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Home My WebLink AboutWQ0034806_Residual Annual Report 2018_20190218INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0034806 SUBMITTAL DATED: 2/18/2019 Project Contact Information Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Martin Mabe Email Address* Phone Number* martin@Wllcomabesoil.com 3363121396 Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0034806 Reviewer* Troy Doby Pe rmittee * Wesley Wooten Facility Name * Coastal Farms and Residuals, LLC County* Pender r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. 2018 Annual Report Please attach all information required or requested for this submittal to be review here. Coastal Farms 2018 Annual Report (NCDEQ).pdf 8MB Application Form Engineering Aans, Specifications, Calculations, @c.) For nein and modification permit applications, the paper copy is required to be subrrutted to the Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic applications have been received_ The paper copy shall include the follo-kAmig: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineenng plan sets • 1 extra set of specifications (in addition to the set of specifications provided in the attachments) • Fee (if required) This shall be mailed to the following address: By U_S_ Postal Service: Division of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigb_ NC 27699-1613 By CourieriSpecial Delivery: Division of Water Resources- Non -Discharge Branch Ag Nathaniel Thornburg- 9th Floor, Office #942WN 512 N_ Salisbury St_ Raleigh,NC 27604 For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov. * I;W By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Sign Submission Date 2/18/2019 2018 ANNUAL REPORT LAND APPLICATION PROGRAM COASTAL FARMS AND RESIDUALS, LLC PERMIT #WQ0034806 Prepared For: Coastal Farms and Residuals, LLC 8155 Malpass Corner Road Currie, North Carolina 28435 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 February 2019 willcox&mabe SOIL SOLUTIONS February 18, 2019 NCDEQ-DWR Non -Discharge Compliance Unit 512 North Salisbury Street 9" Floor Office# 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Compliance Unit Reference: 2017 LAND APPLICATION ANNUAL REPORT Coastal Farms and Residuals, LLC Permit No. WQ0034806 WMSS Project No. 15-19 Ph:01 Non -Discharge Compliance Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Coastal Farms and Residuals, LLC. WMSS compiled this report using data gathered during the compliance year by Coastal Farms and Residuals, LLC. This data includes: 1) certification form, 2) residuals analyses and pathogen 1 vector data, 3) application summaries and field loading rate reports, 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact Coastal Farms and Residuals, LLC or WMSS for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe NC Land Application/Residuals Operator #22753 Enclosures SharedlWMSS Projects12015115-19 Coastal Residuals12018 Annual Report12018 ANNUAL REPORT - COASTAL FARMS.doc Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willooxmabesoil.com TABLE OF CONTENTS SECTION NO. TITLE Certification Form 11 Residuals Analyses & Pathogen / Vector Attraction Data III 2018 Application Summary and Field Loading Rate Reports 1V Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: W00034806 County: Pender Year: 2018 Facility Name (as shown on permit): Coastal Farms and Residuals, LLC Land Application Operator: Mr. Weslev Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? E1 Yes L] No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the ermit: 12 Total number of fields utilized for land application during the yearF 1 Total amount of dry tons applied during the year for all application sites: 390.19 Total number of acres utilized for land application during the year: 93.4 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 21 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .l 105(a) or the Pollutant Loading Rates in 15A NCAC 021'. 1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.."/ Mr. Wesley W000ten, President (/ 2/7/19 Permittee Name and Title (type or print) Signature/31' Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1 102 (26) DENR FORM ACF (12/2006) RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION I p 0 O 0 O V N 0 0 0 0 0 0 0 o p 0 0 o 0 o p 0 0 oimom`. oim oiONnM oO 0 0 0 0 O O O O O O p O 0 0 0 0 0 0 0 0 CrY (rY N M� M N M m r_ M O O N O O O O O 0 0 0 O 0 p 0 O 0 O � N of CJ r � N o p 0 0 0 0 0 O 0 0 O 0 O 0 moi ;o m �j� oirno om pN N N i N 0 "074640--o. 0 p o 0 o V M ono 0 .'�nnr 0 n n o n 0 0 0 O o 0 0 0 00 0 ion �joN�o N 0 p 0 p o 9000 m o o m m m 00606 Oi O1 N p 0] m W V n W p o 0 oM 0 0 0 m�m�mm$d0o�?o M � M V v 0 v E z $ o y E n v E g x v c Y Z O m U U o M Elm E Z F Q I COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 26, 2018 Avendale W WTP 3.85 % Solids 6.88 PH Permit No. WQ0030775 Parameter °lo Mg/Kg Dry Weight % X 1-0,000 Pounds/Dry 141 Kix 0.002L" Nitrogen (TKN) 3.700 37,000.000 74.000 Phos horns 4.310 43,100.000 86.200 Potassium 0.007 72.200 0.144 PAN (injected)* 1.118 11,176.720 22.353 PAN (surface)* 1.118 11,175.420 22.351 Ammonia Nitrogen 0.000 2.600 0.005 Calcium 0.042 423.000 0.846 Calcium Carbonate Eq. --- --- --- Ma nesium --- 44.400 0.089 Sodium --- 214.000 0.428 --- Nitrate N/ Nitrite --- 74.900 0.150 Barium Chloride - - --- ------ --- --- SAR 0.52 - Iron Ceiling Concen.� Aluminum --- 12,500.00 25.000 M K Arsenic 22.30 0.045 75 Cadmium --- 11.80 0.024 8.5 Chromium --- 40.000 0.080 --- Copper 553.00 1.106 4,300 Lead --- 18.90 0.038 840 Mercury 0.416 0.001 57 Molybdenum 11.80 0.024 75 Nickel 29.60 0.059 420 Selenium 1.80 0.024 100 'Linc --- 1,180.00 2.360 7,500 Environmental Chemists 9 2018-19448 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. 9 -EnvironmentalChemists, Inca �4 I (60'_ 41'in�ln4 P "1ay, bViLnti It ton N< 'S 4(1� , 910.3'r2-0223 .1 3, 970392.4421 Y'ax b ... 710 BO\%so town hcad, :v4ant o, NC. 217 51 �'" -_4%?. ), 121- Lib ax rt e 255-A Wilnurl,",fon Iii ll a�', Tad,som ille, AC -26540 n 9 1 347.5843 I_ab%Fax ANALYTICAL & CONSULTING CHEMISTS info a-ellvironmentslc-1lemisu.con. Lewis Farms & Liquid Waste, INC. Date of Report: Dec 18, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2018-19448 WO -1-0 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-49213 Site: Sludge 11/26/2018 2:00 PM Solid/Sludge Client Test _ Method _ Results Date Analyzed Sludge Residuals Aluminum EPA 2003 12500 mg/kg 12/04/2018 Arsenic EPA 2007 22.3 mg/kg 12/07/2018 Cadmium EPA 2007 <11.8mg/kg 12/07/2018 Calcium EPA 200.7 423mg/kq 11/29/2018 Chromium EPA 2007 40.0 mg/kg 12/07/2018 Copper EPA 200 7 553 mq/kq 12/07/2018 Lead EPA 200 7 18.9 mg/kg 12/07/2018 Magnesium EPA 2007 44.4 mg/kg 11/29/201II Molybdenum EPA 200.7 <11.8mg/kg 12/09/2018 Nickel EPA 200.7 29.6 mg/kg 12/07/2018 Potassium EPA 200.7 72.2 mg/kg 11/29/2018 Selenium EPA 2003 <11.8 mg/kg 12/07/2018 Sodium EPA 2007 214 mg/kg 11/29/2018 Zinc EPA 200.7 1180 mg/kg 12/02/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 74.9 mg/kg 12/17/2018 Total Solids (%) SM 2540 B 3,85% 11/27/2018 pH SM 4500 H 6 6.88 units 11/28/2018 Ammonia Nitrogen SM 4500 NH3 C <2.60 mg/kg 11/30/2018 Total Kleldahl Nitrogen (TKN) SM 45000rgB 37000 mg/kg 11/30/2018 Total Phosphorus SM 4500 P F 43100 mg/kg 12/12/2018 Mercury SW84674718 <0.416 mg/kg 12/02/2018 Report U- <^016-19448 Page I o13 Environmental Chemists, Ine. 4W. Ail Gnsulnrlll �° VJiu1m tot NC SIO 311 i)JL _o(� ll13 tl_i i-ax 710 br er town i4o...i, Mina u, N( 272 ? 2.47 , )2 Lab /tax 271,F A W'-h ulgton Hip htra�, Jack n:n ltc, N(285.10 - 91'( 3175843 Lal Ta.x ANALYTICAL-& CONSULTING CHEMISTS irfoii�o�'nironmen lalr:htmi8t>.ccm Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Date of Report: Dec 18, 2018 Customer PC #: Customer ID: 14020008 Report #: 2018-19448 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-49214 Site: 1 11/26/2018 2:10 PM Solid/Sludge Client Test _ Method i ` Results Date Analyzed Total Solids (%) SM2540G 4,22% 11/27/2018 Fecal Density SM 9221C E MPN 24 hr 503 <43 MPN/g 11/27/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-49215 Site: 2 11/26/2018 2:12 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM2540G 4.21 % 11/27/2018 Fecal Density W SM 9221C E MPN wµ �� 24 hr 503 <43 MPN/g 11/27/2018 Lab ID Sample ID Collect Date/Time Collect Date/Time Matrix Sampled by 18-49216 Site: 3 11/26/2018 2:18 PM 11/26/2018 2:14 PM Solid/Sludge Client Test Method Results Analyzed Results Date Analyzed _ _ TDate Total Solids (%) Total Solids (%) SM 2540 G 4.26 % 11/27/2018 4.12% 11127/2018 Fecal Density SM 92210 E MPN 24 hr 503 <44 MPN1g 11/27/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-49217 Site: 4 11/26/2018 2:16 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 4.36 % 11/27/2018 Fecal Density SM 92210 E MPN 24 hr 503 <42 MPN/g 11/27/2018 Lab ID Sample ID: Collect Date/Time _ Matrix Sampled by 18-49218 Site: 5 11/26/2018 2:18 PM Solid/Sludge Client Test _ Method Results Analyzed _ _ TDate Total Solids (%) SM 2540 G 4.26 % 11/27/2018 Fecal Density SM 9221 C E MPN 24 hr 603 <43MPN/g 11/27/2018 ftepor, u, 20,6 194d8 Page 2 o!3 ANALYTICAL R_ CONSMING CHEM IS rS Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Lab ID Sample ID: 18-49219 Site:6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 18-49220 Site:7 Test Environmental Chemists, Inc. 004 4ViednuL 1111-, Wilmmt ion, NC 28105910.392.0223 11t 910392,442-f [=.a 710Lnn-eitown hold, Manz o,x.(:279 d 152_473� ()3LaL/7av 25b A Min Iirgton t flghmay, Jack-,onville, N( ;;540 - 910 X175843 i rli+ aeemiromnen i 0!chemistssom Date of Report: Dec 18, 2018 Customer PO #: Customer ID: 14020008 Report#: 2018-19448 Project ID: sludge Collect Date/Time Matrix Sampled by 11/26/2018 2:20 PM Solid/Sludge Client Method Results Date Analvzed SM 2540 G SM 92210 E MPN 24 h, 503 Method Collect Date/Time 11/26/2018 2:22 PM 4.19% 11/27/2018 <43 MPN/g 11/27/2018 Matrix Solid/Sludge Results Sampled by Client Date Total Solids (%) SM2e40G 4,04% 11/27/2018 Fecal Density^ SM 92210 E WIN 24 hr 503 <45 MPN/g 11/27/2018 Comment: Sludge residuals, except pH, reported on a dry weight basis pH reported on an as received basis. Reviewed by: Repo,i Y: 2018-19448 Payc 3 of 3 `_J H� ZQ W U o Zz Z W r. i C� 1 � a 3 u, J T � a s tl � tl3H10 f Z OIHl �� •... �T QHOVN CCfONH a Q W N ' ' W 40SZH � d I SOH `S OI evl P`y- er yr �� Vr �y-• 4' I/6w aupol4D Ci (D j° ° a a c� a 7 a o a a c� a c� �ouleWop qe,U t)(,DD jo V C7 U U' U U` U C7 U C7 U (.`3 U 0 ailsodwoo ad6y oldweg a fd E d F- a cr o c a + ~ O U a O ` U t0 � I E m I U7 r^ N f i ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Faeility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTP Name: Avendale WWTP NPDES Number: W00030775 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T.1 106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tem) ❑ Alt B (Alk Tieaunent) p Alt. C (Pr or Testing) p A1t.D (No Prior Test) ❑ Process to Purther Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce. Pathogens": Compost C] Heat Drying p Heal Treatme t p Themro hilic EJ Beta Ra ❑ Gamma Ra p Pasteurization p Class B: Ait. (1) Fecal Density U Alt. (2) Process to Significantly Reduce Pathe ens p If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"; Lime Stabilization [] Air Dryin ❑ Corn rastin . ❑ Aerobic Digestion p Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the fo]lowing monitoring data: Parameter' Allowable Level in Sludge Pathogen Density LTCCe- um cr o nnCesof Frequency Analysis Sample TYPe cal nay 'Fech. ninue jMinimuHGeo. Mean Maximum Units Fecal Coliform 2 s 10 to the 6th power PC) gram of total solids MPN 42 43 45 MPN/g 0 Annual Grab sM9221Ce: CFU 1000 mpn per gram oftotaisolid (dry Weight) Sahnonella bacteria (in lieu of fecal coliform) 3 MPN per,igrams total solid (dry weight) vector Attraction 1Geaucuo]I (ADA INI-At: UZI .1luv) - Yicase indicate alternative pertormea: Alt.I (VS reduction) J Alt. 2 (40 -day bench) p I All, 3 (30 -day bench) ❑ Alt. 4 (Spec 02 uptake) Alt 5 (14 -Day Aerobic) [] Alt. 6 (Alk. Stabilization ❑ Ah 7 (Drying - Stable) ❑ Alt. 8 (llrying -Unstable) ❑ Alt, 9 (injection) (J Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed p CERTIFICATION STATEMENT (please check the appropriate statement) U "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement fit 15A NCAC 02T.1107 have been met,' * "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel property gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kirklyn Fields, ORC Wesley Wooten, President Prep rer Name/and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 2/12/19, Signatt e of Prepares-* Date Signature of Land A tier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Avendale WWTP Date Fecal Coliform MPN per gram Log 11/26/18 43 1.6335 11/26/18 43 1.6335 11/26/18 44 1.6435 11/26/18 42 1.6232 11/26/1843 1.6335 11/26/18 43 1.6335 11/26/18 45 1.6532 Total 11.4538 Average 1.6363 Geometric Mean 43 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 10, 2018 _Carolina Beach WWTP Pe•mit No. NC0023256 2.83 % Solids 7.29 pit ' Parameter .. W ? Mg/KgDry Weight t°lua3o,000 Pounds/DttyTon (M /K x9.002.. Nitrogen (T)<N) 7,440 74.400 000 _ 148.800 _ rhos >honls 1.180 11.800.000_ 23.600 Potassium 0.196 1,960.000 3.920 PAN injected)* 2.794 27938.000 55.876 PAN (surface)* 2.405 _ 24-048.000 48.096 Ammonia Nitrogen _ 0.778 7,780.000 15.560 Calcium 3.530 35.300.000 _ 70-600 Calcium Carbonate 13c . - -- MiM�csiam 3.820.000 7.640 Sodium 51160.000 10.320 N in ate teN -- - ------- 172.000 - --0.344 _ _N/Niifi Barium -- i SAR Chloride --- -.