI IIll FY
NUTRIENTS 1 15 , FT 1176
117
PHOSPHOR! FI GA-102B
ACID t 16 Jr-
/�':� ` FILTER
,y, ` MT 102B
PP 101 S PP-101 A FE ' 1;;�
117 �
Hoechst Celanese Corporation January 103 Page 11-5

Attachment B
Raytheon Celrobic" Wastewater Treatment t Operating Manual
Engineers&Consbuctors Hoechst Celanese Corporation
A coasodidatio►►a Badger and UE&C Salisbury, NC
and TT-102B ("A" and "B" trains respectively). Both heat
exchangers are plate and frame type.
The design temperature of the groundwater feed is 58°F. Under
the design conditions (85 gpm per train at 58°F) the amount of
heat exchanged is 1.70 x 10' BTU/hr per exchanger.
The temperature indicators and pressure indicators on the inlets
and outlets of both streams indicate the performance of the
exchanger. At the design hydraulic flow rate (85 gpm), the
pressure drop on the hot water side is 9.3 psi and the pressure
drop is 3.0 psi on the wastewater side. Higher pressure drops
and/or lower temperature differences indicate plate fouling and that
the exchanger should be flushed or cleaned.
Filter feed from MT-101 is heated from 57 °F to at least 98 °F by
Feed Heat Exchangers TT-102A and TT-102B. The heating
medium is hot water at 200 °F which is supplied to the filter feed
heater by the Hot Water Heaters GZ-111A/B. The hot water
supply flow rate into the filter feed heat exchanger is controlled by
the two temperature control valves TV-712 and TV-715 (for trains
A and B respectively) which are three way valves, directing hot
water to the filter feed heater or recycling it back to the hot water
furnace depending on heat input required.
The temperatures of the mixed feed streams are controlled by
temperature controllers TIC-720 and TIC-731 which reset TIC-712
and TIC-715 respectively. PID controller TIC-720 and TIC-731
controls mixed feed temperature The normal set point for TIC-
720 and TIC-731 is 98°F. TIC-720 and TIC-731 are reverse acting
controllers that manipulate the set point of TIC-712 and TIC-715,
the filter feed temperature controllers.
TIC-712 and TIC-715 are reverse acting controllers which
manipulate TV-712 and TV-715 for feed temperature control. TV-
712 is a three way valve directing hot water through or around
Hoechst Celanese Corporation February 1994 Page 11-8

Attachment B
Raytheon Celrobic" Wastewater Treatment Operating Manual
Hoechst Celanese Corporation
A Consolidation d Badger and UE&C Salisbury, NC
feed heater TT-102A and TT-ion. The valve failure position is
to bypass the heater.
TIC-720 and TIC-731 reset TIC-712 and TIC-715 (cascade).
When in automatic (i.e. with TIC-720 and 731 resetting TIC-712
and 715) the output signal of TIC-720 and 713 have high output
limits so the upper set point of TIC-712 and 715 is limited to
120°F' '
High temperature alarms TAH-712 and TAH-715'are set at 120°F
and high/low temperature alarm TAHL-720 and 731 are set at
102°F and 95°F respectively.
iv. Nutrient Control
Nutrients are added to the wastewater stream in order to supply the
biomass with the essential chemical building blocks for
reproduction and digestion of the organic waste. Three sources of
nutrients are included in the Celrobic system: ammonia
(anhydrous) for nitrogen supply, phosphoric acid (35 wt%) for
phosphorus supply,and micronutrient solution(an aqueous solution
of dissolved metals salts) for supply of minerals essential to
enzyme formation.
Ammonia
Ammonia for both filters is supplied by truck and stored in MS-
112 at a pressure of approximately 100 psig. Ammonia vapor is
released to the process system via a backpressure control valve at
the tank. This valve is set to maintain the operating pressure in the
vessel.
The flow rate of the ammonia is set by the operator using the
indicating flow controllers FIC-111 and FIC-114 (for the A and B
trains respectively). The flow rate of the ammonia is set by the
operator through the PLC, based on the expected COD load to the
Hoechst Celanese Corporation February 1994 Page 11-9

Attachment B
Raytheon Celrobic" Wastewater Treatment Operating Manual
Engineers&Constructors Hoechst Celanese Corporation
A Ccossdidation of Badger and UE&C Salisbury, NC
filter and corrected by ammonia concentration in the effluent liquid
stream. The target for the ammonia addition system is to maintain
an excess ammonia concentration in the liquid stream of between
20 and 30 mg/1. This excess ammonia will be consumed in the
downstream aerobic treatment system and will serve to reduce the
ammonia addition requirements for that system.
Phosphoric Acid
Phosphoric Acid for both filters is supplied by truck and stored in
MS-106 at a concentration of 35 wt%. A level indicator (LI-200)
is provided with both local and PLC readouts to indicate the
available quantity of phosphoric acid. In addition, a high level
alarm (LAH-200A) is provided at the truck loading point to
prevent overfilling of the tank.
The flow rate of the phosphoric acid is set by the operator by
adjustment of the stroke controllers on the phosphoric acid feed
metering pumps PD-105A and PD-105B (for the A and B trains
respectively). The flow rate of the phosphoric acid is selected by
the operator based on the expected COD load to the filter and
corrected based on the measured phosphate concentration in the
effluent liquid stream. The target for the phosphorus addition
system is to maintain an excess phosphate concentration in the
liquid stream of between 10 and 20 mg/l. This excess phosphate
will be consumed in the downstream aerobic treatment system and
will serve to reduce the nutrient addition requirements for that
system.
Micronutrient Solution
The micronutrients (Fe, Ni, Co, Mg) are supplied in dry powder
form and mixed up in the Micronutrient Addition System (GZ-
112). A new batch of micronutrients will have to be mixed up
approximately every two to three days depending on the feed rate
to the filters.
Hoechst Celanese Corporation February 1994 Page 11-16

