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HomeMy WebLinkAboutWQ0012980_Residual Annual Report 2018_20190205� lRoe� a It0 For Better Results. Naturally. ` Milorganite , January 30, 2019 ..._ Information Processing Unit Division of Water Quality RECEIVED Department of Environment and Natural Resources 1617 Mail Service Center FEB 0 5 2019 Raleigh, North Carolina 27699 - 1617 lln.'t Subject: Milorganite® Fertilizer Annual Report DWQiF;OG Good day: To demonstrate the quality of the Milorganite® fertilizer sold in North Carolina during 2018, a report is enclosed. The report shows that Milorganite® fertilizer continues to be an exceptional quality biosolids product, according to the applicable regulations (40 CFR 503 and 15A NCAC 2T.1106 and 2T.1107). The report includes the following sample results. Parameter Frequency As, Cd, Cu, Fe, Pb, Mo, Ni, P, K, Se, Zn Daily Al, B, Cr Monthly Hg Weekly Fecal Coliform 3 per month PCB Aroclors Daily Toxic Equivalents: Dioxins, Furans, and PCBs Monthly Priority Pollutants Semi-annually Moisture Daily RECEIVECI NCDFOW, `* FEB 5 2019 Non -Discharge Permitting Unit The Residual Report Form, a report showing distributors and sales, and a report showing an example of product temperatures at the dryer exit are enclosed. The North Carolina Department of Agriculture continues to register Milorganite® fertilizer. If you have questions, please contact me at 414-225-2243 or tnowicki@mmsd.com. If you have no interest in continuing to receive this report, then please notify me. Thanks for your cooperation. Sincerely yours, i)� &t-"_� Thomas A. Nowicki Staff Attorney Enclosures Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204_ Phone: (414) 221-6810 (800) 287-9645 Fax: (414) 221-6818 susrainingTurfgrass Research info@milorganite.com www.milorganite.com NC Henderson NC Hend 04/13/18 INV20545 50CL 50# Bags 21.00 erson 7 Classic Grade Garden & CAROLINA Henderson Mecklenburg BOONE INS Agricultural Agricultural NC Meckl 02/01/18 INV20480 36PD 36# Bags 21 SOUTHERNAG Southern Southern enbur 5 21 SOUTHERNAG Southern Southern BOONE Mecklenburg Watauga BOONE INS Agricultural Agricultural NC Wata 08/03/18 INV20618 50PRO 50# 21 SOUTHERNAG Southern Southern uga 6 MILORGANITE NC Wata 07/24/18 INV20610 50PRO 50# 168.00 uga 7 MILORGANITE NC Wata 03/23/18 INV20525 50CL 50# Bags uga 0 Classic Grade NC Wata 07/06/18 INV20599 50PRO 50# uga 5 MILORGANITE NC Wata 10/17/18 INV20640 50PRO 50# uga 0 MILORGANITE NC Wata 01/26/18 INV20474 50GG 50# Bags uga 4 Greens Grade NC Wata 05/07/18 INV20559 50CL 50# Bags uga 5 Classic Grade NC Wata 07/19/18 INV20607 50PRO 50# uga 8 MILORGANITE Watauga Total: NC Total: Paae 1 of 1 21 SOUTHERNAG Southern Southern HENDERSON INS Agricultural Agricultural VILLE 21.00 21.17 CGP Central NORTH CHARLOTTE Garden & CAROLINA 21.17 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 21 SOUTHERNAG Southern Southern BOONE INS Agricultural Agricultural 168.00 210.17 MKT600 North Carolina Department of Environment and Natural Resources ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ 00 12980 No Discharge Facility Name: Milwaukee Metro Sewerage District Residual Source WQ # or NPDES WWTP Name: Residual Analysis Data WPDES WI 0036820 Jones Island Laboratory: 1) 2) 3) 4) 5) Milwaukee Metro Sewerage District Parameter (mg/kg) Limit ( Limi r) Sample or Composite Date (monthly average) January February March April May June July August September October November December Percent Solids (%) NA 93 94 92 92 93 94 94 96 95 95 94 93 Arsenic 41 <3.7 <3.8 <3.8 <3.9 <6.2 <6.2 <6.2 <6.2 <6.1 <6.2 <6.2 <6.3 Cadmium 39 <0.90 <0.86 <0.86 <0.91 0.37 0.59 0.5 0.56 0.67 0.64 0.45 0.51 Chromium NA 130 160 160 170 160 220 200 170 230 180 230 210 Copper 1,500 200 190 190 200 210 210 210 220 210 200 210 200 Lead 300 26 30 34 32 34 43 46 50 65 57 32 28 Mercury 17 0.064 0.099 0.022 0.011 0.053 0.17 0.2 0.26 0.15 0.058 0.23 0.19 Molybdenum 75 11 9.8 9.3 9.6 9.2 9.1 8.3 9.7 9.4 9.1 10 9.9 Nickel 420 24 26 26 25 30 35 33 33 34 28 27 27 Selenium 100 4.3 5.4 5.9 4.4 <6.6 <6.6 <6.7 <6.6 <6.5 <6.6 <6.6 <6.7 Zinc 2,800 410 410 380 410 420 440 460 500 500 460 430 420 Total Phosphorus NA 23,000 21,000 21,000 21,000 21,000 23,000 24,000 24,000 21,000 21,000 24,000 24,000 Total Nitrogen(%) NA 1 6.8 1 6.7 6.7 6.6 6.3 6.2 5.9 5.7 5.4 5.6 6 6.3 Ammonia -Nitrogen(%) NA 0.18 0.17 0.17 0.20 1 0.15 0.20 0.24 0.20 0.24 0.14 0.17 0.15 Nitrate Nitrogen(%) NA <0.5 0.70 0.54 <0.5 <0.5 <0.5 <0.5 0.60 <0.5 <0.5 0.7 1.3 Sampling frequency: Arsenic, cadmium, copper, lead, molybdenum, nickel, selenium, and zinc are daily; Mercury is weekly; Ammonia, chromium, nitrate, and nitrogen are monthly I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Signature of Preparer * ate *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) For Better Results. t Naturally. Milarganiti Milorganite® Fertilizer North Carolina Exceptional Quality Biosolids Certification Permit for Distribution of Class A Residuals WQ0012980 We, Thomas A. Nowicki, Staff Attorney, Milwaukee Metropolitan Sewerage District, and Todd Schwingle, Operations Manager, Veolia Water Milwaukee LLC, certify that we have personally examined and are familiar with the submitted information. Based upon our inquiry of those individuals immediately responsible collecting the information, we believe the information is true, accurate, and complete. We certify that Milorganite® fertilizer: (1) complied with the limits of 40 CFR § 503.13(b)(3); (2) was dried to achieve a pellet temperature exceeding 176°F/80°C when less than 10% moisture, as required for Class A pathogen destruction, according to 40 CFR § 503.32, Appendix B, B.2, and 15A NCAC 2T.1106(b)(3)(F); and (3) was dried to achieve greater than 75% solids, as required for vector attraction reduction, according to 40 CFR § 503.33(b)(7) and 15A NCAC 2T.1107(a)(7). We made this determination based upon an environmental management system in which qualified personnel properly gather and evaluate information regarding pollutant concentrations, pathogen reduction, and vector attraction reduction. We are aware of the significant penalties for submitting false information, including the possibility of fine and imprisonment. Certified January A 1, 2019 Thomas A. Nowicki, Staff Attorney Certified January r'9, 2019: , To Schwingl , Operatio anager Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204 091211 , Phone: (414) 221-6810 (800) 287-9645 Fax: (414) 221-6818 SurtainingTurfgnusReseareh info@milorganite.com www.milorganite.com Dryer 1 Dryer 2 Dryer 3 Dryer 4 Dryer 5 Dryer 6 Dryer 7 Dryer 8 Dryer 9 Dryer 10 Dryer 11 Dryer 12 Product Product Product Product Product Product Product Product Product Product Product Product Discharge Discharge Discharge Discharge Discharge Discharge Discharge Discharge Discharge Discharge Discharge Discharge Temp Temp Temp Temp Temp Temp Temp Temp Temp Temp Temp Temp of of of of of �F of of of OF OF OF 6/1/18 0:00 182 178 177 182 182 178 176 182 6/1/18 0:01 182 179 177 182 182 179 176 181 6/1/18 0:02 182 179 177 182 182 179 176 181 6/1/18 0:03 181 179 177 182 182 179 176 181 6/1/18 0:04 181 180 177 182 182 180 176 181 6/1/18 0:05 181 180 177 182 181 180 176 181 6/1/18 0:06 180 180 177 182 181 180 176 180 6/1/18 0:07 180 181 177 182 181 180 176 180 6/1/18 0:08 180 181 177 182 181 180 176 180 6/1/18 0:09 180 181 177 182 181 180 176 179 6/1/18 0:10 180 181 177 182 181 180 176 179 6/1/18 0:11 180 182 177 182 181 180 176 179 6/1/18 0:12 179 182 177 182 181 180 176 179 6/1/18 0:13 179 182 177 182 181 180 176 178 6/1/18 0:14 179 182 177 182 181 180 176 178 6/1/18 0:15 179 182 178 182 181 180 176 178 6/1/18 0:16 179 182 178 182 181 179 176 178 6/1/18 0:17 178 182 178 182 181 179 176 177 6/1/18 0:18 178 182 178 182 181 178 176 177 6/1/18 0:19 178 182 178 182 181 178 176 177 6/1/18 0:20 178 182 178 182 181 177 176 177 6/1/18 0:21 178 183 178 182 181 176 176 177 6/1/18 0:22 178 183 178 182 181 176 176 177 6/1/18 0:23 178 183 178 182 181 175 176 177 6/1/18 0:24 178 183 178 182 181 175 177 177 6/1/18 0:25 178 183 178 182 181 174 177 177 6/1/18 0:26 178 183 178 182 181 174 177 177 6/1/18 0:27 179 183 178 182 181 173 177 176 6/1/18 0:28 179 183 178 182 181 173 177 176 6/1/18 0:29 179 183 178 182 181 173 177 176 6/1/18 0:30 180 183 178 182 181 172 177 176 6/1/18 0:31 180 182 178 182 181 172 177 176 6/1/18 0:32 180 182 178 182 181 171 177 176 6/1/18 0:33 180 182 178 181 181 171 178 176 6/1/18 0:34 180 181 179 181 181 171 178 176 6/1/18 0:35 180 181 179 180 181 171 178 176 6/1/18 0:36 181 181 180 180 181 172 178 176 6/1/18 0:37 181 181 180 180 181 172 178 176 6/1/18 0:38 181 181 180 180 181 174 178 176 6/1/18 0:39 182 181 181 180 181 177 180 176 6/1/18 0:40 182 181 181 180 181 178 182 176 6/1/18 0:41 183 181 181 180 181 180 183 177 6/1/18 0:42 184 181 182 180 181 180 184 177 6/1/18 0:43 184 181 182 180 181 181 184 177 6/1/18 0:44 185 180 183 180 181 181 185 178 6/1/18 0:45 185 180 183 180 181 180 185 178 6/1/18 0:46 186 179 184 180 181 180 184 178 6/1/18 0:47 186 179 184 180 181 181 184 179 6/1/18 0:48 186 178 185 180 181 181 184 179 6/1/18 0:49 187 178 185 180 181 181 184 180 6/1/18 0:50 187 179 186 180 181 182 184 181 6/1/18 0:51 187 179 186 180 181 183 184 182 6/1/18 0:52 188 179 186 181 181 184 184 182 6/1/18 0:53 188 180 187 181 181 185 185 183 6/1/18 0:54 188 180 187 182 181 186 186 183 6/1/18 0:55 189 180 187 182 182 187 187 184 6/1/18 0:56 189 181 188 183 182 188 188 184 6/1/18 0:57 189 181 188 183 182 189 189 184 6/1/18 0:58 189 181 189 184 182 190 190 185 6/1/18 0:59 189 182 189 184 182 192 191 185 6/1/18 1:00 189 182 189 184 182 193 192 185 6/1/18 1:01 189 183 188 184 182 195 193 185 6/1/18 1:02 189 183 188 185 182 196 194 185 6/1/18 1:03 190 183 188 185 182 198 194 185 6/1/18 1:04 190 184 188 185 182 199 195 185 6/1/18 1:05 190 184 188 185 182 201 196 185 6/1/18 1:06 190 185 188 185 183 202 197 185 6/1/18 1:07 190 185 187 185 183 203 197 185 6/1/18 1:08 189 186 187 185 184 204 198 185 6/1/18 1:09 189 186 186 186 184 205 199 185 6/1/18 1:10 188 187 186 186 184 206 199 185 6/1/18 1:11 188 187 186 186 184 206 200 185 6/1/18 1:12 188 188 185 187 184 207 200 185 6/1/18 1:13 187 188 185 187 184 207 201 185 6/1/18 1:14 187 189 185 187 184 207 201 186 6/1/18 1:15 186 190 185 187 184 207 202 186 6/1/18 1:16 186 190 185 188 184 207 202 186 6/1/18 1:17 186 191 185 188 184 207 203 186 6/1/18 1:18 185 192 185 188 185 206 203 186 6/1/18 1:19 185 193 185 188 185 206 203 186 6/1/18 1:20 185 194 185 188 185 205 203 186 6/1/18 1:21 185 194 185 188 185 205 203 186 6/1/18 1:22 184 195 185 188 185 204 203 186 6/1/18 1:23 184 196 185 188 185 203 203 186 6/1/181:24 184 197 185 189 185 202 203 186 6/1/181:25 185 198 185 189 185 201 203 186 6/1/181:26 185 199 185 189 185 199 203 187 6/1/18 1:27 185 199 185 189 185 198 203 187 6/1/18 1:28 185 200 185 189 185 197 203 187 6/1/18 1:29 186 200 185 189 185 196 203 187 6/1/18 1:30 186 200 185 189 186 195 202 187 6/1/181:31 186 200 185 189 186 194 202 187 6/1/181:32 187 200 185 189 186 193 202 187 6/1/181:33 187 199 185 189 186 192 201 187 6/1/181:34 187 199 185 189 186 192 201 187 6/1/18 1:35 188 198 185 189 186 191 201 187 6/1/181:36 188 198 185 189 186 190 201 188 6/1/181:37 188 197 185 189 186 189 200 188 6/1/181:38 189 196 184 188 186 188 200 188 6/1/181:39 189 195 184 188 186 187 200 188 6/1/18 1:40 189 195 183 187 186 186 199 188 6/1/18 1:41 189 194 183 187 186 185 199 188 6/1/181:42 189 193 183 187 187 184 198 188 6/1/18 1:43 189 193 182 186 187 183 198 189 6/1/18 1:44 189 192 182 186 186 183 198 189 6/1/18 1:45 188 192 182 186 186 182 197 189 6/1/18 1:46 189 191 182 185 186 182 197 189 6/1/18 1:47 189 191 182 185 187 182 196 189 6/1/18 1:48 189 190 182 185 187 182 196 189 6/1/181:49 189 190 182 185 187 182 195 189 6/1/181:50 189 189 181 184 187 182 195 189 6/1/181:51 189 189 182 184 187 183 195 189 6/1/181:52 189 189 182 184 187 183 194 189 6/1/181:53 189 188 182 184 187 184 194 188 6/1/18 1:54 189 188 182 184 187 185 194 188 6/1/18 1:55 189 188 182 184 187 186 193 188 6/1/18 1:56 189 188 182 184 187 187 193 188 6/1/18 1:57 189 188 183 184 187 188 193 188 6/1/18 1:58 189 188 183 184 187 188 192 187 6/1/18 1:59 189 188 183 184 187 189 192 187 6/1/18 2:00 189 188 183 184 187 189 192 187 6/1/18 2:01 189 187 183 184 187 190 191 186 6/1/18 2:02 189 187 183 184 187 190 191 186 6/1/18 2:03 189 188 183 184 187 191 191 186 6/1/18 2:04 189 188 184 184 188 191 190 185 6/1/18 2:05 189 188 184 184 188 192 190 185 6/1/18 2:06 188 188 184 184 188 192 190 185 6/1/18 2:07 188 188 184 184 188 192 189 185 6/1/18 2:08 188 188 184 184 188 192 189 185 6/1/18 2:09 188 188 184 184 188 192 189 185 6/1/18 2:10 188 188 184 184 188 192 189 184 6/1/18 2:11 188 188 184 184 188 192 188 184 6/1/18 2:12 188 188 184 184 188 192 188 183 6/1/18 2:13 188 187 184 184 188 192 188 183 6/1/18 2:14 188 187 184 184 187 192 187 183 6/1/18 2:15 188 187 184 184 187 192 188 183 6/1/18 2:16 188 187 184 183 186 192 188 182 6/1/18 2:17 188 187 184 183 186 192 188 182 6/1/18 2:18 188 187 184 183 186 192 188 182 6/1/18 2:19 188 186 184 183 186 192 188 183 6/1/18 2:20 188 186 184 183 185 192 188 183 6/1/18 2:21 188 186 184 183 185 192 188 183 6/1/18 2:22 188 186 184 183 185 192 188 184 6/1/18 2:23 188 186 184 183 185 192 188 184 6/1/18 2:24 188 186 184 183 185 191 188 185 6/1/18 2:25 188 186 184 183 185 191 187 185 6/1/18 2:26 188 186 184 184 185 191 187 185 6/1/18 2:27 188 186 184 184 185 190 187 186 6/1/18 2:28 188 187 184 185 185 190 187 186 6/1/18 2:29 188 187 185 185 185 190 187 185 6/1/18 2:30 188 187 185 185 185 190 187 185 6/1/18 2:31 189 187 185 185 185 190 187 185 6/1/18 2:32 188 187 185 185 185 190 187 184 6/1/18 2:33 188 187 185 185 185 190 187 184 6/1/18 2:34 188 187 185 185 185 189 187 184 6/1/18 2:35 188 187 184 186 185 189 187 183 6/1/18 2:36 188 187 184 186 185 189 187 183 6/1/18 2:37 188 187 184 186 185 189 187 182 6/1/18 2:38 187 186 184 186 185 189 187 182 6/1/18 2:39 187 186 184 186 185 189 187 182 6/1/18 2:40 187 186 184 186 185 188 187 182 6/1/18 2:41 187 186 183 186 185 188 187 182 6/1/18 2:42 187 186 183 187 185 188 186 182 6/1/18 2:43 186 185 184 187 185 188 186 182 6/1/18 2:44 186 185 184 186 185 188 186 182 6/1/18 2:45 186 185 184 186 185 188 186 182 6/1/18 2:46 186 184 184 186 185 188 186 182 6/1/18 2:47 186 184 184 186 185 188 186 182 6/1/18 2:48 186 184 184 186 185 187 186 182 6/1/18 2:49 186 184 184 186 185 187 186 183 6/1/18 2:50 186 184 184 185 185 186 186 183 6/1/18 2:51 185 184 184 185 184 186 186 184 6/1/18 2:52 185 184 184 185 184 187 186 185 6/1/18 2:53 185 183 185 185 184 186 185 186 6/1/18 2:54 184 183 185 185 184 186 185 187 6/1/18 2:55 184 184 185 184 184 185 185 187 6/1/18 2:56 184 184 185 184 184 185 185 186 6/1/18 2:57 184 184 185 184 184 184 185 186 6/1/18 2:58 183 184 185 184 184 184 185 185 6/1/18 2:59 183 184 185 184 184 183 185 184 6/1/18 3:00 183 184 185 184 184 182 185 183 6/1/18 3:01 183 184 185 184 184 182 185 181 6/1/18 3:02 183 184 185 184 184 181 184 180 6/1/18 3:03 183 184 185 184 184 180 184 178 6/1/18 3:04 183 185 186 184 184 180 184 176 6/1/18 3:05 183 185 186 184 184 179 184 174 6/1/18 3:06 183 185 186 184 184 179 184 172 6/1/18 3:07 183 186 186 184 184 179 184 171 6/1/18 3:08 183 186 186 184 184 179 184 169 6/1/18 3:09 183 186 186 184 184 179 184 168 6/1/18 3:10 183 186 185 184 184 179 184 167 6/1/18 3:11 183 186 185 184 184 180 184 167 6/1/18 3:12 183 186 185 184 184 180 184 167 6/1/18 3:13 184 186 185 185 183 181 184 167 6/1/18 3:14 184 187 185 185 183 181 184 167 6/1/18 3:15 184 187 185 185 183 181 184 168 6/1/18 3:16 184 188 185 185 183 182 184 169 6/1/18 3:17 184 188 185 185 183 182 184 170 6/1/18 3:18 184 188 186 185 183 183 184 171 6/1/18 3:19 184 188 186 185 183 183 184 172 6/1/18 3:20 184 188 186 185 183 184 184 172 6/1/18 3:21 184 188 186 185 183 184 184 173 6/1/18 3:22 184 188 186 185 183 184 185 174 6/1/18 3:23 184 188 186 185 183 185 185 175 6/1/18 3:24 184 188 187 185 183 185 185 176 6/1/18 3:25 184 188 187 185 183 186 186 178 6/1/18 3:26 185 187 187 185 183 186 186 180 6/1/18 3:27 185 187 187 185 183 187 186 181 6/1/18 3:28 185 187 187 186 184 187 186 182 6/1/18 3:29 185 187 187 186 184 187 186 182 6/1/18 3:30 185 187 187 186 184 187 186 183 6/1/18 3:31 185 186 186 186 184 188 186 184 6/1/18 3:32 185 186 186 186 184 188 186 184 6/1/18 3:33 185 186 186 186 184 188 186 185 6/1/18 3:34 185 186 185 186 184 188 186 185 6/1/18 3:35 185 186 185 186 184 187 186 186 6/1/18 3:36 185 186 185 187 184 187 186 186 6/1/18 3:37 185 185 185 187 184 187 186 186 6/1/18 3:38 185 185 185 187 184 187 185 187 6/1/18 3:39 185 185 185 187 184 187 185 188 6/1/18 3:40 185 185 185 187 185 187 186 188 6/1/18 3:41 185 185 184 187 185 186 186 189 6/1/18 3:42 185 185 184 187 185 186 186 189 6/1/18 3:43 185 185 184 187 185 185 185 189 6/1/18 3:44 185 185 184 187 185 185 185 189 6/1/18 3:45 185 185 184 187 185 185 185 189 6/1/18 3:46 185 185 183 186 185 184 185 189 6/1/18 3:47 185 185 183 186 185 184 185 189 6/1/18 3:48 185 185 183 186 185 184 185 190 6/1/18 3:49 185 185 183 186 185 184 186 190 6/1/18 3:50 185 185 183 186 185 183 186 191 6/1/18 3:51 185 185 184 186 185 183 186 191 6/1/18 3:52 185 185 184 186 185 183 186 192 6/1/18 3:53 186 184 185 186 185 183 186 194 6/1/18 3:54 186 185 185 186 185 183 186 195 6/1/18 3:55 187 185 185 186 185 183 185 196 6/1/18 3:56 187 185 186 186 185 183 185 197 6/1/18 3:57 187 185 186 187 186 183 185 198 6/1/18 3:58 187 185 186 187 186 183 185 198 6/1/18 3:59 187 185 186 187 186 183 185 199 6/1/18 4:00 187 185 186 187 187 183 185 199 6/1/18 4:01 187 185 186 187 187 183 185 199 6/1/18 4:02 187 185 187 187 187 183 184 198 6/1/18 4:03 187 186 186 187 187 183 185 198 6/1/18 4:04 187 186 186 187 187 184 185 198 6/1/18 4:05 187 186 186 187 187 184 185 197 6/1/18 4:06 186 186 186 187 187 184 185 196 6/1/18 4:07 186 186 186 187 187 184 185 196 6/1/18 4:08 186 186 186 187 187 184 185 195 6/1/18 4:09 186 186 185 187 187 184 185 195 6/1/18 4:10 186 186 185 187 187 184 185 194 6/1/18 6:19 186 176 179 181 181 183 183 193 6/1/18 6:20 186 176 179 181 181 183 183 193 6/1/18 6:21 186 176 179 181 181 183 183 192 6/1/18 6:22 187 177 179 181 180 183 183 192 6/1/18 6:23 187 177 179 181 180 183 183 191 6/1/18 6:24 187 176 179 182 180 183 183 191 6/1/18 6:25 187 176 179 182 180 183 183 191 6/1/18 6:26 187 176 178 182 180 182 183 191 6/1/18 6:27 188 176 178 182 180 182 183 191 6/1/18 6:28 188 176 178 182 180 181 183 191 6/1/18 6:29 188 176 178 182 180 180 183 191 6/1/18 6:30 188 176 178 182 180 179 183 191 6/1/18 6:31 188 176 178 183 180 179 184 190 6/1/18 6:32 188 176 178 183 180 178 184 190 6/1/18 6:33 188 177 178 183 180 177 184 189 6/1/18 6:34 187 177 177 183 180 176 184 188 6/1/18 6:35 187 178 177 183 180 176 184 188 6/1/18 6:36 187 178 176 183 180 175 184 187 6/1/18 6:37 187 179 176 184 180 175 184 187 6/1/18 6:38 187 179 175 184 180 175 184 186 6/1/18 6:39 187 180 175 183 180 175 184 186 6/1/18 6:40 187 180 174 183 180 175 184 185 6/1/18 6:41 187 179 174 183 180 175 184 185 6/1/18 6:42 187 179 174 182 180 175 184 184 6/1/18 6:43 187 179 174 182 180 175 184 184 6/1/18 6:44 186 179 174 182 180 176 184 183 6/1/18 6:45 186 178 174 181 180 176 184 182 6/1/18 6:46 186 178 173 180 180 176 183 182 6/1/18 6:47 186 178 173 179 180 176 183 181 6/1/18 6:48 186 178 173 179 179 176 182 181 6/1/18 6:49 186 177 173 178 179 176 182 181 6/1/18 6:50 186 177 173 177 179 176 182 180 6/1/18 6:51 186 177 173 176 179 176 183 180 6/1/18 6:52 186 177 173 175 179 176 183 179 6/1/18 6:53 185 177 173 174 179 176 183 179 6/1/18 6:54 185 177 172 174 179 176 183 179 6/1/18 6:55 184 177 172 173 179 176 183 179 6/1/18 6:56 184 178 172 172 179 176 183 179 6/1/18 6:57 184 178 172 172 179 176 183 179 6/1/18 6:58 184 178 172 171 179 176 183 179 6/1/18 6:59 184 178 172 171 179 176 183 179 6/1/18 7:00 184 178 172 171 179 176 182 179 6/1/18 7:01 184 178 172 172 180 176 182 179 6/1/18 7:02 184 179 172 172 180 176 182 179 6/1/18 7:03 184 179 172 172 180 177 182 179 6/1/18 7:04 184 179 172 173 181 177 182 179 6/1/18 7:05 184 180 172 173 181 177 182 178 6/1/18 7:06 184 180 172 174 181 177 183 178 6/1/18 7:07 184 180 172 174 181 177 182 178 6/1/18 7:08 184 180 172 174 181 177 182 177 6/1/18 7:09 184 181 172 175 181 177 182 177 6/1/18 7:10 184 181 172 175 182 177 182 177 6/1/18 7:11 184 181 173 176 182 177 182 176 6/1/18 7:12 183 181 173 176 182 177 182 176 6/1/18 7:13 183 181 173 177 182 177 182 176 6/1/18 7:14 183 181 173 177 182 177 182 176 6/1/18 7:15 183 181 173 178 182 178 182 176 6/1/18 7:16 183 181 173 178 183 178 182 176 6/1/18 7:17 183 181 173 179 183 178 182 175 6/1/18 7:18 183 181 173 179 183 178 183 175 6/1/18 7:19 183 181 174 180 183 178 183 175 6/1/18 7:20 182 181 174 180 183 178 183 175 6/1/18 7:21 182 181 174 180 183 178 183 175 6/1/18 7:22 182 181 174 180 183 179 183 175 6/1/18 7:23 182 181 174 180 183 179 183 175 6/1/18 7:24 182 181 175 ISO 183 179 183 175 6/1/18 7:25 182 181 175 180 183 179 183 175 6/1/18 7:26 182 181 175 180 183 179 182 175 6/1/18 7:27 181 181 175 180 183 179 182 175 6/1/18 7:28 181 181 175 180 184 180 182 175 6/1/18 7:29 180 182 175 180 184 180 182 175 6/1/18 7:30 180 182 175 180 183 179 182 175 6/1/18 7:31 180 182 176 180 184 179 182 175 6/1/18 7:32 180 182 176 180 183 179 182 175 6/1/18 7:33 180 182 177 180 184 178 183 175 6/1/18 7:34 180 182 177 180 183 178 183 175 6/1/18 7:35 179 182 177 180 183 178 183 175 6/1/18 7:36 179 182 177 180 184 178 182 175 6/1/18 7:37 179 183 177 180 184 178 182 175 6/1/18 7:38 179 183 176 181 184 179 182 175 6/1/18 7:39 179 184 176 181 184 179 182 175 6/1/18 7:40 179 184 177 181 184 179 182 175 6/1/18 7:41 178 184 177 182 184 179 182 175 6/1/18 7:42 178 185 177 182 184 179 183 176 6/1/18 7:43 177 185 178 182 184 180 183 176 6/1/18 7:44 177 186 178 183 184 180 184 177 6/1/18 7:45 177 187 179 183 184 181 184 177 6/1/18 7:46 177 188 180 183 184 181 184 177 6/1/18 7:47 177 189 181 184 184 181 184 177 6/1/18 7:48 177 190 182 184 184 182 184 176 6/1/18 7:49 177 191 183 184 183 183 184 176 6/1/18 7:50 177 192 184 184 183 183 184 176 6/1/18 7:51 176 193 184 184 183 183 184 176 6/1/18 7:52 176 193 185 184 184 183 184 176 6/1/18 7:53 175 193 185 184 184 183 184 176 6/1/18 7:54 175 193 186 184 184 184 184 176 6/1/18 7:55 175 193 186 184 183 184 184 176 6/1/18 7:56 175 193 186 184 183 183 184 176 6/1/18 7:57 175 193 185 184 183 183 184 177 6/1/18 7:58 175 192 185 184 182 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191 188 184 6/1/18 20:01 191 183 183 184 185 191 188 184 6/1/18 20:02 191 184 183 184 185 191 188 184 6/1/18 20:03 191 184 183 184 185 191 188 184 6/1/18 20:04 192 184 184 184 186 191 188 184 6/1/18 20:05 192 184 184 184 186 191 188 184 6/1/18 20:06 192 184 184 184 186 191 188 184 6/1/18 20:07 192 184 184 184 186 191 188 184 6/1/18 20:08 192 184 184 184 186 191 188 184 6/1/18 20:09 192 184 184 184 186 191 187 184 6/1/18 20:10 192 184 184 184 186 191 187 184 6/1/18 20:11 193 184 184 185 187 191 187 184 6/1/18 20:12 193 184 184 185 187 191 187 184 6/1/18 20:13 193 184 184 185 187 191 187 185 6/1/18 20:14 193 184 183 185 187 191 187 185 6/1/18 20:15 193 184 183 185 187 191 187 185 6/1/18 20:16 193 184 183 185 188 191 188 184 6/1/18 20:17 193 184 183 185 188 191 188 184 6/1/18 20:18 193 184 183 185 188 191 188 184 6/1/18 20:19 192 184 183 185 188 191 188 184 6/1/18 20:20 192 184 183 185 188 190 188 184 6/1/18 20:21 192 184 183 185 188 190 188 184 6/1/18 20:22 192 184 184 185 189 189 189 184 6/1/18 20:23 192 184 184 185 189 189 189 184 6/1/18 20:24 192 184 184 185 189 188 189 185 6/1/18 20:25 191 184 184 185 189 188 189 185 6/1/18 20:26 191 184 184 185 189 188 189 184 6/1/18 20:27 191 184 184 184 189 187 189 184 6/1/18 20:28 191 184 184 184 189 187 189 184 6/1/18 20:29 191 184 185 184 188 187 189 184 6/1/18 20:30 191 184 185 184 188 187 189 184 6/1/18 20:31 191 184 185 184 187 187 189 184 6/1/18 20:32 190 184 185 184 187 187 189 184 6/1/18 20:33 190 184 185 184 187 188 189 184 6/1/18 20:34 190 184 185 183 187 188 189 184 6/1/18 20:35 190 184 185 183 186 187 189 183 6/1/18 20:36 190 184 185 183 186 187 188 183 6/1/18 20:37 190 185 185 183 186 187 188 183 6/1/18 20:38 190 185 185 183 186 187 189 183 6/1/18 20:39 190 185 185 183 186 187 189 183 6/1/18 20:40 190 185 185 184 186 187 190 183 6/1/18 20:41 190 185 185 184 185 186 190 184 6/1/18 20:42 189 185 185 184 185 186 190 184 6/1/18 20:43 189 185 186 184 184 187 190 185 6/1/18 20:44 189 185 186 184 184 187 190 185 6/1/18 20:45 189 186 186 184 184 187 190 186 6/1/18 20:46 189 186 186 184 184 187 190 187 6/1/18 20:47 190 186 186 184 184 187 190 187 6/1/18 20:48 190 186 186 185 184 187 190 188 6/1/18 20:49 189 186 186 185 184 186 190 188 6/1/18 20:50 189 186 186 186 184 186 191 188 6/1/18 20:51 189 186 186 186 184 186 191 187 6/1/18 20:52 189 186 186 186 184 186 191 187 6/1/18 20:53 189 186 186 186 184 186 191 187 6/1/18 20:54 189 186 186 186 184 186 191 186 6/1/18 20:55 189 186 186 186 184 186 191 186 6/1/18 20:56 189 186 186 186 184 187 191 186 6/1/18 20:57 189 186 186 186 184 187 192 185 6/1/18 20:58 189 186 186 186 184 187 192 185 6/1/18 20:59 189 185 186 186 184 187 192 185 6/1/18 21:00 188 185 186 186 184 187 192 185 6/1/18 21:01 188 185 186 186 184 187 192 185 6/1/18 21:02 188 185 186 186 184 187 192 184 6/1/18 21:03 188 185 186 186 185 187 192 184 6/1/18 21:04 188 185 186 186 185 187 193 184 6/1/18 21:05 187 185 186 186 185 187 193 184 6/1/18 21:06 187 185 186 186 185 187 193 184 6/1/18 21:07 186 185 187 186 185 187 193 184 6/1/18 21:08 186 185 187 186 186 187 193 184 6/1/18 21:09 186 185 187 186 186 186 193 184 6/1/18 21:10 185 185 187 186 187 186 193 184 6/1/18 21:11 185 185 187 186 187 186 193 184 6/1/18 21:12 185 185 187 185 187 186 193 184 6/1/18 21:13 184 185 187 185 187 186 193 184 6/1/18 21:14 184 185 187 185 187 186 193 184 Notes Regarding Temperature Data For determining compliance with the heat drying requirement, individual temperature measurements are not conclusive because the Milorganite® fertilizer production process involves multiple recycling loops, which are necessary to obtain product consistency, uniformity, and the specific particle size necessary for a consumer product in the fertilizer market. A massive amount of recycling occurs in the Milorganite® fertilizer manufacturing process. The chance is negligible that product will leave the drying system without being heated to a temperature of 176 °F. The drying system has four recycling systems. Three recycling systems operate continuously: 1. Dryer to dryer, 2. Return from central recycling bins, and 3. Return from product sizing. The fourth recycling system is around individual dryers, which is used when the dryer discharge conveyors have mechanical problems. A diagram showing the recycling loops is provided below. Given the very low frequency of exit product temperatures below 176 °F and the very high rates of recycling at the dryers and recycling bin, the probability of a particle being heated to at least 176 °F typically is greater than 99%, without considering recycling from sizing. A probability analysis is available upon request using production rates and temperatures for a specific year. As indicated below, several additional safety factors further reduce the risk of under -heating, making the already the small risk of a particle leaving the recycling bins without being heated to at least 176 °F degrees even smaller. (1) First Safety Factor: Pellet Sizing and Return of Large Pellets for Further Drying After the main recycling bins, product goes to sizing. Sizing returns large pellets to the drying process for additional heating. These large pellets have the highest relative risk for retaining moisture. By returning them for further heat drying, this risk is eliminated. Sufficient data is not available to calculate the return rate of large pellets for further heating, but this rate is likely to be 5% to 10% of total production. (2) Second Safety Factor: Conduction on Belts and in Recycle Bin In addition to the heating that occurs in the dryers, heating occurs within conveyors and the recycle bin, where product from cooler dryers will mix with product from warmer dryers. As the temperature data shows, product exit temperatures are higher than 176 °F much of the time. The heat from this product will warm any cooler product within the conveyors or recycling bin. Data is not available to quantify this additional heating. (3) Third Safety Factor: Low Risk that a Pellet Heated Only Once would be Discharged from a Dryer Less than 176° F Only 1 % of pellets leave the recycle bin after only one pass. Less than 10% of pellet exit temperatures are less than 176° F. Thus, the chance that both conditions would occur simultaneously is very low. In practice, only a portion of single -pass solids would be exposed to insufficient temperatures because low temperatures are not distributed evenly among operating dryers. (4) Fourth Safety Factor: Consistent Extremely Low Fecal Coliform and Moisture Concentrations Demonstrate Minimal Risk To destroy pathogens, the protection from evaporative cooling from water must be eliminated. Daily sample results for Milorganite® fertilizer show moisture concentrations consistently at 10% or less, typically in the range of 7%. At these low levels, the protection from evaporative cooling is minimal, allowing the destruction of pathogens. If a daily sample result is greater than 10%, then product from that day is segregated and re -processed. The degree to which fecal coliform concentrations are below the limit demonstrates this phenomenon. The limit is 1,000 MPN/gTS. Milorganite® fertilizer not only complies, but almost all sample results are below the level of detection (0.22 MPN/gTS). The remaining results are near the level of detection. The only explanation for this extreme degree of fecal coliform destruction is thorough heating. These sample results prove that heating has been sufficient to destroy pathogens as required. Milorganite® Fertilizer Drying Process Flow Diagram Worganibi Twelve dryers are in two sets of six. pppi7— �¢eaqq Dewatered Sludge I I I e � D Tembes awle azure - t at yrr !11-.rs At individualdryers and tram the recycle bins• recycling occurs as needed to maintain the dryer teed ratlo and optimise siring Typically 60-70% of production Typical Dryer Peed = 90% Recycle 10%Dewatered Sludge (dry weight basis) Product Composite Sampler Typically 30-40% of Production Recycl Bin Tao Big Too Small Disposal --� aluetmvsare—tinuous ------- I- Red tl—reiimltedwspecialcondltl— T. Novicki -12/7/17 e. For Better Results. Milorganite Milorganite® Fertilizer FEB 0 5 2019 Exceptional Quality Biosolids Certification We, Thomas A. Nowicki, Staff Attorney, Milwaukee Metropolitan Sewerage District, and Todd Schwingle, Operations Manager, Veolia Water Milwaukee LLC, certify that we have personally examined and are familiar with the submitted information. Based upon our inquiry of those individuals immediately responsible for obtaining the information, we believe the submitted information is true, accurate, and complete. We certify that Milorganite® fertilizer: (1) complied with the limits of 40 CFR § 503.13(b)(3) and Wis. Adm. Code, sec. NR 204.07(5)(c) Table 3; (2) was dried to achieve a pellet temperature exceeding 176'F/80 °C when less than 10% moisture, as required for Class A pathogen destruction, according to 40 CFR § 503.32, Appendix B, sec. B.2, and Wis. Adm. Code, sec. NR 204.07(6)(a)(2)c; and (3) was dried to achieve greater than 75% solids, as required for vector attraction reduction by 40 CFR § 503.33(b)(7) and Wis. Adm. Code, sec. NR 204.07(7)(g). We made this determination based upon an environmental management system in which qualified personnel properly gather and evaluate information regarding pollutant concentrations, pathogen reduction, and vector attraction reduction. We are aware of the significant penalties for submitting false information, including the possibility of fine and imprisonment. Certified January jL 2019: � 't -j 0 _ Thomas A. Nowicki, Staff Attorney Certified January IJ 2019: To d Schwinglef peration Hager Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204'. Phone: (414) 221-6810 (800) 287-9645 Fax: (414) 221-6818 SusrainrngTurfgrarr Research info@milorganite.com www.milorganite.com `SLOW-RELEASE Ih Mmilorganoite NITROGEN FERTILIZER Summary of Sample Results 2018 Parameter Units Highest Day Annual Average Federal Limit Arsenic mg/kg 13 <6.31 41 Cadmium mg/kg 1.1 0.38 39 Chromium mg/kg 230 185 Copper mg/kg 240 204 1,500 Lead mg/kg 77 40 300 Mercury mg/kg 0.36 0.13 17 Molybdenum mg/kg 13 10 75 Nickel mg/kg 52 29 420 Selenium mg/kg 13 <6.71 100 Zinc mg/kg 570 440 2,800 PCB Aroclors (total) mg/kg 0.22 0.02 Dioxin TEQ1 pg/g 60 19 1. These annual averages were below the level of detection 2. TEQ is the sum of the concentrations of various dioxins, furans, and polychlorinated biphenyls multiplied by individual toxic equivalency factors, as established by the U.S. Environmental Protection Agency 't --IN M S Q PARTNERS FOR A CLEANER ENVIRONMENT January 18, 2019 Memorandum TO: Todd Schwingle, Dion Doege, Rodney Gross, Jacob Holbert, Brett Kelly, Sam Lieven FROM: Zach Vogel COPY: S. Unger, T. Nowicki, J. Spence, J. Staufenbeil, B. Stroik, A. Sotomayor, R. Vincent, Lab File SUBJECT: Annual Milorganite Report -2018 Attached is the Annual Milorganite report for the year 2018. The boron and mercury analyses were performed by CT Laboratories, in Baraboo, Wisconsin (Wisconsin Certification ID# 157066030). All other analyses were performed by Milwaukee Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #: 241325920, Florida NELAP Certification #: E571010). There was no Milorganite production on the following dates: a September 19 through September 20, 2018; a October 28 through November 6, 2018. Please contact the Central Laboratory if there are any questions or comments regarding these data. Data Review By: Report Review By: ec/&t'�J/ Richard Vincent Date Zach Vogel Date Laboratory Supervisor Laboratory Project Manager Milwaukee Metropolitan Sewerage District 260 West Seeboth Street, Milwaukee, WI 53204 Annual Milorganite Report January 1 to December 31, 2018 MMSD ALUMINUM ICP Dry wt. 02/10/18 WMC06/18001788 3700 mg/kg D.W. 66 210 68. SW846: 6010C MMSD 03/10/18 WMC10/18003337 3400 mg/kg D.W. 62 200 B8. SW846: 6010C MMSD 04/07/18 WMC14/18005097 4000 mg/kg D.W. 87 240 B8. SW846: 6010C MMSD 05/12/18 WMC19118007645 5500 mg/kg D.W. 80 220 B8. SW846: 6010C MMSD 06/09/18 WMC23/18009867 4900 mg/kg D.W. 86 240 B8. SW846: 6010C MMSD 07/07/18 WMC27118013254 4600 mg/kg D.W. 86 240 B8. SW846: 6010C MMSD 08/11/18 09/08/18 10/13/18 WMC32/18016218 WMC36/18018801 WMC41/18022042 4900 mg/kg D.W. 9000 mg/kg D.W. 10000 mg/kg D.W. 84 85 84 230 230 230 B8. B8. 88. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 11/17/18 WMC46/18024635 6800 mg/kg D.W. 85 230 B8. SW846: 6010C MMSD 12/08/18 WMC49/18026842 5500 mg/kg D.W. 86 240 B8. SW846: 6010C MMSD 11/17/18 Avg Result: 5500 mg/kg D.W. Min LOD: 62 mg/kg D.W. Max Result: 10000 mg/kg D.W. MMSD (Milo) Ammonia in Fertilizer 0.15 % 0.11 AOAC (13) 2.065 MMSD 01/13/18 WMCO2118000434 0.18% 0.11 ADAC (13) 2.065 MMSD 02/10/18 WMC06118001788 0.17% 0.11 AOAC (13) 2.065 MMSD 03/10/18 WMC10118003337 0.17% 0.11 AOAC (13) 2.065 MMSD 04/07/18 WMC14118005097 0.2 % 0.11 AOAC (13) 2.065 MMSD 05/12/18 WMC19/18007645 0.15 % 0.11 AOAC (13) 2.065 MMSD 06/09/18 WMC23/18009867 07/07/18 WMC27/18013254 08/11/18 WMC32/18016218 0.2% 0.11 0.24% 0.11 0.2% 0.11 AOAC (13) 2.065 MMSD AOAC (13) 2.065 MMSD AOAC (13) 2.065 MMSD 09/08/18 WMC36/18018801 0.24% 0.11 AOAC (13) 2.065 MMSD 10/13/18 WMC41/18022042 0.14% 0.11 AOAC (13) 2.065 MMSD 11/17/18 WMC46118024635 0.17% 0.11 AOAC (13) 2.065 MMSD 12/08/18 WMC49/18026842 0.15 % 0.11 AOAC (13) 2.065 MMSD Avg Result: 0.18 a/o Min LOD: 0.11 % Max Result: 0.24 0/6 Page 1 Of 106 SY5/rptlMi/oMonthly 1/10/13 hj Printed. 1/18/19 09:4) Annual Milorganite Report MMSDJanuary 1 to December 31, 2018 M10 F%j WUR xr ARSENIC ICP METHOD 01/01/18 DM0101/18000013 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C SW846: 6010C MMSD 01/02/18 DMO102/18000047 < 3.8 mg/kg D.W. 3.8 13 MMSD SW846: 6010C MMSD 01/03/18 DMO103/18000061 < 4 mg/kg D.W. 4 13 02/03/18 SW846: 6010C MMSD 01/04/18 DMO104118000098 5.2 mg/kg D.W. 3.8 13 J. SW846: 6010C MMSD 01/05/18 DMO105/18000155 5.5 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 01/06/18 DMO106/18000168 4.9 mg/kg D.W. 3.9 13 J. SW846: 6010C J MMSD 01/07/18 DMO107118000189 < 3.9 mg/kg D.W. 3.9 13 13 SW846: 6010C MMSD 01/08/18 DMO108/18000203 4.8 mg/kg D.W. 3.9 13 J. SW846: 6010C MMSD 01/09/18 DMO109/18000232 < 3.9 mg/kg D.W. 3.9 13 MMSD SW846: 6010C MMSD 01/10/18 DM0110118000326 < 3.9 mg/kg D.W. 3.9 13 02/11/18 SW846: 6010C MMSD 01/11/18 DMO 111/18000347 4.4 mg/kg D.W. 3.9 13 J. SW846: 6010C MMSD 01/12/18 DM0112118000363 < 3.9 mg/kg D.W. 3.9 13 < 3.9 mg/kg D.W. SW846: 6010C MMSD 01/13/18 DM0113118000397 < 3.9 mg/kg D.W. 3.9 13 3.8 SW846: 6010C MMSD 01/14/18 DM0114/18000418 < 3.9 mg/kg D.W. 3.9 13 13 SW846: 6010C MMSD 01/15/18 DM0115/18000432 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C SW846: 6010C MMSD 01/16/18 DM0116/18000461 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/17/18 DM0117/18000652 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/18/18 DM0118/18000673 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/19/18 DM0119/18000689 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/20/18 DMO120/18000702 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/21/18 DMO121/18000800 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/22/18 DMO122/18000814 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/23/18 DMO123/18000843 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/24/18 DMO124/18000875 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/25/18 DMO125/18000896 < 3.7 mg/kg D.W. 3.7 12 SW846: 6010C MMSD 01/26/18 DM0126/18000912 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/27/18 DMO127/18000925 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/28/18 DMO128/18000946 < 3.8 mg/kg D.W. 3.8 12 SW846-.6010C MMSD 01/29/18 DM0129/18001200 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/30/18 DM0130/18001229 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/31/18 DMO131/18001259 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/01/18 DM0201/18001280 4.2 mg/kg D.W. 3.9 13 J. SW846: 6010C MMSD 02/02/18 DM0202118001421 4.3 mg/kg D.W. 3.8 13 1 SW846: 6010C MMSD 02/03/18 DM0203/18001434 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/04/18 DM0204/18001455 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/05/18 DM0205/18001469 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/06/18 f DM0206/18001506 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/07/18 DM0207118001599 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/08/18 DM0208/18001620 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C a MMSD 02/09/18 DM0209/18001738 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/10/18 DM0210/18001751 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/11/18 DM0211/18001772 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/12/18 DM0212/18001786 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/13/18 DM0213/18001815 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/14/18 DM0214/18001860 4.1 mg/kg D.W. 3.8 13 J. SW846: 6010C MMSD 02/15/18 DM0215/18001881 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/16/18 DM0216/18001897 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD Page 2 of 106 SYSVIMMoMonthly 1/10/13 tj Printed.• 1/18/19 09:4; eN.MSD wlwvftlnftvvl ARSENIC ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 02/21/18 DM0221/18002077 < 3.9 mg/kg D.W. 3.9 13 02/22/18 DM0222/18002097 02/17/18 DM0217/18001944 < 3.8 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/18/18 DM0218/18001965 < 3.9 mg/kg D.W. 3.9 13 5W846: 6010C MMSD 02/19/18 DM0219/18001979 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/20/18 DM0220/18002047 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/21/18 DM0221/18002077 < 3.9 mg/kg D.W. 3.9 13 02/22/18 DM0222/18002097 < 3.8 mg/kg D.W. 3.8 13 02/23/18 DM0223/18002415 < 3.8 mg/kg D.W. 3.8 12 02/24/18 DM0224/18002427 < 3.9 mg/kg D.W. 3.9 13 02/25/18 DM0225/18002447 < 3.8 mg/kg D.W. 3.8 13 02/26/18 DM0226/18002461 < 3.8 mg/kg D.W. 3.8 13 02/27/18 DM0227/18002537 < 3.8 mg/kg D.W. 3.8 13 02/28/18 03/01/18 DM0228/18002609 DM0301/18002628 4 mg/kg D.W. < 3.9 mg/kg D.W. 3.9 3.9 13 J. 13 03/02/18 DM0302118002711 < 3.9 mg/kg D.W. 3.9 13 03/03/18 DM0303118002722 < 3.9 mg/kg D.W. 3.9 13 03/04/18 DM0304/18002741 < 3.9 mg/kg D.W. 3.9 13 03/05/18 DM0305/18002805 < 3.9 mg/kg D.W. 3.9 13 03/06/18 DM0306/18002862 4.1 mg/kg D.W. 3.9 13 1. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 03/07/18 DM0307/18002927 4.9 mg/kg D.W. 3.9 13 ]. SW846: 6010C MMSD 03/08/18 DM0308/18003015 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 03/09/18 DM0309/18003030 03/10/18 DM0310118003041 03/11/18 DM0311/18003060 03/12/18 03/13/18 DM0312/18003335 DM0313/18003681 03/14/18 DM0314/18003710 03/15/18 DM0315/18003729 03/16/18 DM0316118003744 03/17/18 DM0317/18003755 03/18/18 DM0318118003780 03/19/18 DM0319/18003911 03/20/18 DM0320/18003938 03/21/18 DM0321/18003967 03/22/18 DM0322/18004111 4.9 mg/kg D.W. 4 mg/kg D.W. 3.8 3.9 13 1. 13 1. SW846: 6010C SW846: 6010C MMSD MMSD < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 4.5 mg/kg D.W. < 4 mg/kg D.W. 4 4 13 J, Q3. 13 SW846: 6010C SW846: 6010C MMSD MMSD < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 4.2 mg/kg D.W. 3.9 13 J 4.9 mg/kg D.W. 3.9 13 J 5.6 mg/kg D.W. 4 13 1 < 3.9 mg/kg D.W. 3.9 13 < 4 mg/kg D.W. 4 13 < 3.8 mg/kg D.W. 3.8 13 03/23/18 DM0323/18004126 < 3.8 mg/kg D.W. 3.8 13 03/24/18 DM0324/18004137 < 3.9 mg/kg D.W. 3.9 13 03/25/18 DM0325/18004156 < 4 mg/kg D.W. 4 13 03/26/18 DM0326/18004320 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 03/27/18 DM0327/18004347 < 4 mg/kg D, W. 4 13 SW846: 6010C MMSD 03/28/18 DM0328/18004376 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 03/29/18 DM0329/18004395 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 03/30/18 DM0330/18004410 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 03/31/18 DM0331/18004752 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 04/01/18 DM0401/18004771 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 04/02/18 DM0402/18004784 < 3.9 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 04/03/18 DM0403/18004943 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 04/04/18 DM0404118004972 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD SYSIWIMMOMonthly 1/10/13 0 Page 3 of los Printed: 1/18/19 09:97 MMSD ARSENIC ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 SYSIrptlMAoMoMhly 1/10/13 h Page 4 of 106 Printed: 1/18/19 09:4; 04/05/18 DM0405/18005037 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/06/18 DM0406/18005052 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/07/18 DM0407/18005063 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 04/08/18 DM0408118005082 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 04/09/18 DM0409/18005095 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/10/18 DM0410/18005164 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/11/18 DM0411118005193 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/12/18 DM0412/18005446 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/13/18 DM0413/18005463 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/14/18 DM0414/18005474 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 04/15/18 DM0415/18005605 < 6.6 mg/kg D.W. 6.6 f 20 SW846: 6010C MMSD T 04/16/18 DM0416/18005618 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 04/17/18 DM0417/18005709 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 04/18/18 DM0418/18005738 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 04/19/18 DM0419/18005757 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 04/20/18 DM0420/18006009 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 04/21/18 DM0421/18006020 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 04/22/18 DM0422/18006039 < 6.4 mg/kg D.W. 6.4 19 SWB46: 6010C MMSD 04/23/18 DM0423/18006157 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 04/24/18 DM0424/18006185 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 04/25/18 DM0425/18006214 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 04/26/18 DM0426/18006233 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/27/18 DM0427/18006441 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 04/28/18 DM0428/18006452 <6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 04/29/18 DM0429/18006471 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 04/30/18 DM0430/18006484 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/01/18 DMO501/18006571 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/02/18 DMO502/18006600 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/03/18 DM0503/18006854 < 6.2 mg/kg D.W. 6.2 18 SW846: 6010C MMSD 05/04/18 DM0504/18007005 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 05/05/18 DM0505/18007016 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 05/06/18 DMO506/18007035 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 05/07/18 DMO507/18007257 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 05/08/18 DM0508/18007284 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C T MMSD 05/09/18 DM0509/18007313 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 05/10/18 DM0510/18007340 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/11/16 DMO511/18007418 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/12/18 DM0512/18007429 < 6.5 mg/kg D.W. 6.5 19 SWB46: 6010C MMSD 05/13/18 DMO513/18007476 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C ^` MMSD 05/14/18 DM0514/18007591 < 6.6 mg/kg D.W. 6.6 20 f SW846: 6010C MMSD 05/15/18 DM0515118007976 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 05/16/18 DM0516118008005 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 05/17/18 DMO517118008103 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C l MMSD 05/18/18 DMO518/18008118 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/19/18 DM0519/18008129 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 05/20/18 DM0520/18008196 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 05/21/18 DM0521118008209 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD SYSIrptlMAoMoMhly 1/10/13 h Page 4 of 106 Printed: 1/18/19 09:4; -ekNSD DMO606/18009404 06/07/18 DM0607/18009423 Annual Milorganite Report DM0608/18009822 < 6.4 mg/kg D.W. 6.4 19 B8, D2, Q3 < 6.5 mg/kg D.W. January 1 to December 31, 2018 19 < 6.3 mg/kg D.W. 6.3 19 < 6.5 mg/kg D.W. < 6.5 mg/kg D.W. ARSENIC ICP METHOD 19 19 < 6.3 mg/kg D.W. 6.3 19 < 6.5 mg/kg D.W. Resutt .. LOQ DM0613118010127 05/22/18 DM0522118008236 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 05/23/18 DM0523/18008304 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 05/24/18 DM0524/18008658 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 05/25/18 DM0525/18008673 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 05/26/18 DM0526/18008684 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 05/27/18 DM0527/18008703 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 05/28/18 05/29/18 05/30/18 05/31/18 06/01/18 06/02/18 06/03/18 06/04/18 06/05/18 DM0528/18008716 DM0529/18008888 DMO530/18008917 DM0531/18008936 DM0601118009150 DM0602/18009161 DM0603/18009335 DM0604/18009348 DM0605/18009375 06/06/18 DMO606/18009404 06/07/18 DM0607/18009423 06/08/18 DM0608/18009822 < 6.6 mg/kg D.W. 6.6 20 < 6.6 mg/kg D.W. 6.6 20 < 6.4 mg/kg D.W. 6.4 19 B8, D2, Q3 < 6.5 mg/kg D.W. 6.5 19 < 6.3 mg/kg D.W. 6.3 19 < 6.5 mg/kg D.W. < 6.5 mg/kg D.W. 6.5 6.5 19 19 < 6.3 mg/kg D.W. 6.3 19 < 6.5 mg/kg D.W. 6.5 20 < 6.6 mg/kg D.W. 6.6 20 < 6.5 mg/kg D.W. 6.5 19 < 6.3 mg/kg D.W. 6.3 19 06/09/18 DM0609/18009833 < 6.4 mg/kg D.W. 6.4 19 MMSD 06/10/18 DM0610/18009852 13 mg/kg D.W. 6.3 19 3. 06/11/18 DMO611118009865 < 6.5 mg/kg D.W. 6.5 20 Q2. 06/12/18 DM0612/18010098 < 6.6 mg/kg D.W. 6.6 20 B9. 06/13/18 DM0613118010127 < 6.6 mg/k9 D.W. 6.6 20 B8, D2. 06/14/18 DM0614/18010437 < 6.5 mg/kg D.W. 6.5 19 B8, Q2. 06/15/18 DM0615/18010452 < 6.4 mg/kg D.W. 6.4 19 B9. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 06/16/18 06/17/18 DM0616/18010463 DM0617118010482 < 6.4 mg/kg D.W. < 6.3 mg/kg D.W. 6.4 6.3 19 19� SW846: 6010C SW846: 6010C MMSD MMSD 06/16/18 DMO618/18010639 < 6.5 mg/kg D.W. 6.5 19 D2, Q3. SW846: 6010C MMSD 06/19/18 DM0619/18010666 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 06/20/18 DM0620118010694 < 6.3 mg/kg D.W. 6.3 19 B8. SW846: 6010C MMSD 06/21/18 DMO621/18010713 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 06/22/18 06/23/18 06/24/18 06/25/18 DM0622/18010939 DM0623/18010950 DM0624118011087 DM0625/18011182 < 6.2 mg/kg D.W. < 6.2 mg/kg D.W. < 6.4 mg/kg D.W. < 6.4 mg/kg D.W. 6.2 6.2 6.4 6.4 19 BB. 19 19 19 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 06/26/18 DM0626/18011209 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 06/27/18 DMO627/18011597 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 06/28/18 DM0628/18011616 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 06/29/18 06/30/18 DM0629/18011631 DM0630/18011642 < 6.5 mg/kg D.W. < 6.5 mg/kg D.W. 6.5 6.5 19 20 SW846: 6010C SW846: 6010C MMSD MMSD 07/01/18 DM0701/18011728 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/02/18 07/03/18 07/04/18 07/05/18 DM0702/18011741 DM0703118011881 DM0704/18011909 DM0705/18012390 < 6.5 mg/kg D.W. < 6.4 mg/kg D.W. < 6.3 mg/kg D.W. < 6.4 mg/kg D.W. 6.5 6.4 6.3 6.4 19 19 19 19 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 07/06/18 DM0706/18012405 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 07/07/18 DM0707/18012416 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD Page S of 106 SYS/rptlMiloManthly 1/10/13 q' Printed: 1/18/19 09:47 Annual Milorganite Report e:NNSD January 1 to December 31, 2018 ARSENIC ICP METHOD 07/08/18 DM0708118012435 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/09/18 DM0709/18012448 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 07/10/18 DM0710/18012474 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 07/11/18 DM0711/18012820 < 6.3 mg/kg D.W. 6.3 19 SW846-.6010C MMSD 07/12/18 DM0712/18012861 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/13/18 DM0713/18012876 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/14/18 DM0714/18013220 6.4 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 07/15/18 DM0715/18013239 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/16/18 DM0716/18013252 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/17/18 DM0717118013751 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/18/18 DM0718118013961 < 6.3 mg/kg D.W. 6.3 19 Q2. SW846: 6010C MMSD 07/19/18 DM0719/18014047 6.4 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 07/20/18 DM0720/18014062 < 6.4 mg/kg D.W. 6.4 19 Q2. SW846: 6010C MMSD 07/21/18 f DM0721118014073 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/22/18 DM0722/18014483 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/23/18 DM0723/18014496 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/24/18 DM0724/18014523 6.7 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 07/25/18 DM0725/18014551 < 6.5 m9/kg D.W. 6.5 20 SW846: 6010C MMSD 07/26/18 DM0726118014570 7.9 mg/kg D.W. 6.4 19 1. SW846: 6010C MMSD 07/27/18 DM0727/18014585 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/28/18 DM0728/18014676 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/29/18 DM0729/18014910 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 07/30/16 DM0730/18014925 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 07/31/18 DM0731/18014954 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 08/01/18 DM0801118014969 < 6.3 mg/kg D.W. 6.3 19 68. SW846: 6010C MMSD 08/02/18 DM0802/18015140 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/03/18 DM0803/18015155 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 08/04/18 DM0804/18015252 < 6.3 mg/kg D.W. 6.3 19 B8. SW846: 6010C MMSD 08/05/18 DM0805118015279 < 6.4 mg/kg D.W. 6.4 19 B8. SW846: 6010C MMSD 08/06/18 DM0806/18015385 < 6.3 mg/kg D.W. 6.3 19 88. SW846: 6010C MMSD 08/07/18 DM0807/18015414 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/08/18 DM0808118015473 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/09/18 DM0809/18015500 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/10/18 DM0810/18016899 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/11/18 DM0811/18015910 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/12/18 DM0812/18016203 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/13/18 DM0813/18016216 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/14/18 DMO814/18016254 < 6.3 mg/kg D.W. 6.3- 19 SW846: 6010C MMSD 08/15/18 DM0815/18016281 �< 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/16/18 DMO816/18016300 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 08/17/18 DMO817118016365 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/18/18 DM0818/18016505 < 6.3 mg/kg D.W. 6.3T 19 SW846: 6010C MMSD 08/19/18 DMO819118016525 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/20/18 DMO820/18016539 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 08/21/18 DM0821/18016714 6.7 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 08/22/18 DMO822/18016742 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 08/23/18 DMO823/18017352 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD Page 6 of 106 SYS/rptlM110monlhly 1/10/13 tj Panted' 1/19119 09:4; Annual Milorganite Report e14140 January 1 to December 31, 2018 +"T"IMIli�l�.