- .._ -._1.L'7_.:,-_. hon --- --- --- Ceiling. Concent. Alumin..... 4,030.00 8.060 '`M K Ai:senic __---- - 19.90 0.040 ------75----- Cadmium --- 19.90 0.040 85 Chromium ...- 21.300 0.043 --- (,(Mel __.----- 647.00 L294 4,300 Lead -- - 28.80 _ _ 0.058 - _ 840 Muctliv _ -`- 0.742 ().001 57 Molybdenum -- 19.90 _ 0.040 75 Nickel 19.90 420 Sclunium----- --_-_ 19.90 _0.040 0.040 _ v. 100 7.inc _-_--' -. 947.00 1.894 L_ 7,500 _ linvinvunmrtal Owmisi. it 2018-05592 ^Defermination of Plant Available Nitrogen (PAN): injected Application: (Mincraliration. Rate)( I KN -Ammonia N) + Ammonia N -1 Ninale N i Niuite N -% PAN Surltwe Application: (Mineralization kwe)('I'KN-Ammonia N) i (0.5)(Anvnoma N) f Nim oe N i Mititc N = `7o PAN -Note: Con.stit tic if is K. 1). (Not Detected) ora tic lection limits are listed as detection limits for c:dcolation purposes. Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten F�nvir®nmental Chemists, Inc, ('002 4V'indrnill VVahS "Vi lnlin/;ton, NC 2F..105 < 1)10 3`)2.022:5 Lab , 910392.4174 Fat 71013olwriertowo Road, Mantco, NC271;9 + 2'i2.-173.5702 Lob/Pas 'di'i-A Wi Imilhcgtrin I Inm01'. Jacksonvi l lc, NC 28'i I0 o 910 17.57,8431.;115/ 6az iIt iy"' 11% is 1116 It t91P h ol1'1'.Con1 Date of Report: May 03, 2018 Customer PD #: Customer ID: 14020008 Report #: 2018-05592 Project ID: Carolina Beach WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13860 Site: Sludge 4/10/2018 12:00 PM Solid/Sludge wesley Wooten Test SW 846 Method 8081B13510 Method Results Date Chlordane SW846 Method 80618/3510 <0.03 mg/L 04/19/2018 Endrin SW 646 Method 80818/3510 <0.0005mg/1- 04/19/2018 Heptachlor SW 846 Method 8081B13510 <0.0005mq/L 04/19/2018 Heptachlor epoxide SW846 Method 6081B/3510 <0.0005 mg/L 04/19/2018 Lindane SW 846 Method 80816/3510 <0.0005 mq/L 04/19/2018 Methoxychlor SW646Method BOB 1B/3510 <0.0005mg/L 04/19/2018 Toxaphene SW 846 Whoo 8081 B/3510 <0.05 mg/L 04/19/2018 1,4-Dichlorobenzene(TCLP) SW 846nle1hod8270/3510 <0.050mg/L 04/13/2018 2,4,5-T rich lorophenol(FCLP) $A' 846 method 8270/3510 <0.050mg/L 04/13/2018 2,4,6 -Trichlorophenol (TCLP) SW 840 method 8270/3510 <0.0.50 mg/L 04/13/2018 2,4-Dinitrotoluene (TCLP) SW 840 net hod 8270/3510 <0.050 mg/L 04/13/2018 Cresol(1-CLP) Sw846mothod8270/3610 <0.050mg/L 04/13/2018 Hexachloro-1,3-butadiene(TCLP) SW84r>„lemod8270/3610 <0.050mg/L. 04/13/2018 Hexachlorobenzene(TCLP) SW 846 method8270133tU <0.050mg/1- 04/13/2018 Hexachloroethane(TCLP) SW 846 Method 827013510 <0.050mg/L 04/13/2018 m + p -Cresol (TCLP) SW 846 method 8270/3310 <0.050 rnq/L 04/13/2018 Nitrobenzene (TCLP) SW 846 method 8270/35/0 <0.050 mg/L 04/13/2018 o-Cresol(TCLP) SW 846 method 8270/3510 <0.050mg/L 04/13/2018 Pentachlorophenol (TCLP) SW 846 nlethod8270/3510 <0.250 mg/L 04/13/2018 Pyridine (TCLP) SW 846 metlod827013510 <0.050 mg/L 04/13/2018 2,4,5-1-P SW846 Method8151A <0.003mg/l- 04/17/2018 2,4-0 SW846 fslLslod 8161A <0.003mg/L 04/17/2018 1,1-Dichloroethylene SkV846Method 8280/5030 <0.01 mg/L 04/30/2018 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 04/30/2018 Benzene SW846 Method 8260/5030 <0.01 mg/L 04/30/2018 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 rf 04/30/2018 R-1111 11 mu a nresn RCI Cyanide Environmental Chemists, Inc® 4/16/2018 Sulfide SM 4500 s D 1.49 mg/kg 04/1612018 Ignitability SW 846 method 1010 . t NO' I'Vin, l Im 11 bVay. Wil In inghm, !VC- > :U)b > 9111 02,022;3 L.ib - 9 10 39-1 11 2.7. 'Fax SW 846 Method 0045D 7.29 units 04/24/2018 Sludge Residuals 710 13nwsor town N( Id, "vLmI o, N'(' 279 I 151A73.570' 0h IFax Aluminum EPA 200 7 4030 mg/kg �. ". Y�',-;A W1 111ingiPi1 I1 IttMdV, 1dcI.som III(', Nr(. 28'i 10 0 91 ).417.,8 !3 I ;,I)F.iS ANALYTICAL & CONSt1LnNG CHEMISTS iuiola cncI on:ncn lal<hcmisa.oau Cadmium Lewis Farms & Liquid Waste, INC. Date of Report: May 03, 2018 <19,9mg/kg 8155 Malpass Corner Road Customer PO #: EPA 2003 Currie NC 28435 Customer ID: 14020008 Chromium Attention: Wesley Wooten Report #: 2018-05592 04/17/2018 Copper Project ID: Carolina Beach WWTP 647 mg/kg Chlorobenzene SW846Method 8260/5030 <0.01mg/L 04/30/2018 Chloroform SW846 Method 8 2 6 015 0 30 <0.01 mg/l- 04/30/2018 Methyl ethyl ketone SW846 Melhod 826015030 <0.05 mg/L 04/30/2018 Tetrachloroethylene SW846Method 826016030 <0.01 mg/L 04/30/2018 Trichloroethylene SW846 Method 826015030 <0.01 mg/L 04/30/2018 Vinyl Chloride SW846Method 826015030 <0.01 mg/L 04/30/2018 RCI Cyanide EPA 335.4 <0.05 mq/kg 4/16/2018 Sulfide SM 4500 s D 1.49 mg/kg 04/1612018 Ignitability SW 846 method 1010 >212 °F 04/24/2018 pH SW 846 Method 0045D 7.29 units 04/24/2018 Sludge Residuals Aluminum EPA 200 7 4030 mg/kg 04/17/2018 Arsenic CPA 20U <19.9mg/kg 04/17/2018 Cadmium EPA 200.7 <19,9mg/kg 04117/2018 Calcium EPA 2003 35300 mg/kg 04/16/2018 Chromium EPA 2003 21.3 mg/kg 04/17/2018 Copper EPA 2003 647 mg/kg 04/17/2018 Lead EPA 200 ? 28.8 mg/kg 04/17/2018 Magnesium EPA 2007 3820 mg/kg 04/16/2018 Molybdenum EPA 2007 <19.9mg/kg 04/17/2018 Nickel EPA 200.7 <19.9tnq/kq 04/17/2018 Potassium EPA 2007 1960 mg/kg 04/16/2018 Selenium EPA 2003 <19.9mg/kq 04/17/2018 Sodium EPA 200.7 5160 mg/kg 04/16/2018 Zinc EPA 200 7 947 mg/kg 04/17/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 172mg1kg 04/20/2018 Total Solids M SM 2540 a 2.83% 04112/2018 Ammonia Nitrogen SM 4600NH3 C 7780 mg/kg 04123/2018 Total Kjeldahl Nitrogen (TKN) SM 4500 c15 n 74400 mg/kg 04/23/2018 1AN Environmental. Chemists, Inc. Q9 ' G4U21NinJu1i111\1v, 4V`i6uii ui1,AK °1}17 , 9 9�02:4I il '1039140?d 1=,1\ 7101311Nacrtul-ut !.old, :AInnlco, NV 279,1 2.2:17 iO)Lat�/laa .i. +� ?i'i-7A 4V'ilntingmn I-liellw q,lackanm-ill",1MC. 2H5.{p _ 1)10.3-17""943 k1l), Pats ANALYTICAL & CONSULTING CHEMISTS inihr,oan� iroumar l;de6,misiacom Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Total Phosphorus Mercury TCLP Metals Arsenic Barium Cadmium Chromium Lead Selenium Silver Mercury Date of Report: May 03, 2018 Customer PC #: Customer ID: 14020008 Report #: 2018-05592 Project ID: Carolina Beach WWTP sM 4500 P F 11800 mg/kg 04/25/2018 Sw840 74718 <0.742 mg/kg 04/22/2018 EPA 200.7 <1.0 mg/l. 04/20/2018 EPA 200.7 <1.0 mg/L 04/20/2018 EPA 200 7 <1.0 mg/L 04/20/2018 EPA20o.7 <1.0mg/L 04/20/2018 EPA 200 7 <1.0 mg/L 04/20/2018 EPA 200.7 <1.0 mg/L 04/20/2018 EPA 200.7 <1.0 mg/L 04/20/2018 EPA 245.7 <0.0020 mg/L 04/19/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13861 Site: 1 4/10/2018 12:05 PM Solid/Sludge Wesley wooten Test Method Results Date Analyzed Total Solids (%) SM2540G 3.01 % 04/12/2018 Fecal Density SM 92210 E MPN 24 m 503 116280 MPN/g 04/11/2018 Lab ID Sample ID: 18-13863 Site: 2 Test _ Method Collect Date/Time 4/10/2018 12:07 PM Matrix Solid/Sludge Results Sampled by wesiey wooten Date Analyzed Total Solids (%) sM2540G _— 3.01 % 04/12/2018 Fecal Density SM 922 CE MPN 24 hr 503 36545MPNlg 04/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13864 Site:3 4/10/2018 12:09 PM Solid/Sludge wesley woolen Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.01 % 04/12/2018 Fecal Density SM 9221C E WIN 24 hr 503 56479 MPN/g 04/11/2018 Environmental Chernists, Inc. E ul0_> Windmill 4Va VVi1nrzi};1<n, N(?Sd05 910.392.022; L.,ib 9i0.:ip�.h42d Pu,. x 7!i)13mv se no ba n R 274 1 252..0%�_i702La1,/1:an 2i5..AWil tm';3un l ii,hw"'l Ia<ksoncillc, M' 28i40 o 1i10.i!'..44:11-a I,�/'Pas ANALYTICAL & CONSULTING CHEMISTS inru(n cm irorrotnt;uchcmi:u x.caw Lewis Farms & Liquid Waste, INC. Date of Report: May 03, 2018 8155 Malpass Corner Road Customer PO #: 27336 MPN/g 04/11/2018 Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2018-05592 Test Project ID: Carolina Beach WWTP lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13865 Site: 4 4/10/2018 12:11 PM Solid/Sludge Wesley Wooten Test Method Results pate Total Solids (%) SM 2,540 c 2.89% 04/12/2018 Fecal Density _SMg22C@MPN 24 hr 503 27336 MPN/g 04/11/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-13866 Site: 5 4/10/2018 12:13 PM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) sM 2640 c 2,88% 04/12/2018 Fecal Density _ sM 0221c E. MPN 2111), 503 45139 MPN/g 04/11/2018 Lab ID Sample ID: — Collect Date/Time M _ Y Matrix Sampled by 18-13867 Site: 6 4/10/2018 12:15 PM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) sM2540c 3,01% 04/12/2018 Fecal Density sM922IceMPN 24 fir50: 116280 MPN/g 04/11/2018 Lab ID Sample ID: Collect Date/Time — _. _._. Matrix Sampled by 18-13868 Site: 7 4/10/2018 12:17 PM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) SM 25040 G 2.99% 04/12/2018 Fecal Density SM 92210 e MPN 24 h, 503 43479 MPN/g 04/11/2018 Comment: Sludge rresiduais( reported on a dry weight basis Reviewed by _._i_y�.A.s2 f1,.....__� (--------- P"'-1 11. 11": 11 ..00 �Ny N W � a N Z M E U •L o d � ^•/ O Z Y rnO1 m U ' C O rn c0 1 U 0 Z d o Uw g Z Z w Q Z N - a j F u i , UU N r CC O v f � d o c � W v Ui o a E E w0 b w=_ 0 r w O z p `_J rn FFR c p cn a W U •L � O Z m ' C O rn c0 1 U 0 Z d o Uw g Z Z w Q Z p - a j F u i U Lm UU Q r CC O v f d mm = W ww• O rn c0 Ui o a E E m w p H ~ H FU) -o 0 0 ? a Y a U c c c c c c c rn n D O p 0 C) O o E r Ll LL LL LL LL LL tL HaH>o 11 11 Z OINl X X X X X X X y 'y HOVN U > i X CONN w WCOSZH _ Q CL 'ION » 3 3NON X 01 av i I/&w 5 • oupomo 0� I i m p (� ,o a) ) • p. C7 a C7 0- C7 0- C7 a. 0 0- C7 a c7 0- 0, 7 0- C7 ,(910 i 9ui'J 10 v <i �: 00 U U 0 U( U 0 U 0 aV!sodwoo adA1 aldwoS T CL � E r N C 7 o 4 cc 'o L U M � c .I o U I I C w J W v c ' 1 N ? C1 r 0. i N < (n N Co d' In (D n N F ANNUAL PATHOGEN AND VECTOR A' FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTPName: Carolina Beach WWTP NPDESNumber: NCO023256 Monitoring Period: From 1/1/2018 To 1 12/31/2018 PathoPen Reduction t15A NCAC 02T.1 166) - Please indirate levei achieved and alternative nerfnrined: Class A: Alt. A (time/temp) ❑ All B (Alk Treatntent)p I All. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathe en s ❑ If applicable to alternative performed (Glass A only) Indicate "Process fp Further Reduce Pathogens": Compost ❑ Heat Dryiug ❑ Meat Treattneut [7 1'henno hike ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization rl Class B: Alt. (1) Fecal Density p Alt. (2) Process to Sigifiricantly Reduce Pathogens ❑ If applicable to aiternatlye performed (Class Baily) Indicate "Process to St nIficantly Reduce Pathogens": Lime Stabilization ❑ Air Dr iin= ❑ Coni ostia ❑ Aerobic Di cstion ❑ Anaerobic Digestion 0 If applicable to alternative performed (Class A or Class B) com late the following monitor in data: Parameter Allowable Level in Sludge in Pathogen Density " um eco Excee- Frequency of Analysis y Sample TYpe nay t Tech - ninilo Minimus Geo. Mean aximu Knits Fecal Coliform z x to ro the Gth power per grain of totalsolids MPN 27,336 54,869 116,280 MPN/g 0 Annual Grab SM9221CI? CFtI 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grants total solid (dry weight) Vector Attraction Heddction (15A NCAC 021 .1107) - Please indicate alternative performed: )Alt. 5 (14 -Day Aerobic) U IAIt. 6 (Alk. Stabilization ❑ IAIt 7 (Dryings Stable) ❑ [Alt. 8 (Drying- Unstable) Ll i were U "I certify, under penalty of law, that the pathogen requirements in I5A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 0'71T.1 107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1 106 and the vector attraction reduction requirement in 15A NCAC 0#.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the Phis determination has been made under my direction anti supervision in accordance wml tile system designed to ensure thah:qualificd personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. i am aware that there are significant penalties for false certification including fine and imprisonment." Preparer of rq arcf Date SignatuX of "Preparer is defined i6'40 CFR Part 503.9(r) and 15A NCAC 2T .1102 President e (if appli Applier (if applicable) or DENR FORM PVRF 02T (12/2006) COASTAL, FARMS AND RESIDUALS, LLC WQ0034806 Carolina Beach WWTP Date hecal Coliform MPN per grant Log 04/10/18 116.280 _ 5.0655 04/10/18 36,545 4.5628 04/10/18 _ 56,479 4.7519 04/10/18 27,336 4.4367 04/10/18 45,139 4.6546 04/10/18 116,280 5.0655 04/10/18 43,479 4.6383 Total 33.1753 Average4.7393 Geometric Mean 54,869_ Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class 13 - Alternative 1 Pathogen Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 30, 2018 Morehead City 17.50 % Solids 7.38 PH Permit No. NC0026611 Parameter % -? Mg/Kg Dry Weigbtl i 10,000 PoundsMry Ton, e M x0.002 Nitrogen (I'KN) 1.440 14,400.000 28.800 Phosphorus 2.010 20.100.000 40.200 Potassium 0.539 5.390.000 10.780 PAN (injected)" 0.465 3,869.500 7.739 PAN (surface)* 0.448 1777.000 7.554 Ammonia Nitrogen 0.034 335.000 0.670 Calcium 3.480 34,800.000 69.600 Calcium Carbonate Eq. --- Magnesium 0.514 5,140.000 10.280 Sodium 0.749 7.490.000 14.980 Sulfur --- --- --- Nitrate N / Nitrite N --- 91.100 0.182 Barium Chloride --- --- - --- - --- SAR 4.14 IronCeiling Conceu. Aluminum 12,500.00 25.000 M K Arsenic 7.60 0.015 75 Cadmium --- 5.77 0.012 85 Chromium --- 11.000 --- - --Copperr 691.00 1.382 4,300 Lead --- 1 10.50 0.021 840 Mercury 0.77 0.002 57 Molybdenum 5.77 0.012 75 Nickel 12.70 0.025 420 Selenium 5.77 0.012 100 Zinc --- 663.00 1.326 7,500 Environmental Chemists, lnc. 2018-01484 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(PKN-Ammonia N) + Ammonia N + Nitrate N -s Nitrite N =% PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N =% PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. , �,., R �t , ' a , ANALYTICAL. & CONSULTING CHEMISTS Environmental Chemists, Inc. ('602 VVindmill\M3, lVilmin Ion.N( '8105 b 910392 o,2 ) it> lI0,3r)'3.24 Fay. 710 Bowi;ot, nRotd,A4a, teo AC 2795,4 ? , 1735,0. Lab/Iaa ?i5AVVil milton Iligh1 4y, ladsom ilk., NC 28;40, 91031.X43 Lal,/Fas infor,l ell vi ronown to lohemistscom Town Of Morehead City Date of Report: Mar 19, 2018 706 Arendell Street Customer PO #: Morehead City INC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2018-01484 Cyanide Project ID: <0.0863 mg/kg Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-03665 Site: Sludge 1/30/2018 10:10 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed RCI Ignitability EPA 1030 <0.8mm/sec 02/13/2018 Cyanide EPA 335.4 <0.0863 mg/kg 02/07/2018 Sulfide SM4500SD <0.1727mg/kg 02/05/2018 pH SW 846 Method 9045D 7.38 units 02/14/2018 Sludge Residuals Aluminum EPA 2003 12500 mg/kg 02/13/2018 Arsenic EPA 200.7 7.60 mg/kg 02/13/2018 Cadmium EPA 2001 <5.77 mg/kg 02/12/2018 Calcium EPA 2007 34800 mg/kg 02/14/2018 Chromium EPA 200.7 11.0 mg/kg 02/12/2018 Copper EPA 200.7 691 mg/kg 02/15/2018 Lead EPA 200.7 10.5 mg/kg 02/12/2018 Magnesium EPA 200.7 5140 mg/kg 02/14/2018 Molybdenum EPA 200.7 <5.77mg/kg 02/12/2018 Nickel EPA 2007 12.7 mg/kg 02/12/2018 Potassium EPA 200.7 5390mg/kg 02/14/2018 Selenium EPA 200.7 <5.77 mg/kg 02/13/2018 Sodium EPA 200.7 7490mg/kg 02/14/2018 Zinc EPA 200.7 663 mg/kg 02/12/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 14400 mg/kg 02/01/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 91.1 mg/kg 02/06/2018 Total Solids (%) SM2540a 17.5% 01/31/2018 Ammonia Nitrogen SM 4500NH3 C 335 mg/kg 02/09/2018 Total Phosphorus SM 4500 P F 20100 mg/kg 02/02/2018 Mercury SW84674718 0.7660mg/kg 02/11/2018 Report #,. 