Attachment B Excerpt from documentation retrieved from archived files for NC0004944. Documentation
was submitted to NC DEQ to support 1993 permit modification and Authorization to
Construct for Anaerobic Treatment System.
WWTP Evaluation
Based on the anticipated wasteloads presented in Figure 1, each unit process was
evaluated to determine the current operating conditions of the existing WWTP and
define the anticipated impact of the pretreated anaerobic stream. Current and future
conditions were compared with typical unit process design criteria (see Table 2).
Equalization
One 800,000 gallon basin, with three 2 hp surface mixers, is currently used to equalize
the COD load from Salisbury's process wastewaters. The anaerobic facilities will
include a separate equalization tank for recovered groundwater. The effluent from the
anaerobic unit will be routed downstream of Salisbury's existing equalization basin.
Therefore, operation of the anaerobic system will not impact the performance of
Salisbury's existing equalization basin.
Anaerobic Pretreatment
The anaerobic pretreatment facilities will include an equalization tank with a holding
capacity of 12 hours and two Celrobic high rate anaerobic reactors designed to remove
80 to 95 percent of the influent COD. Plans and specifications for these facilities have
previously been submitted to DEM.
Aeration
The aeration basins have a combined working volume of 3.8 million gallons (MG) and
are aerated using low speed surface aerators (700 horsepower total). At a maximum
historical operating temperature at 32°C and maintaining a minimum dissolved oxygen
(DO) concentration in the aeration basins of 1.5 mg/L, the maximum oxygen available
is 25,300 lb/d. Because the oxygen available exceeds the demand for monthly average
and monthly maximum conditions, the system has adequate COD and BOD removal
capacity for both existing and future (with anaerobic pretreatment) operating
conditions. -r,
Under peak loading conditions the DO concentrations may temporarily drop to zero.
In the future, under extreme maximum conditions (maximum process wasteload and
maximum anaerobic effluent wasteload), approximately 33,700 lb 02/d will be required
to sustain biological activity. Because only 29,400 lb 02/d will be available under these
conditions, it will be necessary to monitor the anaerobic unit to avoid discharging high
organic loads from the pretreatment unit and upsetting the WWTP. To minimize
adverse impacts on the WWTP, equipment (monitoring instruments and an equalizati,on
tank) will be installed to control excursions in effluent quality from the anaerobic
facilities.
ATLR1401039 51 3

Attachment C
tiithersRavenet
February 2,2016
Mr.Tom Belnick
Supervisor
Division of Water Resources
WQ Permitting Section-NPDES
1617 Mail Service Center
Raleigh,NC 27699-1617
RECEIVEDINCDEQIDWR
FEB 0 4 2016
Subject: NPDES Permit Renewal Application
Moncure Holdings West,LLC WWTP Water duality
New Hill,Chatham County,North Carolina Permitting Section
Permit#NC 0001899
Owner: Moncure Holdings West,LLC
282 Century Place,Suite 2000
Louisville,CO 80027
Dear Mr.Belnick
Moncure Holdings West LLC. has recently acquired ownership of site facilities previously owned by
DFTDuraFiber Technologies, Inc.(formerly known as Performance Fibers). DFTDuraFiber is in the process
of demolishing the old polyester manufacturing facility in New Hill, North Carolina. Following transfer of
ownership of the WWTP; Moncure Holdings West LLC.Is requesting renewal of the NPDES Permit(NPDES
Permit No. NC0001899) per Federal Regulations 40 CFR 122.41, and North Carolina Regulations (15A
NCAC 2H.0105(e)). The permit,which expires July 31, 2016,would allow Moncure Holdings West LLC to
continue to operate the waste water treatment facility on this location while the demolition of the existing
facilities are finalized throughout FY 2016. While none of the previously permitted OCPSF industrial
activities are currently ongoing,the stormwater from the site demolition of these facilities has the potential
to continue to discharge OCPSF residuals to the WWTP through the process drains. As areas are completely
demolished these drains will be plugged to prevent further discharge. Until such time the NPDES permit
needs to continue to monitor for and treat any of the OCPSF pollutants in the stormwater and maintain the
existing nutrient limits for the sanitary wastes from the approximately 20 employees retained on the site by
DFTDuraFiber and the demolition contractor. Moncure Holdings West LLC. is separately negotiating with
offsite industrial sources to enter treatment contracts. At such time as these are finalized Moncure Holdings
West LLC. will submit a request to modify the NPDES permit from OCPSF to a Combined Waste Treatment
Facility and will submit the data necessary for DENR to draft revised NPDES permit limits. Until such time
as these offsite waste streams are permitted and WWTP facilities upgraded accordingly Moncure Holdings
West LLC.requests that the NPDES permit be renewed with the current limits.
The existing NPDES Permit allows for discharge of 0.244 mgd of industrial waste into the Haw River(001)
and stormwater into Shaddox Creek(002). Each are in the Cape Fear River Basin.