�a f Er ARSENIC ICP METHOD 08/24/18 DMO824/18017367 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 08/25/18 DMO825/18017378 7.9 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 08/26/18 DMO826/18017397 6.6 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 08/27/18 DMO827/18017410 8 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 08/28/18 DM0828/18017434 8.6 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 08/29/18 DM0829/18017462 6.7 mg/kg D.W. 6.3 19 1 SW846: 6010C MMSD 08/30/18 DM0830/18017483 7.2 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 08/31/18 DMO831/18017498 7.3 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 09/01/18 DM0901/18017520 8.1 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/02/18 DM0902/18017752 8.5 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/03/18 DM0903/18018124 8.4 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 09/04/18 DM0904118018149 7.3 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 09/05/18 DMO905118018305 8.5 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 09/06/18 DM0906/18018326 7.8 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 09/07/18 DM0907/18018342 8.5 mg/kg D.W. 6.3 19 J. SW646: 6010C MMSD 09/08/18 DM0908/18018353 6.6 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/09/18 DMO909/18018724 7.3 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/10/18 DMO910/18018799 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 09/11/18 DM0911/18018825 7.6 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 09/12/18 DMO912/18018854 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 09/13/18 DM0913/18018875 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 09/14/18 DM0914/18018891 7.5 mg/kg D.W. 6.4 19 1 SW846: 6010C MMSD 09/15/18 DMO915/18019159 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 09/16/18 DM0916/18019178 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 09/17/18 DM0917/18019191 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 09/18/18 DM0918118019447 7.6 mg/kg D.W. 6.5 19 J. SW846: 6010C MMSD 09/21/18 DM0921/18019515 7.6 mg/kg D.W. 6.2 18 ]. SW846: 6010C MMSD 09/22/18 DM0922/18019574 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 09/23/18 DM0923/18019665 < 6.1 mg/kg D.W. 6.1 18 SW846: 6010C MMSD 09/24/18 DMO924/18020088 6.8 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/25/18 DM0925/18020314 7.2 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 09/26/18 DMO926/18020343 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 09/27/18 DM0927/18020364 6.4 mg/kg D.W. 6.4 19 1 SW846: 6010C MMSD 09/28/18 DM0928/18020380 13 mg/kg D.W. 6.6 20 J, Q3. SW846: 6010C MMSD 09/29/18 DMO929/18020391 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 09/30/18 DM0930/18020411 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 10/01/18 DM1001/18021136 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 10/02/18 DM1002/18021162 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 10/03/18 DM1003/18021190 6.6 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 10/04/18 DM1004/18021541 < 6.3 mg/kg D.W. 6.3 19 D2, Q3. SW846: 6010C MMSD 10/05/18 DM1005/18021557 11 mg/kg D.W. 6.3 19 D2, J, Q3. SW846: 6010C MMSD 10/06/18 DM1006/18021568 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 10/07/18 DM1007/18021588 6.3 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 10/08/18 DM1008/18021602 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C MMSD 10/09/18 DM1009/18021627 8.4 mg/kg D.W. 6.2 19 J. SW846: 6010C MMSD 10/10/18 DM1010/18021656 10 mg/kg D.W. 6.4 19 J. SW846: 6010C MMSD 10/11/18 DM1011118021975 9.1 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD Page 7 of 106 SY5/rpflMlloMonfhly 1/10/13 tj Printed., 1/18/19 09:4; el MMSD Mil1€Ri Fgt i CIFIAR iii Nff ARSENIC ICP METHOD 10/12/18 DM1012/18021991 9.2 mg/kg D.W. 6.2 10/13/18 DM1013/18022006 7.8 mg/kg D.W. 6.4 10/14/18 DM1014/18022026 7.9 mg/kg D.W. 6.4 10/15/18 DM1015/18022040 7.5 mg/kg D.W. 6.4 10/16/18 DM1016/18022065 9.4 mg/kg D.W. 6.3 10/17/18 DM1017/18022094 10/18/18 DM1018118022133 10/19/18 DM1019118022269 10/20/18 DM1020/18022280 8.2 mg/kg D.W. < 6.3 mg/kg D.W. 9 mg/kg D.W. < 6.3 mg/kg D.W. 10/21/18 DM1021/18022435 11 mg/kg D.W. 6.3 19 J. SW846: 6010C MMSD 10/22/18 DM1022/18022449 11 mg/kg D.W. 6.3 19 D2, J, Q3. SW846: 6010C MMSD 6.3 6.3 6.4 6.3 19 19 19 19 19 19 19 19 19 Annual Milorganite Report January 1 to December 31, 2018 ). SW846: 6010C J. SW846: 6010C MMSD MMSD I SW846: 6010C MMSD ~ J. SW846: 6010C I SW846: 6010C MMSD MMSD J. SW846: 6010C SW846: 6010C MMSD MMSD T I SW846: 6010C MMSD SW846: 6010C MMSD 10/23/18 DM1023118022614 < 6.3 mg/kg D.W. 6.3 19 MMSD 10/24/18 DM1024/18022643 < 6.4 mg/kg D.W. 6.4 19 D2, Q3. 10/25/18 DM1025/18022708 6.5 mg/kg D.W. 6.4 19 J. 10/26/18 DM1026/18022767 6.8 mg/kg D.W. 6.3 19 J. 10/27/18 DM1027/18022778 8.9 mg/kg D.W. 6.2 19 J. 11/07/18 DM1107118023991 7.8 mg/kg D.W. 6.2 19 J. 11/08/18 DM1108/18024012 < 6.2 mg/kg D.W. 6.2 19 SW846: 6010C 11/09/18 DM1109118024028 < 6.3 mg/kg D.W. 6.3 19 11/10/18 DM1110/18024523 < 6.2 mg/kg D.W. 6.2 19 11/11/18 DM1111/18024619 < 6.2 mg/kg D.W. 6.2 19 11/12/18 DM1112/18024633 < 6.4 mg/kg D.W. 6.4 19 11/13/18 DM1113/18025014 < 6.4 mg/kg D.W. 6.4 19 11/14/18 DM1114/18025043 < 6.4 mg/kg D.W. 6.4 19 11/15/18 DM1115/18025064 < 6.4 mg/kg D.W. 6.4 19 11/16/18 DM1116/18025080 < 6.6 mg/kg D.W. 6.6 20 11/17/18 DM1117/18025093 < 6.3 mg/kg D.W.6.3 19 11/18/18 DM1118/18025113 < 6.5 mg/kg D.W. 6.5 19 11/19/18 DM1119/18025127 < 6.3 mg/kg D.W. 6.3 19 11/20/18 DM1120/18025356 < 6.3 mg/kg D.W. 6.3 19 11/21/18 DM1121/18025385 < 6.3 mg/kg D.W. 6.3 19 11/22/18 DM1122/18025406 6.7 mg/kg D.W. 6.4 19 J. 11/23/18 DM1123/18025422 6.8 mg/kg D.W. 6.4 19 J. 11/24/18 DM1124/18025750 7.6 mg/kg D.W. 6.6 20 J. 11/25/18 DMI 125/18025769 < 6.6 mg/kg D.W. 6.6 20 11/26/18 DM1126/18025828 < 6.3 mg/kg D.W. 6.3 19 11/27/18 DM1127/18025860 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD v MMSD SW846: 6010C MMSD SW846: 6010C MMSD 11/28/18 DM 1128/18025888 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C 11/29/18 DM1129/18025956 < 6.4 mg/kg D.W. 6.4 19 Q2. SW846: 6010C 11/30/18 DM1130/18025971 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C 12/01/18 DM1201/18026182 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C 12/02/18 DM1202/18026201 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C 12/03/18 DM1203/18026214 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C 12/04/18 DM1204/18026391 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD 12/05/18 DM1205/18026578 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 12/06/18 DM1206/18026621 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 12/07/18 DM1207/18026797 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD SYS/rptINdoMonthly 1/10/13 tj Page 8 of 106 Punted; 1/18/19 09:4; Annual Milorganite Report Mmcn January 1 to December 31, 2018 12/26/18 DM1226/18027969 < 6.6 mg/kg D.W. 6.6 20 12/27/18 +tlRI ' "P I CHH ; < 6.6 mg/kg D.W. 6.6 20 12/28/18 DM1228/18028005 < 6.7 mg/kg D.W. ARSENIC ICP METHOD 9�1Mllll11lllllW�h-, 20 Q2. 12/29/18 DM1229118028070 < 6.4 mg/kg D.W. 6.4 12/08/18 10 DM1208/18026808 Result < 6.5 mg/kg D.W. LOD 6.5 LOQ QA Flags 20 ArwliO- SW846: 6010C MMSD 12/09/18 DM1209/18026827 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 12/10/18 DM1210/18026840 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 12/11/18 DM1211/18027102 < 6.3 mg/kg D.W. 6.3 19 68. SW846: 6010C MMSD 12/12/18 DM1212/18027130 < 6.3 mg/kg D.W. 6.3 19 B8. SW846: 6010C MMSD 12/13/18 DM1213/18027253 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 12/14/18 DM1214/18027306 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 12/15/18 DM1215/18027317 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 12/16/18 DM1216/18027525 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 12/17/18 DM1217/18027540 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 12/18/18 DM 1218/18027643 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 12/19/18 DM1219/18027676 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 12/20/18 DM1220/18027805 < 6.3 mg/kg D.W. 6.3 19 SW846: 6010C MMSD 12/21/18 DM1221/18027821 < 6.4 mg/kg D.W. 6.4 19 SW846: 6010C MMSD 12/22/18 DM1222/18027832 < 6.5 mg/kg D.W. 6.5 19 SW846: 6010C MMSD 12/23/18 DM1223/18027852 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 12/24/18 DM1224118027883 < 6.5 mg/kg D.W. 6.5 20 SW846: 6010C MMSD 12/25/18 DM1225/18027952 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 12/26/18 DM1226/18027969 < 6.6 mg/kg D.W. 6.6 20 12/27/18 DM1227/18027990 < 6.6 mg/kg D.W. 6.6 20 12/28/18 DM1228/18028005 < 6.7 mg/kg D.W. 6.7 20 Q2. 12/29/18 DM1229118028070 < 6.4 mg/kg D.W. 6.4 19 12/30/18 DM1230/18028089 < 6.3 mg/kg D.W. 6.3 19 12/31/18 DM1231/18028102 < 6.4 mg/kg D.W. 6.4 19 Avg Result: 1.4 mg/kg D.W. Min LOD: 3.7 mg/kg D.W. BORON ICP Dry wt. G`rii�il� rill 01/13/18 WMCO2/18000434 28 mg/kg D.W. 0.99 3.2 AX. 02/10/18 WMC06/18001788 03/10/18 WMC10/18003337 04/07/18 WMC14/18005097 05/12/18 WMC19118007645 06/09/18 WMC23/18009867 07/07/18 WMC27/18013254 08/11/18 WMC32/18016218 09/08/18 WMC36/18018801 10/13/18 WMC41/18022042 11/17/18 WMC46118024635 12/08/18 WMC49/18026842 Avg Result: 18 mg/kg D.W SW646:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Max Result: 13 mg/kg D.W. SW846: 6010C CT Lab 22 mg/kg D.W. 1.1 3.6 SW846: 6010C Cl- Lab 13 mg/kg D.W. 0.94 3 SW846: 6010C CT Lab 19 mg/kg D.W. 1.1 3.5 SWB46: 6010C CT Lab 14 mg/kg D.W. 1.5 4.9 SW846: 6010C CT Lab 17 mg/kg D.W. 1.1 3.3 SW846: 6010C CT Lab 7 mg/kg D.W. 0.58 1.9 SW846: 6010C CT Lab 18 mg/kg D.W. 1.1 3.5 SW846: 6010C CT Lab 22 mg/kg D.W. 1.1 3.7 16 mg/kg D.W. 1 3.3 22 mg/kg D.W. 1.1 3.3 22 mg/kg D.W. 1.2 3.7 Min LOD: 0.58 mg/kg D.W. SW846: 6010C CT Lab SW846: 6010C CT Lab SW846: 6010C CT Lab SW846: 6010C Cr Lab Max Result: 28 mg/kg D.W. Page 9 of 106 SYS/rpUMiloMonthly 1/10/13 U Printed: 1/18119 09:47 MMSD P.110l "1 Citi, CADMIUM ICP METHOD 01/01/18 01/02/18 DMO101/18000013 DMO102/18000047 < 0.88 mg/kg D.W. < 0.88 mg/kg D.W. i 0.88 0.88 1LDK 2.8 2.8 01/03/18 DMO103/18000061 < 0.9 mg/kg D.W. 0.9 2.9 01/04/18 DMO104/18000098 < 0.88 mg/kg D.W. 0.86 2.8 01/05/18 DMO105/18000155 < 0.9 mg/kg D.W. 0.9 2.8 01/06/18 DM0106/18000168 < 0.89 mg/kg D.W. 0.89 2.8 01/07/18 DMO107/18000189 < 0.89 mg/kg D.W. 0.89 2.8 Annual Milorganite Report January 1 to December 31, 2018 SW846:6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 01/08/18 DMO108118000203 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/09/18 DMO109/18000232 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 01/10/18 DM0110/18000326 < 0.88 mg/kg D.W. 0.88 2.8 T SW846: 6010C MMSD 01/11/18 DMO111/18000347 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 01/12/18 DM0112/18000363 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 01/13/18 DM0113/18000397 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/14/18 DMO114/18000418 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/15/18 DM0115/18000432 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/16/18 DM0116118000461 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/17/18 DM0117/18000652 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 01/18/18 DM0118118000673 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/19/18 DM0119/18000689 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/20/18 DMO120/18000702 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/21/18 DMO121/18000800 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/22/18 DMO122/18000814 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 01/23/18 DMO123/18000843 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C _ MMSD 01/24/18 DMO124/18000875 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/25/18 DMO125/18000896 < 0.85 mg/kg D.W. 0.85 2.7 SW846: 6010C MMSD 01/26/18 DMO126/18000912 < 0.86 mg/kg D.W. 0.66 2.7 SW846: 6010C MMSD 01/27/18 DMO127/18000925 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/28/18 DM0128/18000946 < 0.66 mg/kg D.W. 0.86 2.7 SW846: 6010C MMSD 01/29/16 DMO129/18001200 < 0.86 mg/kg D.W. 0.86 2.7 SW846: 6010C MMSD 01/30/18 DMO130/18001229 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/31/18 DMO131/18001259 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/01/18 DM0201/18001280 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/02/18 DM0202/18001421 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/03/18 DM0203/18001434 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/04/18 DM0204118001455 < 0.88 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 02/05/18 DM0205/18001469 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C _ MMSD 02/06/18 DM0206/18001506 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/07/18 DM0207/18001599 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/08/18 DM0208/18001620 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/09/18 DM0209/18001738 < 0.86 mg/kg D.W. 0.86 2.7 SW846: 6010C MMSD 02/10/18 DM0210/18001751 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/11/18 DM0211/18001772 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/12/18 DM0212/18001786 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/13/18 DM0213/18001815 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 02/14/18 DM0214/18001860 < 0.87 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/15/18 DM0215118001881 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/16/18 DM0216/18001897 < 0.67 mg/kg D.W. 0.87 2.7 SW846: 6010C MMSD Page 10 of 106 5Y5/rptlMiloMonthly 1/10/13 tJ Printed: 1/18/19 09:4; 02/23/18 DM0223/18002415 < 0.86 mg/kg D.W. 0.66 Annual Milorganite Report MMSDJanuary MMSD 02/24/18 02/25/18 02/26/18 DM0224/18002427 DM0225/18002447 DM0226/18002461 < 0.88 mg/kg D.W. < 0.86 mg/kg D.W. < 0.88 mg/kg D.W. 1 to December 31, 2018 i9l#11�! f911 [sf Ri3 4i71F3AMf v SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 02/27/18 DM0227/18002537 CADMIUM ICP METHOD 0.88 2.8 SW646: 6010C MMSD �ISiiliifsiilil , 'Resolt 02/17/18 DM0217/18001944 < 0.88 mg/kg D.W. LODLOQ 0.88 QA Ffts 2.8 Analytical Method L111 SW846: 6010C MMSD 02/18/18 DM0218118001965 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/19/18 DM0219/18001979 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 02/20/18 DM0220/18002047 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/21/18 DM0221/18002077 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 02/22/18 DM0222/18002097 0.98 mg/kg D.W. 0.87 2.8 3. SW846: 6010C MMSD 02/23/18 DM0223/18002415 < 0.86 mg/kg D.W. 0.66 2.7 SW846: 6010C MMSD 02/24/18 02/25/18 02/26/18 DM0224/18002427 DM0225/18002447 DM0226/18002461 < 0.88 mg/kg D.W. < 0.86 mg/kg D.W. < 0.88 mg/kg D.W. 0.88 0.86 0.88 2.8 2.7 2.8 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 02/27/18 DM0227/18002537 < 0.88 mg/kg D.W. 0.88 2.8 SW646: 6010C MMSD 02/28/18 03/01/18 03/02/18 03/03/18 DM0228/18002609 DM0301/18002628 DM0302118002711 DM0303/18002722 < 0.88 mg/kg DX < 0.89 mg/kg D.W. < 0.88 mg/kg D.W. < 0.89 mg/kg D.W. 0.88 0.89 0.88 0.89 2.8 2.8 2.8 2.8 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 03/04/18 DM0304/18002741 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 03/05/18 03/06/18 DM0305/18002805 )M0306/18002862 < 0.89 mg/kg D.W. < 0.89 mg/kg D.W. 0.89 0.89 2.8 2.8 SW846: 6010C SW846: 6010C MMSD MMSD 03/07/18 DM0307/18002927 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 03/08/18 03/09/18 DM0308/18003015 DM0309/18003030 < 0.88 mg/kg D.W. < 0.86 mg/kg D.W. 0.88 0.86 2.8 2.7 SW846: 6010C SW846: 6010C MMSD MMSD 03/10/18 03/11/18 DM0310/18003041 DM0311118003060< < 0.89 mg/kg D.W. 0.9 mg/kg D.W. 0.89 0.9 2.8 2.9 SW846: 6010C SW846: 6010C MMSD MMSD 03/12/18 DM0312/18003335 < 0.91 mg/kg D.W. 0.91 2.9 SW846: 6010C MMSD 03/13/18 DM0313/18003681 < 0.91 mg/kg D.W. 0.91 2.9 SW846: 6010C MMSD 03/14/18 DM0314/18003710 < 0.9 mg/kg D.W. 0.9 2.9 SW846: 6010C MMSD 03/15/18 DM0315/18003729 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 03/16/18 DM0316/18003744 < 0.9 mg/kg D.W. 0.9 2.9 SW846: 6010C MMSD 03/17/18 DM0317/18003755 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 03/18/18 DM0318/18003780 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 03/19/18 DM0319/18003911 < 0.92 mg/kg D.W. 0.92 2.9 SW846: 6010C MMSD 03/20/18 DM0320/18003938 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 03/21/18 03/22/18 03/23/18 DM0321/18003967 DM0322/18004111 DM0323/18004126 < 0.9 mg/kg D.W. < 0.87 mg/kg D.W. < 0.86 mg/kg D.W. 0.9 0.87 0.86 2.8 2.8 2.7 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 03/24/18 DM0324/18004137 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 03/25/18 DM0325/18004156 < 0.9 mg/kg D.W. 0.9 2.9 SW846: 6010C MMSD 03/26/18 DM0326/18004320 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 03/27/18 DMO327/18004347 < 0.91 mg/kg D.W. 0.91 2.9 SW846: 6010C MMSD 03/28/18 DM0328/18004376 < 0.9 mg/kg D.W. 0.9 2.8 SW846: 6010C MMSD 03/29/18 DM0329/18004395 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 03/30/18 DM0330/18004410 < 0.92 mg/kg D.W. 0.92 2.9 SW846: 6010C MMSD 03/31/18 DM0331118004752 < 0.88 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 04/01/18 DM0401/18004771 < 0.91 mg/kg D.W. 0.91 2.9 SW846: 6010C MMSD 04/02/18 DM0402/18004784 < 0.89 mg/kg D.W. 0.89 2.8 SW846: 6010C MMSD 04/03/18 DM0403118004943 < 0.31 mg/kg D.W. 0.31 1.4 SW846: 6010C MMSD 04/04/18 DM0404/18004972 < 0.3 mg/kg D.W. 0.3 1.4 SW846: 6010C MMSD SYS/rptlMiloMonthly 1/10/13 tj Page 11 of 106 Printed: 1/18/19 09:4; 04/09/18 04/10/18 DM0409/18005095 DM0410/18005164i 04/11/18 DM0411/18005193 04/12/18 DM0412/18005446 04/13/18 04/14/18^ 04/15/18 04/16/18 04/17/18 04/18/18 04/19/18 DM0419/18005757 04/20/18 DM0420/18006009 04/21/18 DM0421/18006020 04/22/18 DM0422/18006039 DM0413/18005463 DM0414/18005474 DM0415/18005605 DM0416/18005618 DM0417/18005709 DM0418/18005738 04/23/18 DM0423/18006157 04/24/18 DM0424/18006185 Annual Milorganite Report DM0425/18006214 MMSDJanuary DM0426/18006233 04/27/18 DM0427/18006441 04/28/18 1 to December 31, 2018 049TKM tR l MUM TiNMNiKitT DM0429/18006471 1.4 05/17/18 < 0.31 mg/kg D.W. CADMIUM ICP METHOD 1.4 DM0518/18008118 0.4 mg/kg D.W. 0.3 1.4 J. < 0.3 mg/kg D.W. 0.3 1.4 04/05/18 DM0405/18005037 < 0.3 mg/kg D.W. 0.3 1.4 SW846: 6010C MMSD 04/06/18 DM0406/18005052 0.31 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 04/07/18 DM0407/18005063 < 0.3 mg/kg D.W. 0.3 ^ 1.4 SW846: 6010C MMSD 04/08/18 DM0408/18005082 < 0.31 mg/kg D.W. 0.31 1.4 SW846: 6010C MMSD 04/09/18 04/10/18 DM0409/18005095 DM0410/18005164i 04/11/18 DM0411/18005193 04/12/18 DM0412/18005446 04/13/18 04/14/18^ 04/15/18 04/16/18 04/17/18 04/18/18 04/19/18 DM0419/18005757 04/20/18 DM0420/18006009 04/21/18 DM0421/18006020 04/22/18 DM0422/18006039 DM0413/18005463 DM0414/18005474 DM0415/18005605 DM0416/18005618 DM0417/18005709 DM0418/18005738 04/23/18 DM0423/18006157 04/24/18 DM0424/18006185 04/25/18 DM0425/18006214 04/26/18 DM0426/18006233 04/27/18 DM0427/18006441 04/28/18 DM0428/18006452 04/29/18 DM0429/18006471 04/30/18 05/01/18 05/02/18 05/03/18 05/04/18 05/05/18 05/06/18 DM0430/18006484 DMO501 /18006571 DM0502/18006600 DM0503/18006854 DM0504/18007005 DM0505/18007016 DM0506/18007035 < 0.31 mg/kg D.W. 0.31 1.4 < 0.31 mg/kg D.W. 0.31 1.4 < 0.31 mg/kg D.W. 0.31 1.4 05/10/18 0.33 mg/kg D.W. 0.31 1.4 J. < 0.31 mg/kg D.W. 0.31 1.4 0.48 mg/kg D.W. 0.37 mg/kg D.W. < 0.3 mg/kg D.W. 0.3 1.4 05/17/18 < 0.31 mg/kg D.W. 0.31 1.4 DM0518/18008118 0.4 mg/kg D.W. 0.3 1.4 J. < 0.3 mg/kg D.W. 0.3 1.4 MMSD 0.36 mg/kg D.W. 0.3 1.4 J. < 0.3 mg/kg D.W. 0.3 1.4 MMSD < 0.29 mg/kg D.W. 0.29 1.4 MMSD 0.41 mg/kg D.W. 0.3 1.4 J. 0.52 mg/kg D.W. 0.3 1.4 J. 0.4 mg/kg D.W. 0.3 1.4 J. 0.44 mg/kg D.W. 0.3 1.4 J. 0.52 mg/kg D.W. 0.32 1.5 J. 0.36 mg/kg D.W. 0.31 1.4 J. 0.37 mg/kg D.W. 0.29 1.4 J. 0.52 mg/kg D.W. 0.31 1.4 J. 0.36 mg/kg D.W. 0.3 1.4 J. < 0.31 mg/kg D.W. 0.31 1.4 < 0.31 mg/kg D.W. 0.31 1.4 0.34 mg/kg D.W. 0.31 1.4 J. 0.31 mg/kg D.W. 0.29 1.3 J. 0.33 mg/kg D.W. 0.3 1.4 J. 0.39 mg/kg D.W. 0.3 1.4 J. 0.35 mg/kg D.W. 0.3 1.4 J. 05/07/18 DM0507118007257 0.38 mg/kg D.W. 0.3 1.4 J. 05/08/18 05/09/18 DM0508/18007284 DM0509118007313 < 0.3 mg/kg D.W. < 0.3 mg/kg D.W. 05/10/18 DMO510/18007340 0.31 mg/kg D.W. 05/11/18 05/12/18 05/13/18 DMO511/18007418 DM0512118007429 DM0513/18007476 0.48 mg/kg D.W. 0.42 mg/kg D.W. w 0.37 mg/kg D.W. 05/14/18 05/15/18 DM0514/18007591 DM0515/18007976 0.48 mg/kg D.W. 0.37 mg/kg D.W. 05/16/18 DM0516/18008005 0.51 mg/kg D.W. 05/17/18 DMO517/18008103 0.38 mg/kg D.W. 05/18/18 DM0518/18008118 0.43 mg/kg D.W. 05/19/18 DM0519/18008129 0.43 mg/kg D.W. 05/20/18 DM0520118008196 05/21/18 DMO521/18008209 5Y51notimilomonthly 1/10/13 U 0.37 mg/kg D.W. 0.56 mg/kg D.W. 0.3 1.4 0.3 1.4 0.31 1.4 0.31 1.4 0.3 1.4 0.3 1.4 0.31 1.4 0.29 1.4 0.3 1.4 0.3 1.4 0.31 1.4 0.3 1.4 0.3 1.4 0.3 1.4 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 12 of 106 Printed: 1/18/19 09:4; ,-?,kmsD. DMO526/18008684 05/27/18 DM0527/18008703 05/28/18 Annual Milorganite Report 05/29/18 DM0529/18008888 05/30/18 DM0530/18008917 05/31/18 DM0531/18008936 January 1 to December 31, 2018 "t"M OR + CROT B{I Rr 06/02/18 06/03/18 DMO602/18009161 DM0603/18009335 SW846: 6010C MMSD 0.57 mg/kg D.W. CADMIUM ICP METHOD 1.4 J. SW846: 6010C MMSD 0.55 mg/kg D.W. 0.44 mg/kg D.W. 05/22/18 DM0522/18008236 0.36 mg/kg D.W. O. 0.31 LOQ .- 1.4 flags J. Arta lybcal Method Lab SW846: 6010C MMSD 05/23/18 DM0523/18008304 0.33 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 05/24/18 DM0524118008658 0.37 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 05/25/16 DMO525/18008673 0.47 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 05/26/18 DMO526/18008684 05/27/18 DM0527/18008703 05/28/18 DM0528/18008716 05/29/18 DM0529/18008888 05/30/18 DM0530/18008917 05/31/18 DM0531/18008936 06/01/18 DMO601/18009150 06/02/18 06/03/18 DMO602/18009161 DM0603/18009335 0.5 mg/kg D.W. 0.29 1.4 J 0.36 mg/kg D.W. 0.3 1.4 J SW846: 6010C MMSD SW846: 6010C MMSD 0.33 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 0.43 mg/kg D.W. 0.78 mg/kg D.W. 0.31 0.3 1.4 1.4 J. J. SW846: 6010C SW846: 6010C MMSD MMSD 0.45 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 0.57 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 0.55 mg/kg D.W. 0.44 mg/kg D.W. 0.3 0.3 1.4 1.4 J. J. SW846: 6010C SW846: 6010C MMSD MMSD 06/04/18 DMO604/18009348 0.44 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/05/18 DM0605/18009375 0.43 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/06/18 DM0606/18009404 0.56 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 06/07/18 DM0607/18009423 0.58 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/08/18 DM0608/18009822 0.58 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/09/18 DM0609/18009833 0.59 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/10/18 DM0610/18009852 0.64 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 06/11/18 DM0611/18009865 T 0.59 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/12/18 DMO612/18010098 0.58 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 06/13/18 DM0613/18010127 0.61 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 06/14/18 DM0614/18010437 0.6 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/15/18 DM0615/18010452 0.69 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/16/18 DM0616118010463 0.64 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/17/18 DM0617/18010482 0.52 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/18/18 DMO618/18010639 0.61 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/19/18 DM0619/18010666 0.61 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/20/18 DM0620/18010694 0.62 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 06/21/18 DM0621/18010713 0.6 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 06/22/18 DM0622/18010939 0.61 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 06/23/18 06/24/18 06/25/18 DM0623/18010950 DM0624/18011087 DM0625/18011182 0.63 mg/kg D.W. 0.66 mg/kg D.W. 0.54 mg/kg D.W. 0.29 0.3 0.3 1.4 1.4 1.4 J. J. J. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 06/26/18 DM0626/18011209 0.7 mg/kg D.W. 0.3 1.4 1 SW846: 6010C MMSD 06/27/18 DM0627/18011597 0.43 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/28/18 DM0628/18011616 0.86 mg/kg D.W. 0.3 1.4 J, Q3. SW846: 6010C MMSD 06/29/18 DM0629/18011631 0.61 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 06/30/18 07/01/18 DM0630/18011642 DM0701/18011728 0.67 mg/kg D.W. 0.99 mg/kg D.W. 0.3 0.3 1.4 1.4 J. J. SW846: 6010C SW846: 6010C MMSD MMSD 07/02/18 DM0702118011741 0.49 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 07/03/18 DM0703/18011881 0.85 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 07/04/18 07/05/18 DM0704/18011909 DM0705/18012390 0.48 mg/kg D.W. 0.52 mg/kg D.W. 0.29 0.3 1.4 1.4 B7, J. B7, J. SW846: 6010C SW846: 6010C MMSD MMSD 07/06/18 DM0706/18012405 0.58 mg/kg D.W. 0.3 1.4 B7, J. SW846: 6010C MMSD 07/07/18 DM0707/18012416 5Y5/rptimllomanthly 1/10/13 tj 0.77 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD Page 13 of 106 Printed: 1/18/19 09:4; eM,MSD FR A CUM fiflMr, CADMIUM ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 Sample ID ResUlt LOD 0Q 4)-ARags AnalVticaf Method Lab 07/08/18 DM0708/18012435 0.85 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 07/09/18 DM0709/18012448 1 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 07/10/18 07/11/18 07/12/18 07/13/18 07/14/18 07/15/18 07/16/18 07/19/18 07/20/18 07/21/18 07/22/18 07/23/18 07/24/18 07/25/18 07/26/18 07/27/18 07/28/18 07/29/18 07/30/18 07/31/18 08/01/18 DM0710/18012474 1 mg/kg D.W. 0.3 1.4 DM0711/18012820 1 mg/kg D.W. 0.3 1.4 DM0712/18012861 0.6 mg/kg D.W. 0.3 1.4 DM0713/18012876 0.57 mg/kg D.W. 0.3 1.4 DM0714118013220 0.72 mg/kg D.W. 0.3 1.4 DM0715118013239 0.6 mg/kg D.W. 0.3 1.4 DM0716/18013252 0.54 mg/kg D.W. 0.3 1.4 DM0717/18013751 < 0.29 mg/kg D.W. 0.29 1.4 DM0718/18013961 0.61 mg/kg D.W. 0.3 1.4 DM0719/18014047 0.46 mg/kg D.W. 0.29 1.4 DM0720/18014062 < 0.3 mg/kg D.W. 0.3 1.4 DM0721/18014073 0.3 mg/kg D.W. 0.3 1.4 DM0722/18014483 < 0.3 mg/kg D.W. 0.3 1.4 DM0723/18014496 0.36 mg/kg D.W. 0.3 1.4 DM0724/18014523 < 0.3 mg/kg D.W. 0.3 1.4 DM0725/18014551 0.42 mg/kg D.W. 0.3 1.4 DM0726/18014570 0.57 mg/kg D.W. 0.3 1.4 DM0727/18014585 0.52 mg/kg D.W. 0.3 1.4 DM0728/18014676 0.5 mg/kg D.W. 0.29 1.4 DM0729118014910 0.55 mg/kg D.W. 0.29 1.4 DM0730/18014925 0.52 mg/kg D.W. 0.3 1.4 DM0731/18014954 0.46 mg/kg D.W. 0.3 1.4 DMO801/18014969 0.43 mg/kg D.W. 0.29 1.4 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C ]. SW846: 6010C J. SW846: 6010C J. SW846: 6010C B8, I SW846: 6010C B8, J. SW846: 6010C B8, J. SW846: 6010C B8, J. SW846: 6010C B8, J. SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD 08/02/18 DMO802/18015140 0.46 mg/kg D.W. 0.3 1.4 B8, J. SW846: 6010C MMSD 08/03/18 DM0803/18015155 0.54 mg/kg D.W. 0.3 1.4 B8, J. SW846: 6010C MMSD 08/04/18 DMO804/18015252 0.43 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/05/18 DM0805/18015279 0.49 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 08/06/18 DMO806/18015385 0.74 mg/kg D.W. 0.29 1.4 1 SW846: 6010C MMSD 08/07/18 DMO807118015414 0.55 mg/kg D.W. 0.29 1.4 B8, J. SW846: 6010C MMSD 08/08/18 DMO808/18015473 0.47 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/09/18 DMO809/18015500 0.63 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/10/18 DM0810/18015899 0.46 mg/kg D.W. 0.29 1.4 B8, J. SW846: 6010C MMSD 08/11/16 DM0811/18015910 0.52 mg/kg D.W. 0.29 1.4 1. SW846: 6010C MMSD 08/12/18 DM0812/18016203 0.6 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/13/18 DM0813/18016216 0.46 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/14/18 DM0814/18016254 0.4 mg/kg D.W. 0.29 1.4 J, Q3. SW846: 6010C MMSD 08/15/18 DM0815/18016281 0.52 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/16/18 DM0816/18016300 0.65 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/17/18 DMO817/18016365 0.58 mg/kg D.W. 0.29 1.4 J. �! SW846: 6010C MMSD 08/18/18 DM0818/18016505 0.56 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/19/18 DM0819/18016525 0.54 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/20/18 DM0820/18016539 0.5 mg/kg D.W. 0.29 1.4 1 SW846: 6010C MMSD 08/21/18 DMO821/18016714 0.58 mg/kg D.W. 0.3 1.4 1 SW846: 6010C MMSD 08/22/18 T� DMOB22118016742 0.37 mg/kg D.W. 0.29 1.4 1 SW846: 6010C MMSD 08/23/18 DM0823/18017352 0.52 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD Page 14 of 106 SYS/rptimiloMonthly 1/10/13 tj Printed: 1118/19 09:42 'e-kNSD rtrgw 4Mt tliwv Fl"w't CADMIUM ICP METHOD ■ a Result LOD L0,Q QA Flags Annual Milorganite Report January 1 to December 31, 2018 Analytkal MeUwd Lab 08/24/18 DMO824/18017367 0.61 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 08/25/18 DM0825/18017378 0.63 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/26/18 DM0826/18017397 0.59 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 08/27/18 DM0827/18017410 0.54 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 08/28/18 08/29/18 08/30/18 DM0828/18017434 DM0829/18017462 DM0830118017483 0.66 mg/kg D.W. 0.83 mg/kg D.W. 0.57 mg/kg D.W. 0.29 0.29 0.3 1.4 1.4 1.4 J. J. J. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 08/31/18 DMOB31/18017498 0.79 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 09/01/18 DM0901/18017520 0.61 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 09/02/18 DM0902/18017752 0.6 mg/kg D.W. 0.29 1.4 1 SW846: 6010C MMSD 09/03/18 DM0903/18018124 0.47 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 09/04/18 09/05/18 DM0904/18018149 DM0905/18018305 0.56 mg/kg D.W. 0.72 mg/kg D.W. 0.3 0.3 1.4 1.4 J. J. SW846: 6010C SW846: 6010C MMSD MMSD 09/06/18 DMO906/18018326 0.62 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 09/07/18 09/08/18 09/09/18 09/10/18 DM0907/18018342 DMO908/18018353 DMO909/18018724 DMO910118018799 0.85 mg/kg D.W. 0.68 mg/kg D.W. 0.67 mg/kg D.W. 0.81 mg/kg D.W. 0.29 0.29 0.29 0.3 1.4 1.4 1.4 1.4 J. J. J. J. SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 09/11/18 09/12/18 09/13/18 09/14/18 09/15/18 09/16/18 09/17/18 DM0911/18018825 DM0912118018854 DMO913/18018875 DMO914/18018891 DM0915/18019159 DM0916/18019178 DM0917/18019191 0.61 mg/kg D.W. 0.8 mg/kg D.W. 0.62 mg/kg D.W. 0.61 mg/kg D.W. 0.79 mg/kg D.W. 0.64 mg/kg D.W. 0.66 mg/kg D.W. 0.3 0.3 0.3 0.3 0.3 0.3 0.29 1.4 1.4 1.4 1.4 1.4 1.4 1.4 ]. J. J, Q3. J. J. J. J. SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD 09/18/18 09/21/18 09/22/18 DM0918/18019447 DMO921/18019515 DMO922/18019574 0.87 mg/kg D.W. 0.39 mg/kg D.W. 0.79 mg/kg D.W. 0.3 0.29 0.29 1.4 1.3 1.4 J. J. J. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 09/23/18 DM0923/18019665 0.61 mg/kg D.W. 0.28 1.3 J. SW846: 6010C MMSD 09/24/18 DM0924118020088 0.76 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 09/25/18 DMO925/18020314 0.59 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 09/26/18 DM0926/18020343 0.64 mg/kg D.W. 0.3 1.4 1 SW846: 6010C MMSD 09/27/18 09/28/18 DMO927/18020364 DM0928/18020380 0.67 mg/kg D.W. 0.7 mg/kg D.W. 0.3 0.3 1.4 1.4 B8, J. B8, 1. SW846: 6010C SW846: 6010C MMSD MMSD 09/29/18 DMO929/18020391 0.79 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 09/30/18 DM0930/18020411 0.72 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/01/18 DM1001/18021136 0.76 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 10/02/18 DM1002118021162 0.69 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/03/18 DM1003/18021190 0.56 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/04/18 DM1004/18021541 0.76 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 10/05/18 DM1005/18021557 0.58 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/06/18 DM1006/18021568 0.6 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/07/18 DM1007/18021588 0.42 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 10/08/18 DM1008/18021602 0.64 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 10/09/18 DM1009/18021627 0.5 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 10/10/18 DM1010/18021656 1.1 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/11/18 DM1011/18021975 0.66 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD SYS/rpti iloMonth/y 1/10/13 ry Page 15 of 106 Printed: 1/18/19 09:4; t 7 NMsr falf?ItFRi as ,1 MOR I1@�I#Mt CADMIUM ICP METHOD 10/12/16 DM1012/18021991 10/13/18 DM1013118022006 10/14/18 DM1014/18022026 10/15/18 DM1015/18022040 10/16/18 DM1016/18022065 Annual Milorganite Report January 1 to December 31, 2018 0.62 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 0.66 mg/kg D.W. 0.73 mg/kg D.W. 0.3 0.3 1.4 1.4 J. J. SW846: 6010C SW846: 6010C MMSD MMSD 0.71 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 0.74 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/17/18 DM1017/18022094 0.65 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 10/18/18 DM1018/18022133 0.62 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 10/19/18 DM1019/18022269 T 0.86 mg/kg D.W. 0.3 1.4 J. T SW846: 6010C MMSD 10/20/18 DM1020/18022280 0.46 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 10/21/18 DM1021/18022435 0.54 mg/kg D.W. 10/22/18 DM1022118022449 0.53 mg/kg D.W. 10/23/18 10/24/18 DM1023/18022614 DM1024/18022643 0.61 mg/kg D.W. 0.48 mg/kg D.W. 10/25/18 DM1025118022708 0.48 mg/kg D.W. 10/26/18 DM1026/18022767 0.68 mg/kg D.W. 10/27/18 DM1027/18022778 0.56 mg/kg D.W. 11/07/18 11/08/18 DM1107/18023991 DM 1108/18024012 0.47 mg/kg D.W. 0.59 mg/kg D.W. 11/09/18 DM 1109/18024028 0.63 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 0.29 1.4 J. SW846: 6010C MMSD 0.3 1.4 J. SW846: 6010C MMSD 0.3 1.4 J. SW846: 6010C MMSD 0.3 1.4 1 SW846: 6010C MMSD 0.29 1.4 J. SW846: 6010C MMSD 0.29 1.3 J. SW846: 6010C MMSD 0.29 1.3 J. SW846: 6010C MMSD 0.29 1.4 J. SW846: 6010C MMSD 0.29 1.4 J. SW846: 6010C MMSD 11/10/18 DM1110/18024523 0.48 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 11/11/18 DM1111/18024619 0.54 mg/kg D.W. 0.29 1.3 J. SW846: 6010C MMSD 11/12/18 DM1112/18024633 0.52 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 11/13/18 DMI 113/18025014 0.4 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 11/14/18 DM1114/18025043 0.48 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 11/15/18 DM1115/18025064 0.5 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 11/16/18 DM1116/18025080 0.44 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 11/17/18 DM1117118025093 0.5 mg/kg D.W. 0.3 1.4 J. SW846 6010C MMSD 11/18/18 DM1118/18025113 0.39 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 11/19/18 11/20/16 DM 1119118025127 DM 1120/18025356 0.4 mg/kg D.W. 0.54 mg/kg D.W. 0.3 0.29 1.4 1.4 J. J. 11/21/16 DM 1121/18025385 0.34 mg/kg D.W. 0.3 1.4 J. 11/22/18 DMI 122/18025406 0.5 mg/kg D.W. 0.3 1.4 J. 11/23/18 DM 1123/18025422 0.56 mg/kg D.W. 0.3 1.4 J. 11/24/18 DM1124/18025750 0.68 mg/kg D.W. 0.31 1.4 J. 11/25/18 DM1125/18025769 0.4 mg/kg D.W. 0.3 1.4 J. 11/26/18 DM1126/18025828 0.4 mg/kg D.W. 0.29 1.4 J. 11/27/18 DM1127/18025860 0.36 mg/kg D.W. 0.29 1.4 J. 11/28/18 DM1128/18025888 0.31 mg/kg D.W. 0.29 1.4 J. 11/29/18 DM1129/18025956 0.38 mg/kg D.W. 0.3 1.4 J. 11/30/18 DM1130/18025971 < 0.3 mg/kg D.W. 0.3 1.4 12/01/18 DM1201/18026182 0.55 mg/kg D.W. 0.3 1.4 J. 12/02/18 DM1202118026201 0.55 mg/kg D.W. 0.3 1.4 J. 12/03/18 DM1203/18026214 0.51 mg/kg D.W. 0.3 1.4 J. 12/04/18 DM1204/18026391 0.35 mg/kg D.W. 0.3 1.4 J. 12/05/18 DM1205/18026578 0.51 mg/kg D.W. 0.3 1.4 J. 12/06/18 DM1206/18026621 0.38 mg/kg D.W. 0.31 1.4 J. 12/07/18 DM1207/18026797 SYS/rptlMiloMonthly 1/10/13 tj 0.56 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD Page 16 of 106 Printed: 1/18/19 09.•4; MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD Avg Result: 180 mg/kg D.W. Min LOD: 0.48 mg/kg D.W. Max Result: 230 mg/kg D.W. Page 17 of 106 SYS/rptlMiloMonthly 1/10113 tj Printed.- 1/18119 09:47 Annual Milorganite Report eims - January 1 to December 31, 2018 alrUrS PXl 0W CADMIUM ICP METHOD Date le ID Resuft .. LOQ QA flags Analytical methiXf Lab 12/08/18 DM1208/18026808 0.9 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/09/18 DM1209118026827 0.83 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/10/18 DM1210118026840 0.82 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/11/18 DM1211/18027102 0.88 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/12/18 DM1212/18027130 0.8 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 12/13/18 DM1213/18027253 0.35 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/14/18 DM1214/18027306 0.51 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/15/18 DM1215/18027317 0.34 mg/kg D.W. 0.3 1.4 J. SW646: 6010C MMSD 12/16/18 DM1216/18027525 0.58 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/17/18 DM1217/18027540 0.57 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/18/18 J DM1218118027643 0.37 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/19/18 DM1219118027676 0.43 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/20/18 DM1220/18027805 < 0.3 mg/kg D.W. 0.3 1.4 SW846: 6010C MMSD 12/21/18 DM1221118027821 0.53 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/22/18 DM1222/18027832 0.57 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/23/18 DM1223/18027852 0.5 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/24/18 DM1224/18027883 0.54 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/25/18 DM1225118027952 0.51 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/26/18 DM1226/18027969 0.56 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/27/18 DM1227/18027990 < 0.31 mg/kg D.W. 0.31 1.4 SW846: 6010C MMSD 12/28/18 DM1228/18028005 0.32 mg/kg D.W. 0.31 1.4 J. SW846: 6010C MMSD 12/29/18 DM1229/18028070 y 0.58 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD 12/30/18 DM1230/18028089 0.53 mg/kg D.W. 0.29 1.4 J. SW846: 6010C MMSD 12/31/18 DM1231/18028102 0.5 mg/kg D.W. 0.3 1.4 J. SW846: 6010C MMSD Avg Result: 0.38 mg/kg D.W. Min LOD: 0.28 mg/kg D.W. Max Result: 1.1 mg/kg D.W. CHROMIUM ICP Dry wt. .`0 LOQ QA Flags Analytical Method Lab 01/13/18 WMCO2/18000434 130 mg/kg D.W. 0.52 1.7 SW846: 6010C MMSD 02/10/18 WMC06/18001788 160 mg/kg D.W. 0.51 1.7 B8. SW846: 6010C MMSD 03/10/18 WMC10/18003337 160 mg/kg D.W. 0.48 1.6 B8. SW846: 6010C MMSD 04/07/18 WMC14/18005097 170 mg/kg D.W. 1.4 4.4 B8. SW846: 6010C MMSD 05/12/18 WMC19/18007645 160 mg/kg D.W. 1.3 4 B8. SW846: 6010C MMSD 06/09/18 WMC23/18009867 220 mg/kg D.W. 1.4 43 SW846: 6010C MMSD 07/07/18 WMC27/18013254 200 mg/kg D.W. 1.4 4.3 SW846: 6010C MMSD 08/11/18 WMC32/18016218 170 mg/kg D.W. 1.4 4.2 B8. SW846: 6010C MMSD 09/08/18 WMC36/18018801 230 mg/kg D.W. 1.4 4.2 SW846: 6010C MMSD 10/13/18 WMC41/18022042 180 mg/kg D.W. 1.4 4.2 B8. SW846: 6010C MMSD 11/17/18 WMC46118024635 230 mg/kg D.W. 1.4 4.2 B8. SW846: 6010C MMSD 12/08/18 WMC49118026842 210 mg/kg D.W. 1.4 4.3 B8. SW846: 6010C MMSD Avg Result: 180 mg/kg D.W. Min LOD: 0.48 mg/kg D.W. Max Result: 230 mg/kg D.W. Page 17 of 106 SYS/rptlMiloMonthly 1/10113 tj Printed.- 1/18119 09:47 NNSD iA f0t) CUMIX [*VWW COBALT ICP Dry wt. 01/13/18 WMCO2/18000434 02/10/18 WMC06/18001788 3.9 mg/kg D.W. 1.7 5.4 B8, 1. 3.6 mg/kg D.W. 1.7 5.3 B8, 1. Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C MMSD SW846: 6010C T MMSD 03/10/18 WMC10118003337 3.6 mg/kg D.W. 1.6 5 B8, 1, Q2. SW846: 6010C MMSD 04/07/18 WMC14/18005097 3.6 mg/kg D.W. 1.2 3.5 B8. SW846: 6010C MMSD 05/12/18 WMC19/18007645 3.2 mg/kg D.W. 1.1 3.2 B8. SW846: 6010C MMSDf 06/09/18 WMC23118009867 4.5 mg/kg D.W. 1.2 3.4 B8. SW846: 6010C MMSD 07/07/18 WMC27/18013254 4.2 mg/kg D.W. 1.2 3.4 B8. SW846: 6010C MMSD 08/11/18 WMC32/18016218 4.1 mg/kg D.W. 1.1 3.4 B8. SW846: 6010C MMSD 09/08/18 WMC36/18018801 4.4 mg/kg D.W. 1.1 3.4 B8, Q3. SW846: 6010C MMSD 10/13/18 WMC41/18022042 4.2 mg/kg D.W. 1.1 3.4 B8. SW846: 6010C MMSD 11/17/18 WMC46/18024635 3.6 mg/kg D.W. 1.1 3.4 68, Q2. SW846: 6010C MMSD 12/08/18 WMC49118026842 3.9 mg/kg D.W. 1.2 3.4 B8. SW846: 6010C MMSD Avg Result: 3.9 mg/kg D.W. Min LOD: 1.1 mg/kg D.W. Max Result: 4.5 mg/kg D.W. SYSIrptlMiloManthly 1/10/13 tj Page 18 of 106 Printed., 1118119 09:91 ;, Annual Milorganite Report .kNSD January 1 to December 31, 2018 M94W. FY 1 a(Ulf C+�+ 1f� COPPER ICP METHOD Sample Date Sample ID Result LOD LOQ QA Flags AnaNtical Method Lab 01/01/18 DMO101/18000013 200 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/02/18 DMO102/18000047 210 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/03/18 DMO103118000061 200 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 01/04/18 DMO104/18000098 200 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/05/18 DMO105/18000155 200 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 01/06/18 DMO106/18000168 200 mg/kg D.W. 3 10 SW846: 6010C MMSD 01/07/18 DMO107/18000189 200 mg/kg D.W. 3 10 SW846: 6010C MMSD 01/08/18 DMO108/18000203 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/09/18 DMO109/18000232 210 mg/kg D.W. 3 10 SW846: 6010C MMSD 01/10/18 DM0110/18000326 200 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/11/18 DM0111/18000347 220 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/12/18 DM0112/18000363 200 mg/kg D.W. 3 10 SW846: 6010C MMSD 01/13/18 DM0113/18000397 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/14/18 DM0114/18000418 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/15/18 DM0115/18000432 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/16/18 DM0116/18000461 220 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/17/18 DM0117/18000652 210 mg/kg D.W. 3 10 SW846: 6010C MMSD 01/18/18 DM0118/18000673 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/19/18 DM0119/18000689 160 mg/kg D.W. 3 9.9 D2, Q2. SW846: 6010C MMSD 01/20/18 DMO120/18000702 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 01/21/18 DMO121/18000800 180 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/22/18 DMO122/18000814 170 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 01/23/18 DMO123/18000843 160 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 01/24/18 DMO124118000875 180 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/25/18 DMO125/18000896 200 mg/kg D.W. 2.9 9.6 SW846: 6010C MMSD 01/26/18 DMO126/18000912 190 mg/kg D.W. 2.9 9.7 SW846: 6010C MMSD 01/27/18 DMO127/18000925 190 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/28/18 DMO128118000946 190 mg/kg D.W. 2.9 9.6 SW846: 6010C MMSD 01/29/18 DMO129118001200 190 mg/kg D.W. 2.9 9.7 SW846: 6010C MMSD 01/30/18 DMO130/18001229 190 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 01/31/18 DMO131/18001259 200 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/01/18 DM0201118001280 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 02/02/18 DM0202/18001421 210 mg/kg D.W. 3 9.7 SW846: 6010C MMSD 02/03/18 DM0203/18001434 200 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/04/18 DM0204118001455 200 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/05/16 DM0205/18001469 190 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/06/18 DM0206/18001506 170 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/07/18 DM0207/18001599 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 02/08/18 DM0208118001620 190 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/09/18 DM0209/18001738 190 mg/kg D.W. 2.9 9.7 SW846: 6010C MMSD 02/10/18 DM0210/18001751 200 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/11/18 DM0211/18001772 210 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 02/12/18 DM0212118001786 200 mg/kg D.W. 3 9.9 Q2. SW846: 6010C MMSD 02/13/18 DM0213/18001815 200 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 02/14/18 DM0214118001860 190 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/15/18 DM0215/18001881 200 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/16/18 DM0216/18001897 200 mg/kg D.W. 3 9.7 SW846: 6010C MMSD Page 19 of 706 SYSIrptlMiloMonthly 1/10/13 tj Printed.- 1/18119 09.47 • NNSD COPPER ICP METHOD 02/17/18 DM0217/18001944 02/18/18 DM0218/18001965 02/19/18 DM0219/18001979 170 mg/kg D.W. 3 9.8 190 mg/kg D.W. 3 9.9 190 mg/kg D.W. 3 10 Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 02/20/18 DM0220/18002047 190 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 02/21/18 DM0221/18002077 190 mg/kg D.W. 3 9.9 _ SW846: 6010C MMSD 02/22/18 DM0222/18002097 180 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/23/18 DM0223/1 B002415 190 mg/kg D.W. 2.9 9.6 SW846: 6010C MMSD 02/24/18 DM0224/18002427 170 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 02/25/18 DM0225/18002447 180 mg/kg D.W. 3 9.7 SW846: 6010C MMSD 02/26/18 DM0226/18002461 180 mg/kg D.W. 3 9.8 SW846: 6010C MMSD 02/27/18 DM0227/18002537 180 mg/kg D.W. 3 9.9 T ^ SW846: 6010C MMSD 02/28/18 DM0228/18002609 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 03/01/18 DM0301/18002628 190 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/02/18 u DM0302/18002711 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 03/03/18 DM0303/18002722 180 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/04/18 DM0304/18002741 180 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/05/18 DM0305/18002805 180 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/06/18 DMO306/18002862 180 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/07/18 DM0307/18002927 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 03/08/18 DM0308/18003015 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 03/09/18 DM0309/18003030 180 mg/kg D.W. 3 9.7 SW846: 6010C MMSD 03/10/18 DM0310/18003041 180 mg/kg D.W. 3 10 SW846: 6010C MMSD 03/11/18 DM0311/18003060 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 03/12/18 DM0312/18003335 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 03/13/18 DM0313/18003681 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 03/14/18 DM0314/18003710 03/15/18 DM0315/18003729 03/16/18 DM0316/18003744 03/17/18 DM0317/18003755 03/18/18 DM0318/18003780 03/19/18 DM0319118003911 03/20/18 DMO320118003938 03/21/18 DM0321/18003967 03/22/18 DM0322/18004111 03/23/18 DM0323/18004126 03/24/18 DM0324/18004137 03/25/18 DM0325/18004156 03/26/18 DM0326/18004320 03/27/18 DM0327/18004347 03/28/18 DM0328/18004376 03/29/18~ DM0329/18004395 03/30/18 DM0330118004410 03/31/18 DM0331/18004752 04/01/18 DM0401/18004771 04/02/18 DM0402118004784 04/03/18 DM0403/18004943 04/04/18 DM0404/18004972 SYS/rptimiloMonthly 1/10/13 tj 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D.W. 3 10 SW846: 6010C MMSD 190 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D.W. 3 10 SW846: 6010C MMSD 190 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 200 mg/kg D.W. 3 9.8 SW846-.6010C MMSD 200 mg/kg D.W. 2.9 9.7 SW846: 6010C MMSD 190 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D,W. 3.1 10 SW846: 6010C MMSD 200 mg/kg D.W. 3 10 SW846: 6010C MMSD 200 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 180 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 180 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 190 mg/kg D.W. 3 9.9 SW846: 6010C MMSD 180 mg/kg D.W. 3.1 10 180 mg/kg D.W. 3 10 190 mg/kg D.W. 8 24 180 mg/kg D.W. 7.8 24 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 20 o/ 106 Printed? 1/18/19 09.4; e-kNSD Annual Milorganite Report January 1 to December 31, 2018 w?" wR 1 G1 kwk nlwww DM0421/18006020 200 mg/kg D.W. 7.8 24 04/22/18 COPPER ICP METHOD 200 mg/kg D.W. 7.7 24 04/23/18 DM0423/18006157 200 mg/kg D.W. - Result.. 04/24/18 LOQ ,. Flags AnaWkal Method Lab 04/05/18 DM0405/18005037 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/06/18 DM0406/18005052 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/07/18 DM0407/18005063 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 04/08/18 DM0408/18005082 210 mg/kg D.W. 8 24 SW846: 6010C MMSD 04/09/18 DM0409/18005095 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/10/18 DM0410/18005164 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/11/18 DM0411/18005193 180 mg/kg D.W. 8 24 SW846: 6010C MMSD 04/12/18 DM0412/18005446 190 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/13/18 DM0413118005463 190 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/14/18 DM0414/18005474 200 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 04/15/18 DM0415118005605 190 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 04/16/18 DM0416/18005618 190 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 04/17/18 DM0417/18005709 190 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 04/18/18 DM0418/18005738 190 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 04/19/18 DM0419/18005757 200 mg/kg D.W. 7.7 23 Q3. SW846: 6010C MMSD 04/20/18 DM0420/18006009 190 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 04/21/18 DM0421/18006020 200 mg/kg D.W. 7.8 24 04/22/18 DM0422/18006039 200 mg/kg D.W. 7.7 24 04/23/18 DM0423/18006157 200 mg/kg D.W. 7.6 23 04/24/18 DM0424/18006185 190 mg/kg D.W. 7.8 24 04/25/18 DM0425/18006214 180 mg/kg D.W. 8.1 25 04/26/18 DM0426118006233 200 mg/kg D.W. 7.9 24 04/27/18 DM0427/18006441 200 mg/kg D.W. 7.6 23 04/28/18 DM0428/18006452 190 mg/kg D.W. 7.9 24 04/29/18 DM0429/18006471 190 mg/kg D.W. 7.8 24 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 04/30/18 DM0430/18006484 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/01/18 DMO501/18006571 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/02/18 DM0502/18006600 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/03/18 DM0503/18006854 210 mg/kg D.W. 7.4 23 SW846: 6010C MMSD 05/04/18 05/05/18 DMO504/18007005 DM0505/18007016 200 mg/kg D.W. 200 mg/kg D.W. 7.6 7.7 23 24 SW846: 6010C SW846: 6010C MMSD MMSD 05/06/18 DMO506118007035 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/07/18 05/08/18 DMO507/18007257 DMO508/18007284 220 mg/kg D.W. 200 mg/kg D.W. 7.6 7.8 23 Q3. 