2018-01484 Page 1 of 3 ej 0 (-J ...... ....... ---------- ------------ — --- ------ >4 Z�z L it CD 0 .. L ..... ... ---- - -------- - ej 0 ...... ....... ---------- ------------ — --- ------ >4 Z�z L CD 0 oo c-] --- -------- ej 0 l � 4q'- d h Environmental Chemists, Inc. 8801l indmill \a, Wilnvn lun,'Nr- 1840 (II0392,01 23 L b I 91039 1124 Fev 7110 Bowsu'town Road Manleo NC' '7954 ° 2.173,5702 kib7Faa 255 A Wilnt.n„ton Hit,htaa%, )acksonviI1u, NC 28510 910347.581.. Lab, l ax ANALYTICAL & CONSULTING CHEMISTS infiS(a em ironmcnlalchcmist S.com Town Of Morehead City Date of Report: Mar 15, 2018 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2018-03081 Project ID: Sludge Lab ID Sample ID: 18-07592 Site: class b sludge Test Total Solids (%) Chlordane Endrin Heptachlor Heptachlor epoxide Lindane Methoxychlor Toxaphene 1,4 -Dichlorobenzene (TCLP) 2,4,5 -Trichlorophenol (TCLP) 2,4,6-Trichlorophenol(TCLP) 2,4-Dinitrotoluene (TCLP) Cresol (TCLP) Hexachloro-1,3-butadiene (TCLP) Hexachlorobenzene (TCLP) Hexachloroethane (TCLP) m + p-Cresol(TCLP) Nitrobenzene (TCLP) o-Cresol(TCLP) Pentachlorophenol (TCLP) Pyridine (TCLP) 2,4,5 -TP 2,4-D 1,1-Dich loroethylene 1,2-Dichloroethane Benzene Collect Date/Time Matrix 2/27/2018 10:30 AM Solid/Sludge Method SM 2540 G SW 846 Method 8081 B/3510 SW 846 Method 80818/3510 SW 846 Method 8081 613 51 0 SW 846 Method 80816/3510 SW 846 Method 8 081 813 510 SW 846 Method 80813/3510 SW846 Method 80818/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 827013510 SW 846 method 827013510 SW 846 method 8270/3510 SW845 Method 8151A SW846 Method 8151A SW846 Method 8260/5030 SW846 Method 8260/5030 SW846 Method 826015030 Results Sampled by C. Dangerfield Date 20.5% 02/28/2018 <0.02 mg/L 03/02/2018 <0.0005 mg/L 03/02/2018 <0.0005 mg/L 03/02/2018 <0.0005 mg/L 03/02/2018 <0.0005 mg/L 03/02/2018 <0.0005 mg/L 03/02/2018 <0.05 mg/L 03/02/2018 <0.050mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050mg/L 03/01/2018 <0.050mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.050mg/L 03/01/2018 <0.250mg/L 03/01/2018 <0.050 mg/L 03/01/2018 <0.003 mg/L 03/05/2018 <0.003 mg/L 03/05/2018 <0.01 mg/L 03/06/2018 <0.01 mg/L 03/06/2018 <0.01 mg/L 03/06/2018 Report #:: 2018-03081 Pane 1 of 2 h Environmental Chemists, Inc. 03/05/2018 Barium EPA 2001 c7 P vza $s t t E3-�� 6602 Windmill Wa% 1A'ih31 ❑ Ion N(' 2810 91U 49 0'23 ],ab910-3,92.4424 Pas 71013msuttown Road Manteo, NC 27951 152473-57021 b�l'as Cadmium Hil,ht\ 3v, lacksom IIIc, NC 285-10 910.347.5843 Lab/Fax ANALYTICAL CONSULTING CHEMISTS infora2amirUnnitn Udchemists.corn EPA 200.7 Town Of Morehead City Date of Report: Mar 15, 2018 Lead 706 Arendell Street Customer PO #: 03/05/2018 Morehead City NC 28557 Customer ID: 09020011 <1.0 mg/L Attention: C. Sutton Report #: 2018-03081 EPA 200.8 <1.0mg/L Project ID: Sludge Mercury Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 03/06/2018 Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L 03/06/2018 Chloroform SW846 Method 8260/5030 <0.01 mg/L 03/06/2018 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 03/06/2018 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 03/06/2018 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 03/06/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01mg/L 03/06/2018 TCLP Metals Arsenic EPA 2007 <1.0 mg/L 03/05/2018 Barium EPA 2001 <1.0mq/L 03/05/2018 Cadmium EPA 200.7 <1.0mg/L 03/05/2018 Chromium EPA 200.7 <1.0mg/L 03/05/2018 Lead EPA 2003 <1.0mg/L 03/05/2018 Silver EPA 200.7 <1.0 mg/L 03/05/2018 Selenium EPA 200.8 <1.0mg/L 03/12/2018 Mercury EPA 245.1 <0.0020 mg/L 03/04/2018 Comment: Reviewed by Report #;: 2018-03081 ud»� ..... Pane 2 of 2 �� 6A AL✓(�Y .�6��z �( 1�nu ili it \: Kra i ;,�i 3) _ ri � I'd�17 n r .,i_)�LI?1J�h ��° ` i1J Rol ,r rfu�.• ho ,ri biai l o XC Ss, a ANAMICAL& CONSULTING CHEMISTS uNr�d.mi-lix.rinh�hr i.�, cum. Town Of Morehead City Date of Report: Apr 17, 2018 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2018-05174 Matrix Sampled by Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12841 Site: 1 4/3/2018 10:10 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM2-WG 29,9% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 8705 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12844 Site: 2 4/3/2018 10:12 AM Solid/Sludge C. Dangerfield Test Method Results Date Analvzed Total Solids (%) SM 2540 G 26.8% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 2950 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12845 Site: 3 4/3/2018 10:14 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 G 26.9% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 17126 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12846 Site: 4 4/3/2018 10:16 AM Solid/Sludge C. Dangerfield Test _ Method Results Date Analyzed Total Solids (%) SM 2540 G 27.3% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 8798 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12847 Site: 5 4/3/2018 10:18 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) Y SM2540G _ 27.0% 04/04/2018 Fecal Density SM 9221 C E MPN 24 hr 503 2924 MPN/g 04/04/2018 Report fl:: 2018-05174 Page i of 2 'I til k� =Ilnakl I 't! Mantoo, Ak_77 >1 �521r > I-ih/l x l'r.ut„tt>nlit'd W28 40 9 t ,li X5431 d)/ ❑ii?;([.OMIT ,]I it!91C�1CI111.`:ISUpill Town Of Morehead City Date of Report: Apr 17, 2018 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2018-05174 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12848 Site: 6 4/3/2018 10:20 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 c 26.9% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 6318 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12849 Site: 7 4/3/2018 10:22 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 c 27.4% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 16770 MPN/g 04/04/2018 Comment: l l Reviewed by:�'--- Report #:. 2018-05174 � � ” Page 2 of 2 2 mss. ANALYTICAL 8 CONSULTING CHEMISTS 'I til k� =Ilnakl I 't! Mantoo, Ak_77 >1 �521r > I-ih/l x l'r.ut„tt>nlit'd W28 40 9 t ,li X5431 d)/ ❑ii?;([.OMIT ,]I it!91C�1CI111.`:ISUpill Town Of Morehead City Date of Report: Apr 17, 2018 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: C. Sutton Report #: 2018-05174 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12848 Site: 6 4/3/2018 10:20 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 c 26.9% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 6318 MPN/g 04/04/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-12849 Site: 7 4/3/2018 10:22 AM Solid/Sludge C. Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 c 27.4% 04/04/2018 Fecal Density SM 9221C E MPN 24 hr 503 16770 MPN/g 04/04/2018 Comment: l l Reviewed by:�'--- Report #:. 2018-05174 � � ” Page 2 of 2 2 _ r H{III i O ( t I t I1 y 1 �. i ofIIru — !11-Z� clj� _I _,_ ANNUAL PATHOGEN AND VECTOR ATTRAC'T'ION REDUCTION. FORM (503 Rules) Facility Name: Coastal Farina and Residuals, LLC WQ Permit Number: WQ0034806 WWTP Name: Town of Morehead City NPDES Number: NCO02661 I Monitoring Period: From 111!2018 TO 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Altemative 3 ❑ Altetmative 4 ❑ Alternative 5 ❑ Altemative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce P11-1110119e0–f:" Compost ❑ Heat Drying EJ Heat Treatment ❑ 'Themhilic 1:1 Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ Class B; Altemative 1 O Alternative 2 ❑ If applicable to allernative performed (Class B on1)') indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dt in ❑ Composting ❑ Aerobic Di estion ❑ Anaerobic Di estion LI If applicable to alternative perfarmed Class A or Class B) complete the llowing monitoring data: Parameter Allowable Level in Sludge Pathogen Densityer $ o um RXcce- Frequency ofAnalysis Sample Type na yuca Tech - niolle Minimun Goo. MeanMaximw Units Fecal Coliform 2 x 10 to the 6th power Pei' gram of total solids MPN 2,924 7,386 17,126 MPN/ 0 Annual Grab SM 9221 CR. CPU 1000 mpn per gram ortotai solid (dry wci hp Sabnonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grains total solid (dry ieei"ht vector riurttcuun iecuucuon tvu uric ow.aal - rieese marcate option pertormea: Alt. (VS reduction) ❑ JAR. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑Alt, 4 (Spec. 02 uptake) C] Alt. 5 (14 -Day Aerobic} ❑ Alt. 6 (Alk. Stabilization ❑ JAR 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ jAlt, 10 (incorporation) El INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." _ ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Chad Sutton, W WTP Superintendent Wesley Wooten, President Preparer n T' I e 0�- ytt) band Applier Name and Title (if applicable)(type or print) 1.31- / 9 _ (� � 2/7119 Signature of Preparer* Date Signature of I d Applier (if applicable) Date '"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 503 (12/2006) COASTAL FARMS AND RESIDUALS, LLC W00034806 Morehead City WWTP Date Fecal Coliform MPN per grain Log 04/03/18 8,705 3.9398 04/03/18 2,950 3.4698 04/03/18 17,126 4.2337 04/03/18 8,798 3.9444 04/03/18 2,924 3.4660 04/03/18 6,318 3.8006 04/03/18 16,770 4.2245 Total 27.0787 Average 3.8684 Geometric Mean 7,386 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 27, 2018 Northwest Regional WR F Permit No. WQ0034367 3.26 % Solids 7.17 pH Parameter % Mg11ZgDiryWeight (%490,000) '� Pouods/Diylan (M xU.Q02 Nitrogen (TKN) 4.460 44,600.000 89.200 phosphorus 3.330 33.300.000 66.600 I'otassimn 0.272 2,720.000 5.440 PAN (infected)* 1.369 13.692.100 27.384 PAN (surface)* 1.356 13,560.600 27.121 Ammonia Nitrogen 0.026 263.000 0.526 Calcium 2.140 21,400.000 42.800 Calcium Carbonate Eq. --- --- --- Magnesium 2,030.000 4.060 Sodium 4,050.000 8.100 Sulfur Nitrate N / Nitrite N --- 128.000 0.256 Bal iuln --- --- --- Chloride --- --- --- Iron -'- --- --- Aluminum --- 32.900.00 65.800 Arsenic 17.40 0.035 Cadmium --- 17.40 0.035 Chromium --- 37.400 --- Co er 337.00 0.674 Lead --- 23.10 0.046 Mercury 0.736 0.001 Molybdenum 17.40 0.035 Nickel 22.90 0.046 Selenium 17.40 0.035 Zinc --- 1,120.00 2.240 Environmental Chemists # 2018-21432 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(fKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(fKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N+ Nitrite N = % PAN Note. Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. Environmental Chemists, r609'rVindmul bV1 ltii6 un t /n, N( >S}tl 1 ('10 392 l0>31 il 970597 3 i24 Fax i uh 3.u7z� �� 3ren 71u Ho 14 er,own Igo;d Mai io NC 27951 o d7., 5702 1.3u/1 1x 28140 e 910 34 >2743 1 ab/lax ANALYTICAL & CONSULTING CHEM6TS rola-cnvirxnnncntulc!;emistacoin Onslow Water & Sewer Authority Date of Report: Jan 21, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2018-21432 Project ID: Northwest Reg. WRF Lab ID Sample ID: N1852323 Collect Date/Time Matrix Sampled by 18-53946 Site: Digester Sludge 12/27/2018 6:45 AM Solid/Sludge M. Young Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8 081 B/351 0 <0.02mg/L 01/10/2019 Endrin (TCLP) SW 846 Method 80818/3510 <0.0005mg/L 01/10/2019 Heptachlor (TCLP) SW 846 Method 8081B/3510 <0.0005mq/L 01/10/2019 Heptachlor epoxide (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 01/10/2019 Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005mg/L 01/10/2019 Methoxychlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/10/2019 Toxaphene (TCLP) SW846 Method 8081B13510 <0.05mg/L 01/10/2019 1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 2,4,5-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 2,4,6-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 2,4-Dinitrotoluene(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/04/2019 Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/04/2019 Hexachloroethane(TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 m + p -Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/04/2019 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050mg/L 01/04/2019 o -Cresol (TCLP) SW 646 method 8270/3510 <0.050 mg/L 01/04/2019 Pentachlorophenol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 01/04/2019 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 rri 01/04/2019 2,4,5 -TP SW846 Method 8151A <0.003mg/L 01/10/2019 2,4-D SW846 Method 8151A <0.003 mg/L 01/10/2019 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/03/2019 1,2-Dichloroethane(TCLP) SW846 Method 8260/5030 <0.01mg/L 01/03/2019 Benzene (TCLP) SW846 Method 8260/5030 <0.01mg/L 01/03/2019 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/03/2019 Repel Nr. 2018 21432 vm....m_v.