CONTINUED FROM THE FRONT Attachment C
VII.SIC CODES(4-digit in order of priority)
A.FIRST B.SECOND
C 2824 (specify) 7 2821 (specify)
s ,s 17Manmade Organic Fibers, except s 16 19 Plastics, Materials, Synthetic Resins and
Cellusoic Nonvulcanizable Elastomers
C.THIRD D.FOURTH
c (specify) 7 (specify)
15 16 17 t5 16 19
VIII.OPERATOR INFORMATION
A.NAME B.Is the name listed in Item
c Moncure Holdings West, LLC formerly DFTDuralFiber Technologies, Inc. VIII-A also the owner?
8 ®YES ❑NO
18 19 55
C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if'Other,"specify.) D.PHONE area code&no.)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) A 303 516 3478
S=STATE 0=OTHER(specify)
P=PRIVATE 56 15 16 18 19 21 22 25
E.STREET OR PO BOX
338 Pea Ridge Road
26 55
F.CITY OR TOWN G.STATE H.ZIP CODE IX.INDIAN LAND
c New Hill NC 27562 Is the facility located on Indian lands?
B ❑YES ®NO
15 16 40 42 42 47 51
X.EXISTING ENVIRONMENTAL PERMITS
A.NPDES(Discharges to Surface Water) D.PSD(Air Emissions from Proposed Sources)
9 N I ' NC0001899 9 PI 16 17 18 30 15 16 17 18 30
B.UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
C T I C T 8 WQ0023197 WTP Alum Residuals
9
Land Application
15 16 17 18 30 15 18 17 18 30
Program Permit
C.RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
C TR I NC0053488409 c T 8 NCS000100 NPDES Stormwater
15 16 17 18 9
30 ,5 ,6 17 1B 30 Permit
9XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma• area. See instructions for •recise re.uirements.
XII.NATURE OF BUSINESS •rovide a brief descri.tion
A chemical plant engaged in the manufacture of industrial of synthetic polyester fiber and organic polyester resin
previously owned and operated on the site. This process facility is now being demolished. The administration
building, cafeteria, locker room, rest rooms and general storage warehouses will remain but currently are
unoccupied except for demolition crew and security staff. The site will be re-purposed following demolition and
a permit modification requested once knowledge of future waste components is available.
XIII.CERTIFICATION (see instructions)
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, 1 believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information,including the possibilit of fine and imprisonment.
A.NAME&OFFICIAL TITLE(type or print) B.SIG URE i C.DATE SIGNED
Jason Kaplan, Manager '/ `� C�-
COMMENTS FOR OFFICIAL USE ONLY
c
C
15 16 55
EPA FORM 3510-1(8-90)

From NC0001899 (DuraFibers Moncure, NC) February 2, 2016
Attachment C NPDES Permit Renewal Application.
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY You may report some or all of this information EPA I D.NUMBER(tom/rnrnfhvrr 1 ofhhrni I)
on separate sheets(use the same format)instead of completing these pages NCDO c 34 884 09
SEE INSTRUCTIONS
OUTFALL NO
✓ INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall See Instructions for additional detaiis
3 UNITS 4 INTAKE
2 EFFLUENT (y><arfi'i/ht.(I (.yvnuiul) __
b MAXIMUM 30 DAY VALUE c LONG TERM AVRG VALUE a LONG TERM
a MAXIMUM DAILY VALUE (I4,110rluhlr) (i/inudirhle) AVERAGE VALUE
(1) (1) d NO OF a CONCEN- 1 b NO OF
1 POLLUTANT CONCENTRATION (21 MASS CONCENTRATION (2)MASS I11 CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION 121 MASS ANALYSES
a Biochemical Oxygen 7 8 1 0 4.9 0.5 m 2.51 0.5 40 /1 lb/day
Demand Oft a i) 9 y
b Chemical Oxygen _ T
Demand(r(.h)
c Total Organic Carbon
(fur-)
d Total Suspended
Solids(/tti) 14.6 7.2 9.4 2.3 5.55 1.01 40 mg/1 lb/day
e Ammonia(in t) 6.9 3.5 6.9 2.3
VALUE VALUE VALUE VALUE
f Flow 0.118 MGD 0.066 MOD 135
g Temperature VALUE VALUE VALUE VALUE
(ii rr.r) 19.5 17.2 73 'C
h Temperature VALUE VALUE VALUE VALUE
(.r,„r+,,..} 28.8 25.4 62 C
MINIMUM_ MAXIMUM MINIMUM MAXIMUM ;, tir is ,- ' +< -_ s .r -'r - -
PH 6. /8 8.8 6.78 B.8 �_ ". r• `A' " ' 135 STANDARD UNITS I,
PART B- Mark"X-in column 2-a for each pollutant you know or have reason to believe is present Mark X in column 2-b for each pollutant you believe to be absent If you mark column 2a for any pollutant which is limited either
directly or indirectly but expressly, in an effluent limitations guideline you must provide the results of at least one analysis for that pollutant For other pollutants for which you mark column 2a you must provide
quantitative data or an explanation of their presence in your discharge Complete one table for each outfall See the instructions for additional details and requirements
2 MARK'X' 3 EFFLUENT 4 UNITS 5 INTAKE(upa..iarl)
1 POLLUTANT b MAXIMUM 30 DAY VALUE c LONG TERM AVRG VALUE a LONG TERM AVERAGE
AND a o a MAXIMUM DAILY VALUE (Uuiuilrrh/i) (rl(Ir. Mute) VALUE
CAS NO BELIEVED BELIEVED ;11 (1) (1) d NO OF a CONCEN- (11 b NO OF
plat,idah/c) PRESENT ABSENT CONCENTRAT ION 121 MASS CONCENTRATION (2)MASS CONCENTRATION i2r MASS ANALYSES TRATION b MASS_CONCENTRATION (2)MASS ANALYSES
a Bromide
(24959 62-91
+b Chicane,Total
Residual
c Color
d I ecal Coliform
r e rtuoude
(16984-48-8)
t Nitrate Nitrite
(as N)
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

