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HomeMy WebLinkAboutWQ0004095_Residual Annual Report 2018_20190212Mut/rien- Feeding the Future - January 25, 2019 NCDEQ-DWQ Information Processing Center 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: 2018 Annual Monitoring and Reporting Requirements Treatment and Land Application of Residuals Permit No: WQ0004095 PCS Phosphate Co., Inc.'- Aurora Division Beaufort County RE�EIVEDINCDFQIDWR FEB 1 2 2019 Non-pischar9e perm0ing Un1t As required by Specific Condition No. 8, Section IV, MONITORING AND REPORTING REOUIREMENTS of the above referenced permit, enclosed are three copies of the 2018 Annual Report for PCS Phosphate's Land Application Sites. Please do not hesitate to contact me at (252) 322-8283 should you require any additional information pertaining to this matter. /Sincerely, ILAD. Daniel Winstead III Senior Environmental Engineer Nutrien Enclosures PC: 12-05-01 L. D. Davis w/ attachments w/o attachment RF(`FII/Fp FFR 12 2019 INFOR OWR SECTION NATION PROCESSING UNIT 1530 NC Hwy 306 South, Aurora, NC USA 278% % nutrfen.com 1- Effective Jmuary 1, 2018, PCS Phosphate Co - -- _.. - emains the 1 �P Company, lac. is eo tadirect subsidiary of Nutri® Lid. PCS Phosphate Company, lac. r B� oPe+u�B ®city end permittee. PCS Phosphate, Aurora Residuals Land Application Program Permit No. WQ0004095 2015 Annual Report Table of Contents 1. Annual Land Application Certification Form: ACF 2. Annual Residual Sampling Summary Report Forms: RSSF 3. TCLP Statement 4. Annual Land Application Field Summary Form: FSF 5. Residual Analysis Lab Sheets 6. Annual Pathogen & Vector Attraction Reduction Form: RF 7. Pathogens & Vector Attraction Reduction Lab Sheets/Records 8. Soil Analysis ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0004095 County: Facility Name (as shown on permit): Land Application Operator: PCS Beaufort PCS Inc. Year: 2019 my, Inc. Phone: 252-322-8283 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ONo - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Total number of application fields in the it: I Two Total number of fields utilized for land application during the year: One Total amount of dry tons applied during the year for all application sites: 5.2 Total number of acres utilizes for land application during the year: 5.5 Part B - Annual Comolance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes 0 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mark Johnson, General Manager I/�-- i 1r_c OIq Permittee Name and Title (type or print) Signatur of Permittee Date Signature of Preparer* Date (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T Signature of Land Applier Date (if different from Permittee and Preparer) .1102 (26) DENR FORM ACF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00004095 Laboratory: 1) Facility Name: PCS Phosphate, Inc. Z) Residual Source WQ # or WQ0000889 3) NPDES #: 4) WWTP Name: PCS Phosphate, Inc. 5) Residual Analvsis Data Microbac ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of L Z wi ate DENR FORM RSSF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0004095 Laboratory: 1) Facility Name: PCS Phosphate Company, Inc. 2) Residual Source W00000889 3) NPDES # or WQ#: 4) WWTP Name: PCS Phosphate Company, Inc. 5) Residual Analvsis Data Microbac Laboratories, Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Z5 2ol to •Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) -_-- 111 ------- ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Z5 2ol to •Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) Monitoring Frequency of Condition IV. 2. Exempt 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: 15. The Permittee shall acquire from each landowner or lessee%operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required b . the US Department �l � Y of Agriculture —National .Resources Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. I Ve MONITQR— NG AND RE PORTMG REQ TS Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, igmitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. 