�.w_ ..YY... ...a. .........� Page 1 of 3 u eY EnvIroninental Chemists, Inc. 0679 N'indnll/lav Willm1wfon AC 28}(11 910 c'0 'Slab 1)10.3924424 1 1\ '�` t a ' ,✓ a'� "+ ,u� 7i0`ro �ertoui i c2cc iel 4,an o ?\!(' 2795i 9.2A73a 9(ab/I a x 235- lbitmmuton i ligh v, ay, Jac k om illc, N, c 28710 , 1) 1 ,34 b -I:3 1.ab/Fax ANALYrICAL & CONSULTING CHEMISTS info,iueuvironmentalchvuisl6.uom Onslow Water & Sewer Authority EPA 335.4 Date of Report: Jan 21, 2019 01/08/2019 228 Georgetown Road SM 4500 SD Customer PO #: 01/16/2019 Jacksonville NC 28540 SW846 method 1010 Customer ID: 08100092 12/31/2018 Attention: Todd Roberts SW 846 Method 9045D Report #: 2018-21432 01/11/2019 Sludge Residuals Project ID: Northwest Reg. WRF Chlorobenzene (TCLP) 9W846 Method 8260/5030 <0.01 mg/L 01/03/2019 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/03/2019 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 01/03/2019 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01mg/L 01/03/2019 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01mg/L 01/03/2019 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/03/2019 id Cyanide EPA 335.4 <0.05 mg/kg 01/08/2019 Sulfide SM 4500 SD 0.66 mg/kg 01/16/2019 Ignitability SW846 method 1010 >215°F 12/31/2018 pH SW 846 Method 9045D 7.17 units 01/11/2019 Sludge Residuals Aluminum EPA 200.7 32900 mg/kg 01/02/2019 Arsenic EPA 2001 <17.4mg/kg 12/31/2018 Cadmium EPA 200.7 <17.4mg/kg 12/31/2018 Calcium EPA 2003 21400 mg/kg 01/01/2019 Chromium EPA 200.7 37.4 mg/kg 12/31/2018 Copper EPA 200.7 337 mg/kg 12/31/2018 Lead EPA 200.7 23.1 mg/kg 12/31/2018 Magnesium EPA 200.7 2030 mg/kg 01/01/2019 Molybdenum EPA 2007 <17.4mg/kg 12/31/2018 Nickel EPA 2003 22.9 mg/kg 12/31/2018 Potassium EPA 200,7 2720 mg/kg 01/01/2019 Selenium EPA 200.7 <17.4mg/kg 01/06/2019 Sodium EPA 200.7 4050 mg/kg 01/01/2019 Zinc EPA 200.7 1120 mg/kg 12/31/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 128 mg/kg 01/18/2019 Total Solids (%) SM 2540 e 3.26% 12/27/2018 Ammonia Nitrogen SM 4500NH3 C 263 mg/kg 01/11/2019 Total Kjeldahl Nitrogen (TKN) SM 4600or90 44600 mg/kg 01/11/2019 Report #. 2018-21432 ...,..,.a....».1)..........v..,......R,...-.-..,..e...�...,.a- - - - Page 2 of 3 ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Environmental Cherrasts, Inc. 6002 Winds ill Wa 4V'iln a hton, N( 28105 910 92.0223 1 a = 910.39) 4424 };a.x 71;1 r cat 5u iuwn Ro ui, ulanfio NC 279r)4, /25 %479 70) 1,11)/Fax v5 A Wilmua}yton ti t.h�+a>.lacksrm villc, NC a540 0 9r0 t4 .F843 Lab/1,Iv Total Phosphorus SM 4500 P F Mercury SW8467471B TCLP Metals ill loGc`emhnnIII enurlchemist,com Date of Report: Jan 21, 2019 Customer PO #: Customer ID: 08100092 Report #: 2018-21432 Project ID: Northwest Reg. WRF 33300 mg/kg 01108/2019 <0.736 mg/kg 01/09/2019 Arsenic EPA 2007 <1.0mg/L 01/17/2019 Barium EPA 200.7 <1.0mg/L 01/17/2019 Cadmium EPA 200.7 <1.0mg/L 01/17/2019 Chromium EPA 2007 <1.0mg/L 01/17/2019 Lead EPA 2007 <1.0mg/L 01/17/2019 Selenium EPA 2667 <1.0mg/L 01/17/2019 Silver EPA 200.7 <1.0 mg/L 01/17/2019 Mercury EPA 2451 <0.0002mg/L 01/08/2019 Comment: Sludge residuals results reported on a dry weight basis. TCLP and RCI results reported on an as received basis. Reviewed by: Report it: 2016-21432 Page 3 of 3 z� N �Y n M tLNzZ iO Cl) O FN W M W ° U LL0 b O S S Q Jb L) U ago Z= Z Za° W 0a ix LU W Z ° J ° J 0 o O 1i z w b Z° Z W a W I LL a _ N L d U LL Z � C Q n 7M■.' S. O n � N N 11 y C N J } n J � 11 �V J E c„LL vH3H10 n T Z Owl m 0HOVN v n _ Y U > �. Qom' tONH i W — VOSZH j I 3NON X ». J r NgownN j 41 BVI U�1 116ui C • aupoly� i O � 1 (�'o d) � (7 a (9 a (D a (9 a C7 T(D a (� a C9 \ 'auleiuop I gejE) Jo U U � (i (D U U J(D (i (7 U (D J( -D ailsodwo� ad61 aldweS 0 i p of m i � o w J T U aJ Y � � N N 'F .1 O R G � V w a 3 fn N K Environmental Chemists, Inc. ('.0 "find )IM lln, WiSnin tc.n, NU 28W. IHO » 0223 1 il �)I(', > 'l tan 9 3n 710fio jw,n C,tI Nhinhu AC ^7051 2;2273 02!:u)_! n A V' ilm.nl;ton I hs l wav, j.acl. cin dle, A'C 3_ IJ a 910 4/.t,b13 I on; Fas ANAf_Y11CAL & CONSULTING CHEMISTS ini ron;rreitielclier»i;(9.cmr. Onslow Waver & Sewer Authority Date o Report: May 08, 2018 228 Geoioetcv✓n Road Customer PO #: Jacksonv!fle NC 28540 Custo!xjcr ID: 08100092 Attention Maik, Young Report ;t: 2018 06842 Project 11): Northwest Reg WRF Lab ID Sample ID: Collect Date/Time ( Orix Sampled by 18-17089 Site: 001 5/2/2018 9:10 AM Sn, ,t+Sludge Mark Young Test Method Results Date Analyzed Total Solids i` -;l sk-;::.11,0 e. Fecal Densitv Sid 9121C e MPN 2N n: scs Lab ID Saniple ID: Collect DatelTimc 18-170£0 Site: 002 5/2/20'18 9:13 AM Test Method Total oiirf � (, ,z , Fecal Da isrty Lab ID Sample ID: 18-1701±0 site: Oct.? Yc-st Tota' So:ios 'r.,. Feca ."unsity Lab ID Sample ID. 18-170sd= Site: 004 Test Collect Date/Time. 5/2/2018 9:15 AM Method ,r la s 6Mo—,I lot 2. Collect Date/Time `i/;?r rt118 9 18 AM 0.90 °iL 05/03/2018 <200MPN/g 05/03/2018 :sampled by Sol!J/Siudge Murk Young Results Date Analyzed 0-93 05/03/2018 < v t P�1._P1!, 05/03/2018 arix Sampled by S .Nudge Mark Young Results Date Analyzed 0.98 "rS 05/03/2018 <1d 4 MI ,Nig 05/03/2018 r..vir. Sampled by �Wdgc �1;erk Young Method ReSUIlS Date Analyzed Tota! Scuds z SI1I2 BG Fec ' of siiy Lab ID S lillpie 10: Co lect Date/Time 5/Z, 3'i8 9:20 AN. Test Method Total s,ho, Fecai si .. f 0.87 "/•: 05/03/2018 2 xt M ��i1g 05/03/2018 r' .trix Sampled by Sludg; ar Young Results Date Analyzed 0.90V 05/03/2018 05/03/2018 ANALY IICAL & CONSULTING CHWISTS Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville; NC 28540 Attention. Nkr<Young Lab ID Ssrnhle ID: 18-17094 Site:006 Test Total Solids i`A,) Fecal Density Lab ID Sample ID: 18 1 (, `IG 5 Pe: 00i t t n.dm it 411 ''1'ilil m h n �'M '11111 )10 "'41'1Pa; > sol tu11a 1, Monte,), '7V,) 1 2>2,473,57i I A,11 iv 1 1 bA n �i ;ton 1-ligh v.lad. on%flle,'XC °S..10 "',3 E; 1.. - 'ray i nin(a: en\ roun,d�malclt mists.com Date o- oport: May 03. 20'18 CustoP`er PO #: 05/03/2018 custolr:e>ID: 08400092 Report „t. 2016 06842 Project iCr Northwest Reg. WRF Collect Date/Time n ..IN Sampled by 5/2/2018 9:22 AV Sci;:}ASludge Mark Young rvlethod Results Date Analyzed sm r+;a c 0 99 05/03/2018 SM Baa,c FMPN 2n 687 MPN/q 05/03/2018 Collect Date/Time. Sampled by 5/2/20 18 9.24 AMSludge viark Young Teri iU'iethod Total Solids U -v c Fec Jenaity ,n+s2;a f'WN Carm,n;i klisLd(s reported on a dry yr igirt basis Rev f- vved ! ry f2eSURS Date Analyzed 0 86'i;, 05/03/2018 52 NPM/q 05/03/2018 aq< 0 Ti B MP 12 ------ > cr w U) (1) a) Q) —cu —(o —(U —M 76 Q u LL LL LL LL LL LL LL U3HIO Q 01"i xI x x HOYN 4 CC EON" ul ( L 0 u OOSA cc UaSYYnN v (11 awl -vow (o jo d) W 0.'m clejo 10 ojisodw,o adA.L oldwas U) co co 0 co co Q ca cc d) 0 L) CO 0 LN co Lo co F'- A (1) (D a) 0. a a E a E a E E E E C/) MP ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastai Farms and Residuals, LLC WQ Permit Number: W00034806 W WTP Name: Northwest Regional WRF NPDES Number: W00034367 Monitoring Period: From 1/1/2018 To 12/31/2018 n_at........ n-A....R.... (ICA W11 A f' M'P I IAt) _ PtnneP tnIUPQtP IPVPI aebleved and alternative performed: -- Class A: Alt. A (time/tem �) ❑ Alt B (Alk Treatntcn9❑ Alt. C (Prior Testin )p A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Patho ens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Hent Drying ❑ 1 tical Treatment p Theitno hilie ❑ Beta Ra ❑ Gamma Ray p 1 Class B: JAII. (1) Fecal Density El I Alt. (2) Process to SignMcat fly Reduce Pathogens❑ If applicable to alternative performed (Class B only) indicate "Process to Si niticantl Reduce Pathogens": Lime Stabilization 013o DI in =E3 Com ostia p Aerobic Di estion ❑ Anaerobic Digestion ❑; If applicable to alternative erformed (Class A or Class B) complete the tollowin monitorin data: Allowable Level Pathogen Density a'" r ° na y ica Frequency Sample Tech Excee• Parameter in Sludge Minimus Geo.MeanMaximu Units of Analysis Type 2 x 10 to the MPN 184 277 687 MPN/g 0 Annual Grab SM92210E 6th power per gram of Fecal Coliform Local solids CFU 1000 mpn per gram oftotaisolid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) fd• Vector Attraction Reduction (i5A NCAC 02T .1107) -Please indicate alternative per Orme . ❑ "I certify, in vector attrac p "I certify, u vector attrac if you check penalty of law, that the pathogen requirements in 15A NCAC 02T,1106 and the reduction reouirement in 15A NCAC 02T.1107 have been met." penalty of law, that and the reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note statement attach an explanation why you have not met one or both of the re uirements. "This determination has been made under my direction and supervision in accordance with the system designed to ensure that;qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for;false certification including fine and imprisonment." Mark Young, ORC Wesley Wooten President Prepar Name and itle (t pe or print)4Dtc Land Applier Nape and Title (if applicable)(type or print) i�nature of Pr rer* Signa re of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Northwest Regional WRF Date Fecal Coliform MPN per gram Log 05/03/18 200 2.3010 05/03/18 184 2.2648 05/03/18 184 2.2648 05/03/18 230 2.3617 05/03/18 223 2.3483 05/03/18 687 2.8370 05/03/18 524 2.7193 Total 17.0970 Average 2.4424 Geometric Mean I==Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class S - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: May 9, 2018 Pluris Hampstead WWTF Permit No. WQ0037287 2.88 % Solids 6.35 vH Parameter I Q/o bMg/<g DryWeight %x10,000 Pounds/Dry Ton: (M gKx0.002) Nitrogen (TKN) 7.860 78,600.000 157.200 Phosphorus 2.300 23.000.000 46.000 Potassium 1.240 12.400.000 24.800 PAN (injected)* 2.661 26.611.690 53.223 PAN (surface)* 2.445 24,446.690 48.893 Ammonia Nitrogen 0.433 4,330.000 8.660 Calcium 2.190 21,900.000 43.800 Calcium Carbonate F, . --- --- --- Ma nesium 5.210.000 10.420 Sodium -- 6,040.000 12.080 Sulfur --- Nitrate N / Nitrite N --- 0.690 0.001 Barium Chloride --- --- --- --- SAR 1.61 bon --- --- --- Ceiling Concen. Aluminum --- 14,200.00 28.400 M K Arsenic --- 16.70 0.033 75 Cadmium --- 16.70 0.033 85 Chromium --- 67.700 0.135 --- copper 196.00 0.392 4,300 Lead --- 16.70 0.033 840 Mercury - 0.59 0.001 57 Molybdenum 16.70 0.033 75 Nickel 41.00 0.082 420 Selenium 13.70 0.027 100 'Linc --- 528.00 1.056 7,500 Environmental Chemists # 2018-07412 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rale)(fKN-Ammonia N) + Ammonia N +Nitrate N -i- Nitrite N = % PAN Surface Application: (Mineralization Rale)(fKN-Ammonia N) + (0.5)(Atmnonia N) + Nitrate N -i- Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation proposes. Environmental Chemists, Inc. ,� 9 �>t.�� 4 k 6602 6Vlinclmill /Nay, Wi6ningron, 1C' °ti105 910 392 W23 Lab - 910. 91 412 t Fax 71Q &nvsertown P.oad, Nlenl�n, '\(' 27);1 252.17; 3702 Lab/Pax 255-A Wilmington I filgimay, Jar.ksonvMe, NC 23540 910347S643 Lab/Pax ANALYTICAL& CONSULTING CHEMISTS infwa'em-iron 11 ren I alchenlisU.con1 Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Lab ID Sample ID: 18-18475 Site: Sludge Test Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Nickel Potassium Selenium Sodium Zinc Molybdenum Nitrate+Nitrite-N itroge n Total Solids (%) pH Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Total Phosphorus Mercury Date of Report: Jun 25, 2018 Customer PO #: Customer ID: 14020008 Report #: 2018-07412 Project ID: Pluris-Hampstead Collect Date/Time Matrix Sampled by 5/9/2018 11:30 AM Solid/Sludge Client Method Results Date EPA 200.7 14200 mg/kg 06/08/2018 EPA 200.7 <16.7 mg/kg 06/02/2018 EPA 2007 <16.7 mg/kg 06/02/2018 EPA 200.7 21900 mg/kg 05/11/2018 EPA 200.7 67.7 mg/kg 06/02/2018 EPA 2007 196 mg/kg 06/02/2018 EPA 200.7 <16.7 mg/kg 06/02/2018 EPA 200.7 5210 mg/kg 05/11/2018 EPA 200.7 41.0 mg/kg 06/02/2018 EPA 200.7 12400 mg/kg 05/11/2018 EPA 200.7 <13.7 mg/kg 06/02/2018 EPA 200.7 6040 mg/kg 05/11/2018 EPA 2003 528 mg/kg 06/02/2018 EPA 200.8 <16.7mg/kq 06/18/2018 EPA 353.2 <0.69 mg/kg 05/17/2018 SM 2540 B 2.88% 05/10/2018 SM4500HB 6.35 units 05/21/2018 SM 4500 NH3 C 4330 mg/kg 05/17/2018 SM 4500 Org B 78600 mg/kg 05/17/2018 SM 4500 P F 23000 mg/kg 05/17/2018 SW8467471B <0.590mq/kg 05/31/2018 Report #:: 2018-07412 Page I of 3 Environ nental Chemists, Ince 4m, (,602 Windmb1ill lhaylmn ion, A' ?8405 ' 910 ? 