1
1

Irrom NL,uuu189a tuuraFioers IJloncure, NC) reuruary c, cU16
Attachment C NPDES Permit Renewal Application.
ITEM V-B CONTINUED FROM FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5 INTAKE(uppoul)
1 POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a b a MAXIMUM DAILY VALUE (,/uwduhle) (r/uvudublr) AVERAGE VALUE
CAS NO BELIEVED BELIEVED (1) (1) 1) d NO OF a.CONCEN- (1) b NO OF
warm/able) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2)MASS ANALYSES
g Nitrogen,
Total Organic(u,
A7
h Oil and
Grease
i.Phosphorus
(as P).Total
(7723-14-0)
).Radioactivity
(1)Alpha.Total
(2)Beta,Total
(3)Radium,
Total
(4)Radium 226,
Total
k Sulfate
(u,T),)
(14808-79-8)
I Sulfide
(m.$)
m Sulfite
(a%.S0.)
(14265-45-3)
n.Surfactants
o Aluminum.
Total
(7429-90-5)
p Barium,Total
(7440-39-3)
q.Boron,Total
(7440-42-8)
r Cobalt,Total
(7440-48.4)
s.Iron,Total
(7439-89-6)
1.Magnesium,
Total
(7439-95-4)
u.Molybdenum,
Total
(7439-98-7)
✓ Manganese.
Total
(7439-96-5)
w.Tin,Total
(7440-31.5)
x Titanium,
Total
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

Attachment C
DAK Americas
FIBERS,MONOMERS&RESINS
DAK Americas LLC
Cedar Creek Site
3468 Cedar Creek Road
Fayetteville,NC 28312
NPDES Permit No. NC0003719
Renewal Application
RECEIVED/NCDEGYDWR
MAY 11 2016
May 3,2016 Water Quality
Permitting Section
Prepared by:
Elizabeth Wike,Donald Allbright,and Gary Slater
DAK Americas LLC
3468 Cedar Creek Road
Fayetteville,North Carolina 28312

Attachment C
Continued From The Front
VII. SIC Codes (4 t,in order of priority
A.First B.Second
2821 Plastics Materials,Synthethic Resins,and 8182 Plastics materials and basic forms and shapes
Norwuicarraable Elastomers
C.Third D.Fourth
I
ViII. Operator Information
A Marne B. Is the name listed
in item VW-A also
OAK Americas LLC the owner?
El Yes NO
C.Status of Operator(flew the appcpdale tatter lab the ensue(box;if TOW,Wpec+y'.) D.Phone(cods d no) ❑
�
F=Federal M rr Public(other than federal or slate)
S=State O=(apeciJy) P (specify) [phone]
P=Private _
E.Street or P.O.Box
P.O.Sox 1590
F.City or Town G.Stale H.Zip Code IX. Indian Laud
Fayetteville NC 28302 Is the facility located on Indian lands?
_D Yee ®No
X. Existing Environmental Permits
A NPOES Oedemas to Surface WON) D.PSD(Air Emissions from Proposed Sources)
NC0003719 WA
B.UIC(thrde pti nd Injection of Ph s) E.Other(specify) (eps4ilY)
WA 04319122 Air Quality Title V
C.RCRA(Hazardous Wastes) E Other(specify) (ate)
WA NCS0003119 &ammeter Discharge
211SRF Permit to Discharge Wastewater Under
the Public Works Commission's
Industrial Pretreatment Program
XL Map
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show
the outline of the facility,the location of each of its existing and proposed intake and discharge structures,each of its hazardous waste
treatment storage, or disposal facilities,and each well where it Injects fluids underground. Include all springs,rivers and other surface
water bodies in the map area. See instructions for precise requirements.
XII. Nature of Business (provide a brief aescriaition)
DAK is engaged in the manufacture of polyester chip used to produce various plastic items for industrial and consumer use. The Cedar Creek site
consists of four maim areas:
1 The Resins Plana,located in the southwest portion of the property, is comprised of the continuous polymerization(CP)aces and the solid state
polymerization(SSP)plant. Railroad trod('are located on the southeastern portion of the property for the loading of product and the unloading
of raw materials.
2. The Batch Plant,located north of the Resins plan and fomttrty the Dupont Teilln Film plant,producers specialty plastics.
3. Clear Path Recycling,located on the east side of the site,recycles post-consumer plastic beds*with operations to separate,wash,and Aske
bottles.
4. The Services Complex,located in the center of the site,supplies utilities for all areas. Utilities include steam,cooling water,chilled water,
dsmineralized wafer,and wastewater treatment
XI I i. Certification (see instructions)
i certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this
application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the
information contained in the application, I believe that the information is true, accurate and complete. I am aware that ff._._
are signifcant penalties for submitting false information, including possibility of fine and imprisonment
Name 4 Official Title(type orprfat) B.Signature C.Date Signed
Matthew Hendrickson
Cedar Creek Site Mana er 3/ 16
EPA Form 3510-1(Rev, 10-80) Reverse