1®E tT All gT���,-- �Il+;i�l'I' A - Approved Residual Sources 1[ SL-i.®RIP 71) Certification Date: Oe e'er I, 8014 Permit Number: WQ0004095 Version: 3.0 Monitoring Monitoring ®caner Facility Name County Permit Biologicalr uenc for Fre 'ito for Y q Monitoring Fr uenc forNumber Y Approved lrtesdduals y n -hazardous Metals arrd 4TF Pathogen �cfi1rnerallzation aracteristics z Nutrients s Potash Co PCS Phosphate High Rate Vector Attraction 1Rate ISeductions4'sInfiltration Facili Beaufort WQ0000889 Yes Exempt p Annually Total Annually Ally 0.30 10.00 1. Maximum Dry Tons per Year is the amount of residuals approved- for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as •stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. Permit application indicated that lime stabilization will be requirements, alkaline stabilization will be performed to meet vector attraction reductions. However, performed to meet pathogen red on demonstrate compliance with this permit requirement. g used other methods listed under ISA NCAC 02T .l 106(6) and .l107(a) can also be used to 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Generated Monitoring Frequency short tons er ear Established in 40 CFR 503 and 15A NCAC 02T .1111 <319 1 /Year =>319 - <1,650 I/Quarter 4 times er ,ear =>1 650 - <16,500 1/60 ®a s 6times er ear =>16,500 1/month (12 times ner vearl If no land application events occur during a required sampling sampling data is required during the period of inactivity. The annual report shall includean explanation for missing sampling data. Those monitoring o submi eche a en no l report to EPA nnay be required to matte up the missed sampling, contact the EPA for additional information and clarification, required t® submit the annual Page 1 of I ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: PCS Phosphate Company, Inc. Land Owner: Reservco, Inc. Operator: PCS Phosphate Company, Crop I Name: WQ Permit #: WQ0004095 Field #: PCS 01 Annual Dry Tons Applied: 5.2247 Site #: PCS Predominant Soil Series: Sand Crop 1 Max. PAN: Crop 2 Name: Acres Utilized: 5.5 Acres Permitted: 5.5 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Y ❑ ° Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons Volume Residual Sources /o A lied pp per (NPDES #, WQ#, Solids Acre Fen., Animal (Dry Tons/Ac) Waste, etc) Soil Cond. (Dry, Wet' Moist) Precip. Pas[ 24 firs. inches Y a b en o m a c a m w ; w 3 a m * TKN mg/kg 2 > q �' o B 2. mg/kgmglkg Nitrate and Nitrite m PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 17crop 2 Crop I Crop 2 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 May 19,700 6.36 0.950 PCS WWTP Dry 0 S 0.5 0.3 383 29.3 81.7 0.385 NA Bermuda 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF Supp ( attach FORM FSF Supp to this form): TOTALS: 0 19700 >_ As Cd Cu I Cr Pb I Ha Mo Ni I Se I Zn I P 0.385 0.000 Lime Aimlied Annual Ibs/acre 0.000 0.000 0.152 0.042 0.005 0.003 0.000 0.025 0.028 1.307 0.304 - Date lbs/ac Prior Years Cumulative lbs/ac 0.058 0.243 17.261 0.052 0.646 0.024 0.242 0.459 0.091 65.021 Current Cumulative lbs/ac 0.058 0.243 17.413 0.094 0.651 0.027 0.242 0.484 0.119 66.328 Permitted C. P. L. R.**** 36 34 1,338 n/a 267 IS Na 374 89 2,498 Permit PAN Limit Ist/2nd Crop 220 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation ZG� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) OMICROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8B1035 Nutrien Project Name: Stabilized Sludge - 4 Elf. Basin, Pt 1 Mr. Brad Lee Project/ PO Number. 