92.0223 Lal' 910.39 }424 l=ox 70 13o�'sertowrr Road, Manlro, NC 27251 " 252.4 3.5702 Lab"Fax 7,55-A Wilmington I f.ghway, laclvsonvi l le, NC 25540 ° 910.347.5848 1 ab/Fax ANALYTICAL & CONSULTING CHEMISTS in:bia;cm I ronnlentalchemistaconI Lewis Farms & Liquid Waste, INC. Date of Report: Jun 25, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2018-07412 Project ID: Pluris-Hampstead Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18476 Site: 1 5/9/2018 12:00 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.86% 05/10/2018 Fecal Density $M 9221C E MPN 24 hr 503 18882 MPN/g 05/10/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18477 Site: 2 5/9/2018 12:02 PM Solid/Sludge Client Test Method Results Date Analvzed Total Solids (%) SM 2540 G 2.67% 05/10/2018 Fecal Density SM 9221C E MPN 24 hr 503 4869 MPN/g 05/10/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18478 Site: 3 5/9/2018 12:04 PM Solid/Sludge Client Test Method Results Date Analvzec Total Solids (%) SM 2540 G 2,66% 05/10/2018 Fecal Density SM 9221C E MPN 24 hr 503 13158 MPN/g 05/10/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18479 Site: 4 5/9/2018 12:06 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.68% 05/10/2018 Fecal Density SM 9221C E MPN 24 hr 503 2948 MPN/g 05/10/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18480 Site: 5 5/9/2018 12:08 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.65 % 05/10/2018 Fecal Density SM 9221C E MPN 24 hr 503 9057 MPN/g 05/10/2018 Report #'.'. 2018-07412 Page 2 of 3 Environmental Chemists, Inco 0602 Windmill Way°. Wilmington, n(:28405 , 910.392.02231..ab ' 9103302.4421 Faa 710 Brnvsertown Road, Manteo, NC 2795+ m 252 5 47 702 Lab/Pas 255-A Wilmington I-iighl+ay; Jacksmwille, NC 28540 ' 9IJ.347.15813 Lab/Fas ANALYTICAL & CONSULTING CHEMISTS in Ri(ri znviromnemal<hzinisu.com Lewis Farms & Liquid Waste, INC. Date of Report: Jun 25, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2018-07412 Project ID: Pluris-Hampstead Lab ID Sample ID: Collect Dateffime Matrix Sampled by 18-18481 Site: 6 5/9/2018 12:10 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM2540G 2.57% 05/10/2018 Fecal Density SM92210EMPN 24 hr 503 13619 MPN/g 05/10/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-18482 Site: 7 5/9/2018 12:12 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.44% 05/10/2018 Fecal Density SM 9221C E MPN 24 hr 503 5328 MPN/g 05/10/2018 Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: _.MWOL n 1 Report It. 2013-07412 _ Page 3 of 3 N Z ro OE E c d 0 w rnO1 w L M�y O TN 3 d o c U 9 LL O LL C O �I c L Li Z Z O F W a Sirl, to w c a a o U Q `I ? 7 fl] 17 ro y CL v lu o W_ N M w o O fL 0 N J 0 U f � 3 2 B H3H10 m I OOIHl QHOVN 1y�J N fr SONH W EOS2H j O. 10H t 3NON of eve'r� 7 7 T E_ -vow aulmlga 0 i9Uo a_ C7 a. O a- C7 a c7 a - lo a. 0 a. 0 a (7 a. 0 isulefu0a geaE) 'o 0 0 U aflsodwoa adAl oldw,S CL m E I— N ° U fu � D � C O U S C N � H D C A W F n r 04 `I ? 7 fl] 17 ro y CL v lu o ANNUAL PA'PIIO(;iN AND VECTOR ATTRACTION REDUCTION FORM (o2T Rules) Facility Name: Coastal Farms and Residuals, lA,C WQ Permit Number: W00034806 WWTP Name: Hampstead W kM IT WDYS Plumber: MI00037287 lvtonitoriugPeriod: Iron __ 1/1;2018_ To _ 12'31/2018 Pathogen Reduction (15A NCAC 022 ,1106) - Please indicate level achieved and alternative performed: Class A: Alt- A (flute/temp) C7 Alt 13 (Alk "1 reatment) ❑ Alt. C (Prior Testing) Ll _ A1t.D (No Prior "Pest) (] Process to Further lte<hicc Patting ngs C] - if applicable fo alternative perfoi'nud (Class A only) indicate "Process to PurtherReduce. Pathogens": - ('ompou LI I Tont the w LF Beta Rn} Ciamutt Iia, 1 _ iii i1 l i4nun(] luat ht unuphalic U-1 Pnstcuvmlon f:7_ i Class 13, V Alt. (I) Fecal Densit} :L:--LAlt. (2) Process to Simtilicantly Reduce 1'athoxcus LJ Pf applirlble to alternative performed (glass 11 only) iudica(e"Process to Significantly Reduce Pathogens": _- Lime Stabilization Cl Air Drying U Com posting CI IIAerobic Digestion ED Anaerobic Di lestion ❑ If applicable to alternative performed (Class A or Class 13) complete the £ollotving monitoring data: — — '..--_`- -- -..-. -_ ----- --- - "ICuiu�icl�oi. Allowable Level - Pathogen Density }'requcncy Sample. _ ammeter in.Sludge 'vlinintunlGco.Idean 4aximun Units Gsccc ofnnxiy:;is JA,pc fech. - osi0mlhc,- . aPN 2948 81 18;882 MlINfg 0 Annual Giab SW 22KA 6ii1 pou'cr - - - per gram of FecalColiform malsolids CI'U 1000 in p1 per gxalll ofuilal5olid (dry SBCI(!i?l) Salnwrclla laaulma 3 M11'ti per 4 grams (in lieu of heat local solid (dry colifol'm) 5yci;ht Vector Attraction Reduction 0 SA NCAC 02T _110) Please indiente alternative nerfortned: AIt.1 (VS reduction) 1 Alt 2 (40 -day bench) ] Alt 3 (30 -day bench) - Ali.4 (Spec O7. uptake) ❑ Alt 5(14 DrvAerobic) L� Alt 6(Alk Stabilization'-] Alt 7(Divmp-Stable) Ll jAh, 8(Dlying, Unstable) LI Alt9(InliUlon) ] Ale10�Incrnpolntlonj l Yo�ectolntu2ctionieducr:onnlremttia�5��i(per(oilned l{ f'3.?I2'111�ICA TION 'I'ATL 171?NxT (pla ese. cites lI the appropriate statement) R1 "I em'ti£y, under penalty of la5v, ihat the pathogen requirements in 15A NCAC 02T A 106 ;and tate _ vector aHIse doit reduction re umbemeut in I5A NCAC o2,r .1107 have been met." certify, under penalty of law, that the pathogen requirements in 1,5A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T A 107 have not been met," (Please tote if you chock tills statemeu( attach an explanation wvhy you have not mat one or both ottic req uiremew) `OI'his gleterillination has b4'CII made UndCl' my (h t'eCilOtl gild SllpCl'i'iSi011 111 aCL'Ol'(1a14Ce With iliC Sy3tet11 Qe yned to ensure that qualified peasonnO properly ;lather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisountenL" Randy I loffer, ORC Wesley Wooten, President --- Pre.paror Name and Title (tvpc orprihn) ]-and Appher'Name and Rdo Ot'applicable)(type or print) 1/31/19 Jlpilati 11 FC of' Date Signature of La/d Apphoi (if applicable) Date *Pmpwvr k defined in 40 CPR Part 503.9(x) and 15A NCAC 2T .I 102 (26) DfsiNR FORM PVRF 02f (12/2006) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Pluris Hampstead WWTF Date Fecal Coliform MPN per =ram Log 05/09/18 18,882 4.2760 05/09/18 4,869 3.6874 05/09/18 13,158 4.1192 05/09/18 2,948 3.4695 05/09/18 9.057 3.9570 05/09/18 13,619 4.1341 05/09/18 5,328 3.7266 Total 27.3699 Average 3.9100 Geometric Mean8,128 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 21, 2018 Oak Island WWTP 2.63 % Solids 6.28 off Permit No. W 00005790 Parameter % Mg/Kg Dry Weight P/e x 40,000) Pounds/Dry Ton? M x 0.002 Nitrogen (TKN) 3.290 32,900.000 65.800 Phosphorus 0.251 2,510.000 5.020 Potassium 0.180 1,800.000 3.600 PAN (injected)* 1.333 13,328.230 26.656 PAN (Surface)* 1.086 10,858.230 21.716 AmmoniaNitogen 0.494 4,940.000 9.880 Calcium 1.870 18.700.000 37.400 Calcium Carbonate Eq. --- --- --- Magnesium 1,300.000 2.600 Sodium 1.860.000 3.720 Sulfur Nitrate N /Nitrite N --- 0.230 0.000 Barium --- --- --- Chloride --- --- --- tion Aluminum --- 2,930.00 5.860 Arsenic 19.00 0.038 Cadmium --- 19.00 0.038 Chromium --- 19.000 0.038 Copper 151.00 0.302 Lead --- 19.00 0.038 Mercury --- 2.66 0.005 Mol bdenum --- 11.40 0.023 Nickel --- 19.00 0.038 Selenium --- 19.00 0.038 Zinc --- 510.00 1.020 Environmental Chemists # 2018-01049 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Ratc)(1-KN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rale)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note. Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. 6002 VViadmil I lhxy, Wiluunniori 'Vl 28405) 9104202231 ib 910.392.4124 Fix 710 }3ot, nrtowu La ld �(irhu '�C 279-}3 2,2.473O2 Lzb/I x . R '_ . A1ArtLnmgtm� Htbh« zy, lackxin, tl!c, NC 25 40 9701.,47,,843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inCoG? mr; iro��men Ltichcmists.tom Town of Oak Island 4601 East Oak Island Drive Oak Island NC 28465 Attention: David Kelly, II Lab ID Sample ID: 19-02638 Site: Sludge Test Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Revised Report: Feb 04, 2019 Original Report Date: Feb 01, 2019 Report #: 2019-01049 Customer ID: 11100035 Project ID: Fish Factory WWTP Collect Date/Time Matrix Sampled by 12/21/2018 10:00 AM Solid/Sludge Kenneth Von Voigt Method Results Date Analyzed EPA 200.'7 EPA 200 7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200 7 EPA 200.7 EPA 200.7 EPA 200.7 2930 mg/kg <19.0 mg/kg <19.0 mg/kg 18700 mg/kg <19.0 mg/kg 151 mg/kg <19.0 mg/kg 1300 mg/kg <11.4 mg/kg <19.0 mg/kg 01/30/2019 01/30/2019 01/30/2019 01/23/2019 01/30/2019 01130/2019 01/30/2019 01123/2019 01/25/2019 01/30/2019 EPA 200.7 1800 mg/kg 01/23/2019 EPA 2007 <19.0mg/kg 01/30/2019 EPA 200.7 1860 mg/kg 01/24/2019 Zinc EPA 2007 510 mg/kg 01/30/2019 Nitrate+Nitrite-Nitrogen EPA 3532 0.23 mg/kg 02/01/2019 Total Solids I%) SM 25406 2.63% 01/21/2019 pH SM 4500 H s 6.28 units 01/29/2019 Ammonia Nitrogen SM 4500 NH3 c 4940 mg/kg 01/23/2019 Total Kjeldahl Nitrogen (TKN) SM 4500org8 32900 mg/kq 01/23/2019 Total Phosphorus SM 4500 P F 2510 mg/kg 01/30/2019 Mercury SW8467471e 2.66 mg/kg 01/26/2019 Comment: Results, except pH reported on a dry weight basis. pH reported on an as received basis. Revised to remove hold time notifications, no hold time for sludge matrix. Reviewed by: Report N. 20 19-0104 9 Page I of 1 ;c ❑ n c a C c Q ' (� N is Qj R 3 ❑ TL Z ❑ �9 p a U I a = w - R � � W O Q U Y z d 01 O o F U U m m m m m a � - V v a IR � N n W— N — f- 13 h N ✓J c. N VI in OV O OO V (l Nv V7N V)a�_ v)v VJN hN Nv V)v VJ c� V'a� •- P p d N a J E T _ \o F - w o J V) o' m o 6 \n — N - Q p 2 ❑ H h cd OI IN N N CI ❑ Y Z p p ry Y K m M m } m m m z m g s m 5 z o; N F h 0 0 m Q N N !J N O N IO V N V V N C N M U 0 N I 0 z z - a 2 (j m rt v io � n c. I I z o v N) C t E m m ii (o v u N C YJ m S o Q W W Z W Nw tq wv tqw NN rqw l9v tqv VJw Nv Vim Nw v)w w w w v v v w v c � L NO N N N N N N N m m ry iD U O O O O Cl O U O rn -L m S J S m }S W 0 N I e e ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTP Name: Oak Island WWTP NPDES Number: W00005790 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) L1Alt B (Alk Treatment) LiAlt. C (Prior Testing)❑ AIt.D ('No Prior Test) LlProcess to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ heat Drying ❑ IIeat Treatment ❑ Thermophilic ❑ Leta Ray ❑ GantmaRay ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density ❑ Alt. (2) Process to SiDtificantly Reduce Pathogens ❑ If applicable to alternative performed (Class 13 only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 27 1 Air Drying ❑ Composting ❑ JAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class Tor Class B) complete the following monitoring data: Parameter Allowable Level in Sludge PathogDensity wn er oen 6xcee- d, Frequency of Analysis Sample 'type - na yuca Tech - nioue Miniinurr Geo. Mean Maxiinurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFI] 1000 mpn per gram oftotal solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight Vector Attraction Reduction (15A NCAU UTI .IIU7) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ I Alt. 4 (Spec. Oz uptake) L1 Alt. 5 (14 -Day Aerobic) ❑ Alt, 6 (Alk. Stabilization rJ Alt 7 (Drying -Stable) ❑ I Alt. 8 (Drying - Unstable) L,Alt. 9 (Injection) LJAlt. 10 (Incorporation) No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) �l "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the "This my acco system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Name and Title (type or print) Signature Of reparer* Land Applier Name and Title (if applicable)(type or print) 2/7/19 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 21'.1102 (26) DENR FORM PVRF 02T (12/2006) Q) 0 C13 W 3 O LO_ r N m y LU2 J Q co o M O it 0 2 %I HIIIIIIIIIIIIIIIII u COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 2, 2018 Summerhouse 1.33 % Solids 6.7 Of Permit No. WQ0029945 Parameter %Mg/Kg Dry Weight x 10,000) "Pounds/Dry Ton (Mk/,Kg(Mk/,Kg x 0.002) Nitrogen (TKN) 5.630 56,300.000 112.600 Phos horus 4.100 41,000.000 82.000 Potassium 0.655 6,550.000 13.100 PAN (injected)* 2.113 21,131.600 42.263 PAN surface)* 1.813 18,131.600 36.263 Ammonia Nitrogen 0.600 6.000.000 12.000 Calcium 2.880 28.800.000 57.600 Calcium Carbonate Eq. --- --- --- Magnesium 3,570.000 7.140 Sodium 4,800.000 9.600 Sulfur Nitrate N / Nitrite N --- 41.600 0.083 Barium --- --- --- Chloride --- --- --- 11,011 --- --- --- Muminun --- 5.460.00 10.920 Arsenic --- 37.70 0.075 Cadmium --- 37.70 0.075 Chromium --- 76.700 --- Copper 158.00 0.316 Lead --- 37.70 0.075 Mercury 1.28 0.003 Mol ybdcnum 37.70 0.075 Nickel 50.10 0.100 Selenium 37.70 0.075 zinc --- 2,790.00 5.580 Environmental Chemists # 2018-00042 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Anunonia N) i- Ammonia N + Nitrate N +Nitrite N — %PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N i- Nitrite N= % PAN Note: Constituents N.D. (Not Defected) or <detection limits are listed as detection limits for calculation purposes. Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Lab ID Sample ID: 18-00116 Site: Sludge Test Chlordane Endrin Heptachlor Heptachlor epoxide Lindane Methoxychlor Toxaphene 1,4 -Dichlorobenzene (TCLP) 2,4,5 -Trichlorophenol (TCLP) 2,4,6-Trichlorophenol(TCLP) 2,4-Dinitrotoluene (TCLP) Cresol (TCLP) Hexachloro-1,3-butadiene (TCLP) Hexachlorobenzene(TCLP) Hexachloroethane (TCLP) m + p -Cresol (TCLP) Nitrobenzene (TCLP) o-Cresol(TCLP) Pentachlorophenol (TCLP) Pyridine (TCLP) 2,4,5 -TP 2,4-D 1,1-Dichloroethylene 1,2-Dichloroethane Benzene Carbon Tetrachloride Reehtl #" 9018-00049 Environmental Chemists, Inc. 6602 Windmill 1Nav, t-Vilnlington, NC 28-105 „ 910.192.0223 Lab 410.392.442.4 Far 71013ot�serhtnm Road, N1antvo, NC 27954 0 252.473.5702 Lab/Pa.x 258-A Wilmington I-Lighway, Jacksonville, NC; 28540 0 910.317.5841 Lab/F,)\, inli)(r,environmcnudchemi;tsrnm ................ .. . Date of Report: Feb 01, 2018 Customer PO #: Customer ID: 08100092 Report#: 2018-00042 Project ID: Summerhouse Collect Date/Time Matrix 1/2/2018 11:26 AM Solid/Sludge Method SW 846 Method 8081 B/3510 SW 846 Method 8087 B/3510 SW 846 Method 80816/3510 SW 846 Method 8081 B13510 SW 846 Method 8081 W3510 SW 846 Method 8081813510 SW 846 Method 80810/3510 SW 846 method 8270/3510 SW 646 method 8270/3510 SW 846 method 8270/3510 SW 848 method 8270/3510 SW 846 method 8270,3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 87.70/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 82.70/3510 SW 846 method 8270/3510 SW846 Method 8151A SW846 Method 8151A SW846 Method 8260/5030 SW846 Method 8260/5030 SW846 Method 8260/5030 SW846 Method 8260/5030 Results Sampled by Mike Lutz Date Ana <0.05mg/L 01/18/2018 <0.0005mg/L 01/18/2018 <0.0005 mg/L 01/18/2018 <0.0005 mg/L 01/18/2018 <0.0005mg/L 01/18/2018 <0.0005mg/L 01/18/2018 <0.05 mg/L 01/18/2018 <0.050mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050 mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050 mg/L 01115/2018 <0.050mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.050 mg/L 01/15/2018 <0.250mg/L 01/15/2018 <0.050mg/L 01/15/2018 <0.003mg/L 01/18/2018 <0.003mg/L 01/18/2018 <0.01 mg/L 0111 0/2 01 8 <0.01 mg/L 01/10/2018 <0.01 mg/L 01/10/2018 <0.01 mg/L 01/10/2018 Environmental Chemists, Inca 6602 Windmill Way, lh/ihnin74h71L N( 28W5 e 910.392.0223 Lab , 910,392.4421 Pax 710 llowtserrown Fuad, Manlco, NC 27954 2:92.4735702 l.ah/ Fnx 25:3-A IAli Imington I-Iil,hwny, )ecksomi I Ic, NC 28540 � 910.347.5813 Lab/Pas inIi)hl; cnci ron men la IcheIII i., I,taom -.1-1 1. ..-_.... ,. _..... .............._ Onslow Water & Sewer Authority Date of Report: Feb 01, 2018 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID; 08100092 Attention: Todd Roberts Report #: 2018-00042 Project ID: Summerhouse Chlorobenzene SW846Method 8260/5030 <0.01 mg/L 01/10/2018 Chloroform SW846 Method 826015030 <0.01 mg/L 01/10/2018 Methyl ethyl ketone SW846Method 8260/5030 <0.05mg/L 01/10/2018 Tetrachloroethylene SW846Method 8260/5030 <0.01mg/L 01/10/2018 Trichloroethylene SW846Method 8260/5030 <0.01 mg/L 01/10/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 01/10/2018 RCI EPA 200.7 <37.7 mg/kg 01/10/2018 Cyanide EPA 335.4 <0.025 mg/kg 01/08/2018 Sulfide SM 1.500 S D 0.21 mg/kg 01/08/2018 Ignitability SW 646 method 1010 >212 OF 01/19/2018 Sludge Residuals Aluminum EPA 200.7 5460 mg/kg 01/10/2018 Arsenic EPA 200.7 <37.7 mg/kg 01/10/2018 Cadmiurn EPA 200.7 <37.7 mg/kg 01/10/2018 Calcium EPA 2007 28800 mg/kg 01/08/2018 Chromium EPA 2007 76.7 mg/kg 01/10/2018 Copper EPA 200,7 158 mg/kg 01/10/2018 Lead EPA 200.7 <37.7 mg/kg 01/10/2018 Magnesium EPA 2007 3570 mg/kg 01/08/2018 Molybdenum EPA 2007 <37.7 mg/kg 01/10/2018 Nickel EPA 2.00 .7 50.1 mg/kg 01/10/2018 Potassium EPA 200.7 6550 mg/kg 01/08/2018 Selenium EPA 200.7 <37.7 mg/kg 01/10/2018 Sodium EPA 200.7 4800 mg/kg 01/08/2018 Zinc EPA 2007 2790 mg/kg 01/10/2018 Nitrate4Nitrite-Nitrogen EPA 353.2 41.6 mg/kg 01/10/2018 Total Solids (%) SM 2540 B 1.33% 01/03/2018 pH SM4500HB 6.70 units 01/08/2018 Ammonia Nitrogen SM 4500NH3 C 6000 mg/kg 01/11/2018 Total Kjeldahl Nitrogen (TKN) SIM 45000rgB 56300 mg/kg 01/11/2018 Reoort#'.: 2016-00042 .. Environmental Chemists, Ince ,r w S :.IF N,02 WindmiII Wav, V6lminglon, NC 28405 , 910.392,02-2 1 Lab , 910.392A 121 Prix ;, • - 71013owsertolc n Road, Mantco, NC 27951 ?52.4735702 Lib/F,iN si= 255 :A Wilmington FiigMeny,),w),som iIle, ;NC 28 i4 , 910347.5543 Lab/1@u ANALYTICAL & CONSULTING CHEMISTS in low cm irnnmewalchclmstsxo nl Onslow Water & Sewer Authority Date of Report: Feb 01, 2018 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2018-00042 Project ID: Summerhouse Total Phosphorus SM4500P1: 41000 mg/kg 01/11/2018 Mercury SW8467471B <1.28 mg/kg 01/05/2018 TCLP Metals Arsenic EPA 200.7 <1.0mg/L 01/15/2018 Barium EPA 2007 <1.0mg/L 01/15/2018 Cadmium CPA 200.7 0.0mg/L 01/15/2018 Chromium EPA 200.7 <1,0mg/L 01/15/2018 Lead EPA 200.7 <1.0mg/L 01/15/2018 Selenium EPA 2003 <1.0mg/L 01/15/2018 Silver EPA 200.7 <1.0 mg/L 01/15/2018 Mercury EPA 245'1 <0.0020mg/L 01/14/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00117 Site: sludge #1 1/2/2018 11:27 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) sM2540G 1.24% 01/03/2018 Fecal Density SM 92210 E MPN 24 hr 503 193549 MPN/g 01/03/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00118 Site: sludge #2 1/2/2018 11:28 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 G 1,28% 01/03/2018 Fecal Density SM92210EMPN 24 hr 503 101563MPN/g 01/03/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00119 Site: sludge #3 1/2/2018 11:29 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SrA 2540 G 1.31 % 01/03/2018 Fecal Density SM 9221C E MPN 24 hr 503 99237 MPN/g 01/03/2018 Rep ri#- 2018.00042 Environmental Chemists, Inc. ��'�_ Q, 4 ® d `Fe, C+G021Nlnamill t1�<ty, 4Vi I minglon, NC 25145 , 9 10.3910223 J,,)[, < 910 392.4414 F,1x 71003 w set Lim n Road, M,m(oo NC 27954 >>Z. 173.5702 1_n1)/1 ax " � '25-A 4Vilmingi�al Ftighway, jacAsunwllr, N1C '.h.. 1(7 � 9 P 34 $N,3 Lab/Pax ANALYTICAL & CONSUL -TING CHEMISTS inlitiii;cmirinnnenl;dchcmisls.ann Onslow Water & Sewer Authority Date of Report: Feb 01, 2018 228 Georgetown Road Customer PO #: SM 0221C E MPN 24 hr 503 Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2018-00042 18-00121 Site: sludge #5 Project ID: Summerhouse Solid/Sludge Mike Lutz Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00120 Site: sludge #4 1/2/2018 11:30 AM Solid/Sludge Mike Lutz Test Method Results Date Total Solids (%) SM 2540 G 1.25% 01/03/2018 Fecal Density SM 0221C E MPN 24 hr 503 24000 MPN/g 01/03/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00121 Site: sludge #5 1/2/2018 11:31 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM2540G 1,11 % 01/03/2018 Fecal Density SM 92210EMPN 24fit 503 45046 MPN/g 01/03/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00122 Site: sludge #6 1/2/2018 11:32 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM2540G 1.27% 01/03/2018 Fecal Density SM 9221C E MPN 24 nr 503 70867 MPN/g 01/03/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-00123 Site: sludge #7 1/2/2018 11:33 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM2540G 1.32% 01/03/2018 Fecal Density SM 92210 E MPN 24 hr 503 83334 MPN/.q 01/03/2018 Comment: Sludge residuals, except pH, reported on a dry weight basis. Reviewed by: /a4(ee�ag Rewd # 20175.00042 J zo LL. V / � y C j V � E .♦ M 0 V.1 a Wr O O N ✓ t� LL O N� ap H31/AO U w p CC 4 r N 4 v N O olHx H04N .o. r M > `— > coNH U bOSZHcn U Jt 4 ,oH O Wtt ,�,'' N J IL J tl36WpN w m (� 4I to d) Z g 2 o iouleluo� (.L (� (.L C7 CL C7 0- M F z Q Q 4 f .wi n n. U U Z Z Q ae pejo — �... ...� wW W Q O N allsodwo� U U` U U U U' U C7 U U C7 U C� U z z Q C7 U C7 (.) C:7 ,moiO 4 0. C 4 1 U� UQ (QJ olAwus C) m a m Y a Li _ J o M c ? • U w `. iC W O� -MC m ✓� .2Cc a R ; �� 1 n •-s� (� 3 n ..... m m w N N O J ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) FacilityName: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 W WTP Name: Summerhouse W WTP NPDES Number: WQ0029945 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T.1 1061 - Please indicate Ievol "PhiP„Pd s"d P1�PYnPE: a P.o . nea. Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) D I Process to Further Reduce Pathogen ❑ If applicable to alternative performed (Class A onl , indicate "Proem to Farther Reduce Pathogens": Compost 01 Heat Di ' g ❑ Heat Treatment ❑ Thermo hitic ❑ Beta RaX 01 Gamma Re ❑ Pasteurization p Class B: AR. (1) Fecal Densi El All. (2) Process to Si ificantl Reduce Pntho ens ❑ If ap licable to alternative Performed (Class B only) indicate "Process to Significantly Reduce Pathogens"; Lime Stabilization ❑ Air D iu , ❑ Com ostin ❑ Acrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed Class A or Class B complete the [lowing monitorin data: Parameter Allowable Level in Sludge Be Pathogen Density um ero Cx�- Frequency of Anal ysis Sample Type Analytical Tech - Malle Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 24,000 74,261 193,549 MPN/g 0 Annual Grab SM92210E CFU 1000 mpn per gram of total solid (dry wei t Salmonella bactenal (in lieu of fecal coliform) ♦rn..4Ash—....A[...- 3 MPN per 4 grams total solid (dry weight) -----------••-••-•-•-.•�•...•. �..+.� ....tea. vv • .A ay.) - r1V=V ltrulWtc alll'rnaC1VC perlermeq: Alt. l (VS reduction) ❑ JAlt. 2 (40 -day bench) ❑ Alt. 3 (30 day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Ait 7 (Drying- Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (injection) El Alt. 10 (Incorporation) +❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) mi ••t certtty, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1 106 and the vector attraction reduction requirement in 15A NCAC 02T.1 107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the YP/...i YP,sfnnM I A...P "c.a..umuwoa nas vuen mane unuer my atrectlon ano supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Lutz, ORC Wesley Wooten, President Preparer Name and T' (ty or print) Land Appiier Nam' e-andjale (if applicable)(type or print) S ignkfure of Preparers Date Signature of Land Applier (if applicable) Date 'Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T. 1102 (26) COASTAL FARMS & RESIDUALS, LLC W00034806 Summerhouse Date Fecal Coliform MPN per gram Log 01/02/18 193,549 5.2868 01/02/18 101,563 5.0067 01/02/18 99,237 4.9967 01/02/18 24,000 4.3802 01/02/18 45,046 4.6537 01/02/18 1 70,867 4.8504 01/02/18 1 83,334 4.9208 Total 34.0953 Average 4.8708 Geometric Mean74,261 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: May 15, 2018 Surf City W WTP 2.82 % Solids 6.73 pH Permit No. WQ000079.5 Parameter % Mg/KDryWeight x 70,000 ' Pounds[Dry Ton M /K x O.002 Nitrogen (f KN) 5.520 55,200.000 110.400 Phosphorus 0.403 4.030.000 8.060 Potassium 0.278 2.780.000 5.560 PAN (injected)* 1.795 17.947.000 35.894 PAN (surface)* 1.727 17.272.000 34.544 Ammonia Nitrogen 0.135 1,350.000 2.700 Calcium 4.320 43,200.000 86.400 Calcium Carbonate Eq. --- --- --- Magnesium -- 2.790.000 5.580 Sodium --- 7.160.000 14.320 Sulfur --- --- --NitrateN/NitriteN Nitrate N / Nitrite N --- 442.000 0.884 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 3.440.00 6.880 Arsenic 17.70 0.035 Cadmium --- 17.70 0.035 Chromium --- 22.000 0.044 copperr 461.00 0.922 Lead --- 17.70 0.035 Mercury 0.851 1 0.002 Molybdenum 17.70 0.035 Nickel 17.70 0.035 Selenium 17.70 0.035 Zinc --- 3.040.00 6.080 13nvironmcntal Chemists N 2018-07724 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rale)(iKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(fKN-Ammonia N) + (0.5)(Annnonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.U. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. g ? $? 6602 Windmill AVaµ VTilmin, ton, N( 2810; )ttl 39'.02231..ab a 910.302 1324 Rix 710 Bow rn t na n Road, Mantco, NC 27934 a 25)2.47/157702 Lib/Fax . 255-A Wilmini;ton Itighw avl )acksonv ille, NC 211540 ^ 9107 34/ S&73 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS inli)(a environmentnlchemisU.com Lewis Farms & Liquid Waste, INC. Date of Report: Jun 25, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2018-07724 Project ID: Surf City Lab ID Sample ID: Collect Dateffime Matrix Sampled by 18-19323 Site: Sludge 5/15/2018 1:00 PM Solid/Sludge Client Test Method Results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.03mg/L 05/25/2018 Endrin SW 846 Method 8081B/3510 <0.0005 mg/L 05/25/2018 Heptachlor SW 846 Method 80818/3510 <0.0005 mg/L 05/25/2018 Heptachlor epoxide SW 846 Method 80818/3510 <0.0005mg/L 05/25/2018 Lindane SW 846 Method 80818/3510 <0.0005 mg/L 05/25/2018 Methoxychlor SW 846 Method 80818/3510 <0.0005mg/L 05/25/2018 Toxaphene SW 846 Method 80816/3510 <0.05 mg/L 05/25/2018 1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050mg/L 05/25/2018 2,4,5 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 2,4,6 -Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0.050mg1L 05/25/2018 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 m + p -Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 o -Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 05/25/2018 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/25/2018 2,4,5 -TP SW846 Method 8151A <0.003mg/L 05/29/2018 2,4-D SW846 Method 8151A <0.003mg/L 05/29/2018 1,1-Dichloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Benzene SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Report #: 2018-07724 Page 1 of 4 Environmental Chemists, Inc. 6602 \Vindtnil I /lay, Wilmington, NC 244 Cc. " 910192 022:1 Lab* ° 9103`42.-1424 Fax . �> 7Ili 1kn+selioty load, A4enteo S'C-27 54 252,471702Lab/1'ix ...� 253-A bVilmingtoll lfighsaav, lac Lsonv111e, NC 28540 ° 920347.5893 Lab/ Fin ANALYTICAL & CONSULI ING CHEMISTS info<,z imlironmen[elclicmisu.conl Lewis Farms & Liquid Waste, INC, Date of Report: Jun 25, 2018 <0.05 mg/kg 8155 Malpass Corner Road Sulfide Customer PO #: <0.1 mg/kg Currie NC 28435 Reporting limit elevated due to matrix interference. Customer ID: 14020008 Attention: Wesley Wooten SW 846 method 1010 Report #: 2018-07724 05/30/2018 Sludge Residuals Project ID: Surf City Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Chloroform SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Methyl ethyl ketone SW846 Method 8260/5030 <0.05 mg/L 05/25/2018 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Trichloroethylene SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 Vinyl Chloride SW846 Method 8260/5030 <0.01 mg/L 05/25/2018 RCI Cyanide EPA 335.4 <0.05 mg/kg 05/21/2018 Sulfide SM4500SD <0.1 mg/kg 05/21/2018 Reporting limit elevated due to matrix interference. Ignitability SW 846 method 1010 >212 OF 05/30/2018 Sludge Residuals Aluminum EPA 2007 3440 mg/kg 06/05/2018 Arsenic EPA 200.7 <17.7 mg/kg 06/05/2018 Cadmium EPA 2007 <17.7mg/kg 06/02/2018 Calcium EPA 2007 43200 mg/kg 05/27/2018 Chromium EPA 200.7 22.0 mg/kg 06/05/2018 Copper EPA 2007 461 mg/kg 06/05/2018 Lead EPA 200.7 <17.7mg/kg 06/05/2018 Magnesium EPA 200.7 2790 mg/kg 05/27/2018 Nickel EPA 200.7 <17.7 mg/kg 06/05/2018 Potassium EPA 200.7 2780 mg/kg 06/01/2018 Selenium EPA 200.7 <17,7mg/kg 06/03/2018 Sodium EPA 2007 7160 mg/kg 05/31/2018 Zinc EPA 2003 3040 mg/kg 06/02/2018 Molybdenum EPA 200.8 <17.7mg/kg 06/18/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 442 mg/kg 06/07/2018 Total Solids (%) SM 2540 s 2.82% 05/17/2018 pH SM 4500 H 6 6.73 units 05/23/2018 Ammonia Nitrogen SM 4500 NH3 C 1350 mg/kg 05/24/2018 Report #.. 2018-07724 Page 2 of 4 a-. Environmental Chemists, Inc. 4' 6602 VA ndil ill 5 o%, l%flminglon, NC�28405 e 01 0,312.0223 Lal) ' 510.3914-124 rax < 710 Rm;>erto+cn Road, Mantu,,;NC 2795-1 ° 2h2.47I57021.aI01 ax 255-A lhihninl ton I lg0i%v ay, Jaclisunvillu, N(1 28510 ' v10 S4 7.5843 Lal,/Fax ANALYTICAL & CONSULTING CHEMISTS info;a;cnvinamlcnt;tichemi5tscpm Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Total Kjeldahl Nitrogen (TKN) Total Phosphorus Mercury TCLP Metals Arsenic Barium Cadmium Chromium Lead Selenium Silver Mercury Date of Report: Jun 25, 2018 Customer PO #: Customer ID: 14020008 Report #: 2018-07724 Project ID: Surf City SM 4500 Org B 55200 mg/kg 05/24/2018 SM 4500 P F 4030 mg/kg 05/24/2018 SW8467471B 0.8510 mg/kg 05/31/2018 EPA 200.7 <1.0 mg/L 06/05/2018 EPA 200.7 <1.0 mg/L 06/02/2018 EPA 2003 <1.0 mg/L 06/02/2018 EPA 200.7 <1.0 mg/L 06/05/2018 EPA 200.7 <1.0 mg/L 06/05/2018 EPA 200.7 <1.0 mg/L 06/06/2018 EPA 200.7 <1.0 mg/L 06/06/2018 EPA 245.1 <0.0002 mq/L 06/07/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-19324 Site: 1 5/15/2018 1:10 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.76% 05/17/2018 Fecal Density SM 9221C E MPN 24 hr 503 39856 MPN/g 05/16/2018 Lab ID Sample ID: 18-19325 Site:2 Test Total Solids (%) Fecal Density Lab ID Sample ID: 18-19326 Site:3 Test Total Solids (%) Fecal Density Collect Date[Time 5/15/2018 1:11 PM Method SM 2540 G SM 9221C EMPN 24 hr 503 Collect DatelTime 5/15/2018 1:12 PM Method SM 2540 G SM 9221C E MPN 24 or 503 Matrix Sampled by Solid/Sludge Client Results Date Analyzec 2,81% 05/17/2018 11744 MPN/g 05/16/2018 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2.67% 05/17/2018 4869 MPN/g 05/16/2018 Report #:: 2018.07724 Page 3 of 4 h Environmental Chemists, Inco 3' 4 A s 6:602 b0indnmII %a)-, VV II a gton, W 28405 ` 910 §9'.0223 Lab ' Q 1031014,121 Pax 110 Bo1veert(m n Road, Mantel), N( 2795-1 ' 252,4733702 Leib/Par 255-A Wilmington I I } mn-eV, Iack,onc iI Ic, NC 28510 ° 910347.5843 Ln I, /Fax ANALYTICAL & CONSULTING CHEMISTS ill to", em i ronmcn t OlclCntisls.Coilt Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Lab ID Sample ID: 18-19327 Site:4 Test Total Solids (% Fecal Density Lab ID Sample ID: 18-19328 Site:5 Test Date of Report: Jun 25, 2018 Customer PO #: Customer ID: 14020008 Report #: 2018-07724 Project ID: Surf City Collect Date/Time 5/15/2018 1:13 PM Method SM 2540 G SM 9221C E MPN 24 hr 503 Collect Date/Time 5/15/2018 1:14 PM Method Total Solids (%) SM 2540 G Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 18-19329 Site: 6 5/15/2018 1:15 PM Test Method Total Solids (%) SM 2540 G Fecal Density SM 0221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 18-19330 Site: 7 5/15/2018 1:16 PM Test Method Total Solids (%) SM 2540 G Fecal Density SM 9221C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2,69% 05/17/2018 11525 MPN/g 05/16/2018 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2.78% 05/17/2018 11871 MPN/g 05/16/2018 Matrix Sampled by Solid/Sludge Client Results Date Analvzec 2.81% 05/17/2018 28114 MPN/g 05/16/2018 Matrix Sampled by Solid/Sludge Client Results Date Analyze( 2.66% 05/17/2018 17294 MPN/9 05/16/2018 Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received basis. ' Reviewed by: nko Vc, Qpp) k�j Report #: 2018-07724 Page 4 of 4 0 N 1 N Z M O l L 0 d w 1 L d O y o m � � L r � FFE M 09 C O 7 6 a A y y II y � 3 di ? c c �v U_ N 4 O 0 z v a a O G J ft 6 LL7 a ? O I'm T Z� c� V/ Z, N U Q LL F C F jr � W 0 U LLO U Z =a J= F z Q Za O W ZILL J U J po 0 fid. U Z w /' o Z z W ui zz z O F- O W ¢ I.- I— O z a a d O x o 51 m 1 l L 1 L d ui zz z O F- O W ¢ I.- I— O z a a d O x o 51 m m O d o m � � \ FFE M O 7 6 a A y y II y �v a J R � U I I n T tl3H10 11 11 = OIH1 k �' m O QHOVN i CONH W WbOSA 3NON n I a a �a ti HRIaWnN .�,� a a V- �(r- .^ V, a, N m E VBw F aupo140 U� t0 � i Q (0 10 d) a (9 a a a 0 a 0 a C7 a C7 a C7 a C7 a C7 �eUlBiuop i gei.O ao U C7 U C7 U C7 U C7 U C7 U U' U U' U 0 U (7 a7lsodwo0 W1 oldwu$ Z i a T m E < F— L W C O c 6 d F- 0 O U N d t � G ^j ti n N F- m O ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Nante: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTP Name: Surf City WWTP NPDES Number: W00000795 Monitoring Period: From 1/1/2018 To 12/31/2018 T Pathogen Reduction (15A NCAC 021'. 1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timehernp) ❑ 1 Alt 13 (Alk'hivalment)U I AIL C (Prior Testing) El AIt.D (No Prior Teso ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 _ Heat Drying ❑ Heat Treatment 0 1 1'henno)bilic L7 Beta Ray 01 Gamma Ray ❑ Ptlsteurirtuiou ❑ Class B: jAlt. (1) Fecal Density rJ Alt. (2) Process to Significantly Reduce Pathogens C1 11'applicable to alternative performed (Class 11 only) indicate "I'vocess to Significantly Reduce Pathogens": Lime Stabilization LJ AiiDrying ❑ Com iostin, 0 Acrobic Digestion U Anaerobic Di estion Ll If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameterin Allowable Level Sludge Pathogen Density uu' ie1 o !icnce- cos Prcquency ol'Analysis Sample Type Analytical ime Minimun Geo. Mean Maximun Units Fecal Coliform 2 x 10 to the 6th power Pei, gram of total solids MPN 4,869 14,746 39,856 MPN/g 0 Annual Grab SM922)a` (TU 1000 mpn per grade oftoa)solid (dry wei lo) Salmonella bacteria (in lieu of fecal coliform)) I 3 MPN per4 grains total solid(d)y weight) VCetOr AttraCtl0u Reduction (1bA IN CAU U21 -.I IUV) - Please indicate alternative PeriormeU: !Alt.] (VS reduction) Ll Alt. 2 (40 -day bench) [] AIt.3 (30 -day bench) tj] Alt. 4 (Spec. O> uptake) El '.Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization [j Alt 7 (Drying -Stable) (_] Alt. S (Drying -Unstable) Lj Alt. 9 (Injection) 0 Alt. 10 (incorporation) E INo vector atu'action reduction alternatives were.perfoimed 0 CERTIFICATION STATEMENT (please check tate appropriate statement) LI 9 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." CJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in ISA NCAC 021'.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Smith, ORC Prepare�r N`aamm_e and Title (type poi- print) Signature of Preparer* Wesley Wooten, President Land Applier Name and Tit pplicabte)(type or print) 101 _ 2/7/19 Date Sign Stu re of Lal App I ier (i f app I icable) Date *Pieparcr is defined in 40 CFR 1'erl 503.9(x) and 15A 1vCA(.2T.1102(26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS WQ0000455 Surf City W WTP Date Fecal Coliform MPN per gram Log 05/15/18 39,856 4.6005 05/15/18 11,744 4.0698 05/15/18 4,869 3.6874 05/15/18 11,525 4.0616 05/15/18 11,871 4.0745 05/15/18 28,114 4.4489 05/15/18 17,294 4.2379 Total 29.1807 Average 4.1687 Geometric Mean 14,746 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 2, 2018 Swausboro 2.55 % Solids 5.82 pH Permit No. W00034806 Parameter I % Mg/Kg DryWeight (% x 10,000)S°1°1 Pounds7Dry Ton s (Mg/Kg(Mg/Kg x 0,002) Nitrogen JKN) 5.050 50,500.000 101.000 Phosphorus 4.100 41.000.000 82.000 Potassium 0.326 3,260.000 6.520 PAN injected)* 2.730 27,299.000 54.598 PAN (Surface)* 2.436 24,364.000 48.728 Ammonia Nitrogen 0.587 5,870.000 11.740 Calcium 4.410 44,100.000 88.200 Calcium Carbonate 6 . --- --- --- Magnesium 2,050.000 4.100 Sodium 4,780.000 9.560 Sulfur --- --- --- Nitrate N / Nitrite N --- 8,040.000 16.080 BILLium _- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 6.750.00 13.500 Arsenic 19.60 0.039 Cadmium --- 19.60 0.039 Chromium --- 19.600 --- Copper --- 400.00 0.800 Lead --- 19.60 0.039 Mercer --- 1.69 0.003 M01-) enunn 19.60 0.039 Nickel 19.60 0.039 Selenium --- 19.60 0.039 Zinc --- 4.630.00 9.260 1',imionmental Chemists tt 2018-00045 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Ratc)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N _ % PAN Surface Application: (Mineralization Rate)(TKN-Amnnonia N) + (0.5)(Ammonia N) + Nitrate N + MIT ite N = % PAN Note: Constituents N.D. (Not Detected) or<detection limits are listed as detection limits for calculation proposes. 85 840 57 7,5 420 100 Total Solids (%) Fecal Density Lab ID Sample ID: 18-00132 Site: Fecal # 5 Test Total Solids (%) Fecal Density SM 2540 G 2.79% 01/03/2018 SM 92210 E MPN 24 hr 503 1254481 MPN/g 01/03/2018 Collect DatelTime Matrix Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM 2540 G SM92210EMPN 24hr503 2.68% 01/03/2018 2014926 MPN/g 01/03/2018 Re(wn II . 2016-00045 Vaoe 1 of 3 Environmental Chemists, Inc (,b02 bVindIII tl111 w, Wil Tilington, NC 28405 = 91039),02_3 1 tb 910 3 ° 4-421 Fax 710 Bm% soi town Road, Manteo, NC 42F,12"5 �' 1)10.3 17 A Wthnm ton I Ii 11c. a\,, Jacksonvi IIe, \C40 5813 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS illfo a cnvironmenl:ddiemisucom Onslow Water & Sewer Authority Date of Report: Jan 18, 2018 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2018-00045 Project ID: Swansboro WWTP Lab ID Sample ID ^�W m m Collect DatelTime MatrixMY M Sampled by WA 18-00127 Site: Fecal # 1 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Test Method Results Date Analyzed Total Solids (%) SM2540G 2,78% 01/03/2018 Fecal Density SM 9221C E MPN 24 hr 503 863310 MPN/q 01/03/2018 Lab ID Sample ID. Collect Date/Time Matrix Sampled by 18-00129 Site: Fecal # 2 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Test Method Results Date Analyzed Total Solids (%) SM2540G 2.71 % 01/03/2018 Fecal Density _...__ _._-. .. SM 9221 C E MPN 24 hr 503 1291513 MPN/q 01/03/2018 Lab ID Sample ID: _.__ . .___._ _-__...._-_....-- ---._. ._-.--- ---------- _..___._.-___. Collect Date/Time Matrix Sampled by 18-00130 Site: Fecal # 3 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Test Method Results Date Analyzed Total Solids (%) SM2540G 2.60% 01/03/2018 Fecal Density SM 92210 E MPN 24 hr 503 846154 MPN/g 01/03/2018 Lab ID Sample ID: ___-..-�. Collect Date/Time Matrix Sampled by 18-00131 Site: Fecal # 4 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Test Method Results Date Analvzed Total Solids (%) Fecal Density Lab ID Sample ID: 18-00132 Site: Fecal # 5 Test Total Solids (%) Fecal Density SM 2540 G 2.79% 01/03/2018 SM 92210 E MPN 24 hr 503 1254481 MPN/g 01/03/2018 Collect DatelTime Matrix Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM 2540 G SM92210EMPN 24hr503 2.68% 01/03/2018 2014926 MPN/g 01/03/2018 Re(wn II . 2016-00045 Vaoe 1 of 3 Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Lab ID Sample ID: 18-00133 Site: Fecal # 6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 18-00134 Site: Fecal # 7 Test Total Solids (%) Fecal Density Date of Report: Jan 18, 2018 Customer PO #: Customer ID: 08100092 Report #: 2018-00045 Project ID: Swansboro WWTP -&ctDateftime Matrix � Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM2540G 2,82% 01/03/2018 SM 9221C E MPN 24 hr 503 1914894 MPN/g 01/03/2018 _____.___._.....---....__..__...__.__-------- .-------- .—--- --_--- Collect Date/Time Matrix Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM 2540 G SM 922.1C E MPN 24 hr 503 2.72% 01/03/2018 808824 MPN/g 01/03/2018 Report #:'. 2018-00045 pane 9 nr 3 Environmental Chemists, Inca r ((,02 Windmill tVa °, Wilmington, NC 28105 , 910 3920223Lab - 910342 44241-'4.,, 710 Bm% ortolan Read Mcmwo, NC 27954 252.=b7 v0) Lab/) ix :55-AWrlmmglonf-L„h��ay, laJ:6wnc I Ile, N( )840 9711W70833 Lab/FaA ANALYTICAL & CONSULTING CHEMISTS InIB!gy:environmCnla lchL'mistscatu Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Lab ID Sample ID: 18-00133 Site: Fecal # 6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 18-00134 Site: Fecal # 7 Test Total Solids (%) Fecal Density Date of Report: Jan 18, 2018 Customer PO #: Customer ID: 08100092 Report #: 2018-00045 Project ID: Swansboro WWTP -&ctDateftime Matrix � Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM2540G 2,82% 01/03/2018 SM 9221C E MPN 24 hr 503 1914894 MPN/g 01/03/2018 _____.___._.....---....__..__...__.__-------- .-------- .—--- --_--- Collect Date/Time Matrix Sampled by 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Method Results Date Analyzed SM 2540 G SM 922.1C E MPN 24 hr 503 2.72% 01/03/2018 808824 MPN/g 01/03/2018 Report #:'. 2018-00045 pane 9 nr 3 y Environmental Chemists, Inc 0602 VJindliulI W3v, wih, inInon nuc 7110 9 0,392 0223 1,ab 1,a 970. 192.442 t F0\ 1��;,�� ":�v` >i> 710 Bo t x rtm\ n Rod Mantc N("7954 °.7 47 5702 1. tb/I is :�-"d -A l4 ilntmg(oli iity,htay, )acI som ill _, NC 25 -7U 910 4!i Sd3 i ab/bar ANALYTICAL & CONSULTING CHEMISTS info,q emironnicn4i I, heiwsts.com Onslow Water & Sewer Authority Date of Report: Jan 18, 2018 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2018-00045 Project ID: Swansboro WWTP Lab ID Sample ID: w% _ Collect Date/Time Matrix Sampled by w 18-00135 Site: Sludge 1/2/2018 10:15 AM Solid/Sludge Josh Meadows Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 2007 6750 mg/kg 01/10/2018 Arsenic EPA 2007 <19.6mg/kg 01/10/2018 Cadmium EPA 2003 <19.6mg/kg 01/10/2018 Calcium EPA 200.7 44100 mg/kg 01/08/2018 Chromium EPA 200.7 <19.6mg/kq 01/10/2018 Copper EPA 2007 400 mg/kg 01/10/2018 Lead EPA 2007 <19.6mg/kg 01/10/2018 Magnesium EPA 200 7 2050 mg/kg 01/08/2018 Molybdenum EPA 200.7 <19.6mg/kg 01/10/2018 Nickel EPA 200.7 <19.6mg/kg 01/10/2018 Potassium EPA 2007 3260 mg/kg 01/08/2018 Selenium EPA 200.7 <19,6mg/kg 01/10/2018 Sodium EPA 2007 4780 mg/kg 01/08/2018 Zinc EPA 200.7 4630 mg/kg 01/10/2018 Nitrate+Nitrite-Nitrogen EPA363.2 8040 mg/kg 01/10/2018 Total Solids (%) SM 2540 B 2.55% 01/03/2018 pH SM 4500 H B 5.82 units 01/08/2018 Ammonia Nitrogen SM 4500N113C 5870 mg/kg 01/11/2018 Total Kjeldahl Nitrogen (TKN) SM 45000rgB 50500 mg/kg 01/11/2018 Total Phosphorus sM4500Pr- 41000 mg/kg 01/11/2018 Mercury ..._ .._.... _ _,___. Sw8467471B _.__.__._ 1.69 mg/kg 01/05/2018 ....___..,_ _.._._ , . _ . _ .__... _. _.... _. _... -------- ----- Comment: Sludge residuals, except pH, reported on a dry weight basis. _- . _ ... . .......... Reviewed by: XVWIL Repot d.' 2018-00045 Pane 3 of 3 }§ ® \ « - Z § ~ { ..� \ e;! )^ ~f z w 0 E 1 ® HaHio / ƒ @ e § »,2 �cn J 0cl $ } CC m \; § « » / \ ) ®® n\ : %BNON & )�IOH \ / \^®� LL 2 fHRER� r o , M a e * \\�11 116W ,m ) § L) $«/ \}\, LLJ �J ecce zz= cyCODD e=o �; ( § z z o § a \§\((° ` o o=0 000 0 0=o%o=c= Gg°� \ \ƒS)S eS \»� CL E © m 2 m A M ) 0 )® f s } � & .G N \ \ 2 \ j r � % f § \J�§ w S / ) :3m S / E ƒ 7 / \ \ \ § ] G« 2 ? © w&/\E ANNUAL PATHOGEN AND VEC1'012 A'T'TRACTION 12F,DU(710N FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LL,C WQ Permit Number: WQ0034806 WWTPName: SwansbroWW'l'I NPDESNumber: WQ0023261 Monitoring Period: From 1/1/2018 'ro 12/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Lj I Alt B (Alk Treatment) FI I Alt C (Prion• Tcsting)LI V AILD (No Prior'I est) LJ I Process to Further Reduce Pathogenus L7 2 (40 -day bench) CI If applicable to alternative performed (Caass A only) indicate 'Process to Further Reduce Pathogens": Compost C7 Heat Drying 1-1 Meat Treatment [:] I I hernnu philie Beta Ray Li Gannna Ra L7 Pasteurization Li Class B: JAII. (I ) Fecal Density U Alt. (2) Process to Significantly Reduce Pathogens Ld If applicable to alternative performed (Class 13 only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization l Air Drying La Composting LJ lAciobic Digestion iJ Anaerobic Digestion LI If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Iy arameter Allowable Level in Sludgc Pathogen Density um er o Excec- Frequency of Analysis Sample 'hype —n a— a rc Tech - Ilicino Minimun Geo. Mean ivlaximun Unitsonro� Fecal Coliform 2x 10 to the 611) power per gram of total solids MIN 808,824 1,205,209 2,014,926 MPN/g I Annual Grab SM9221C& CFU 1000 ntpn per gram oftotal solid (city Weight) Salmonella bacteria (it) lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight Vector Attraction Reduction (15A NCAC 02T.1 107) - Please indicate alternative performed: Alt.l (VS reduction) V lAlt. 2 (40 -day bench) CI I Alt 3 (30 -day bench) ❑ jAlt. 4 (Spec. O, uptake) LI Alt. 5 (14 -Day Aerobic) iJ lAlt. 6 (Alk. Stabilization (;;1 jAlt 7 (Drying - Stable) IJ jAh. 8 (Drying - Unstable) [_l Alt. 9 (Injection) U JAIt. 10 (Incorporation) L�j INIo vector attraction reduction alternatives were performed LI CERTIFICATION STATEMENT (please check the appropriate statement) &.I "I certify, under penalty, of law, that the pathogen requirements in 15A NCAC 02T A 106 and the vector attraction reduction requirement in 15A NCAC 02T.1 107 have been met." L] "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Lutz, ORC Wesley Wooten, President Preparer Name and "Title (type or print) Land Applier Name and Title (if applicable)(type or print) 1/30/19 2/7/19 Signature of Preparer* Date Signature of Ond Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T. 1 102 (26) DENR FORM PVRF 02T (12/2006) CASTAL FARMS AND RESIDUALS, LLC WQ0034806 Swansboro Date Fecal Coliform MPN per gram Log 01/02/18 863,310 5.9362 01/02/18 1,291,513 6.1111 01/02/18 846,154 5.9274 01/02/18 1,254,481 6.0985 01/02/18 2,014,926 6.3043 01/02/18 1,914,894 6.2821 01/02/18 808,824 5.9079 Total 42.5674 Average 6.0811 Geometric Mean 1,205,209 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class S - Alternative 1 Pathogen for Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: August 3, 2018 The Cane 2.85 % Solids 7.27 pH Permit No. NC0057703 Parameter I p/o Mg/KgDryWelght I% x 10,000 Pounds/DryTon<i (M K x Od102 Nitrogen (PKN) 4.060 40,600.000 81.200 Phosphorus 5.670 56.700.000 113.400 Potassium 0.277 2,770.000 5.540 PAN (injected)* 1.285 11851.900 25.704 PAN surface)* 1.247 11468.400 24.937 Ammonia Nitrogen 0.077 767.000 1.534 Calcium 2.210 22.100.000 44.200 Calcium Carbonate Eq. --- --- --- Ma nesium 17,000.000 34.000 Sodium 1090.000 4.180 Sultiu Nitrate N / Nitrite N --- 135.000 0.270 Panum --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 97.100.00 194.200 Arsenic --- 19.10 0.038 Cadmium --- 19.10 0.038 Chromium -- 28.300 --- Co er --- 589.00 1.178 Lead --- 19.10 0.038 Merctay 0.526 0.001 Moly clonum 19.10 0.038 Nickel 19.10 0.038 Selenium 19.10 0.038 Zinc --- 1.340.00 2.680 Grvironmental Chemists, Inc. N 2018-11178 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Niu'ate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(PKN-Ammonia N) t (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Enviro.amert. Cal Chemists, Ine. lrs�F�'s�Y 3ta�°rf3 N(tl �\„h illA1t. 1h41i n ri,,� 1 `�It 1SI L 'U.1 r!"'i Pas 1 16 M 73,5702 Jb, VI I,Y1r lI„n1'1 rla<„oin it l.., Ai -18-'-!t ' 9111, '8�;3 I ab Inx ANALYHOAL& CONSUL_rING CI EMs11STS i:')11111: Lewis Farms & Liquid Waste, INC, Date of Report: Aug 03, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2018-11178 �k�1��C�e.VY1VTP Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28213 Site: Sludge 7/11/2018 3:00 PM Solid/Sludge Client Test _ Method Results Date Analyze( Sludge Residuals _ Aluminum EPA 2007 97100 mg/kg 07/27/2018 Arsenic EPA 200.7 <19.1 mg/kq 07/28/2018 Cadmium EPA 200.7 <19.1 mg/kg 07/26/2018 Calcium EPA 200.7 22100 mg/kg 07/19/2018 Chromium EPA 2003 28.3 mg/kg 07/26/2018 Copper EPA 200.7 589 mg/kg 07/26/2018 Lead EPA 200.7 <19.1 mg/kg 07/26/2018 Magnesium EPA 200.7 17000 mg/kg 07/19/2018 Molybdenum EPA 2003 <19.1 mg/kg 08/01/2018 Nickel EPA 2007 <19.1 mg/kg 07/26/2018 Potassium EPA 2003 2770 mg/kg 07/19/2018 Selenium EPA 200.7 <19.1 mg/kg 07/26/2018 Sodium EPA 200.7 2090 mg/kg 07/19/2018 Zinc EPA 2003 1340 mg/kg 07/26/2018 Nitrate+Nitrite-Nitrogen EPA 353,2 135 mg/kg 08/02/2018 Total Solids (%) SM 2540 s 2.85% 07/13/2018 pH SM 4600 H e 7.27 units 07/19/2018 Ammonia Nitrogen SM 4500 NH3 C 767 mg/kg 07/17/2018 Total Kjeldahl Nitrogen (TKN) SM 4500orge 40600 mg/kg 07/17/2018 Total Phosphorus SM 4500 P F 56700 mg/kg 07/18/2018 Mercury SW8467471E <0.526 mg/kg 07/16/2018 Report #:: 2016-11178 Page 1 of 3 r � r Enwronmental Chem sts, Inc. Kl.7r� ;r.�� C t� e Es- eek ��a �w� 1 II r1 nd it 1A �. cr i� � u1 a •1. �.( > n t ? I �1 l.' i I � F1: 1 Itoo, n ;IoIli II I v, l')r I, dW,v ' lU ull1 ANAIYII CAL F. MCNSLILTING CHEMISTS cni irznur nlal,,h`mkt"C nom Lewis Farms & Liquid Waste, INC. Date of Report: Aug 03, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2018-11178 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28214 Site: Sludge 7/11/2018 3:10 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM2540G 2.86% 07/13/2018 Fecal Density SM 9221C E MPN 24 hr 503 <630 MPN/g 07/12/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28215 Site: Sludge 7/11/2018 3:11 PM Solid/Sludge Client Test Method _ Results Date Analyzed Total Solids (%) SM 2540 G 2.81 % 07/13/2018 Fecal Density _ SM 9221C E MPN 24 hr 503 <641 MPN/g 07/12/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28216 Site: Sludge 7/11/2018 3:12 PM Solid/Sludge Client Test Method _ Results Date Analyzed Total Solids (%) SM 25406 2.69% 07/13/2018 Fecal Density SM 92210 E MPN 24 hr 503 <670 MPN/g 07/12/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28217 Site: Sludge 7/11/2018 3:13 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.73% 07/13/2018 Fecal Density SM 9221C E MPN 24 hr 503 <660 MPN/g 07/12/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28218 Site: Sludge 7/11/2018 3:14 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3,08% 07/13/2018 Fecal Density SM 922 1 C E MPN 24 hr 503 <585MPN/g 07/12/2018 Report #:. 2018 11178 paye 2 of 3 WNI Environmental Chemists, 111C. �.�� v� W �r�Skz1 a�r��J3 2i) ,� Ja,k )m llo, :A(_2bi 10 ,l ,�,�8 I u;l'�r ANAIYTiCAL & CONSULTING CHEMISTS irtri[cnciruomcntalcit� Ili i.G.c�ml Lewis Farms & Liquid Waste, INC. Date of Report: Aug 03, 2018 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2018-11178 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28219 Site: Sludge 7/11/2018 3:15 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 c 2.90% 07/13/2018 Fecal Density SM 9221 E MPN 24 hr 5o3 <621 MPN/g 07/12/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-28220 Site: Sludge 7/11/2018 3:16 PM Solid/Sludge Client Test _ Method Results Date Analyzed Total Solids (%) SM 2540 c 2.85% 07/13/2018 Fecal Density SM 92210 E MPN 24 hr 503 <632 MPN/g 07/12/2018 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ,/` Report# 2018-11178.-mmWT Paye 3of3 a N N T v Z h O c d u N o y � m y y E � aEi n r U � Q G 3 N y m E E_ a 0 c c 3 w v O N=® O LL� Z m 0 c O Z M � w U Z N "M 4 cl - -y Q Z 0 z C I u f 1 u 0 u n o°, L O N y E_ M � w O ?N I � h h � f- ♦- f - (A o O O O o O O 0 Z G 7 N N N N N N N N ' N N N N Z LL LL L LL LL L LL LLL LL G � H3N10 Y. I Z OIHl XX X X X X X m p v QHOVN U > CONH d N W VOSZH d I IDN HNON X i 838 Wf1N OI BVICD _E 1/bw C ou1ioIVO N I TO C) (0 o_ c7 a U a U CL C7 a (D a C7 d d Q) a c7 iaulluoujuOD 4a)E) ,o U (7 0 0 0 0 v C7 U CD U C9 U C7 U C7 U C7 allsodwop ad61 oldwu$ CL m E F H c a LA U v C O 1 iryp U C 1 ' w J d) U) N 'C3 m 1- Q � E N A 1 F 7 � L F+ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC W WTP Name: The Cape W W'IT Monitoring Period: From 1/1/2018 WQ Permit Number: W00034806 NPDES Number: NCO057703 To 12/31/2018 Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tines/temp) L71 Alt I3 (Alk'I'rcaunent)LI I Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ 1 Process to Further Reduc Patho en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens"; Compost LI I Meat Drying. ❑ Heat Treatment Cl I'll ermo Ihilic ❑ Beta Ray 01 Gamma Ra ❑ I Pasteurization U Class B: JAft. (1) Fecal Density Cl I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dr ine ❑ Com ostia, U Aerobic Digestion ❑ Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density unt er o F.xoee- erlcp�of Prequency Analysis Sample 'Type na y tca Tech - Minirruty Geo. Mean Max imun Units Fecal Coliform 2 x to to the Gth power per gram of total solids MPN 585 634 670 MPN/g 0 Annual Grab SM9221Cs CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) V CCT0r ATTI MCTI0I1 KeanCT1011 1AJA tVI.AT, U/ A .1 AU /1 - Ylease nuoicate alternative perierineu: Alt.I (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) FI jAlt, 4 (Spec. 0, uptake) U Alt. 5 (14 -Day Aerobic) L) jAh. 6 (Alk. Stabilization i] JAIt 7 (Drying - Stable) © 1 Alt. 8 (Drying -Unstable) ❑ Alt. 9 (injection) U JAIt. 10 (Incorporation) M JNo vector attraction reduction alternatives were performed Cl CERTIFICATION STATEMENT (please check the appropriate statement) Ll "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 021'.) 106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the reauirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Eric Youngs, ORC Wesley Wooten, President Preparer Name and Title (type or print)_ Land Applier Name and Title (if applicable)(type or print) L`� 2/15/19 4EIrepai �:j----q ....__....Signatuer* Date Signature of La/d Applier (if applicable) Date *Preparer is defined in 40 CFR Pail 503.9(1) and 15A NCAC 2T.] 102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC W00034806 The Cape W WTP Date Fecal Coliform MPN per gram Log 07/11/18 630 2.7993 07/11/18 641 2.8069 07/11/18 670 2.8261 07/11/18 660 2.8195 07/11/18 585 2.7672 07/11/18 621 2.7931 07/11/18 632 2.8007 Total 19.6128 Average 2.8018 Geometric Mean 634 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. 2018 APPLICATION SUMMARY 0 r FIELD APPLICATION SUMMARIES J] ) { w \ ) 7 / ) 3 - E2lmlE-:glt�itl,�! % ! 8 / § \ u $ » § � a / § \ u $ » § � a \ 2. 3§. tr a J a� k Ig E�\ � | k%� c @ a J � | ; ; -------------- ()/ �§) «a; u t °°$ � } \ 2 \ \ | � (}E�]�I�»:�:±:�� /•2 2 o § e 2 « f 3 g } § a a �] z 2A! <a§ } 3■E2 E a k�) 00 00 k/ v■\ def 22 2 ) �] )7§ K f CD / $ CD \ & 2 m k/ v■\ def 22 2 ) )7§ f u 2 Q \)\ . \ Em .a■ ® kCY\ )�$ 3 e� q u\ / E7w'#w(§)`)) ZD ƒ)|�#a:�|■l,��,�e 22 2 i \/\ $ } § § & �. #[m)®!®:/;t|}�2�° 4 t2 / ` a = 3 a = E f } 0 ) ) . 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