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Attachment C
NPDES PERMIT RENEWAL APPLICATION
CNA Holdings LLC > Shelby Facility
Prepared By:
Kim Teofilak-Senior Consultant-Trinity Consultants,Inc.
Jose Orsini-Principal Consultant-Trinity Consultants,Inc.
TRINITY CONSULTANTS
325 Arlington Ave.
Suite 500
Charlotte,NC 28203
[phone]
February 2018
Project 183402.0012
Trinity/A
Gnsu1tants
Environmental solutions delivered uncommonly well

Attachment C
CONTINUED FROM THE FRONT
VII SIC CODES 4-di.it,in order of.nont
A FIRST B SECOND
---tI I I I (spe'cll'))Establishments primarily engaged in manu:acturing 7' 2182111
I$2I1I spfye tEosc tarebsinsm enptlsa spc mrailtye rensg,eda nd nomannwulaccantubg
e
712824 mamae organic fibers, except cellulosoc
elastomers
15 16 - 19 16 16 19
C THIRD D FOURTH
I I I (1p„,fi,) c I I I (specify)
15 16 19 _ 5 16 - 19
VIII OPERATOR INFORMATION
A NAME B Is the name listed in Item
c I I I I I I I 1 I 1 I 1 I I I I 1 1 I 1 I 1 1 I I I I 1 I I I I I I 1 I I I I VIII-A also the Owner'?
g]CNA HOLDINGS LLC - CELANESE SHELBY FACILITY p YES ❑NO
15 16 55 66
C STATUS OF OPERATOR(Enter the appropriate leller into the answer hos if"Other "specify) D PHONE(area axle&no)
F=FEDERAL (specify)
S=STATE M=PUBLIC(other than federal or state) p A (704) 480-5726
P=PRIVATE 0=OTHER(specify)
58 15 6 • 18 119 21 I22 • 26
ff II II ll II E STREET OR P O BOX
$L 2125 ACKSBURG 1209DI I I ' ' l i ( I I I I I I l )
28 55
F CITY OR TOWN G STATE H ZIP CODE IX INDIAN LAND
c I I I I I I I I I 1 1 I 1 1 I I 1 1 I I I I I I 1 I I 1 I Is the facility located on Indian lands'?
B GROVER NC 28073 ❑YES 121 NO
52
15 16 40 41 82 47 - 51
X EXISTING ENVIROMAENTAL11.1111111111111111111 PERMITS
A NPDES(Disc%a es to Surface Fate2) D PSD(Air Emissions from Proposed Sources)
CT I I I I I I I I I I 1 I I CT , I I I I I I I I I I I
9 N NC0004952 9 P
16 16 17 18 30 16 16 17 18 30
B UIC(Under vaund Infection of Fluids) E OTHER(specly)
c r i I ( I I I I 1 1 1 1 I c T l 1 1 1 1 I 1 1 I I (speCif))LAND APPLICATION OF SLUDGE
9 U 9 wt}Oalio3$
15 18 17 18 30 15 16 17 18 30
C RCRA(Hazardous Wastes) E OTHER(speck')
C T I I I 11 I I 11 III I c r I T 1 1 1 1 I I I 11 I l (spec )NPDES STORMWATER PERMIT
IIIi9 R NCD003446721 g NCS000064
15 16 17 18 30 15 16 17 18 30
XI MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries The map must show the outline of the facility,the
location of each of its existing and proposed intake and discharge structures,each of its hazardous waste treatment,storage,or disposal facilities,and each well where it
injects fluids underground Include all springs,rivers,and other surface water bodies in the map area See instructions for precise requirements
XII NATURE OF BUSINESS .rovide a bnef descn.tion
MANUFACTURER OF THERMOPLASTIC AND ELASTOMER POLYESTER RESINS INCLUDING COMPOUNDING OPERATIONS
XIII CERTIFICATION(see instructions)
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that,based on my
inquiry of those persons immediately responsible for obtaining the information contained in the application,I believe that the information is true,accurate,and complete /
am aware that there are significant penalties for submitting false information,including the possibility of fine and imprisonment
A NAME&OFFICIAL TITLE(type in print) B ATURE C DATE SIGNED
NICOLE B COFFEE - DIRECTOR OF
PRODUCTION V-1 0 .--
COMMENTS FOR OFFICIAL USE ONLY
C
IS 16
ss
EPA Form 3510-1(8-90)