2101085005 1530 NC Highway #306 South Received: 0228/2018 Aurora, NC 27806-9245 Reported: 0328/2018 Case Nonrative Nitrate/Nitrite results from work order K8C0114 was used in the PAN calculation Analytical Testing Parametan Cflont Sample ID: WWrP Sludge, grab Sample Matrix: Solid CoBaeMd By: Davis Lab Sample ID: KBB1035-01 Collection Date: 02/26/2018 11:00 Method: Calculation Plant Available Nitrogen Methal: SM 2540 G-2011 % Solids Method: 3M 4500 NH3 C-2011 Ammonia as N Method: SM 4600-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Result RL Unft Nob Prepared Analyzed Analyst 202 m9/kg 03128/18 1611 03/28/18 1611 NO Method: Calculation Sodium Adsorption Ratio, SAR Method: 3M 4500 H+6,2011 (Non.Aqueous) pH at 25 °C Method: SM 4500 P F-2011 Phosphorus, Total (as P) 6.36 1.00 % 29.3 0.100 mg/kg 03/08/18 1106 MT 08/08/18 0853 JR 383 0.500 mglkg 03/09/10 0845 TAB Result RL Units Nob Prepared Analyzed Analyst Aluminum 1160 0.910 mg/kg (dry) mg/kg 03/28/181811 03/281181611 JMO 11.8 1.0 pH Units H 03105118 1458 TAB ISO 0.25 mg/kg 031091181010 DSK Metals Result RL Units Nob Prepared Analyzed Analyst Method: EPA 200.7 Rev 4A 1994 Aluminum 1160 7.72 mg/kg (dry) 03/13118 1238 JAW Arsenic c0.061 0.061 mg/kg (dry) 03/18/18 1152 03118118 1225 JAW Cadmium <0.D03 0.003 mg/kg (dry) 03118/18 1152 03119/18 1225 JAW Calcium 613000 3.07 mg/kg (dry) 03/18118 1152 03118118 1225 JAW Chromium 22.0 0.003 mg/kg (dry) 03/13/18 1238 JAW Copper 79.S 0.015 mglkg (dry) 03/18/18 1152 03/18/18 1225 JAW Lead 2.67 0.009 mg/kg (dry) 08/18/18 1238 JAW Microbac Laboratories, Inc. 2692 Hope Milk Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com P 1 of 3 0MICR®BAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8B1035 Client Sample ID: VJWTP Sludge. grab Sample Matrix: Solid Collected By: Davis Lab Sample ID: K8B1035-01 Collection Date: 02/26/2018 11:00 Metals Result RL Units Note Prepared Analyzed Analyst Magnesium 5010 3.09 mglkg (dry) 03/13118 1238 JAW Molybdenum <0.003 0.003 mglkg (dry) 03/18118 1152 03/18/18 1225 JAW Nickel 13.1 0.003 mg/kg (dry) 03/13/18 1238 JAW Potassium 2660 6.17 mg/kg (dry) 03118/18 1238 JAW Selenium 14.6 0.010 mg/kg (dry) 0313/18 1238 JAW Sodium 3390 3.07 mg/kg (dry) 03/1&18 1152 03118/18 1225 JAW Zinc 688 0.031 mg/kg (dry) 03118/18 1152 03118118 1225 JAW Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Memory _ Result RL Units Note Prepared Analyzed Analyst Method: SW471A Mercury, Total <1.71 1.71 mg/kg DRY 03/19/180759 03/21/181031 PDM Percent SoNft Result RL Units Note Propend Analyzed Analyst Method: D2216 Percent Solids 13.9 1.00 weight % 03/20/18 0814 KMG Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Report Comments Reviewed and Approved By: Samples ware received in proper unless'on and the reported results conform to applicable accreditation standard unless otherwise noted. � ' The data and information on this, and other accompanying documents, represents Ronnie K Sanders only the samples) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bonnle.sanders0microbac.com 03/26/2018 16:15 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com page 2 of 3 W m Cliem g+mple ID o f (rww Pc�sinla Nazar) WeP: -.duo. Cnnments TV12Cj .1 E 41Cm.�a^FaY,Wa11N 'K8B1035' ;ECORO LO M I C PC. 9A; :»x HaN air w. DaN?me 1-z4a j /vb d .naNnOA INNER, Lae Eeprrt• osr�a.. ratl . , r. �- Te••arpmm Ti. fl,C DIIR4N:o:rre:.Rl�y1dF .Y.. tlRouUne (6 W T bual. dayq _Jclj Collected .rr 11 RUSH•owfy Nbl AEd.+ : µbeg 10" Q 'Eurm: Holding Tl..Mt �(qi>> CHY A«.'zJO. IN N - 1406 'IN. St.. De: breaded by) U.m RecNv .lca' % NIA Contin: a(kk D..s me Co.: Report Typo OeaNdy Seals$mea a.i YHe L�r �areornne NP LS -Z1 y0 z_nq TeNpeoire tip.: I1YNautN OnM IILeveIt llLw.