24 SW846: 6010C SW846: 6010C MMSD MMSD 05/09/18 DMO509/18007313 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/10/18 05/11/18 05/12/18 - DM0510/18007340 DM0511/18007418 DM0512118007429 200 mg/kg D.W. 210 mg/kg D.W. 200 mg/kg D.W. 7.9 8 7.8 24 24 24 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 05/13/18 DMO513/18007476 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/14/18 DM0514/18007591 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/15/18 DM0515/18007976 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 05/16/18 DM0516/18008005 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/17/18 DM0517/18008103 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/18/18 DM0518/18008118 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/19/18 DMO519/18008129 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/20/18 DMO520/18008196 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/21/18 DMO521/18008209 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD SYS/rptimmoMonthly 1/10/13 tj Page 21 of 106 Primed; 1/18/19 09:4; • MMSD ionm F& 1 Man S Annual Milorganite Report January 1 to December 31, 2018 COPPER ICP METHOD OD LOQ 05/22/18 DMO522/18008236 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/23/18 DMO523/18008304 210 mg/kg D.W. 7.8 24 Q3. SW846: 6010C MMSD 05/24/18 DM0524/18008658 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 05/25/18 DMO525118008673 210 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 05/26/18 DM0526/18008684 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 05/27/18 DMO527118008703 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 05/28/18 DMO528/18008716 230 mg/kg D.W. 8 24 SW846: 6010C MMSD 05/29/18 DMO529/18008888 220 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 05/30/18 DMO530/18008917 210 mg/kg D.W. 7.7 24 B8. SW846: 6010C MMSD 05/31/18 DMO531118008936 230 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/01/18 DM0601/18009150 240 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/02/18 DM0602/18009161 220 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/03/18 DM0603/18009335 220 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/04/18 DMO604/18009348 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/05/18 DM0605/18009375 220 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/06/18 DMO606/18009404 240 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 06/07/18 DM0607118009423 230 mg/kg D.W. 7.8 24 Q3. SW846: 6010C MMSD 06/08/18 DM0608/18009822 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/09/18 DM0609/18009833 200 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 06/10/18 DM0610/18009852 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/11/18 DM0611/18009865 230 mg/kg D.W. 7.8 24 Q3. SW846: 6010C MMSD 06/12/18 DM0612/18010098 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 06/13/18 DM0613/18010127 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 06/14/18 DM0614/18010437 220 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/15/18 DM0615/18010452 220 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 06/16/18 DM0616/18010463 190 mg/kg D.W. 7.6 23 B8. SW846: 6010C MMSD 06/17/18 DM0617118010482 190 mg/kg D.W. •7.6 23 38. SW846: 6010C MMSD 06/18/18 DM0618/18010639 190 mg/kg D.W. 7.8 24 B8. SW846: 6010C MMSD 06/19/18 DMO619/18010666 T 210 mg/kg D.W. 7.8 24 88. SW846: 6010C MMSD 06/20/18 DM0620118010694 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/21/18 DM0621/18010713 200 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 06/22/18 DM0622/18010939 210 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 06/23/18 DM0623/18010950 210 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 06/24/18 DM0624/18011087 210 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 06/25/18 DMO625/18011182 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 06/26/18 DM0626/18011209 200 mg/kg D.W. 7.7 24 SWB46: 6010C MMSD 06/27/18 DM0627/18011597 200 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 06/28/18 DM0628/18011616 180 mg/kg D.W. 7.7 24 Q3. SW846: 6010C MMSD 06/29/18 DM0629/18011631 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 06/30/18 DM0630/18011642 190 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 07/01/18 DM0701/18011728 200 mg/kg D.W. 7.7 24 SW846: 6010C T MMSD 07/02/18 DM0702/18011741 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 07/03/18 DM0703/18011881 200 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 07/04/18 _ DM0704/18011909 210 mg/kg D.W. 7.6 23 Y SW846: 6010C MMSD 07/05/18 DM0705/18012390 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/06/18 DM0706/18012405 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 07/07/18 DM0707/lBO12416 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD Page 11 of 106 SYS/rptlMiloMonfhly 1/10/13 tj Printed: 1/18119 09.4; 07/11/18 DM0711/18012820 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/12/18 DM0712/18012861 190 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/13/18 DM0713/18012876 07/14/18 DM0714/18013220 07/15/18 DM0715/18013239 190 mg/kg D.W. 7.6 23 230 mg/kg D.W. 7.6 23 220 mg/kg D.W. 7.7 24 07/16/16 Annual Milorganite Report 220 mg/kg D.W. January 1 to December 31, 2018 IrMF rte s ryrixY tvrnr r SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C COPPER ICP METHOD DM0717/18013751 �. �.ID 07/08/18 DM0708/18012435 Re5ult LOD LQQ QA FLIV AnaNtkal Method lab 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/09/18 DM0709/18012448 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 07/10/18 DM0710/18012474 190 mg/kg D.W. 7.8 24 _ SW846: 6010C MMSD 07/11/18 DM0711/18012820 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/12/18 DM0712/18012861 190 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 07/13/18 DM0713/18012876 07/14/18 DM0714/18013220 07/15/18 DM0715/18013239 190 mg/kg D.W. 7.6 23 230 mg/kg D.W. 7.6 23 220 mg/kg D.W. 7.7 24 07/16/16 DM0716/18013252 220 mg/kg D.W. 7.6 23 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C 07/17/18 DM0717/18013751 230 mg/kg D.W. 7.6 23 23 23 07/18/18 DM0718/18013961 220 mg/kg D.W. 7.6 23 7.5 7.5 7.5 07/19/18 DM0719/18014047 220 mg/kg D.W. 7.5 23 220 mg/kg D.W. 07/20/18 DM0720/18014062 220 mg/kg D.W. 7.7 23 Q2. 07/21/18 DM0721/18014073 220 mg/kg D.W. 7.6 23 08/14/18 08/15/18 07/22/18 DM0722118014483 230 mg/kg D.W. 7.7 23 MMSD MMSD 07/23/18 DM0723/18014496 220 mg/kg D.W. 7.7 24 SW846: 6010C 07/24/18 DM0724/18014523 230 mg/kg D.W. 7.7 24 87. 07/25/18 DM0725/18014551 230 mg/kg D.W. 7.8 24 7.5 07/26/18 DM0726118014570 230 mg/kg D.W. 7.7 24 220 mg/kg D.W. 07/27/18 DM0727/18014585 210 mg/kg D.W. 7.6 23 Q3. 07/28/18 DM0728/18014676 180 mg/kg D.W. 7.5 23 08/21/18 07/29/18 DM0729/18014910 200 mg/kg D.W. 7.5 23 MMSD 07/30/18 DM0730/18014925 190 mg/kg D.W. 7.7 24 SW846: 6010C 07/31/18 DM0731/18014954 220 mg/kg D.W. 7.6 23 23 08/01/18 DMO801/18014969 210 mg/kg D.W. 7.6 23 B8. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 08/02/18 08/03/18 08/04/18 08/05/18 DM0802/18015140 DMO803/18015155 DMOB04/18015252 DMO805/18015279 210 mg/kg D.W. 200 mg/kg D.W. 200 mg/kg D.W. 200 mg/kg D.W. 7.6 7.6 7.5 7.6 23 23 23 23 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 08/06/18 08/07/18 DMO806118015385 DMO807/18015414 210 mg/kg D.W. 220 mg/kg D.W. 7.5 7.6 23 23 a SW846: 6010C SW846: 6010C MMSD MMSD 08/06/18 08/09/18 08/10/18 DMOB08/18015473 DM0809/18015500 DMO810/18015899 220 mg/kg D.W. 230 mg/kg D.W. 220 mg/kg D.W. 7.5 7.5 7.5 23 23 23 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 08/11/18 DM0811/18015910 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 08/12/18 08/13/18 DM0812/18016203 DM0813/18016216 220 mg/kg D.W. 220 mg/kg D.W. 7.5 7.5 23 23 SW846: 6010C SW846: 6010C MMSD MMSD 08/14/18 08/15/18 DM0814/18016254 DM0815/18016281 190 mg/kg D.W. 220 mg/kg D.W. 7.6 7.6 23 23 SW846: 6010C SW846: 6010C MMSD MMSD 08/16/18 DMO816/18016300 190 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/17/18 DM0817/18016365 210 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/18/18 DMO818/18016505 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/19/18 DMOB19/18016525 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/20/18 DMO820/18016539 230 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/21/18 DMOB21/18016714 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 08/22/18 DMOB22/18016742 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/23/18 DM0823/18017352 220 mg/kg D.W. 7.4 23 SW846: 6010C MMSD SYS/rptlMMOMonthly 1/10113 tj Page 13 of 106 Printed: 1118119 09.•47 NSD RUCU"I COPPER ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 08/24/16 08/25/18 08/26/18 08/27/18 08/28/18 DMO824/18017367 DMO825/18017378 DM0826/18017397 DM0827/18017410 DM0828/18017434 210 mg/kg D.W. 220 mg/kg D.W. 210 mg/kg D.W. 230 mg/kg D.W. 220 mg/kg D.W. 7.5 7.6 7.5 7.5 7.6 23 23 23 23 23 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD 08/29/18 OM0829/18017462 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 08/30/16 DMO830/18017483 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 08/31/18 DMO831/18017498 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/01/18 DMO901/18017520 230 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/02/16 DM0902/18017752 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/03/18 DMO903/18018124 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/04/18 DM0904/18018149 230 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 09/05/18 DMO905/18018305 220 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 09/06/16 DMO906118018326 220 mg/kg D.W. 7.6 23 ^ SW846: 6010C MMSD 09/07/18 DMO907118018342 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/08/16 DM0908/18018353 230 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/09/16 DMO909/18018724 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/10/16 DMO910/18018799 220 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/11/18 DMO911/18018825 210 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 09/12/18 DMO912118018854 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/13/18 DM0913/18018875 210 mg/kg D.W. 7.7 24 Q3. SW846: 6010C MMSD 09/14/18 DMO914/18018891 210 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 09/15/18 DM0915/18019159 220 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 09/16/18 DM0916/18019178 210 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 09/17/18 DMO917/18019191 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/18/18 DMO918118019447 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 09/21/18 DMO921/18019515 210 mg/kg D.W. 7.4 23 SW846: 6010C MMSD 09/22/18 DMO922/18019574 210 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/23/18 DMO923/18019665 200 mg/kg D.W. 7.3 22 SW846: 6010C MMSD 09/24/18 DMO924/18020088 210 mg/kg D.W. 7.4 23 SW846: 6010C MMSD 09/25/18 DMO925/18020314 200 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 09/26/18 DMO926/18020343 190 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 09/27/18 DMO927/18020364 09/28/18 DM0928/18020380 09/29/18 DMO929/18020391 190 mg/kg D.W. 180 mg/kg D.W. 7.6 7.9 23 24 SW846: 6010C SW846: 6010C MMSD MMSD 190 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 09/30/18 10/01/18 DM0930/18020411 Y DM1001118021136 190 mg/kg D.W. 190 mg/kg D.W. 7.6 23 7.6 23 10/02/18 DM1002118021162 200 mg/kg D.W. 7.6 23 10/03/18 DM 1003/18021190 190 mg/kg D.W. 7.6 23 10/04/18 DM1004/18021541 210 mg/kg D.W. 7.5 23 10/05/18 DM1005/18021557 200 mg/kg D.W. 7.6 23 10/06/18 DM1006/18021568 200 mg/kg D.W. 7.8 24 10/07/18 DM1007/18021588 200 mg/kg D.W. 7.4 23 10/08/18 DM1008118021602 200 mg/kg D.W. 7.4 23 10/09/18 DM1009/18021627 10/10/18 DM1010118021656 10/11/16 DM1011118021975 SYSIrptiMiloMonth/y 1/10/13 tj 200 mg/kg D.W. 7.5 23 210 mg/kg D.W. 7.7 23 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD Q3. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 24 of 106 Printed.' 1/18/19 09:41 10/16/18 DM1016/18022065 10/17/18 DM1017/18022094 10/18/16 DM1018118022133 10/19/18 DM1019/18022269 10/20/18 DM1020/18022280 200 mg/kg D.W. 7.6 23 210 mg/kg D.W. Annual Milorganite Report NNSD 200 mg/kg D.W. 7.5 23 January 1 to December 31, 2018 ftNt r. Mf ! WOR 8 23 190 mg/kg D.W. 7.5 23 B8. COPPER ICP METHOD DM1025118022708 200 mg/kg D.W. 7.6 23 fi= DM1026/18022767 ' LOQ QA Flags Anatyfiml Method L26 10/27/18 DM1027/18022778 210 mg/kg D.W. 7.5 10/12/18 DM1012/18021991 200 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 10/13/18 DM1013/18022006 200 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 10/14/18 DM1014/18022026 190 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 10/15/18 DM1015/18022040 200 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 10/16/18 DM1016/18022065 10/17/18 DM1017/18022094 10/18/16 DM1018118022133 10/19/18 DM1019/18022269 10/20/18 DM1020/18022280 200 mg/kg D.W. 7.6 23 210 mg/kg D.W. 7.6 23 200 mg/kg D.W. 7.5 23 210 mg/kg D.W. 7.7 23 190 mg/kg D.W. 7.5 23 B8. 10/21/16 DM1021/18022435 190 mg/kg D.W. 7.6 23 B8. 10/22/18 DM1022/18022449 200 mg/kg D.W. 7.5 23 68. 10/23/18 10/24/18 DM1023/18022614 DM1024/18022643 200 mg/kg D.W. 210 mg/kg D.W. 7.6 7.6 23 23 10/25/18 DM1025118022708 200 mg/kg D.W. 7.6 23 10/26/18 DM1026/18022767 210 mg/kg D.W. 7.6 23 10/27/18 DM1027/18022778 210 mg/kg D.W. 7.5 23 11/07/18 DM1107/18023991 T 240 mg/kg D.W. 7.4 23 11/08/18 DM1108/18024012 240 mg/kg D.W. 7.5 23 11/09/18 11/10/18 DM1109/18024028 DM 1110/18024523 240 mg/kg D.W. 210 mg/kg D.W. 7.5 7.4 23 23 11/11/18 DM1111118024619 220 mg/kg D.W. 7.5 23 11/12/18 DM1112/18024633 200 mg/kg D.W. 7.6 23 11/13/18 DM 1113/18025014 210 mg/kg D.W. 7.6 23 11/14/18 11/15/18 DM1114/18025043 DM1115118025064 220 mg/kg D.W. 220 mg/kg D.W. 7.7 7.7 24 23 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 11/16/18 DM1116118025080 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 11/17/18 DM 1117/18025093 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 11/18/18 DM1118/18025113 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 11/19/18 DM1119/18025127 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 11/20/18 DM1120/18025356 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 11/21/18 DM1121/18025385 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 11/22/18 DM1122118025406 210 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 11/23/18 DM1123118025422 210 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 11/24/18 DM 1124/18025750 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 11/25/18 DMI 125/18025769 210 mg/kg D.W. 7.9 24 SW846: 6010C MMSD 11/26/18 DM 1126/18025828 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 11/27/18 DMI 127/18025860 220 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 11/28/18 DM1128118025888 210 mg/kg D.W. 7.5 23 SW846: 6010C MMSD 11/29/18 DM1129/18025956 210 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 11/30/18 DM1130/18025971 200 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 12/01/18 DM1201/18026182 200 mg/kg D.W. 7.7 24 SW846: 6010C MMSD 12/02/18 DM1202/18026201 200 mg/kg D.W. 7.7 23 SW846: 6010C MMSD 12/03/18 DM1203/18026214 200 mg/kg D.W. 7.6 23 SW846: 6010C MMSD 12/04/18 DM1204/18026391 200 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 12/05/18 DM1205/18026578 210 mg/kg D.W. 7.8 24 SW846: 6010C MMSD 12/06/18 DM1206/18026621 200 mg/kg D.W. 8 24 SW646: 6010C MMSD 12/07/18 DM1207/18026797 200 mg/kg D.W. 7.9 24 SW846: 6010C MMSD PageHoflN SYS/rptlMiloMonthly 1/10/13 tj Printed: 1/18/19 09:47 MMSD IM A CLUM I+t Illi COPPER ICP METHOD 12/08/18 DM1208/18026808 210 mg/kg D.W. 7.8 24 12/09/18 DM1209/18026827 200 mg/kg D.W. 7.7 24 12/10/18 DM1210/18026840 200 mg/kg D.W. 8 24 12/11/18 DM1211/18027102 200 mg/kg D.W. 7.6 23 12/12/18 DM1212118027130 200 mg/kg D.W. 7.6 23 B8. 12/13/18 DM1213/18027253 200 mg/kg D.W. 7.7 24 12/14/18 DM1214/18027306 210 mg/kg D.W. 7.6 23 12/15/18 DM1215/18027317 200 mg/kg D.W. 7.6 23 12/16/18 DM1216/18027525 190 mg/kg D.W. 7.8 24 12/17/18 DM1217118027540 200 mg/kg D.W. 7.9 24 12/18/18 DM1218/18027643 200 mg/kg D.W. 8 25 12/19/18 DM1219/18027676 210 mg/kg D.W. 7.7 24 12/20/18 DM1220/18027805 220 mg/kg D.W. 7.6 23 12/21/18 DM1221/18027821 220 mg/kg D.W. 7.7 24 12/22/18 DM1222/18027832 200 mg/kg D.W.7.8 24 12/23/18 DM1223/18027852 210 mg/kg D.W. 7.8 24 12/24/18 DM1224118027883 200 mg/kg D.W. 7.8 24 12/25/18 DM1225/18027952 190 mg/kg D.W. 7.9 24 12/26/18 DM1226/18027969 200 mg/kg D.W. 7.9 24 12/27/18 DM1227/18027990 220 mg/kg D.W. 7.9 24 12/28/18 DM1228/18028005 210 mg/kg D.W. 8 24 12/29/18 DM1229/18028070 200 mg/kg D.W. 7.7 24 12/30/18 DM1230/18028089 220 mg/kg D.W. 7.6 23 12/31/18 DM1231118028102 210 mg/kg D.W. 7.7 24 Avg Result: 200 mg/kg D.W. Min LOD: 2.9 mg/kg D.W. SYS/rptlMiloMonth/y 1/10/13 tj Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C Max Result: 240 mg/kg D.W. MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD Page 26 of 106 Printed: 1/18/19 09:4; 03/06/18 MF/18004517 < 0.2 MPN/g TS Annual Milorganite Report e-NNSD EPA 1680 MMSD January 1 to December 31, 2018 1rrovi PW I Cl[ r k 38 MPN/g TS 0.2 FECAL COLIFORM SLUDGE MMSD 03/20/18 MF/18005637 Sample ID 01/09/18 MF/18000778 Result < 0.2 MPN/g TS .. LOQ QA Flags 0.2 Anatftkal Method Lab EPA 1680 MMSD 01/16/18 MF/18001401 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 01/23/18 MF/18001831 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 02/06/18 MF/18002784 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 02/13/18 MF/18003114 < 1.9 MPN/g TS 1.9 EPA 1680 MMSD 02/20/18 MF/18003654 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 02/27/18 MF/18004083 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 03/06/18 MF/18004517 < 0.2 MPN/g TS 0.2 A0. EPA 1680 MMSD 03/13/18 MF/18005131 38 MPN/g TS 0.2 EPA 1680 MMSD 03/20/18 MF/18005637 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 03/27/18 MF/18006135 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 04/10/18 MF/18007088 270 MPN/g TS 2 EPA 1680 MMSD 04/17/18 MF/18007858 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 04/24/18 MF/18008290 0.45 MPN/g TS 0.2 EPA 1680 MMSD 05/01/18 MF/18008744 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 05/08/18 MF/18009261 < 2 MPN/g TS 2 EPA 1680 MMSD 05/15/18 MF/18010064 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 05/22/18 MF/18010621 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 05/29/18 MF/18011151 < 2 MPN/g TS 2 EPA 1680 MMSD 06/05/18 MF/18011790 < 2 MPN/g TS 2 EPA 1680 MMSD 06/12/18 MF/18012253 16 MPN/g TS 2 EPA 1680 MMSD 06/19/18 MF/18013039 0.42 MPN/g TS 0.19 EPA 1680 MMSD 06/26/18 MF/18013969 1.4 MPN/g TS 0.2 EPA 1680 MMSD 07/03/18 MF/18014837 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 07/10/18 MF/18015325 2.6 MPN/g TS 0.19 EPA 1680 MMSD 07/17/18 MF/18016119 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 07/24/18 MF/18016685 < 0.19 MPN/g TS 0.19 D2, Q3. EPA 1680 MMSD 07/31/18 MF/18017239 < 0.19 MPN/g TS 0.19 CQ. EPA 1680 MMSD 08/07/18 MF/18017956 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 08/14/18 MF/18018703 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 08/21/18 MF/18019360 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 08/28/18 MF/18019981 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 09/04/18 MF/18020506 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 09/11/18 MF/18021257 < 0.19 MPN/g TS 0.19 Q2. EPA 1680 MMSD 09/25/18 MF/18022492 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 10/02/18 MF/18023190 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD 10/09/18 MF/18023854 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 10/16/18 MF/18024568 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 10/23/18 MF/18025179 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 11/13/18 MF/18026478 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 11/19/18 MF/18026717 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 11/27/18 MF/18027155 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 12/04/18 MF/18027455 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 12/11/18 MF/18027929 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 12/18/18 MF/18028261 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 12/26/18 MF/18028429 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD Page 27 of 106 SY5/rpt1miloMonthly 1/10/17 tj Printed: 1/18/19 09: 4i Annual Milorganite Report N145k; January 1 to December 31, 2018 nprrfrt FN I [hiss" Rfew, FECAL COLIFORM SLUDGE Min LOD: 0.19 MPN/g TS Page 28 of 106 SYSIrptI iloMonthly 1/10113 tj Printed: 1118/19 09:9; ,r DMO106/18000168 29000 mg/kg D.W. 100 Annual Milorganite Report SW846: 6010C MMSD 01/07/18 DMO107/18000189 28000 mg/kg D.W. January 1 to December 31, 2018 mess 8X 1 tv" R #II�@1ifER' SW846: 5010C MMSD 01/08/18 DM0108/18000203 IRON ICP METHOD 99 300 SW846: 6010C MMSD 01/01/18 DMO101/18000013 30000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/02/18 DMO102118000047 30000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/03/18 DM0103/18000061 31000 mg/kg D.W. 100 310 SW846: 6010C MMSD 01/04/18 DMO104/18000098 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/05/18 DMO105118000155 28000 mg/kg D.W. 100 310 SW846: 6010C MMSD 01/06/18 DMO106/18000168 29000 mg/kg D.W. 100 300 SW846: 6010C MMSD 01/07/18 DMO107/18000189 28000 mg/kg D.W. 100 300 SW846: 5010C MMSD 01/08/18 DM0108/18000203 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/09/18 DMO109/18000232 27000 mg/kg D.W. 100 300 SW846: 6010C MMSD 01/10/18 DM0110/18000326 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/11/18 DMO111/18000347 29000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/12/18 DMO 112/18000363 29000 mg/kg D.W. 100 300 SW846: 6010C MMSD 01/13/18 DM0113/18000397 30000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/14/18 DM0114/18000418 29000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/15/18 DM0115/18000432 26000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/16/18 DM0116/18000461 31000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/17/18 DM0117/18000652 31000 mg/kg D.W. 100 300 SW846: 6010C MMSD 01/18/18 DM0118/18000673 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/19/18 DM0119/18000689 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/20/18 DMO120/18000702 27000 mg/kg D.W. 99 300 SW846: 6010C MMSD 01/21/18 DMO121/18000800 27000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/22/18 DMO122/18000814 25000 mg/kg D.W. 100 310 SW846: 6010C MMSD 01/23/18 DMO123/18000843 25000 mg/kg D.W. 100 310 SW846: 6010C MMSD 01/24/18 DMO124/18000875 26000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/25/18 DMO125/18000896 30000 mg/kg D.W. 96 290 SW846: 6010C MMSD 01/26/18 DMO126/18000912 27000 mg/kg D.W. 97 290 SW846: 6010C MMSD 01/27/18 DMO127/18000925 30000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/28/18 DMO128/18000946 32000 mg/kg D.W. 96 290 SW846: 6010C MMSD 01/29/18 DMO129/18001200 30000 mg/kg D.W. 97 290 SW846: 6010C MMSD 01/30/18 DMO130/18001229 28000 mg/kg D.W. 98 300 SW846: 6010C MMSD 01/31/18 DMO131/18001259 30000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/01/18 DM0201/18001280 26000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/02/18 DM0202/18001421 26000 mg/kg D.W. 97 300 SW846: 6010C MMSD 02/03/18 DM0203/18001434 27000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/04/18 DM0204118001455 27000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/05/18 DM0205/18001469 26000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/06/18 DM0206118001506 23000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/07/18 DM0207/18001599 24000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/08/18 DM0208/18001620 31000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/09/18 DM0209/18001738 32000 mg/kg D.W. 97 290 SW846: 6010C MMSD 02/10/18 DM0210/18001751 27000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/11/18 DM0211/18001772 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/12/18 DM0212118001786 29000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/13/18 DM0213/18001815 31000 mg/kg D.W. 100 310 SW846: 6010C MMSD 02/14/18 DM0214/18001860 31000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/15/18 DM0215/18001881 32000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/16/18 DM0216/18001897 31000 mg/kg D.W. 97 300 SW846: 6010C MMSD Page 29 of 106 SYS/rptimiloMonthly 1/10/13 tj Printed: 1/18/19 09:41 ki 03/02/18 03/03/18 03/04/18 03/05/18 03/06/18 03/07/18 03/08/18 03/09/18 03/10/18 03/11/18 03/12/18 03/13/18 03/14/18 03/15/18 03/16/18 03/17/18 DM0302/18002711 DM0303/18002722 DM0304/18002741 28000 mg/kg D.W. 27000 mg/kg D.W. 27000 mg/kg D.W. DM0305/18002805 28000 mg/kg D.W. DM0306/18002862 Annual Milorganite Report MMSDJanuary DM0307/18002927 29000 mg/kg D.W. DM0308/18003015 1 to December 31, 2018 PlNIMFOtielURI DM0309118003030 28000 mg/kg D.W. DM0310/18003041 26000 IRON ��METHOD IC�ICP DM0311/18003060 26000 mg/kg D.W. DM0312/18003335 26000 mg/kg D.W. 02/17/18 DM0217/18001944 34000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/18/18 OM0218/18001965 36000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/19/18 DM0219/18001979 36000 mg/kg D.W. 100 300 SW846: 6010C MMSD 02/20/18 DM0220/18002047 30000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/21/18 DM0221/18002077 29000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/22/18 DM0222/18002097 27000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/23/18 DM0223118002415 27000 mg/kg D.W. 96 290 SW846: 6010C MMSD 02/24/18 DM0224/18002427 26000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/25/18 DM0225/18002447 27000 mg/kg D.W. 97 300 SW846: 6010C MMSD 02/26/18 DM0226/18002461 28000 mg/kg D.W. 98 300 SW846: 6010C MMSD 02/27/18 DM0227118002537 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 02/28/18 DM0228/18002609 28000 mg/kg D.W. 99 300 SW846: 6010C MMSD 03/01/18 DM0301/18002628 28000 mg/kg D.W. 100 300 SW846: 6010C MMSD 03/02/18 03/03/18 03/04/18 03/05/18 03/06/18 03/07/18 03/08/18 03/09/18 03/10/18 03/11/18 03/12/18 03/13/18 03/14/18 03/15/18 03/16/18 03/17/18 DM0302/18002711 DM0303/18002722 DM0304/18002741 28000 mg/kg D.W. 27000 mg/kg D.W. 27000 mg/kg D.W. DM0305/18002805 28000 mg/kg D.W. DM0306/18002862 28000 mg/kg D.W. DM0307/18002927 29000 mg/kg D.W. DM0308/18003015 29000 mg/kg D.W. DM0309118003030 28000 mg/kg D.W. DM0310/18003041 26000 mg/kg D.W. DM0311/18003060 26000 mg/kg D.W. DM0312/18003335 26000 mg/kg D.W. OM0313/18003681 25000 mg/kg D.W. DM0314/18003710 26000 mg/kg D.W. DM0315/18003729 28000 mg/kg D.W. 03/18/18 DM0318/18003780 03/19/18 OM0319/18003911 03/20/18 DM0320/18003938 03/21/18 DM0321118003967 03/22/18 DM0322/18004111 03/23/18 DM0323/18004126 27000 mg/kg D.W. 28000 mg/kg D.W. 29000 mg/kg D.W. 31000 mg/kg D.W. 32000 mg/kg D.W. 31000 mg/kg D.W. 32000 mg/kg D.W. 33000 mg/kg D.W. 99 300 100 300 100 300 100 300 100 300 100 310 99 300 97 300 100 300 100 310 100 310 100 310 100 310 _ 99 300 100 310 100 310 100 300 100 310 100 300 100 310 T 98 300 97 290 03/24/18 DM0324/18004137 29000 mg/kg D.W. 100 310 03/25/18 DM0325/18004156 30000 mg/kg D.W. 100 310 03/26/18 DM0326/18004320 32000 mg/kg D.W. 100 300 03/27/18 DM0327/18004347 35000 mg/kg D.W. 100 310 03/28/18 DM0328/18004376 34000 mg/kg D.W. 100 310 03/29/18 DM0329/18004395 31000 mg/kg D.W. 99 300 03/30/18 DM0330/18004410 ` 29000 mg/kg D.W. 100 310 03/31/18 DM0331118004752 30000 mg/kg D.W. 99 300 04/01/18 DM0401118004771 30000 mg/kg D.W. 100 310 04/02/18 DM0402/18004784 31000 mg/kg D.W. 100 300 04/03/18 DM0403/18004943 34000 mg/kg D.W. 270 780 04/04/18 DM0404/18004972 32000 mg/kg D.W. 260 760 SYS/rptlMiloMonthly 1/10/13 t1' SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MKACn MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD Page 30 of 106 Printed; 1/18/19 09:4; r _ Annual Milorganite Report MMSD January 1 to December 31, 2018 fm 0 mw f IRON ICP METHOD Sampte ID Result .. LOQ .• Fhigs AnalytiCit Method Lob 04/05/18 DM0405/18005037 39000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/06/18 DM0406/18005052 39000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/07/18 DM0407118005063 31000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/08/18 DM0408/18005082 30000 mg/kg D.W. 270 780 SW846: 6010C MMSD 04/09/18 DM0409/18005095 32000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/10/18 DM0410/18005164 36000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/11/18 DM0411/18005193 34000 mg/kg D.W. 260 780 SW846: 6010C MMSD 04/12/18 DM0412/18005446 33000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/13/18 DM0413/18005463 32000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/14/18 DM0414/18005474 36000 mg/kg D.W. 260 750 SW846: 6010C MMSD 04/15/18 DM0415/18005605 34000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/16/18 DM0416/18005618 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 04/17/18 DM0417/18005709 33000 mg/kg D.W. 260 750 SW846: 6010C MMSD 04/18/18 DM0418118005738 33000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/19/18 DM0419/18005757 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 04/20/18 DM0420/18006009 29000 mg/kg D.W. 250 740 SW846: 6010C MMSD 04/21/18 DM0421/18006020 38000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/22/18 DM0422/18006039 38000 mg/kg D.W. 260 750 SW846: 6010C MMSD 04/23/18 DM0423/18006157 J 36000 mg/kg D.W. 250 740 SW846: 6010C MMSD 04/24/18 DM0424/18006185 33000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/25/18 DM0425/18006214 28000 mg/kg D.W. 270 790 SW846: 6010C MMSD 04/26/18 DM0426/18006233 29000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/27/18 DM0427/18006441 30000 mg/kg D.W. 250 740 SWB46: 6010C MMSD 04/28/18 DM0428/18006452 28000 mg/kg D.W. 260 770 SW846: 6010C MMSD 04/29/18 DM0429/18006471 28000 mg/kg D.W. 260 760 SW846: 6010C MMSD 04/30/18 DM0430/18006484 31000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/01/18 DMO501/18006571 32000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/02/18 DM0502/18006600 31000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/03/18 DM0503/18006854 32000 mg/kg D.W. 250 720 SW846: 6010C MMSD 05/04/18 DM0504/18007005 33000 mg/kg D.W. 250 740 SW846: 6010C MMSD 05/05/18 DM0505/18007016 30000 mg/kg D.W. 260 750 SW846: 6010C MMSD 05/06/18 DM0506/18007035 33000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/07/18 DM0507/18007257 34000 mg/kg D.W. 250 740 SW846: 6010C MMSD 05/08/18 DM0508/18007284 34000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/09/18 DMO509/18007313 32000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/10/18 DMO510/18007340 33000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/11/18 DM0511/18007418 33000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/12/18 DM0512/18007429 33000 mg/kg D.W. 260 750 SW846: 6010C MMSD 05/13/18 DM0513/18007476 32000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/14/18 DM0514/18007591 32000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/15/18 DM0515/18007976 33000 mg/kg D.W. 250 740 SW846: 6010C MMSD 05/16/18 DM0516/18008005 29000 mg/kg D.W. 260 750 SW846: 6010C MMSD 05/17/18 DMO517/18008103 31000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/18/18 DMO518/18008118 31000 mg/kg D.W. 260 770 SW846: 6010C MMSD 05/19/18 DM0519/18008129 30000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/20/18 DM0520/18008196 32000 mg/kg D.W. 260 760 SW846: 6010C MMSD 05/21/18 DM0521/18008209 32000 mg/kg D.W. 260 760 SW846: 6010C MMSD Page 31 of 106 SYS/rptl MiloMonthly 1/10/13 tj Punted: 1/18/19 09:4) IL L f �-J NNSD w,"i a A Clio IRON ICP METHOD mg/kg D.W. 260 05/22/18 DM0522/18008236 33000 mg/kg D.W. 260 770 05/23/18 DM0523/18008304 34000 mg/kg D.W. 260 760 05/24/18 DM0524/18008658 32000 mg/kg D.W. 250 730 05/25/18 DMO525118008673 33000 mg/kg D.W. 260 750 05/26/18 DM0526118008684 34000 mg/kg D.W. 250 740 05/27/16 DMO527/18008703 33000 mg/kg D.W. 260 760 05/28/18 DMO528/18008716 33000 mg/kg D.W. 260 770 05/29/18 05/30/18 05/31/18 06/01/18 06/02/18 06/03/18 06/04/18 06/05/18 06/06/18 06/07/18 06/08/18 06/09/18 06/10/18 06/11/18 06/12/18 06/13/18 06/14/18 06/15/18 DMO529118008888 DMO530118008917 DMO531/18008936 DM0601/18009150 DM0602/18009161 DM0603/18009335 DM0604/18009348 DM0605/18009375 DM0606/18009404 DM0607118009423 DM0608118009822 DM0609/18009833 DM0610/18009852 DM0611118009865 DM0612/18010098 DM0613/18010127 DM0614/18010437 DM0615/18010452 32000 mg/kg D.W. 260 770 34000 mg/kg D.W. 260 750 32000 mg/kg D.W. 260 760 32000 mg/kg D.W. 250 740 30000 mg/kg D.W. 260 750 29000 mg/kg D.W. 260 760 29000 mg/kg D.W. 250 740 31000 mg/kg D.W. 260 760 31000 mg/kg D.W. 260 770 29000 mg/kg D.W. 260 760 31000 mg/kg D.W. 250 740 32000 mg/kg D.W. 260 750 33000 mg/kg D.W. 250 740 37000 mg/kg D.W. 260 760 35000 mg/kg D.W. 260 770 37000 mg/kg D.W. 260 770 36000 mg/kg D.W. 260 760 37000 mg/kg D.W. 260 740 Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 06/16/18 DM0616/18010463 36D00 mg/kg D.W. 260 740 SW846: 6010C MMSD 06/17/18 DM0617118010482 36000 mg/kg D.W. 250 740 SW846: 6010C MMSD 06/18/18 DM0618/18010639 36000 mg/kg D.W. 260 750 SW846: 6010C MMSD 06/19/18 DM0619/18010666 36000 mg/kg D.W. 260 760 SW846: 6010C MMSD 06/20/18 DM0620/18010694 38000 mg/kg D.W. 250 740 SW846: 6010C MMSD 06/21/18 DM0621/18010713 35000 mg/kg D.W. 250 730 SW846: 6010C MMSD 06/22/18 DM0622/18010939 37000 mg/kg D.W. 250 730 SW846: 6010C MMSD 06/23/18 DM0623/18010950 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD 06/24/18 DM0624/18011087 34000 mg/kg D.W. 260 750 SW846: 6010C MMSD 06/25/18 DM0625/18011182 34000 mg/kg D.W. 260 740 SW846: 6010C MMSD 06/26/18 DM0626/18011209 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 06/27/18 DMO627/18011597 32000 mg/kg D.W. 260 740 SW846: 6010C J MMSD 06/28/18 DM0628/18011616 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 06/29/18 DM0629/18011631 34000 mg/kg D.W. 260 760 SW846: 6010C MMSD 06/30/18 DM0630/18011642 33000 mg/kg D.W. 260 760 SW846: 6010C MMSD 07/01/18 DM0701/18011728 35000 mg/kg D.W. 260 750 SW846: 6010C MMSD 07/02/18 DM0702/18011741 35000 mg/kg D.W. 260 760 SW846: 6010C MMSD 07/03/18 DM0703/18011881 36000 mg/kg D.W. 260 750 SW846: 6010C MMSD 07/04/18 DM0704/18011909 36000 mg/kg D.W. 250 740 SW846: 6010C MMSD 07/05/18 DM0705/18012390 35000 mg/kg D.W. 250 J 740 SW846: 6010C MMSD 07/06/18 DM0706/18012405 34000 mg/kg D.W. 260 760 SW846: 6010C MMSD 07/07/18 DM0707/18012416 35000 mg/kg D.W. 260 760 SW846: 6010C MMSD Page 32 of 106 SYSACtimiloMonth/y 1/10/13 U Printed, 1/18/19 09.4; -e'MMSD IRON ICP METHOD Sample Date SBMP�e 10 Result LOD LOQ QA RMS Annual Milorganite Report January 1 to December 31, 2018 Ana""[ Method Lab 07/08/18 DM0708118012435 35000 mg/kg D.W. 260 740 SW846: 6010C MMSD 07/09/18 OM0709118012448 34000 mg/kg D.W. 260 760 SW846: 6010C MMSD 07/10/18 07/11/18 OM0710/18012474 DM0711/18012820 36000 mg/kg D.W. 34000 mg/kg D.W. 260 250 760 740 SW846: 6010C SW846: 6010C MMSD MMSD 07/12/18 07/13/18 DM0712/18012861 DM0713/18012876 33000 mg/kg D.W. 33000 mg/kg D.W. 250 250 740 740 SW846: 6010C SW846: 6010C MMSD MMSD 07/14/18 07/15/18 07/16/18 07/17/18 DM0714/18013220 DM0715/18013239 DM0716/18013252 DM0717/18013751 33000 mg/kg D.W. 34000 mg/kg D.W. 33000 mg/kg D.W. 34000 mg/kg D.W. 250 260 250 250 740 750 740 740 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 07/18/18 DM0718/18013961 33000 mg/kg D.W. 250 740 SW846: 6010C MMSD 07/19/18 07/20/18 DM0719/18014047 DM0720/18014062 33000 mg/kg D.W. 32000 mg/kg D.W. 250 260 730 740 SW846: 6010C SW846: 6010C MMSD MMSD 07/21/18 DM0721/18014073 35000 mg/kg D.W. 250 740 SW846: 6010C MMSD 07/22/18 DM0722/18014483 35000 mg/kg D.W. 260 740 SW846: 6010C MMSD 07/23/18 DM0723/18014496 34000 mg/kg D.W. 260 750 SW846: 6010C MMSD 07/24/18 DM0724/18014523 33000 mg/kg D.W. 260 750 SW846: 6010C MMSD 07/25/18 07/26/18 DM0725/18014551 DM0726/18014570 32000 mg/kg D.W. 32000 mg/kg D.W. 260 260 760 750 SW846: 6010C SW846: 6010C MMSD MMSD 07/27/18 DM0727/18014585 34000 mg/kg D.W. 250 740 SW846: 6010C MMSD 07/28/18 07/29/18 07/30/18 07/31/18 DM0728/18014676 DM0729/18014910 DM0730118014925 DM0731/18014954 35000 mg/kg D.W. 34000 mg/kg D.W. T 34000 mg/kg D.W. 34000 mg/kg D.W. 250 250 260 250 730 730 750 740 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 08/01/18 DMO801/18014969 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 08/02/18 DM0802/18015140 33000 mg/kg D.W. 250 740 SW846: 6010C MMSD 08/03/18 DM0803/18015155 32000 mg/kg D.W. 2S0 740 SW846: 6010C MMSD 08/04/18 DM0804/18015252 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/05/16 DM0805/18015279 34000 mg/kg D.W. 250 740 SW846: 6010C MMSD 08/06/18 DM0806/18015385 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/07/18 DMO807/18015414 37000 mg/kg D.W. 250 740 SW846: 6010C MMSD 08/08/18 08/09/18 08/10/18 08/11/18 DM0808/18015473 DM0809/18015500 DM0810/18015899 DM0811/18015910 37000 mg/kg D.W. 37000 mg/kg D.W. 37000 mg/kg D.W. 32000 mg/kg D.W. 250 250 250 250 730 730 730 730 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD 08/12/18 08/13/18 08/14/18 DMO812/18016203 DM0813/18016216 DMO814/18016254 34000 mg/kg D.W. 32000 mg/kg D.W. 29000 mg/kg D.W. 250 250 250 730 730 730 Q3. SW846: 6010C SW846: 6010C ` Y SW846: 6010C MMSD MMSD MMSD 08/15/18 DM0815/18016281 33000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/16/18 DMO816/18016300 26000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/17/18 DM0817/18016365 29000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/18/18 DM0818/18016505 31000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/19/18 DM0819118016525 33000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/20/18 DMO820/18016539 34000 mg/kg D.W. 2S0 730 SW846: 6010C MMSD 08/21/18 DM0821/18016714 34000 mg/kg D.W. 250 740 SW846: 6010C MMSD 08/22/18 DM0822/18016742 33000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/23/18 DMO823/18017352 32000 mg/kg D.W. 250 720 SW846: 6010C MMSD SY.S1WI MiloMonthly 1/10/13 q Page 33 of 106 Printed: 1/18/19 09:9; V a Annual Milorganite Report MMSD January 1 to December 31, 2018 41 TM R A CHUB Btu' IRON ICP METHOD Sample Date ReSUlt .. LOQ QA Flags Arahikal MethW Lab 08/24/18 DM0824/18017367 31000 mg/kg D.W. 250 730 SW846: 6010C MMSD 08/25/18 DMO825/18017378 33000 mg/kg D.W. 250 730 08/26/18 DMO826118017397 32000 mg/kg D.W. 250 720 08/27/18 DMO827/18017410 32000 mg/kg D.W. 250 730 08/28/18 DM0828/18017434 32000 mg/kg D.W. 250 730 08/29/18 DM0829/18017462 33000 mg/kg D.W. 250 730 08/30/18 DM0830/18017483 32000 mg/kg D.W. 250 740 08/31/18 DM0831/18017498 32000 mg/kg D.W. 250 740 09/01/18 DM0901/18017520 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD v SW646:6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD 09/02/18 DMO902118017752 32000 mg/kg D.W. 250 730 SW846: 6010C MMSD 09/03/18 DM0903/18018124 35000 mg/kg D.W. _ 250 730 SW846: 6010C MMSD 09/04/18 DM0904/18018149 35000 mg/kg D.W. 260 740 SW846: 6010C MMSD 09/05/18 DMO905/18018305 35000 mg/kg D.W. 260 750 SW846: 6010C MMSD 09/06/18 DMO906/18018326 36000 mg/kg D.W. 260 740 SW846: 6010C MMSD 09/07/18 DM0907/18018342 34000 mg/kg D.W. 250 740 SW846: 6010C MMSD 09/08/18 DM0908/18018353 35000 mg/kg D.W. 250 730 SW846: 6010C MMSD 09/09/18 DM0909/18018724 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD 09/10/18 DMO910118018799 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 09/11/18 DM0911/18018825 33000 mg/kg D.W. 260 740 SW846: 6010C MMSD 09/12/18 DM0912/18018854 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 09/13/18 DMO913/18018875 33000 mg/kg D.W. 260 750 Q3. SW846: 6010C MMSD 09/14/18 DM0914118018891 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 09/15/18 09/16/18 09/17/18 DMO915/18019159 DM0916/18019178 DM0917118019191 09/18/18 DM0918/18019447 09/21/18 DM0921118019515 09/22/18 DM0922/18019574 09/23/18 DMO923/18019665 09/24/18 DMO924118020088 09/25/18 DMO925/18020314 34000 mg/kg D.W. 260 750 SW846: 6010C MMSD 33000 mg/kg D.W. 260 750 SW846: 6010C MMSD 32000 mg/kg D.W. 250 730 SW846: 6010C MMSD 31000 mg/kg D.W. 260 760 SW846: 6010C MMSD 30000 mg/kg D.W. 250 720 SW846: 6010C MMSD 31000 mg/kg D.W. 250 730 SW846: 6010C MMSD 31000 mg/kg D.W. 240 710 SW846: 6010C MMSD 31000 mg/kg D.W. 250 720 SW846: 6010C MMSD 31000 mg/kg D.W. 250 730 Y SW846: 6010C MMSD 09/26/18 DMO926118020343 29000 mg/kg D.W. 260 740 SW846: 6010C MMSD 09/27/18 DM0927/18020364 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 09/28/18 DM0928/18020380 30000 mg/kg D.W. 260 760 SW846: 6010C MMSD 09/29/18 DMO929/18020391 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 09/30/18 DM0930/18020411 30000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/01/18 10/02/18 DM1001/18021136 DM1002/18021162 29000 mg/kg D.W. 27000 mg/kg D.W. 250 250 730 740 SW846: 6010C SW846: 6010C MMSD `MMSD 10/03/18 DM 1003/18021190 28000 mg/kg D.W. 260 740 SW846: 6010C MMSD 10/04/18 DM1004/18021541 32000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/05/16 DM1005/18021557 29000 mg/kg D.W. 250 740 SW846: 6010C ` MMSD 10/06/18 DM1006118021568 31000 mg/kg D.W. 260 750 SW846: 6010C MMSD 10/07/18 10/08/18 DM1007/18021588 DM1008/18021602 32000 mg/kg D.W. 31000 mg/kg D.W. 250 250 720 720 SW846: 6010C SW846: 6010C MMSD MMSD 10/09/18 DM1009118021627 30000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/10/18 DM1010/18021656 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 10/11/18 DM1011/18021975 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD Page 34 of 106 SYS/rptiMilomonthly 1/10/13 cj Printed: 1/18/19 09:4; Annual Milorganite Report 'e'ONSD January 1 to December 31, 2018 IRON ICP METHOD .. LOQ QA Flags Artalytkal Method Lab 10/12/18 DM1012/18021991 33000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/13/18 DM1013/18022006 31000 mg/kg D.W. 260 750 SW846: 6010C MMSD 10/14/18 DM1014/18022026 32000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/15/18 DM1015118022040 32000 mg/kg D.W. 260 750 SW846: 6010C MMSD 10/16/18 DM1016/18022065 33000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/17/18 DM1017/18022094 36000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/18/18 DM1018118022133 34000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/19/18 DM1019/18022269 34000 mg/kg D.W. 260 750 SW846: 6010C MMSD 10/20/18 DM1020/18022280 38000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/21/18 DM1021118022435 38000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/22/18 DM1022/18022449 40000 mg/kg D.W. 250 730 SW846: 6010C MMSD 10/23/18 10/24/18 DM1023/18022614 DM1024/18022643 41000 mg/kg D.W. 40000 mg/kg D.W. 250 250 740 740 SW846: 6010C SW846: 6010C MMSD MMSD 10/25/18 DM1025/18022708 39000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/26/18 DM1026/18022767 38000 mg/kg D.W. 250 740 SW846: 6010C MMSD 10/27/18 DM1027/18022778 38000 mg/kg D.W. 250 720 SW846: 6010C MMSD 11/07/18 DM1107118023991 48000 mg/kg D.W. 250 720 SW846: 6010C MMSD 11/08/16 DM1108/18024012 47000 mg/kg D.W. 250 _ 730 SW846: 6010C MMSD 11/09/16 DM1109118024028 48000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/10/16 DM1110/18024523 44000 mg/kg D.W. 250 720 SW846: 6010C MMSD 11/11/18 DM1111/18024619 43000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/12/18 11/13/18 11/14/18 DM1112/18024633 DM1113/18025014 DM1114/18025043 39000 mg/kg D.W. 43000 mg/kg D.W. 44000 mg/kg D.W. 260 250 260 740 740 750 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 11/15/18 DM1115/18025064 45000 mg/kg D.W. 260 740 SW846: 6010C MMSD 11/16/18 11/17/18 11/18/18 DM1116/18025080 DM1117/18025093 DM 1118/18025113 44000 mg/kg D.W. 43000 mg/kg D.W. 40000 mg/kg D.W. 260 250 260 770 740 760 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 11/19/18 DM1119118025127 41000 mg/kg D.W. 250 740 SW846: 6010C MMSD 11/20/18 DM1120/18025356 42000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/21/18 DM1121/18025385 41000 mg/kg D.W. 250 740 SW846: 6010C MMSD 11/22/18 DM1122118025406 42000 mg/kg D.W. 260 750 SW846: 6010C MMSD 11/23/18 11/24/18 DM1123118025422 DM1124/18025750 42000 mg/kg D.W. 42000 mg/kg D.W. 260 260 750 760 SW846: 6010C SW846: 6010C MMSD MMSD 11/25/18 DM1125/18025769 43000 mg/kg D.W. 260 760 SW846: 6010C MMSD 11/26/18 DM 1126/18025828 46000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/27/18 DM1127/18025860 46000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/28/18 DM1128/18025888 46000 mg/kg D.W. 250 730 SW846: 6010C MMSD 11/29/18 11/30/18 DM1129/18025956 DM 1130/18025971 46000 mg/kg D.W. 42000 mg/kg D.W. 250 260 740 750 SW846: 6010C SW846: 6010C MMSD MMSD 12/01/18 DM1201118026182 43000 mg/kg D.W. 260 750 SW846: 6010C MMSD 12/02/18 DM1202/18026201 43000 mg/kg D.W. 260 740 SW846: 6010C MMSD 12/03/18 DM1203/18026214 43000 mg/kg D.W. 250 740 SW846: 6010C MMSD 12/04/18 DM1204/18026391 41000 mg/kg D.W. 260 750 SW846: 6010C MMSD 12/05/18 DM1205/18026578 41000 mg/kg D.W. 260 750 SW846: 6010C MMSD 12/06/18 DM1206/18026621 41000 mg/kg D.W. 260 780 SW846: 6010C MMSD 12/07/18 DM1207/18026797 42000 mg/kg D.W. 260 770 SW846: 6010C MMSD SYSIrptiMiloMonthly 1/10/13 of Page 35 o/ 106 Printed.- 1/16/19 09:47 i Annual Milorganite Report MSD January 1 to December 31, 2018 HNA [IIWI FYl Mflr IRON ICP METHOD :sample Date SarnpIe ID Rj�suft .. LOQ QA "s Ana ethDd Lab 12/08/18 DM1208/18026808 49000 mg/kg D.W. 260 760 SW846: 6010C MMSD 12/09/18 DM1209/18026827 49000 mg/kg D.W. 260 750 12/10/18 DM1210/18026840 48000 mg/kg D.W. 270 780 12/11/18 DM1211/18027102 50000 mg/kg D.W. 250 740 12/12/18 DM1212/18027130 50000 mg/kg D.W. 250 730 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 12/13/18 DM1213118027253 40000 mg/kg D.W. 260 750 SW846: 6010C MMSD 12/14/18 DM1214118027306 43000 mg/kg D.W. 250 740 SW846: 6010C MMSD 12/15/18 DM1215/18027317 42000 mg/kg D.W. 250 740 SW846: 6010C MMSD 12/16/18 DM1216/18027525 42000 mg/kg D.W. 260 760 SW846: 6010C MMSD 12/17/18 DM1217/18027540 42000 mg/kg D.W. 260 770 SW846: 6010C MMSD 12/18/18 DM1218/18027643 44000 mg/kg D.W. 270 780 SW846: 6010C MMSD 12/19/18 DM1219/18027676 50000 mg/kg D.W. 260 750 Q3. SW846: 6010C MMSD 12/20/18 DM1220118027805 47000 mg/kg D.W. 250 740 SW846: 6010C MMSD 12/21/18 DM1221/18027821 48000 mg/kg D.W. 260 7S0 SW846: 6010C T MMSD 12/22/18 DM1222/18027832 50000 mg/kg D.W. 260 760 SW846: 6010C MMSD 12/23/18 DM1223/18027852 50000 mg/kg D.W. 260 760 SW846: 6010C MMSD 12/24/18 DM1224/18027883 48000 mg/kg D.W. 260 760 SW846: 6010C MMSD 12/25/18 DM1225/18027952 47000 mg/kg D.W. 260 770 SW846: 6010C MMSD 12/26/18 DM1226/18027969 47000 mg/kg D.W. 260 770 SW846: 6010C MMSD 12/27/18 DM1227/18027990 43000 mg/kg D.W. 260 770 SW846: 6010C MMSD 12/28/18 DM1228/18028005 45000 mg/kg D.W. 270 780 SW846: 6010C MMSD 12/29/18 DM1229/18028070 48000 mg/kg D.W. 260 750 SW846: 6010C MMSD 12/30/18 DM1230/18028089 50000 mg/kg D.W. 250 740 SW846: 6010C MMSD 12/31/18 DM1231/18028102 48000 mg/kg D.W. 260 750 SW846: 6010C MMSD Avg Result: 34000 mg/kg D.W. Min LOD: 96 mg/kg D.W. Max Result: 50000 mg/kg D.W. Page 36 of 106 SYS/rptt MilaMonthly 1/10/13 U Printed: 1/18/19 09:4i 01/14/18 DM0114/18000418 22 mg/kg D.W. 3.9 Annual Milorganite Report 414SD MMSD 01/15/18 DM0115/18000432 January 1 to December 31, 2018 3.9 13 SW846: 6010C MMSD 01/16/18 DM0116/18000461 LEAD ICP METHOD 3.8 13 SW846: 6010C MMSD 01/17/18 DM0117/18000652 26 mg/kg D.W. .� ..211111 !!IIj!IjjI!III!!I SW846: 6010C MMSD 01/18/18 DM0118118000673 26 mg/kg D.W. 3.8 13 SW846: 6010C 01/01/18 DMO101/18000013 21 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/02/18 DMO102/18000047 20 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/03/18 DMO103/18000061 20 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/04/18 DMO104/18000098 32 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/05/18 DMO105/18000155 18 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/06/18 DMO106/18000168 18 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/07/18 DMO107/18000189 17 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/08/18 DMO108118000203 19 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/09/18 DMO109/18000232 19 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/10/18 DM0110/18000326 19 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/11/18 DMO111/18000347 21 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/12/18 DM0112118000363 20 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/13/18 DM0113/18000397 19 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/14/18 DM0114/18000418 22 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/15/18 DM0115/18000432 22 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/16/18 DM0116/18000461 30 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/17/18 DM0117/18000652 26 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/18/18 DM0118118000673 26 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/19/18 DM0119/18000689 26 mg/kg D.W. 3.9 13 D2, Q2. SW846: 6010C MMSD 01/20/18 DMO120/18000702 27 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/21/18 DMO121/18000800 29 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/22/18 DMO122/18000814 24 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 01/23/18 DMO123/18000843 26 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/24/18 DMO124/18000875 26 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/25/18 DMO125/18000896 52 mg/kg D.W. 3.7 12 SW846: 6010C MMSD 01/26/18 DMO126/18000912 34 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/27/18 DMO127118000925 36 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/28/18 DMO128118000946 31 mg/kg D.W. 3.6 12 SW846: 6010C MMSD 01/29/18 DMO129/18001200 31 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 01/30/18 DMO130/18001229 34 mg/kg D.W. 3.6 13 SW846: 6010C MMSD 01/31/18 DMO131/18001259 31 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/01/18 DM0201/18001280 26 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/02/18 DM0202/18001421 24 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/03/18 DM0203/18001434 26 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/04/18 DM0204/18001455 25 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/05/18 DM0205/18001469 27 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/06/18 DM0206118001506 26 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/07/18 DM0207/18001599 27 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/08/18 OM0208/18001620 33 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/09/18 DM0209/18001738 29 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/10/18 DM0210/18001751 28 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/11/18 DM0211118001772 29 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/12/18 DM0212118001786 27 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/13/18 DM0213118001815 28 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/14/18 DM0214/18001860 29 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/15/18 DM0215/18001881 24 mg/kg D.W. 3.6 13 SW846: 6010C MMSD 02/16/18 DM0216/18001897 26 mg/kg D.W. 3.8 13 SW846: 6010C MMSD Page 37 of 106 SYS/rptimiloMonthly 1/10/13 fj Panted: 1/18/19 09.•47 + NNSD " PArW= LEAD ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 02/24/18 DM0224/18002427 02/25/18 DM0225/18002447 02/26/18 DM0226/18002461 02/27/18 02/17/18 DM0217/18001944 32 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/18/18 DM0218/18001965 30 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/19/18 DM0219/18001979 30 mg/kg D.W. 3.9 u 13 SW846: 6010C MMSD 02/20/18 DM0220/18002047 25 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/21/18 DM0221/18002077 26 mg/kg D.W. 3.9 13 SW846: 6010C MMSD 02/22/18 DM0222118002097 35 mg/kg D.W. 3.8 13 SW846: 6010C MMSD 02/23/18 DM0223/18002415 40 mg/kg D.W. 3.8 12 SW846: 6010C MMSD 02/24/18 DM0224/18002427 02/25/18 DM0225/18002447 02/26/18 DM0226/18002461 02/27/18 DM0227/18002537 02/28/18 03/01/18 DM0228/18002609 DM0301/18002628 03/02/18 03/03/18 03/04/18 03/05/18 03/06/18 03/07/18 03/08/18 03/09/18 03/10/18 03/11/18 03/12/18 03/13/18 03/14/18 03/15/18 03/16/18 03/17/18 03/18/18 03/19/18 03/20/18 03/21/18 03/22/18 03/23/18 DM0302/18002711 DM0303/18002722 DM0304/18002741 37 mg/kg D.W. 36 mg/kg D.W. 36 mg/kg D.W. 36 mg/kg D.W. 38 mg/kg D.W. 39 mg/kg D.W. 37 mg/kg D.W. 33 mg/kg D.W. 36 mg/kg D.W. 3.9 3.8 3.8 3.8 3.9 3.9 3.9 3.9 3.9 13 13 13 13 13 13 13 13 13 DM0305/18002805 35 mg/kg D.W. 3.9 13 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C DM0306/18002862 32 mg/kg D.W. 3.9 13 SW846: 6010C DM0307/18002927 32 mg/kg D.W. 3.9 13 SW846: 6010C DM0308/18003015 32 mg/kg D.W. 3.9 13 SW846: 6010C DM0309/18003030 35 mg/kg D.W. 3.8 13 SW846: 6010C DM0310118003041 38 mg/kg D.W. 3.9 13 SW846: 6010C DM0311/18003060 36 mg/kg D.W. 4 13 SW846: 6010C DM0312/18003335 40 mg/kg D.W. 4 13 SW846: 6010C DM0313/18003681 35 mg/kg D.W. 4 13 SW846: 6010C DM0314/18003710 36 mg/kg D.W. 4 13 SW846: 6010C DM0315/18003729 39 mg/kg D.W. 3.9 13 SW846: 6010C DM0316/18003744 34 mg/kg D.W. 4 13 SW846: 6010C DM0317118003755 36 mg/kg D.W. 3.9 13 SW846: 6010C DM0318/18003780 37 mg/kg D.W. 3.9 13 SW846: 6010C DM0319/18003911 37 mg/kg D.W. 4 13 SW846: 6010C DM0320/18003938 32 mg/kg D.W. 3.9 13 SW846: 6010C DM0321/18003967 33 mg/kg D.W. 4 13 SW846: 6010C DM0322/18004111 32 mg/kg D.W. 3.8 13 SW846: 6010C DM0323/18004126 34 mg/kg D.W. 3.8 13 SW846: 6010C 03/24/18 03/25/18 DM0324/18004137 DMO325/18004156 31 mg/kg D.W. 30 mg/kg D.W. 3.9 4 13 13 03/26/18 DM0326/18004320 29 mg/kg D.W. 3.9 13 03/27/18 03/28/18 03/29/18 DM0327/18004347 DM0328/18004376 DM0329/18004395 30 mg/kg D.W. 31 mg/kg D.W. 31 mg/kg D.W. 4 3.9 3.9 13 13 13 03/30/18 DM0330/18004410 30 mg/kg D.W. 4 13 03/31/18 DM0331/18004752 32 mg/kg D.W. 3.9 13 04/01/18 DM0401118004771 31 mg/kg D.W. 4 13 04/02/18 04/03/18 DM0402/18004784 DM0403/18004943 27 mg/kg D.W. 30 mg/kg D.W. 3.9 4.9 13 14 04/04/18 DM0404/18004972 26 mg/kg D.W. 4.7 14 SY51WIMiloMonthly 1/10/13 h MMSD MMSD mmr,n MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD mm,n MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW646:6010C MMSD SW846: 6010C MMSD ~ SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SWB46:6010C MMSD Page 38 of 106 Printed: 1/18/19 09:4; r Annual Milorganite Report 'kNSD January 1 to December 31, 2018 WINIiFk FM Argun F 1Yf LEAD ICP METHOD 04/05/18 DM0405/18005037 34 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/06/18 DM0406/18005052 33 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/07/18 DM0407/18005063 30 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/08/18 DM0408/18005082 30 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 04/09/18 DM0409/18005095 28 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/10/18 DM0410/18005164 29 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/11/18 DM0411/18005193 29 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 04/12/18 DM0412/18005446 28 mg/kg U.W. 4.8 14 SW846: 6010C MMSD 04/13/18 DM0413/18005463 28 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/14/18 DM0414/18005474 25 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/15/18 DM0415/18005605 26 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/16/18 DM0416/18005618 29 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/17/18 DM0417/18005709 29 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/18/18 DM0418/18005738 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/19/18 DM0419/18005757 32 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/20/18 DM0420/18006009 34 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/21/18 DM0421/18006020 37 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/22/18 DM0422/18006039 39 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/23/18 DM0423/18006157 38 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/24/18 DM0424/18006185 40 mg/kg D.W. 4.8 14 SW846: 6010C _ MMSD 04/25/18 DM0425/18006214 40 mg/kg D.W. 5 15 SW846: 6010C MMSD 04/26/18 DM0426/18006233 36 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/27/18 DM0427/18006441 37 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/28/18 DM0428/18006452 36 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/29/18 DM0429/18006471 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 04/30/18 DM0430/18006484 28 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/01/18 DM0501/18006571 24 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/02/18 DM0502/18006600 29 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/03/18 DM0503/18006854 25 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 05/04/18 DM0504118007005 25 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/05/18 DM0505118007016 32 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/06/18 DM0506/18007035 27 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/07/18 DM0507/18007257 31 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/08/18 DM0508/18007284 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/09/18 DM0509/18007313 31 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/10/18 DMO510/18007340 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/11/18 DMO511/18007418 32 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 05/12/18 DMO512/18007429 33 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/13/18 DMO513/18007476 37 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/14/18 DM0514/18007591 35 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/15/18 DMO515/18007976 39 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/16/18 DMO516/18008005 41 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/17/18 DM0517/18008103 40 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/18/18 DM0518/18008118 41 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/19/18 DM0519/18008129 38 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/20/18 DM0520/18008196 38 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/21/18 DM0521/18008209 38 mg/kg D.W. 4.8 14 SW846: 6010C MMSD Page 39 of 106 5YS/rpt.tMi1bMonth1y 1/10/13 0 Printed: 1118/19 09,14; • 05/26/18 DMO526/18008684 36 mg/kg D.W. 4.6 Annual Milorganite Report MMSD MMSD 05/27/18 DM0527/18008703 35 mg/kg D.W. January 1 to December 31, 2018 14 SW846: 6010C MMSD 05/28/18 DMO528/18008716 LEAD ICP METHOD 4.9 14 SW846: 6010C MMSD 05/22/18 DM0522/18008236 37 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/23/18 DM0523/18008304 38 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/24/18 DM0524/18008658 39 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/25/18 DMO525/18008673 35 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/26/18 DMO526/18008684 36 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/27/18 DM0527/18008703 35 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/28/18 DMO528/18008716 35 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 05/29/18 DMO529/18008888 34 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 05/30/18 DMO530/18008917 30 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 05/31/18 DMO531118008936 37 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/01/18 DM0601/18009150 37 mg/kg D.W. 4.6 14 SW846: 6010C MMSD f 06/02/18 DM0602/18009161 35 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/03/18 DMO603/18009335 37 mg/kg D.W. 4.7 14 SW846-.6010C MMSD 06/04/18 DM0604118009348 37 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/05/18 DM0605118009375 35 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/06/18 DM0606/18009404 36 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/07/18 DM0607/18009423 39 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/08/18 DM0608/18009822 36 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/09/18 DM0609/18009833 40 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/10/18 DM0610/18009852 39 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/11/18 DM0611/18009865 41 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/12/18 DM0612/18010098 42 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/13/18 DM0613/18010127 41 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/14/18 DM0614/18010437 41 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/15/18 DM0615/18010452 45 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/16/18 DM0616/18010463 39 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/17/18 DM0617/18010482 44 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/18/18 DM0618/18010639 43 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/19/18 DMO619/18010666 47 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 06/20/18 DM0620/18010694 49 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/21/18 DM0621/18010713 48 mg/kg D.W. 4.6 14 SW846: 6010C J� MMSD 06/22/18 DM0622/18010939 56 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/23/18 DM0623/18010950 61 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/24/18 DM0624/18011087 54 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/25/18 DM0625/18011182 51 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/26/18 DM0626118011209 41 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/27/18 DM0627/18011597 37 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/28/18 DM0628/18011616 43 mg/kg D.W. 4.7 14 Q3. SW846: 6010C MMSD 06/29/18 DMO629/18011631 50 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 06/30/18 DM0630/18011642 44 mg/kg D.W. 4.8 14 SWB46: 6010C MMSD 07/01/18 DM0701/18011728 46 mg/kg D.W. 4.7 14 SWB46: 6010C MMSD 07/02/18 DM0702118011741 48 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 07/03/16 f DM0703/18011881 46 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 07/04/18 DM0704/18011909 48 mg/kg D.W. 4.6 14 SW846: 6010C - MMSD 07/05/18 DM0705/18012390 41 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 07/06/18 DM0706/18012405 42 mg/kg D.W. 4.7 14 f SW846 6010C MMSD 07/07/18 DM0707/18012416 54 mg/kg D.W. 4.8 14 SW846: 6010C MMSD SY5/rptlMiloManthly 1/10/13 0 Page 40 of 104 Printed: 1/18/19 09:4; 'e-kNSD DM0716/18013252 07/17/18 DM0717/18013751 Annual Milorganite Report DM0718/18013961 07/19/18 DM0719/18014047 07/20/18 January 1 to December 31, 2018 olfrm,. Flo 10!iBilis'L^11lp1 4.7 14 07/27/18 DM0727/18014585 49 mg/kg D.W. LEAD ICP METHOD Samplk� ID Result .. LOQ .. Flalp. .Lab 07/08/18 DM0708/18012435 54 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 07/09/18 DM0709118012448 47 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 07/10/18 DM0710/18012474 43 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 07/11/18 DM0711/18012820 42 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 07/12/18 DM0712/18012861 51 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 07/13/18 DM0713/18012876 48 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 07/14/16 DM0714/18013220 45 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 07/15/18 DM0715/18013239 07/16/18 DM0716/18013252 07/17/18 DM0717/18013751 07/18/18 DM0718/18013961 07/19/18 DM0719/18014047 07/20/18 DM0720/18014062 07/21/18 DM0721118014073 07/22/18 DM0722/18014483 07/23/18 DM0723/18014496 43 mg/kg D.W. 4.7 14 41 mg/kg D.W. 4.6 14 44 mg/kg D.W. 4.6 14 43 mg/kg D.W. 4.6 14 45 mg/kg D.W. 45 mg/kg D.W. 4.6 14 4.7 14 42 mg/kg D.W. 4.6 14 45 mg/kg D.W. 4.7 14 46 mg/kg D.W. 4.7 14 07/24/18 DM0724/18014523 48 mg/kg D.W. 4.7 14 07/25/18 DM0725/18014551 50 mg/kg D.W. 4.8 14 07/26/18 DM0726/18014570 53 mg/kg D.W. 4.7 14 07/27/18 DM0727/18014585 49 mg/kg D.W. 4.6 14 07/28/18 DM0728/18014676 45 mg/kg D.W. 4.6 14 07/29/16 07/30/18 DM0729/18014910 DM0730/18014925 45 mg/kg D.W. 46 mg/kg D.W. 4.6 14 4.7 14 07/31/18 08/01/18 DM0731/18014954 DM0801/18014969 48 mg/kg D.W. 44 mg/kg D.W. 4.7 14 4.6 14 08/02/18 DM0802/18015140 46 mg/kg D.W. 4.6 14 08/03/18 DM0803/18015155 45 mg/kg D.W. 4.7 14 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 08/04/18 DM0804/18015252 46 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/05/18 DM0805/18015279 45 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 08/06/18 DM0806/18015385 45 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/07/18 DMO807/18015414 44 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/08/18 DMO808118015473 50 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/09/18 08/10/18 08/11/16 DMO809/18015500 DMO810/18015899 DMO811118015910 48 mg/kg D.W. 53 mg/kg D.W. 49 mg/kg D.W. 4.6 4.6 4.6 14 14 14 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 08/12/16 08/13/18 08/14/18 DMO812/18016203 DM0813118016216 v DM0814/18016254 47 mg/kg D.W. 46 mg/kg D.W. 43 mg/kg D.W. 4.6 4.6 4.6 14 14 14 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 08/15/18 DMO815/18016281 54 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/16/18 DM0816/18016300 55 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/17/18 DMO817/18016365 51 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/18/18 DM0818/18016505 47 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/19/18 08/20/18 DM0819/18016525 DMO820/18016539 50 mg/kg D.W. 50 mg/kg D.W. 4.6 4.6 14 14 SW846: 6010C SW846: 6010C MMSD MMSD 08/21/18 DM0821/18016714 49 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/22/18 DM0822/18016742 47 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/23/18 DMO823/18017352 52 mg/kg D.W. 4.6 13 SW846: 6010C MMSD SYSIXPUMMONontMy 1/10/13 tj Page 41 of 106 Printed: 1/18/19 09:4; A. MMSD LEAD ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 08/24/18 DMO824/18017367 55 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 08/25/18 DM0825/18017378 57 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/26/18 DM0826/18017397 53 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 08/27/18 DM0827/18017410 51 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/28/18 DM0828/18017434 T 54 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/29/18 DM0829/18017462 �59 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 08/30/18 DMOS30/18017483 60 mg/kg D.W. 4.6 14 T SW846: 6010C MMSD 08/31/18 DM0831/18017498 57 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/01/18 DMO901/18017520 r 63 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/02/18 DM0902/18017752 60 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/03/18 DMO903118018124 60 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/04/18 DMO904/18018149 57 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/05/18 DMO905/18018305 60 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/06/18 DMO906/18018326 59 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/07/18 DMO907/18018342 62 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/08/18 DMO908/18018353 66 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/09/18 DMO909/18018724 63 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/10/18 DMO910118018799 62 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/11/18 DMO911/18018825 63 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/12/18 DMO912118018854 63 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/13/18 DMO913118018875 61 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/14/18 DM0914118018891 61 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/15/18 DM0915/18019159 64 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/16/18 DMO916/18019178 62 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/17/18 DM0917/18019191 63 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/18/18 DMO918/18019447 68 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 09/21/16 DM0921/18019515 70 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 09/22/18 DM0922/18019574 72 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/23/18 DM0923/18019665 76 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 09/24/18 DMO924/18020088 75 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 09/25/18 DM0925118020314 72 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/26/18 DM0926/18020343 74 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/27/18 DM0927/18020364 73 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 09/28/18 DM0928/18020380 66 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 09/29/18 DM0929/18020391 62 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 09/30/18 DM0930/18020411 61 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/01/18 DM1001/18021136 `64 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/02/18 DM1002118021162 68 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/03/18 DM1003/18021190 66 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/04/18 DM1004/18021541 74 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/05/18 DM1005/18021557 77 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/06/18 DM1006/18021668 69 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/07/18 DM1007/18021588 72 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 10/08/18 ` DM1008/18021602 67 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 10/09/18 DM1009/18021627 62 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/10/18 DM1010/18021656 64 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/11/18 DM1011/18021975 59 mg/kg D.W. 4.6 14 SW846: 6010C MMSD Page 42 of 106 SYS/rptlMiloMonthly 1/10/13 tj Printed., 1/18/19 09:4; Annual Milorganite Report MMSD January 1 to December 31, 2018 MI0r8� RR 1 [if 1�R f11f1Dllq'af LEAD ICP METHOD a OD LOQ QA Flags Analytical Method Lat� 10/12/18 DM1012/18021991 56 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/13/18 DM1013118022006 53 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/14/18 DM1014/18022026 53 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/15/18 DM1015/18022040 51 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/16/18 DM1016/18022065 53 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/17/18 DM1017/18022094 52 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/18/18 DM1018/18022133 49 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/19/18 DM1019/18022269 51 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/20/18 DM1020/18022280 56 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/21/18 OM1021/18022435 51 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/22/18 DM1022/18022449 49 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/23/18 DM1023/18022614 48 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/24/18 DM1024/18022643 44 mg/kg D.W. 4.7 14 SW646: 6010C MMSD 10/25/18 DM1025/18022708 42 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 10/26/18 DM1026/18022767 42 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 10/27/18 DM1027/18022778 43 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 11/07/18 DM 1107/18023991 36 mg/kg D.W. 4.5 13 SW846: 6010C MMSD 11/08/18 DM 1108/18024012 36 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/09/18 DM1109/18024028 39 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/10/18 DM 1110/ 18024523 36 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 11/11/18 DMI 111/18024619 38 mg/kg D.W. 4.6 13 SW846: 6010C MMSD 11/12/18 DM 1112/18024633 35 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/13/18 DM 1113/18025014 34 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/14/18 DM1114/18025043 35 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/15/18 DM 1115/18025064 33 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/16/18 DM1116/18025080 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 11/17/18 DM1117/18025093 33 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/18/18 DM1118/18025113 31 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/19/18 DM1119/18025127 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/20/18 DM1120118025356 32 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/21/18 DM1121/18025385 31 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/22/18 DM1122118025406 31 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/23/18 DM 1123/18025422 30 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/24/18 DM 1124/18025750 31 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 11/25/18 DM 1125/18025769 29 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 11/26/18 DM1126/18025828 28 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/27/18 DM1127/18025860 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/28/18 DM1128118025888 27 mg/kg D.W. 4.6 T 14 SW846: 6010C MMSD 11/29/18 DM1129/18025956 31 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 11/30/18 DMI 130/18025971 T! 26 mg/kg D,W. 4.7 14 SW846: 6010C MMSD 12/01/18 DM1201/18026182 28 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/02/18 DM1202/18026201 26 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/03/18 DM1203/18026214 28 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/04/18 DM1204/18026391 30 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/05/18 DM1205/18026578 33 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/06/18 DM1206/18026621 32 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 12/07/18 DM1207/18026797 32 mg/kg D.W. 4.8 14 SW846: 6010C MMSD Page 43 of 106 SYS/rptlMiloMonthly 1/10/13 tj Printed: 1/18/19 09:47 SYS/ratlMiloMonthfy 1/10/13 tj Page 44 of 106 Printed: 1/18/19 09:4i Annual Milorganite Report e-MMSD January 1 to December 31, 2018 LEAD ICP METHOD Date Sample I D Resuft LOD LOQ QA Rags Analrtkaf Mettwd Lab 12/08/18 DM1208/18026808 30 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/09/18 DM1209/18026827 28 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/10/18 DM1210/18026840 28 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 12/11/18 DM1211/18027102 28 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/12/18 Y DM1212/18027130 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/13/18 DM1213/18027253 29 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/14/18 DM1214/18027306 31 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/15/18 DM1215/18027317 28 mg/kg D.W. 4.7 14 ~ SW846: 6010C MMSD 12/16/18 DM1216/18027525 28 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/17/18 DM1217/18027540 27 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/18/16 DM1218/18027643 27 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 12/19/18 DM1219118027676 28 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/20/18 DM1220/18027805 26 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/21/18 DM1221/18027821 28 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/22/18 DM1222/18027832 29 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/23/18 DM1223118027852 27 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/24/18 DM1224/18027883 26 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/25/18 DM1225118027952 26 mg/kg D.W. T 4.8 14 SW846: 6010C MMSD 12/26/18 DM1226/18027969 26 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/27/18 DM1227/18027990 26 mg/kg D.W. 4.8 14 SW846: 6010C MMSD 12/28/18 DM1228/18028005 25 mg/kg D.W. 4.9 14 SW846: 6010C MMSD 12/29/18 DM1229/18028070 29 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/30/18 DM1230/18028089 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/31/18 DM1231/18028102 29 mg/kg D.W. 4.7 14 SW846: 6010C MMSD Avg Result: 40 mg/kg D.W. Min LOD: 3.7 mg/kg D.W. Max Result: 77 mg/kg D.W. SYS/ratlMiloMonthfy 1/10/13 tj Page 44 of 106 Printed: 1/18/19 09:4i 02/03/18 02/17/18 03/10/18 03/17/18 03/24/18 WMC05/18001471 0.13 mg/kg D.W. 0.0024 0.0082 Annual Milorganite Report eNNSD WMC06/18001788 0.14 mg/kg D.W. 0.0023 0.0078 January 1 to December 31, 2018 Cr Lab WMC07/18001981 0.078 mg/kg D.W. 0.0024 0.0081 MERCURYby M. 7471 (sludge) Cr Lab � � � , • 0.0023 �iliiliYr�. 01/06/18 WMC01/18000205 0.04 mg/kg D.W. 0.0023 • , 0.0078 AX. EPA 7471B CT Lab 01/13/18 WMCO2/18000434 0.041 mg/kg D.W. 0.0023 0.0077 EPA 7471B CT Lab 01/20/18 WMC03118000816 0.074 mg/kg D.W. 0.0023 0.0077 EPA 7471B Cr Lab 01/27/18 WMC04/18001202 0.1 mg/kg D.W. 0.0022 0.0076 AX. EPA 74716 Cr Lab 02/03/18 02/17/18 03/10/18 03/17/18 03/24/18 WMC05/18001471 0.13 mg/kg D.W. 0.0024 0.0082 EPA 7471B Cr Lab WMC06/18001788 0.14 mg/kg D.W. 0.0023 0.0078 EPA 7471B Cr Lab WMC07/18001981 0.078 mg/kg D.W. 0.0024 0.0081 EPA 74716 Cr Lab WMC08/18002463 0.048 mg/kg D.W. 0.0023 0.0077 EPA 7471B Cr Lab WMC09118002807 WMC10/18003337 0.076 mg/kg D.W. 0.014 mg/kg D.W. 0.0023 0.0024 0.008 0.0082 EPA 74718 EPA 7471B Cr Lab Cr Lab WMC11/18003913 < 0.0024 mg/kg D.W. 0.0024 0.008 WMC12/18004322 0.019 mg/kg D.W. 0.0024 0.0081 03/31/18 WMC13/18004786 < 0.0025 mg/kg D.W. 0.0025 0.0085 EPA 74718 Cr Lab EPA 7471B Cr Lab EPA 7471B Cr Lab 04/07/18 WMC14/18005097 0.0087 mg/kg D.W. 0.0024 0.0082 EPA 74716 Cr Lab 04/14/18 04/21/18 WMC15/18006159 WMC16118006160 < 0.0025 mg/kg D.W. < 0.0023 mg/kg D.W. 0.0025 0.0023 0.0085 0.0079 EPA 7471B EPA 7471B Cr Lab Cr Lab 04/28/18 05/05/18 05/12/18 05/19/18 05/26/18 06/02/18 06/09/18 06/16/18 06/23/18 06/30/18 07/07/18 WMC17/18006486 WMC18118007259 WMC19/18007645 WMC20/18008211 WMC21/18008718 WMC22/18009350 WMC23/18009867 WMC24/18010641 WMC25118011184 WMC26/18011743 WMC27118013254 0.036 mg/kg D.W. < 0.0024 mg/kg D.W. < 0.0024 mg/kg D.W. 0.19 mg/kg D.W. 0.021 mg/kg D.W. 0.23 mg/kg D.W. 0.24 mg/kg D.W. 0.048 mg/kg D.W. 0.062 mg/kg D.W. 0.25 mg/kg D.W. 0.22 mg/kg D.W. 0.0023 0.0024 0.0024 0.0023 0.0024 0.0023 0.0024 0.0024 0.0022 0.0024 0.0023 0.0077 0.0082 0.0082 0.0077 0.0083 0.0079 0.0081 0.0083 0.0074 0.0083 0.0077 AX. AX. AX. EPA 74716 EPA 74716 EPA 7471B EPA 7471B EPA 74718 EPA 74718 EPA 7471B EPA 7471B EPA 74718 EPA 7471B EPA 74718 Cr Lab CT Lab Cr Lab Cr Lab Cr Lab CT Lab CT Lab Cr Lab Cr Lab Cr Lab CT Lab 07/14/18 WMC28/18013259 0.21 mg/kg D.W. 0.0057 0.019 EPA 74718 Cr Lab 07/21/18 WMC29/18014498 0.27 mg/kg D.W. 0.0054 0.018 AX. EPA 74716 Cr Lab 07/28/18 WMC30/18014929 0.084 mg/kg D.W. 0.0057 0.019 EPA 74716 Cr Lab 08/04/18 WMC31/18015389 0.21 mg/kg D.W. 0.0056 0.019 EPA 7471B Cr Lab 08/11/18 WMC32/18016218 0.29 mg/kg D.W. 0.0053 0.018 EPA 74718 Cr Lab 08/18/18 08/25/18 09/01/18 WMC33/18016543 WMC34/18018126 WMC35/18018151 0.3 mg/kg D.W. 0.22 mg/kg D.W. < 0.0052 mg/kg D.W. 0.0057 0.0056 0.0052 0.019 0.019 0.018 AX. EPA 7471B EPA 74718 EPA 7471B Cr Lab Cr Lab Cr Lab 09/08/18 WMC36/18018801 0.34 mg/kg D.W. 0.0054 0.018 EPA 74716 CT Lab 09/15/18 WMC37/18019193 0.23 mg/kg D.W. 0.0057 0.019 EPA 74716 Cr Lab 09/22/18 WMC38/18021138 0.025 mg/kg D.W. 0.0057 0.002 EPA 74718 Cr Lab 09/29/18 WMC39118021139 0.16 mg/kg D.W. 0.0052 0.018 EPA 74716 Cr Lab 10/06/18 WMC40118021604 < 0.0058 mg/kg D.W. 0.0058 0.02 AX. EPA 74716 Cr Lab 10/13/18 WMC41/18022042 < 0.0052 mg/kg D.W. 0.0052 0.018 AX. EPA 74716 Cr Lab 10/20/18 WMC42/18022451 0.2 mg/kg D.W. 0.0058 0.02 EPA 74718 Cr Lab 10/27/18 WMC43/18022969 0.033 mg/kg D.W. 0.0058 0.02 EPA 74718 CT Lab 11/10/18 WMC45/18025129 0.3 mg/kg D.W. 0.0057 0.019 EPA 74716 Cr Lab 11/17/18 WMC46/18024635 0.36 mg/kg D.W. 0.0058 0.02 EPA 74716 Cr Lab 11/24/18 WMC47/18025830 0.041 mg/kg D.W. 0.0057 0.019 EPA 74718 Cr Lab 12/01/18 WMC48/18026216 0.13 mg/kg D.W. 0.0055 0.019 EPA 7471B Cr Lab SYSIrpt1M/loMonthly 1/10/13 U Page 45 of 106 Printed., 1/18/19 09:47 Q a eNNSD w71tFt3 fm A cum E>I k[!77 MERCURY by M. 7471 (sludge) 12/08/18 WMC49/18026842 0.17 mg/kg D.W. 12/15/18 WMC50118027542 0.13 mg/kg D.W. 12/22/18 WMC51/18027885 0.28 mg/kg D.W. 12/29/18 WMC52/18028104 Avg Result: 0.12 mg/kg D.W. SY51rpt1M110N0nthly 1110/13 tj Annual Milorganite Report January 1 to December 31, 2018 0.0058 0.02 EPA 7471B CT Lab 0.0057 0.019 EPA 7471B CT Lab 0.0059 0.02 EPA 74718 CT Lab 0.22 mg/kg D.W. 0.0057 0.02 EPA 74716 CT Lab Min LOD: 0.0022 mg/kg D.W. Max Result: 0.36 mg/kg D.W. Page 46 of 106 Printed: 1/18/19 09:4; -e-MMSD DMO129/18001200 9.9 mg/kg D.W. 0.84 Annual Milorganite Report SW846: 6010C MMSD 01/30/18 DMO130/18001229 10 mg/kg D.W. January 1 to December 31, 2018 0WIT {aA[!t", SW846: 6010C MMSD 01/31/18 DMO131/18001259 10 mg/kg D.W. 0.85 MOLYBDENUM ICP METHOD Sample .. SW846: 6010C MMSD LGQ Flags AnaMkal MethW Lab 01/01/18 DMO101/18000013 11 mg/kg D.W. .. 0.86 QA 2.8 SW846: 6010C MMSD 01/02/16 DMO102/18000047 12 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 01/03/18 DMO103/18000061 it mg/kg D.W. 0.88 2.9 SW846: 6010C MMSD 01/04/18 DMO104118000098 10 mg/kg D.W. 0.86 2.8 SW646: 6010C MMSD 01/05/18 DMO105/18000155 10 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/06/18 DMO106/18000168 11 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/07/18 DMO107118000189 10 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/08/18 DMO108/18000203 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/09/18 DMO109/18000232 12 mg/kg D.W. 0.87 2.8 ^� SW846: 6010C MMSD 01/10/18 DM0110118000326 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/11/18 DM0111/18000347 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/12/18 DM0112118000363 10 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/13/18 DM0113/18000397 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/14/18 DM0114/18000418 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/15/18 DM0115/18000432 11 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/16/18 DM0116/18000461 12 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/17/18 DM0117/18000652 11 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 01/18/18 DM0118/18000673 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/19/18 DM0119/18000689 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/20/18 DMO120/18000702 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/21/18 DMO121/18000800 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 01/22/18 DMO122/18000814 9.4 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/23/18 DMO123/18000843 9.7 mg/kg D.W. 0.88 2.8 SW846: 6010C MMSD 01/24/18 DMOl24/18000875 11 mg/kg D.W. 0.65 2.8 SW846: 6010C MMSD 01/25/18 DMO125/18000896 12 mg/kg D.W. 0.83 2.7 SW846: 6010C MMSD 01/26/18 DMO126/18000912 11 mg/kg D.W. 0.84 2.7 SW846: 6010C MMSD 01/27/18 DMO127/18000925 10 mg/kg D.W. 0.85 2.8 SWB46: 6010C MMSD 01/28/18 DMO128118000946 10 mg/kg D.W. 0.84 2.7 SW846: 6010C MMSD 01/29/18 DMO129/18001200 9.9 mg/kg D.W. 0.84 2.7 SW846: 6010C MMSD 01/30/18 DMO130/18001229 10 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 01/31/18 DMO131/18001259 10 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 02/01/18 02/02/18 02/03/18 DM0201/18001280 DM0202/18001421 DM0203/18001434 10 mg/kg D.W. 10 mg/kg D.W. 9.3 mg/kg D.W. 0.86 0.85 0.85 2.8 2.8 2.8 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 02/04/18 DM0204/18001455 9.8 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 02/05/18 02/06/18 DM0205/18001469 DM0206/18001506 9.2 mg/kg D.W. 9 mg/kg D.W. 0.86 0.85 2.8 2.8 SW846: 6010C SW846: 6010C MMSD MMSD 02/07/18 DM0207/18001599 9.2 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 02/08/18 DM0208/18001620 9.9 mg/kg D.W. 0.85 2.8 SW646: 6010C MMSD 02/09/18 DM0209/18001738 9.6 mg/kg D.W. 0.84 2.7 SW846: 6010C MMSD 02/10/18 DM0210/18001751 9.8 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 02/11/18 DM0211/18001772 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 02/12/18 DM0212/18001786 10 mg/kg D.W. 0.86 2.8 SW846: 6010C MMSD 02/13/18 DM0213/18001815 9.6 mg/kg D.W. 0.87 2.8 SW846: 6010C MMSD 02/14/18 DM0214/18001860 9.6 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 02/15/18 DM0215/18001881 10 mg/kg D.W. 0.85 2.8 SW846: 6010C MMSD 02/16/18 DM0216/18001897 10 mg/kg D.W. 0.84 2.7 SW846: 6010C MMSD Page 47 of 106 SYS/rptlMiloMonthly 1/10/13 tj Panted: 1/18/19 09:4) ?, MMSD hATYM fm A CUM Y MOLYBDENUM ICP METHOD 02/17/18 DM0217/18001944 11 mg/kg D.W. 0.86 02/18/18 DM0218/18001965 13 mg/kg D.W. 0.86 02/19/18 DM0219/18001979 11 mg/kg D.W. 0.87 02/20/18 02/21/18 02/22/18 02/23/18 02/24/18 02/25/18 02/26/18 DM0220/18002047 10 mg/kg D.W. 0.86 DM0221/18002077 DM0222/18002097 DM0223118002415 DM0224/18002427 DM0225118002447 DM0226/18002461 02/27/18 DM0227/18002537 02/28/18 DM0228/18002609 03/01/16 DM0301/18002628 03/02/18 DM0302/18002711 03/03/18 DM0303/18002722 03/04/18 DM0304/18002741 03/05/18 DM0305/18002805 03/06/18 DM0306/18002862 03/07/18 DM0307/18002927 03/08/18 DM0308/18003015 03/09/18 DM0309/1 8003030 03/10/18 DM0310/18003041 03/11/18 DM0311/18003060 03/12/18 DM0312118003335 03/13/18 DM0313/18003681 03/14/18 DM0314/18003710 03/15/18 DM0315/18003729 03/16/18 DM0316118003744 03/17/18 DM0317/18003755 03/18/18 DM0318/18003780 03/19/18 DM0319/18003911 03/20/18 DM0320/18003938 03/21/18 DM0321/18003967 03/22/18 DM0322118004111 03/23/18 DM0323/18004126 03/24/18 DM0324118004137 03/25/18 DM0325/18004156 03/26/18 DM0326/18004320 03/27/18 DM0327/18004347 03/28/18 DM0328/18004376 03/29/18 DM0329/18004395 03/30/18 DM0330/180044101 03/31/18 DM0331/18004752 04/01/18 DM0401/18004771 04/02/18 DM0402118004784 Annual Milorganite Report January 1 to December 31, 2018 2.8 SW846: 6010C MMSD 2.8 SW846: 6010C MMSD 2.8 SW846: 6010C MMSD 2.8 SW846: 6010C MMSD 9.8 mg/kg D.W. 0.86 2.8 9.2 mg/kg D.W. 0.85 2.8 9.1 mg/kg D.W. 0.84 2.7 8.8 mg/kg D.W. 0.86 2.B 9.2 mg/kg D.W. 0.84 2.7 9.2 mg/kg D.W. 0.85 2.8 9 mg/kg D.W. 0.86 2.8 9.6 mg/kg D.W. 10 mg/kg D.W. 0.86 0.87 2.8 2.8 9.3 mg/kg D.W. 0.86 2.8 8.6 mg/kg D.W. 0.87 2.8 9.2 mg/kg D.W. 0.86 2.8 9.3 mg/kg D.W. 0.87 2.8 9.5 mg/kg D.W. 0.86 2.8 9.5 mg/kg D.W. 0.88 2.8 - - 9.2 mg/kg D.W. 0.86 2.8 9.5 mg/kg D.W. 0.84 2.7 9 mg/kg D.W. 0.87 2.8 9 mg/kg D.W. 0.88 2.9 9.1 mg/kg D.W. 0.89 2.9 9.6 mg/kg D.W. 0.89 2.9 9.8 mg/kg D.W. 0.88 2.9 9.2 mg/kg D.W. 0.86 2.8 9 mg/kg D.W. 0.88 2.9 10 mg/kg D.W. 0.88 2.8 10 mg/kg D.W. 0.87 2.8 10 mg/kg D.W. 0.89 2.9 9.2 mg/kg D.W. 0.87 2.8 9.5 mg/kg D.W. 0.88 ' 2.8 9.5 mg/kg D.W. 0.85 2.8 9.4 mg/kg D.W. 0.84 2.7 8.2 mg/kg D.W. 0.88 2.8 8.2 mg/kg D.W. 0.88 2.9 8.9 mg/kg D.W. 0.87 2.8 -- 9.5 mg/kg D.W. 0.88 2.9 9.3 mg/kg D.W. 0.88 2.8 8.8 mg/kg D.W. 0.86 2.8 8.7 mg/kg D.W. 0.9 2.9 9.6 mg/kg D.W. 0.86 2.8 9.8 mg/kg D.W. 0.89 2.9 9.4 mg/kg D.W. 0.86 2.8 04/03/18 DM0403/18004943 9.8 mg/kg D.W. 1.3 5.8 04/04/18 DM0404/18004972 SYSIVIM&Nonthly 1/10/13 U 8.8 mg/kg D.W. 1.3 5.6 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 48 of 106 Printed: 1/18/19 09.4; Annual Milorganite Report efffl% January 1 to December 31, 2018 Iltl 7w iv1 nEl►' MOLYBDENUM ICP METHOD 04/05/18 DM0405/18005037 10 mg/kg D.W. .. 1.3 LOQ QA Sags 5.7 Analyt" Method SW846: 6010C Ub MMSD 04/06/18 DM0406/18005052 12 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/07/18 DM0407/18005063 10 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/08/18 DM0408/18005082 10 mg/kg D.W. 1.3 5.8 SW846: 6010C MMSD 04/09/18 DM0409/18005095 10 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/10/18 DM0410/18005164 10 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/11/18 DM0411/18005193 9.5 mg/kg D.W. 1.3 5.8 SW846: 6010C MMSD 04/12/18 DM0412/18005446 9.6 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/13/18 DM0413/18005463 9.5 mg/kg D.W. 1.3 5.7 _ SW846: 6010C MMSD 04/14/18 DM0414/18005474 9.5 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/15/18 DM0415/18005605 9.2 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/16/18 DM0416/18005618 9.3 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/17/18 DM0417118005709 9 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/18/18 DM0418/18005738 9.5 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/19/18 DM0419/18005757 9.2 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 04/20/18 DM0420118006009 9 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 04/21/18 DM0421/18006020 9.8 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/22/18 DM0422/18006039 9.9 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/23/18 DM0423118006157 9.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 04/24/18 DM0424/18006185 9.4 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 04/25/18 DM0425/18006214 10 mg/kg D.W. 1.4 5.9 SW846: 6010C MMSD 04/26/18 DM0426/18006233 9.4 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/27/18 DM0427118006441 9.6 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 04/28/18 DM0428/18006452 9.2 mg/kg D.W. y 1.3 5.7 SW846: 6010C MMSD T 04/29/18 DM0429/18006471 8.9 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 04/30/18 DM0430/18006484 9.6 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/01/18 DM0501/18006571 9 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/02/18 DM0502/18006600 9.4 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/03/18 DM0503118006854 8.8 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 05/04/18 DM0504118007005 9.4 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 05/05/18 DM0505/18007016 9.6 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/06/18 DM0506/18007035 10 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/07/18 DMO507/18007257 10 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 05/08/18 DM0508/18007284 9.4 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/09/18 DMO509/18007313 8.6 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/10/18 DM0510/18007340 9.3 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/11/18 DMO511/18007418 9.9 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/12/18 DM0512/18007429 T 9.5 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/13/18 DMO513/18007476 9.2 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/14/18 DM0514/18007591 9.3 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/15/18 DM0515/18007976 8.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 05/16/18 DM0516/18008005 8.9 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/17/18 DMO517/18008103 8.7 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/18/18 DM0518/18008118 8.9 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/19/18 DMO519/18008129 8.4 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 05/20/18 DM0520/18008196 8.7 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 05/21/18 DM0521/18008209 9.3 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD Page 49 of 106 SYS/rptl MiloMonthly 1/10/13 tj Prrnted.• 1/18/19 09:42 11 MMSD P.ul W i C113,1FR FYd�1R4tfMt MOLYBDENUM ICP METHOD Z= --i 05/22/18 DM0522/18008236 05/23/18 DMO523/18008304 05/24/18 DM0524118008658 05/25/18 DM0525/18008673 05/26/18 DMO526118008684 05/27/18 DM0527/18008703 05/28/18 DMO528/18008716 05/29/18 DMO529/18008888 05/30/18 05/31/18 06/01/18 06/02/18 06/03/18 06/04/18 06/05/18 06/06/18 06/07/18 9.3 mg/kg D.W. 1.3 5.7 9.3 mg/kg D.W. 8.5 mg/kg D.W. 1.3 1.2 5.6 5.4 8.6 mg/kg D.W. 9 mg/kg D.W. 1.3 1.3 5.5 5.5 9.2 mg/kg D.W. 1.3 5.7 9.2 mg/kg D.W. 1.3 5.7 9 mg/kg D.W. 1.3 5.7 Annual Milorganite Report January 1 W December 31, 2018 SW846:6010C SW846:6010C MMSD MMSD SW846:6010C MMSD SW846:6010C MMSD DM0530/18008917 9.6 mg/kg D.W. 1.3 5.6 DM0531/18008936 J� 9.1 mg/kg D.W. 1.3 5.6 DM0601/18009150 9.9 mg/kg D.W. 1.3 5.5 ^` DM0602/18009161 9.3 mg/kg D.W. 1.3 5.6 DM0603/18009335 9.1 mg/kg D.W. 1.3 5.6 DM0604/18009348 T 9.2 mg/kg D.W. 1.3 5.5 DM0605118009375 9.2 mg/kg D.W. 1.3 5.6 DM0606/18009404 9.2 mg/kg D.W. 1.3 5.7 DM0607/18009423 8.9 mg/kg D.W. 1.3 5.6 06/08/18 DM0608/18009822 06/09/18 DM0609/18009833 8.7 mg/kg D.W. 1.3 5.5 8.7 mg/kg D.W. 1.3 5.5 06/10/18 DM0610/18009852 8.8 mg/kg D.W. 06/11/18 DM0611/18009865 9.5 mg/kg D.W. 06/12/18 DM0612/18010098 10 mg/kg D.W. 06/13/18 DM0613/18010127 9.6 mg/kg D.W. 06/14/18 DM0614/18010437 10 mg/kg D.W. 06/15/18 DM0615118010452 10 mg/kg D.W. 06/16/18 DM0616/18010463 06/17/18 DM0617/18010482 06/18/18 DM0618/18010639 06/19/18 DM0619/18010666 06/20/18 DM0620/18010694 06/21/18 DM0621/18010713 06/22/18 DM0622118010939 06/23/18 06/24/18 DM0623/18010950 DM0624118011087 06/25/18 DM0625/18011182 06/26/18 DM0626/18011209 06/27/18 DM0627118011597 06/28/18 DM0628118011616 06/29/18 DM0629/18011631 06/30/18 DM0630/18011642 07/01/18 DM0701/18011728 07/02/18 DM0702/18011741 07/03/18 DM0703/18011881 07/04/18 OM0704/18011909 07/05/18 07/06/18 i DM0705118012390 DM0706/18012405 07/07/18 DM0707/18012416 SYSIrptlMMoMonthly 1/10/13 U SW846: 6010C MMSD ` SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD 1.3 5.5 1.3 5.7 1.3 5.7 1.3 5.7 1.3 5.6 1.3 5.5 9 mg/kg D.W. 8.2 mg/kg D.W. 8.8 mg/kg D.W. 1.3 1.3 1.3 5.5 5.5 5.6 9.5 mg/kg D.W. 10 mg/kg D.W. 9.2 mg/kg D.W. 9.2 mg/kg D.W. 8 mg/kg D.W. 8.8 mg/kg D.W. 1.3 1.3 1.2 1.2 1.2 1.3 5.6 5.5 5.4 5.4 5.4 5.6 8.7 mg/kg D.W. 1.3 5.5 9.3 mg/kg D.W. 7.8 mg/kg D.W. 1.3 1.3 5.6 5.5 8.7 mg/kg D.W. 1.3 5.6 Q3. 8.9 mg/kg D.W. 1.3 5.6 r 7.7 mg/kg D.W. 1.3 5.6 8.1 mg/kg D.W. 1.3 5.6 7.9 mg/kg D.W. 1.3 5.6 8.4 mg/kg D.W. 1.3 5.6 7.4 mg/kg D.W. 1.3 5.5 7.5 mg/kg D.W. 1.3 5.5 9 mg/kg D.W. 1.3 5.6 8.5 mg/kg D.W. 1.3 5.6 SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C SW846:6010C SW846:6010C SW846:6010C MMSD MMSD MMSD MMSD SW846:6010C MMSD SW846:6010C SW846:6010C SW846:6010C MMSD MMSD MMSD SW846:6010C MMSD SW846:6010C MMSD J SW846:6010C MMSD T SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD Page 50 of 106 Printed- 1/18/19 09:4) 07/21/18 DM0721/18014073 8.7 mg/kg D.W. 1.3 Annual Milorganite Report MMSDJanuary 07/22/18 DM0722/18014483 9.3 mg/kg D.W. 1.3 5.5 1 to December 31, 2018 �'14►i i4f � ilt11IR f�IR'RtIi DM0723/18014496 DM0724118014523 DM0725/18014551 9.1 mg/kg D.W. 9 mg/kg D.W. 9.3 mg/kg D.W. 1.3 1.3 1.3 5.6 5.6 5.6 SW846: 6010C SW846: 6010C SW846: 6010C MOLYBDENUM ICP METHOD DM0726/18014570 8.7 mg/kg D.W. 1.3 5.6 SW846: 6010C Sample .. 07/08/18 DM0708/18012435 7.1 mg/kg D.W. .. 1.3 LOQ ►. Flap 5.5 Analytkal Method SW846: 6010C Lab MMSD 07/09/18 DM0709/18012448 7.6 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 07/10/18 DM0710/18012474 8.4 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 07/11/18 DM0711/18012820 7.9 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/12/18 DM0712/18012861 6.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/13/18 DM0713/18012876 6.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/14/18 DM0714/18013220 8.7 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/15/18 DM0715/18013239 8.3 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 07/16/18 DM0716118013252 8.7 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/17/18 DM0717/18013751 9.2 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/18/18 DM0718/18013961 8.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/19/18 DM0719/18014047 8.7 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 07/20/18 DM0720/18014062 9.1 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 07/21/18 DM0721/18014073 8.7 mg/kg D.W. 1.3 5.5 SW846: 6010C 07/22/18 DM0722/18014483 9.3 mg/kg D.W. 1.3 5.5 SW846: 6010C 07/23/18 07/24/18 07/25/18 DM0723/18014496 DM0724118014523 DM0725/18014551 9.1 mg/kg D.W. 9 mg/kg D.W. 9.3 mg/kg D.W. 1.3 1.3 1.3 5.6 5.6 5.6 SW846: 6010C SW846: 6010C SW846: 6010C 07/26/18 DM0726/18014570 8.7 mg/kg D.W. 1.3 5.6 SW846: 6010C 07/27/18 DM0727/18014585 8.4 mg/kg D.W. 1.3 5.5 SW846: 6010C 07/28/18 07/29/16 07/30/18 07/31/18 08/01/18 08/02/18 08/03/18 08/04/18 DM0728118014676 7.9 mg/kg D.W. 1.2 5.4 SW846: 6010C DM0729/18014910 8.2 mg/kg D.W. 1.2 5.4 SWB46: 6010C DM0730/18014925 8.2 mg/kg D.W. 1.3 5.6 SW846: 6010C DM0731/18014954 8.8 mg/kg D.W. 1.3 5.5 SW846: 6010C DM0801/18014969 8.2 mg/kg D.W. 1.3 5.5 B8. SW846: 6010C DMO802/18015140 8.6 mg/kg D.W. 1.3 5.5 SW846: 6010C DM0803118015155 8.4 mg/kg D.W. 1.3 5.5 SW846: 6010C DM0804118015252 9.1 mg/kg D.W. 1.2 5.4 SW846: 6010C 08/05/18 DM0805118015279 08/06/18 DMO806118015385 08/07/18 DM0807/18015414 08/08/18 DM0808118015473 08/09/18 08/10/18 DMO809/18015500 DMO810/18015899 08/11/18 DMO811/18015910 08/12/18 08/13/18 DMO812/18016203 DM0813/18016216 08/14/18 DMO814/18016254 9.6 mg/kg D.W. 1.3 5.5 10 mg/kg D.W. 1.2 5.4 9.8 mg/kg D.W. 1.3 5.5 10 mg/kg D.W. 1.2 5.4 10 mg/kg D.W. 9.8 mg/kg D.W. 1.2 1.2 5.4 5.4 9.6 mg/kg D.W. 1.2 5.4 9.3 mg/kg D.W. 9.7 mg/kg D.W. 1.2 1.2 5.4 5.4 8.1 mg/kg D.W. 1.2 5.4 Q3. MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 08/15/18 DM0815/18016281 9.5 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/16/18 DM0816118016300 8.9 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/17/18 DM0817/18016365 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/18/18 DM0818/18016505 9.7 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/19/18 DM0819/18016525 9.9 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/20/18 DM0820/18016539 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/21/18 DM0821/18016714 10 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 08/22/18 DM0822/18016742 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/23/18 DMOB23/18017352 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD SY51wimiloMonthly 1/10/13 ti Gage 51 of 106 Punted: 1/18/19 09: 4i e.MNSD MOLYBDENUM ICP METHOD Sample Date Sample ID Result LOD LGQ QA Flags Annual Milorganite Report January 1 to December 31, 2018 Analytical Method Lab 08/24/18 DM0824/18017367 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/25/18 DM0825/18017378 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/26/18 DM0826/18017397 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD �^ 08/27/18 DM0827/18017410 11 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/28/18 DM0828/18017434 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 08/29/18 DM0829/18017462 11 mg/kg D.W. 1.2 5.4 SW646: 6010C MMSD 08/30/18 DMO830/18017483 08/31/18 DMO831/18017498 09/01/18 DM0901/18017520 09/02/18 DM0902/18017752 09/03/18 DMO903/18018124 09/04/18 DM0904/18018149 09/05/18 DMO905/18018305 09/06/18 DMO906/18018326 09/07/18 DMO907/18018342 09/08/18 DM0908/18018353 10 mg/kg D.W. 10 mg/kg D.W. 1.3 1.3y 5.5 5.5 SW846: 6010C SW846: 6010C 10 mg/kg D.W. 1.2 5.4 SW846: 6010C 9.8 mg/kg D.W. 1.2 5.4 l SW846: 6010C 9.9 mg/kg D.W. 1.2 5.4 SW646: 6010C 10 mg/kg D.W. 1.3 5.5 SW846: 6010C 10 mg/kg D.W. 1.3 5.5 SW846: 6010C 9.9 mg/kg D.W. 1.3 5.5 SW846: 6010C 10 mg/kg D.W. 1.3 5.5 SW846: 6010C 10 mg/kg D.W. 1.2 5.4 SW846: 6010C 09/09/18 DM0909118018724 9.7 mg/kg D.W. 1.2 5.4 09/10/18 DMO910/18018799 9.6 mg/kg D.W. 1.3 5.5 09/11/18 DM0911/18018825 9.2 mg/kg D.W. 1.3 5.5 09/12/18 DMO912118018854 9.2 mg/kg D.W. 1.3 5.5 09/13/18 DMO913118018875 9.2 mg/kg D.W. 1.3 5.6 09/14/18 DM0914/18018891 6.5 mg/kg D.W. 1.3 5.6 09/15/18 DM0915/18019159 9.4 mg/kg D.W. 1.3 5.6 09/16/18 DM0916/18019178 8.8 mg/kg D.W. 1.3 5.5 09/17/18 DM0917/18019191 8.8 mg/kg D.W. 1.2 5.4 09/18/18 DM0918/18019447 9.2 mg/kg D.W. 1.3 5.6 09/21/18 DMO921/18019515 9.4 mg/kg D.W. 1.2 5.4 09/22/18 DMO922/18019574 9.9 mg/kg D.W. 1.2 5.4 09/23/18 DMO923/18019665 10 mg/kg D.W. 1.2 5.3 09/24/18 DMO924/18020088 9.8 mg/kg D.W. 1.2 5.4 09/25/18 DM0925118020314 9.3 mg/kg D.W. 1.2 5.4 09/26/18 09/27/18 09/28/18 09/29/18 DM0926118020343 8.7 mg/kg D.W. 1.3 5.5 DM0927/18020364 Y 8.8 mg/kg D.W. 1.3 5.5 DM0928/18020380 8.9 mg/kg D.W. 1.3 5.7 DMO929118020391 9.4 mg/kg D.W. 1.3 5.5 N,� M SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 09/30/18 DMO930/18020411 8.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/01/18 DM1001/18021136 8.9 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 10/02/18 DM1002/18021162 y 8.7 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/03/18 DM1003/18021190 8.6 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/04/18 DM1004/18021541 8.9 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 10/05/18 DM1005/18021557 10/06/18 DM1006/18021568 10/07/18 DM1007/18021588 10/08/18 DM1008/18021602 10/09/18 DM1009/18021627 10/10/18 DM1010/18021656 10/11/18 DM1011/18021975 SY51wiMiloMonthly 1/10/13 or 10 mg/kg D.W. 9.2 mg/kg D.W. 9.3 mg/kg D.W. 1.3 1.3 1.2 5.5 5.6 5.4 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 9.2 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 8.4 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 9.2 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 9.3 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD Page 572 of 106 Printed: 1/18/19 09:4; 10/23/18 DM1023/18022614 8.8 mg/kg D.W. 1.3 Annual Milorganite Report NSDJanuary DM1024118022643 10 mg/kg D.W. 1.3 5.5 1 to December 31, 2018 W4100,10MMI 9.3 mg/kg D.W. 1.3 5.5 10/26/18 DM1026/18022767 MOLYBDENUM ICP METHOD I I I I I F I I I I 1 11 1 1! 10/27/18 DM1027/18022778 10/12/18 - AI DM1012/18021991 9.7 mg/kg D.W. ! 1.2 ! ► • 5.4 1 SW846: 6010C MMSD 10/13/18 DM1013118022006 8.4 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/14/18 DM1014/18022026 8.1 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/15/18 DM1015/18022040 8.6 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/16/18 DM1016/18022065 9.1 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/17/18 DM1017/18022094 9.4 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/18/18 DM1018/18022133 8.8 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 10/19/18 DM1019/18022269 9.2 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 10/20/18 DM1020/18022280 8.9 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 10/21/18 DM1021/18022435 9 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 10/22/18 DM1022118022449 9.6 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 10/23/18 DM1023/18022614 8.8 mg/kg D.W. 1.3 5.5 10/24/18 DM1024118022643 10 mg/kg D.W. 1.3 5.5 10/25/18 DMID25118022708 9.3 mg/kg D.W. 1.3 5.5 10/26/18 DM1026/18022767 9.9 mg/kg D.W. 1.3 5.5 10/27/18 DM1027/18022778 9.4 mg/kg D.W. 1.2 5.4 11/07/18 DM 1107/18023991 11/08/18 DM1108/18024012 11/09/18 DM1109118024028 11/10/18 DM1110/18024523 11/11/18 DM1111/18024619 11/12/18 DM1112/18024633 11/13/16 DM1113118025014 11/14/18 DM1114118025043 11/15/16 DM1115/18025064 13 mg/kg D.W. 1.2 5.4 12 mg/kg D.W. 1.2 5.4 12 mg/kg D.W. 1.2 5.4 10 mg/kg D.W. 1.2 5.4 10 mg/kg D.W. 1.2 5.4 9.9 mg/kg D.W. 1.3 5.5 10 mg/kg D.W. 1.3 5.5 10 mg/kg D.W. 1.3 5.6 11 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 4 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 11/16/18 11/17/18 DM1116/18025080 DMI 117/18025093 10 mg/kg D.W. 10 mg/kg D.W. 1.3 1.3 5.7 5.5 SW846: 6010C SW846: 6010C MMSD MMSD 11/18/18 DM 1118/18025113 9.6 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 11/19/18 DM1119/18025127 10 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 11/20/18 DM 1120/18025356 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 11/21/18 DM1121/18025385 10 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 11/22/18 DM 1122/18025406 10 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 11/23/18 11/24/18 DM1123/18025422 DMI 124/18025750 10 mg/kg D.W. 10 mg/kg D.W. 1.3 1.3 5.6 5.7 SW846: 6010C SW846: 6010C MMSD MMSD 11/25/18 DM 1125/18025769 10 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD 11/26/18 DM 1126/18025828 11 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 11/27/18 DM1127/18025860 11 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 11/28/18 DM1128/18025888 10 mg/kg D.W. 1.2 5.4 SW846: 6010C MMSD 11/29/18 DM1129/18025956 10 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 11/30/18 DM1130/18025971 9.7 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/01/18 DM1201/18026182 10 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/02/18 DM1202/18026201 9.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 12/03/18 DM1203/18026214 9.8 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD 12/04/18 DM1204/18026391 9.6 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/05/18 DM1205/18026578 9.9 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/06/18 DM1206/18026621 9.2 mg/kg D.W. 1.3 5.8 SW846: 6010C MMSD 12/07/18 DM1207/18026797 9.6 mg/kg D.W. 1.3 5.7 SW846: 6010C MMSD SYSIWIM&Monthly 1/10/13 tj Page 53 of Job Printed: 1/18/19 09:4; e. MMSD WTM lot A chit I Annual Milorganite Report January 1 to December 31, 2018 MOLYBDENUM ICP METHOD 10 mg/kg D.W. 1.3 5.5 �. 12/08/18 DM1208/18026808 �. 9.2 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/09/18 DM1209/18026827 9.2 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD 12/10/18 DM1210/18026840 9 mg/kg D.W. 1.3 5.8 SW846: 6010C MMSD 12/11/18 12/12/18 12/13/18 12/14/18 12/15/18 12/16/18 12/17/18 12/18/18 12/19/18 12/22/18 12/23/18 12/24/18 12/25/18 12/26/18 12/27/18 12/28/18 12/29/18 12/30/18 12/31/18 DM1211/18027102 10 mg/kg D.W. 1.3 5.5 DM1212/18027130 10 mg/kg D.W. 1.2 5.4 DM1213/18027253 DM1214/18027306 9.5 mg/kg D.W. 10 mg/kg D.W. 1.3 5.6 1.3 5.5 DM1215/18027317 9.1 mg/kg D.W. 1.3 5.5 DM1216/18027525 ^J 9.2 mg/kg D.W. 1.3 5.6 DM1217/18027540 9.5 mg/kg D.W. 1.3 5.7 DM1218/18027643 10 mg/kg D.W. 1.3 5.8 DM1219/18027676 9.9 mg/kg D.W. 1.3 5.6 DM1220/18027805 10 mg/kg D.W. 1.3 5.5 DM1221/18027821 13 mg/kg D.W. 1.3 5.6 DM1222/18027832 10 mg/kg D.W. 1.3 5.6 DM1223/18027852 10 mg/kg D.W. 1.3 5.7 DM1224/18027883 10 mg/kg D.W. 1.3 5.7 DM1225/18027952 10 mg/kg D.W. 1.3 5.7 DM1226/18027969 10 mg/kg D.W. 1.3 5.7 DM1227/18027990 9.8 mg/kg D.W. 1.3 5.7 DM1228/18028005 10 mg/kg D.W. 1.3 5.8 DM1229/18028070 11 mg/kg D.W. 1.3 5.6 DM1230/18028089 11 mg/kg D.W. 1.3 5.5 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD DM1231/18028102 10 mg/kg D.W. 1.3 5.6 SW846: 6010C MMSD Avg Result: 9.5 mg/kg D.W. Min LOD: 0.83 mg/kg D.W. Max Result: 13 mg/kg D.W. Page 54 of 106 5Y5/rp[IMVoMo1?th1y 1110/13 of Printed: 1118/19 09:4) 01/05/18 DMO105/18000155 01/06/18 Annual Milorganite Report MMSDJanuary DMO107/18000189 01/11/18 DMD 111/18000347 1 to December 31, 2018 MITIM M 1 CIl1 I FR'"wk DM0115/18000432 22 mg/kg D.W. 1 3.2 02/04/18 NICKEL ICP METHOD Sample Date Sample ID Result 28 mg/kg D.W. 1 01/01/18 DMO101118000013 ,D 22 mg/kg D.W. 1 LOQ .• Higs 3.2 Anafytkal method Lab SW846: 6010C MMSD 01/02/18 DMO102118000047 22 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 01/03/18 DMO103/18000061 21 mg/kg D.W. 1.1 3.3 SW846: 6010C MMSD 01/04/18 DMO104/18000098 21 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 01/05/18 DMO105/18000155 01/06/18 DMO106/18000168 01/07/18 DMO107/18000189 01/08/18 DMO108/18000203 01/09/18 DMO109/18000232 01/10/18 DM0110/18000326 01/11/18 DMD 111/18000347 20 mg/kg D.W. 1.1 3.3 22 mg/kg D.W. 1.1 3.2 21 mg/kg D.W. 1.1 3.3 22 mg/kg D.W. 1 3.2 22 mg/kg D.W. 1.1 3.3 21 mg/kg D.W. 1 3.2 22 mg/kg D.W. 1 3.2 01/12/18 DM0112/18000363 21 mg/kg D.W. 1.1 3.2 01/13/18 DM0113/18000397 23 mg/kg D.W. 1 3.2 01/14/18 DM0114/18000418 23 mg/kg D.W. 1 3.2 01/15/18 DM0115/18000432 22 mg/kg D.W. 1 3.2 01/16/18 DM0116/18000461 01/17/18 DM0117/18000652 01/18/18 DM0118/18000673 01/19/18 DM0119/18000689 01/20/18 DMO120/18000702 01/21/18 DMO121/18000800 01/22/16 DMO122/18000814 01/23/18 DMO123/18000843 01/24/18 DMO124/18000875 01/25/18 DMO125/18000896 01/26/18 DMO126/18000912 01/27/18 ^ DMO127/18000925 01/28/18 DMO128/18000946 01/29/18 DMO129/18001200 01/30/18 DM0130/18001229 01/31/18 DMO131/18001259 02/01/18 DM0201/18001280 02/02/18 DM0202/18001421 02/03/18 DM0203/18001434 02/04/18 DM0204/18001455 25 mg/kg D.W. 1 3.2 25 mg/kg D.W. 1.1 3.2 26 mg/kg D.W. 1 3.2 28 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1 3.2 25 mg/kg D.W. 24 mg/kg D.W. 24 mg/kg D.W. 1 1.1 1.1 3.2 3.3 3.3 28 mg/kg D.W. 1 3.2 34 mg/kg D.W. 1 3.1 28 mg/kg D.W. 1 3.2 28 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1 3.1 24 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1 3.2 25 mg/kg D.W. 1 3.2 25 mg/kg D.W. 1 3.2 ^� 26 mg/kg D.W. 1 3.2 28 mg/kg D.W. 1 3.2 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW946:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 02/05/18 02/06/18 02/07/18 DM0205/18001469 DM0206/18001506 DM0207/18001599 24 mg/kg D.W. 23 mg/kg D.W. 24 mg/kg D.W. 1 1 1 3.2 3.2 3.2 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 02/08/18 02/09/18 DM0208/18001620 DM0209/18001738 26 mg/kg D.W. 26 mg/kg D.W. t 1 3.2 3.2 SW846: 6010C SW846: 6010C MMSD MMSD 02/10/18 DM0210/18001751 25 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 02/11/18 DM0211118001772 26 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 02/12/18 DM0212118001786 26 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 02/13/18 DM0213/18001815 27 mg/kg D.W. 1.1 3.3 SW846: 6010C MMSD 02/14/18 DM0214/18001860 28 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 02/15/18 DM0215118001881 26 mg/kg D.W. 1 3.2 SW846: 6010C MMSD 02/16/18 DM0216/18001897 SYSIAPUMi/OMonthly 1110113 tj 26 mg/kg D.W. 1 3.2 SW846: 6010C MMSD Page 55 of 106 Printed: 1118119 09:4; Annual Milorganite Report MMSD January 1 to December 31, 2018 MPM Pot d Et1U�if OM1 NICKEL ICP METHOD bite Sampie ID Result Lot) LGQ . a 02/17/18 DM0217/18001944 28 mg/kg D.W. 1 3.2 SW846: 6010C 02/18/18 DM0218/18001965 30 mg/kg D.W. 1 3.2 SW846: 6010C 02/19/18 DM0219/18001979 30 mg/kg D.W. 1.1 3.2 SW846: 6010C 02/20/18 DM0220/18002047 26 mg/kg D.W. 1 3.2 SW846: 6010C 02/21/18 DM0221/18002077 25 mg/kg D.W. 1 3.2 SW846: 6010C 02/22/18 DM0222/18002097 24 mg/kg D.W. 1 3.2 SW846: 6010C 02/23/18 DM0223/18002415 24 mg/kg D.W. 1 3.1 SW846: 6010C 02/24/18 DM0224/18002427 23 mg/kg D.W. 1 3.2 SW846: 6010C 02/25/18 DM0225/18002447 24 mg/kg D.W. 1 3.2 4 SW846: 6010C 02/26/18 DM0226118002461� 24 mg/kg D.W. 1 3.2 SW846: 6010C 02/27/18 DM0227/18002537 23 mg/kg D.W. 1 3.2 SW846: 6010C 02/28/18 DM0228/18002609 24 mg/kg D.W. 1 3.2 SW846: 6010C 03/01/18 DM0301/18002628 34 mg/kg D.W. 1.1 3.2 SW846: 6010C 03/02/18 DM0302/18002711 25 mg/kg D.W. 1 3.2 SW846: 6010C 03/03/18 DM0303/18002722 23 mg/kg D.W. 1.1 3.2 SW846: 6010C 03/04/18 03/05/18 03/06/18 03/07/18 03/08/18 03/09/18 03/10/18 03/11/18 03/12/18 03/13/18 03/14/18 03/15/18 03/16/18 03/17/18 03/18/18 03/19/18 03/20/18 03/21/18 03/22/18 03/23/18 03/24/18 03/25/18 03/26/18 03/27/18 03/28/18 03/29/18 03/30/18 03/31/18 04/01/18 04/02/18 04/03/18 DM0304/18002741 DM0305/18002805 DM0306/18002862 DM0307/18002927 DM0308/18003015 DM0309/18003030 1'1AAhJAIIIA OlII]!lI A DM0312/18003335 DM0313/18003681 DM0314/18003710 DM0315/18003729 DM 031 6/ 1 8003744 DM0317118003755 DM0318/18003780 DM0319/18003911 DM0320/18003938 DM0321/18003967 DM0322/18004111 DM0323/18004126 DM0324/18004137 DM0325/18004156 DM0326/18004320 DM0327/18004347 DM0328/18004376 DM0329/18004395 DM0330/18004410 DM 0331 / 18004752 DM0401 / 18004771 DM0402/18004784 DM0403/18004943 26 mg/kg D.W. 1.1 3.2 26 mg/kg D.W. 1.1 3.2 24 mg/kg D.W. 1.1 3.2 24 mg/kg D.W. 1.1 3.3 23 mg/kg D.W. 1 3.2 24 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1.1 3.3 26 mg/kg D.W. 1.1 3.3 26 mg/kg D.W. 1.1 3.3 27 mg/kg D.W. 1.1 3.3 27 mg/kg D.W. 1.1 3.3 27 mg/kg D.W. 1 3.2 26 mg/kg D.W. 1.1 3.3 27 mg/kg D.W. 1.1 3.3 28 mg/kg D.W. 1.1 3.3 28 mg/kg D.W. 1.1 3.4 26 mg/kg D.W. 1.1 3.3 27 mg/kg D.W. 1.1 3.3 26 mg/kg D.W. 1 3.2 27 mg/kg D.W. 1 3.2 25 mg/kg D.W. 25 mg/kg D.W. 25 mg/kg D.W. 27 mg/kg D.W. 1.1 1.1 1.1 1.1 25 mg/kg D.W. 1.1 24 mg/kg D.W. 1 23 mg/kg D.W. 1.1 24 mg/kg D.W. 1 26 mg/kg D.W. 1.1 24 mg/kg D.W. 1.1 24 mg/kg D.W. 4.7 3.3 3.3 T 3.3 3.3 3.3 3.2 3.4 3.2 3.3 3.2 - 14 04/04/18 DM0404118004972 22 mg/kg D.W. 4.5 14 SYS/rptI iloMonthly 1/10/13 tj SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW646: 6010C SW646: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD Page 56 of 106 Printed: 1/18/19 09:97 04/20/18 04/21/18 04/22/18 04/23/18 04/24/18 04/25/18 04/26/18 04/27/18 04/28/18 04/29/18 04/30/18 05/01/18 05/02/18 05/03/18 05/04/18 05/05/18 05/06/18 05/07/18 05/08/18 DM0420/18006009 24 mg/kg D.W. 4.4 14 DM0421/18006020 Annual Milorganite Report e-MNsf) DM0422/18006039 27 mg/kg D.W. 4.5 14 DM0423/18006157 January 1 to December 31, 2018 4.4 14 DM0424/18006185 26 mg/kg D.W. 4.6 14 MMSD SW846: 6010C MMSD NICKEL ICP METHOD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C 'Result SW846: 6010C LOD LOQ r• Flags Analytical ME%thad Lab 04/05/18 DM0405/18005037 28 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/06/18 DM0406/18005052 29 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/07/18 DM0407118005063 26 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 04/08/18 DM0408/18005082 26 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 04/09/18 DM0409/18005095 26 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/10/18 DM0410/18005164 26 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/11/18 DM0411118005193 27 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/12/18 DM0412/18005446 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/13/18 DM0413/18005463 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/14/18 DM0414118005474 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 04/15/18 DM0415/18005605 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/16/18 DM0416/18005618 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 04/17/18 DM0417/18005709 24 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 04/18/18 DM0418/18005738 23 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 04/19/18 DM0419/18005757 23 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 04/20/18 04/21/18 04/22/18 04/23/18 04/24/18 04/25/18 04/26/18 04/27/18 04/28/18 04/29/18 04/30/18 05/01/18 05/02/18 05/03/18 05/04/18 05/05/18 05/06/18 05/07/18 05/08/18 DM0420/18006009 24 mg/kg D.W. 4.4 14 DM0421/18006020 25 mg/kg D.W. 4.5 14 DM0422/18006039 27 mg/kg D.W. 4.5 14 DM0423/18006157 25 mg/kg D.W. 4.4 14 DM0424/18006185 26 mg/kg D.W. 4.6 14 DM0425/18006214 DM0426/ 18006233 DM0427/18006441 DM0428/18006452 DM0429118006471 DM0430/18006484 DM0501/18006571 DM0502/18006600 DMO503/18006854 DMO504/18007005 DMO505/18007016 DM0506/18007035 DM0507118007257 DMO508/18007284 30 mg/kg D.W 25 mg/kg D.W 25 mg/kg D.W 27 mg/kg D.W 26 mg/kg D.W 26 mg/kg D.W 25 mg/kg D.W 25 mg/kg D.W 25 mg/kg D.W 25 mg/kg D.W 29 mg/kg D.W 30 mg/kg D.W 29 mg/kg D.W 27 mg/kg D.W 4.7 15 4.6 4.4 4.6 4.6 4.6 4.6 4.6 4.3 4.4 4.5 4.6 4.4 4.5 14 14 14 14 14 14 14 13 14 14 14 14 14 SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 05/09/18 DMO509/18007313 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/10/18 DMO510/18007340 25 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/11/18 DMO511/18007418 28 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/12/18 DM0512/18007429 28 mg/kg D.W. 4.5 14 SW846: 6010C _ MMSD 05/13/18 OM0513/18007476 29 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/14/18 DMO514/18007591 28 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/15/18 DMO515118007976 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 05/16/18 DM0516/18008005 31 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/17/18 DM0517/18008103 30 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/18/18 DMO518/18008118 32 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/19/18 DMO519118008129 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/20/18 DM0520/18008196 05/21/18 DM0521/18008209 32 mg/kg D.W. 4.6 14 32 mg/kg D.W. 4.6 14 SW846: 6010C MMSD SW846: 6010C MMSD Page 57 of 10b SYS/rptlMiloMonthly 1/10/13 tj Printed: 1/18/19 09:4; NSD wMWAalQUIPOW NICKEL ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 - -r• DM0702/18011741 33 mg/kg D.W. 4.5 a•a r; -I MMSD 05/22/18 DM0522/18008236 33 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/23/18 DM0523/18008304 30 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/24/18 DM0524/18008658 30 mg/kg D.W. �4.4 14 SW846: 6010C MMSD 05/25/18 DMO525/18008673 30 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 05/26/18 DM0526118008684 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 05/27/18 DMO527/18008703 33 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/28/18 DMO528/18008716 34 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/29/18 DM0529/18008888 34 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 05/30/18 DM0530/18008917 32 mg/kg D.W. 4.5 14 B8. SW846: 6010C MMSD 05/31/16 DM0531/18008936 32 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/01/18 DM0601/18009150 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/02/18 DM0602/18009161 31 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/03/18 DM0603/18009335 31 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/04/18 DM0604/18009348 32 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/05/18 DM0605118009375 32 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/06/18 DM0606/18009404 32 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/07/18 DM0607/18009423 32 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/08/18 DM0608/18009822 31 mg/kg D.W. 4.4 14 SW646: 6010C MMSD 06/09/18 DM0609/18009833 35 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/10/18 DM0610/18009852 34 mg/kg D.W. 4.4 14 SW846: 60100 MMSD 06/11/18 DM0611/18009865 52 mg/kg D.W. 4.6 14 Q3. SW846: 60100 MMSD 06/12/18 DM0612/18010098 37 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/13/18 DM0613/18010127 38 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/14/18 DM0614/18010437 38 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/15/18 DMO615/18010452 36 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/16/18 DM0616/18010463 35 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/17/18 DM0617/18010482 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/18/18 DM0618118010639 36 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/19/18 DM0619/18010666 37 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 06/20/18 DM0620118010694 39 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/21/18 DM0621/18010713 37 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/22/18 DMO622/18010939 38 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/23/18 DM0623/18010950 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 06/24/18 DM0624/18011087 36 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/25/18 DMO625/18011182 36 mg/kg D.W.4.5 14 SW846: 6010C MMSD 06/26/18 DMO626118011209 30 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/27/18 DM0627/18011597 29 mg/kg D.W. 4.5 14 SW846: 6010C MMSD Y 06/28/18 DM0628/18011616 30 mg/kg D.W. 4.5 14 Q3. SW846: 6010C MMSD 06/29/18 DM0629/18011631 36 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 06/30/18 DM0630118011642 30 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 07/01/18 DM0701/18011728 31 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/02/18 DM0702/18011741 33 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/03/18 DM0703/18011881 32 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/04/18 DM0704/18011909 32 mg/kg D.W. 4.4 14 B9. SW846: 6010C MMSD 07/05/18 DM0705/18012390 33 mg/kg D.W. 4.4 14 B9. SW846: 6010C MMSD 07/06/18 DM0706/18012405 30 mg/kg D.W. 4.5 14 B9. SW846: 6010C MMSD 07/07/18 DM0707/18012416 31 mg/kg D.W. 4.6 14 SW846: 6010C MMSD SYS/rptlMiloMonthly 1/10/13 q Page 58 of 106 Printed. 1118/19 09.47 Page 59 of 105 SY5/rptlMiloMonth/y 1/10/19 tj Printed. 1/18/19 09: 4i Annual Milorganite Report e.kMSD January 1 to December 31, 2018 +wrlr�ts sae s tllM� r NICKEL �ICP METHOD 07/08/18 'ReskjR DM0708/18012435 29 mg/kg D.W. LOD 4.5 L0Q QA Flags 14 Analytkal Method SW846: 6010C Lob MMSD 07/09/18 DM0709/18012448 2B mg/kg D.W. 4.6 14 SW846: 6010C MMSD 07/10/18 DM0710/18012474 30 mg/kg D.W. 4.5 14 B9. SW846: 6010C MMSD 07/11/18 DM0711/18012820 30 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/12/18 DM0712/18012861 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/13/18 DM0713/18012876 34 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/14/18 DM0714/18013220 35 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/15/18 DM0715/18013239 36 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/16/18 DM0716118013252 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/17/18 DM0717/18013751 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/18/18 DM0718/18013961 34 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/19/18 DM0719118014047 34 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/20/18 DM0720118014062 33 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/21/18 DM0721/18014073 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/22/18 DM0722/18014483 34 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/23/18 DM0723/18014496 34 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/24/18 DM0724/18014523 35 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/25/18 DM0725/18014551 36 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 07/26/18 DM0726/18014570 34 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/27/18 DM0727/18014585 43 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/28/18 DM0728/18014676 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/29/18 DM0729118014910 32 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 07/30/18 DM0730/18014925 31 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 07/31/18 DM0731/18014954 34 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 08/01/18 DM0801/18014969 32 mg/kg D.W. 4.4 14 B8. SW846: 6010C MMSD 08/02/18 DM0802118015140 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/03/18 DM0803/18015155 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/04/18 DMO804/18015252 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/05/18 DMO805/18015279 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/06/18 DMO806/18015385 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/07/18 DMO807/18015414 35 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/08/18 DMO808118015473 34 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/09/18 DMO809/18015500 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/10/18 DMOB10/18015899 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/11/18 DMO811/18015910 30 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/12/18 DMO812/18016203 30 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/13/18 DMO813/18016216 31 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/14/18 DMOB14/18016254 28 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/15/18 DMOB15/18016281 32 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/16/18 DMO816/18016300 27 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/17/18 DMOB17/18016365 28 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/18/18 DM0818/18016505 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/19/18 DM0819/18016525 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/20/18 DM0820/18016539 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/21/18 DMO821/18016714 32 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/22/18 DM0822118016742 33 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 08/23/18 DM0823/18017352 34 mg/kg D.W. 4.3 13 SW846: 6010C MMSD Page 59 of 105 SY5/rptlMiloMonth/y 1/10/19 tj Printed. 1/18/19 09: 4i L NICKEL ICP METHOD 08/24/18 DMO824/18017367 08/25/18 DM0825/18017378 08/26/18 08/27/18 08/28/18 08/29/18 08/30/18 08/31/18 Annual Milorganite Report January 1 to December 31, 2018 33 mg/kg D.W. 4.4 13 SW846: 6010C MMSD 34 mg/kg D.W. 4.4 14 SW646: 6010C MMSD DM0826/18017397 35 mg/kg D.W. 4.4 13 SW846: 6010C MMSD DMO827/18017410 35 mg/kg D.W. 4.4 14 SW846: 6010C MMSD DMO828/18017434 35 mg/kg D.W. 4.4 14 SW846: 6010C MMSD DMO829/18017462 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD DMO830/18017483 36 mg/kg D.W. 4.4 14 SW846: 6010C MMSD DMO831/18017498 36 mg/kg D.W. 4.4 14 09/01/18 DM0901/18017520 36 mg/kg D.W. 4.4 14 09/02/18 DM0902/18017752 35 mg/kg D.W. 4.4 14 09/03/18 DMO903/18018124 35 mg/kg D.W. 4.4 14 09/04/18 DMO904/18018149 36 mg/kg D.W. 4.5 14 09/05/18 DMO905/18018305 39 mg/kg D.W. 4.5 14 09/06/18 DMO906/18018326 37 mg/kg D.W. 4.5 14 09/07/18 DMO907/18018342 38 mg/kg D.W. 4.4 14 09/08/18 DM0908/18018353 38 mg/kg D.W. 4.4 14 09/09/18 DMO909/18018724 36 mg/kg D.W. 4.4 14 09/10/18 DMO910/18018799 35 mg/kg D.W. 4.4 14 09/11/18 DMO911/18018825 34 mg/kg D.W. 4.5 14 09/12/18 DM0912/18018854 35 mg/kg D.W. 4.4 14 09/13/18 DMO913/18018875 35 mg/kg D.W. 4.5 14 09/14/18 DMO914/18018891 34 mg/kg D.W. 4.5 14 09/15/18 DMO915/18019159 36 mg/kg D.W. 4.5 14 09/16/18 DMO916/18019178 35 mg/kg D.W. 4.5 14 09/17/18 DMO917/18019191 33 mg/kg D.W. 4.4 14 09/18/18 OM0918/18019447 32 mg/kg D.W. 4.5 14 09/21/18 DMO921/18019515 33 mg/kg D.W. 4.3 13 09/22/18 DMO922/18019574 33 mg/kg D.W. 4.4 14 09/23/18 DMO923/18019665 33 mg/kg D.W. 4.3 13 09/24/18 DMO924/18020088 32 mg/kg D.W. 4.3 13 09/25/18 DM0925/18020314 31 mg/kg D.W. 4.4 14 09/26/18 DM0926/18020343 30 mg/kg D.W. 4.5 14 09/27/18 DM0927/18020364 30 mg/kg D.W. 4.4 14 09/30/18 10/01/18 10/02/18 10/03/18 10/04/18 10/05/18 DM0928/18020380 31 mg/kg D.W. 4.6 14 DM0929/18020391 29 mg/kg D.W. 4.4 14 DM0930/18020411 28 mg/kg D.W. 4.4 14 DM1001/18021136 28 mg/kg D.W. 4.4 14 DM1002118021162 28 mg/kg D.W. DM1003/18021190 27 mg/kg D.W. DM1004/18021541 34 mg/kg D.W. DM1005/18021557 34 mg/kg D.W. 4.5 14 4.5 14 4.4 14 4.4 14 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Q3. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 10/06/18 DM1006/18021568 31 mg/kg D.W. 4.5 14 SWB46: 6010C MMSD 10/07/18 _ DM1007/18021588 30 mg/kg D.W. 4.3 13 SW846: 6010C MMSD 10/08/18 DM1008/18021602 30 mg/kg D.W. 4.3 13 SW846: 6010C MMSD 10/09/18 DM1009/18021627 28 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 10/10/18 DM1010/18021656 29 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 10/11/18 DM1011/18021975 28 mg/kg D.W. 4.4 14 SW846: 6010C MMSD SYS/rptlMiloMonthly 1/10/13 t/ Page 60 of 106 Printed: 1118119 09:4; 10/18/18 DM1018118022133 10/19/18 DM1019/18022269 10/20/18 DM1020118022280 10/21/18 10/22/18 DM1021/18022435 DM1022/18022449 Annual Milorganite Report e.k "sP 10/26/18 DM1026118022767 10/27/18 January 1 to December 31, 2018 irlq: ;,4 1 8111 DM 1112/18024633 31 mg/kg D.W. 30 mg/kg D.W. 31 mg/kg D.W. 28 mg/kg D.W. 4.5 4.4 4.5 4.5 14 14 14 14 NICKEL ICP METHOD Date Sampfe ID Result .D LOQ QA Flags AnaNtw 10/12/18 DM1012118021991 27 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 10/13/18 DM1013/18022006 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 10/14/18 DM1014/18022026 25 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 10/15/18 DM1015/18022040 26 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 10/16/18 DM1016118022065 26 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 10/17/18 DM1017/18022094 26 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 10/18/18 DM1018118022133 10/19/18 DM1019/18022269 10/20/18 DM1020118022280 10/21/18 10/22/18 DM1021/18022435 DM1022/18022449 10/23/18 10/24/18 10/25/18 DM1023/18022614 DM1024/18022643 DM1025118022708 10/26/18 DM1026118022767 10/27/18 DM1027/18022778 11/07/18 DM1107/18023991 11/08/18 DM1108/18024012 11/09/18 13101109/18024028 11/10/18 DM1110/18024523 11/11/18 DM1111/18024619 11/12/18 DM 1112/18024633 11/13/18 DM1113118025014 11/14/18 DM1114118025043 11/15/18 DM 1115/18025064 11/16/18 DM1116/18025080 11/17/18 DM 1117/18025093 11/18/18 DM 1118/18025113 11/19/18 DM 1119/18025127 26 mg/kg D.W. 4.4 14 27 mg/kg D.W. 4.5 14 29 mg/kg D.W. 4.4 14 31 mg/kg D.W. 4.4 14 29 mg/kg D.W. 4.4 14 29 mg/kg D.W. 4.4 14 30 mg/kg D.W. 4.5 14 26 mg/kg D.W. 4.4 14 25 mg/kg D.W. 4.4 14 26 mg/kg D.W. 4.4 13 33 mg/kg D.W. 4.3 13 27 mg/kg D.W. 4.4 14 31 mg/kg D.W. 4.4 14 30 mg/kg D.W. 29 mg/kg D.W. 4.3 4.4 13 13 31 mg/kg D.W. 30 mg/kg D.W. 31 mg/kg D.W. 28 mg/kg D.W. 4.5 4.4 4.5 4.5 14 14 14 14 27 mg/kg D.W. 4.6 14 28 mg/kg D.W. 4.4 14 26 mg/kg D.W. 4.5 14 26 mg/kg D.W. 4.4 14 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 11/20/18 11/21/18 DM1120/18025356 DM1121/18025385 26 mg/kg D.W. 25 mg/kg D.W. 4.4 4.4 14 14 SW846: 6010C SW846: 6010C MMSD MMSD 11/22/18 11/23/18 11/24/18 DM1122118025406 DM1123118025422 DM1124/18025750 26 m9/kg D.W. 25 mg/kg D.W. 24 mg/kg D.W. 4.5 4.5 4.6 14 14 14 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 11/25/18 DM1125/18025769 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 11/26/18 DM1126/18025828 25 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 11/27/18 DM1127118025860 26 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 11/28/18 DM1128/18025888 24 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 11/29/18 DM1129118025956 26 mg/kg D.W. 4.4 14 SW846: 6010C MMSD 11/30/18 DM1130/18025971 23 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/01/18 DM1201/18026182 24 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/02/18 DM1202118026201 23 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/03/18 DM1203118026214 23 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/04/18 DM1204/18026391 23 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/05/18 DM1205/18026578 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/06/18 DM1206/18026621 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/07/18 DM1207/18026797 24 mg/kg D.W. 4.6 14 SW846: 6010C MMSD Page 61 of 106 SYS/rptI iloMondrly 1/10/13 tj Printed: 1/18/19 09: 4i 12/14/18 12/15/18 12/16/18 12/17/18 12/18/18 12/19/18 12/20/18 12/21/18 12/22/18 12/23/18 12/24/18 12/25/18 12/26/18 12/27/18 12/28/18 12/29/18 12/30/18 12/31/18 DM1214/18027306 27 mg/kg D.W. 4.4 14 Annual Milorganite Report NSD 4.5 14 DM1216/18027525 January 1 to December 31, 2018 POWMAWOMEW 14 DM1217118027540 26 mg/kg D.W. 4.6 NICKEL ICP METHOD Sample Date Sample TO Result LOD LOQ 14 12/08/18 DM1208118026808 26 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 12/09/18 DM1209118026827 26 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/10/18 DM1210/18026840 26 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 12/11/18 DM1211/18027102 26 mg/kg D.W. 4.4 14 B8. SW846: 6010C MMSD 12/12/18 DM1212/18027130 25 mg/kg D.W. 4.4 14 B8. SW846: 6010C MMSD 12/13/18 DM1213/18027253 25 mg/kg D.W. 4.5 14 SW846: 6010C MMSD 12/14/18 12/15/18 12/16/18 12/17/18 12/18/18 12/19/18 12/20/18 12/21/18 12/22/18 12/23/18 12/24/18 12/25/18 12/26/18 12/27/18 12/28/18 12/29/18 12/30/18 12/31/18 DM1214/18027306 27 mg/kg D.W. 4.4 14 DM1215/18027317 25 mg/kg D.W. 4.5 14 DM1216/18027525 26 mg/kg D.W. 4.6 14 DM1217118027540 26 mg/kg D.W. 4.6 14 DM1218118027643 26 mg/kg D.W. 4.7 14 DM1219/18027676 28 mg/kg D.W. 4.5 14 DM1220118027805 29 mg/kg D.W. 4.4 14 DM1221/18027821 31 mg/kg D.W. 4.5 14 DM1222/18027832 30 mg/kg D.W. 4.5 14 DM1223/18027852 32 mg/kg D.W. 4.6 14 DM1224/18027883 31 mg/kg D.W. 4.6 14 DM1225/18027952 30 mg/kg D.W. 4.6 14 DM1226/18027969 30 mg/kg D.W. 4.6 14 DM1227/18027990 28 mg/kg D.W. 4.6 14 DM1228/18028005 26 mg/kg D.W. 4.7 14 DM 1229/18028070 30m/k D WA 5 14 DM 1230/18028089 DM 1231 /18028102 Avg Result: 29 mg/kg D.W. NITRATE NITROGEN 01/13/18 WMCO2118000434 02/10/18 03/10/18 WMC06/18001788 WMC10/18003337 04/07/18 WMC14/18005097 05/12/18 WMC19/18007645 06/09/18 WMC23/18009867 07/07/18 WMC27118013254 08/11/18 WMC32/18016218 09/08/18 WMC36/18018801 10/13/18 WMC41/18022042 11/17/18 WMC46/18024635 12/08/18 WMC49/18026842 Avg Result: 0.32 azo g g 31 mg/kg D.W. 4.4 14 29 mg/kg D.W. 4.5 14 Min LOD: 1 mg/kg D.W. 1.3 % 0.5 Min LOD: 0.5 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C T SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD < 0.5 % 0.5 0.7% 0.5 0.54% 0.5 < 0.5 % 0.5 < 0.5 % 0.5 < 0.5 % 0.5 < 0.5 % 0.5 0.6% 0.5 < 0.5 % 0.5 < 0.5 % 0.5 0.7% 0.5 1.3 % 0.5 Min LOD: 0.5 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C T SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C f MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Max Result: 52 mg/kg D.W. AOAC (16) 930.01 ADAC (16) 930.01 AOAC (16) 930.01 MMSD MMSD MMSD AOAC (16) 930.01 MMSD AOAC (16) 930.01 MMSD AOAC (16) 930.01 T MMSD ADAC (16) 930.01 ADAC (16) 930.01 MMSD MMSD ADAC (16) 930.01 MMSD ADAC (16) 930.01 MMSD AOAC (16) 930.01 MMSD ADAC (16) 930.01 Max Result: 1.3 % MMSD Page 62 of 106 SYS/rptlMiloMonthly 1110113 tj Printed: 1118/19 09:4; e'kNSD Annual Milorganite Report January 1 to December 31, 2018 NITROGEN-Total(Manual) Sanspie 7D Result O. LOQ QA Flags Analytkal Method 01/13/18 WMCO2/18000434 6.8% 0.11 AOAC (16) 955.04 MMSD 02/10/18 WMC06/18001788 6.7% 0.11 AOAC (16) 955.04 MMSD 03/10/18 WMC10/18003337 04/07/18 WMC14/18005097 05/12/18 WMC19/18007645 06/09/18 WMC23/18009867 07/07/18 WMC27/18013254 6.7% 0.11 6.6% 0.11 6.3% 0.11 6.2% 0.11 5.9% 0.11 AOAC (16) 955.04 MMSD ADAC (16) 955.04 MMSD ADAC (16) 955.04 MMSD AOAC (16) 955.04 MMSD AOAC (16) 955.04 MMSD 08/11/18 WMC32/18016218 5.7% 0.11 AOAC (16) 955.04 MMSD 09/08/18 WMC36/18018801 5.4% 0.11 ADAC (16) 955.04 MMSD 10/13/18 WMC41/18022042 5.6% 0.11 AOAC (16) 955.04 MMSD 11/17/18 WMC46/18024635 6% 0.11 AOAC (16) 955.04 MMSD 12/08/18 WMC49/18026842 6.3% 0.11 AOAC (16) 955.04 MMSD Avg Result: 6.2 % Min LOD: 0.11 % Max Result, 6.8'/0 NITROGEN -Water Insoluble .... .. 01/13/18 WMCO2/18000434 5.4 % LOQ Flags 0.5 Analytkal Method ADAC (16) 945.01 Lab MMSD 02/10/18 WMC06/18001788 5.4% 0.5 ADAC (16) 945.01 MMSD 03/10/18 WMC10/18003337 04/07/18 05/12/18 WMC14/18005097 WMC19/18007645 06/09/18 WMC23/18009867 07/07/18 WMC27/18013254 08/11/18 WMC32118016218 09/08/18 WMC36/18018801 10/13/18 WMC41118022042 11/17/18 WMC46118024635 12/08/18 WMC49/18026842 Avg Result: 4.9 0/6 5.2 % 5.2 % 4.9% 0.5 0.5 0.5 4.8% 0.5 4.6% 0.5 4.4% 0.5 4.5% 0.5 4.7% 0.5 4.9% 0.5 4.5% 0.5 Min LOD. 0.5 0/6 AOAC (16) 945.01 MMSD AOAC (16) 945.01 AOAC (16) 945.01 MMSD MMSD AOAC (16) 945.01 MMSD ADAC (16) 945.01 MMSD AOAC (16) 945.01 MMSD AOAC (16) 945.01 AOAC (16) 945.01 MMSD MMSD AOAC (16) 945.01 MMSD AOAC (16) 945.01 MMSD Max Result: 5.4 Page 63 of 106 SY51WIM110month/y 1110/13 Of Printed: 1/18/19 09:4; MMSD pH -Solids Annual Milorganite Report January 1 to December 31, 2018 01/06/18 WMC01/18000205 5.64 Stnd. Units 0.1 SW846: 9045D MMSD 01/13/18 WMCO2/18000434 5.72 Stnd. Units 0.1 SW846: 9045D MMSD 01/20/18 WMC03/18000816 5.72 Stnd. Units 0.1 SW846: 9045D MMSD 01/27/18 WMC04/18001202 5.74 Stnd. Units 0.1 SW846: 9045D MMSD 02/03/18 WMC05/18001471 5.82 Stnd. Units 0.1 SW846: 9045D MMSD 02/10/18 WMC06/18001788 5.81 Stnd. Units 0.1 SW846: 9045D MMSD 02/17/18 WMC07/18001981 5.76 Stnd. Units 0.1 SW846: 9045D MMSD 02/24/18 WMC08118002463 5.78 Stnd. Units 0.1 SW846: 9045D MMSD 03/03/18 WMC09118002807 5.79 Stnd. Units 0.1 y SW846: 9045D MMSD 03/10/18 WMC10/18003337 5.85 Stnd. Units 0.1 SW846: 9045D MMSD 03/17/18 WMC11118003913 5.81 Stnd. Units 0.1 SW846: 9045D MMSD 03/24/18 WMC12/18004322 5.87 Stnd. Units 0.1 SW846: 9045D MMSD 03/31/18 WMC13118004786 5.91 Stnd. Units 0.1 SW846: 904SD MMSD 04/07/18 WMC14118005097 5.93 Stnd. Units 0.1 SW846: 9045D MMSD 04/14/18 WMC15/18006159 5.8 Stnd. Units 0.1 SW846: 9045D MMSD 04/21/18 WMC16118006160 5.81 Stnd. Units 0.1 SW846: 9045D MMSD 04/28/18 WMC17118006486 6.02 Stnd. Units 0.1 SW846: 9045D MMSD 05/05/18 WMC18118007259 5.99 Stnd. Units 0.1 SW846: 9045D MMSD 05/12/18 WMC19118007645 6.09 Stnd. Units 0.1 SW846: 9045D MMSD 05/19/18 WMC20/18008211 6.19 Stnd. Units 0.1 SW846: 9045D MMSD 05/26/18 WMC21/18008718 6.18 Stnd. Units 0.1 SW846: 9045D MMSD 06/02/18 WMC22/18009350 6.25 Stnd. Units 0.1 SW846: 9045D MMSD 06/09/18 WMC23/18009867 6.11 Stnd. Units 0.1 SW846: 9045D MMSD 06/16/18 WMC24/18010641 6.25 Stnd. Units 0.1 SW846: 9045D MMSD 06/23/18 WMC25/18011184 6.23 Stnd. Units 0.1 T SW846: 9045D MMSD 06/30/18 WMC26/18011743 6.21 Stnd. Units 0.1 SW846: 9045D MMSD 07/07/18 WMC27/18013254 6.29 Stnd. Units 0.1 SW846: 9045D MMSD 07/14/18 WMC28/18013259 6.18 Stnd. Units 0.1 SW846: 9045D MMSD 07/21/18 WMC29/18014498 6.25 Stnd. Units 0.1 SW846: 9045D MMSD 07/28/18 WMC30118014929 6.32 Stnd. Units 0.1 SW846: 9045D MMSD 08/04/18 WMC31/18015389 J 6.24 Stnd. Units 0.1 SW846: 9045D MMSD 08/11/18 WMC32/18016218 6.34 Stnd. Units ` 0.1 SW846: 9045D MMSD 08/18/18 WMC33/18016543 6.29 Stnd. Units 0.1 SW846: 9045D MMSD 08/25/18 WMC34/18018126 6.38 Stnd. Units 0.1 SW846: 9045D MMSD 09/01/18 WMC35/18018151 6.53 Stnd. Units 0.1 SW846: 9045D MMSD 09/08/18 WMC36/18018801 6.57 Stnd. Units 0.1 SW846: 9045D MMSD 09/15/18 WMC37/18019193 6.57 Stnd. Units 0.1 SW846: 9045D MMSD 09/22/18 T WMC38/18021138 6.45 Stnd. Units 0.1 SW846: 9045D MMSD 09/29/18 WMC39/18021139 6.37 Stnd. Units 0.1 SW846: 9045D MMSD 10/06/18 WMC40/18021604 6.19 Stnd. Units 0.1 SW846: 9045D MMSD 10/13/18 WMC41/18022042 6.52 Stnd. Units 0.1 SW846: 9045D MMSD 10/20/18 WMC42/18022451 6.51 Stnd. Units 0.1 SW846: 9045D MMSD 10/27/18 WMC43/18022969 6.62 Stnd. Units 0.1 SW846: 9045D MMSD 11/10/18 WMC45/18025129 6.52 Stnd. Units 0.1 SW846: 9045D MMSD 11/17/18 WMC46/18024635 6.42 Stnd. Units 0.1 SW846: 9045D MMSD 11/24/18 WMC47118025830 6.44 Stnd. Units 0.1 SW846: 9045D MMSD 12/01/16 WMC48/1802621'6 6.35 Stnd. Units 0.1 SW846: 9045D MMSD Page 64 of 106 SYS/rptlMifoMonthly 1/10/13 U Printed: 1/18/19 09:41 MSD I't1r;If[S"I fIIeri fM►AINfEli' pH -Solids 12/08/18 12/15/18 Annual Milorganite Report January 1 to December 31, 2018 5- Sample 10 Result .D LOQ QA Flags ArUllybcal MeIflod Lab WMC49/18026842 6.28 Stnd. Units 0.1 SW846: 9045D MMSD WMC50/18027542 12/22/18 WMC51/18027885 12/29/18 WMC52/18028104 Avg Result: 6.2 Stnd. Units 6.37 Stnd. Units 0.1 6.26 Stnd. Units 0.1 6.35 Stnd. Units 0.1 Min LOD: 0.1 Stnd. Units SW846: 9045D SW846: 9045D SW846: 9045D Max Result: 6.62 Stnd. Units MMSD MMSD MMSD Page 65 of 106 SYS/rptlMiloMonth/y 1/10113 tj printed. 1118/19 09:4; I y Annual Milorganite Report NNSD January 1 to December 31, 2018 URi1F3 f&A UFOR FWVW PHOSPHORUS ICP METHOD Sample Date Sample 10 Resuft LOD LOQ QA flags Analytkal Method 01/01/18 DMO101/18000013 23000 mg/kg D.W. 6 19 SW846: 6010C MMSD 01/02/18 DMO102/18000047 23000 mg/kg D.W. 6 19 SW846: 6010C MMSD 01/03/18 DMO103118000061 01/04/18 DMO104/18000098 24000 mg/kg D.W. 6.2 20 23000 mg/kg D.W. 6 19 01/05/18 DMO105/18000155 23000 mg/kg D.W. 6.1 20 01/06/18 DMO106/18000168 24000 mg/kg D.W. 6.1 20 01/07/18 DMO107118000189 23000 mg/kg D.W. 6.1 20 01/08/18 DMO108/18000203 23000 mg/kg D.W. 6 19 01/09/18 DMO109/18000232 22000 mg/kg D.W. 6.1 20 01/10/18 D100110/18000326 22000 mg/kg D.W. 6 19 01/11/18 DM0111/18000347 24000 mg/kg D.W. 6 19 01/12/18 DM0112/18000363 23000 mg/kg D.W. 6.1 20 01/13/18 DM0113/18000397 24000 mg/kg D.W. 6 19 01/14/18 DM0114/18000418 24000 mg/kg D.W. 6 19 01/15/18 DM0115/18000432 23000 mg/kg D.W. 6 19 01/16/18 DMO 116/18000461 25000 mg/kg D.W. 6 19 01/17/18 DM0117/18000652 26000 mg/kg D.W. 6.1 20 01/18/18 DM0118118000673 24000 mg/kg D.W. 6 19 01/19/18 DMO 119/18000689 25000 mg/kg D.W. 6 19 01/20/18 DMO120/18000702 23000 mg/kg D.W. 6 19 01/21/18 DMO121/18000800 23000 mg/kg D.W. 6 19 01/22/18 DMO122/18000814 23000 mg/kg D.W. 6.1 20 01/23/18 DMO123/18000843 23000 mg/kg D.W. 6.2 20 01/24/18 DMO124/18000875 23000 mg/kg D.W. 5.9 19 01/25/18 DMO125/18000896 24000 mg/kg D.W. 5.8 19 01/26/18 DMO126118000912 23000 mg/kg D.W. 5.9 19 01/27/18 DMO127118000925 22000 mg/kg D.W. 6 19 01/28/18 DMO128/18000946 22000 mg/kg D.W. 5.9 19 01/29/18 DMO129/18001200 22000 mg/kg D.W. 5.9 19 01/30/18 DMO130/18001229 23000 mg/kg D.W. 6 19 01/31/18 DMO131/18001259 24000 mg/kg D.W. 5.9 19 02/01/18 DM0201/18001280 23000 mg/kg D.W. 6 19 02/02/18 DM0202/18001421 23000 mg/kg D.W. 5.9 19 02/03/18 DM0203118001434 23000 mg/kg D.W. 6 19 02/04/18 DM0204/18001455 23000 mg/kg D.W. 6 19 02/05/18 DM0205/18001469 22000 mg/kg D.W. 6 19 02/06/18 DM0206/18001506 21000 mg/kg D.W. 6 19 02/07/18 DM0207118001599 02/08/18 DM0208118001620 02/09/18 DM0209118001738 02/10/18 DM0210/18001751 02/11/18 DM0211/18001772 02/12/18 DM0212/18001786 21000 mg/kg D.W. 6 19 23000 mg/kg D.W. 5.9 19 23000 mg/kg D.W. 5.9 19 22000 mg/kg D.W. 6 19 22000 mg/kg D.W. 6 19 22000 mg/kg D.W. 6 19 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846* 6010C MMSD SW846: 6010C MMSD Q2 Q2. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 02/13/18 DM0213/18001815 22000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 02/14/18 DM0214/18001860 02/15/18 DM0215/18001881 02/16/18 DM0216/18001897 SYS/rptiMiloMonthly 1/10/13 tj 22000 mg/kg D.W. 6 19 SW846: 6010C MMSD 23000 mg/kg D.W. 6 19 SW846: 6010C MMSD 23000 mg/kg D.W. S.9 19 SW846: 6010C MMSD Page 66 of 106 Printed: 1/18/19 09:4; 02/21/18 DM0221118002077 21000 mg/kg D.W. 6 Annual Milorganite Report e.iNSD SW846: 6010C MMSD 02/22/18 January 1 to December 31, 2018 19000 mg/kg D.W. 6 19 SW846: 6010C PHOSPHORUS ICP METHOD 02/23/18 DM0223/18002415 19000 mg/kg D.W. 5.9 Sample 10 02/17/18 DM0217/18001944 Result 23000 mg/kg D.W. .. 6 LGQ QA Flap 19 knaWkal Mev" Lab SW846: 6010C MMSD 02/18/18 DM0218/18001965 23000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/19/18 DM0219/18001979 22000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 02/20/18 DM0220/18002047 21000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/21/18 DM0221118002077 21000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/22/18 DM0222/18002097 19000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/23/18 DM0223/18002415 19000 mg/kg D.W. 5.9 19 SW846: 6010C MMSD 02/24/18 DM0224/18002427 18000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/25/18 DM0225/18002447 18000 mg/kg D.W. 5.9 19 SW846: 6010C MMSD 02/26/18 DM0226/18002461 19000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/27/18 DM0227/18002537 18000 mg/kg D.W. 6 19 SW846: 6010C MMSD 02/28/18 DM0228/18002609 19000 mg/kg D.W. 6 19 Q2. SW846: 6010C MMSD 03/01/18 DM0301/18002628 19000 mg/kg D.W. 6.1 19 SW846: 6010C MMSD 03/02/18 DM0302/18002711 19000 mg/kg D.W. 6 19 Q2. SW846: 6010C MMSD 03/03/18 DM0303/18002722 18000 mg/kg D.W. 6.1 19 SW846: 6010C MMSD 03/04/18 DM0304/18002741 19000 mg/kg D.W. 6.1 19 SW646: 6010C MMSD 03/05/18 DM0305/18002805 20000 mg/kg D.W. 6.1 19 SW846: 6010C MMSD 03/06/18 DM0306/18002862 20000 mg/kg D.W. 6 19 SW846: 6010C MMSD 03/07/18 DM0307/18002927 20000 mg/kg D.W. 6.1 20 Q2. SW846: 6010C MMSD 03/08/18 DM0308/18003015 20000 mg/kg D.W. 6 19 SW846: 6010C MMSD 03/09/18 DM0309/18003030 19000 mg/kg D.W. 5.9 19 SW846: 6010C MMSD 03/10/18 DM0310/18003041 _ 20000 mg/kg D.W. 6.1 20 m SW846: 6010C MMSD 03/11/18 DM0311/18003060 20000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/12/18 DM0312/18003335 20000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/13/18 DMO313/18003681 20000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/14/18 DM0314/18003710 21000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/15/18 DM0315118003729 20000 mg/kg D.W. 6 19 SW846: 6010C MMSD 03/16/18 DM0316/18003744 20000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/17/18 DM0317118003755 21000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/18/18 DM0318/18003780 22000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/19/18 DM0319/18003911 22000 mg/kg D.W. 6.3 20 SW846: 6010C MMSD 03/20/18 DM0320118003938 21000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/21/18 DM0321118003967 22000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/22/18 DM0322/18004111 22000 mg/kg D.W. 6 19 SW846: 6010C MMSD 03/23/18 DM0323118004126 22000 mg/kg D.W. 5.9 19 SW846: 6010C MMSD 03/24/18 DM0324/18004137 21000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/25/18 DM0325/18004156 22000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/26/18 DM0326/18004320 21000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/27/18 DM0327/18004347 22000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 03/28/18 DM0328/18004376 22000 mg/kg D.W. 6.1 20 SW846: 6010C MMSD 03/29/18 DM0329/18004395 21000 mg/kg D.W. 6 19 SW846: 6010C MMSD 03/30/18 DM0330/18004410 21000 mg/kg D.W. 6.3 20 SW846: 6010C MMSD 03/31/18 DM0331/18004752 21000 mg/kg D.W. 6 19 SW846: 6010C MMSD 04/01/18 DM0401/18004771 22000 mg/kg D.W. 6.2 20 SW846: 6010C MMSD 04/02/18 DM0402/18004784 21000 mg/kg D.W. 6.1 19 SW846: 6010C MMSD 04/03/18 DM0403/18004943 22000 mg/kg D.W. 19 86 SW846: 6010C MMSD 04/04/18 DM0404118004972 20000 mg/kg D.W. 18 84 SW846: 6010C MMSD Page 67 of 106 SYS/rptimiloMonthty 1/10/13 tj Viinfe0: 1/18/19 09:4; N 04/14/18 04/15/18 04/16/18 04/17/18 04/18/18 04/19/18 04/20/18 04/21/18 04/22/18 04/23/18 04/24/18 04/25/18 04/26/18 04/27/18 04/28/18 04/29/18 04/30/18 05/01/18 05/04/18 05/05/18 05/06/18 05/07/18 05/08/18 05/09/18 DM0414/18005474 OM0415/18005605 T 23000 mg/kg D.W. 22000 mg/kg D.W. 18 19 84 86 Annual Milorganite Report e-NNSD 18 84 DM0417/18005709 January 1 to December 31, 2018 RM FR a atter NOW 84 DM0418/18005738 20000 mg/kg D.W. 18 PHOSPHORUS ICP METHOD DM0419/18005757 20000 mg/kg D.W. 18 83 ME E 04/05/18 DM0405/18005037 Resuit 24000 mg/kg D.W. LOD 18 LOQ s 85 SW846: 6010C MMSD 04/06/18 DM0406118005052 23000 mg/kg D.W. 19 86 SW846: 6010C MMSD 04/07/18 DM0407/18005063 20000 mg/kg D.W. 18 84 B8. SW846: 6010C MMSD 04/08/18 DM0408/18005082 19000 mg/kg D.W. 19 87 B8. SW846: 6010C MMSD 04/09/18 DM0409118005095 21000 mg/kg D.W. 19 86 B8, Q3. SW846: 6010C MMSD 04/10/18 DM0410/18005164 23000 mg/kg D.W. 19 86 SW846: 6010C MMSD ^ 04/11/18 DM0411/18005193 21000 mg/kg D.W. 19 86 SW846: 6010C MMSD 04/12/18 DM0412/18005446 21000 mg/kg D.W. 19 86 SW846: 6010C MMSD 04/13/18 DM0413/18005463 21000 mg/kg D.W. 19 86 SW846: 6010C MMSD 04/14/18 04/15/18 04/16/18 04/17/18 04/18/18 04/19/18 04/20/18 04/21/18 04/22/18 04/23/18 04/24/18 04/25/18 04/26/18 04/27/18 04/28/18 04/29/18 04/30/18 05/01/18 05/04/18 05/05/18 05/06/18 05/07/18 05/08/18 05/09/18 DM0414/18005474 OM0415/18005605 T 23000 mg/kg D.W. 22000 mg/kg D.W. 18 19 84 86 DM0416/18005618 21000 mg/kg D.W. 18 84 DM0417/18005709 21000 mg/kg D.W. 18 84 DM0418/18005738 20000 mg/kg D.W. 18 85 DM0419/18005757 20000 mg/kg D.W. 18 83 DM0420/18006009 20000 mg/kg D.W. 16 82 DM0421/18006020 21000 mg/kg D.W. 18 84 DM0422118006039 f 22000 mg/kg D.W. 18 84 DM0423/18006157 21000 mg/kg D.W. 18 83 DM0424118006185 21000 mg/kg D.W. 18 85 DM0425/18006214 22000 mg/kg D.W. 19 88 DM0426/18006233 20000 mg/kg D.W. 19 85 OM0427/18006441 20000 mg/kg D.W. 18 82 DM0428/18006452 20000 mg/kg D.W. 19 86 DM0429118006471 20000 mg/kg D.W. 18 85 DM0430118006484 21000 mg/kg D.W. 19 86 DMO501/18006571 21000 mg/kg D.W. 19 86 DM0502/18006600 21000 mg/kg D.W. 19 85 DMO503/18006854 22000 mg/kg D.W. 18 So DM0504118007005 21000 mg/kg D.W. 18 82 DMO505/18007016 20000 mg/kg D.W. 18 83 DM0506/18007035 22000 mg/kg D.W. 18 85 DM0507/18007257 20000 mg/kg D.W. 18 82 DM0508/18007284 20000 mg/kg D.W. 18 84 DMO509/18007313 20000 mg/kg D.W. 18 84 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD 05/10/18 DM0510/18007340 20000 mg/kg D.W. 18 85 SW846: 6010C MMSD 05/11/18 05/12/18 DMO511/18007418 DMO512/18007429 22000 mg/kg D.W. 21000 mg/kg D.W. 19 18 86 84 SW846: 6010C SW846: 6010C MMSD MMSD 05/13/18 DM0513/18007476 20000 mg/kg D.W. 18 84 SW846: 6010C MMSD 05/14/18 05/15/18 05/16/18 DM0514/18007591 DM0515/18007976 DM0516/18008005 21000 mg/kg D.W. 20000 mg/kg D.W. 20000 mg/kg D.W. 19 18 18 86 �82 84 SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 05/17/18 05/18/18 DM0517/18008103 DM0518118008118 20000 mg/kg D.W. 20000 mg/kg D.W. 18 19 84 86 SW846: 6010C SW846: 6010C MMSD MMSD 05/19/18 DMO519/18008129 19000 mg/kg D.W. 18 85 SW846: 6010C MMSD 05/20/18 DM0520/18008196 20000 mg/kg D.W. 18 84 SW846: 6010C MMSD 05/21/18 DM0521/18008209 20000 mg/kg D.W. 18 85 SW846: 6010C MMSD SYS1rptSMdoMonthly 1110/13 0 Page 68 of 106 Printed: 1118119 09:4; -?.kNSD Annual Milorganite Report January 1 to December 31, 2018 �sltAil4 i9i 1 rlil�fi iim!!�kt� PHOSPHORUS ICP (METHOD Result OD LOQ QA Flags Anahlical Method Lab 05/22/18 DMO522/18008236 20000 mg/kg D.W. 19 86 SW846: 6010C MMSD 05/23/18 DMO523/18008304 20000 mg/kg D.W. 18 84 Q3. SW846: 6010C MMSD 05/24/18 DM0524/18008658 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 05/25/18 DM0525/18008673 20000 mg/kg D.W. 18 83 SW846: 6010C MMSD 05/26/18 DMO526/18008684 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 05/27/16 DMO527/18008703 22000 mg/kg D.W. 18 85 SW846: 6010C MMSD 05/28/18 DM0528118008716 22000 mg/kg D.W. 19 86 SW846: 6010C MMSD 05/29/18 DM0529/18008888 22000 mg/kg D.W. 19 86 SW846: 6010C MMSD 05/30/18 DM0530118008917 24000 mg/kg D.W. 18 83 B8. SW846: 6010C MMSD 05/31/18 DM0531/18008936 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/01/18 DM0601/18009150 23000 mg/kg D.W. 18 82 Q2. SW846: 6010C MMSD 06/02/18 DM0602/18009161 22000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/03/18 DM0603/18009335 22000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/04/18 DM0604/18009348 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 06/05/18 DM0605/18009375 22000 mg/kg D.W. 18 85 SW846: 6010C MMSD 06/06/18 DM0606/18009404 23000 mg/kg D.W. 19 86 SW846: 6010C MMSD 06/07/18 DM0607/18009423 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/08/18 DM0608/18009822 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 06/09/18 DM0609/18009833 24000 mg/kg D.W. 18 83 AO. SW846: 6010C MMSD 06/10/18 DM0610118009852 24000 mg/kg D.W. 18 82 AO. SW846: 6010C MMSD 06/11/18 DM0611/18009865 25000 mg/kg D.W. 18 85 AO. SW846: 6010C MMSD 06/12/18 DM0612/18010098 25000 mg/kg D.W. 19 85 SW846: 6010C MMSD 06/13/18 DM0613118010127 25000 mg/kg D.W. 19 86 SW846: 6010C MMSD 06/14/18 DM0614118010437 25000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/15/18 DM0615/18010452 25000 mg/kg D.W. 18 83 SW846: 6010C MMSD 06/16/18 DMO616/18010463 23000 mg/kg D.W. 18 83 SW846: 6010C MMSD 06/17/18 DM0617118010482 24000 mg/kg D.W. 18 82 SW846: 6010C MMSD 06/18/18 DM0618118010639 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/19/18 DM0619/18010666 24000 mg/kg D.W. 18 85 SW846: 6010C MMSD 06/20/18 DM0620/18010694 24000 mg/kg D.W. 18 82 SW846: 6010C MMSD 06/21/18 DM0621/18010713 24000 mg/kg D.W. 18 81 SW846: 6010C MMSD 06/22/18 DM0622/18010939 23000 mg/kg D.W. 18 81 SW846: 6010C MMSD 06/23/18 DM0623118010950 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD 06/24/18 DM0624/18011087 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 06/25/18 DM0625/18011182 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 06/26/18 DM0626/18011209 22000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/27/18 DM0627/18011597 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 06/28/18 DM0628/18011616 22000 mg/kg D.W. 18 84 Q3 SW846: 6010C MMSD 06/29/18 DM0629/18011631 24000 mg/kg D.W. 18 84 SW846: 6010C MMSD 06/30/18 DM0630/18011642 22000 mg/kg D.W. 18 85 SW846: 6010C MMSD 07/01/18 DM0701/18011728 23000 mg/kg D.W. 18 83 SW846: 6010C MMSD 07/02/18 DM0702/18011741 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 07/03/18 DM0703118011881 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 07/04/18 DM0704/18011909 24000 mg/kg D.W. 18 82 SW846: 6010C MMSD 07/05/18 DM0705/18012390 24000 mg/kg D.W. 18 83 SW846: 6010C MMSD 07/06/18 DM0706/18012405 24000 mg/kg D.W. 18 84 SW846: 6010C MMSD 07/07/18 DM0707/18012416 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD Page 69 of 106 5Y51rptlM11aMonthly 1/10/13 tj Printed.1/18/19 09: 4i 1. MMS PHOSPHORUS ICP METHOD 07/08/18 DM0708/18012435 23000 mg/kg D.W. 18 63 DM0812/18016203 07/09/18 DM0709/18012448 23000 mg/kg D.W. 18 85 DM0816/18016300 DM0817/18016365 DM0818/18016505 07/10/18 DM0710/18012474 25000 mg/kg D.W. 18 84 DM0821/18016714 07/11/18 DM0711/18012820 24000 mg/kg D.W. 18 82 MMSD 07/12/18 DM0712118012861 25000 mg/kg D.W. 18 83 MMSD 07/13/18 DM0713118012876 25000 mg/kg D.W. 18 83 MMSD 07/14/18 DM0714/18013220 25000 mg/kg D.W. 18 82 MMSD 07/15/18 DM0715/18013239 25000 mg/kg D.W. 18 83 07/16/18 DM0716/18013252 25000 mg/kg D.W. 18 82 Q2. 07/17/18 DM0717/18013751 26000 mg/kg D.W. 18 82 07/18/18 DM0718/18013961 26000 mg/kg D.W.18 82 Q2. 07/19/18 DM0719/18014047 26000 mg/kg D.W. 18 81 Q2. 07/20/18 DM0720/18014062 26000 mg/kg D.W. 18 83 Q2. 07/21/18 DM0721/18014073 26000 mg/kg D.W. 18 82 07/22/18 DM0722118014483 25000 mg/kg D.W. 18 83 07/23/18 DM0723/18014496 24000 mg/kg D.W. 18 84 Q2. 07/24/18 DM0724/18014523 25000 mg/kg D.W. 18 83 Q2. 07/25/18 DM0725/18014551 24000 mg/kg D.W. 18 85 07/26/18 DM0726118014570 24000 mg/kg D.W. 18 84 07/27/18 DM0727/18014585 23000 mg/kg D.W. 18 82 07/28/18 DM0728/18014676 23000 mg/kg D.W. 18 82 07/29/18 DM0729118014910 24000 mg/kg D.W. 18 82 07/30/18 DM0730/18014925 24000 mg/kg D.W. 18 84 07/31/16 DM0731118014954 25000 mg/kg D.W. 18 83 08/01/18 DM0801/18014969 23000 mg/kg D.W. 18 62 B8, Q3. 08/02/18 DMOB02/18015140 24000 mg/kg D.W. 18 82 08/03/18 DM0803/18015155 24000 mg/kg D.W. 18 83 08/04/18 DMOB04/18015252 25000 mg/kg D.W. 16 81 08/05/18 DM0805/18015279 24000 mg/kg D.W. 18 83 08/06/18 DMO806/18015385 26000 mg/kg D.W. 18 82 08/07/18 08/08/18 08/09/18 08/10/18 DMO807118015414 DMO808/18015473 DM0809/18015500 DM0810/18015899 08/11/18 DM0811/18015910 08/12/18 DM0812/18016203 08/13/18 08/14/18 DM0813/18016216 DM0814/18016254 08/15/18 DMO815/18016281 08/16/18 08/17/18 08/18/18 DM0816/18016300 DM0817/18016365 DM0818/18016505 08/19/18 DM0819/18016525 08/20/18 DM0820/18016539 08/21/18 DM0821/18016714 06/22/18 DM0822/18016742 08/23/18 DMO823/18017352 SYS/rptlMi/oMonthly 1/10/13 tj Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 27000 mg/kg D.W. 18 82 26000 mg/kg D.W. 18 82 27000 mg/kg D.W. 18 82 26000 mg/kg D.W. 18 82 25000 mg/kg D.W. 18 82 25000 mg/kg D.W. 18 81 25000 mg/kg D.W. 18 81 22000 mg/kg D.W. 18 62 26000 mg/kg D.W. 18 82 SW846: 6010C SW846: 6010C SW846: 6010C MMC11 MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 23000 mg/kg D.W. 18 81 SW846: 6010C MMSD 23000 mg/kg D.W. 18 81 _ SW846: 6010C MMSD 25000 mg/kg D.W. 18 82 SW846: 6010C MMSD 24000 mg/kg D.W. 18 81 SW846: 6010C MMSD 24000 mg/kg D.W. 18 81 SW846: 6010C MMSD 24000 mg/kg D.W. 18 82 SW846: 6010C MMSD 24000 mg/kg D.W. 18 82 SW846: 6010C MMSD 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD Page 70 of 106 Printed: 1/18/19 09:4; Milorganite Report _Annual 0145D January 1 to December 31, 2018 WWI Fj* 1 it k" [IY�PAMi� PHOSPHORUS ICP METHOD 08/24/18 DM0824/18017367 21000 mg/kg D.W. O. 18 LOQ 81 QA Flags Analytir-al Metbod SW846: 6010C Lab MMSD 08/25/18 DM0825118017378 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 08/26/18 DM0826/18017397 21000 mg/kg D.W. 18 81 SW846: 6010C MMSD 08/27/18 DM0827/18017410 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD 08/28/18 DM0828/18017434 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 08/29/18 DM0829/18017462 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 08/30/18 DMO830/18017483 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 08/31/18 DM0831/18017498 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/01/18 DM0901/18017520 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/02/18 DMO902/18017752 21000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/03/18 DM0903/18018124 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/04/18 DM0904/18018149 23000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/05/18 DMO905/18018305 23000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/06/18 DM0906/18018326 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/07/18 DMO907/18018342 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/08/18 DMO908/18018353 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/09/18 DM0909/18018724 22000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/10/18 DM0910/18018799 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/11/18 DMO911/18018825 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/12/18 DMO912/18018854 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/13/18 DM0913/18018875 22000 mg/kg D.W. 18 84 Q3. SW846: 6010C MMSD 09/14/18 DM0914/18018891 21000 mg/kg D.W. 18 84 SW846: 6010C MMSD 09/15/18 DM0915/18019159 23000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/16/18 DM0916/18019178 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/17/18 DMO917/18019191 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/18/18 DMO918/18019447 21000 mg/kg D.W. 18 84 SW846: 6010C MMSD 09/21/18 DM0921/18019515 21000 mg/kg D.W. 18 80 SW846: 6010C MMSD 09/22/18 DM0922/18019574 21000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/23/18 DM0923/18019665 21000 mg/kg D.W. 17 80 SW846: 601DC MMSD 09/24/18 DM0924/18020088 21000 mg/kg D.W. 18 81 Q2. SW846: 6010C MMSD 09/25/18 DM0925/18020314 21000 mg/kg D.W. 18 81 SW846: 6010C MMSD 09/26/18 DMO926/18020343 20000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/27/18 DMO927/18020364 21000 mg/kg D.W. 18 83 SW846: 6010C MMSD 09/28/18 DM0928/18020380 20000 mg/kg D.W. 18 85 SW846: 6010C MMSD 09/29/18 DM0929/18020391 20000 mg/kg D.W. 18 82 SW846: 6010C MMSD 09/30/18 DM0930/18020411 20000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/01/18 DM1001118021136 20000 mg/kg D.W. 18 82 SW846: 6010C _ MMSD 10/02/18 DM1002/18021162 19000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/03/18 DM1003/18021190 18000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/04/18 DM1004/18021541 21000 mg/kg D.W. 18 82 Q3. SW846: 6010C MMSD 10/05/18 DM1005/18021557 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/06/18 DM1006/18021568 20000 mg/kg D.W. 18 84 SW846: 6010C MMSD 10/07/18 DM1007/18021588 20000 mg/kg D.W. 18 81 SW846: 6010C MMSD 10/08/18 DM1008/18021602 20000 mg/kg D.W. 18 81 SW846: 6010C MMSD 10/09/18 DM1009/18021627 20000 mg/kg D.W. 18 81 SW846: 6010C MMSD 10/10/18 DM1010/18021656 21000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/11/18 DM1011118021975 20000 mg/kg D.W. 18 82 SW846: 6010C MMSD Page 71 of 106 SYSIrptlMiloMonthly 1/10/13 0 Printed: 1/18/19 09:47 t 10/27/18 11/07/18 DM 1026/9 8022767 DM1027/18022778 DM 1107/18023991 11/08/18 DM1108/18024012 Annual Milorganite Report NNSDJanuary 11/10/18 DM 1110/18024523 11/11/18 DM1111/18024619 1 to December 31, 2018 wMa FfIt A, Cita RMOW 11/13/18 DM1113/18025014 11/14/18 DM1114/18025043 11/15/18 PHOSPHORUS ICP METHOD Sampie Date Sample ID Result LOD LOQ QA Rags Analytkal Pleffiod Lab 10/12/18 DM1012118021991 20000 mg/kg D.W. 18 81 SW846: 6010C MMSD 10/13/18 DM1013/18022006 20000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/14/18 DM1014/18022026 20000 mg/kg D.W. 18 83 SW846: 6010C W MMSD 10/15/18 DM1015/18022040 21000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/16/18 DM1016/18022065 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/17/18 DM1017/18022094 21000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/18/18 DM1018118022133 21000 mg/kg D.W. 18 82 ` SW846: 6010C MMSD 10/19/18 DM1019/18022269 21000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/20/18 DM1020118022280 22000 mg/kg D.W. 18 ^ 81 SW846: 6010C MMSD 10/21/18 DM1021/18022435 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/22/18 DM1022/18022449 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/23/18 DM1023/18022614 22000 mg/kg D.W. 18 82 SW846: 6010C MMSD 10/24/18 DM1024/18022643 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/25/18 10 26 18 DM1025/18022708 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 10/27/18 11/07/18 DM 1026/9 8022767 DM1027/18022778 DM 1107/18023991 11/08/18 DM1108/18024012 11/09/18 DM1109/18024028 11/10/18 DM 1110/18024523 11/11/18 DM1111/18024619 11/12/18 DM1112/18024633 11/13/18 DM1113/18025014 11/14/18 DM1114/18025043 11/15/18 DM1115/18025064 11/16/18 DM 1116118025080 11/17/18 11/18/18 11/19/18 11/20/18 11/21/18 11/22/18 11/23/18 11/24/18 11/25/18 11/26/18 110711R 11/29/18 11/30/18 12/01/18 12/02/18 12/03/18 12/04/18 DM 1117/18025093 DM 1118/18025113 DM 1119/18025127 DM 1120/18025356 DM1121/18025385 DM 1122/18025406 DM 1123/18025422 DM 1 124/18025750 DM1125118025769 DM1126/18025828 DM1127118025860 DM1128118025888 DM 1129/18025956 DM1130/18025971 22000 mg/kg D.W. 22000 mg/kg D.W. 26000 mg/kg D.W. 25000 mg/kg D.W. 26000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 23000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 25000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 25000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 25000 mg/kg D.W. 26000 mg/kg D.W. 25000 mg/kg D.W. 27000 mg/kg D.W. 24000 mg/kg D.W. 18 82 SW846:6010C MMSD 18 81 SW846: 6010C MMSD 18 81 SW846: 6010C MMSD 18 81 SW846: 6010C MMSD 18 81 SW946:6010C MMSD 18 81 SW846: 6010C MMSD 18 81 SW846: 6010C MMSD 18 83 SW846: 6010C MMSD 18 63 SW846:6010C MMSD 18 84 SW846: 6010C MMSD 18 83 SW846: 6010C MMSD 19 86 SW846: 6010C MMSD 10 18 18 18 18 18 18 18 18 18 18 18 10 18 DM1201/18026182 25000 mg/kg D.W. 18 DM 1202/18026201 24000 mg/kg D.W. 18 DM1203118026214 24000 mg/kg D.W. 18 DM1204/18026391 23000 mg/kg D.W. 18 OL 84 82 82 82 84 0j 85 85 81 82 82 83f �! 84 84 83 83 84 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 601DC SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD w[UNI J I"II`I�V MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 12/05/18 DM1205/18026578 23000 mg/kg D.W. 18 84 SW846: 6010C MMSD 12/06/18 DM1206118026621 23000 mg/kg D.W. 19 86 SW846: 6010C MMSD 12/07/18 DM1207/18026797 22000 mg/kg D.W. 19 86 SW846: 6010C MMSD SYS/rptlMiloMonthly 1/10/13 tj Page 72 of 106 Printed., 1/18/19 09:4; Ott'I4i5 0 t WINI f h PHOSPHORUS ICP METHOD fiiW"rliililli7s — � � 12/08/18 DM1208/18026808 25000 mg/kg D.W. 18 84 12/09/18 12/10/18 12/11/18 12/12/18 12/13/18 12/14/18 DM1209/18026827 DM1210118026840 DM1211/18027102 24000 mg/kg D.W. 24000 mg/kg D.W. 24000 mg/kg D.W. 18 84 19 ^87 18 82 DM1212/18027130 26000 mg/kg D.W. 18 82 DM1213/18027253 22000 mg/kg D.W. 18 84 DM1214/18027306 23000 mg/kg D.W. 18 82 Annual Milorganite Report January i to December 31, 2018 .y SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW646:6010C MMSD 12/15/18 DM1215/18027317 22000 mg/kg D.W. 18 83 SW846: 6010C MMSD 12/16/18 DM1216/18027525 22000 mg/kg D.W. 18 84 SW846: 6010C MMSD 12/17/18 DM1217/18027540 22000 mg/kg D.W. 19 86 SW846: 6010C MMSD 12/18/18 DM1218/18027643 23000 mg/kg D.W. 19 87 SW846: 6010C MMSD 12/19/18 12/20/18 DM1219/18027676 DM1220/18027805 23000 mg/kg D.W. 24000 mg/kg D.W. 18 18 83 82 12/21/18 DM1221/18027821 25000 mg/kg D.W. 18 83 Q2. 12/22/18 DM1222/18027832 25000 mg/kg D.W. 18 84 12/23/18 DM1223/18027852 25000 mg/kg D.W. 18 85 12/24/18 DM1224/18027883 24000 mg/kg D.W. 18 85 12/25/18 DM1225/18027952 24000 mg/kg D.W. 19 86 12/26/18 DM1226118027969 25000 mg/kg D.W. 19 86 12/27/18 12/28/18 DM1227/18027990 DM1228/18028005 25000 mg/kg D.W. 24000 mg/kg D.W. 19 19 86 87 12/29/18 12/30/18 DM1229/18028070 DM1230/18028089 25000 mg/kg D.W. 26000 mg/kg D.W. 18 18 83 82 12/31/18 DM1231/18028102 Avg Result: 22000 mg/kg D.W. 26000 mg/kg D.W. 18 84 Men LOD: 5.8 mg/kg D.W. 5Y5/rptIN,10M0nfhly 1/10/13 tj SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Max Result: 27000 mg/kg D.W. Page 73 of 106 Printed: 1/18/19 09:97 Ll W W WW WW", POTASSIUM ICP METHOD 01/01/18 DMO101/18000013 01/02/18 DMO102/18000047 4500 mg/kg D.W. 64 200 BE 4200 mg/kg D.W. 64 200 B8 01/03/18 DM0103/18000061 5000 mg/kg D.W. 66 210 B9, Q3. 01/04/18 DMO104/18000098 4600 mg/kg D.W. 64 200 B8, Q3. 01/05/18 DMO105/18000155 4600 mg/kg D.W. 66 210 B8. 01/06/18` DM0106/18000168 4800 mg/kg D.W. 65 210 B8. 01/07/18 DMO107118000189 4500 mg/kg D.W. 65 210 B8. 01/08/18 DMO108/18000203 4500 mg/kg D.W. 65 200 B8. 01/09/18 DMO109/18000232 4400 mg/kg D.W. 65 210 B8. 01/10/18 DMO110118000326 4300 mg/kg D.W. 65 200 B8. 01/11/18 DMO 111/18000347 4200 mg/kg D.W. 65 200 01/12/18 DMO112/18000363 4400 mg/kg D.W. 65 200 01/13/18 DM0113/18000397 3900 mg/kg D.W. 65 200 B8. 01/14/18 DM0114/18000418 4300 mg/kg D.W. 64 200 B8. 01/15/18 DM0115/18000432 4100 mg/kg D.W. 64 200 88. 01/16/18 DM0116/18000461 5400 mg/kg D.W. 64 200 01/17/18 OM0117/18000652 5800 mg/kg D.W. 65 210 01/18/18 DM0118/18000673 5800 mg/kg D.W. 64 200 01/19/18 DM0119/18000689 6800 mg/kg D.W. 65 200 Q2. 01/20/18 DMO120/18000702 6200 mg/kg D.W. 64 200 B8. 01/21/18 DMO121/18000800 6300 mg/kg D.W. 64 200 B8. 01/22/18 DMO122/18000814 6500 mg/kg D.W. 66 210 B8. 01/23/18 DMO123/18000843 5700 mg/kg D.W. 66 210 68. 01/24/18 DMO124/18000875 5000 mg/kg D.W. 64 200 B8. 01/25/18 DMO125/18000896 5800 mg/kg D.W. 62 200 88. 01/26/18 DMO126/18000912 6600 mg/kg D.W. 63 200 B8, Q2. 01/27/18 OM0127/18000925 6600 mg/kg D.W. 64 200 68. 01/28/18 DMO128/18000946 6200 mg/kg D.W. 63 200 B6. 01/29/18 DMO129/18001200 6200 mg/kg D.W. 63 200 B8, Q2. 01/30/18 DMO130/18001229 6200 mg/kg D.W. 64 200 B8. 01/31/18 DMO131/18001259 6100 mg/kg D.W. 64 200 B8, Q3. 02/01/18 DM0201118001280 4600 mg/kg D.W. 64 200 02/02/18 DM0202/18001421 4600 mg/kg D.W. 64 200 02/03/18 DM0203/18001434 5300 mg/kg D.W. 64 200 88. 02/04/18 DM0204/18001455 5000 mg/kg D.W. 64 200 B8, 02/05/18 DM0205/18001469 T 5400 mg/kg D.W. 64 200 B8. 02/06/18 DM0206/18001506 5700 mg/kg D.W. 64 200 B8. 02/07/18 DM0207/18001599 5600 mg/kg D.W. 64 200 B8, Q3. 02/08/18 DM0208/18001620 6000 mg/kg D.W. 64 200 02/09/18 DM0209/18001738 5700 mg/kg D.W. 63 200 02/10/18 DM0210/18001751 5400 mg/kg D.W. 64 200 02/11/18 DM0211/18001772 5100 mg/kg D.W. 64 200 02/12/18 DM0212/18001786 4900 mg/kg D.W. 65 200 Annual Milorganite Report January 1 to December 31, 2018 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD 02/13/18 DM0213/18001815 4900 mg/kg D.W. 66 210 SW846: 6010C MMSD 02/14/18 DM0214/18001860 5000 mg/kg D.W. 64 200 SW846: 6010C MMSD 02/15/18 02/16/18 DM0215/18001881 DM0216/18001897 5100 mg/kg D.W. 5600 mg/kg D.W. 64 63 200 200 SW846: 6010C SW846: 6010C MMSD MMSD SYS/iptlMlloMonth/y 1/10/13 q Page 74 of 106 Printed 1/18/19 09:4) 03/04/18 DM0304/18002741 5300 mg/kg D.W. 65 200 Annual Milorganite Report MMSD MMSD 03/05/18 DM0305/18002805 5100 mg/kg D.W. 65 January 1 to December 31, 2018 HK'*h FA 1 Of" f1, SW846: 6010C MMSD 03/06/18 DM0306/18002862 5100 mg/kg D.W. 65 200 POTASSIUM ICP METHOD SW846: 6010C MMSD 03/07/18 DM0307/18002927 5300 mg/kg D.W. 66 02/17/18 ' DM0217/18001944 Result 6500 mg/kg D.W. LOD 64 LOQ 200 QA Flags AnalytIcal MOW SW846: 6010C Lab MMSD 02/18/18 DM0218/18001965 6000 mg/kg D.W. 64 200 DM0309/18003030 SW846: 6010C MMSb 02/19/18 DM0219/18001979 5800 mg/kg D.W. 65 210 DM0310/18003041 SW846: 6010C MMSD 02/20/18 DM0220/18002047 4800 mg/kg D.W. 64 200 B8. SW846: 6010C MMSD 02/21/18 DM0221/18002077 5000 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 02/22/18 DM0222/18002097 5200 mg/kg D.W. 64 200 B8. SW846: 6010C MMSD 02/23/18 DM0223/18002415 5200 mg/kg D.W. 63 200 B8. SW846: 6010C MMSD 02/24/18 DM0224/18002427 5600 mg/kg D.W. 64 200 AO. SW846: 6010C MMSD 02/25/18 DM0225118002447 4800 mg/kg D.W. 63 200 A0. SW846: 6010C MMSD 02/26/18 DM0226/18002461 5100 mg/kg D.W. 64 200 A0, Q3. SW846: 6010C MMSD 02/27/18 DM0227/18002537 4900 mg/kg D.W. 64 200 SW846: 6010C MMSD 02/28/18 DM0228/18002609 5200 mg/kg D.W. 64 200 SW846: 6010C MMSD 03/01/18 DM0301/18002628 5500 mg/kg D.W. 65 200 SW846: 6010C MMSD 03/02/18 DM0302/18002711 5400 mg/kg D.W. 65 200 SW846: 6010C MMSD 03/03/18 DM0303/18002722 5100 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 03/04/18 DM0304/18002741 5300 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 03/05/18 DM0305/18002805 5100 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 03/06/18 DM0306/18002862 5100 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 03/07/18 DM0307/18002927 5300 mg/kg D.W. 66 210 B8. SW846: 6010C MMSD 03/08/18 DM0308/18003015 5300 mg/kg D.W. 65 200 B8. SW846: 6010C MMSD 03/09/18 DM0309/18003030 5300 mg/kg D.W. 63 200 B8. SW846: 6010C MMSD 03/10/18 DM0310/18003041 5500 mg/kg D.W. 65 210 B8. SW846: 6010C MMSD 03/11/18 DM0311/18003060 5600 mg/kg D.W. 66 210 B8. SW846: 6010C MMSD 03/12/18 DM0312118003335 5400 mg/kg D.W. 66 210 B8. SW846: 6010C MMSD 03/13/18 DM0313118003681 5400 mg/kg D.W. 67 210 68. SW846: 6010C MMSD 03/14/18 DM0314118003710 5300 mg/kg D.W. 66 210 B8. SW846: 6010C MMSD 03/15/18 DM0315118003729 5400 mg/kg D.W. 64 200 SW846: 6010C MMSD 03/16/18 DM0316118003744 5100 mg/kg D.W. 66 210 SW846: 6010C MMSD 03/17/18 DM0317/18003755 5800 mg/kg D.W. 66 210 89. SW846: 6010C MMSD 03/18/18 03/19/18 03/20/18 03/21/18 03/22/18 DM0318/18003780 DM0319/18003911 DMO320/18003938 D M0321 / 18003967 DM0322/18004111 03/23/18 DM0323/18004126 03/24/18 DM0324/18004137 03/25/18 DM0325/18004156 03/26/18 DM0326/18004320 03/27/18 DM0327/18004347 5500 mg/kg D.W. 65 210 69. SW846: 6010C MMSD 5500 mg/kg D.W. 67 210 B9. 5600 mg/kg D.W. 65 210 Q3. 5200 mg/kg D.W. 5100 mg/kg D.W. 66 64 210 200 64 5200 mg/kg D.W. 63 200 Q2. 5000 mg/kg D.W. 66 210 B8. 4800 mg/kg D.W. 4600 mg/kg D.W. 66 65 210 210 B8. B8, Q3. 4600 mg/kg D.W. 66 210 B8. SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD 03/28/18 DM0328/18004376 4600 mg/kg D.W. 66 210 B8. SW846: 6010C MMSD 03/29/18 DM0329/18004395 4700 mg/kg D.W. 64 200 B8. SW846: 6010C MMSD 03/30/18 03/31/18 DM0330/18004410 DM0331118004752 4800 mg/kg D.W. 4300 mg/kg D.W. 67 65 210 200 B8. SW846: 6010C SW846: 6010C MMSD MMSD 04/01/18 DM0401/18004771 4600 mg/kg D.W. 67 210 SW846: 6010C MMSD 04/02/18 DM0402/18004784 4600 mg/kg D.W. 65 200 SW846: 6010C MMSD 04/03/18 DM0403/18004943 5300 mg/kg D.W. 140 750 AO. SW846: 6010C MMSD 04/04/18 DM0404/18004972 4600 mg/kg D.W. 140 730 AO, B8. SW846: 6010C MMSD SYS/rptiMiloMonthly 1/10/13 hf Page 75 of 106 Printed: 1/18/19 09:4; V emmsr FUTM ►RJCUSHNXW POTASSIUM ICP METHOD 04/05/18 DM0405/18005037 04/06/18 DM0406/18005052 04/07/18 DM0407/18005063 04/08/18 DM0408/18005082 04/09/18 DM0409/18005095 04/10/18 DM0410118005164 04/11/18 DM0411118005193 04/12/18 DM0412/18005446 04/13/18 DM0413/18005463 04/14/18 04/15/18 04/16/18 04/17/18 04/18/18 04/19/18 04/20/18 04/21/18 04/22/18 04/23/18 04/24/18 04/25/18 04/28/18 04/29/18 04/30/18 05/01/18 05/02/18 DM0414/18005474 DM0415118005605 DM0416/18005618 DM0417/18005709 DM0418118005738 DM0419118005757 DM0420118006009 D M0421 /18006020 OM0422/18006039 DM0425/18006214 DM0426/18006233 DM0427/18006441 DM0428/18006452 DM0429/18006471 DM0430/18006484 DM0501 /18006571 DM0502/18006600 05/03/18 DM0503/18006854 05/04/18 DM0504/18007005 05/05/18 DM0505118007016 05/06/18 DMO506/18007035 05/07/18 DMO507/18007257 05/08/18 DM0508/18007284 05/09/18 DMO509/18007313 05/10/18 DM0510/18007340 05/11/18 DM0511/18007418 05/12/18 DM0512/18007429 05/13/18 DM0513118007476 05/14/18 DM0514/18007591 05/15/18 DM0515/18007976 05/16/18 DMO516118008005 05/17/18 DMO517/18008103 05/18/18 f DM0518/18008118 05/19/18 DMO519/18008129 05/20/18 DMO520/18008196 Annual Milorganite Report January 1 to December 31, 2018 4900 mg/kg D.W. 140 740 68. SW846: 6010C MMSD 4900 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD J4300 mg/kg D.W. 140 730 SW846: 6010C MMSD 4500 mg/kg D.W. 140 760 SW846: 6010C MMSD 4700 mg/kg D.W. 140 750 SW846: 6010C MMSD 4600 mg/kg D.W. 140 750 SW846: 6010C MMSD 5000 mg/kg D.W. 140 750 5100 mg/kg D.W. 140 750 4400 mg/kg D.W. 140 750 B8, Q3. 4800 mg/kg D.W. 140 730 4600 mg/kg D.W. 140 750 4700 mg/kg D.W. 140 730 4800 mg/kg D.W. 140 730 4600 mg/kg D.W. 140 740 4700 mg/kg D.W. 140 720 4800 mg/kg D.W. 140 710 5000 mg/kg D.W. 140 730 5000 mg/kg D.W. 4900 mg/kg D.W. 5200 mg/kg D.W. 5600 mg/kg D.W. 5200 mg/kg D.W. 5000 mg/kg D.W. 5200 mg/kg D.W. 5100 mg/kg D.W. 4900 mg/kg D.W 4400 mg/kg D.W AO. 88. 140 730 D.W. D.W. D.W. 140 720 68 BB 140 740 B8. 150 770 88, C AO B8, E 140 740 D.W. 140 710 B8. 140 750 B8. 140 740 B8. 140 750 B8. 140 750 140 740 D.W. D.W. 130 700 B8. 4700 4200 4400 mg/kg mg/kg mg/kg D.W. D.W. D.W. 140 140 140 720 730 740 68 BB 4100 4800 4600 mg/kg mg/kg mg/kg D.W. D.W. D.W. 140 140 140 720 740 730 88, C AO B8, E 4900 mg/kg D.W. 140 740 4400 mg/kg D.W. 140 750 B8 4600 5000 mg/kg mg/kg D.W. D.W. 140 140 730 730 4900 4800 mg/kg mg/kg D.W. D.W. 140 140 750 720 4200 mg/kg D.W. 140 730 88. 4300 mg/kg D.W. 140 740 AC, E 4600 mg/kg D.W. 140 750 B8. 4200 mg/kg D.W. 140 740 B8. 4300 mg/kg D.W. 140 740 B8. SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD 05/21/18 DM0521/18008209 4300 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD SYS/rptlMiloMonthly 1/10/13 U Page 76 of 106 Printed: 1/18/19 09:9; e-MIMSD ftfw"wtC1 POTASSIUM ICP METHOD W.imple .. te 05/22/18 Sample TO DM0522/18008236 05/23/18 DMO523118008304 05/24/18 DMO524/18008658 05/25/18 DM0525/18008673 05/26/18 DMO526/18008684 05/27/18 DMO527/18008703 05/28/18 DMO528/18008716 5000 mg/kg D.W. 140 750 Q3. 4700 mg/kg D.W. 140 730 Q3. 4000 mg/kg D.W. 140 710 B8. 3800 mg/kg D.W. 140 720 B8. 4200 mg/kg D.W. 140 720 DM0613/18010127 DM0614/18010437 4000 mg/kg D.W. 140 740 140 4000 mg/kg D.W. 140 750 DM0620/18010694 Annual Milorganite Report January 1 to December 31, 2018 SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 05/29/18 DM0529118008888 4000 mg/kg D.W. 140 750 Q2. SW846: 6010C MMSD 05/30/18 DM0530/18008917 4300 mg/kg D.W. 140 730 Q3. SW846: 6010C MMSD 05/31/18 DMO531/18008936 4200 mg/kg D.W. 140 740 SW846: 6010C MMSD 06/01/18 DM0601/18009150 3800 mg/kg D.W. 140 720 SW846: 6010C MMSD 06/02/18 DM0602118009161 3900 mg/kg D.W. 140 730 B8. SW846: 6010C MMSD 06/03/18 DM0603/18009335 3800 mg/kg D.W. 140 730 B8. SW846: 6010C MMSD 06/04/18 DM0604/18009348 3700 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 06/05/18 DM0605/18009375 4200 mg/kg D.W. 140 740 DM0613/18010127 DM0614/18010437 SW846: 6010C MMSD 06/06/18 DM0606/18009404 4200 mg/kg D.W. 140 750 B8. SW846: 6010C MMSD 06/07/18 DM0607/18009423 4000 mg/kg D.W. 140 730 138. 06/08/18 DM0608118009822 3900 mg/kg D.W. 140 720 B8. 06/09/18 06/10/18 DM0609/18009833 DM0610/18009852 4000 4500 mg/kg D.W. mg/kg D.W. 140 140 720 720 A0. A0. 06/11/18 06/12/18 DM0611/18009865 DM0612/18010098 4300 3400 mg/kg D.W. mg/kg D.W. 140 140 740 740 AO, Q3. B8. 06/13/18 06/14/18 DM0613/18010127 DM0614/18010437 3400 3200 mg/kg D.W. mg/kg D.W. 140 140 750 740 AO, B8. AO, B8. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 06/15/18 DM0615118010452 3900 mg/kg D.W. 140 720 SW846: 6010C MMSD 06/16/18 DMO616/18010463 3700 mg/kg D.W. 140 720 A0, B8, B9. SW846: 6010C MMSD 06/17/18 DMO617/18010482 3800 mg/kg D.W. _ 140 720 AO, B8, B9. SW846: 6010C MMSD 06/18/18 DM0618/18010639 3800 mg/kg D.W. 140 730 A0, B8, B9. SW846: 6010C MMSD 06/19/18 DM0619/18010666 3800 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD 06/20/18 DM0620/18010694 3500 mg/kg D.W. 140 720 A0, B8. SW846: 6010C MMSD 06/21/16 DM0621/18010713 3100 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 06/22/18 DM0622/18010939 3700 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 06/23/18 06/24/18 06/25/18 DM0623/18010950 OM0624/18011087 DM0625/18011182 3600 mg/kg D.W. 4000 mg/kg D.W. 3800 mg/kg D.W. 140 140 140 710 730 720 B9. B9. B9. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 06/26/18 DMO626118011209 4700 mg/kg D.W. 140 730 A0, B8, B9, Q3. SW846: 6010C MMSD 06/27/18 DM0627/18011597 3900 mg/kg D.W. 140 720 Q2. SW846: 6010C MMSD 06/28/18 DM0628118011616 3800 mg/kg D.W. 140 730 AO, B8, B9, Q3. SW846: 6010C MMSD 06/29/18 DM0629118011631 4000 mg/kg D.W. 140 730 B9. SW846: 6010C MMSD 06/30/18 DM0630/18011642 3900 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD 07/01/18 DM0701/18011728 3600 mg/kg D.W. 140 730 B8. SW846: 6010C MMSD 07/02/18 07/03/18 DM0702118011741 DM0703/18011881 3800 mg/kg D.W. 4600 mg/kg D.W. 140 140 740 730 B8. B9, Q3. SW846: 6010C SW846: 6010C MMSD MMSD 07/04/18 DM0704/18011909 3400 mg/kg D.W. 140 710 68, B9. SW846: 6010C MMSD 07/05/18 DM0705/18012390 3500 mg/kg D.W. 140 720 B8, 139, Q3. SW846: 6010C MMSD 07/06/18 DM0706/18012405 3900 mg/kg D.W. 140 730 B8. SW846: 6010C MMSD 07/07/18 DM0707/18012416 4500 mg/kg D.W. 140 740 A0, B8, B9. SW846: 6010C MMSD SYSIWIMiloMonthly 1/10/13 h Page 77 of 106 Printed: 1/18/19 09: 9i 07/13/18 DM0713/18012876 4000 mg/kg D.W. 140 720 Annual Milorganite Report ehiliju MMSD 07/14/18 DM0714/18013220 3800 mg/kg D.W. January 1 to December 31, 2018 720 DM0816/18016300 SW846: 6010C MMSD 07/15/18 DM0715/18013239 RfR iCi KR A CtNe BloAlftf(? 140 730 08/19/18 SW846: 6010C MMSD POTASSIUM ICP METHOD DM0716/18013252 3400 mg/kg D.W. 140 720 3700 mg/kg D.W. SW846: 6010C MMSD 07/17/16 DM0717/18013751 3900 mg/kg D.W. 140 720 AO. SW846: 6010C MMSD 07/18/18 07/08/18 DM0708/18012435 4000 mg/kg D.W. 140 720 A0, B8, B9. SW846: 6010C MMSD 07/09/18 DM0709118012448 3800 mg/kg D.W. 140 740 A0, B8, 69. SW846: 6010C MMSD 07/10/18 DM0710/18012474 3800 mg/kg D.W. 140 740 A0, B8. SW846: 6010C MMSD 07/11/18 DM0711/18012820 3700 mg/kg D.W. 140 720 A0, B8, B9, Q3. SW846: 6010C MMSD 07/12/18 DM0712118012861 3900 mg/kg D.W. 140 720 B8, Q2. SW846: 6010C MMSD 07/13/18 DM0713/18012876 4000 mg/kg D.W. 140 720 A0, B9. SW846: 6010C MMSD 07/14/18 DM0714/18013220 3800 mg/kg D.W. 140 720 DM0816/18016300 SW846: 6010C MMSD 07/15/18 DM0715/18013239 3800 mg/kg D.W. 140 730 08/19/18 SW846: 6010C MMSD 07/16/18 DM0716/18013252 3400 mg/kg D.W. 140 720 3700 mg/kg D.W. SW846: 6010C MMSD 07/17/16 DM0717/18013751 3900 mg/kg D.W. 140 720 AO. SW846: 6010C MMSD 07/18/18 DM0718/18013961 3800 mg/kg D.W. 140 720 Q2.� SW846: 6010C MMSD 07/19/16 DM0719/18014047 3800 mg/kg D.W. 140 710 SW846: 6010C MMSD 07/20/18 DM0720118014062 4200 mg/kg D.W. 140 720 SW846: 6010C MMSD 07/21/18 DM0721/18014073 3900 mg/kg D.W. 140 720 SW846: 6010C MMSD 07/22/18 DM0722/18014483 3700 mg/kg D.W. 140 720 SW846: 6010C MMSD 07/23/18 DM0723/18014496 3600 mg/kg D.W. 140 730 SW846: 6010C MMSD 07/24/18 DM0724/18014523 3500 mg/kg D.W. 140 730 SW846: 6010C MMSD 07/25/18 DM0725/18014551 3600 mg/kg D.W. 140 740 AO. SW846-.6010C MMSD 07/26/18 DM0726/18014570 3900 mg/kg D.W. 140 730 A0, B8. SW846: 6010C MMSD 07/27/18 DM0727/18014585 3400 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 07/28/18 DM0728118014676 3600 mg/kg D.W. 140 710 SW846: 6010C MMSD 07/29/18 DM0729/18014910 3600 mg/kg D.W. 140 710 SW846: 6010C MMSD 07/30/18 DM0730/18014925 4200 mg/kg D.W. 140 730 Q3. SW846: 6010C MMSD 07/31/18 DM0731/18014954 3600 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 08/01/18 DM0801/18014969 3500 mg/kg D.W. 140 710 B8, B9. SW846: 6010C MMSD 06/02/18 DM0802/18015140 3500 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 06/03/18 DMO803118015155 3600 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 08/04/18 DMO804/18015252 3400 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/05/18 DMOB05/18015279 3500 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 08/06/18 DMOB06/18015385 3400 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/07/18 DM0807/18015414 3500 mg/kg D.W. 140 710 Q3. SW846: 6010C MMSD 08/08/18 DMO808/18015473 2800 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/09/18 DM0809/18015500 3000 mg/kg D.W. 140 710 SW846: 6010C MMSD 08/10/18 DMO810/18015899 3300 mg/kg D.W. 140 710 AO. SW846: 6010C MMSD 08/11/18 DM0811/18015910 3400 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/12/18 DM0812118016203 3400 mg/kg D.W. 08/13/18 DM0813118016216 3600 mg/kg D.W. 08/14/18 DM0814/18016254 3400 mg/kg D.W. 08/15/18 DM0815/18016281 4100 mg/kg D.W. 08/16/18 DM0816/18016300 5800 mg/kg D.W. 08/17/18 DMO817/18016365 5200 mg/kg D.W. 08/18/18 DMO818/18016505 4100 mg/kg D.W. 08/19/18 DMO819/18016525 3700 mg/kg D.W. 08/20/18 DM0820/18016539 3600 mg/kg D.W. 08/21/18 DM0821/18016714 3700 mg/kg D.W. 08/22/18 DM0822118016742 3500 mg/kg D.W. 08/23/18 DM0823/18017352 3600 mg/kg D.W. 140 710 B8. 140 710 B8. 140 140 140 140 140 710 B8, Q3. 710 B8. 710 A0, B8. 710 710 B8. SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD 140 140 710 710 B8. B8. SW846: 6010C SW846: 6010C MMSD MMSD 140 720 SW846: 6010C MMSD 140 710 B8, Q3. SW846: 6010C MMSD 130 700 BB, Q3. SW846: 6010C MMSD Page 78 of M SYSIrptlMMOMonthly 1/10/13 ry' Printed.., 1/18/19 09:4; 09/12/18 DMO912/18018854 09/13/18 DM0913/18018875 09/14/18 DMO914/18018891 09/15/18 DM0915/18019159 09/16/18 09/17/18 09/18/18 09/21/18 09/22/18 09/23/18 DMO916/18019178 DMO917/18019191 DMO918/18019447 DMO921/18019515 DMO922/18019574 DM0923/18019665 09/24/18 DMO924/18020088 09/25/18 DMO925/18020314 09/26/18 Annual Milorganite Report ei NNSD DM0927/18020364 09/28/18 DM0928/18020380 10/04/18 DM1004/18021541 January 1 to December 31, 2018 IIRam Is 1 CUANN ri, 10/06/18 DM1006/18021568 10/07/18 DM1007/18021588 10/08/18 DM1008/18021602 D.W. POT�ASSI�rUyM ICP METHOD 730 A0. 3800 mg/kg D.W. 140 1ilYlf+liilil��- �Samp)L' ID Result mg/kg , 140 710 A0, Q3. 08/24/18 DMO824118017367 3500 mg/kg D.W. 130 700 B8• SW846: 6010C MMSD 08/25/18 DMO825118017378 3600 mg/kg D.W. 140 710 88. SW846: 6010C MMSD 08/26/18 DMO826118017397 3400 mg/kg D.W. 130 700 138. SW846: 6010C MMSD 08/27/18 DMO827/18017410 3300 mg/kg D.W. 140 710 68. SW846: 6010C MMSD 08/28/18 DMO828/18017434 3500 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/29/18 DMO829/18017462 3400 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 08/30/18 DMOB30/18017483 3600 mg/kg D.W. 140 720 SW846: 6010C MMSD 08/31/18 DM0831/18017498 3300 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 09/01/18 DM0901/18017520 3500 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 09/02/18 DMO902118017752 3500 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 09/03/18 DMO903118018124 3600 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 09/04/18 DMO904/18018149 3600 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 09/05/18 DM0905118018305 3500 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 09/06/18 DMO906/18018326 3300 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 09/07/18 DMO907/18018342 3400 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 09/08/18 DMO908118018353 3500 mg/kg D.W. 140 710 A0. SW846: 6010C MMSD 09/09/18 DMO909/18018724 3500 mg/kg D.W. 140 710 A0. SW846: 6010C MMSD 09/10/18 DM0910/18018799 3600 mg/kg D.W. 140 720 AO. SW846: 6010C MMSD 09/11/18 DMO911/18018825 3800 mg/kg D.W. 140 720 AO, B9. SW846: 6010C MMSD 09/12/18 DMO912/18018854 09/13/18 DM0913/18018875 09/14/18 DMO914/18018891 09/15/18 DM0915/18019159 09/16/18 09/17/18 09/18/18 09/21/18 09/22/18 09/23/18 DMO916/18019178 DMO917/18019191 DMO918/18019447 DMO921/18019515 DMO922/18019574 DM0923/18019665 09/24/18 DMO924/18020088 09/25/18 DMO925/18020314 09/26/18 DMO926/18020343 09/27/18 DM0927/18020364 09/28/18 DM0928/18020380 09/29/18 DMO929/18020391 09/30/18 DMO930/18020411 10/01/18 DM1001/18021136 10/02/18 DM1002/18021162 10/03/18 DM1003/18021190 10/04/18 DM1004/18021541 10/05/18 DM1005/18021557 10/06/18 DM1006/18021568 10/07/18 DM1007/18021588 10/08/18 DM1008/18021602 3600 mg/kg D.W. 140 720 68, B9. 3700 mg/kg D.W. 140 730 AO, B8, Q3. 3700 mg/kg D.W. 140 730 B8. 3700 mg/kg D.W. 140 730 A0. 3800 mg/kg D.W. 140 720 AO. 4300 mg/kg D.W. 140 710 A0, Q3. 4400 mg/kg D.W. 140 740 B8, B9. 3500 mg/kg D.W. 130 700 B8, B9. 3800 mg/kg D.W. 140 710 B9. 3600 mg/kg D.W. 130 690 B9. SW846: SW846: 6010C 6010C MMSD MMSD SW846: 6010C MMSD T SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 3800 mg/kg D.W. 130 700 B9. SW846: 6010C MMSD 4400 mg/kg D.W. 140 710 B8, Q3. 4700 mg/kg D.W. 140 720 B8. 4800 mg/kg D.W. 140 720 4200 mg/kg D.W. 140 740 B8. 3900 mg/kg D.W. 140 720 AO, B8, B9. 4200 mg/kg D.W. 140 720 AO, B8, B9. 4400 mg/kg D.W. 140 710 AO, B8, B9. 4500 mg/kg D.W. 140 720 B8, B9. 4100 mg/kg D.W. 140 720 138. 4600 mg/kg D.W. 140 710 Q3. 5000 mg/kg D.W. 140 720 Q2. 4600 mg/kg D.W. 140 730 4300 mg/kg D.W. 130 700 4500 mg/kg D.W. 130 700 Q3. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 10/09/18 DM1009/18021627 4400 mg/kg D.W. 140 710 B8. SW846: 6010C MMSD 10/10/18 DM1010/18021656 5000 mg/kg D.W. 140 720 SW846: 6010C MMSD 10/11/18 DM1011118021975 4800 mg/kg D.W. 140 720 AO, B8, B9. SW846: 6010C MMSD Page 79 of 106 SYSIrpt- M IdNonthly 1/10/13 OF Printed: 1/18/19 09: 4i t 0 Annual Milorganite Report MMSD January 1 to December 31, 2018 a 1 Ci_IO R E1tfR 4�ilz POTASSIUM ICP METHOD 10/12/18 DM1012/18021991 4200 mg/kg D.W. 140 710 AO. SW846: 6010C MMSD 10/13/18 DM1013118022006 4400 mg/kg D.W. 140 720 AO, B8. SW846: 6010C MMSD 10/14/18 DM1014118022026 4400 mg/kg D.W. 140 720 AO, B8. 10/15/18 'f DM1015/18022040 4200 mg/kg D.W. 140 720 AO, B8. 10/16/18 DM1016118022065 4300 mg/kg D.W. 140 720 B8, Q3. 10/17/18 DM1017/18022094 4000 mg/kg D.W. 140 720 AO, B9, Q3. 10/18/18 DM1018/18022133 4000 mg/kg D.W. 140 710 AO, B8. 10/19/18 DM1019/18022269 4000 mg/kg D.W. 140 730 68. 10/20/18 DM1020/18022280 3600 mg/kg D.W. 140 710 10/21/18 DM1021118022435 3600 mg/kg D.W. 140 720 T 10/22/18 DM1022/18022449 3600 mg/kg D.W. 140 710 10/23/18 DM1023118022614 3500 mg/kg D.W. 140 720 B8. 10/24/18 DM1024/18022643 3600 mg/kg D.W. 140 720 68. 10/25/18 DM1025/18022708 4000 mg/kg D.W. 140 720 B8. 10/26/18 DM1026/18022767 3600 mg/kg D.W. 140 720 A0, B8, Q3. 10/27/18 DM1027/18022778 3900 mg/kg D.W. 130 700 AO, B8. 11/07/18 DMI 107/18023991 2700 mg/kg D.W. 130 700 B8. 11/08/18 DM 1108/18024012 2800 mg/kg D.W. 140 710 68. 11/09/18 DM 1109/18024028 2800 mg/kg D.W. 140 710 B8. 11/10/18 DM 1110/18024523 3400 mg/kg D.W. 130 700 AO, 88. 11/11/18 DM 1111/18024619 3500 mg/kg D.W. 130 700 AO, 88. 11/12/18 DM 1112/18024633 3400 mg/kg D.W. 140 720 AO, B8. 11/13/18 DM 1113/18025014 3600 mg/kg D.W. 140 720 AO, B8. 11/14/18 DM 1114/18025043 3700 mg/kg D.W. 140 730 AO, B8, B9. 11/15/18 DM 1115/18025064 3400 mg/kg D.W. 140 720 AO, B8. 11/16/18 11/17/18 11/18/18 11/19/18 11/20/18 11/21/18 11/22/18 11/23/18 11/24/18 11/27/18 11/28/18 DM 1116/18025080 DM 1117/18025093 DM 1118/18025113 DM 1119/18025127 DM 1120/18025356 DM 1121 /18025385 DM1122/18025406 DM 1123/18025422 DMI 124/18025750 DM1125/18025769 DM1126/18025828 DM 1127/18025860 DM 1128118025888 11/29/18 DM1129/18025956 11/30/18 DM1130/18025971 12/01/18 DM1201/18026182 12/02/18 DM1202118026201 12/03/18 DM1203/18026214 12/04/18 DM1204/18026391 12/05/18 12/06/18 3700 mg/kg D.W 3600 mg/kg D.W 3900 mg/kg D.W 3800 mg/kg D.W 3900 mg/kg D.W 4200 mg/kg D.W 3800 mg/kg D.W. 3800 mg/kg D.W. 3800 mg/kg D.W. 3800 mg/kg D.W. 3500 mg/kg D.W. 3400 mg/kg D.W. 3800 mg/kg D.W. 140 750 140 720 140 740 140 720 140 710 140 720 140 730 140 720 140 740 140 740 140 710 140 710 140 710 AO, B9. B9 B8 B8, Q3. B8. B8. B8. B8. 88. B8. 89. - SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846:6010C MMSD SW846: 6010C MMSD 4600 mg/kg D.W. 140 720 A0. SW846: 6010C 4300 mg/kg D.W. 140 `730 88. SW846: 6010C 4200 mg/kg D.W. 140 730 A0, B8. SW846: 6010C 4100 mg/kg D.W. 140 720 AO, B8. SW846: 6010C 4000 mg/kg D.W. 140 720 AO, B8. SW846: 6010C 3900 mg/kg D.W. 140 730 AO, 88. DM1205/18026578 4200 mg/kg D.W. 140 730 B8. DM1206/18026621 4100 mg/kg D.W. 140 750 B8, Q3. DM1207/18026797 4000 mg/kg D.W. 140 750 B8, B9. SYS/rptIlOoMonthly 1/10/13 tj SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD Page 80 of 106 Printed: 1/18/19 09:47 'e-kNSD Annual Milorganite Report January 1 to December 31, 2018 PUAW KA, nlwf 1i11MDllull8 POTASSIUM ICP METHOD 12/08/18 'ReSult DM1208/18026808 3600 mg/kg D.W. LOD 140 LGQ 740 QA Flags B8. Analytical Method SW846: 6010C Lab MMSD 12/09/16 DM1209/18026827 3500 mg/kg D.W. 140 730 B8. SW846: 6010C MMSD 12/10/18 DM1210/18026840 3600 mg/kg D.W. 140 760 B8. SW846: 6010C MMSD 12/11/18 DM1211118027102 3400 mg/kg D.W. 140 720 SW846: 6010C MMSD 12/12/18 DM1212/18027130 3700 mg/kg D.W. 140 710 SW846: 6010C MMSD 12/13/18 DM1213/18027253 4200 mg/kg D.W. 140 730 88. SW846: 6010C MMSD 12/14/18 DM1214118027306 4300 mg/kg D.W. 140 720 SW846: 6010C MMSD 12/15/18 DM1215/18027317 4200 mg/kg D.W. 140 720 B8. SW846: 6010C MMSD 12/16/18 DM1216/18027525 4300 mg/kg D.W. 140 740 88. SW846: 6010C MMSD 12/17/18 DM1217/18027540 4200 mg/kg D.W. 140 750 B8. SW846: 6010C MMSD 12/18/18 DM1218/18027643 4200 mg/kg D.W. 140 760 AO, B8. SW846: 6010C MMSD 12/19/18 DM1219/18027676 4000 mg/kg D.W. 140 730 A0, B8. SW846: 6010C MMSD 12/20/18 DM1220/18027805 3800 mg/kg D.W. 140 720 A0, 88. SW846: 6010C MMSD 12/21/18 DM1221/18027821 4200 mg/kg D.W. 140 730 SW846: 6010C MMSD 12/22/18 DM1222/18027832 3500 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD 12/23/18 DM1223/18027852 3400 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD 12/24/18 DM1224118027883 3600 mg/kg D.W. 140 740 B8. SW846: 6010C MMSD 12/25/18 DM1225/18027952 3700 mg/kg D.W. 140 750 B8. SW846: 6010C MMSD 12/26/18 DM1226118027969 12/27/18 DM1227/18027990 12/28/18 12/29/18 12/30/18 12/31/18 DM1228/18028005 3700 mg/kg D.W. 140 750 B8. 4300 mg/kg D.W. 140 750 AO, B8. 4100 mg/kg D.W. 140 760 A0, B8. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD DM1229/18028070 3300 mg/kg D.W. 140 730 SW846: 6010C DM1230/18028089 3700 mg/kg D.W. 140 720 SW846: 6010C DM1231/18028102 3900 mg/kg D.W. 140 730 SW846: 601DC Avg Result: 4300 mg/kg D.W. Min LOD: 62 mg/kg D.W. Max Result: 6800 mg/kg D.W. MMSD MMSD MMSD Page 81 of 106 SYS/rptZMlloMonthly 1/10/13 (f Printed: 1/18/19 09:4; f V MMSD MTN KR J CtUM tVRWM, SELENIUM ICP METHOD 01/01/18 DMO101/18000013 01/02/18 DM0102/18000047 Annual Milorganite Report ]anuary 1 to December 31, 2018 9.7 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 5.3 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 01/03/18 DMO103/18000061 6.7 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 01/04/18 DM0104/18000098 8.1 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/05/18 DMO105/18000155 9 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 01/06/18 DMO106/18000168 4.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/07/18 DM0107116000189 4.7 mg/kg D.W. 4.1 13 J. SW846: 6010C F MMSD 01/08/18 DM0108/1 8000203 < 4.1 mg/kg D.W. 4.1 13 SW846: 6010C MMSD 01/09/18 DM0109/18000232 4.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/10/18 DM0110/18000326 4.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/11/18 DM0111/18000347 6.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/12/18 DM0112/18000363 7.1 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/13/18 DM0113/18000397 4.9 mg/kg D.W. 4.1 13 ] SW846: 6010C MMSD 01/14/18 DM0114/18000418 4.5 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/15/18 DM0115/18000432 6.6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/16/18 DM0116/18000461 5.2 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/17/18 DM0117/18000652 4.8 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/18/18 DMO118/18000673 6.6 mg/kg D.W. 4.1 13 ]. SW846: 6010C MMSD 01/19/18 DM0119/18000689 5.8 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 01/20/18 DMO120/18000702 <4.1 mg/kg D.W. 4.1 13 SW846: 6010C MMSD 01/21/18 DMO121/18000800 < 4.1 mg/kg D.W. 4.1 13 SW846: 6010C MMSD 01/22/18 DMO122/18000814 < 4.2 mg/kg D.W. 4.2 13 SW846: 6010C MMSD 01/23/18 DMO123118000843 < 4.2 mg/kg D.W. 4.2 13 SW846: 6010C MMSD 01/24/18 DMO124/18000875 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/25/18 DMO125/18000896 4.8 mg/kg D.W. 4 12 J. SW846: 6010C MMSD 01/26/18 DMO126118000912 5.2 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 01/27/18 DMO127/18000925 4.6 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 01/28/18 DMO128/18000946 4.S mg/kg D.W. 4 12 J. SW846: 6010C MMSD 01/29/18 DMO129/18001200 4.6 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 01/30/18 DMO130/18001229 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 01/31/18 DMO131/18001259 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 02/01/18 DM0201/18001280 4.6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/02/18 DM0202/18001421 5.9 mg/kg D.W. 4 13 ]. SW846: 6010C MMSD 02/03/18 DM0203/18001434 6.3 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/04/18 DM0204/18001455 5.6 mg/kg D.W. 4.1 13 ]. SW846: 6010C MMSD 02/05/18 DM0205118001469 6.5 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/06/18 DM0206/18001506 7.2 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/07/18 DM0207/18001599 5.6 mg/kg D.W. 4.1� 13 3. SW846: 6010C MMSD 02/08/18 DM0208/18001620 < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 02/09/18 DM0209/18001738 T < 4 mg/kg D.W. 4 13 SW846: 6010C MMSD 02/10/18 DM0210/18001751 6.1 mg/kg D.W. 4 13 ]. SW846: 6010C MMSD 02/11/18 DM0211/18001772 4.9 mg/kg D.W. 4.1 13 J. SW846: 6010C _ MMSD 02/12/18 DM0212/18001786 5.2 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/13/18 DM0213/18001815 4.9 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 02/14/18 DM0214/18001860 5.4 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/15/18 DM0215/18001881 7.9 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/16/18 DM0216/18001897 6.8 mg/kg D.W. 4 13 J. SW846: 6010C MMSD Page 82 of 106 SYSIWIMilaMonthly 1/10/13 U Printed: 1/18/19 09:4; 03/20/18 DM0320118003938 03/21/18 03/22/18 DM0321118003967 DM0322/18004111 03/23/18 Annual Milorganite Report MMSDJanuary DM0324/18004137 03/25/18 DM0325/18004156 03/26/18 DM0326/18004320 1 to December 31, 2018 r�rW Re 1 WMR w1 03/28/18 DM0328/18004376 5.1 mg/kg D.W. 4.1 13 J, Q3. 5.3 mg/kg D.W. EL�SELENIUM�UM ICP METHOD J. 5.4 mg/kg D.W. 4.2 13 J. 13 Ii1�Wlriiliiili� 02/17/18 Sample ID DM0217/18001944 Result < 4.1 mg/kg D.W. LOD 4.1 LOQ 13 QA Flap Analytkal Method SW846: 6010C Lab MMSD 02/18/18 DM0218/18001965 4.7 mg/kg D.W. 4.1 13 1 SW846: 6010C MMSD 02/19/18 DM0219/18001979 5.3 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/20/18 DM0220/18002047 6.2 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/21/18 DM0221118002077 4.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/22/18 DM0222118002097 8.2 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/23/18 DM0223118002415 8.1 mg/kg D.W. 4 12 J. SW846: 6010C MMSD 02/24/18 DM0224/18002427 6.4 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/25/18 DM0225/18002447 8 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/26/18 DM0226/18002461 6.3 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 02/27/18 DM0227/18002537 5.6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 02/28/18 DM0228/18002609 5.3 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/01/18 DM0301118002628 5.8 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/02/18 DM0302/18002711 6.5 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/03/18 DM0303/18002722 6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/04/18 DM0304/18002741 5.9 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/05/18 DM0305/18002805 5.3 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/06/18 DM0306/18002862 4.9 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/07/18 DM0307/18002927 6.4 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/08/18 DM0308/18003015 5.7 mg/kg D.W. 4.1 13 �1. SW846: 6010C MMSD 03/09/18 DM0309/18003030 7 mg/kg D.W. 4 13 J. SW846: 6010C MMSD 03/10/18 DM0310/18003041 5.7 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/11/18 DM0311/18003060 6.6 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/12/18 DM0312/18003335 7.8 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/13/18 DM0313/18003681 9.9 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/14/18 DM0314/18003710 7.8 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/15/18 DM0315/18003729 5.6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/16/18 DM0316/18003744 6.3 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/17/18 i DM0317118003755 8 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/18/18 DM0318118003780 11 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 03/19/18 DM0319118003911 6.5 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 03/20/18 DM0320118003938 03/21/18 03/22/18 DM0321118003967 DM0322/18004111 03/23/18 DM0323118004126 03/24/18 DM0324/18004137 03/25/18 DM0325/18004156 03/26/18 DM0326/18004320 03/27/18 DM0327/18004347 03/28/18 DM0328/18004376 7.4 mg/kg D.W. 4.1 13 J. 5.8 mg/kg D.W. < 4 mg/kg D.W. 5.5 mg/kg D.W. 4.2 4 4 13 13 13 J. J. y < 4.2 mg/kg D.W. 4.2 13 4.2 5.6 mg/kg D.W. 4.2 13 J. 5.1 mg/kg D.W. 4.1 13 J, Q3. 5.3 mg/kg D.W. 4.2 13 J. 5.4 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 03/29/18 DM0329/18004395 < 4.1 mg/kg D.W. 4.1 13 B8. SW846: 6010C MMSD 03/30/18 DM0330/18004410 4.5 mg/kg D.W. 4.2 13 B8, J. SW846: 6010C MMSD 03/31/18 DM0331/18004752 6.6 mg/kg D.W. 4.1 13 J. SW846: 6010C MMSD 04/01/18 DM0401/18004771 7.5 mg/kg D.W. 4.2 13 J. SW846: 6010C MMSD 04/02/18 04/03/18 DM0402118004784 DM0403/18004943 7.2 mg/kg D.W. < 7.1 mg/kg D.W. 4.1 7.1 13 21 1 SW846: 6010C SW846: 6010C MMSD MMSD 04/04/18 DM0404/1B004972 <6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD SY51WIMMoNanthly 1110/13 L7 Page 83 of 106 Printed: 1/18/19 09:47 IN Page 84 of 106 SYS/rptiMiloMonthly 1/10/13 U Printed: 4418/19 09:4) Annual Milorganite Report e-1414SD January 1 to December 31, 2018 W- T" HN a C1tu R WNW, SELENIUM ICP METHOD 04/05/18 DM0405118005037 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 04/06/18 DM0406/18005052 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 04/07/18 DM0407/18005063 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 04/08/18 DM0408/18005082 7.8 mg/kg D.W. 7.2 21 J. SW846: 6010C MMSD 04/09/18 DM0409/18005095 7.6 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 04/10/18 DM0410/18005164 7.9 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 04/11/18 DM0411118005193 < 7.1 mg/kg D.W. 7.1 21 SW846: 6010C MMSD 04/12/18 DM0412/18005446 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 04/13/18 DM0413/18005463 7.2 mg/kg D.W. 7 21 J. SW846: 60100 MMSD 04/14/18 DM0414/18005474 8.3 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 04/15/18 DM0415/18005605 7.5 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 04/16/18 DM0416/18005618 10 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 04/17/18 DM0417/18005709 9.4 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 04/18/18 DM0418/18005738 8.4 mg/kg D.W. 7 21 T J. SW846: 6010C MMSD 04/19/18 DM0419/18005757 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 04/20/18 DM0420/18006009 6.9 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 04/21/18 DM0421118006020 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 04/22/18 DM0422/18006039 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 04/23/18 DM0423/18006157 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 04/24/18 DM0424/18006185 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 04/25/18 DM0425/18006214 < 7.2 mg/kg D.W. 7.2 21 Q2. SW846: 6010C MMSD 04/26/18 DM0426/18006233 12 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 04/27/18 DM0427/18006441 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 04/28/18 DM0428/18006452 7.3 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 04/29/18 DM0429/18006471 7.3 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 04/30/18 DM0430/18006484 8.7 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 05/01/18 DM0501/18006571 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 05/02/18 DMO502118006600 9.4 mg/kg D.W. 7 21 1 SW846: 6010C MMSD 05/03/18 DMO503/18006854 7.8 mg/kg D.W. 6.6 20 J. SW846: 6010C MMSD 05/04/18 DM0504/18007005 7.4 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 05/05/18 DMO505/18007016 7.4 mg/kg D.W. 6.8 20 3. SW846: 6010C MMSD 05/06/18 DM0506/18007035 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 05/07/18 DM0507/18007257 7.3 mg/kg D.W. 6.8 20 S1 J. SW846: 6010C MMSD 05/08/18 DM0508/18007284 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 05/09/18 DM0509/18007313 7.3 mg/kg D.W. 6.9 20 - J. i i - ! SW846: 60100 MMSD 05/10/18 DM0510/18007340 7.7 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 05/11/18 DMO511/18007418 < 7.1 mg/kg D.W. 7.1^ 21 SW846: 6010C MMSD 05/12/18 DM0512118007429 8 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 05/13/18 DM0513/18007476 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 05/14/18 DMO514/18007591 7.8 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 05/15/18 DMO515118007976 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 05/16/18 DM0516/18008005 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 05/17/18 DMO517/18008103 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 05/18/18 DM0518/18008118 7.4 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 05/19/18 DM0519/18008129 7.1 mg/kg D.W. 7 21 3. SW846: 6010C MMSD 05/20/18 DM0520118008196 < 6.9 mg/kg D.W. 6.9 21 SW846: 6010C MMSD 05/21/18 DMO521/18008209 9 mg/kg D.W. 7 21 3. i SW846: 6010C MMSD Page 84 of 106 SYS/rptiMiloMonthly 1/10/13 U Printed: 4418/19 09:4) 'e-OMSD Annual Milorganite Report January 1 to December 31, 2018 KnW rA i sup• l SELENIUM ICP METHOD GriillfiYil . 05/22/18 7- Sample ID DM0522/18008236 Result < 7.1 mg/kg D.W. LOD 7.1 LDQ 21 QA Flags Anafybwl we�t�� SW846: 6010C MMSD 05/23/18 DM0523/18008304 7.2 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 05/24/18 DM0524/18008658 8.9 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 05/25/18 DM0525/18008673 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 05/26/18 DMO526/18008684 9.3 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 05/27/18 DM0527/18008703 8.2 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 05/28/18 DM0528/18008716 < 7.1 mg/kg D.W. 7.1 21 SW846: 6010C MMSD 05/29/18 DM0529118008888 8 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 05/30/18 DMO530/18008917 < 6.8 mg/kg D.W. 6.8 20 B8. SW846: 6010C MMSD 05/31/18 DM0531/18008936 8.6 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 06/01/18 DM0601/18009150 7 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 06/02/18 DMO602118009161 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 06/03/18 DM0603/18009335 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 06/04/18 DM0604/18009348 6.8 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 06/05/18 DM0605/18009375 9.2 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 06/06/18 DM0606/18009404 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 06/07/18 DM0607/18009423 8.3 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 06/08/18 DM0608/18009822 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 06/09/18 DM0609118009833 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 06/10/18 DM0610/18009852 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 06/11/18 DM0611/18009865 9.9 mg/kg D.W. 7 21 J, Q3. SW846: 6010C MMSD 06/12/18 DM0612/18010098 < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD 06/13/18 DM0613/18010127 < 7 mg/kg D.W. 7 21 88. SW846: 6010C MMSD 06/14/18 DM0614/18010437 < 6.9 mg/kg D.W. 6.9 20 B7, B9. SW846: 6010C MMSD 06/15/18 DM0615/18010452 < 6.8 mg/kg D.W. 6.8 20 Q3. SW846: 6010C MMSD 06/16/18 DM0616/18010463 < 6.8 mg/kg D.W. 6.8 20 B8, B9. SW846: 6010C MMSD 06/17/18 DM0617/18010482 < 6.8 mg/kg D.W. 6.8 20 B8, B9. SW846: 6010C MMSD 06/18/18 DM0618/18010639 < 6.9 mg/kg D.W. 6.9 20 B8, B9, D2, Q3. SW846: 6010C MMSD 06/19/18 DM0619/18010666 9.1 mg/kg D.W. 6.9 21 J. SW846: 6010C MMSD 06/20/18 DM0620/18010694 < 6.7 mg/kg D.W. 6.7 20 D2, Q2. SW846: 6010C MMSD 06/21/18 DM0621/18010713 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 06/22/18 DM0622118010939 < 6.7 mg/kg D.W. 6.7 20 Q2. SW846: 6010C MMSD 06/23/18 DMO623118010950 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 06/24/18 DM0624/18011087 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 06/25/18 DM0625/18011182 < 6.8 mg/kg D.W. 6.8 20 D2. SW846: 6010C MMSD 06/26/18 DM0626/18011209 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 06/27/18 DM0627/18011597 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 06/28/18 DM0628/18011616 < 6.8 mg/kg D.W. 6.8 20 B8. SW846: 6010C MMSD 06/29/18 DM0629/18011631 < 6.9 mg/kg D.W. 6.9 20 D2, Q2. SW846: 6010C MMSD 06/30/18 DM0630118011642 9.1 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 07/01/18 DM0701/18011728 7.4 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 07/02/18 DM0702/18011741 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 07/03/18 DM0703/18011881 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 07/04/18 DM0704/18011909 7.7 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 07/05/18 DM0705/18012390 8.9 mg/kg D.W. 6.8 20 J, Q3. SW846: 6010C MMSD 07/06/18 DM0706/18012405 < 6.9 mg/kg D.W. 6.9 20 B8. SW846: 6010C MMSD 07/07/18 DM0707118012416 9.2 mg/kg D.W. 6.9 21 J. SW846: 6010C MMSD Page 85 of 106 SYS/rptlMl/oMonthly 1/10/13 t/ Printed: 1/18/19 09:47 0 eMNSD firram U* I NUM I SELENIUM ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 07/13/18 DM0713/18012876 J 11131111931=- DM0714/18013220 DM0715/18013239 07/16/18 DM0716118013252 _ - 07/08/18 DM0708118012435 12 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 07/09/18 DM0709/18012448 8.5 mg/kg D.W. 7 21 J. SW846: 6010C MMSD 07/10/18 DM0710/18012474 9.9 mg/kg D.W. 6.9 20 1, Q3. SW846: 6010C MMSD 07/11/18 DM0711/18012820 6.8 mg/kg D.W. 6.8 20 B8, 1. SW846: 6010C MMSD 07/12/18 DM0712/18012861 < 6.8 mg/kg D.W. 6.8 20 B9, Q2. SW846: 6010C MMSD 07/13/18 DM0713/18012876 J 07/14/18 07/15/18 DM0714/18013220 DM0715/18013239 07/16/18 DM0716118013252 07/17/18 DM0717/18013751 07/18/18 07/19/18 07/20/18 DM0718/18013961 DM0719/18014047 l DM0720118014062 07/21/18 DM0721/18014073 07/22/18 DM0722/18014483 07/23/18 DM0723/18014496 07/24/18 DM0724/18014523 07/25/18 DM0725/18014551 07/26/18 DM0726/18014570 07/27/18 DM0727/18014585 07/28/18 DM0728/18014676 07/29/18 DM0729/18014910 07/30/18 DM0730/18014925 07/31/18 DM0731/18014954 08/01/18 DM0801/18014969 08/02/18 08/03/18 08/04/18 08/05/18 08/06/18 08/07/18 08/08/18 08/09/18 08/10/18 08/11/18 DMO802/18015140 DM0803/18015155 DMO804/18015252 DM0805/18015279 DM0806/18015385 DM0807/18015414 DM0808/18015473 DM0809/18015500 DM0810/18015899 DM0811/18015910 < 6.8 mg/kg D.W. 6.8 20 B8. 11 mg/kg D.W. 6.7 20 1 9 mg/kg D.W. 6.8 20 1. 10 mg/kg D.W. 6.8 20 J. 11 mg/kg D.W. 6.7 20 1. - - - 8.4 mg/kg D.W. 6.8 20 1. - - 8.7 mg/kg D.W. 6.7 20 J. 7.8 mg/kg D.W. 6.8 20 1. 7.6 mg/kg D.W. 6.8 20 1. 6.8 mg/kg D.W. 6.8 20 J. < 6.9 mg/kg D.W. 6.9 20 Q2. 7.1 mg/kg D.W. 6.8 20 1. 8 mg/kg D.W. 6.9 21 1. < 6.9 mg/kg D.W. 6.9 20 MMSD < 6.8 mg/kg D.W. 6.8 20 6.8 6.7 6.6 < 6.7 mg/kg D.W. 6.7 20 MMSD MMSD MMSD < 6.7 mg/kg D.W. 6.7 20 10 mg/kg D.W. 6.9 20 1. 12 mg/kg D.W. 6.8 20 B7, 1, Q3. < 6.7 mg/kg D.W. 6.7 20 7.2 mg/kg D.W. 6.7 20 1, Q3. < 6.8 mg/kg D.W. 6.8 20 D2, Q2. < 6.7 mg/kg D.W. 6.7 20 6.7 < 6.8 mg/kg D.W. 6.8 20 MMSD < 6.7 mg/kg D.W. 6.7 20 - - < 6.7 mg/kg D.W. 6.7 20 MMSD < 6.7 mg/kg D.W. 6.7 20 B7. - - - 7.5 mg/kg D.W. 6.7 20 J. < 6.7 mg/kg D.W. 6.7 20 6.7 7.3 mg/kg D.W. 6.7 20 1. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C c�n�onc. cm nr• SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD nnnncn MMSD MMSD MMSD MMSD 08/12/18 08/13/18 DM0812/18016203 DMO813/18016216 8.2 mg/kg D.W. 7.4 mg/kg D.W. 6.7 6.7 20 20 1. J. SW846: 6010C SW846: 6010C MMSD MMSD 08/14/18 DM0814/18016254 < 6.7 mg/kg D.W. 6.7 20 B7, D2. SW846: 6010C MMSD 08/15/18 DM0815/18016281 10 mg/kg D.W. 6.7 20 D2, J, Q3. SW846: 6010C MMSD 08/16/18 08/17/18 DMO816/18016300 DM0817/18016365 < 6.6 mg/kg D.W. < 6.7 mg/kg D.W. 6.6 6.7 20 20 SW846: 6010C SW846: 6010C MMSD MMSD 08/18/18 DMO818/18016505 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 08/19/18 DMOB19/18016525 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 08/20/18 DM0820/18016539 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 08/21/18 08/22/18 08/23/18 - DMOS21/18016714 DM0822/18016742 DM0823/18017352 7.1 mg/kg D.W. < 6.7 mg/kg D.W. < 6.6 mg/kg D.W. 6.8 6.7 6.6 20 20 20 J. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 5YS/rpf1M11oMonth1y 1/10/13 ti Page 86 of 106 Printed: 1/18/19 09:47 'tONSD DMO828/18017434 8.5 mg/kg D.W. 6.7 Annual Milorganite Report J. SW846: 6010C MMSD 08/29/18 DMOB29/18017462 < 6.7 mg/kg D.W. January 1 to December 31, 2018 nPW P4 t I'MVf IP SW846: 60100 MMSD 08/30/18 SELENIUM ICP METHOD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 08/24/18 DM0824/18017367 08/25/18 DM0825/18017378 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 08/26/18 DM0826118017397 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 08/27/18 DMO827/18017410 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 08/28/18 DMO828/18017434 8.5 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 08/29/18 DMOB29/18017462 < 6.7 mg/kg D.W. 6.7 20 SW846: 60100 MMSD 08/30/18 DM0830/18017483 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 08/31/18 DM0831/18017498 8.2 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 09/01/18 DMO901118017520 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 09/02/18 DMO902/18017752 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 09/03/18 DMO903/18018124 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 09/04/18 DM0904/18018149 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/05/18 DMO905/18018305 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/06/18 DMO906/18018326 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/07/18 DMO907/18018342 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD D9/08/18 DM0908/18018353 6.9 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD 09/09/18 DM0909/18018724 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 09/10/18 T DM0910/18018799 8.4 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 09/11/18 DM0911/18018825 < 6.8 mg/kg D.W. 6.8 20 Q2. SW846: 6010C MMSD 09/12/18 DM0912118018854 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/13/18 DMO913/1 B018875 < 6.9 mg/kg D.W. 6.9 20 B8. SW846: 6010C MMSD 09/14/18 DMO914/18018891 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 09/15/18 DM0915/18019159 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/16/18 DMO916/18019178 7.2 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 09/17/18 DM0917/18019191 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 09/18/18 DMO918118019447 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 09/21/18 DMO921/18019515 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 09/22/18 DM0922118019574 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 09/23/18 DM0923/18019665 7.2 mg/kg D.W. 6.5 19 J. SW846: 6010C MMSD 09/24/18 DMO924/18020088 < 6.6 mg/kg D.W. 6.6 20 Q2. SW846: 6010C MMSD 09/25/18 DM0925/18020314 < 6.7 mg/kg D.W. 6.7 20 SW646: 6010C MMSD 09/26/18 DM0926118020343 < 6.8 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 09/27/18 DM0927/18020364 < 6.8 mg/kg D.W. 6.8 20 87, Q2. SW846: 6010C MMSD 09/28/18 DMO928/18020380 < 7 mg/kg D.W. 7 21 68, Q3. SW846: 6010C MMSD 09/29/18 DM0929/18020391 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 09/30/18 DM0930/18020411 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 10/01/18 DM1001/18021136 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 10/02/18 DM1002/18021162 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 10/03/18 DM1003/18021190 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 10/04/18 DM 1004/18021541 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 10/05/18 DM1005/18021557 < 6.8 mg/kg D.W. 6.8 20 D2, Q3. SW846: 6010C MMSD 10/06/18 DM1006/18021568 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 10/07/18 DM1007/lB021588 < 6.6 mg/kg D.W. 6.6 20 SW846: 6010C MMSD 10/08/18 DM1008/18021602 < 6.6 mg/kg D.W. 6.6 20 Q2. SW846: 6010C MMSD 10/09/18 DM1009/18021627 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 10/10/18 DM1010/18021656 7.4 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 10/11/18 DM1011/18021975 6.9 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD Page 87 of 106 SYSImUmiloMonthly 1/10/13 0 Printed.• 1/18/19 09:47 1414 S V 4i.R'IR RRdrifisR RT SELENIUM ICP METHOD 10/12/18 DM1012/18021991 10/13/18 DM1013/18022006 10/14/18 DM1014/18022026 10/15/18 DM1015/18022040 10/16/18 DM1016/18022065 10/17/18 DM1017/18022094 10/18/18 DM1018/18022133 10/19/18 DM1019/18022269 10/20/18 DM1020/18022280 10/21/18 10/22/18 OM1021/18022435 J DM1022/18022449 10/23/18 DM1023/18022614 10/24/18 DM1024/18022643 10/25/18 DM1025/18022708 10/26/18 DM1026/18022767 10/27/18 DM1027/18022778 11/07/18 DM1107/18023991 11/08/18 DM1108/18024012 11/09/18 OM1109/18024028 11/10/18 DM1110/18024523 11/11/18 DM 1111/18024619 11/14/18 DM1114/18025043 11/15/18 DM1115/18025064 11/16/18 11/17/18 11/18/18 11/19/18 11/20/18 11/21/18 11/22/18 11/23/18 11/24/18 11/25/18 11/26/18 11/27/18 11/28/18 11/29/18 12/02/18 12/03/18 12/04/18 12/05/18 12/06/18 12/07/18 DM1116118025080 DMI 117/18025093 DM 1 118/18025113 DM 1119/18025127 DM1120/18025356 DM1121/18025385 DM 1122/18025406 DM 1123/18025422 DM 1124/18025750 DM 1125/18025769 DMI 1 26/1 8025828 DM 1127/18025860 DM 1128/18025888 DM 1129/18025956 DM 1 130/18025971 DM 1201 / 18026182 DM1202118026201 DM1203/18026214 DM1204/18026391 ^ DM1205/18026578 DM 1206/18026621 Annual Milorganite Report January 1 to December 31, 2018 8.3 mg/kg D.W. 6.7 20 J. SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 7.9 mg/kg D.W. 6.8 20 J. 7 mg/kg D.W. 6.7 20 J. - 9.7 mg/kg D.W. 6.8 20 J. < 6.7 mg/kg D.W. 6.7 20 < 6.7 mg/kg D.W. 6.7 20 < 6.7 mg/kg D.W. 6.7 20 MMSD < 6.8 mg/kg D.W. 6.8 20 D2, Q3. < 6.8 mg/kg D.W. 6.8 20 D2, Q2. < 6.8 mg/kg D.W. 6.8 20 MMSD MMSD < 6.7 mg/kg D.W. 6.7 20 6.7 < 6.6 mg/kg D.W. 6.6 20 MMSD 8.5 mg/kg D.W, 6.6 20 J. < 6.6 mg/kg D.W. 6.6 20 6.8 < 6.7 mg/kg D.W. 6.7 20 f < 6.6 mg/kg D.W. 6.6 20 6.9 mg/kg D.W. 6.6 20 J. 7.4 mg/kg D.W. 6.8 20 J. 7.5 mg/kg D.W. 6.8 20 J. - -- 8.6 mg/kg D.W. 6.9 20 J. < 6.8 mg/kg D.W. 6.8 20 MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C SW846:6010C MMSD MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD < 6.8 mg/kg D.W.6.8 20 SW846: 6010C MMSD < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD < 6.7 mg/kg D.W. 6.7 20 SW646: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 7.1 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD < 7 mg/kg D.W. 7 21 SW846: 6010C MMSD �7.8 mg/kg D.W. 7 21 J. SW846:6010C MMSD < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD < 6.7 mg/kg D.W. 6.7 20 Q2. SW846: 6010C MMSD < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 Q2. SW846: 6010C MMSD 8.4 mg/kg D.W. 6.8 20 J. SW846: 6010C MMSD 7.7 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 9.5 mg/kg D.W. 6.9 20 J. SW846: 6010C MMSD 9.6 mg/kg D.W. 7.1 21 J. SW846: 6010C MMSD DM1207/18026797 8.6 mg/kg D.W. 7 21 J. SYS/rptlMrloMonthly 1/10/13 0 SW846:6010C MMSD Page 88 o/ 106 Printed: 1/18/19 09:4; - - DM1223/18027852 12/24/18 12/25/18 DM1224/18027883 DM1225/18027952 Annual Milorganite Report DM1226/18027969 MSDJanuary DM1227118027990 12/28/18 DM1228/18028005 12/29/18 1 to December 31, 2018 gmRrt Q4 DM1230/18028089 12/31/18 DM1231/18028102 7 21 J. SELENIUM ICP METHOD < 7.1 mg/kg D.W. 7.1 21 sampomw Sample ID Result .. O -Q QA Vags Analytkal Method J 13 mg/kg D.W. 6.7 20 J. 12/08/18 DM1208118026808 < 6.9 mg/kg D.W. 6.9 21 SW846: 6010C MMSD 12/09/18 DM1209118026827 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 12/10/18 DM1210/18026840 < 7.1 mg/kg D.W. 7.1 21 SW846: 6010C MMSD 12/11/18 DM1211/18027102 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 12/12/18 DM1212/18027130 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 12/13/18 DM1213/18027253 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 12/14/18 DM1214/18027306 < 6.7 mg/kg D.W. 6.7 20 SW846: 6010C MMSD 12/15/18 DM1215/18027317 < 6.8 mg/kg D.W. 6.8 20 SW846: 6010C MMSD 12/16/18 DM1216/18027525 < 6.9 mg/kg D.W. 6.9 20 SW846: 6010C MMSD 12/17/18 12/18/18 12/19/18 12/20/18 12/21/18 12/22/18 DM 1217/18027540 DM1218/18027643 DM1219/18027676 DM1220/18027805 DM 1221 /18027821 DM1222/18027832 12/23/18 DM1223/18027852 12/24/18 12/25/18 DM1224/18027883 DM1225/18027952 12/26/18 DM1226/18027969 12/27/18 DM1227118027990 12/28/18 DM1228/18028005 12/29/18 DM1229118028070 12/30/18 DM1230/18028089 12/31/18 DM1231/18028102 Avg Result: 3.7 mg/kg D.W. < 7 mg/kg D.W. 7 21 < 7.2 mg/kg D.W. 7.2 21 < 6.8 mg/kg D.W. 7.6 mg/kg D.W. 6.8 6.7 20 20 J. < 6.8 mg/kg D.W. 6.8 20 Q2. 8.6 mg/kg D.W. 6.9 20 J. 9.6 mg/kg D.W. 7 21 J. SW846:6010C MMSD SW846: 6010C MMSD SW846: 6010C SW846: 6010C MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 8.3 mg/kg D.W. 7 21 J. SW846: 6010C 8.6 mg/kg D.W. 7 21 J. SW846: 6010C < 7 mg/kg D.W. 7 21 SW846: 6010C < 7.1 mg/kg D.W. 7.1 21 SW846: 6010C < 7.1 mg/kg D.W. 7.1 21 SW846: 6010C 12 mg/kg D.W. 6.8 20 J. SW846: 6010C 13 mg/kg D.W. 6.7 20 J. SW846: 6010C 13 mg/kg D.W. A 6.9 20 J, SW846: 6010C Min LOD: 4 mg/kg D.W. Max Result: 13 mg/kg D.W. MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD Page 89 of 106 SYS/rptl MrloMonthly 1110113 tj Printed: 1/18119 09.•41 i MMSD r'#tiIM FDt i NUN ilff�filMtElO Solids (% Moisture) Daily Composite DMO106/18000168 01/01/18 DMO101/18000013 01/02/18 DMO102/18000047 01/03/18 DMO103/18000061 01/04/18 DMO104118000098 01/05/18 DMO105118000155 6.8% 0.1 6.3% 0.1 9.4% 0.1 6.7% 0.1 8.9% 0.1 01/06/18 DMO106/18000168 7.8% 0.1 01/07/18 DMO107/18000189 8.1% 0.1 01/08/18 DMO108/18000203 7.3 9/6 0.1 01/09/18 DMO109118000232 8.4% 0.1 01/10/18 DMO 110/18000326 7.2% 0.1 01/11/18 DMO111/18000347 7.5 % 0.1 01/12/18 DMO112/18000363 7.8% 0.1 01/13/18 DMO113/18000397 7.2% 0.1 01/14/18 DM0114/18000418 6.9% 0.1 01/15/18 DMO115/18000432 7% 0.1 Annual Milorganite Report January 1 to December 31, 2018 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 01/16/18 DMO116/18000461 6.4% 0.1 SM 2540 G (1997) MMSD 01/17/18 DMO117/18000652 7.8% 0.1 SM 2540 G (1997) MMSD 01/18/18 DMO118/18000673 6.7% 0.1 SM 2540 G (1997) MMSD 01/19/18 DMO119/18000689 7.3% 0.1 SM 2540 G (1997) MMSD 01/20/18 DMO120/18000702 6.7% 0.1 SM 2540 G (1997) MMSD 01/21/18 DMO121/18000800 6.5% 0.1 SM 2540 G (1997) MMSD 01/22/18 DMO122/18000814 8.6% 0.1 SM 2540 G (1997) MMSD 01/23/18 DMO123118000843 9 0/0 0.1 SM 2540 G (1997) MMSD 01/24/18 DMO124/18000875 5.7 0/6 0.1 SM 2540 G (1997) MMSD 01/25/18 DMO125/18000896 3.9% 0.1 SM 2540 G (1997) MMSD 01/26/18 DMO126118000912 5 % 0.1 SM 2540 G (1997) MMSD 01/27/18 DMO127/18000925 6.2% 0.1 SM 2540 G (1997) MMSD 01/28/18 DMO128/18000946 4.7% 0.1 SM 2540 G (1997) MMSD 01/29/18 DMO129/18001200 5 % 0.1 SM 2540 G (1997) MMSD 01/30/18 DMO130/18001229 6.3 % 0.1 SM 2540 G (1997) MMSD 01/31/18 DMO131/18001259 5.8% 0.1 SM 2540 G (1997) MMSD 02/01/18 DM0201/18001280 6.9 % 0.1 SM 2540 G (1997) MMSD 02/02/18 DM0202/18001421 5.5% 0.1 SM 2540 G (1997) MMSD 02/03/18 DM0203/18001434 6% 0.1 SM 2540 G (1997) MMSD 02/04/18 DM0204/18001455 6.6% 0.1 fSM 2540 G (1997) MMSD 02/05/18 DM0205/18001469 02/06/18 DM0206/18001506 02/07/18 DM0207/18001599 02/08/18 DM0208/18001620 02/09/18 DM0209/18001738 02/10/18 DM0210118001751 02/11/18 DM0211/18001772 02/12/18 DM0212/18001786 02/13/18 DM0213/18001815 02/14/18 DM0214/18001860 02/15/18 DM0215/18001881 SY5/rpti iloMonthly 1/10/13 q 6.4% 0.1 6.4% 0.1 6.9% 0.1 5.8% 0.1 5 % 0.1 6.2% 0.1 7.1 °/a 0.1 7.4% 0.1 8.5 % 0.1 6.2% 0.1 6.4% 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD Page 90 of 106 Printed: 1/18/19 09.•4; Annual Milorganite Report eNNSD January 1 to December 31, 2018 WW mr a/car r Solids (% Moisture) 02/16/18 DM0216/18001897 5.4% .. LOQ .• Flags 0.1 Anafftical Method SM 2540 G (1997) Lab MMSD 02/17/18 DM0217118001944 6.5 % 0.1 SM 2540 G (1997) MMSD 02/18/18 DM0218/18001965 6.9% 0.1 SM 2540 G (1997) MMSD 02/19/18 DM0219/18001979 7.9 % 0.1 SM 2540 G (1997) MMSD 02/20/18 DM0220/18002047 6.7% 0.1 SM 2540 G (1997) MMSD 02/21/18 DM0221/18002077 7.3 % 0.1 SM 2540 G (1997) MMSD 02/22./18 DM0222/18002097 6.1 % 0.1 SM 2540 G (1997) MMSD 02/23/18 DM0223/18002415 4.4% 0.1 SM 2540 G (1997) MMSD 02/24/18 DM0224/18002427 6.9 % 0.1 SM 2540 G (1997) MMSD 02/25/18 DM0225/18002447 5.2 % 0.1 SM 2540 G (1997) MMSD 02/26/18 DM0226/18002461 6.3 % 0.1 SM 2540 G (1997) MMSD 02/27/18 DM0227/18002537 6.7% 0.1 SM 2540 G (1997) MMSD 02/28/18 DM0228118002609 6.8% 0.1 SM 2540 G (1997) MMSD 03/01/18 DM0301/18002628 7.6% 0.1 SM 2540 G (1997) MMSD 03/02/18 DM0302118002711 7.3% 0.1 SM 2540 G (1997) MMSD 03/03/18 DM0303118002722 7.6% 0.1 SM 2540 G (1997) MMSD 03/04/18 DM0304/18002741 7.6% 0.1 SM 2540 G (1997) MMSD 03/05/18 DM0305/18002805 7.7% 0.1 SM 2540 G (1997) MMSD 03/06/18 DM0306/18002862 7.6 % 0.1 SM 2540 G (1997) MMSD 03/07/18 DM0307/18002927 8.6 % 0.1 SM 2540 G (1997) MMSD 03/08/18 DM0308/18003015 7.2% 0.1 SM 2540 G (1997) MMSD 03/09/18 DM0309/18003030 5.1 % 0.1 SM 2540 G (1997) MMSD 03/10/18 DM0310/18003041 8.1% 0.1 T9. SM 2540 G (1997) MMSD 03/11/18 DM0311/18003060 9.4% 0.1 SM 2540 G (1997) MMSD 03/12/18 DM0312/18003335 9.7% 0.1 T9. SM 2540 G (1997) MMSD 03/13/18 DM0313/18003681 9.9% 0.1 SM 2540 G (1997) MMSD 03/14/18 DM0314/18003710 9.4% 0.1 SM 2540 G (1997) MMSD 03/15/18 DM0315118003729 7.1 % 0.1 SM 2540 G (1997) MMSD 03/16/18 DM0316/18003744 9.4% 0.1 SM 2540 G (1997) MMSD 03/17/18 DM0317/18003755 8.7% 0.1 SM 2540 G (1997) MMSD 03/18/18 DM0318118003780 8.3 % 0.1 SM 2540 G (1997) MMSD 03/19/18 DM0319/18003911 10% 0.1 SM 2540 G (1997) MMSD 03/20/18 DM0320118003938 8.2% 0.1 SM 2540 G (1997) MMSD 03/21/18 DM0321/18003967 9% 0.1 SM 2540 G (1997) MMSD 03/22/18 DM0322/18004111 6% 0.1 SM 2540 G (1997) MMSD 03/23/18 DM0323118004126 4.8% 0.1 SM 2540 G (1997) MMSD 03/24/18 DM0324/18004137 T 8.8% 0.1 SM 2540 G (1997) MMSD 03/25/18 DM0325/18004156 9.4% 0.1 SM 2540 G (1997) MMSD 03/26/18 DM0326/18004320 8.2 % 0.1 SM 2540 G (1997) MMSD 03/27/18 DM0327/18004347 9.7% 0.1 SM 2540 G (1997) MMSD 03/28/18 DM0328/18004376 8.6% 0.1 SM 2540 G (1997) MMSD 03/29/18 DM0329/18004395 6.7% 0.1 SM 2540 G (1997) MMSD 03/30/18 DM0330/18004410 11 % 0.1 SM 2540 G (1997) MMSD 03/31/18 DM0331118004752 7.3 % 0.1 SM 2540 G (1997) MMSD 04/01/18 DM0401/18004771 10% 0.1 SM 2540 G (1997) MMSD 04/02/18 DM0402/18004784 7.6% 0.1 SM 2540 G (1997) MMSD 04/03/18 DM0403118004943 9.9% 0.1 SM 2540 G (1997) MMSD Page 91 of 106 SYS/rptlM110Monthly 1/10/13 tj Panted: 1/18/19 09:4; t MMSD FAMM RR f CIFO f ffl= F Solids (% Moisture) Annual Milorganite Report January 1 to December 31, 2018 05/09/18 05/10/18 DMO509/18007313 DMO510/18007340 05/11/18 DMO511/18007418 05/12/18 DM0512/18007429 04/04/18 DM0404118004972 7.4 % 0.1 SM 2540 G (1997) MMSD 04/05/18 DM0405/18005037 6.5 % 0.1 SM 2540 G (1997) MMSD 04/06/18 DM0406118005052 8.8% 0.1 SM 2540 G (1997) MMSD 04/07/18 DM0407/18005063 7.4% 0.1 SM 2540 G (1997) MMSD 04/08/18 DM0408/18005082 10% 0.1 SM 2540 G (1997) MMSD 04/09/18 DM0409/18005095 9% 0.1 SM 2540 G (1997) MMSD 04/10/18 DM0410/18005164 9.2 % 0.1 SM 2540 G (1997) MMSD 04/11/18 DM0411/18005193 9.7 % 0.1 SM 2540 G (1997) MMSD 04/12/18 DM0412/18005446 9.1 % 0.1 SM 2540 G (1997) MMSD 04/13/18 DM0413/18005463 9.1% 0.1 SM 2540 G (1997) MMSD 04/14/18 DM0414/18005474 6.9% 0.1 SM 2540 G (1997) MMSD 04/15/16 DM0415/18005605 9.3% 0.1 S5. SM 2540 G (1997) MMSD 04/16/18 DM0416/18005618 7.2 % 0.1 SM 2540 G (1997) MMSD 04/17/18 DM0417/18005709 6.7 0/6 0.1 SM 2540 G (1997) MMSD 04/18/18 DM0418/18005738 8.4% 0.1 SM 2540 G (1997) MMSD 04/19/18 DM0419/18005757 6.2 % 0.1 SM 2540 G (1997) MMSD 04/20/18 DM0420/18006009 4.9% 0.1 SM 2540 G (1997) MMSD 04/21/18 DM0421/18006020 7.4% 0.1 SM 2540 G (1997) MMSD 04/22/18 DM0422/18006039 6.7% 0.1 SM 2540 G (1997) MMSD 04/23/18 DM0423/18006157 5.8 0/0 0.1 SM 2540 G (1997) MMSD 04/24/18 DM0424/18006185 8% 0.1 SM 2540 G (1997) MMSD 04/25/18 DM0425118006214 11 % 0.1 SM 2540 G (1997) MMSD 04/26/18 DM0426/18006233 8.7% 0.1 SM 2540 G (1997) MMSD 04/27/18 DM0427/18006441 4.8% 0.1 SM 2540 G (1997) MMSD 04/28/18 DM0428/18006452 9.2 % 0.1 SM 2540 G (1997) MMSD 04/29/18 DM0429118006471 8.2% 0.1 SM 2540 G (1997) MMSD 04/30/18 DM0430/18006484 9% 0.1 SM 2540 G (1997) MMSD 05/01/18 DM0501/18006571 8.9 % 0.1 SM 2540 G (1997) MMSD 05/02/18 DMO502/18006600 8.8 % 0.1 SM 2540 G (1997) MMSD 05/03/18 DMO503/18006854 3.2% 0.1 SM 2540 G (1997) MMSD 05/04/18 DM0504/18007005 5.4 % 0.1 SM 2540 G (1997) MMSD 05/05/18 DMO505/18007016 6.5 % 0.1 SM 2540 G (1997) MMSD 05/06/18 DMO506/18007035 8.1 % 0.1 SM 2540 G (1997) MMSD 05/07/18 DMO507/18007257 55%- 0.1 SM 2540 G (1997) MMSD 05/08/18 DM0508/18007284 7.6% 0.1 SM 2540 G (1997) MMSD 05/09/18 05/10/18 DMO509/18007313 DMO510/18007340 05/11/18 DMO511/18007418 05/12/18 DM0512/18007429 05/13/18 DM0513/18007476 05/14/18 DMO514/18007591 05/15/18 DMO515/18007976 05/16/18 05/17/18 DM0516118008005 DMO517/18008103 05/18/18 DM0518/18008118 05/19/18 DMO519/18008129 05/20/18 DM0520/18008196 SYS/rptiMMoMonthly 1/10/13 tj 7.4% 0.1 8.6°/a 0.1� 7.1% 0.1 7.4% 0.1 9% 0.1 5% 0.1 7.2% 0.1 7.6 % 0.1 8.9% 0.1 �8.3 % 0.1 W 7.8% 0.1 T9. ^ SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD Page 92 of IOL Printed: 1/18/19 09:4; 05/27/18 DMO527/18008703 8.2% 0.1 05/28/18 DM0528/18008716 9.5 % 0.1 05/29/18 DM0529/18008888 9.1% 0.1 05/30/18 DMO530/18008917 05/31/18 Annual Milorganite Report MMSD DM0601/18009150 DM0602/18009161 06/03/18 06/04/18 DM0603/18009335 DM0604/18009348 January 1 to December 31, 2018 'aro W 1(IFUR 8#11N(AME�I' 06/06/18 DM0606/18009404 06/07/18 So�lidss (% Moisture) 8.3% 0.1 06/12/18 SaMple ID Result LOD LOQ QA Rao Arkalytkal Method Lab DM0613/18010127 9.2 % 0.1 05/21/18 DM0521/18008209 8.3 % 0.1 SM 2540 G (1997) MMSD 05/22/18 DMO522118008236 9.4% 0.1 SM 2540 G (1997) MMSD 05/23/18 DM0523118008304 7.3 % 0.1 SM 2540 G (1997) MMSD 05/24/18 DM0524/18008658 4.7% 0.1 SM 2540 G (1997) MMSD 05/25/18 DM0525/18008673 6.3 % 0.1 SM 2540 G (1997) MMSD 05/26/18 DM0526/18008684 5 % 0.1 SM 2540 G (1997) MMSD 05/27/18 DMO527/18008703 8.2% 0.1 05/28/18 DM0528/18008716 9.5 % 0.1 05/29/18 DM0529/18008888 9.1% 0.1 05/30/18 DMO530/18008917 05/31/18 DMO531/18008936 06/01/18 06/02/18 DM0601/18009150 DM0602/18009161 06/03/18 06/04/18 DM0603/18009335 DM0604/18009348 06/05/18 DM0605/18009375 06/06/18 DM0606/18009404 06/07/18 DM0607/18009423 6.4% 0.1 7.6 % 0.1 J 5.1 % 0.1 7.1% 0.1 7.3% 0.1 5.5% 0.1 8% 0.1 8.9% 0.1 7.4% 0.1 06/08/18 OM0608/18009822 5.3 % 0.1 06/09/18 DMO609/18009833 6.3 % 0.1 06/10/18 DM0610/18009852 5 % 0.1 06/11/18 DM0611/18009865 8.3% 0.1 06/12/18 DM0612/18010098 8.8% 0.1 06/13/18 DM0613/18010127 9.2 % 0.1 06/14/18 DM0614/18010437 7.6 % 0.1 06/15/18 DMO615118010452 6.1 % 0.1 06/16/18 DMO616/18010463 5.9 % 0.1 06/17/16 DM0617/18010482 5.5 0/0 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 06/18/18 DM0618/18010639 7.3% 0.1 SM 2540 G (1997) MMSD 06/19/18 DM0619/18010666 7.8% 0.1 D1. SM 2540 G (1997) MMSD 06/20/18 DM0620/18010694 5 % 0.1 SM 2540 G (1997) MMSD 06/21/18 DM0621/18010713 3.8% 0.1 SM 2540 G (1997) MMSD 06/22/18 06/23/18 DM0622118010939 DM0623/18010950 4.1% 3.9% 0.1 0.1 SM 2540 G (1997) SM 2540 G (1997) MMSD MMSD 06/24/18 DM0624/18011087 6.5% 0.1 SM 2540 G (1997) MMSD 06/25/18 DMO625/18011182 5.9% 0.1 SM 2540 G (1997) MMSD 06/26/18 DMO626/18011209 06/27/18 DM0627/18011597 06/28/18 DM0628/18011616 06/29/16 DM0629/18011631 06/30/16 DM0630/18011642 07/01/18 DM0701118011728 07/02/18 DM0702/18011741 6.6% 0.1 6% 0.1 6.6 % 0.1 7.3 % 0.1 8% 0.1 6.4% 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 7.6% 0.1 SM 2540 G (1997) MMSD 07/03/18 DM0703/18011881 6.7% 0.1 SM 2540 G (1997) MMSD 07/04/18 DM0704/18011909 4.8% 0.1 SM 2540 G (1997) MMSD 07/05/18 DM0705/18012390 5.7% 0.1 SM 2540 G (1997) MMSD 07/06/18 DM0706118012405 SYSIVINiloMonlhly 1/10/13 tj 7.3 % 0.1 SM 2540 G (1997) MMSD Page 93 o1106 Pnnle0: 1/18/19 09.4; f A 'NSD F� k Cllil�FR Fl��i Solids (% Moisture) . 4 0.1 07/07/18 DM0707/18012416 07/08/18 DM0708/18012435 07/09/18 DM0709/18012448 07/10/18 DM0710/18012474 07/11/18 DM0711/18012820 07/12/16 DM0712/18012861 07/13/18 DM0713/18012876 ^ ^T 07/14/18 DM0714/18013220 07/15/18 DM0715118013239 07/16/18 DM0716/18013252 07/17/18 DM0717/18013751 07/18/18 DM0718/18013961 07/19/18 DM0719/18014047 07/20/18 DM0720/18014062 07/21/18 DM0721/18014073 07/22/18 DM0722/18014483 07/23/18 DM0723118014496 07/24/18 DM0724/18014523 07/25/18 DM0725/18014551 07/26/18 DM0726/18014570 07/27/18 DM0727/18014585 07/28/18 DM0728118014676 07/29/18 DM0729/18014910 07/30/18 DM0730118014925 07/31/18 DM0731/18014954 08/01/18 DM0801/18014969 08/02/18 DM0802/18015140 08/03/18 DM0803/18015155 08/04/18 DMO804/18015252 08/05/18 DMO805/18015279 08/06/18 DMO806/18015385 08/07/18 DM0807/18015414 08/08/18 DM0808/18015473 08/09/18 DM0809/18015500 08/10/18 DMO810118015899 08/11/18 DMO811/18015910 08/12/18 DM0812/18016203 08/13/18 DM0813/18016216 08/14/18 DM0814/18016254 08/15/18 DMO815/18016281 08/16/18 DM0816/18016300 08/17/18 DM0817/18016365 08/18/18 DM0818/18016505 08/19/18 DMO819/18016525 08/20/18 DM0820/18016539 08/21/18 DM0821/18016714 Annual Milorganite Report January 1 to December 31, 2018 7.8% 0.1 SM 2540 G (1997) MMSD 5.9 % 0.1 SM 2540 G (1997) MMSD 8.1 % 7.6% 0.1 0.1 SM 2540 G (1997) SM 2540 G (1997) MMSD MMSD 5.2% 5.8 % 5.8 % 5.1 % 6.4 % 5.4% SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 5 % 0.1 5.4% 0.1 4.1 o/a 0.1 6% 0.1 5.2 % 0.1 55. 6% 0.1 6.7% 0.1 6.4 % 0.1 7.8% 0.1 6.8% 0.1 5.4 % 0.1 4.4% 0.1 4.4% 0.1 7% 0.1 5.8% 0.1 4.9% 0.1 5.1 % 0.1 5.7% 0.1 4.3 % 0.1 5.6 % 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 4.6% 0.1 SM 2540 G (1997) MMSD 4.9% 0.1 SM 2540 G (1997) MMSD 4.6% 0.1 SM 2540 G (1997) MMSD 4.5% 0.1 SM 2540 G (1997) MMSD 4.6% 0.1 SM 2540 G (1997) MMSD 4.6% 0.1 SM 2540 G (1997) MMSD 4.2% 0.1 SM 2540 G (1997) MMSD 4.2% 0.1 SM 2540 G (1997) MMSD �4.7 % 0.1 SM 2540 G (1997) MMSD 4.6% 0.1 SM 2540 G (1997) MMSD 3.8% 0.1 SM 2540 G (1997) MMSD 4.2% 0.1 4.3% 0.1 4.3% 0.1 T9. 3.9% 0.1 5.5 % 0.1 08/22/18 DM0822/18016742 4.5 % 0.1 SYSIWIMiloMonfhly 1/10/13 U SM 2540 G (1997) MMSD SM 2540 G (1997) _ MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD Page 94 of 10d Prinled: 1/18/19 09:4; �IMS� nvow 01: i nfm (tnt!IE�(y Solids (% Moisture U7,Tullfa DM0829/18017462 4.4% 0.1 08/23/18 DM0823/18017352 3.4% 0.1 06/24/18 DM0824/18017367 3.6% 0.1 08/25/18 DM0825/18017378 4.8% 0.1 08/26/18 DMO826/18017397 3.6% 0.1 08/27/18 DM0827/18017410 4% 0.1 08/28/18 DM0828/18017434 4.7% 0.1 Annual Milorganite Report January 1 to December 31, 2018 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 08/29/18 DM0829/18017462 4.4% 0.1 SM 2540 G (1997) MMSD 08/30/18 DMO830/18017483 5.2% 0.1 SM 2540 G (1997) MMSD 08/31/18 DM0831/18017498 5 % 0.1 SM 2540 G (1997) MMSD 09/01/18 DMO901/18017520 4.1% 0.1 SM 2540 G (1997) MMSD 09/02/18 DM0902/18017752 3.7% 0.1 _ SM 2540 G (1997) MMSD 09/03/18 DM0903/18018124 4.7% 0.1 SM 2540 G (1997) MMSD 09/04/18 DM0904/18018149 6% 0.1 SM 2540 G (1997) MMSD 09/05/18 DM0905/18018305 6.2% 0.1 SM 2540 G (1997) MMSD 09/06/18 DM0906/18018326 y 5.9% 0.1 Dl. SM 2540 G (1997) MMSD 09/07/18 DM0907/18018342 5 % 0.1 SM 2540 G (1997) MMSD 09/08/18 DM0908/18018353 4.2 % 0.1 SM 2540 G (1997) MMSD 09/09/18 DMO909/18018724 3.7 % 0.1 SM 2540 G (1997) MMSD 09/10/18 DM0910/18018799 5.4% 0.1 S5. SM 2540 G (1997) MMSD 09/11/18 DM0911/18018825 6.2 % 0.1 SM 2540 G (1997) MMSD 09/12/18 DMO912118018854 5.4% 0.1 SM 2540 G (1997) MMSD 09/13/18 DMO913/18018875 6.8% 0.1 SM 2540 G (1997) MMSD 09/14/18 DM0914/18018891 6.8% 0.1 S5. SM 2540 G (1997) MMSD 09/15/18 DMO915/18019159 6.6% 0.1 SM 2540 G (1997) MMSD 09/16/18 DMO916/18019178 6.2% 0.1 SM 2540 G (1997) MMSD 09/17/18 DM0917/18019191 4.7% 0.1 SM 2540 G (1997) MMSD 09/18/18 DM0918/18019447 7.6% 0.1 SM 2540 G (1997) MMSD 09/21/18 DM0921/18019515 3.1 % 0.1 SM 2540 G (1997) MMSD 09/22/18 DMO922/18019574 4% 0.1 SM 2540 G (1997) MMSD 09/23/18 DMO923/18019665 2% 0.1 SM 2540 G (1997) MMSD 09/24/18 DM0924/18020088 3.3% 0.1 SM 2540 G (1997) MMSD 09/25/18 DM0925/18020314 4% 0.1 SM 2540 G (1997) MMSD 09/26/18 DM0926/18020343 6% 0.1 SM 2540 G (1997) MMSD 09/27/18 DMO927/18020364 5.8% 0.1 SM 2540 G (1997) MMSD 09/28/16 DM0928/18020380 8.5 % 0.1 S5. SM 2540 G (1997) MMSD 09/29/18 DM0929/18020391 5.5 % 0.1 SM 2540 G (1997) MMSD 09/30/18 DM0930/18020411 5.8% 0.1 SM 2540 G (1997) MMSD 10/01/18 DM1001/18021136 4.7% 0.1 T^ SM 2540 G (1997) MMSD 10/02/18 DM1002/18021162 5.9 % 0.1 SM 2540 G (1997) MMSD 10/03/18 DM1003118021190 5.9% 0.1 SM 2540 G (1997) MMSD 10/04/18 DM1004/18021541 4.3% 0.1 SM 2540 G (1997) MMSD 10/05/18 DM1005/18021557 5.5 % 0.1 SM 2540 G (1997) MMSD 10/06/18 DM1006/18021568 7.2 % 0.1 SM 2540 G (1997) MMSD 10/07/18 DM1007/18021588 3.3% 0.1 SM 2540 G (1997) MMSD 10/08/18 DM1008/18021602 3.2% 0.1 SM 2540 G (1997) MMSD 10/09/18 DM1009118021627 4.1% 0.1 SM 2540 G (1997) MMSD 10/10/16 DM1010/18021656 6.2% 0.1 SM 2540 G (1997) MMSD Page 95 of 106 SYS/rptimifoMonfhly 1/10/13 hi Printed: 1/18/19 09:4i 0 11/07/18 DM 1107/18023991 3.3% Annual Milorganite Report MMSD DM1108/18024012 3.8 9/o 0.1 January 1 to December 31, 2018 v1A1M fat a CLW IYOWNT 4.3% 0.1 11/10/18 DM 1110/ 18024523 Solids (% Moisture) 0.1 11/11/18 DM1111/18024619 3.6% 10/11/18 DM1011/18021975 5% 0.1 SM 2540 G (1997) MMSD 10/12/18 DM1012/18021991 4% 0.1 SM 2540 G (1997) MMSD 10/13/18 DM1013/18022006 6.2% 0.1 SM 2540 G (1997) MMSD 10/14/18 DM1014/18022026 5.8% 0.1 T� SM 2540 G (1997) MMSD 10/15/18 DM1015/18022040 6.2% 0.1 SM 2540 G (1997) MMSD 10/16/18 DM1016/18022065 5.4% 0.1 SM 2540 G (1997) MMSD 10/17/18 DM1017/18022094 5.4% 0.1 SM 2540 G (1997) MMSD 10/18/18 DM1018/18022133 4.4% 0.1 SM 2540 G (1997) MMSD 10/19/18 DM1019/18022269 6.4% 0.1 SM 2540 G (1997) MMSD 10/20/18 DM1020/18022280 4.2% 0.1 SM 2540 G (1997) MMSD 10/21/18 DM1021/18022435 5%- 0.1 SM 2540 G (1997) MMSD 10/22/18 DM1022/18022449 4.4% 0.1 SM 2540 G (1997) MMSD 10/23/18 DM1023/18022614 5.3% 0.1 SM 2540 G (1997) MMSD 10/24/18 DM 1024/18022643 T 5.8% 0.1 SM 2540 G (1997) MMSD 10/25/18 DM1025/18022708 5.6% 0.1 SM 2540 G (1997) MMSD 10/26/18 DM1026/18022767 T 4.9% 0.1 SM 2540 G (1997) MMSD 10/27/18 DM1027/18022778 3.5% 0.1 SM 2540 G (1997) MMSD 11/07/18 DM 1107/18023991 3.3% 0.1 11/08/18 DM1108/18024012 3.8 9/o 0.1 11/09/18 DM1109/18024028 4.3% 0.1 11/10/18 DM 1110/ 18024523 3.4 0/0 0.1 11/11/18 DM1111/18024619 3.6% 0.1 11/12/18 DM 1112/18024633 6% 0.1 11/13/18 DM 1113/18025014 5.7% 0.1 11/14/18 DM 1114/18025043 7% 0.1 11/15/18 DM1115/18025064 6.1 % 0.1 11/16/18 DM1116/18025080 8.9% 0.1 11/17/18 DM1117/18025093 5.3% 0.1 11/18/18 DM 1118/18025113 7.6% 0.1 11/19/18 DM 1119/18025127 5.1 1/0 10.1 11/20/18 DM1120/18025356 4.7% 0.1 11/21/18 DM1121118025385 5.3% 0.1 11/22/18 DM1122/18025406 6.6 % 0.1 T 11/23/18 DM1123/18025422 6.3 % J 0.1 11/24/18 DM1124/18025750 8.5% 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM SM 2540 G 2540 G (1997) (1997) MMSD MMSD SM 2540 G (1997) MMSD 11/25/18 DM1125/18025769 8.5 % 0.1 SM 2540 G (1997) MMSD 11/26/18 DM1126/18025828 11/27/18 11/28/18 T DM1127/18025860 DM1128/18025888 11/29/18 DM 1129/18025956 f 11/30/18 DM 1130/18025971 12/01/18 DM1201118026182 12/02/18 DM 1202/18026201 12/03/18 DM1203/18026214 12/04/18 DM1204/18026391 12/05/18 DM1205/18026578 12/06/18 DM1206118026621 SYS/rptlMiloMonthly 1/10/13 tj 4.2 °/a 0.1 SM 2540 G (1997) MMSD 4.5% 0.1 SM 2540 G (1997) MMSD 4.5% 0.1 SM 2540 G (1997) MMSD 5.6 % 0.1 SM 2540 G (1997) MMSD T 6.6% 0.1 SM 2540 G (1997) MMSD 7% 0.1 SM 2540 G (1997) MMSD 6% 0.1 SM 2540 G (1997) MMSD 5.9% 0.1 SM 2540 G (1997) MMSD 7.1% 0.1 SM 2540 G (1997) MMSD 7.3% 0.1 SM 2540 G (1997) MMSD 9.7% 0.1 SM 2540 G (1997) MMSD Page 96 of 106 Printed: 1/18/19 09:4; 12/14/18 DM1214/18027306 12/15/18 12/16/18 Annual Milorganite Report e.14149 DM1217/18027540 12/18/18 12/19/18 January 1 to December 31, 2018 MIT" "I 1 WAIR 11 MWNT DM1220/18027805 12/21/18 DM1221/18027821 Solids (% Moisture) Sample Date sampic, 10 Result LOD LGQ QA Hags Anatytical Method Lab 12/07/18 DM1207/18026797 8.9% 0.1 SM 2540 G (1997) MMSD 12/08/18 DM1208/18026808 7.8% 0.1 SM 2540 G (1997) MMSD 12/09/18 DM1209/18026827 7% 0.1 SM 2540 G (1997) MMSD 12/10/18 DM1210/18026840 10 % 0.1 SM 2540 G (1997) MMSD 12/11/18 DM1211/18027102 5.2% 0.1 SM 2540 G (1997) MMSD 12/12/1_8 DM1212/18027130 4.7% 0.1 SM 2540 G (1997) MMSD 12/13/18 DM1213/18027253 6.9% 0.1 SM 2540 G (1997) MMSD 12/14/18 DM1214/18027306 12/15/18 12/16/18 DM1215/18027317 DM1216/1802.7525 12/17/18 DM1217/18027540 12/18/18 12/19/18 DM1218118027643 DM1219/18027676 12/20/18 DM1220/18027805 12/21/18 DM1221/18027821 12./22/18 DM1222/18027832 12/23/18 DM1223/18027852 12/24/18 DM1224/18027883 12./25/18 DM1225/18027952 12/26/18 DM1226/18027969 12/27/18 DM1227/18027990 12/28/18 DM1228/18028005 12/29/18 DM1229118028070 12/30/18 DM1230118028089 12/31/18 DM1231/18028102 9% Avg Result: 6.5 % Weekly Composite 01/06/18 WMC01/18000205 01/13/18 WMCO2/18000434 01/20/18 WMC03/18000816 01/27/18 WMC04/18001202 9% 0.1 - - 11 % 0.1 6.4% 0.1 5.1 % 0.1 6.5% 0.1 7.7% 0.1 6.1 % 0.1 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD 8.4% 0.1 SM 2540 G (1997) MMSD 8.9% 9.3 % 0.1 0.1 SM 2540 G (1997) SM 2540 G (1997) MMSD MMSD 9.4% 0.1 SM 2540 G (1997) MMSD 10% 0.1 SM 2540 G (1997) MMSD 6.4% 0.1 4.9% 0.1 7% 0.1 Min LOD: 0.1 % 7.3% 0.1 SM 2540 G (1997) S5. SM 2540 G (1997) SM 2540 G (1997) Max Result: 11 % SM 2540 G (1997) MMSD MMSD MMSD MMSD 7.7% 0.1 SM 2540 G (1997) MMSD 6.8% 0.1 SM 2540 G (1997) MMSD 6.4% 0.1 SM 2540 G (1997) MMSD 02/03/18 02/10/18 WMC05/18001471 WMC06/18001788 5.4% 6.2% 0.1 0.1 SM 2540 G (1997) SM 2540 G (1997) MMSD MMSD 02/17/18 WMC07/18001981 6.3% 0.1 SM 2540 G (1997) MMSD 02/24/18 WMC08/18002463 6.4% 0.1 SM 2540 G (1997) MMSD 03/03/18 03/10/18 03/17/18 WMC09/18002807 WMC10/18003337 WMC11118003913 6.8% 7.4% 8.8% 0.1 0.1 T9. 0.1 SM 2540 G (1997) SM 2540 G (1997) SM 2540 G (1997) MMSD MMSD MMSD 03/24/18 WMC12/18004322 7.8% 0.1 SM 2540 G (1997) MMSD 03/31/18 WMC13118004786 8.4% 0.1 SM 2540 G (1997) MMSD 04/07/18 WMC14/18005097 8% 0.1 SM 2540 G (1997) MMSD 04/14/18 WMC15/18006159 9.1% 0.1 SM 2540 G (1997) MMSD 04/21/18 WMC16/18006160 7.1 % 0.1 SM 2540 G (1997) MMSD 04/28/18 WMC17/18006486 7.1% 0.1 SM 2540 G (1997) MMSD 05/05/18 WMC18/18007259 7.5 % 0.1 SM 2540 G (1997) MMSD 05/12/18 WMC19/18007645 7.6% 0.1 SM 2540 G (1997) MMSD SYS/iptlMiloMonthly 1/10/13 ty Page 97 o/ 106 Pnnted: 1/18/19 09:4; 0 MMSD PUMajCUM I Solids (% Moisture) 05/19/18 WMC20/18008211 7.6% 0.1 05/26/18 WMC21/18008718 7.8% 0.1 06/02/18 WMC22/18009350 7.5 % 0.1 06/09/18 WMC23/18009867 06/16/18 WMC24/18010641 06/23/18 WMC25118011184 06/30/18 WMC26/18011743 07/07/18 WMC27/18013254 07/14/18 WMC28/18013259 07/21/18 WMC29/18014498 07/28/18 WMC30/18014929 06/04/18 WMC31/18015389 08/11/18 WMC32/18016218 08/18/18 WMC33118016543 08/25/18 WMC34/18018126 09/01/18 WMC35118018151 09/08/18 WMC36118018801 09/15/18 WMC37/18019193 09/22/18 WMC38/18021138 09/29/18 WMC39/18021139 10/06/18 WMC40/18021604 10/13/18 WMC41/18022042 10/20/18 WMC42/18022451 10/27/18 WMC43/18022969 11/10/18 WMC45/18025129 11/17/18 WMC46/18024635 11/24/18 WMC47/18025830 12/01/18 WMC48/18026216 12/08/18 WMC49/18026842 12/15/18 WMC50/18027542 12/22/18 WMC51/18027885 12/29/18 WMC52/18028104 SYS/rptlMl/oMonthly 1/10/13 0 7% 0.1 7.4% 0.1 5.2 % 0.1 G (1997) MMSD 6.6% 0.1 6.4% 0.1 5.5 % 0.1 - - 6.4% 0.1 5.5% 0.1 5% 0.1 44% 0.1 4.5 % 0.1 4.5% 0.1 5.7% 0.1 6% 0.1 5.2% 0.1 5.3% 0.1 5.7 % 0.1 5 % 0.1 5.2 % 0.1 5 % 0.1 3.9 % 0.1 6.2 % 0.1 6.3% 0.1 5.9 % 0.1 7.2 % 0.1 6.3 % 0.1 7.1 % 0.1 8.3 % 0.1 Min LOD: 0.1 Annual Milorganite Report January 1 to December 31, 2018 SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD _ SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD SM 2540 G (1997) MMSD Page 98 of 106 Printed: 1/18/19 09:4; Annual Milorganite Report NSDJanuary 1 to December 31, 2018 h�'iP11 F�ii l firF,�FHYf�i''+{Sd31' Solids (% Volatile) . 1 .. 01/13/18 WMCO2/18000434 78% 0.1 SM 2540 G (1997) MMSD 02/24/18 WMC08118002463 75 % 0.1 SM 2540 G (1997) MMSD 03/10/18 WMC10/18003337 75 % 0.1 SM 2540 G (1997) MMSD 04/07/18 WMC14/18005097 75% 0.1 SM 2540 G (1997) MMSD 05/12/18 WMC19/18007645 74% 0.1 SM 2540 G (1997) MMSD 06/09/18 WMC23/18009867 72% D.1 SM 2540 G (1997) MMSD 07/07/18 WMC27/18013254 69% 0.1 SM 2540 G (1997) MMSD 08/11/18 09/08/18 10/13/18 11/17/18 12/08/18 WMC32118016218 WMC36/18018801 WMC41 / 18022042 WMC46/18024635 WMC49/18026842 Avg Result: 72 a/o 70% 0.1 SM 2540 G (1997) MMSD 66% 0.1 SM 2540 G (1997) MMSD 66% 0.1 S5. SM 2540 G (1997) MMSD 70% 0.1 S5. SM 2540 G (1997) MMSD 72% 0.1 SM 2540 G (1997) MMSD Min LOD: 0.1 a/o Max Result: 78 a/a Page 99 of 106 SYS/rptlMMOMonthly 1/10/13 tj Printed: 1/18/19 09:4; U -IMMSD F. ZINC ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 01/06/18 01/07/18 01/08/18 01/09/18 01/10/18 01/11/18 01/12/18 01/13/18 01/14/18 miivio 01/16/18 01/17/18 01/18/18 01/19/18 01/20/18 01/21/18 01/22/18 01/23/18 01/24/18 01/25/18 01/26/18 01/27/18 01/28/18 01/29/18 01/30/18 01/31/18 02/01/18 02/02/18 02/03/18 02/04/18 02/05/18 02/06/18 02/07/18 02/08/18 ni ino l i a 02/11/18 02/12/18 02/13/18 02/14/18 02/15/18 02/16/18 DMO105118000155 DMO106/18000168 DMO107/18000189 DMO 108/ 18000203 DMO109/18000232 DMO 110/18000326 DM0111/18000347 DMO112/18000363 DM0113/18000397 DM0114/18000418 DM0115118000432 DM0116/18000461 DMO117/18000652 DMO118/18000673 DM0119/18000689 DMO120/18000702 DMO121 / 18000800 DMO122/18000814 DMO123/18000843 DM0124/18000875 DMO125/18000896 DMO126/18000912 DMO127/18000925 DMO128/18000946 DMO129/18001200 DMO130/18001229 DM0131/18001259 DM0201/18001280 DM0202/18001421 DM0203/18001434 DM0204/18001455 DM0205/18001469 DM0206/18001506 DM0207/18001599 DM0208/18001620 DM0209/18001738 DM0210/18001751 DM0211 /18001772 DM0212/18001786 DM0213/18001815 DM0214/18001860 DM0215/18001881 DM0216/18001897 SYS/rPUMMOManthly 1/10/13 lj 370 mg/kg D.W. 3.3 11 370 mg/kg D.W. T 3.2 11 380 mg/kg D.W. 01/01/18 DMO101/18000013 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 01/02/18 DMO102/18000047 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 01/03/18 DMO103/18000061 390 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 01/04/18 DMO104/18000098 370 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 01/06/18 01/07/18 01/08/18 01/09/18 01/10/18 01/11/18 01/12/18 01/13/18 01/14/18 miivio 01/16/18 01/17/18 01/18/18 01/19/18 01/20/18 01/21/18 01/22/18 01/23/18 01/24/18 01/25/18 01/26/18 01/27/18 01/28/18 01/29/18 01/30/18 01/31/18 02/01/18 02/02/18 02/03/18 02/04/18 02/05/18 02/06/18 02/07/18 02/08/18 ni ino l i a 02/11/18 02/12/18 02/13/18 02/14/18 02/15/18 02/16/18 DMO105118000155 DMO106/18000168 DMO107/18000189 DMO 108/ 18000203 DMO109/18000232 DMO 110/18000326 DM0111/18000347 DMO112/18000363 DM0113/18000397 DM0114/18000418 DM0115118000432 DM0116/18000461 DMO117/18000652 DMO118/18000673 DM0119/18000689 DMO120/18000702 DMO121 / 18000800 DMO122/18000814 DMO123/18000843 DM0124/18000875 DMO125/18000896 DMO126/18000912 DMO127/18000925 DMO128/18000946 DMO129/18001200 DMO130/18001229 DM0131/18001259 DM0201/18001280 DM0202/18001421 DM0203/18001434 DM0204/18001455 DM0205/18001469 DM0206/18001506 DM0207/18001599 DM0208/18001620 DM0209/18001738 DM0210/18001751 DM0211 /18001772 DM0212/18001786 DM0213/18001815 DM0214/18001860 DM0215/18001881 DM0216/18001897 SYS/rPUMMOManthly 1/10/13 lj 370 mg/kg D.W. 3.3 11 370 mg/kg D.W. T 3.2 11 380 mg/kg D.W. 3.3 T 11 400 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.3 11 390 mg/kg D.W. 3.2 10 410 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.2 11 460 mg/kg D.W. 3.2 10 440 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 460 mg/kg D.W. 3.2 10 420 mg/kg D.W. 3.2 11 390 mg/kg D.W. 3.2 10 390 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.3 11 390 mg/kg D.W. 3.3 11 430 mg/kg D.W. 3.2 10 460 mg/kg D.W. 3.1 10 440 mg/kg D.W. 3.2 10 440 mg/kg D.W. 3.2 10 440 mg/kg D.W. 3.1 10 430 mg/kg D.W. 3.2 10 420 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 420 mg/kg D.W. 3.2 10 410 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 390 mg/kg D.W. 3.2 10 370 mg/kg D.W. 3.2 10 380 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.2 10 400 mg/kg D.W. 3.2 10 410 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 430 mg/kg D.W. 3.2 10 410 mg/kg D.W. 3.3 11 420 mg/kg D.W. 3.2 10 410 mg/kg D.W. 3.2 10 420 mg/kg D.W. 3.2 10 D2, Q2. SW846: 6010C MMSD SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C v SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6D10C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6D10C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMCf1 MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 100 of 106 Printed: 1/18/19 09.•4; :; Annual Milorganite Report MMSD January 1 to December 31, 2018 ZINC ICP METHOD 02/17/18 Sample 10- DM0217/18001944 Resutt 440 mg/kg D.W. O. 3.2 LOQ QA Flags 10 Analytical Method SW846: 6010C MMSD 02/18/18 DM0218/18001965 470 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/19/18 DM0219/18001979 470 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 02/20/18 DM0220/18002047 420 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/21/18 DM0221/18002077 420 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/22/18 DM0222/18002097 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/23/18 DM0223118002415 420 mg/kg D.W. 3.1 10 SW846: 6010C MMSD 02/24/18 DM0224118002427 400 mg/kg D.W. 3.2 10 SW646: 6010C MMSD 02/25/18 DM0225/18002447 410 mg/kg D.W. 3.2. 10 SW846: 6010C MMSD 02/26/18 DM0226/18002461 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/27/18 DM0227/18002537 390 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 02/28/18 DM0228/18002609 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/01/18 DM0301/18002628 410 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 03/02/18 DM0302/18002711 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/03/18 DM0303/18002722 380 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 03/04/18 DM0304118002741 380 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 03/05/18 DMO305/18002805 380 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 03/06/18 DM0306/18002862 370 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 03/07/18 DM0307/18002927 360 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/08/18 DM0308/18003015 360 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/09/18 DM0309118003030 360 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/10/18 DM0310/18003041 360 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/11/18 DM0311/18003060 360 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/12/18 DM0312/18003335 360 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/13/18 DM0313/18003681 360 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/14/18 DM0314118003710 380 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/15/18 DM0315/18003729 380 mg/kg D.W. 3.2 y 10 SW846: 6010C MMSD 03/16/18 DM0316118003744 370 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/17/18 DM0317/18003755 380 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/18/18 DM0318/18003780 400 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/19/18 DM0319/18003911 390 mg/kg D.W. 3.4 11 SW846: 6010C MMSD 03/20/18 DM0320/18003938 370 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/21/18 DM0321/18003967 J 390 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/22/18 DM0322/18004111 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/23/18 DM0323/18004126 410 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/24/18 DM0324/18004137 390 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/25/18 DM0325/18004156 400 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/26/18 DM0326/18004320 390 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/27/18 DM0327/18004347 410 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/28/18 DM0328118004376 410 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 03/29/18 DM0329/18004395 390 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 03/30/18 DM0330118004410 380 mg/kg D.W. 3.4 11 SW846: 6010C MMSD 03/31/18 DM0331/18004752 400 mg/kg D.W. 3.2 10 SW846: 6010C MMSD 04/01/18 DM0401/18004771 400 mg/kg D.W. 3.3 11 SW846: 6010C MMSD 04/02/18 DM0402/18004784 390 mg/kg D.W. 3.2 11 SW846: 6010C MMSD 04/03/18 DM0403/18004943 400 mg/kg D.W. 17 49 SW846: 6010C MMSD 04/04/18 DM0404/18004972 370 mg/kg D.W. 16 47 SW846: 6010C MMSD Page 101 of 106 SYS/rpllMilamonthly 1/10/13 tj Printed: 1/18/19 09:9; 0 4 -MMSD ZINC ICP METHOD 04/05/18 DM0405/18005037 450 mg/kg D.W. 16 04/06/18 DM0406/18005052 440 mg/kg D.W. 16 04/07/18 DM0407/18005063 450 mg/kg D.W. 16 04/08/18 DM0408/18005082 450 mg/kg D.W. 17 04/09/18 DM0409/18005095 440 mg/kg D.W. 16 04/10/18 DM0410/18005164 420 mg/kg D.W. 16 04/11/18 DM0411/18005193 380 mg/kg D.W. 17 04/12/18 DM0412/18005446 380 mg/kg D.W. 16 04/13/18 DM0413/18005463 390 mg/kg D.W. 16 04/14/18 DM0414/18005474 410 mg/kg D.W. 16 04/15/18 DM0415/18005605 390 mg/kg D.W. 16 04/16/18 DM0416/18005618 380 mg/kg D.W. 16 04/17/18 DM0417118005709 390 mg/kg D.W. 16 04/18/18 DM0418118005738 390 mg/kg D.W. 16 04/19/18 DM0419/18005757 390 mg/kg D.W. 16 04/20/18 DM0420/18006009 390 mg/kg D.W. 16 04/21/18 DM0421/18006020 430 mg/kg D.W. 16 04/22/18 DM0422/18006039 440 mg/kg D.W. 16 04/23/18 DM0423/18006157 420 mg/kg D.W. 16 04/24/18 DM0424/18006185 420 mg/kg D.W. 16 04/25/18 DM0425/18006214 430 mg/kg D.W. 17 04/26/18 DM0426/18006233 420 mg/kg D.W. 16 04/27/18 DM0427/18006441 400 mg/kg D.W. 16 04/28/18 DM0428/18006452 380 mg/kg D.W. 16 04/29/18 DM0429/18006471 360 mg/kg D.W. 16 04/30/18 DM0430/18006484 380 mg/kg D.W. 16 05/01/18 DM0501/18006571 360 mg/kg D.W. 16 05/02/18 DM0502118006600 360 mg/kg D.W. 16 05/03/18 DM0503/18006854 370 mg/kg D.W. 15 05/04/18 DM0504/18007005 370 mg/kg D.W. 16 05/05/16 DMO505/18007016 400 mg/kg D.W. 16 05/06/18 DM0506/18007035 390 mg/kg D.W. 16 05/07/18 DMO507/18007257 410 mg/kg D.W. 16 05/08/18 DM0508118007284 400 mg/kg D.W. 16 05/09/18 DM0509/18007313 400 mg/kg D.W. 16 05/10/18 DM0510/18007340 400 mg/kg D.W. 16 05/11/18 DM0511/18007418 440 mg/kg D.W. 16 05/12/18 DM0512118007429 420 mg/kg D.W. 16 05/13/18 DMO513118007476 410 mg/kg D.W. 16 05/14/18 05/14/18 DM0514/18007591 410 mg/kg D.W. 16 05/15/18 DM0515/18007976 440 mg/kg D.W. 16 05/16/18 DM0516/18008005 440 mg/kg D.W. 16 05/17/18 DMO517/18008103 430 mg/kg D.W. 16 05/18/18 T DM0518/18008118 430 mg/kg D.W. 16 05/19/18 DM0519/18008129 400 mg/kg D.W. 16 05/20/18 DM0520/18008196 420 mg/kg D.W. 16 05/21/18 DM0521/18008209 430 mg/kg D.W. 16 SYS/rptlMiloMonthly 1/10/13 fj 48 48 48 48 49 48 48 47 48 47 47 48 47 46 48 47 47 48 50 48 46 48 48 48 48 48 45 46 47 48 46 48 48 48 49 47 48 48 46 47 48 48 48 48 48 Annual Milorganite Report January 1 to December 31, 2018 SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6D10C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C T MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD SW846:6010C MMSD Page 102 of 106 Printed: 1118/19 09:9; 06/07/18 DM0607/18009423 430 mg/kg D.W. 16 Annual Milorganite Report SW846: 6010C MSDJanuary 06/08/18 DM0608/18009822 f 420 mg/kg D.W. 1 to December 31, 2018 kr:-412-. 01' 7 '1.1P•a l±l'�iWry' SW846: 6010C MMSD 06/09/18 DMO609/18009833 430 mg/kg D.W. ZINC ICP METHOD 47 SW846: 6010C MMSD 06/10/18 DM0610/18009852 05/22/18 DM0522/18008236 420 mg/kg D.W. 16 48 SW846: 6010C MMSD 05/23/18 DMO523118008304 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 05/24/18 DM0524/18008658 430 mg/kg D.W. 16 46 SW846: 6010C _ MMSD 05/25/18 DM0525/18008673 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 05/26/18 DMO526/18008684 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 05/27/18 DM0527/18008703 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 05/28/18 DM0528/18008716 440 mg/kg D.W. 16 49 SW846: 6010C MMSD 05/29/18 DM0529/18008888 440 mg/kg D.W. 16 48 SW846: 6010C MMSD 05/30/18 DM0530/18008917 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 05/31/18 DM0531/18008936 450 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/01/18 DM0601/18009150 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/02/18 DM0602118009161 440 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/03/18 DM0603/18009335 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/04/18 DM0604118009348 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/05/18 DM0605118009375 440 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/06/18 DM0606118009404 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/07/18 DM0607/18009423 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/08/18 DM0608/18009822 f 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/09/18 DMO609/18009833 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/10/18 DM0610/18009852 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/11/18 DM0611/18009865 460 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/12/18 DMO612/18010098 470 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/13/18 DM0613/18010127 460 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/14/18 DM0614/18010437 470 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/15/18 DM0615/18010452 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/16/18 DM0616/18010463 440 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/17/18 DM0617/18010482 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/18/18 DM0618/18010639 430 mg/kg D.W. 16 f 47 SW846: 6010C MMSD 06/19/18 DM0619/18010666 450 mg/kg D.W. 16 48 SW846: 6010C MMSD 06/20/18 DM0620/18010694 06/21/18 DM0621/18010713 06/22/18 DMO622/18010939 06/23/18 DMO623/18010950 06/24/18 DMO624/18011087 06/25/18 DMO625/18011182 460 mg/kg D.W. 16 46 470 mg/kg D.W. 16 46 460 mg/kg D.W. 16 46 460 mg/kg D.W. 16 46 450 mg/kg D.W. 16 47 440 mg/kg D.W. 16 47 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 06/26/18 06/27/18 06/28/18 DMO626/18011209 DMO627118011597 DMO628/18011616 430 mg/kg D.W. 400 mg/kg D.W. 410 mg/kg D.W. 16 16 16 47 47 47 Q3. SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD 06/29/18 DM0629/18011631 450 mg/kg D.W. 16 47 SW846: 6010C MMSD 06/30/18 DM0630/18011642 400 mg/kg D.W. 16 48 SW846: 6010C MMSD 07/01/18 DM0701/18011728 410 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/02/18 DM0702118011741 400 mg/kg D.W. 16 48 SW846: 6010C MMSD 07/03/18 DM0703118011881 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/04/18 DM0704/18011909 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/05/18 DM0705/18012390 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/06/18 DM0706/18012405 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/07/18 DM0707/18012416 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 5Y5/rpt1MiloMon[h1y 1/10/13 tj Page 103 of 106 Printed: 1118119 09: 4i 0 Page 104 of 106 SYS/rptlMikMonthly 4110/13 tj Printed: 1/18/19 09.4) Annual Milorganite Report e-MMSD January 1 to December 31, 2018 ZINC ICP METHOD 07/08/18 DM0708/18012435 440 mg/kg D.W. .. 16 .. ."1 47 SW846: 6010C MMSD 07/09/18 DM0709/18012448 440 mg/kg D.W. 16 48 SW846: 6010C MMSD 07/10/18 DM0710/18012474 440 mg/kg D.W. 16 48 4 SW846: 6010C MMSD 07/11/18 DM0711/18012820 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/12/18 DM0712/18012861 430 mg/kg D.W. 16 47 J SW846: 6010C MMSD 07/13/18 DM0713/18012876 440 mg/kg D.W. 16 47 ` SW846: 6010C MMSD 07/14/18 DM0714118013220 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/15/18 DM0715/18013239 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/16/18 DM0716/18013252 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/17/18 DM0717/18013751 490 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/18/18 DM0718118013961 470 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/19/18 DM0719/18014047 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/20/18 DM0720/18014062 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/21/18 DM0721/18014073 470 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/22/18 DM0722/18014483 490 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/23/18 DM0723118014496 490 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/24/18 DM0724118014523 520 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/25/18 DM0725/18014551 510 mg/kg D.W. 16 48 SWB46: 6010C MMSD 07/26/18 DM0726/18014570 500 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/27/18 DM0727/18014585 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/28/18 DM0728118014676 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/29/18 DM0729/18014910 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 07/30/18 DM0730/18014925 470 mg/kg D.W. 16 47 SW846: 6010C MMSD 07/31/18 DM0731/18014954 490 mg/kg D.W. 16 47 SW846: 6010C MMSD 08/01/18 DM0801/18014969 470 mg/kg D.W. 16 46 B8. SW846: 6010C MMSD 08/02/18 DMO802/18015140 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/03/18 DMO803/18015155 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 08/04/18 DM0804/18015252 470 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/05/18 DM0805/18015279 470 mg/kg D.W. 16 47 SW846: 6010C MMSD 08/06/18 DMO806/18015385 490 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/07/18 DM0807/18015414 510 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/08/18 DMO808/18015473 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/09/18 DMO809/18015500 520 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/10/18 DM0810/18015899 510 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/11/18 DM0811118015910 490 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/12/18 DM0812/18016203 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/13/18 JDM0813/18016216 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/14/18 DM0814/18016254 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 06/15/18 DMO815/18016281 500 mg/kg D.W. 16 46 SW846: 60100 MMSD 08/16/18 DM0816/18016300 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/17/18 DM0817/18016365 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/18/18 DM0818/18016505 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/19/18 DM0819118016525 500 mg/kg D.W. 16 46 SW846: 6010C T MMSD 08/20/18 J DMO820/18016539 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/21/18 DMO821118016714 490 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/22/18 DMO822/18016742 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/23/18 DMO823/18017352 4 510 mg/kg D.W. 16 46 SW846: 6010C MMSD Page 104 of 106 SYS/rptlMikMonthly 4110/13 tj Printed: 1/18/19 09.4) 09/08/18 DM0908/18018353 09/09/18 DM0909118018724 Annual Milorganite Report MMOJanuary 09/11/18 DM0911/18018825 09/12/18 DM0912/18018854 1 to December 31, 2018 DM0913/18018875 09/14/18 DM0914/18018891 09/15/18 09/16/18 DMO915/18019159 DMO916/18019178 09/17/18 DMO917/18019191 ZINC ICP METHOD 14WSample MMSD 540 mg/kg D.W. 16 46 SW846: 6010C :qe 08/24/18 ID DMO824/18017367 Result 500 mg/kg D.W. OP 16 LGQ .• Flags 46 Analytical Method SW846: 6010C Lab MMSD 08/25/18 DM0825/18017378 520 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/26/18 DMO826/18017397 510 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/27/18 DMO827/18017410 520 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/28/18 DM0828/18017434 530 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/29/18 DM0829/18017462 540 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/30/18 DM0830118017483 550 mg/kg D.W. 16 46 SW846: 6010C MMSD 08/31/18 DM0831/18017498 530 mg/kg D.W. 16 46 SW846: 6010C MMSD 09/01/18 DM0901/18017520 530 mg/kg D.W. 16 46 SW846: 6010C MMSD 09/07./18 DMO902/18017752 520 mg/kg D.W. 16 46 SW846: 6010C MMSD 09/03/18T DM0903/18018124 510 mg/kg D.W. 16 46 SW846: 6010C MMSD 09/04/18 DM0904/18018149 520 mg/kg D.W. 16 47 SW846: 6010C MMSD 09/05/18 DMO905/18018305 540 mg/kg D.W. 16 47 SW846: 6010C MMSD 09/08/18 DM0908/18018353 09/09/18 DM0909118018724 09/10/18 DMO910/18018799 09/11/18 DM0911/18018825 09/12/18 DM0912/18018854 09/13/18 DM0913/18018875 09/14/18 DM0914/18018891 09/15/18 09/16/18 DMO915/18019159 DMO916/18019178 09/17/18 DMO917/18019191 09/18/18 DMO918/18019447 09/21/18 DMO921/18019515 09/22/18 DMO922/18019574 09/23/18 DMO923/18019665 09/24/18 DMO924/18020088 09/25/18 DMO925/18020314 09/26/18 DMO92.6/18020343 09/27/18 DMO927/18020364 09/28/18 DM0928/18020380 530 mg/kg D.W. 16 47 SW846: 6010C MMSD 550 mg/kg D.W. 16 46 SW846: 6010C MMSD 570 mg/kg D.W. 16 46 SW846: 6010C MMSD 550 mg/kg D.W. 16 46 SW846: 6010C MMSD 540 mg/kg D.W. 16 46 SW846: 6010C MMSD 530 mg/kg D.W. 16 47 SW846: 6010C MMSD 540 mg/kg D.W. 16 46 SW846: 6010C MMSD 510 mg/kg D.W. 16 47 Q3. SW846: 6010C MMSD 500 mg/kg D.W. 16 47 SW846: 6010C MMSD 530 mg/kg D.W. 16 47 SW846: 6010C MMSD 490 mg/kg D.W. 16 47 SW846: 6010C MMSD 470 mg/kg D.W. 16 46 SW846: 6010C MMSD 480 mg/kg D.W. 16 48 490 mg/kg D.W. 15 45 500 mg/kg D.W. 16 46 500 mg/kg D.W. 15 45 500 mg/kg D.W. 16 46 490 mg/kg D.W. 16 46 460 mg/kg D.W. 16 47 470 mg/kg D.W. 16 47 440 mg/kg D.W. 16 48 SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD 09/29/18 DM0929/18020391 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 09/30/18 10/01/18 10/02/18 10/03/18 10/04/18 DM0930/18020411 DM1001/18021136 DM1002/18021162 DM1003118021190 DM1004118021541 440 mg/kg D.W. 450 mg/kg D.W. 450 mg/kg D.W. 450 mg/kg D.W. 520 mg/kg D.W. 16 16 16 16 16 47 46 47 47 46 SW846: 60100 SW846: 6010C SW846: 6010C SW846: 6010C SW846: 6010C MMSD MMSD MMSD MMSD MMSD 10/05/18 DM1005/18021557 520 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/06/18 DM1006/18021568 480 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/07/18 DM1007/18021588 480 mg/kg D.W. 16 45 SW846: 6010C MMSD 10/08/18 DM1008/18021602 480 mg/kg D.W. 16 45 SW846: 6010C MMSD 10/09/18 DM1009/18021627 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/10/18 DM1010118021656 490 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/11/18 DM1011/18021975 460 mg/kg D.W. 16 46 SW846: 6010C MMSD SY5/rptlMlloMonthly 1/10/13 0 Page 105 of 106 Printed., 1/18/19 09:9; 0 MMSD OfF7K7C W R PI;iML fYltN7NR17" Annual Milorganite Report January 1 to December 31, 2018 ZINC ICP METHOD 10/12/18 DM1012/18021991 450 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/13/18 DM1013/18022006 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/14/18 DM1014/18022026 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/15/18 DM1015/18022040 440 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/16/18 DM1016/18022065 450 mg/kg D.W. 16 46 4 SW846: 6010C MMSD 10/17/18 DM1017/18022094 450 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/18/18 DM1018118022133 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/19/18 DM1019/18022269 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/20/18 DM1020/18022280 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/21/18 DM1021/18022435 470 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/22/18 DM1022/18022449 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/23/18 DM1023/18022614 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/24/18 DM1024/18022643 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/25/18 DM 1025/18022708 440 mg/kg D.W. 16 47 SW846: 6010C MMSD 10/26/18 DM1026/18022767 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 10/27/18 DM1027/18022778 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/07/18 DM1107/18023991 500 mg/kg D.W. 16 45 SW846: 6010C MMSD 11/08/18 DM1108/18024012 480 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/09/18 DM1109/18024028 500 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/10/18 DM1110/18024523 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/11/18 DM1111/18024619 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/12/18 DM1112/18024633 400 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/13/16 DM 1113118025014 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/14/18 DM 1114/18025043 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/15/18 DM 1115/18025064 440 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/16/18 DM1116/18025080 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 11/17/18 DM1117118025093 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/18/18 DM1118/18025113 410 mg/kg D.W. 16 48 SW846: 6010C MMSD 11/19/18 DM 1119/18025127 410 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/20/18 DM1120/18025356 410 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/21/18 DM1121/18025385 410 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/22/18 DM 1122/18025406 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/23/18 DM1123/18025422 410 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/24/18 DM1124/18025750 400 mg/kg D.W. 16 48 SW846: 6010C MMSD 11/25/18 DM 1125/18025769 400 mg/kg D.W. 16 48 SW846: 6010C MMSD 11/26/18 DM1126/18025828 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/27/18 DM1127/18025860 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/28/18 DM1128/18025888 410 mg/kg D.W. 16 46 SW846: 6010C MMSD 11/29/18 DM 1129/18025956 460 mg/kg D.W. 16 47 SW846: 6010C MMSD 11/30/18 DM1130/18025971 410 mg/kg D.W 16 47 SW846: 6010C MMSD 12/01/18 DM 1201/18026182 400 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/02/18 DM1202/18026201 390 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/03/18 DM1203/18026214 f 400 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/04/18 DM1204/18026391 400 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/05/18 DM1205/18026578 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/06/18 DM1206/18026621 410 mg/kg D.W. 17 49 SW846: 6010C MMSD 12/07/18 DM1207118026797 410 mg/kg D.W. 16 48 SW846: 6010C MMSD SYS/rp"MiloMonthly 1/10/13 tj Page 106 of 106 Printed.' 1/18/19 09.'4; .r MMSD suwli RN i filto 4w!t4#flifY ZINC ICP METHOD Annual Milorganite Report January 1 to December 31, 2018 12/08/18 DM1208/18026808 430 mg/kg D.W. 16 48 B8. SW846: 6010C MMSD 12/09/18 DM1209/18026827 420 mg/kg D.W. 16 47 88. SW846: 6010C MMSD 12/10/18 DM1210/18026840 410 mg/kg D.W. 17 49 B8. SW846: 6010C MMSD 12/11/18 DM1211/18027102 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 12/12/18 DM1212/18027130 440 mg/kg D.W. 16 46 SW846: 6010C MMSD 12/13/18 DM1213/18027253 400 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/14/18 DM1214/18027306 420 mg/kg D.W. 16 46 SW846: 6010C MMSD 12/15/18 DM1215/18027317 380 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/16/18 DM1216/18027525 380 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/17/18 DM1217/18027540 390 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/18/18 DM1218/18027643 400 mg/kg D.W. 17 49 SW846: 6010C MMSD 12/19/18 DM1219/18027676 420 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/20/18 DM1220/18027805 430 mg/kg D.W. 16 46 SW846: 6010C MMSD 12/21/18 DM1221/18027821 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/22/18 DM1222/18027832 440 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/23/18 DM1223/18027852 450 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/24/18 DM 1224/18027883 430 mg/kg D.W. 16 _ 48 SW846: 6010C MMSD 12/25/18 DM1225/18027952 420 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/26/18 DM1226/18027969 430 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/27/18 DM1227/18027990 420 mg/kg D.W. 16 48 SW846: 6010C MMSD 12/28/18 DM1228/18028005 410 mg/kg D.W. 17 49 SW846: 6010C MMSD 12/29/18 DM1229/18028070 430 mg/kg D.W. 16 47 SW846: 6010C MMSD 12/30/18 y DM1230/18028089 460 mg/kg D.W. 16 46 SW846: 6010C MMSD 12/31/18 DM1231/18028102 450 mg/kg D.W. 16 47 SW846: 6010C MMSD Avg Result: 440 mg/kg D.W. Mian LOD: 3.1 mg/kg D.W. Max Result: 570 mg/kg D.W. Page 107 of 106 SYS/rptlMi/oMonthly 1/10/13 q Printed: 1/18119 09:97 NMSD Ww"AM1101 Fta4 De- a Pdons AO Other -- Flag requires additional explanation AX Qualified data - see contract lab report B3 Target analyte detected in method blank > 10% of sample concentration. B7 1 -CS recovery was above control limits. B8 LCS recovery was below control limits. B9 Low Level CCV recovery was outside of method acceptance limits CQ Data used for calculation of result was qualified 131 Duplicate precision control limit was exceeded. D2 Matrix spike precision control limit was exceeded. D3 Sample is heterogeneous. Sample homogeneity could not be readily achieved using routine laboratory practices. D4 Sample matrix interferences did not allow completing the analysis. DS The reported result is an estimate because the concentration of HEM in this sample exceeded the maximum allowed in the method for the sample volume collected. H1 Sample was received past holding time. H3 Analysis performed beyond holding time. H4 Initial analysis within holding time. Reanalysis for the required dilution was past holding time. HS Analysis performed beyond holding time. Annual Milorganite Report January 1 to December 31, 2018 IS Insufficient sample volume for analysis. ] Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit LA Not analyzed - lab accident. M1 Too numerous to count. M2 Sample incubation period outside method requirement. M3 Spreading colonies - unable to determine result. M4 Results are an approximation due to spreading colonies. MS Incubator/water bath temperature was outside method requirements. _ M7 Micro sample received without adequate headspace. M9 Target organism detected in associated method blank. NR Not usable data. (Water Quality only.) NU Not usable Data. P_2 Sample received with improper or inadequate chemical preservation. Q2 Matrix spike recovery for this sample was above control limits. Q3 Matrix spike recovery for this sample was below control limits. RT Sample temperature upon receipt exceeded regulatory or project requirements. SS Reading was not confirmed by a constant weight measurement SD Supplemental details provided. (Water Quality only.) T3 The dilution water D.O. depletion was > 0.2 mg/L. T4 GGA BOD was below method acceptance criteria. TS GGA BOD was above method acceptance criteria. T7 The dilution water D.O. increase was > 0.2 mg/L. T_8 Sample matrix did not allow adjusting sample pH for BOD. T9 Sample exceeded prescribed method temperature range. Page 108 of 106 SYS/rpflMiloMonrhly 1110113 hj Printed: 1118/19 09:4; in 1t"!'NHSD PARTNERS FOR A CLEANER ENVIRONMENT January 15, 2019 TO: Tom Nowicki and Steve Unger FROM: Zach Vogel COPY: A. Sotomayor, Lab File Memorandum SUBJECT: Annual PCB Milorganite Report --2018 Attached is the Annual PCB Milorganite report for the year 2018. Daily Milorganite samples are 24-hour composite samples, representative of a full day of production. All analyses were performed by Pace Analytical Services, Inc. in Green Bay, WI (Wisconsin Certification #: 405132750). full laboratory results are available upon request. There was no Milorganite production on the following dates: • September 19 through September 20,2018; • October 28 through November 5, 2018. Please coiatact the Central Laboratory if there are any questions or comments regarding these data. Data/Report Review By: Zach Vogel Date Laboratory Project Manager Milwaukee Metropolitan Sewerage District 260 West Seeboth Street, Milwaukee, WI 53204 2018 Milorganite Daily Production Samples PCB Aroclors (ppb)' COLLECTION DATE PCB -1242_ PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 1/1/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 1/2/18 < 54 < 54 < S4 < S4 < 54 < 54 < 54 <54 1/3/18 < 55 < 55 <55 < 55 < S5 < 55 < 55 < 55 1/4/18 < 54 < 54 < 54 < 54 < S4 < 54 < S4 < 54 1/5/18 < 55 < 55 <55 <55 < 55 < 55 < 55 < S5 1/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/7/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/8/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/9/18 < 55 < 55 < 55 < 55 <55 < 55 < 55 < 55 1/10/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/11/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/12/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 1/13/18 < 54 < 54 < 54 < 54 < 54 56 < 54 56 1/14/18 < 54 < 54 < 54 < 54 < 54 < S4 < 54 < 54 1/15/18 < 54 < 54 < 54 < 54 < 54 69 < 54 69 1/16/18 72 60 < 54 < 54 < 54 75 < 54 210 1/17/18 55 < 54 < 54 < 54 < 54 66 < 54 120 1/18/18 < 54 < S4 < 54 < 54 < 54 58 < 54 58 1/19/18 < S3 < 53 < 53 < 53 < 53 < 53 < 53 <53 1/20/18 < 53 < 53 < 53 < 53 < 53 57 < 53 57 1/21/18 < 54 < 54 < 54 < 54 < 54 54 < 54 54 1/22/18 < 55 < 55 < 55 < S5 < SS < 55 < 55 < 55 1/23/18 < 55 < 55 < 55 < SS < SS 61 < 55 61 1/24/18 < 53 < 53 < 53 < 53 < 53 69 < 53 69 1/25/18 < 52 56 <52 <52 <52 73 < 52 130 1/26/18 < 53 < 53 < 53 < 53 < 53 62 < S3 62 1/27/18 < 53 < 53 < 53 < 53 < 53 54 < 53 54 1/28/18 < 52 < 52 <52 < 52 < 52 < 52 < 52 <52 1/29/18 < 53 < 53 < 53 < 53 < 53 57 < 53 57 1/30/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 1/31/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 t 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)' PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCBAroclors 2/1/18 < 53 < 53 < S3 <S3 < 53 < 53 < 53 < 53 2/2/18 < 53 < S3 < S3 <53 < 53 < 53 < 53 < 53 2/3/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 < 53 2/4/18 < 54 < 54 < 54 < S4 < 54 < 54 < 54 < 54 2/5/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/7/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/8/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 2/9/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 2/10/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 2/11/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 2/12/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/13/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 2/14/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/15/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < S3 2/16/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 2/17/18 < 54 < 54 < 54 < 54 < 54 < S4 < 54 < 54 2/18/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/19/18 < 55 < 55 <55 < S5 < 55 < 55 < 55 < 55 2/20/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/21/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/22/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/23/18 < 52 < 52 < 52 <52 < 52 < 52 < 52 <52 2/24/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/25/18 < 53 88 < 53 < 53 <53 < 53 < 53 88 2/26/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 2/27/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2/28/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/1/18 < 55 < 55 < 55 <55 < 55 < 55 < 55 < SS 3/2/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/3/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)l PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 3/4/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/5/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/6/18 < 54 < 54 <54 < 54 < 54 < 54 < 54 < 54 3/7/18 < 55 < SS < 55 < 5S < SS < 55 < 55 < 55 3/8/18 < 54 < 54 <54 < 54 < 54 < 54 < 54 < 54 3/9/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 3/10/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/11/18 < 55 < 55 < 55 <55 < 55 < 5S < 55 < 55 3/12/18 < 55 < 55 < 55 <55 < 55 < 55 < 55 < 55 3/13/18 < 56 < 56 <56 < 56 < 56 < 56 < 56 <56 3/14/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 3/15/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < S4 3/16/18 < 55 < 55 <55 < 55 < 55 < 55 < 55 < 55 3/17/18 < 55 <55 < 55 <55 < 55 < 55 < 55 < 55 3/18/18 < 55 < 55 < 55 <5S < 55 < 55 < 55 < 55 3/19/18 < 56 < 56 < 56 <56 < S6 <56 < 56 < 56 3/20/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/21/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 3/22/18 < 53 < 53 < 53 < 53 < 53 < S3 < 53 < 53 3/23/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 3/24/18 < 54 < 54 < 54 < 54 < 54 < 54 < S4 < 54 3/25/18 < 55 < SS < 55 < 55 < 55 < 55 < 55 < 55 3/26/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 3/27/18 < 56 < 56 < S6 < 56 < 56 <56 <56 <S6 3/28/18 < 55 < 55 <55 < 55 < 55 < 55 < 55 < 55 3/29/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 3/30/18 < 56 < 56 <56 < 56 < 56 < 56 < 56 < 56 3/31/18 < 54 < 54 < 54 < S4 < 54 < 54 < 54 < 54 4/1/18 < 56 < 56 <56 <56 < 56 < S6 < 56 <56 4/2/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/3/18 < 56 < 56 <56 < 56 < 56 < 56 < 56 < 56 2018 Milorganite Daily Production Samples I PCB Aroclors (ppb)' COLLECTION DATE PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 4/4/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/5/18 < SS < 55 < SS < 55 < SS < 55 < 55 <55 4/6/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 4/7/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/8/18 < 56 < 56 < 56 < 56 < 56 < 56 <56 <56 4/9/18 < 55 < 55 < SS < 5S < SS < 55 < 55 <55 4/10/18 < 55 < SS < 55 < 55 < 55 < 55 < 55 <55 4/11/18 < 56 < 56 <56 <56 < S6 < 56 <56 <56 4/12/18 < 55 < 55 < 55 < 55 < SS < 55 < SS < SS 4/13/18 < 55 < 55 <55 < 55 < 55 < 55 < 55 < 5S 4/14/18 <54 < 54 < 54 < 54 < S4 < 54 < 54 < 54 4/15/18 < 55 < 55 < 55 < SS < 55 < SS < 55 < SS 4/16/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/17/18 < 54 < 54 < 54 < 54 <54 < S4 < 54 < 54 4/18/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 <55 4/19/18 < 54 < 54 < 54 <54 <54 < 54 < 54 < 54 4/20/18 < S3 < 53 < 53 < 53 < 53 < 53 < 53 <53 4/21/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/22/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 4/23/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 4/24/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/25/18 < 57 < 57 < 57 < 57 < 57 < 57 < 57 < 57 4/26/18 < 55 < S5 < 55 < 55 < 55 < 55 < 55 < 55 4/27/18 < 53 < S3 <53 < 53 < 53 < 53 < 53 <53 4/28/18 < 55 < 55 < S5 < 55 <55 < 55 < 55 < 55 4/29/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 4/30/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/1/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 5/2/18 < 55 < 55 < 55 < 55 < 55 < 55 < SS < 5S 5/3/18 <52 <52 < 52 <52 < 52 < 52 < 52 <52 5/4/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 <53 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)l PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 5/5/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 5/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/7/18 < 52 < 52 <52 < 52 < 52 < 52 <52 < 52 5/8/18 < 54 < 54 < 54 < S4 < 54 < 54 < 54 < 54 5/9/18 < 54 < 54 < 54 <54 < 54 < 54 < 54 < 54 5/10/18 < 54 < 54 < 54 < S4 < 54 < 54 < 54 < 54 S/11/18 <55 < 55 < 55 <55 < 55 < 55 < 55 < 55 5/12/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/13/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/14/18 < S5 < 55 < 55 < 55 <55 < SS < 55 < 55 5/15/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 5/16/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/17/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/18/18 64 < 55 < S5 < 55 < 55 < 55 < 55 64 5/19/18 < 55 < 55 <55 < 55 <55 < 55 < 55 < 55 5/20/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 5/21/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/22/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 5/23/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/24/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 5/25/18 < 54 < S4 < 54 < 54 < 54 < 54 < 54 <54 5/26/18 < 53 < S3 < 53 < 53 < 53 < 53 < 53 <53 5/27/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < SS 5/28/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 5/29/18 < 55 < 55 < 5S < 55 < 55 < 55 < 55 < 55 5/30/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 5/31/18 < 55 <55 < S5 < SS < 55 < 55 < 55 < 55 6/1/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 6/2/18 < 54 < 54 < 54 < 54 <54 < 54 < 54 < 54 6/3/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/4/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 i 2018 Milorganite Daily Production Samples PCB Aroclors (ppb)' COLLECTION DATE PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 6/5/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/7/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/8/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 6/9/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/10/18 < 53 < 53 <53 < 53 <53 < 53 < 53 <53 6/11/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/12/18 < 55 < 55 <55 < 55 < 55 < 55 < 55 < 55 6/13/18 < 55 <55 <55 < 55 < 55 < 55 < 55 < 55 6/14/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/15/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/16/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 6/17/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 6/18/18 < 54 <54 < 54 < 54 < 54 < 54 < 54 < 54 6/19/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/20/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 6/21/18 < 52 <52 < 52 < 52 < 52 < 52 < 52 <52 6/22/18 < 53 < S3 < 53 < 53 < 53 < S3 < 53 <53 6/23/18 < 52 <52 <52 < 52 < 52 60 < 52 60 6/24/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 6/25/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 <53 6/26/18 < 54 58 < 54 < 54 < 54 < 54 < 54 58 6/27/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 6/28/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 6/29/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 6/30/18 < 54 <54 < 54 < 54 < 54 < 54 < 54 < 54 7/1/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/2/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/3/18 < 54 < 54 < 54 < 54 <54 < 54 < 54 <54 7/4/18 < 53 58 < 53 < 53 < S3 < S3 < S3 58 7/5/18 < 53 62 < 53 < 53 < 53 < 53 < 53 62 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)l PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 7/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/7/18 < 54 58 < 54 < 54 < 54 < 54 < 54 58 7/8/18 < 53 < 53 < 53 < 53 <53 <53 < 53 < 53 7/9/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/10/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/11/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 7/12/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 7/13/18 <53 < 53 < 53 <53 < 53 < 53 < 53 < 53 7/14/18 <52 < 52 < 52 <52 <52 < 52 <52 < 52 7/15/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/16/18 < 53 < 53 < 53 < 53 <53 < S3 < 53 < 53 7/17/18 < 53 < 53 < 53 < 53 <53 < S3 < 53 < 53 7/18/18 < 53 61 < 53 < 53 <53 84 < 53 140 7/19/18 <52 53 <52 <52 < 52 < 52 < 52 53 7/20/18 < 54 120 < 54 < 54 < 54 55 < 54 180 7/21/18 < 52 < 52 < 52 <52 <52 < 52 < 52 <52 7/22/18 < 53 < 53 <53 < 53 < 53 < 53 < S3 < 53 7/23/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/24/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/25/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/26/18 < S4 56 < S4 < 54 < 54 < 54 < 54 S6 7/27/18 < 53 < 53 < 53 < 53 < 53 56 < 53 56 7/28/18 < 52 57 < 52 <52 < S2 < 52 < 52 57 7/29/18 < 52 56 < 52 <52 <52 < 52 < S2 56 7/30/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 7/31/18 < S3 < 53 < 53 < 53 < 53 < 53 < 53 < 53 8/1/18 <52 < 52 < 52 < 52 <52 < 52 <52 < 52 8/2/18 < 53 < 53 < 53 <53 <53 < 53 < S3 < 53 8/3/18 < 53 < 53 < 53 < 53 <53 < 53 < 53 < 53 8/4/18 < 52 <52 <52 <52 <52 < 52 < 52 < 52 8/5/18 < 53 < 53 < 53 < S3 < 53 < 53 < 53 < 53 2018 Milorganite Daily Production Samples TDO L kglON DATE PCB Aroclors (ppb)1 PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 8/6/18 < 52 < 52 <S2 < 52 < 52 < 52 < 52 < 52 8/7/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 8/8/18 < 53 < 53 < 53 < 53 < 53 < S3 < 53 < 53 8/9/18 < 53 < 53 < 53 < 53 < 53 56 < S3 56 8/10/18 < S3 < 53 < S3 < S3 < 53 66 < 53 66 8/11/18 < 53 < 53 < 53 < 53 <53 65 < S3 65 8/12/18 < 52 < 52 <S2 < 52 < 52 82 < S2 82 8/13/18 < 52 < 52 <52 < 52 < 52 67 < 52 67 8/14/18 < 52 < 52 < 52 <52 < 52 < 52 < 52 <52 8/15/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 <53 8/16/18 < 52 < 52 <52 < 52 < 52 < 52 < 52 <52 8/17/18 < 53 < 53 < 53 < 53 < 53 < 53 <53 <53 8/18/18 < 52 < 52 <52 < 52 < 52 < 52 < 52 <52 8/19/18 < 52 < 52 <52 <52 < 52 < 52 < 52 <52 8/20/18 < 52 < 52 <52 < 52 < 52 58 < 52 58 8/21/18 < 53 < 53 <53 <53 <53 < 53 < 53 < 53 8/22/18 < 52 < 52 <52 < 52 <52 < 52 < 52 <52 8/23/18 57 65 <52 < 52 <52 87 < 52 210 8/24/18 61 62 < 52 < 52 <S2 88 < 52 210 8/2S/18 <56 83 < 56 < 56 < 56 100 < 56 190 8/26/18 < 52 <52 <52 < S2 < 52 69 <S2 69 8/27/18 < S2 60 < 52 < 52 < 52 78 < 52 140 8/28/18 < 52 < 52 <52 < 52 < 52 79 < 52 79 8/29/18 < 52 <52 < 52 < 52 < 52 71 < 52 71 8/30/18 < 53 < 53 < 53 < 53 < 53 71 < 53 71 8/31/18 < 53 63 < 53 < 53 < 53 74 < 53 140 9/1/18 71 <52 <52 < 52 <52 80 < 52 150 9/2/18 67 <52 <52 < 52 <52 72 < 52 140 9/3/18 62 < 53 < 53 < 53 < 53 66 < 53 130 9/4/18 57 < 54 < 54 < 54 < 54 65 < 54 120 9/5/18 62 <53 < 53 < 53 < 53 73 < 53 130 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)' PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 9/6/18 64 54 <53 < 53 <53 67 < 53 180 9/7/18 70 58 <53 < 53 <53 82 < 53 210 9/8/18 69 66 <52 < 52 <52 87 < 52 220 9/9/18 59 57 <52 <S2 < 52 76 < S2 190 9/10/18 64 55 <53 < 53 <53 80 < 53 200 9/11/18 < 54 < 54 < 54 < 54 < 54 77 < 54 77 9/12/18 < 53 < 53 < 53 <53 < 53 82 < 53 82 9/13/18 < 54 < 54 < 54 < 54 < 54 72 < 54 72 9/14/18 < 54 < 54 <54 < 54 <54 77 < 54 77 9/15/18 < 54 57 < 54 < 54 < 54 68 < 54 120 9/16/18 < 54 < 54 < 54 < 54 < S4 60 < 54 60 9/17/18 < 53 58 <53 < 53 < 53 71 < 53 130 9/18/18 < 54 < 54 < 54 < 54 < 54 73 < 54 73 9/21/18 < 52 < 52 <52 <52 < 52 80 < 52 80 9/22/18 < 52 63 <52 <52 <52 78 < 52 140 9/23/18 <51 56 <51 <51 <51 64 < 51 120 9/24/18 < 52 54 <52 < 52 <52 62 < 52 120 9/25/18 54 56 <52 < 52 <52 68 < 52 180 9/26/18 < 53 < 53 < 53 < 53 < 53 60 < 53 60 9/27/18 < 53 < 53 <S3 < 53 <53 64 < 53 64 9/28/18 63 57 < SS < 55 <S5 75 < 55 200 9/29/18 < 53 < 53 <53 < 53 <53 58 < 53 58 9/30/18 < 53 < 53 <53 <53 <53 64 < 53 64 10/1/18 < 53 < 53 < 53 <53 <53 70 < 53 70 10/2/18 < 53 < 53 <53 <53 <53 69 < 53 69 10/3/18 < 53 < 53 <53 < 53 < S3 < 53 < 53 < 53 10/4/18 < 52 < S2 < 52 <52 < 52 S9 < 52 59 10/5/18 < 53 < 53 <53 < 53 < S3 < 53 < 53 < 53 10/6/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 10/7/18 < 52 160 <52 <52 < 52 69 < 52 220 10/8/18 < 52 < 52 <52 <52 <52 54 < 52 54 2018 Milorganite Daily Production Samples PCB Aroclors (ppb)l COLLECTION DATE PCB -1242 PGB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 10/9/18 <52 < 52 <52 < 52 < 52 < 52 < 52 < 52 10/10/18 < 53 < 53 <53 < 53 < 53 < S3 < S3 < 53 10/11/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 <S3 10/12/18 < 52 < 52 <52 <52 < 52 < 52 < 52 <52 10/13/18 < 54 < 54 < 54 < 54 < S4 < 54 < 54 < 54 10/14/18 < 53 < 53 < S3 <53 < S3 < 53 < 53 <53 10/15/18 < 54 < 54 < 54 < 54 < 54 < 54 < S4 < 54 10/16/18 < 53 < 53 < 53 < 53 < S3 < 53 < 53 < 53 10/17/18 < 53 < 53 < S3 < 53 < 53 < 53 < 53 < 53 10/18/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 <53 10/19/18 < 54 < S4 < S4 < S4 < 54 < 54 < 54 < 54 10/20/18 < 52 < S2 <S2 <52 < 52 < 52 < 52 <52 10/21/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 10/22/18 < 52 <52 < 52 < 52 < 52 < 52 < 52 <52 10/23/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 10/24/18 < 53 < 53 < 53 <53 <53 < 53 < 53 <53 10/25/18 < 53 < 53 < 53 <53 <53 < S3 < 53 < 53 10/26/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 <53 10/27/18 < 52 < 52 <52 <52 <52 < 52 < 52 < 52 11/7/18 <51 <51 <51 <51 <51 <Sl <51 <51 11/8/18 < 52 <52 < 52 <52 < 52 < 52 < 52 < S2 11/9/18 < 52 < 52 <52 < 52 < 52 < 52 < 52 < 52 11/10/18 <52 < 52 <52 <S2 < S2 < 52 < 52 <52 11/11/18 < 52 < 52 <52 <52 < S2 < 52 < 52 <52 11/12/18 < 53 < 53 <53 < 53 < S3 < 53 < 53 < 53 11/13/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 < 53 11/14/18 < 54 57 < 54 < 54 < 54 < 54 < 54 57 11/15/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 11/16/18 < SS < 55 < 55 < 55 < 55 < 55 < 55 < 55 11/17/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 11/18/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 <54 2018 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)' PCB4242 PCB -125 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 11/19/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 11/20/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 11/21/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 11/22/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 < 53 11/23/18 < 54 < S4 < 54 < 54 < 54 < 54 < 54 < 54 11/24/18 < 55 < SS < 55 < 55 < 55 < 55 < 55 < 55 11/25/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 11/26/18 < 52 < 52 <52 < S2 <52 < 52 < 52 < 52 11/27/18 < 52 < 52 < 52 < 52 <52 < 52 < 52 < 52 11/28/18 < 52 < 52 <52 <52 <52 < 52 < 52 < 52 11/29/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 11/30/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/1/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/2/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 < 53 12/3/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 12/4/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/5/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/6/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 12/7/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 12/8/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/9/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/10/18 < 56 < 56 <56 < 56 <56 < 56 <S6 < 56 12/11/18 < 53 < 53 < 53 < 53 <53 < 53 <S3 < 53 12/12/18 <52 < 52 <52 < 52 <52 < 52 <52 <52 12/13/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/14/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 12/15/18 < 53 < 53 <53 < 53 < 53 < 53 < 53 < 53 12/16/18 < S4 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/17/18 < 55 < 55 < 55 < S5 < 55 < 55 < 55 <55 12/18/18 < 56 < 56 <56 < 56 < 56 < 56 < 56 < 56 12/19/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 k 2018 Milorganite Daily Production Samples I PCB Aroclors (ppb)' COLLECTION DATE PCB -1242 PCB -1254 PCB -1221 PCB -1232 PCB -1248 PCB -1260 PCB -1016 Total PCB Aroclors 12/20/18 < 53 < 53 < 53 <53 < 53 < 53 < 53 < 53 12/21/18 < 27 < 27 < 27 < 27 < 27 < 27 < 27 < 27 12/22/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/23/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/24/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/25/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 12/26/18 < 55 < 55 < 55 < 55 < 55 < 55 < 55 < 55 12/27/18 < 56 < 56 < 56 < 56 < 56 < 56 < 56 <56 12/28/18 < 56 < 56 < 56 < 56 < 56 < 56 < 56 <56 12/29/18 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 12/30/18 < 53 < 53 < 53 < 53 < 53 < 53 < 53 < 53 12/31/18 < 54 56 < 54 < 54 < 54 < 54 < 54 56 amples analyzed by Pace Analytical Services, Green Bay, Wisconsin (WI Certification #405132750) by EPA 8082. All P results reported on a dry weight basis. MMSD W W A Ciito WW f March 3/10/18 Monthly Milorganite: Priority Pollutant and VOC Analysis March 2018 Milo. Priority Pollutant Sample 1,2,4-Trichlorobenzene Dry wt. 3/19/18 < 1300 ug/kg D.W. 1300 890 AX. 8270D Test America Buffalo 1,2-Diphenylhydrazine Dry wt. 3/19/18 < 990 ug/kg D.W. 990 D.W. 8270D Test America Buffalo 2,4,6 -Trichlorophenol Dry wt. i 3/19/18 < 1800 ug/kg D.W. 1800 ug/kg 8270D Test America Buffalo 2,4-Dichlorophenol Dry wt. 3/19/18 < 940 ug/kg D.W. 940 AX. 8270D Test America Buffalo 2,4 -Dimethylphenol Dry wt. 3/19/18 < 2100 ug/kg D.W. 2100 8270D Test America Buffalo 2,4-Dinitrophenol Dry wt. 3/19/18 < 41000 ug/kg D.W. 41000 8270D Test America Buffalo 2,4-Dinitrotoluene Dry wt. 3/19/18 < 1800 ug/kg D.W. 1800 8270D Test America Buffalo 2,6-Dinitrotoluene Dry wt. 3/19/18 < 1000 ug/kg D.W. 1000 AX. 8270D Test America Buffalo 2-Chloronaphthatene Dry wt. 3/19/18 < 1500 ug/kg D.W. 1500 8270D Test America Buffalo 2 -Chlorophenol Dry wt. 3/19/18 < 1600 ug/kg D.W. 1600 AX. 8270D Test America Buffalo 2-Nitrophenol Dry wt. 3/19/18 < 2500 ug/kg D.W. 2500 8270D Test America Buffalo 3,3'-Dichlorobenzidine Dry wt. 3/19/18 < 10000 ug/kg D.W. 10000 8270D Test America Buffalo 4,4 -DDD Dry wt. 3/16/18 < 6.8 ug/kg D.W. 6.8 AX. 8081B Test America Buffalo 4,4 -DDE Dry wt. 3/16/18 < 7.3 ug/kg D.W. 7.3 AX. 8081B Test America Buffalo 4,4 -DDT Dry wt. 3/16/18 < 8.2 ug/kg D.W. 8.2 AX. 8081B Test America Buffalo 4,6-Dinitro-o-Cresol Dry wt. 3/19/18 < 8900 ug/kg D.W. 8900 8270D Test America Buffalo 4-Bromophenyl Phenyl Ether Dry wt. 3/19/18 < 1300 ug/kg D.W. 1300 8270D Test America Buffalo 4 -Chloro -phenyl -phenyl ether Dry wt. 3/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo 4-Nitrophenol Dry wt. 3/19/18 < 6200 ug/kg D.W. 6200 8270D Test America Buffalo A -BHC -Alpha Dry wt. 3/16/18 9.1 ug/kg D.W. 6.3 J 80816 Test America Buffalo Acenaphthene Dry wt. 3/19/18 < 1300 ug/kg D.W. 1300 8270D Test America Buffalo f Acenaphthylene Dry wt. 3/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo Aldrin Dry wt. 3/16/18 < 8.6 ug/kg D.W. 8.6 AX. 80816 Test America Buffalo ALUMINUM ICP Dry wt. 3/16/18 4200 mg/kg D.W. 4.6 6010C Test America Buffalo Anthracene Dry wt. 3/19/18 < 2200 ug/kg D.W. 2200 8270D Test America Buffalo ANTIMONY ICP Dry wt. 3/16/18 < 0.42 mg/kg D.W. 0.42 6010C Test America Buffalo ARSENIC ICP Dry wt. 3/16/18 4 mg/kg D.W. 0.42 6010C Test America Buffalo B -BHC -Beta Dry wt. 3/16/18 < 6.3 ug/kg D.W. 6.3 80816 Test America Buffalo Benzidine Dry wt. 3/19/18 < 110000 ug/kg D.W. 110000 8270D Test America Buffalo Benzo(a)Anthracene Dry wt. Benzo(a)Pyrene Dry wt. Benzo(b)Fluoranthene Dry wt. Benzo(g,h,i)Perylene Dry wt. Benzo(k)Fluoranthene Dry wt. BERYLLIUM ICP Dry wt. BHC -Delta Dry wt. Bis(2-Chloroethoxy)Methane Dry wt. Bis(2-Chloroethyl)Ether Dry wt. Bis(2-Chloroisopropyl)Ether Dry wt. Bis(2-Ethylhexyl)Phthalate Dry wt. BORON ICP Dry wt. Butyl Benzyl Phthalate Dry wt. CADMIUM ICP Dry wt. 3/19/18 < 890 ug/kg D.W. 890 AX. 8270D Test America Buffalo 3/19/18 < 1300 ug/kg D.W. 1300 AX. 8270D Test America Buffalo 3/19/18 < 1400 ug/kg D.W. 1400 AX. 8270D Test America Buffalo 3/19/18 < 940 ug/kg D.W. 940 8270D Test America Buffalo 3/19/18 3/16/18 3/16/18 3/19/18 3/19/18 3/16/18 3/19/18 3/16/18 < 1100 ug/kg D.W. 0.087 mg/kg D.W 12 ug/kg D.W. < 1900 ug/kg D.W. < 1100 ug/kg D.W. < 1800 ug/kg D.W. 12000 ug/kg D.W. 16 mg/kg D.W < 1500 ug/kg D.W. 0.58 mg/kg D.W 1100 AX. 0.029 J 6.5 J 1900 1100 1800 3000 0.2 1500 AX. 0.031 8270D Test America Buffalo 6010C Test America Buffalo 80818 Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 6010C Test America Buffalo 8270D Test America Buffalo 6010C Test America Buffalo CALCIUM ICP Dry wt. 3/16/18 18000 mg/kg D.W. 3.4 6010C Test America Buffalo Page 1 of 5 SVS1rpt1 MltoPP 1110113 tj Panted. 4117118 09:54 eNIMSD %A11 R M! , (as N MC-11WIV, March 3/10/18 Chlordane Dry wt. CHROMIUM ICP Dry wt. Chrysene Dry wt. COBALT ICP Dry wt. COPPER ICP Dry wt. Cyanide - Total (solids) Dibenzo(a,h)Anthracene Dry wt. Dieldrin Dry wt. Diethyl Phthalate Dry wt. Dimethyl Phthalate Dry wt. Di. n- Butylphthalate Dry wt. Di-n-octyl phthalate Dry wt. Endosulfan alpha Dry wt. Endosulfan beta Dry wt. Endosulfan Sulfate Dry wt. Endrin Aldehyde Dry wt. Endrin Dry wt. Fluoranthene Dry wt. Fluorene Dry wt. Heptachlor Dry wt. Monthly Milorganite: Priority Pollutant and VOC Analysis March 2018 Milo. Priority Pollutant Sample 3/16/18 < 78 ug/kg D.W. 78 80818 Test America Buffalo 3/16/18 170 mg/kg D.W. 0.21 6010C Test America Buffalo 3/19/18 < 2000 ug/kg D.W. 2000 8270D Test America Buffalo 3/16/18 4.6 mg/kg D.W. 0.052 6010C Test America Buffalo 3/16/18 190 mg/kg D.W. 0.22 6010C Test America Buffalo 3/28/18 3.2 mg/kg D.W. 0.48 AX. 9012B Test America Buffalo 3/19/18 < 1600 ug/kg D.W. 1600 8270D Test America Buffalo 3/16/18 < 8.4 ug/kg D.W. 8.4 AX. 3/19/18 3/19/18 < 1100 < 1000 ug/kg ug/kg D.W. D.W. 1100 1000 3/19/18 < 1500 ug/kg D.W. 1500 AX. 3/19/18 < 1000 ug/kg D.W. 1000 AX. 3/16/18 < 6.7 ug/kg D.W. 6.7 AX. 3/16/18 < 6.3 ug/kg D.W. 6.3 LEAD ICP Dry wt. 3/16/18 13 ug/kg D.W. 6.5 3 AX 3/16/18 < 8.9 ug/kg D.W. 8.9 AX. 3/16/18 < 6.9 ug/kg D.W. 6.9 AX. 3/19/18 1000 ug/kg D.W. 940 3 3/19/18 < 1000 ug/kg D.W. 1000 < 1100 ug/kg D.W. 3/16/18 < 7.6 ug/kg D.W. 7.6 3/16/18 8081B Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 8081B Test America Buffalo 80818 Test America Buffalo 8081B Test America Buffalo 8081B Test America Buffalo 8081B Test America Buffalo 8270D Test America Buffalo 8270D Test America Buffalo 80818 Test America Buffalo Heptachlorepoxide Dry wt. Hexachlorobenzene Dry wt. 3/16/18 3/19/18 < 9 ug/kg D.W. < 1200 ug/kg D.W. 9 1200 AX. AX. 80818 8270D Test America Buffalo Test America Buffalo Hexachlorobutadiene Dry wt. Hexachlorocyclopentadiene Dry wt. Hexachloroethane Dry wt. 3/19/18 3/19/18 3/19/18 < 1300 ug/kg D.W. < 1200 ug/kg D.W. < 1100 ug/kg D.W. 1300 1200 1100 8270D 8270D 8270D Test America Buffalo Test America Buffalo Test America Buffalo Indeno(1,2,3-cd)Pyrene Dry Wt. 3/19/18 < 1100 ug/kg D.W. 1100 AX. 8270D Test America Buffalo IRON ICP Dry wt. 3/16/18 27000 mg/kg D.W. 3.6 6010C Test America Buffalo Isophorone Dry wt. 3/19/18 < 1900 ug/kg D.W. 1900 8270D Test America Buffalo LEAD ICP Dry wt. 3/16/18 35 mg/kg D.W. 0.25 6010C Test America Buffalo MAGNESIUM ICP Dry wt. MANGANESE ICP Dry wt. 3/16/18 3/16/18 5900 mg/kg D.W. 2500 mg/kg D.W. 0.96 0.033 6010C 6010C Test America Buffalo Test America Buffalo MERCURY by M. 7471 (sludge) 3/26/18 0.29 mg/kg D.W. 0.0082 AX. 74718 Test America Buffalo MOLYBDENUM ICP Dry wt. 3/16/18 9.6 mg/kg D.W. 0.14 6010C Test America Buffalo Naphthalene Dry wt. 3/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo NICKEL ICP Dry wt. 3/16/18 25 mg/kg D.W. 0.24 6010C Test America Buffalo Nitrobenzene Dry wt. 3/19/18 < 990 ug/kg D.W. 990 8270D Test America Buffalo N-Nitrosodimethylamine Dry wt. 3/19/18 < 3800 ug/kg D.W. 3800 8270D Test America Buffalo N-Nitrosodi-n-propylamine Dry wt. 3/19/18 < 1500 ug/kg D.W. 1500 AX. 8270D Test America Buffalo N-Nitrosodiphenylamine Dry wt. 3/19/18 < 7200 ug/kg D.W. 7200 8270D Test America Buffalo PCB -1016 3/16/18 < 0.043 mg/kg D.W. 0.043 8082A Test America Buffalo PCB -1221 PCB -1232 3/16/18 3/16/18 < 0.043 mg/kg D.W. < 0.043 mg/kg D.W. 0.043 0.043 8082A 8082A Test America Buffalo Test America Buffalo PCB -1242 3/16/18 < 0.043 mg/kg D.W. 0.043 8082A Test America Buffalo PCB -1248 SY8/rpt1miloPP 1110113 tj 3/16/18 < 0.043 mg/kg D.W. 0.043 8082A Test America Buffalo Page 2 of 5 Printed. 4117118 09:54 T t Monthly Milorganite: Priority Pollutant and VOC Analysis MMSD March 2018 WA.Cluel March 3110/18 Milo. Priority Pollutant Sample PCB -1254 3/16/18 < 0.1 mg/kg D.W. 0.1 8082A Test America Buffalo PCB -1260 _ 3/16/18 < 0.1 mg/kg D.W. 0.1 8082A Test America Buffalo p -Chloro -m -Cresol Dry wt. T 3/19/18 < 2200 ug/kg D.W. 2200 �^ 8270D Test America Buffalo Pentachlorophenol Dry wt. 3/19/18 < 8900 ug/kg D.W. 8900 8270D Test America Buffalo Phenanthrene Dry wt. 3/19/18 < 1300 ug/kg D.W. 1300 AX. 8270D Test America Buffalo Phenol Dry wt. 3/19/18 < 1400 ug/kg D.W. 1400 8270D Test America Buffalo PHOSPHORUS ICP Dry wt. 3/21/18 14000 mg/kg D.W. 71 SM 4500 P E Test America Buffalo Pyrene Dry wt. 3/19/18 1300 ug/kg D.W. 1000 1 8270D Test America Buffalo SELENIUM ICP Dry wt. 3/16/18 1.3 mg/kg D.W. 0.42 1 6010C Test America Buffalo SILVER ICP Dry wt. 3/16/18 1.7 mg/kg D.W. 0.21 6010C Test America Buffalo SODIUM ICP Dry wt. 3/16/18 2200 mg/kg D.W. 14 6010C Test America Buffalo Solids for dry weight determination (Test America) 3/27/18 94 % 0.1 Moisture Test America Buffalo Solids for dry weight determination (Test America) 3/27/18 94 % 0.1 Moisture Test America Buffalo Solids for dry weight determination (Test America) 3/27/18 94 % 0.1 Moisture Test America Buffalo THALLIUM ICP Dry wt. 3/16/18 < 0.31 mg/kg D.W. 0.31 6010C Test America Buffalo Total PCB Aroclors 3/16/18 < 0.1 mg/kg D.W. 0.1 8082A Test America Buffalo Toxaphene Dry wt. 3/16/18 < 200 ug/kg D.W. 200 8081B Test America Buffalo Y-BHC-Gamma(Lindane) Dry wt. 3/16/18 < 6.4 ug/kg D.W. 6.4 8081B Test America Buffalo ZINC ICP Dry wt. 3/16/18 340 mg/kg D.W. 0.67 6010C Test America Buffalo Page 3 of 5 SYS/rpfI MiloPP 1/10/13 fj Printed 4/17/18 09 54 eN,MSD "W 101 Q1i++H t19�1Y[Y' March 3/12/18 1,1,1 -Trichloroethane Dry wt. 1,1,2,2 -Tetrachloroethane Dry wt. 1,1,2 -Trichloroethane Dry wt. 1,1-Dichloroethane Dry wt. Monthly Milorganite: Priority Pollutant and VOC Analysis March 2018 Milo. Priority Pollutant Sample 3/21/18 < 270 ug/kg D.W. 270 8260C Test America Buffalo 3/21/18 < 160 ug/kg D.W. 160 8260C Test America Buffalo 3/21/18 < 200 ug/kg D.W. 200 8260C Test America Buffalo 3/21/18 < 300 ug/kg D.W. 300 8260C Test America Buffalo 1,1-Dichloroethylene Dry wt. 3/21/18 < 340 ug/kg D.W. 340 8260C Test America Buffalo 1,2 -Dichlorobenzene Dry Wt. 1,2-Dichloroethane Dry wt. 1,2-Dichloropropane Dry wt. 1,3 -Dichlorobenzene Dry Wt. 1,4 -Dichlorobenzene Dry Wt. 2 Chloroethylvinyl Ether Dry wt. Acrolein Dry wt. Acrylonitrile Dry wt. Benzene Dry wt. Bromodichloromethane Dry wt. Bromoform Dry wt. Carbon Tetrachloride Dry wt. Chlorobenzene Dry wt. Chloroethane Dry wt. Chloroform Dry wt. cis-1,3-Dichloropropene Dry wt. Dibromochloromethane Dry wt. 3/21/18 < 250 ug/kg D.W. 250 3/21/18 < 400 ug/kg D.W. 400 3/21/18 3/21/18 3/21/18 < 160 < 260 < 140 ug/kg ug/kg ug/kg D.W. D.W. D.W. 160 260 140 3/21/18 3/21/18 < 310 < 2000 ug/kg ug/kg D.W. D.W. 310 2000 3/21/18 < 2400 ug/kg D.W. 2400 3/21/18 < 180 ug/kg D.W. 180 3/21/18 < 190 ug/kg D.W. 190 3/21/18 < 480 ug/kg D.W. 480 3/21/18 < 250 ug/kg D.W. 250 3/21/18 < 130 ug/kg D.W. 130 3/21/18 < 200 ug/kg D.W. 200 3/21/18 < 660 ug/kg D.W. 660 3/21/18 < 230 ug/kg D.W. 230 3/21/18 < 470 ug/kg D.W. 470 Ethylbenzene Dry wt. Methyl Bromide Dry wt. 3/21/18 3/21/18 < 280 ug/kg D.W. < 210 ug/kg D.W. 280 210 Methyl Chloride dry wt. 3/21/16 < 230 ug/kg D.W. 230 Methylene Chloride Dry wt. 3/21/18 210 ug/kg D.W. 190 1 AX Solids for dry weight determination (Test America) 3/27/18 Y 86 % 0.1 Tetrachloroethylene Dry wt. 3/21/18 < 130 ug/kg D.W. 130 Toluene Dry wt. 3/21/18 < 260 ug/kg D.W. 260 Trans-1,2-Dichloroethylene Dry wt. Trans-1,3-Dichloropropene Dry wt. 3/21/18 3/21/18 < 230 ug/kg D.W. < 95 ug/kg D.W. 230 95 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C 8260C Test America Buffalo Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C 8260C Test America Buffalo Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C 8260C Test America Buffalo Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo Moisture Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C 8260C Test America Buffalo Test America Buffalo Trichloroethylene Dry wt. 3/21/18 < 270 ug/kg D.W. 270 8260C Test America Buffalo Vinyl Chloride Dry wt. 3/21/18 < 320 ug/kg D.W. 320 8260C Test America Buffalo Page 4 of 5 SYs/rptiMiloPP 1110113 tj Printed: 411 711 8 09:54 r J. Milorganite: Priority Pollutant and VOC Analysis eMNSD Fall 2018 "MMAC11 September _ ^ 918/18 Milo. Priority Pollutant Sample 1,2,4-Trichlorobenzene Dry wt. 1,2-Diphenylhydrazine Dry wt. 2,4,6 -Trichlorophenol Dry wt. 2,4-Dichlorophenol Dry wt. 2,4 -Dimethylphenol Dry wt. 2,4-Dinitrophenol Dry wt. 9/19/18 9/19/18 9/19/18 9/19/18 9/19/18 9/19/18 < 1300 ug/kg D.W. < 1100 ug/kg D.W. < 1900 ug/kg D.W. < 1000 ug/kg D.W. T < 2300 ug/kg D.W. < 44000 ug/kg D.W. 1300 1100 1900 1000 2300 44000 8270D 8270D 8270D 8270D 8270D 8270D Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo 2,4-Dinitrotoluene Dry wt. 9/19/18 < 2000 ug/kg D.W. 2000 8270D Test America Buffalo 2,6-Dinitrotoluene Dry wt. 9/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo 2-Chloronaphthalene Dry wt. 9/19/16 < 1600 ug/kg D.W. 1600 8270D Test America Buffalo 2 -Chlorophenol Dry wt. 9/19/18 < 1.700 ug/kg D.W. 1700 6270D Test America Buffalo 2-Nitrophenol Dry wt. 9/19/18 < 2700 ug/kg D.W. 2700 8270D Test America Buffalo 3,3'-Dichlorobenzidine Dry wt. 9/19/18 < 11000 ug/kg D.W. 11000 8270D Test America Buffalo 4,4 -DDD Dry wt. 9/18/16 < 7.3 ug/kg D.W. 7.3 80816 Test America Buffalo 4,4 -DDE Dry wt. 9/18/18 < 7.9 ug/kg D.W. 7.9 80816 Test America Buffalo 4,4 -DDT Dry wt. 9/18/18 < 8.7 ug/kg D.W. 8.7 80818 Test America Buffalo 4,6-Dinitro-o-Cresol Dry wt. 9/19/18 < 9500 ug/kg D.W. 9500 8270D Test America Buffalo 4-Bromophenyl Phenyl Ether Dry wt. 9/19/18 < 1300 ug/kg D.W. 1300 8270D Test America Buffalo 4 -Chloro -phenyl -phenyl ether Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo 4-Nitrophenol Dry wt. 9/19/18 < 6700 ug/kg D.W. 6700 8270D Test America Buffalo A -BHC -Alpha Dry wt. 9/18/18 < 6.7 ug/kg D.W. 6.7 80818 Test America Buffalo Acenaphthene Dry wt. 9/19/18 < 1400 ug/kg D.W. 1400 8270D Test America Buffalo Acenaphthylene Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo Aldrin Dry wt. 9/18/18 < 9.2 ug/kg D.W. 9.2 8081B Test America Buffalo ALUMINUM ICP Dry wt. 9/18/18 8500 mg/kg D.W. 4.9 6010C Test America Buffalo Anthracene Dry wt. 9/19/18 < 2400 ug/kg D.W. 2400 8270D Test America Buffalo ANTIMONY ICP Dry wt. 9/18/18 2.4 mg/kg D.W. 0.45 1 6010C Test America Buffalo ARSENIC ICP Dry wt. 9/18/18 6.3 mg/kg D.W. 0.45 6010C Test America Buffalo B -BHC -Beta Dry wt. 9/18/18 < 6.7 ug/kg D.W. 6.7 80818 Test America Buffalo Benzidine Dry wt. 9/19/18 < 120000 ug/kg D.W. 120000 8270D Test America Buffalo Benzo(a)Anthracene Dry wt. 9/19/18 < 950 ug/kg D.W. 950 8270D Test America Buffalo Benzo(a)Pyrene Dry wt. 9/19/18 < 1400 ug/kg D.W. 1400 8270D Test America Buffalo Benzo(b)Fluoranthene Dry wt. 9/19/18 2000 ug/kg D.W. 1500 3 8270D Test America Buffalo Benzo(g,h,i)Perylene Dry wt. 9/19/18 < 1000 ug/kg D.W. 1000 8270D Test America Buffalo Benzo(k)Fluoranthene Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo BERYLLIUM ICP Dry wt. 9/18/18 0.19 mg/kg D.W. 0.031 J 6010C Test America Buffalo BHC -Delta Dry wt. 9/18/18 < 7 ug/kg D.W. 7 80816 Test America Buffalo Bis(2-Chloroethoxy)Methane Dry wt. 9/19/18 < 2000 ug/kg D.W. 2000 8270D Test America Buffalo Bis(2-Chloroethyl)Ether Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo Bis(2-Chloroisopropyl)Ether Dry wt. 9/19/18 < 1900 ug/kg D.W. 1900 8270D Test America Buffalo Bis(2-Ethylhexyl)Phthalate Dry wt. 9/19/18 14000 ug/kg D.W. 3300 8270D Test America Buffalo BORON ICP Dry wt. 9/18/18 19 mg/kg D.W. 0.21 AX. 6010C Test America Buffalo Butyl Benzyl Phthalate Dry wt. 9/19/18 < 1600 ug/kg D.W. 1600 8270D Test America Buffalo CADMIUM ICP Dry wt. 9/18/18 0.84 mg/kg D.W. T 0.034 6010C Test America Buffalo CALCIUM ICP Dry wt. 9/18/18 27000 mg/kg D.W. 3.7 AX. 6010C Test America Buffalo SYS/rptlWoPP 1110113 tj Page 1 of 5 Printed: 12/21118 13:18 Milorganite: Priority Pollutant and VOC Analysis el"N'NSD Fall 2018 September 9/8/18 Milo. Priority Pollutant Sample Chlordane Dry wt. 9/18/18 260 ug/kg D.W. 83 1 8081B Test America Buffalo CHROMIUM ICP Dry wt. 9/18/18 210 mg/kg D.W. 0.22 6010C Test America Buffalo Chrysene Dry wt. 9/19/18 < 2100 ug/kg D.W. 2100 8270D Test America Buffalo COBALT ICP Dry wt. 9/18/18 5 mg/kg D.W. 0.056 6010C Test America Buffalo COPPER ICP Dry wt. 9/18/18 230 mg/kg D.W. 0.24 6010C Test America Buffalo Cyanide - Total (solids) 9/18/18 6 mg/kg D.W. 0.53 AX. 90128 Test America Buffalo Dibenzo(a,h)Anthracene Dry wt. 9/19/18 < 1700 ug/kg D.W. 1700 8270D Test America Buffalo Dieldrin Dry wt. 9/18/18 < 9 ug/kg D.W. 9 80818 Test America Buffalo Diethyl Phthalate Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo Dimethyl Phthalate Dry wt. 9/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo Di-n-Butylphthalate Dry wt. 9/19/18 < 1600 ug/kg D.W. 1600 8270D Test America Buffalo Di-n-octyl phthalate Dry wt. 9/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo Endosulfan alpha Dry wt. 9/18/18 < 7.2 ug/kg D.W. 7.2 8081B Test America Buffalo Endosulfan beta Dry wt. 9/18/18 18 ug/kg D.W. 6.7 J 80818 Test America Buffalo Endosulfan Sulfate Dry wt. 9/18/18 < 7 ug/kg D.W. 7 8081B Test America Buffalo Endrin Aldehyde Dry wt. 9/18/18 < 9.6 ug/kg D.W. 9.6 8081B Test America Buffalo Endrin Dry wt. 9/18/18 < 7.4 ug/kg D.W. 7.4 80818 Test America Buffalo Fluoranthene Dry wt. 9/19/18 1400 ug/kg D.W. 1000 1 8270D Test America Buffalo Fluorene Dry wt. 9/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo Heptachlor Dry wt. 9/18/18 < 8.1 ug/kg D.W. 8.1 8081B Test America Buffalo Heptachlorepoxide Dry wt. 9/18/18 < 9.6 ug/kg D.W. 9.6 8081B Test America Buffalo Hexachlorobenzene Dry wt. 9/19/18 < 1300 ug/kg D.W. 1300 8270D Test America Buffalo Hexachlorobutadiene Dry wt. 9/19/18 < 1400 ug/kg D.W. 1400 8270D Test America Buffalo Hexachlorocyclopentadiene Dry wt. 9/19/18 < 1300 ug/kg D.W. 1300 8270D Test America Buffalo Hexachloroethane Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo Indeno(1,2,3-cd)Pyrene Dry Wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo IRON ICP Dry wt. 9/18/18 33000 mg/kg D.W. 3.9 6010C Test America Buffalo Isophorone Dry wt. 9/19/18 < 2000 ug/kg D.W. 2000 8270D Test America Buffalo LEAD ICP Dry wt. 9/18/18 63 mg/kg D.W. 0.27 6010C Test America Buffalo MAGNESIUM ICP Dry wt. 9/18/18 9500 mg/kg D.W. 1 AX. 6010C Test America Buffalo MANGANESE ICP Dry wt. 9/18/18 2000 mg/kg D.W. 0.036 AX. 60100 Test America Buffalo MERCURY by M. 7471 (sludge) 9/18/18 0.49 mg/kg D.W. 0.0091 74718 Test America Buffalo MOLYBDENUM ICP Dry wt. 9/18/18 9.5 mg/kg D.W. 0.15 6010C Test America Buffalo Naphthalene Dry wt. 9/19/18 < 1200 ug/kg D.W. 1200 8270D Test America Buffalo NICKEL ICP Dry wt. 9/18/18 40 mg/kg D.W. 0.26 6010C Test America Buffalo Nitrobenzene Dry wt. 9/19/18 < 1100 ug/kg D.W. 1100 8270D Test America Buffalo N-Nitrosodimethylamine Dry wt. 9/19/18 < 4000 ug/kg D.W. 4000 8270D Test America Buffalo N-Nitrosodi-n-propylamine Dry wt. 9/19/18 < 1600 ug/kg D.W. 1600 8270D Test America Buffalo N-Nitrosodiphenylamine Dry wt. 9/19/18 < 7700 ug/kg D.W. 7700 8270D Test America Buffalo PCB -1016 9/21/18 < 0.05 mg/kg D.W. 0.05 8082A Test America Buffalo PCB -1221 9/21/18 < 0.05 mg/kg D.W. 0.05 8082A Test America Buffalo PCB -1232 9/21/18 < 0.05 mg/kg D.W. 0.05 8082A Test America Buffalo PCB -1242 9/21/18 < 0.05 mg/kg D.W. 0.05 8082A Test America Buffalo PCB -1248 9/21/18 < 0.05 mg/kg D.W. 0.05 8082A Test America Buffalo Page 2 o/ 5 SYS1rpt1Mi1oPP 1/10/13 tj Printed: 12/21/18 13:18 J. Milorganite: Priority Pollutant and VOC Analysis eMNSD Fall 2018 KM Rit A C1M MW4111' September 9/8/18 Milo. Priority Pollutant Sample PCB -1254 PCB -1260 p -Chloro -m -Cresol Dry wt. Pentachlorophenol Dry wt. Phenanthrene Dry wt. Phenol Dry wt. PHOSPHORUS ICP Dry wt. POTASSIUM ICP Dry wt. Pyrene Dry wt. SELENIUM ICP Dry wt. SILVER ICP Dry wt. SODIUM ICP Dry wt. Solids for dry weight determination (Test America) Solids for dry weight determination (Test America) 9/21/18 9/21/18 9/19/18 9/19/18 9/19/18 9/19/18 9/26/18 9/18/18 9/19/18 9/18/18 9/14/18 9/14/18 < 0.12 mg/kg D.W. < 0.12 mg/kg D.W. < 2400 ug/kg D.W. < 9500 ug/kg D.W. < 1400 ug/kg D.W. < 1500 ug/kg D.W. 17000 mg/kg D.W. 3000 mg/kg D.W. 1500 ug/kg D.W. 2.3 mg/kg D.W. 0.12 8082A Test America Buffalo 0.12 2400 8082A 8270D Test America Buffalo Test America Buffalo 9500 8270D Test America Buffalo 1400 1500 77 22 1100 1 0.45 J 1.9 mg/kg D.W. 0.22 1200 mg/kg D.W —89 90 % THALLIUM ICP Dry wt. 9/18/18 < 0.34 mg/kg D.W. Y-BHC-Gamma(Lindane) Dry wt. ZINC ICP Dry wt. SYS/rptW1oPP 1110113 tj 9/21/18 < 0.12 mg/kg D.W. 9/18/18 < 220 ug/kg D.W. 9/18/18 < 6.9 ug/kg D.W. 9/18/18 510 mg/kg D.W. 15 8270D 8270D SM 4500 P E 6010C 8270D 6010C 6010C 6010C 0.1 Moisture 0.1 Moisture 0.34 6010C 0.12 8082A 220 80818 6.9 80818 0.72 AX. 6010C Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Page 3 of 5 Printed: 12121118 13:19 Milorganite: Priority Pollutant and VOC Analysis -e'kNSD Fall 2018 September 9/10/18 Milo. Priority Pollutant Sample 1,1,1-Trichloroethane Dry wt. 9/17/18 < 1.8 ug/kg D.W. 1.8 8260C Test America Buffalo 1,1,2,2-Tetrachloroethane Dry wt. 9/17/18 < 4 ug/kg D.W. 4 8260C Test America Buffalo 1,1,2-Trichloroethane Dry wt. 1,1-Dichloroethane Dry wt. 1,1-Dichloroethylene Dry wt. 1,2-Dichlorobenzene Dry Wt. 1,2-Dichloroethane Dry wt. 1,2-Dichloropropane Dry wt. 1,3-Dichlorobenzene Dry Wt. 1,4-Dichlorobenzene Dry Wt. 2-Chloroethylvinyl Ether Dry wt. Acrolein Dry wt. Acrylonitrile Dry wt. Benzene Dry wt. Bromodichloromethane Dry wt. Bromoform Dry wt. Carbon Tetrachloride Dry wt. Chlorobenzene Dry wt. 9/17/18 < 3.2 ug/kg D.W. 3.2 8260C 9/17/18 < 3 ug/kg D.W. 3 8260C 9/17/18 < 3 ug/kg D.W. 3 8260C 9/17/18 < 1.9 ug/kg D.W. 1.9 9/17/18 < 1.2 ug/kg D.W. 1.2 9/17/18 < 12 ug/kg D.W. 12 9/17/18 < 1.3 ug/kg D.W. 1.3 9/17/18 < 3.5 ug/kg D.W. 3.5 9/17/18 < 12 ug/kg D.W. 12 9/17/18 < 39 ug/kg D.W. 39 AX. 9/17/18 < 22 ug/kg D.W. 22 9/17/18 1.3 ug/kg D.W. 1.2 3 9/17/18 < 3.3 ug/kg D.W. 3.3 9/17/18 < 12 ug/kg D.W. 12 9/17/18 < 2.4 ug/kg D.W. 2.4 9/17/18 < 3.3 ug/kg D.W. 3.3 Chloroethane Dry wt. 9/17/18 < 5.6 ug/kg D.W. 5.6 Chloroform Dry wt. 9/17/18 < 1.5 ug/kg D.W. 1.5 cis- 1,3-Dichloropropene Dry wt. 9/17/18 < 3.6 ug/kg D.W. 3.6 Dibromochloromethane Dry wt. 9/17/18 < 3.2 ug/kg D.W. 3.2 Ethylbenzene Dry wt. 9/17/18 < 1.7 ug/kg D.W. 1.7 Methyl Bromide Dry wt. 9/17/18 < 2.2 ug/kg D.W. 2.2 8260C 8260C 8260C 8260C 8260C 8260C 8260C Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo 8260C Test America Buffalo Methyl Chloride dry wt. 9/17/18 < 1.5 ug/kg D.W. 1.5 8260C Test America Buffalo Methylene Chloride Dry wt. 9/17/18 55 ug/kg D.W. 11 8260C Test America Buffalo Solids for dry weight determination (Test America) 9/17/18 93 % 0.1 Moisture Test America Buffalo Tetrachloroethylene Dry wt. 9/17/18 < 3.3 ug/kg D.W. 3.3 8260C Test America Buffalo Toluene Dry wt. 9/17/18 5.7 ug/kg D.W. 1.9 1 8260C Test America Buffalo Trans-1,2-Dichloroethylene Dry wt. 9/17/18 < 2.5 ug/kg D.W. 2.5 8260C Test America Buffalo Trans- 1,3-Dichloropropene Dry wt. 9/17/18 < 11 ug/kg D.W. 11 8260C Test America Buffalo Trichloroethylene Dry wt. 9/17/18 < 5.4 ug/kg D.W. 5.4 8260C Test America Buffalo Vinyl Chloride Dry wt. 9/17/18 < 3 ug/kg D.W. 3 8260C Test America Buffalo Page 4 of 5 SYS/rp( MIOPP11101131j Printed: 12/21/1813:18 Milorganite Dioxin Toxic Equivalent Concentrations 2018 Measured Concentration (p(g/9 or t Factor AS Congener 11131201812t.1012018 3/1012018 4x712018 161121201W 6/9/2018 717/2018 8111/2018 9/8/2018 10113/2018 11/17/2018 12/8/2018 EPA Maine 1746-01-6 2,3,7,8- Tetrachlorodibenzo-p-dioxin 0 0 0 0 0 0 0 0 0 0 0 0 1.0 1.0 40321-76-4 1,2,3,7,8- Pentachlorodibenzo-p-dioxin 0 0 0 0 0 0 0 0 0 0 0 0 1.0 0.5 39227-28-6 1,2,3,4,7,8- Hexachlorodibenzo-p-dioxin 0 0 0 0 0 0 5.5 0.0 5.9 6.3 0 0 0.1 0.1 57653-85-7 1,2,3,6,7,8- Hexachlorodibenzo-p-dioxin 0 0 7.4 6.8 82 6.3 15 9.4 16 14 5.9 5.9 0.1 0.1 19408-74-3 1,2,3,7,8,9- Hexachlorodibenzo-p-dioxin 0 0 0.0 0.0 7.00 5.9 12 7.5 14 12 0 0 0.1 0.1 35822-46-9 1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin 59 74 130 120 150 140 310 220 340 360 150 140 0.01 0.01 3268-87-9 1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin 560 760 1300 1100 1300 1300 2900 2300 3000 3400 1500 1400 0.0001 0.001 51207-31-9 2,3,7,8- Tetrachlorodibenzofuran 8.3 34 20.0 12.0 5.3 5.3 5.7 6 8.7 5.3 3.2 3.1 0.1 0.1 57117-41-6 1,2,3,7,8- Pentachlorodibenzofuran 0 0 0 0 0 0 0 0 0 0 0 0 0.05 0.05 57117-31-4 2,3,4,7,8- Pentachlorodibenzofuran 20 110 56 31 11 12 16 13 22 6.4 0 7.7 0.5 0.5 70648-26-9 1,2,3,4,7,8- Hexachlorodibenzofuran 0 0 0 0 0 0 9.7 0 8.2 7.2 0 0 0.1 0.1 57117-44-9 1,2,3,6,7,8- Hexachlorod ibenzofu ran 0 0 0 0 0 0 12 0 11 8.3 0 0 0.1 0.1 72918-21-9 1,2,3,7,8,9- Hexachlorod ibenzofu ran 0 0 0 0 0 0 0 0 0 0 0 0 0.1 0.1 60851-34-5 2,3,4,6,7,8- Hexachlorod ibenzofu ran 0 0 0.0 0 0 0 7.6 0 11 9.6 0 0 0.1 0.1 67562-39-4 1,2,3,4,6,7,8-Heptachlorodibenzofuran 19 0 0 50 65 76 0 100 180 170 64 0 0.01 0.01 55673-89-7 1,2,3,4,7,8,9- Heptachlorodibenzofuran 0 0 0.0 0 0 0 8.6 0 9 7.2 0 0 0.01 0.01 39001-02-0 1,2,3,4,6,7,8,9-Octachlorodibenzofu ran 40 69 130 100 120 140 300 190 310 330 140 150 0.0001 0.001 32598-13-3 3,3',4,4'- Tetrachlorobiphenyl 184 279 201 202 188 255 402 319 409 421 251 254 0.0001 0.0005 70362-50-4 3,4,4',5-Tetrachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.0001 57465-28-8 3,3',4,4',5- Pentachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.1 0.1 32598-14-4 2,3,3',4,4'- Pentachlorobiphenyl 1200 1210 1160 1330 1020 1370 2410 1760 2680 2430 1400 1420 0.0001 0.0001 31508-00-6 2,3',4,4',5- Pentachlorobiphenyl 2670 2710 1680 2860 2300 3300 5420 4330 5780 5640 3300 3000 0.0001 0.0001 65510-44-3 2',3,4,4',5- Pentachlorobiphenyl 0 0 0 0 0 0 0 0 0 127 0 0 0.0001 0.0001 74472-37-0 2,3,4,4',5- Pentachlorobiphenyl 0 0 0 0 0 0 172 107 126 142 0 0 0.0005 0.0005 32774-16-6 3,3',4,4',5,5'- Hexachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.01 0.01 38380-08-4 2,3,3',4,4',5-Hexachlorobiphenyl 631 589 580 581 469 605 1090 790 1310 1190 619 589 0.0005 0.0005 69782-90-7 2,3,3',4,4',5'- Hexachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.0005 0.0005 52663-72-6 2,3',4,4',5,5'-Hexachlorobiphenyl 221 194 191 177 144 203 368 264 375 356 204 0 0.00001 0.00001 39635-31-9 2,3,3',4,4',5,5'- Heptachlorobiphenyl 0 0 0 0 0 0 0 105 200 169 0 0 0.0001 0.0001 35065-30-6 2,2',3,3',4,4',5-Heptachlorobiphenyl 1580 1650 1630 1380 1280 1390 3130 2430 3640 2380 1350 1150 0.0001 69782-91-8 2,2',3,4,4',5,5'-Heptachlorobiphenyl 4090 4130 4310 4030 3470 3820 8990 6470 10300 5490 3130 2590 0.0001 LTotalEPA Toxic Equivalent (TEQ) 12.4 59.9 32.8 19.9 10.4 10.9 19.7 133 25.7 16.8 4.0 7.1 Maine Toxic Equivalent (TEQ) 13.6 61.4 34.7 21.6 12.3 12.8 24.0 16.6 30.3 21.1 6.0 8.9 ..situ. 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