From NC0004952 (Celanese Shelby NC) February 2018 NPDES
Permit Renewal Application.
,, Laboratory Report
PRISM Full-Service Analytical a
Environmental Solutions 02/19/2018
iwaon.To*IFS INC
Celanese Project 2018 Permit Renewal Client Sample ID 001 EFF(Comp)
Attn Michael Sparks Prism Sample ID 8010261-01
2525 Blacksburg Road Prism Work Order 8010261
Grover, NC 28073 Sample Matrix Water Time Collected 01/18/18 14 40
Time Submitted 01/18/18 16 45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Fluoride 0 43 mg/L 0 10 0.013 1 '300 0 2/13/18 17 34 EGC P880275
Sulfate 12 mg/L 1.0 0 20 1 '300 0 2/13/18 17 34 EGC P8B0275
General Chemistry Parameters
Total Nitrogen 0.62 mg/L 0 60 0 17 1 'Total Nitrogen 2/1/18 9 42 CLB jCALC]
Nitrate/Nitrite as N BRL mg/L 0 10 0 0024 1 'SM4500-NO3 F 2/1/18 9 42 CLB P8B0002
Phosphorus-Total 0 050 mg/L 0 050 0 011 1 'SM4500-P F 1/26/18 11 12 CLB P8A0352
Total Dissolved Solids 230 mg/L 60 1 4 1 'SM2540 C 1/23/18 14 58 SLS P8A0332
Total Hardness 21 mg/L 0 66 0 052 1 *200 8 1/22/18 19 53 EGC [CALC]
Total Kjeldahl Nitrogen 0 62 mg/L 0 50 0 17 1 *351 2 1/24/18 12 26 CLB P8A0316
Ammonia as N BRL mg/L 0 10 0 0046 1 'SM4500-NH3 G 1/29/18 10 32 CLB P8A0360
Total Metals 1
Aluminum 0 062 mg/L 0 050 0 0086 1 '200 8 1/22/18 19 53 EGC P8A0294
Antimony 0 0053 mg/L 0.0010 0 000030 1 *200 8 1/22/18 19 63 EGC P8A0294
Arsenic BRL mg/L 0 0010 0 000052 1 '200 8 1/22/18 19 53 EGC P8A0294
Beryllium BRL mg/L 0 0010 0 000095 1 '200 8 1/22/18 19 53 EGC P8A0294
Boron BRL mg/L 0 20 0 038 1 '200 8 1/22/18 19 53 EGO P8A0294
Cadmium BRL mg/L 0 0010 0 00015 1 '200 8 1/22/18 19 53 EGC P8A0294
Calcium 5 6 mg/L 0 10 0 010 1 "200 8 1/22/18 19 53 EGC P8A0294
Chromium BRL mg/L 0 0010 0 00017 1 '200 8 1/22118 19 53 EGC P8A0294
Copper BRL mg/L 0 0050 0 00012 1 '200 8 1/22/18 19 53 EGO P8A0294
Iron BRL mg/L 0 10 0 0070 1 '200 8 1/22/18 19 53 EGC P8A0294
Lead BRL mg/L 0 0010 0 00013 1 '200 8 1/22/18 19 53 EGC P8A0294
Magnesium 1 7 mg/L 0 10 0 0066 1 '200 8 1/22/18 19 53 EGC P8A0294
Nickel BRL mg/L 0 0020 0 00012 1 '200 8 1/22/18 19 53 EGC P8A0294
Selenium BRL mg/L 0 0010 0 00029 1 '200 8 1/22/18 19 53 EGC P8A0294
Silver BRL mg/L 0 0010 0 000012 1 *200 8 1/22/18 19 53 EGC P8A0294
Thallium BRL mg/L 0 0010 0 000024 1 '200 8 1/22/18 19 53 EGC P8A0294
Zinc 0 017 mg/L 0 015 0 0012 1 '200 8 1/22/18 19 63 EGC P8A0294
This reportshould not be reproduced,except in its entirety,without the written consent of Prism Laboratories,Inc
P � P
449 Springbrook Road-P 0 Box 240543-Charlotte,NC 28224-0543
Phone [phone]-Toll Free Number 1-800/529-6364-Fax [phone] Page 4 of 45

Attachment C
INVISTA
NPDES PERMIT No. NC0001112 RENEWAL APPLICATION
INVISTA S.A R.L. • WILMINGTON, NC PLANT
October 2014
Prepared by:
COURY -
SCIENCE 8 ENGINEERING PIIC
NC FIRM#P-1120
FOR
INVISTA S.a r.I.
4600 Hwy 421 North
Wilmington, NC 28401