+l lReva1911Lavv,; IlEDo Sere Report .v ;I•'v.. li send 1.v.ria: IIJAM [I Fax I)e-mail(Md ) ProfeC: �y1 f Loratlon: &JTP S,"�C y�iLM PON ComDllarrca Noneotlngi IIYm I1 No IAgmCyMgMm samplAd lr 4W fC �i�Vl) MMP_ sgneun: ci Ho.: P�a,ene ten<Zl YDZ-OY 5� Mar^a fYpes Srl5olN (9). BLrtlpe, Oil. wipe. `�.,,' rYMNa onnNnp waw ( ).0 ler IGW1, Surleu Waw (s`N�. WUN Wa4r (w 0 (speedy) ' HNOS.!zi HT80A. (d) NCI. (a) Na0N. 151 zinc AcebN. (6) YAtleHCI, (i) SpdMn BiaWN4. (9)5odlum Tt,M. N. (a) HwrN. (U) Unpr .d REQUESTED ANALYSIS W m Cliem g+mple ID o f (rww Pc�sinla Nazar) WeP: -.duo. Cnnments TV12Cj .1 E Ot,ma . {/!-.nNanrdo. ;IRad:oatlive Relbp He �s$gnmrel Reli Rub BY(signmIM) Rel W4"lan}0 By (fyrwtua) AdOltii,.'Wl( T .10 U.IWDNPeattion Il Disrose as aeCODnale IIRFWrr' IIAr_OW De n,* Recelyed By g ') DaN?me 1-z4a j /vb d .naNnOA Det. rime 8 - vreservauve Collected collected z F .) Types' 2 -Zi, IY It 00 1 S G Nof Ot,ma . {/!-.nNanrdo. ;IRad:oatlive Relbp He �s$gnmrel Reli Rub BY(signmIM) Rel W4"lan}0 By (fyrwtua) AdOltii,.'Wl( T .10 U.IWDNPeattion Il Disrose as aeCODnale IIRFWrr' IIAr_OW De n,* Recelyed By g ') DaN?me 1-z4a j /vb d .naNnOA on.a Received By gre) Dat.I Will ime Receiaee By NlgnaNrel Date lme Pace of Page 3 o! 3 *MICROBAC' Fayetteville Division Certificate of Analysis Nutrien Date Reported: 03/10/18 Mr. Larry Davis Project: Stabilized Sludge - 4 EtT. Basin, Pt 2 Date Received: 03/07/18 1530 NC Highway #306 South Date Sampled: 03/06/18 Aurora NC, 27806-9245 Sampled By: Davis W W TP Sludge, grab Analyte Result units Analyzed Analyzed By Method Qualifier Maly[m by: Mic. Laboratories, Inc. - FayelaeWle Nitrate as N 80.0 mg/kg 03/09/18 14:20 DSK EPA 300.0, Rev. 2.1 (1993) Nitrite as N 1.70 mg/kg 03/09/18 14:20 DSK EPA 300.0, Rev. 2.1 (1993) Field Temp (by client): 14.0 State Certifications: Respectfully Submitted NCDNR All NCDOH A377I4 �\_✓1 /_""`ter-a—� Bonnieie K. Sanders. Senior Project Managei Thank you for your business. We imitelvar jsedhack m our level ofmmim ro ynu. Please a ffwl rhe DWsim Mawger, Rob Dernier al 910-864-1930 wuh arty queshom. You may alm coniucr J. Trevor Boyce. Pmsidenl al perldrnr®microba,. m Microbac Laboratories, Inc. Page 1 Of 1 2692 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: PCS Phosphate Company, Inc. WQ Permit Number: W00004095 W WTP Name: PCS Phosphate Company, Inc. NPDES Number: Non Discharge Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternativp nprfnrmpd- Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑• 1 Alt. C (Prior Testing) ❑ Jt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) lndkate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray L31 Gamma Ra ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative rformed Class B on Indicate "Process to significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting ❑ lAcrobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monito ng data: Parameter Allowable Level in Sludge Pathogen Density EXece ber° Frequency of Analysis Sample Type Analytica Tech ninue MinimumlGeo. Mean Maximunj Units Fecal Coliform 2 x 10 to the 6th power o t �sorlids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacterial (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) . cs & �aaa acuuu rcuucuou k 10 11 l.A%. VL t .11V ) - Please indicate alternative performed: Stabilization )Alt. 9 (Injection) []Aft. 10 (Incorporation) OJo vector attraction reduction alternatives were performed C CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mark Johnson, General Manager N/A Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature ofiPreparer D 019 Date Signature of Land Applier (if applicable) Date •Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL028179 N'IL'kt, Client: Dale Davis Advisor: +�.94t . 