Attachment C
CONTINUED FROM THE FRONT
VII.SIC CODES (4-digit, in order of priority)
A.FIRST • 8.SECOND
2821 (specfi`) UM (specify)
7 1e ITPlastic materials, synthetic resins , 15 1e Industrial Organic Chemicals not
and non vulcanized elastomers elsewhere classified
C.THIRD D.FOURTH
c 4959 (specify) Z (specify)
s ,e 17 Sanitary Services 7 1 1.
VIII.OPERATOR INFORMATION
A.NAME B,Is the name listed In Rem
c INVISTA S.ar.l VIII-A also the owner?
8 0 YES 0 NO
to 19 58
C.STATUS OF OPERATOR(Entangazimmgralkajaljgalhe answer box,'if"Other,"specify.) 0.PHONE jarea code&no.)
F=FEDERAL M=PUBLIC(other than federal orstate) p (specify) C 910 341 5500
S=STATE O=OTHER(specify)
P=PRIVATE Se 15 i 16 18 19 21 22 25
E.STRZIF?R PO BOX
4600 Highway 421 North
F.CITY OR TOWN G.STATE H.ZIP CODE IX.INDIAN LAND
c Wilmington NC 28401 Is the facility located on Indian lands?
B ❑YES Ile NO
15 16 - -----...._ i0 42 3 47 et
X.EXISTING ENVIRONMENTAL PERMITS
A.NPDES(Discharges to Surface Water) D.PSD(Air Emissions from Proposed Sources)
C T ' . NC0001112 c 1 •
9 N 9 P
15 16 17 1e � �- --� 30 15 16 17 to 30
B.UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
C T ' c , 7 * NCS000118 NPDES, Stormwater
9 to 17 18 30 916 17 iQ 30 1
C.RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
9 R ' NCD990734055 9 1 ' 00164T51 Title V Air Quality
15 16 17 to 30 ti 16 17 to 30
Xi. MAP
Attach to this application a topographic map of the area extending to at least one mite beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivets and other surface water bodies in the ma. area. See instructions for precise 6uirements.
XII.NATURE OF BUSINESS(provide a brief descri p ion
Principal Products of INVISTA S.ar.!Wilmington
The INVISTA, Wilmington facility manufactures a number of polyester polyols products which are chemical
intermediates used in the production of polyurethane foams used for commercial and residential insulation.
XIiI.CERTIFICATION(see instructions
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information,including the possibil' of fine a imprisonment.
A.NAME&OFFICIAL TITLE(type or print) B : • 1'- 1 C DATE SIGNED
Richard Bayless, Site Manager 4 R to/A, 14
COMMENTS FOR OFFICIAL USE ONLY
c
15 16 551 ____ -
EPA FORM 3510-1(8-90)

• From NC0001112 (Invista Wilmington, NC) October
12014 NPDES Permit Renewal Application. 1 0
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy/nee Item I of Form 1)
on separate sheets(use the same format)instead of completing these pages. NCD 9 9 0 7 3 4 0 S 5
SEE INSTRUCTIONS.
OUTFALL NO
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (.rpee -if blank) Corinna)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (riarmlahlr) (rJas'ailahlr) AVERAGE VALUE
(1) II) d,NO.OF a.CONCEN- (1) b.NO.OF
1.POLLUTANT
CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b,MASS CONCENTRATION (2)MASS ANALYSES
a,Biochemical Oxygen 39 85.9 6.6 14.5 1.94 4.5 249 mg/L lb/day
Demand(HOI1)
6.Chemical Oxygen 20.1 1 35.2 m 2 1 /L lb/day(Mori) g
c Total Organic Carbon 4.02 7.04 1 mg/L lb/day x) g
d.Total Suspended
Solids(MS) 34.9 101.3 9.8 29.0 7.0 16.4 248 mg/L lb/day
e.Ammonia(asM 0.13 0.314 1 mg/L lb/day
VALUE VALUE VALUE VALUE
t.Flow 0.619 0.404 0.294 365 MGD
g.Temperature VALUE VALUE VALUE VALUE
(winter) 35 30.9 25.5 129 'C
h.Temperature VALUE VALUE VALUE VALUE
(summer) 35.6 32.7 30.8 135 'C
MINIMUM MAXIMUM MINIMUM MAXIMUM
i.pH 7.7 8.9 8.2 8.5 264 STANDARD UNITS
PART 8- Mark*X'in column 2-a for each pollutant you know or have reason to believe is present Mark'X`in column 2-b for each pollutant you believe to be absent If you mark column 2a for any pollutant which is limited either
directly. Co indirectly but expressly, in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a.you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(opnonal)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG,VALUE a.LONG TERM AVERAGE
AND a b a.MAXIMUM DAILY VALUE ({farYulohlr) (if available) VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- Ill b.NO.OF
(r/available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide /
(24959-67.9) /� _ _
b.Chlorine.Tote! X 6.75 0.016 1 ug/L lb/d
Residual
c.Color X 15 N/A 1 PCU N/A
d.Fecal Cdiform 1.78 N/A 1 cl/100mLy N/A
_ -e.Fluoride v
(16984-48-8) ^ 0.0965 0.17 1 mg/L lb/d
t tVitratrNtrta 38.7 103.28 13.0 31.9 10 mg/L lb/d
(as M
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

I I From NC0001112 (Invista Wilmington, NC) October
Attac C 2014 NPDES Permit Renewal Application.
ITEM V-B CONTINUED FROM FRONT
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a b. a.MAXIMUM DAILY VALUE (ifavailable) (ifava+lahle) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (i) b.NO.OF
(I/available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION - (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen.
Total Organic(as X 0.673 1.62 1 mg/L lb/d
M
Gram s Oil e d X 1.61 1.34 1 mg/L lb/d
I.Phosphorus
(as P),Total X 7.61 19.6 3.12 8.08 12 mg/L lb/d
(7723-14-0)
J.Radioactivity \ /
(1)Alpha,Total X
(2)Beta,Total X
(3)Radium. \/
Total �\
(4)Radium 228,
Total
k.Sulfate
(a.SO,) X
(14808-798)
I.Sulfide X(a*SI
m.Sulfite
(m S0} X ND
1
(14285 45 3)
n.Surfactants X ND 1
o.AfurNnun.
TOE X 65.2 0.11 1 ug/L lb/d
(7429-90-5)
p.Barium,Total
(7440-39-3) X 4.41 0.007 1 ug/L lb/d
q.(7440-Boro
n,
Total) X 31.5 0.055 1 ug/L lb/d
(7440-
r.
(2C 4)) X 229 0.401 1 ug/L lb/d
a.Iron,Total X
(7439-89-8) ND 1
L Magnesium. ,
To ) X 1130 1.98 1 ug/L lb/d
u.Molybdenum. - .
TOE X 23.7 0.04 1 ug/L lb/d
(7439-98-7)
v.Manganese,
Total
(7439965) X 33.6 0.06 1 ug/L lb/d
w.Tin,Total X
(7440-31-5) ND 1
x.Titanium,
Total X ND 1
(7440-32-6) �\
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

Excerpt from 2017 Annual Groundwater Report
Attachment D
2017 ANNUAL GROUNDWATER REPORT
FOR
DURAFIBER TECHNOLOGIES
SALISBURY, NORTH CAROLINA
CNA HOLDINGS LLC
Prepared for:
CNA Holdings LLC
222 W. Las Colinas Blvd.
Suite 900 North
Irving, Texas 75039
Prepared by:
AECOM
1360 Peachtree Street NE, Suite 500
Atlanta, Georgia 30309
February 13, 2018
Project No. 60313948

Attachment D
2017 Annual Groundwater Report
DuraFiber Technologies—Salisbury, NC
CNA Holdings LLC
Project No. 60313948
1.0 INTRODUCTION
On October 4, 2000, CNA Holdings LLC (CNA, formerly Hoechst Celanese Corporation) entered into a
Final Administrative Order on Consent (Consent Order) with the U.S. Environmental Protection Agency
(EPA) Region IV office in Atlanta, Georgia, for the DuraFiber Technologies* (formerly known as
KoSa/Hoechst Celanese/FII) in Salisbury, North Carolina. This Consent Order directed that CNA submit
annual groundwater reports summarizing the data collected during the previous year's site monitoring
activities. This report summarizes data collected during 2017. This corresponds to the period since the
last annual status report was issued in February 2017.
Two groundwater extraction systems were active at the site through late 2004. The source-area
groundwater collection systems included twelve groundwater extraction wells near the former glycol
recovery unit bottoms (GRUB) landfill, two groundwater extraction wells at the former chromate reduction
unit (CRU) basins, and three groundwater extraction wells in the DowTherm Heaters Area. The perimeter
containment system was comprised of 43 extraction wells along the eastern and northern property
boundaries.
On September 27, 2004, the EPA approved recommendations to cease extraction activities from the
GRUB, CRU, and perimeter extraction systems. The approved systems were shut down between
October 27 and November 2, 2004.
In 2007, the EPA approved a transition to an annual monitoring program for the facility. Annual sampling
events have been completed in October of each year.
During this reporting period, potentiometric and groundwater quality data were collected in October 2017.
Figure 1 presents the wells and other sample points that comprise the 2017 monitoring scheme for the
site. Sampling and analytical results are presented in further detail in Section 3.
*ln the fall of 2017, DuraFiber Technologies closed the facility and filed for chapter 7 bankruptcy.
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Attachment D
2017 Annual Groundwater Report
DuraFiber Technologies—Salisbury, NC
CNA Holdings LLC
Project No. 60313948
2.0 GROUNDWATER EXTRACTION SYSTEM SUMMARY
A DowTherm ATM extraction system was historically operated at the facility. The system was not
operational during an inspection completed in January 2011. The system had not produced any
measureable quantity of separable phase material during the operational period. In addition, the
DowTherm ATM concentrations in samples from this location were below detection limits in the samples
collected from 2008 through 2010. The results of<0.010 milligrams per liter (mg/L), compared to a high
concentration of 1,080 mg/L (diphenyl ether, July 2002) demonstrate the decline in DowTherm ATM
presence at this former extraction location. Therefore, the system was not returned to service. The
downgradient DowTherm ATM plume has remained stable to declining. Therefore, the extraction system
remains inactive, and the plume will continue to be monitored. Additional activity will be recommended if
future data suggests changes are needed.
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