'rr Predictive 1530 NC Hwy 306 S w ` Aurora, NC 27806 Soil Report Mehlich-3 Extraction =� Sampled County: Beaufort F" l...... Links to Helpful Information Client ID: 446314 Advisor ID: Sampled: 02/26/2018 Received: 02/28/2018 Completed: 03/09/2018 Perm: Nutrien Sample to: 00001 Recommendations: Lime Nutrients (Ib/acre) Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B More Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 100 0 0 0 0 2 -Bermuda hay/past., M 0.0 180-220 0 190 0 pH$ 0 Note: 12 Note: 0 H$ 0 0 0 Note: 12 Note: Test Results [units - WN In g/crn;; CEC and Na in meq/100 cm3; NO3-N in mg/dm;]: Soil Class: Mineral HM% WN CEC BS% Ac pH Pd K4 Ca% Mg% S4 Mn4 Mn -All Mn-Al2 Zn -1 Zn -AI Cu -1 Na ESP SSa NO3-N 0.51 1.46 6.6 99 0.1 7.1 230 18 88 9 30 58 36 36 740 740 309 0.2 3 Sample ID: 00002 Recommendations: Lime Nutrients (Ib/acre) Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B More Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 100 0 0 pH$ 0 0 0 0.10 tons/acre; 4/2017 2 - Bermuda ha /past., M 0.0 180-220 0 190 0 0 Note: 12 Note: pH$ 0 0 0 Note: 12 Note: Test Results [units -WN in g/cm;; CEC and Na In meq/100 cm;; NO3-N in mg/dm°]: Mineral Soil Class: HM%, WN CEC BS% Ac pH P4 K4 Ca% Mg%. Sd Mn -I Mn -All Mn-Al2 Zn4 Zn -AI Cu4 Na ESP SS -1 NO3-N 0.51 1.45 5.7 100 0.0 7.3 209 19 89 9 39 74 42 42 371 371 151 0.2 4 North Carolina _', TMAM" Tr Y*t lMd (W1Vr16%%NM Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve TtOXIer. Commissioner of Aariculture NCDA3C3 Agronomic Division Phone: (919) 733-2955 Website: www.ncagr.govlagronomu Report No. FY18SL028179 Date Davis Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu4 copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for fled crops or other large areas are listed separately for each nutrient to be added (in units of Ka potassium index Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/Field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they M9% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0.22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 Ibr acre alone or in a fertilizer blend will usual) appear Pe y satisfy crop needs, SS-1 levels a Mn manganese only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn4 manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients in general, homeowners do not M-O mineral-organic soil class need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit N nitrogen ncagr.gov/agronomi/pubs.htm. Na sodium NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncacr.cov/acronomUoboart4.hnd information that P4 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer P20s phosphate Sa sulfur index Test Results SS4 soluble salt index WN weight per volume The first seven values [soil class, HM%, WN, CEC. BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-4 zinc availability index remaining 16 [P-i, K-I, Ca%, Mg%, Mn-1, Mn-All 1, Mn-Al2, Zn-I, Zn-AI, Cu-I, S4, SS-I, Na, ESP, SS-I, NO 3-N (not routin Zn a zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www ncaor aov/acronoml/uvrst him PotashCorr Helping Nature Provide Sludge Stabilization *All pH readings are in S.U. Instrument ID- Oakton 150 serial # 2537117 pH Meter Cal. Date/ Time Startine pH * pH in S.U. pH Temp in oC pH meter CBI. 4.0= Date/Time After Lime * PH in S.U. 4.0= �1•� pH temp oC Buff pH Meter Buff pH Meter 5 7--7orr 7.0= oc kDe 12.45= g-yS � 7.0= 731 1 7.0= la -o oc °Z D 12.45=17,0, Y®�� 7.0=7.00 Zo/ 24 Hours Basin Starting Date Starting pH / Temp oC Added #'s of Lime Limed Sludge pH /Temp oC Time Date Limed sludge pH/ Temp. oC 1 ,J' �r01 O /Ol4 �/ Y®�� �'l9 +�� /1 �ZoC.� 2 L -1,9J / aO lZ,31 l9 101`% 3 .3L) / lots e. 12-Z1) Waste Basin N f%�- �✓LA ORC. Signature & Date Comments: