WQ0035720_Annual Report_20190207

Denali
WATER SOLUTIONS
January30, 2019
3308 !smite Avenue
"Al AR 72802
PO BOK 3036 • Ruohlb, AR 72811
ftm: 419498-0500
North Carolina Department of Environment and Natural Resources RECEI' fr!^ fk'Incrn iTMR
Division of Water Quality
Information Processing Unit FEB 7 2019
1617 Mail Service Center
Raleigh, NC 27699-1617 Non-D � Ye
Permil'ung Unit
Subject: 2018 Annual Report - Distribution of Class A Residuals: Denali Water
Solutions (Lake Kilby Water Treatment Plant) Permit No. W00035720
To Whom it May Concern:
Denali Water Solutions is submitting the required 2018 Annual Report for Permit No.
W00035720. This permit is associated with the distribution of water treatment residuals
produced at the City of Portsmouth - Lake Kilby Water Treatment Plant located in Suffolk,
Virginia, with distribution in Gates County, North Carolina.
This Annual Report contains the following information:
• Form DMSDF
• Form RSSF RFrFIVF®
• Form MFLSF FE11 0 7 ?019
• Form FSF
• Lab Reports DWR SECTION
NFORWTION PROCESSING UNIT
If you have any questions, or need any additional information, please do not hesitate to
contact me at [phone] or via email at Jeff retzkePdenaliwater com.
JEff Retzke
Senior Environmental Manager, East Region
cc: Nathan Litteral (Water Plant Manager, City of Portsmouth, Virginia)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
VQ PERMIT #: WQ0035720 FACILITY NAME: Lake Kilby Water Treatment Plant
PHONE: [phone] COUNTY: Suffolk, VA OPERATOR: Nathan Litteral (Water Plant Manager)
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
'as the facilitv in operation durine the past calendar year? Yes 2 No ❑ If No skip parts A, B, C and certify form below
Part A*: Part B*:
Volume (dry tons) Recipient Information
Month Sources(s) (include NPDES # if Amendment/
applicable) n..11.:— A ---4- 1 Residual In I Product Out Name(s) Volume (dry tons) Intended use(s)
Inu
.arch
Dril
ine
;ptember
ctober Lake Kilby WTP 0 605.81 605.81 See FSF 605.81 Soil Amendment
ovember Lake Kilby WTP 0 1323.18 1323.18 See FSF 1323.18 Soil Amendment
ecember Lake Kilby WTP 0 406.21 406.21 See FSF 406.21 Soil Amendment
Total from FORM DMSDF (sup)
)tals: Annual (dry tons): 0' 2335.2 2335.2 2335.2
Amendments used: 1 Bulking Agent(s) used:
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
in C:
acility was compliant during the past calendar year with all conditions of the land application permit R] Yes
acluding but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No 0 If No, Explain in Narritive
All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
malties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Digitally signed by Jeff Retzke
f ii DN: rn=Jeff HeVke, o=Denah
z Water, ou, i ? 'email=[e-mail]
m, r-U$
Date: 2019.01.3017:03:14-06'00'
gnature of Permittee
Date Signature of Preparer* *
(if different from Permittee)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0035720 Laboratory:
Facility Name: Lake Kilby WTP
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
1) Waypoint Analytical, Richmond, VA
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
m /k a
Sample or Composite Date
9/26/18
9/26/18
10/06/18
10/06/18
10/23/18
10/23/18
Max
Percent Solids (%)
NA
13.42
13.66
14.72
14.88
14.8
15.13
15.13
Arsenic
75
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
85
1
1
1
2
1
1
2
Copper
4,300
144
151
55
49
87
89
151
Chromium
NA
167
172
153
157
135
140
172
Lead
840
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
57
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molybdenum
75
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
420
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
100
5
5
5
5
15
5
5
Zinc
7,500
108
104
162
161
255
270
270
Total Phosphorus
NA
2320
2070
2020
1830
1520
1440
2320
TKN
NA
7740
7610
7270
7190
7770
7860
7860
Ammonia -Nitrogen
NA
1120
1320
1020
1140
945
1120
1320
Nitrate and Nitrite
NA
2.31
2.34
2.29
2.29
2.37
2.33
2.37
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penaltir- I"---'--~ittjpg gjAWrmation, including the possibility of fines and imprisonment for knowing violations."
DN:cn Jeff Retzke,o=Denali
1! .� Water, ou,
&,naliFi,[e-mail]
ria
* Date: Signatur., .,l 1 1 VYal\.1 JJ 2019.01.3017:02:55-06'00' Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 455.47
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
Acres Used: 58.2 Acres Permitted: 58.2 Site #: NC-GT-03 Field #: 1
Residual Analvsis Data (Heavv Metals and Total Phosphorus use my/ku. % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
9/26/18
21
9/26/18
3
10/6/18
4
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids
13.42
13.66
14.72
14.88
14.8
15.13
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium.167
172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
tiemim
2.5
2.5
2.5
5
2.5
2:5
5
Nickel 1
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
Heavy Metal Meld Loadings
(Ualculated in ins/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
y
DT/Ac./
C
App.
Event
7.83
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000 .
0.00.0;
0,000
0' 000
0.000
0.000
0.18S
0.10
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0031
0.031
Copper
0.000
0.000
0.000 '
0.000
0.000
0.000 ,'
0.000
0.0.00
0.000
0.000
0.000
2.363
2.363
Chromium
OA00
0.000
0.000 `
0.000
0.000
0.000
! OA00'
0.000
O'.000
0.000
0.000
2692
2.692
Lead
0.000
0.000
0.000 `
0.000
0.000
0.000
0.000.
0.000
0000
0.000'
0.000
0.321
0.321 :
Mercury
0.000
0.000
0,000 ,':
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,006
0.006
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
! 0.000
0.000
0.000
0.000
0.000
0.078
0.078
Nickel
0.000
0.000
0.000 '
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.202
0.202
Selenium
0.000
0.000
0.000 'i
0.00'0
0.000
0.000
0.000
0.0.00
0.000
0.000
0.000
0 078
0.07$
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0.00
0.000
0.000°,
0.000
4 226
4.226
Total
Phos-
0.000
.0..000
0.066
0.000
Oa000
0.000
'' 0.000
0.000
0.000
0.000'
0.000
136.313
36.313',
nhorus'
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
iml " %,M9ydpgyjQlations".
D:cn=Jeff Retrke,o=Denali a
emretzke@denaliwater.c
'"'Oin;'t=US
Date: 2019.0130 17:07:55-06'00'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 1
Acres Utilized: 58.2
Land
Owner: Edwin Miller, etal
Annual Dry Tons Applied: 4554682
Site #: NC-GT-03
Acres Permitted: 58.2
Operator: Ed Miller Farms
Predominant Soil Series: NoA
Cation Exchange
Capacity (non 503): 42,300 mg/kg
Crop 1 Name: Wheat
Crop 1 Max. PAN: 123
Crop 2 Name:
N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
it
Precip.
Y
o
Nitrate
PAN Applied
Name of Crop Type
+J
enter one Solids/
( )
D
/D
Applied per
PP P
(NPDES #, WQ#,
Co
Past 24
0 b
K' �'
w* "
TKN
o 9
as o
and
( lbs/acre)
Receiving Residual
j
d
Liquid
9
Solids
Acre
Fert., Animal
(Dry'
Hrs.
o w
o
N'
w
CD �•
w
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Moist
inches
*
o'
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
Sept
2654
15.13
5.811
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
38.098
NA
Wheat
0
Oct
920.52
15.13
2.615
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
13.214
NA
Wheat
0
><
Residuals Applications totals on FORM FSF supp (attach
FORM
FSF supp to this form):
)TALS:
3574.52
o
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
51.312
0.0001
Lime A lied
nnual lbs/acre
0.185
0.031
2.363'
2.692
0:321
0.006
0.078
0.202
0.078
J. 4.226
3b 313
Date
lbs/ac
-ior Years Cumulative lbs/ac
0.362
0.064
3.78
4.374
0.222
0.014
0.161
0.51
0.184
7.02
urrent Cumulative lbs/ac
0.547
0.095
6.143'
7.066
0.543
0.020
0.239
0.712'
0.262
11.246
;rmitted C. P. L. R.****
36.49
34.71
1335
N/A
267
15.13
N/A
373.8
89
2492
xmit PAN Limit 1 st/2nd Crop........
123
N/A
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
aalified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation, includinL7 the possibility of fines and imprisonment for knowing violations."
Digitally signed by Jeff Re2ke
a / DN:—JeffRetzke,u=D-ail Water,0u, �*Application Method: S - Surface, IN - Injection, INC - Incorporation - email_,eH.retzke�denaliwater.cum.
**Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0
Date: i019.013017.0237 -WW
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinLFRate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 517.69
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: BoB
Acres Used: 59 Acres Permitted: 59 Site #: NC-GT-03 Field #: 9
Residual Analvsis Data (Heave Metals and Total Phosphorus use me/ka, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
9/26/18
2
9/26/18
3
10/6/18
_4j
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids
13.42
13.66
14.72 1
14.88
14.8
15.13
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium.167
172
153
157
135
140
172
Lead 1
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
1 5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
Heavy Metal Field Loadings
(Ualculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
H
DT/Ac./
0
App.
Event
8.78
Arsenic
0.000
0.000
0.000
O.D00
0.000
0.000
0.000
0.000
O.000
0.000
0.000
0.207.
0.207
Cadmium
0.0.00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0000
0.000
0.000
0035
0.035
Copper
0.000
0.000
OA00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2:b50
2.650
Chromium0.000
0.000
0.000 .`
0.000
0.000::.0.000
O.00OI
0.000
O;.000
0.000
0.000
3,019
3.019
Lead
0.000
0.000
:0.000
0.000
0.000
6.000 .
0.000'
0.000
0.000
' 0.000
0.0.00
0,360
0.360
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
': 0.000
0.0.00
0.000
0.000
0.000
0 007
0.007
Molyb-
demim
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000`:
0.000
0:088
0.088
Nickel
OA00
0.000
0.000 ;
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000 !
0.000
0.226
0.226
Selenium
0.000
0. .0
0.000 ''
0.000
0.000
6.000
0.000
0.000
O'.000
0.000
0.000
0.088
0.088
Zinc
0.0.0.0
0.000
0.000
0.000
0.000
0.000
` 0.0001
0.000
0.000
''. 0.000'
0.000
4,.739
4.739
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0 000
0.000'
0.000
40.3161,410.7116
ohorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imnrisonment for knowing violations".
Digitally signed by Jeff Retake
DN: cn=leH Retyce,=Denali
:AWater,au,
`email=feftrenlce@denaliwater.m
Date: 2019.013017:0737 -06'00'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 9
Acres Utilized: 59
Land
Owner: Edwin Miller, etal
Annual Dry Tons Applied: 5176916
Site #:
NC-GT-03
Acres Permitted: 59.0
Operator: Ed Miller Farms
Predominant Soil Series: BoB
Cation Exchange Capacity (non 503): 42,300 mg/kg
Crop 1 Name:
Wheat
Crop 1 Max. PAN: 102
Crop 2 Name:
N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
Precip.
Y
o
p 4
Z
Nitrate
PAN Applied
Name of Crop Type
a
(enter one) Solids/
%
Applied per
(NPDES #, W #,
Q
Cond.
Past 24
F b
w .-
w 'n
TKN
o
as o
and
( lbs/acre)
Receiving Residual
d °
Liquid
Solids
Acre
Fert., Animal
(Dry,
Hrs.
0a. w
*
�
N•
g w•
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Wet,
Moist
inches
* 0
o.
p
* w
o
mg/kg
mg/kg
mg/kg
Crop 1
Frop 2
Crop 1
Crop 2
Oct
875.02
15.13
1.890
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
12.391
NA '
Wheat
0
Nov
3187.83
15.13
6.895
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
45.141
NA
Wheat
0
)TALSf 4062MI
nnual lbs/acre
•ior Years Cumulative lbs/ac
urrent Cumulative lbs/ac
;rmitted C. P. L. R.****
xmit PAN Limit 1 st/2nd C
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
0207
0.035
2.650
3.019
0.360
0.007
0.088
0.226`
0.088
4.739
40.71
0.128
0.051
3.557
0
0.446
0.001
0.078
0.275
0.363
4.553
6.335
0.086 `
6.207`
3.019
0.806
0.008
0.166
0.501'
0.451
9.292
36.49
34.71
1335
N/A
267
15.13
N/A
373.8
89
2492
Lime Applied
Date I lbs/ac
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
.formation, including the Dossibility of fines and imprisonment for knowing violations."
Digitallysign hyJeHRet:ke
DN:m=IeffI—,o=Denah *Application Method: S - Surface, IN - Injection, INC - Incorporation
! t11=JeR.ret&e@denaliwaterca
! jii m;�'=v5 **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 147.89
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: GoA
Acres Used: 15.1 Acres Permitted: 15.1 Site #: NC-GT-03 Field #: 14
Residual Analvsis Data (Heavv Metals and Total Phosphorus use me/ke, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
9/26/18
2
9/26/18
3j
10/6/18
4j
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids
13.42
13.66
14.72
14.88
14.8
15.13
15.13
Arsenic 1
11.8
11.3
11.2
10
7.18
10.5 1
1
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium
167
1 172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
denilm
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annuai
tieavy ivtetai r ieia i,oaaings
kt-aicuiatea in iosiacre):
Total
1
2
3
4
5
6
7
81
9
10
ill
12
N
DT/Ac./
0
App.
Event
9.79
Arsenic
O.000
0.000
u00
0.000
01000
0.000
0.000
0.000
0.000
0.000
0.000
. 0.231
0.231
Cadmium
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
OvOW
0.000
0.09
0.039
Copper
0.000
0.000
0.000 :
0.000
0.000,::0.000
OA00 .
0.000
00000
0.000
0.000
1958
2.958'
Chromiu
0.00.0
0.000
0.000,
0.000
0.000,
0.000
0.000
0.000
0.000
0.000
3.3 69
3.369
Lead 1
0.000
0.000
Oa000
0.000
0.000
0.000
0.000
0.000
0.000
` 0.000
0.000
0 402
0.402..''
Mercury
0.000
0.000
0.000:,;
0.000
0.000
0.600
0.000
0.000
0.000
0.000!
0.000
0 008
0.008
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000''
0.000
0.098
0.098
Nickel
0.000
0.000
0.000
0.000
0.000
0.000::
0.000
0.000
0.000
;; 0.000'
0.000
0.253
0253
Selenium
0.000
0.000
0.000
0.000
0.000
U90
01000
0.000
0.000
' 0.000
0.000
0 098
0.098 `.
Zinc
0.000
ORO
0.000
0.000
0.06,0­1
0.000 `
0.000
0.000
Oaow
'i 0.000
0.000
5289
5.289
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000'
0.000
45.444
45.444'
nhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprknnmimt fot l�pOw�l} VlolatlOIIS".
ig0a ysigned y evke
D:cn=Jeff l7etzke, o=Denali
ater,au,
!' 'eT. jjZjeffretzke®denalimte co
c-S
Date: 2019.01301797:22 -0800'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX
WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 14
Acres Utilized: 15.1
Land Owner: Edwin Miller, etal
Annual Dry Tons Applied. 1478884
.............. Site #: NC-GT-03
Acres Permitted: 15.1
Operator: Ed Miller Farms
Predominant Soil Series: GoA
Cation Exchange
Capacity (non 503): 42,300 mg/kg
Crop 1 Name:
Wheat
Crop 1 Max. PAN: 136
Crop 2 Name: N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
Precip.
Y
cs
o
p _
Z
Nitrate
PAN Applied
Name of Crop Type
a
(enter one) Solids/
%
Applied per
(NpDES #, WQ#,
Cond.
past 24
b
8
�.
w 0
w
TKN
o o
n
and
(lbs/acre)
Receiving Residual
o
Liquid
Solids
Acre
Fert., Animal
(Dry.
Hrs.
Zr
o:
* 5
N•
] �,•
Nitrite
Application
PP
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Wet,
Moist)inches
a.
o
o'
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
Oct
1160.63
15.13
9.794
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
64.216 j
NA
Wheat
0
)TALS] I460.631 0�
nnual lbs/acre
-ior Years Cumulative lbs/ac
arrant ('mmillativa llhc/ar
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this
As Cd Cul CrI PbJHgJMoJ Nil Se Zn
0.23 11 0.039 2.958 3.369 0.402 0.008 1 0.098 0.253 0.098 5.289 _
0.297 0.052 3.253 3.305 0.0196 0.01 1 0.13 0.44 0.13 5.855
;rmitted C. P. L. R.**** 36.49 I 34.71J 1335 I N/A �267 15.13 I N/A 373.8 89 I 2492
;rmit PAN Limit lst/2nd Crop
Lime
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation, including the possibility of fines and imprisonment for knowing violations."
�; :ti DIg1U11y S19Ae by Jefi R,tk,
f� DN:an=,eBNehke,aDemIIW=,�• *Application Method: S - Surface, IN - Injection, INC - Incorporation
PU
:'. D.t,.3619.U-11-14 W **Volatilization Rate: Surface - 0.5. Iniection/Incoraoration - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinL7 Rate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual): 103.Q9
...
WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: GoA
11.7
Acres Permitted: 11.7 Site #: NC-GT-03 Field #:
16
Residual Analysis Data (Heavy Metals and Total Phosphorus use ma/ks, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
9/26/18
__2j
9/26/18
3
10/6/18
4
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids
13.42
13.66
14.72
14.88
14.8
15.13
1
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
1
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium
167
172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0:4
0.4
0.4
Molyb-
tipniim
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
heavy metal r lew Loadings
(ualculateci In lbs/acre):
Total
1
2
3
4
5
6
71
8
9
Al-11
12
DT/Ac./
o
App.
y
Event
8.81
Arsenic
0.000
0.000
O:000
0.000
0.000
0.000
0,000
4.000
0.000
0.000'
0.000
Q208
0.208
Cadmium
O.g00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
01.
.000
0.000
0.000
0 035
0,035
Copper
0.000
0,000 '
0,000 '
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0:000
2.661
2,661
Chromium.."0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0U0
3031
3,031
Lead
0.000 rr.0.000
0.000
0.000
0,000
0.000
O000
0.000
0.000
0.000
0.000
0361
0.361
Mercury
0.000
0.000
0.000
0.000
0.000
0.00Q
0.000
0.000
Q.000
O.000'
0.000
0 007
0.007
Molyb-
0.000
0.000
0.000 'i
0.000
0.000
0.000
O.00q
0.000
0.000
Q.000'
Q.000
0088
0.088
Nickel
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
00'00
0.000
0.000
0.000
0.227
1 0.227
Selenium
0.000
0.000
0.000 ''
0.000
0.000
0.000
O.00O
0.000
O.OQO .
0.000
0.000
0 08&
0.088
Zinc
0.000
0.000
0.000
0.000
0.000
.0.000'
0.000,
O.000
0.000
0.000'
0.000
4757
4.757
Total
Phos-
0.000
0.000
0.000 ''
0.000
0.000:0.000
0.000
0.000
0.000
0.000'
0.000
40.878
40.878
nhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
[ DigRall ,igned by JWR-ke
6DN,atiJeR V=Denali y
emnikje(Lretzke@ke@denaliwatenc
=US
Date: 2019.0130170106-0 '00'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 16
Acres Utilized: 11.7
Land Owner: Edwin Miller, etal
Annual Dry Tons Applied: ,1030860
Site #: NC-GT-03
Acres Permitted: 11.7
Operator: Ed Miller Farms
Predominant Soil Series: GoA
Cation. Exchange
Capacity (non 503): 42,300 mg/kg
Crop 1 Name: Wheat
Crop 1 Max. PAN: 136
Crop 2 Name:
N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
precip.
Y
o
0
Z ��
Nitrate
PAN Applied
Name of Crop Type
y
(enter one) Solids/
D/D
Applied per
(NpDES # WQ#,
Cond.
past 24
b
w <
�.
Py C
w "
TKN
o n
ac o
and
(lbs/acre)
Receiving Residual
g
Liquid
Solids
Acre
Fert., Animal(Dry
Wets '
Hrs.
o
CD
w
N•
g w•
Nitrite
Application
Crop 1
Crop 2
Crop 1
Crop 2
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)o•
Moist
inches
n
o
* w'
o
mg/kg
mg/kg
mg/kg
Oct
809.02
15.13
8.911
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
57.770
NA
Wheat
0
VWu:., .
Izum�
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
)TALS: 809.021, As Cd Cul CrJPbJHgJMoJ Nil Se Zn P 57.770 .000 0Lime Applied
nnual lbs/acre 0208 0.035 2.661,; 3.031 0.361 0.007 0.089 0.227 0.088 4.757 40 878 , Date lbs/ac
...:::..::.:.:
-ior Years Cumulative lbs/ac 0.329 0.058 3.61 3.668 0.218 0.012 0.144 0.488 0.144 6.498
urrent Cumulative lbs/ac 0.537 0.093 6.271 6.699 0.579 0.019 0.232 ' 0.715: 0.232 11 255
-rmitted C. P. L. R.**** 36.49 34.71 1335 N/A 267 15.13 N/A 373.8 89 2492
;rmit PAN Limit l st/2nd Crop
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation, includine the. possibility of fines and imprisonment for knowing violations."
i; Digitally signed by Jeff Reuke
r DN ^=,et(Re2ke,u=DenalWater, *Application Method: S - Surface, IN - Injection, INC - Incorporation
s:;ema�keff.retzkePdena�iwater.cnm.
eDS;, 1.3017A7:46-06'00' **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0
Date: 2079.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Lake Kilby WTP Total Dry Tons Applied (Annual): 430.45
WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
44.5 Acres Permitted: 44.5 Site #: NC-GT-03 Field #:
20
Residual Analvsis Data (Heavv Metals and Total PhosDhorus use me/kff. % Solids use Raw Percent #):
Sample or
Com-
posite
Date
L1J
9/26/18
2
9/26/18
3
10/6/18
4
10/6/18
5
10/23/18
6
10/23/18
7
8j
9
10
11 j
12
Max
% Solids
13.42
13.66
14.72
14.88
14.8
15.13
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium
167
172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
demim
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
Heavy Metal Yield Loadings
(Ualculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
o
App.
y
Event
9.67
Arsenic
0.000
0.000
0.., j0.000
0.000
00000
0.000
0.0'00
0.000
0.000
0.000
0228
0.228
Cadmium
0.000
0,000
0.000:1
0.000
0.000
0.000
0.000
0.0'00
0.000
0.000'
0.000
0.039
0.039
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.921
2.921
Chromium:,0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0'00
0.000
0.000
0.000
3.328
3.328
Lead
0.00.01z...,0.000
0.000
0.000
0.000
0.000
0.000
0.000
0..000
0.000'
0.000
0397
0.397
Mercury 1.
0.000
6.000
0.000
0.000
0.00V
11 0.000
0.000
0.000
0.000
0.00al.
0.000
4.008
0.008
Molyb-
clanum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.097
0.097
Nickel
0.000
0.000
0.000 '
O.O0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0 250
0.250
Selenium
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0097
0.097
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000''
0.000
5123
5.223
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
44.883
44.883'
Dhorus
"I certifv, under Denalty of law, that this document was ureDared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Dgrt Ily igned bykff R,uke
DN 1 fr RzkDenali
Wt
ff.retzk,@d.naLwaterxa
"m -1i5
Dale 2019.01.3017U6A9-06'00'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP WQ Permit #: WQ0035720 Field #: 20 Acres Utilized: 44.5
Land Owner: Edwin Miller, etal Annual Dry Tons Applied: 430A606 Site #: NC-GT-03 Acres Permitted: 44.5
Operator: Ed Miller Farms Predominant Soil Series: NoA Cation Exchange Capacity (non 503): 42,300 mg/kg
Crop 1 Name: Wheat Crop 1 Max. PAN: 123 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
precip.
�Y
c
z�
Nitrate
PAN Applied
Name of Crop Type
j
(enter one) Solids/
%
Applied per
(NpDES #, WQ#,
Cond.
past 24
b
w
Pd
TKN
o
on o
and
( Ibs/acre)
Receiving Residual
Liquid
Solids
Acre
Fert., Animal
(Dry,
e '
Hrs.
o
* sv
RL
g E.
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Moist
inches
$
* o'
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
Sept
1291.19
15.13
3.697
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
24.241
NA
Wheat
0
Oct
2087.07
15.13
5.976
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
59.184
NA j
Wheat
0
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
)TALS: 331.8i26 0 As Cd Cu Cr Pb H Mo Ni Se Zn P 63 425 4.000 Lime A lied
...
nnual lbs/acre 0.228 0.039 2 921 3.328 0.397 0;008 0.097 0.250; 0.097 5.223 44 883 Date I lbs/ac
-ior Years Cumulative lbs/ac 1 0.743 1 0.139 1 9.426 1 10.4 1 0.855 1 0.031 1 0.345 1 1.116 1 1.491 1 17.91
urrent Cumulative lbs/ac 0.971 0.178 12.347 13.728 1.252 D0391 0.442 1.. 1.366 1.588 23.133 [<
;rmitted C. P. L. R.****1 36.49 34.71 1335 N/A 1 267 15.13 N/A 373.8 1 89 1 2492
;rmit PAN Limit 1 st/2nd Crop 123 N/A ;r
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation, including the possibility of fines and imprisonment for knowing violations."
2. DigitallyaignedbyJeffRetzke
DN: cn=Jeff Retzke, o=Dena11 Water, ou,
j) jf m Application Method: S -Surface, IN -Injection, INC -Incorporation
lefl.retzke@denaliwatecmm,
Y {( Date:Im.01301TV29-0600' **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual): 539.42
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: GoA
Acres Used: 57.7 Acres Permitted: 57.7 Site #: NC-GT-03 Field #: 23
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
9/26/18
2
9/26/18
3
10/6/18
4
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids
13.42
13.66
14.72
14.88
14.8
15.13 1
1
1
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium
167
172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
demim
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
Heavy Metal Meld Loadings
(Ualculated in lbs/acre):
Total
1
2
3
4
5
6
:IF
81
9
10
111
12
DT/Ac./
APP•
Event
9.35
Arsenic
0.000
0000
0.000 :
0..000
.0.000
0.000
0.000
0.000
0.000
0.000'
11 0.000
0221
_'0.221
Cadmium
, 0.000
0:000
0.000 :
0:000
0.000
0.000 `
0.000
0.000
0.000
' 0.000
0.000
0:037
0.037''
Copper
0.000
0.000
0.000
0.00,0
O.000
0.000
0.000
0.000
Q.000
< 0.000
0.000
2;823
2.823
Chromium
0.000
0.000
0.000
0.000
0.000.
0.060:`
0.000
AAM
0.000
0.000
0.000
3?216
3.216
Lead
0.000
0000
0.000
0:000
OA00
0.000
0.000
0.000
0.000
0.000
0.000
0383
0.383
Mercury
0.000
0,000
0.000
0.000
0.000
0.000
0.000::0.0.00
0.000
0.000
0.000
O';007
0.007'
Molyb-
denum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0093
0.093
Nickel
0.00`0
0.000
0.000
0.000
0LL ..000
0.000
0.00'0
0.000
0.000
0.000
0.000
O.241
0.241
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0:093
0.093
Zinc
0:000
0000
-0.000
0000
O'000
0.000
0.000
0.000
0.000
0.000'
0.000
5048
5.048
Total
Phos-
0.000
0.000
0.000
0.000
0.000 ' ]
0.000
0.000
0.000
0.000
0.000
0.000
43.379
43.379'
vhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
V Y ! E msmnrvs dMimn.nt.
5 ortH�drx.o-t..o=o.,vu
4ma!�ett,.at<aeewn�cnmm
. me zoixm.3a nuers.ason
Signature of Land Applier

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX
WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 23
Acres Utilized: 57.7
Land Owner: Edwin Miller, etal
Annual Dry Tons Applied 539.4169
Site #: NC-GT-03
Acres Permitted: 57.7
Operator: Ed Miller Farms
Predominant Soil Series GoA
Cation Exchange Capacity (non 503): 42,300 mg/kg
Crop 1 Name:
Wheat
Crop 1 Max. PAN: 136
Crop 2 Name: N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
precip.
Y
�
o
o 4
Z
Nitrate
PAN Applied
Name of Crop Type
(enter one) Solids/
o
/o
Applied per
(1.1pDES #, WQ#,
Cond.
Past 24
c? b
7� w
w �.
7y
�, „
TKN
o
ac o
and
( lbs/acre)
Receiving Residual
b °
Liquid
Solids
Acre
Fert., Animal
(Dry'
Hrs.
a w
* N
N•
w•
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Wasteetc)
,
Wet'
Moist
inches
o
o
w
o
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
Oct
14233.35
1
15.13
9.349
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
61.297
NA.....;..•I
Wheat
1 0
Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form):
)TALS1 4233.35 : o. As I Cd I Cu I CrI PblHglMol Nil Se IZn P 61.297 0.000 Lime Applied
nnual lbs/acre
-ior Years Cumulative lbs/ac 1 o 1 0 0 1 0 1 0 1 0 1 0 1 0 1 0 I 0
urrent Cumulative lbs/ac
C. P. L. R.**** 1 36.49 1 34.71 1 1335 1 N/A 1 267 1 15.13 1 N/A 1 373.8 1 89 1 2492
xmit PAN Limit 1
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
.formation, includine the possibility of fines and imprisonment for knowing violations."
/, Olg,aly Igned byleHPetzke
r DN 1 HFepke, r-Denal Waler,
} 44 ,de@denalwat som, *Application Method: S -Surface, IN -Injection, INC -Incorporation
oa,e:2019.01301b,:,aW Volatilization Rate: Surface - 0.5, Iniection/Incornoration -1.0
Signature of Land Applier Date Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Lake Kilby WTP Total Dry Tons Applied (Annual):
Permit #: WQ0035720 Cation Exchange Capacity (non 503 only): 42,300 mg/kg
Operator: Ed Miller Farms Owner: Edwin Miller, etal Predominant Soil Series: NoA
Acres Used: 17 Acres Permitted: 17 Site #: NC-GT-03 Field #: 24
Residual Analvsis Data (Heave Metals and Total Phosphorus use me/ke, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
9/26/18
2
9/26/18
3
10/6/18
4
10/6/18
5
10/23/18
6
10/23/18
7
8
9
10
11
12
Max
% Solids 1
13.42
13.66
14.72
14.88
14.8
15.13 1
15.13
Arsenic
11.8
11.3
11.2
10
7.18
10.5
11.8
Cadmium
1
1
1
2
1
1
2
Copper
144
151
55
49
87
89
151
Chromium
167
172
153
157
135
140
172
Lead
18.5
20.5
10.1
8.1
11.8
13.1
20.5
Mercury
0.4
0.4
0.02
0.02
0.4
0.4
0.4
Molyb-
clemim
2.5
2.5
2.5
5
2.5
2.5
5
Nickel
12.4
1 12.4
11.5
11.3
12.8
12.9
12.9
Selenium
5
5
5
5
5
5
5
Zinc
108
104
162
161
255
270
270
Total
Phos-
horus
2320
2070
2020
1830
1520
1440
2320
Annual
Heavy 1Vletal Vield Loadings
(Ualculated in lbs/acre):
Total
1
2
31
81
9
10
ill12
DT/Ac./
°may
App.
Event
8.30
Arsenic
Q000
0.000
0.000
0.000
0.000
0 000 '
O.fl00
0.000
0.000
0.000
0.004
0 196
0:196 :
Cadmium
0,00:0
0.000
0.000
0.000
O.000
0.000
0.000
0.000
0.000
0.000'
0.000
0033
0,033
Copper
0..90
0.000
0.000
0.000
O.fl00
OA00 !
fl.000
0.000
Q.000
0.000
0.000
15.107
2,507
Chromium.:,
0,000
0.000
0:000
0.000
0,000
0.000 ':.
0.000
0.000
0.000
0.000I
0.000
2855.
2.855
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0340
0.340
Mercury
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000'
. 0.000
0007
0.007
Molyb-
0.000-::­0,000
0_fl00
0.000
0.000
0.000
0.000
0,000
0,000
0,000
' 0.000
0 0$3
... 0 0$3
Nickel
0.000
O.00O _..
0.000 ''
0.000
.....
0.000
O.00O
0.000
0.000
0.000
0.000
0,000
0214
Selenium
0.000
0000
!0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0083
_
0083 __
Zinc
0.000
0000
0.000 f
0.
.000
0.000
0,000
0.000
0.000
0.000
° 0.000
0.000
4482
4.482
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0 000
0.000
0.000
38.512
38.512''
nhorus
"I certify. under venalty of law. that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
F: DI9RaIlY sl9ned byJeff ReUke
/1 " •" mcn=JeRReKke, r�Denali
Wa. res ou,
!/ 'email,=jeR.reVke@derialiwalerw
c�tis:
Date: 2019.013012:06:16 -06'00'
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Lake Kilby WTP
WQ Permit #: WQ0035720
Field #: 24
Acres Utilized: 17
Land Owner: Edwin Miller, etal
Annual Dry Tons Applied. 1411071
Site #:
NC-GT-03
Acres Permitted: 17
Operator: Ed Miller Farms
Predominant Soil Series: NoA
Cation Exchange Capacity (non 503): 42,300 mg/kg
Crop 1 Name:
Wheat
Crop 1 Max. PAN: 123
Crop 2 Name:
N/A
Crop 2 Max. PAN: N/A
Volume applied
Volume
Residual Sources
Soil
precip.
y
o
4
Z
Nitrate
PAN Applied
Name of Crop Type
v
(enter one) Solids/
%
Applied per
(NPDES #, WQ#,
Cond.
past 24
�'E
w �'
.» ._
Pd a'
K
TKN
o
as o
and
( lbs/acre)
Receiving Residual
Liquid
Solids
Acre
Fert., Animal
(Dry,
e '
Hrs.
a m
* .
"
w•
]
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Moist
inches
o'
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
Oct
1107.41
15.13
8,300
WQ0035720
M
0
S
0.5
0.4
7860
1320
2.37
54 424
NA
Wheat
0
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
)TALS: t 107.41 o As Cd Cu Cr Pb H Mo Ni Se Zn P 54 424: ,0.006 Lime Applied
nnual lbs/acre 0.196 0,033' 2.507 2.855 0.1,40 Q,007 0,083 0 214.: 0.083 4.482 38 512 ! . Date lbs/ac
•ior Years Cumulative lbs/ac 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0
urrent Cumulative lbs/ac 0.1'96 0.033 ;� 2.507' i 2.855 0.340 0.007 0.083 0.214 0.083 4.482
;rmitted C. P. L. R.**** 36.49 34.71 1335 N/A 267 I 15.13 N/A 373.8 89 1 2492
:rmit PAN Limit lst/2nd Crop
[ certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
.formation. including the possibility of fines and imprisonment for knowing violations."
DlglWly lg dbyleffkehke
WI ( ffHeVke.mDenaOWa,er,ou, *Application Method: S - Surface, IN - Injection, INC -Incorporation
" all) H [e-mail],c US
bat2'.YQ19.013Ol7y 059-0600
Volatilization Rate: Surface - 0.5, Iniection/Incornoration - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

Way'.�:M
P
AIUALYTIGAL
10/5/2018
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 18-270-0204
Project Description: Lake Kilby WTP 2018 1 of 6
1621 White pine Road, FOchohond, vA 23237
Main 864 743-94oi 0 Fax [phone]
i VWW.Waypointanalytiml.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/27/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
&.d' 0 6,-?-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
c
a
a Y.S

Waypoil
.
ANALYTICAL
7621 Whit 64 Road, Richrrrand, VA 1U47
Main $04-743.9401 ° F;;0k 804-2A-644fi
vvvvuvwayptiiitarralytieal.cori
Client: Denali Water CASE NARRATIVE
Project: Lake Kilby WTP 2018 1 of 6
Lab Report Number: 18-270-0204
Date: 10/5/2018
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 62878 (1)
Analyte: NO3+NO2-N
QC Batch No: E66207/E66163
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Solids Total Mercury Analysis - CVAA Method SW-7471B
Sample 62879
Analyte: Hg
QC Batch No: E66217
MS/MSD Recovery failed, PDS confirmed matrix interference

•
�,u 7621 Whitepine Road, Richmond, VA 23237
Waypoin
Mein 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-270-0204
Client Project Description: Lake Kilby WTP 2018 1 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62878 1 Solids 09/26/2018 13:50 09/27/2018
62878 1 Solids 09/26/2018 13:50 09/27/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-270-0204
a
Account Number: 07274 ,M 7621 Wiiitepine Road, Richmond; VA 23237
waypoi
Main 804-743-9401 ° Fax $04-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: Denali Water Project: Lake Kilby WTP 2018 1 of 6
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
REPORT OF ANALYSIS Date Sampled: 9/26/2018 13:50:00
Lab Number: 62878 Date Received: 09/27/2018 00:00
Sample Id: 1 Date Reported: 10/05/2018
Total Solids *
13.42
134200
100.0
JM
09/27/2018 14:10
SM-2540G
Moisture "
86.57
100.0
JM
09/27/2018 14:10
SM-254OG
Total Kjeldahl Nitrogen
0.77
7740
50.0
R D
09/28/2018 08:00
SM-4500-NH3C-TKN
Phosphorus
0.23
2320
50.0
BKN
10/02/201818:25
6010D
Potassium
0.02
205
50.0
BKN
10/02/201818:25
601OD
Sulfur
1.51
15100
50.0
BKN
10/02/201818:25
601OD
Calcium
0.36
3570
100
BKN
10/02/201818:25
601OD
Magnesium
0.04
439
50.0
BKN
10/02/201818:25
6010D
Sodium
0.04
396
250
BKN
10/02/201818:25
6010D
Iron
24600
50.0
BKN
10/02/201818:25
601OD
Aluminum
198000
500
BKN
10/04/201811:38
601OD
Manganese
5080
50.0
KKM
10/03/201818:42
6010D
Copper
144
2.50
BKN
10/02/201818:25
6010D
Zinc
108
5.00
BKN
10/02/201818:25
6010D
Ammonia Nitrogen
0.11
1120
50.0
R D
09/28/2018 08:00
SM-4500-NH3C
Organic N
0.66
6620
50.0
09/28/2018 08:00
CALCULATION
Nitrate+Nitrite-N
<2.31
2.31
MMT
10/01/201815:56
4500NO3F-2011
All values are on a dry weight basis
except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding Time
��
fAl
Our reports and letters are for the exclusive and corrttcJar?±ial use or our clwms, and n:ay not ba reproduces° in ;•thole or part. not may any reference
be made
Pauric McGroary
to tf? :•vc;rtc, the resuitfi. or the company in any <:dter?;sine
news re"Oese, er othcar
x,ubfic arn?ounce;:rs;rrts
wivwui o^iainrnp our prior writle,i atAorflasr`ion..
Agronomist

Report Number: 18-270-0204
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 62878
Sample Id : 1
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio
Comments:
6
Way
poi
t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-749-9401 ° Fax [phone]
www.Waypointanaiytical.com
Project: Lake Kilby WTP 2018 1 of 6
REPORT OF ANALYSIS
Date Sampled: 9/26/2018 13:50:00
Date Received: 09/27/2018 00:00
Date Reported: 10/05/2018
<1.00
1.00
BKN
10/02/201818:25
601OD
167
2.50
BKN
10/02/201818:25
601OD
12.4
2.50
BKN
10/02/201818:25
6010D
18.5
3.00
BKN
10/02/201818:25
6010D
11.8
5.00
KKM
10/03/201818:57
601OD
<0.400
0.400
MMT
10/02/2018 14:51
SW-7471 B
<5.00
5.00
BKN
10/02/201818:25
601OD
7.1
1.0
R D
09/28/2018 08:00
9045D
4.23 42300
2500
R D
09/28/2018 12:30
AOAC 955.01
45.94 459400
100.0
JM
09/27/201814:10
SM-254OG
<2.50
2.50
BKN
10/02/201818:25
601OD
1.66
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our teports and ieifers are for the exclusive and confidenUaf fuse of ourcite! ts. and !my riot be !"aproduced in whole or putt, w inay any r Bference be ft1ade
to fhO WCtk 4,40 MSUMs. or the co.:rpany in any adVP!fiS:!?q' Pews release, or Other iwbfic 3C.P.o ncei7lents i ithouf obtaining our pike widen aufhorizahion.
611C., FV- 1�'
Pauric McGroary
Agronomist

Waypoint.
ANALYTICAL
7621 Whitepine•Road,.Richmond, VA 23237
Main $44-743-9461 ° Fax.8i 4-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-270-0204
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
.............................
._....._:..._.............
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F777
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F- High concentration container (48 hr) [— Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F- Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes I* No
Comments:
Signature: IMorgan Tichacek I Date & Time: 09/27/2018 13:29:19

q.S
QWI
0777
7621 Whitepinc Road Richmond S Lake K"hV WTP 20181 c G of g 13 28.27 sup�nrtale e�,"t at tcrti:cum
Suhm'stted: i•#y . _. Ctaat ge is .:, Copy To..
Jeff Retzke../benali Water
PO: DEW
eodenaliwa,6r9Cam
35 Refreshment Place
a'ei f ' s Celli 285. 503.4300
Decatur, AL 35*601.
Prnject
Lake -Ki.1by WTP 2015 1&2 o
, 6
SarnpW Rnformaflon
Lob Number,
Collection Idormatinn
Contatrler Intormatlon
`'
Piaas� �h�cic pssited
i est
=Yoe
Date
Time
Numisef
ol;Bottles
?ype
Volume
SL1
Si,2
603
ggetais
Nitrogen
Series
tC
Ag
Cl
ttotat le
Solids
Sample lD
(Lab Uss
fancy)
n
Crab
/ ,
IWit"
,
_x Glass
PlaiUa
oz
—K --.Ont
V
composite
,
,/ t
.
qt
2
Grab
r,,
i
_Glass
x
Aint
---`^�+t
Plastic
Com tssite
!
Grab
_Glass
Plastic
02
int
- --pI
Gom .Waite
I
Grab
glass
F4astic
-- oz
----!Int
Basic Test SLl
or'10.181.1
Md Zinc
Account
Others
S`eme as.

ay
.Point,
ANALYTICAL
10/5/2018
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 18-270-0205
Project Description: Lake Kilby WTP 2018 2 of 6
76�11Nititep�ne itaad, �cliinond,:ilA �3237'
Main 8(34-743=9401 ° Fax [phone]
www.Waypoiatanatytical.ioz
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/27/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.d- P e&7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
AM

ANALYTICAL.
Waypoint.
7621 V11hitepine goad, tSichiriond, ttA 23237
Main,804-743-0401 0 Fax 80+ 271 64A6
v�nuw:waypciinta nalytica I.coiri
Client: Denali Water CASE NARRATIVE
Project: Lake Kilby WTP 2018 2 of 6
Lab Report Number: 18-270-0205
Date: 10/5/2018
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 62878
Analyte: NO3+NO2-N
QC Batch No: E66207
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Solids Total Mercury Analysis - CVAA Method SW-7471B
Sample 62879 (2)
Analyte: Hg
QC Batch No: E66217/E66189
MS/MSD Recovery failed, PDS confirmed matrix interference

Waypol a 7611 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www waypointanalyticai.com
Sample SummaryTable
Report Number: 18-270-0205
Client Project Description: Lake Kilby WTP 2018 2 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62879 2 Solids 09/26/2018 14:00 09/27/2018
62879 2 Solids 09/26/201814:00 09/27/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-270-0205
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 62879
Sample Id: 2
gum
a
Waypoint".7.11W
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytica Isom
Project: Lake Kilby WTP 2018 2 of 6
REPORT OF ANALYSIS
Date Sampled: 9/26/2018 14:00:00
Date Received: 09/27/2018 00:00
Date Reported: 10/05/2018
Total Solids *
13.66
136600
100.0
JM
09/27/2018 14:10
SM-2540G
Moisture *
86.33
100.0
JM
09/27/2018 14:10
SM-254OG
Total Kjeldahl Nitrogen
0.76
7610
50.0
R D
09/28/2018 08:00
SM-4500-NH3C-TKN
Phosphorus
0.21
2070
50.0
BKN
10/02/201818:30
601OD
Potassium
0.01
136
50.0
BKN
10/02/201818:30
601OD
Sulfur
1.52
15200
50.0
BKN
10/02/201818:30
601OD
Calcium
0.20
1950
100
BKN
10/02/201818:30
6010D
Magnesium
0.04
384
50.0
BKN
10/02/201818:30
601OD
Sodium
0.04
381
250
BKN
10/02/201818:30
601OD
Iron
25200
50.0
BKN
10/02/201818:30
6010D
Manganese
4930
5.00
KKM
10/03/201819:03
6010D
Copper
151
2.50
BKN
10/02/201818:30
6010D
Zinc
104
5.00
BKN
10/02/201818:30
6010D
Ammonia Nitrogen
0.13
1320
50.0
R D
09/28/2018 08:00
SM-4500-NH3C
Organic N
0.63
6290
50.0
09/28/2018 08:00
CALCULATION
Nitrate+Nitrite-N
<2.34
2.34
MMT
10/01/201815:58
4500NO3F-2011
Cadmium
<1.00
1.00
BKN
10/02/201818:30
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time?04or
6,0W
Our reports and letters are for the exclusive anal cortideniial use or our ctrerrts, and rx:ay
not ba reproduced in
wrote or part: ror inay
any reference be mate
Pauric McGroary
%o the work, th r0srAits. or the rorSr pary in any;-'.C}ver?irhag,
news roleasc, or othor.pubfic
ar?P.ouncer7??:ri%i without obtaining oar pnbr
rvrtd`C• n authorization,
Agronomist

Report Number: 18-270-0205
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 62879
Sample Id: 2
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio
Comments:
Waypol tw.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanaly.tcal.com
Project: Lake Kilby WTP 2018 2 of 6
REPORT OF ANALYSIS
Date Sampled: 9/26/2018 14:00:00
Date Received: 09/27/2018 00:00
Date Reported: 10/05/2018 .
172
2.50
BKN
10/02/201818:30
6010D
12.4
2.50
BKN
10/02/201818:30
601OD
20.5
3.00
BKN
10/02/201818:30
6010D
11.3
5.00
KKM
10/03/201819:03
601OD
<0.400
0.400
MMT
10/02/2018 14:53
SW-7471 B
<5.00
5.00
BKN
10/02/201818:30
601OD
7.0 -
1.0
R D
09/28/2018 08:00
9045D
2.51 25100
2500
R D
09/28/2018 12:30
AOAC 955.01
45.58 455800
100.0
JM
09/27/201814:10
SM-2540G
<2.50
2.50
BKN
10/02/201818:30
6010D
1.95
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports arid taiters are for the exclusive and confidential use of our' o watts' 3!"d rvay not be reproduced f , whole or part, nor-ana}y any referericv be made
to tho worir, the r suiN. or the compal}'i in any ad ndis.0q, ne4Ya release:, or ether.pub.ic announcements without obtaining our pnOr written aUtborizatioP..
Pauric McGroary
Agronomist

:Q)
Wayo�nt
PNALYTICAL
7021 Whitevine Road..Richmond, VA 23237
Main 804-743-94010 Fax 804-17i-6446
www.wtaypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-270-0205
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
is UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
• Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
4D Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 - compliance criteria met
0 Yes
0 No
N/A
F- High concentration container (48 hr) F- Low concentration EnCore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) F- Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: IMorgan Tichacek Date & Time: 09/27/2018 13:33.09

Wayp'0*1..
ANALYTICAL.
10/17/2018
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 18-281-0200
Project Description: Lake Kirby WTP 2018
7621 Whitepine Road, Richmond, VA 2323*7
Main 804443446i 0 Fax [phone]
'"W waypedinUnalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.,,:.. 0 607-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania. 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007

Wayp. :
ANALYTICAL.
Client: Denali Water
Project: Lake Kirby WTP 2018
Lab Report Number: 18-281-0200
Date: 10/17/2018
1621'Whitep ne Roast, ftitinrriond, vA 23237
Main 904-743-9401 ° Fax 8ti4- 1i-644s
Www.waypointa nblytica lxon
CASE NARRATIVE
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 63041 (3)
Analyte: Nitrate+Nitrite N
QC Batch No: E66337/E66314
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Metals Analysis Method 6010D
Sample 63028
Analyte: Aluminum
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L403805
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.

Waynoint,
ANALYTICAL..
76�11ik/hitepine f�tiad, ��th�andr ilA 232�?
Win.9 43-9401 ° Fax 804»271-6446
vvvuwiwaypoinian6jy"tAco

Way �nt' PA ICAI
Report Number:
Client Project Description:
7621 Whitepine !toad, R',.chmond, VA 23737
Main 804443-9401 0 fax [phone]
www.waypointanalytical.cor
Sample Summary Table
18-281-0200
Lake Kirby WTP 2018
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63041
3
Solids
10/06/2018 09:30
10/08/2018
63041
3
Solids
10/06/2018 09:30
10/08/2018 SW-7471B WTN
63041
3
Solids
10/06/2018 09:30
10/08/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-281-0200
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63041
Sample Id : 3
way to
P I - .'
7621 Wt itepine Road, Richmond, VA 231.37
Main 804-743-9401' Fax [phone]
www.waypointanatyticaLcom
Project: Lake Kirby WTP 2018
REPORT OF ANALYSIS
Date Sampled: 10/6/2018 09:30:00
Date Received: 10/08/2018 00:00
Date Reported: 10/17/2018
Total Solids *
14.72
147200
100.0
R D
10/08/2018 14:00
SM-2540G
Moisture *
85.28
100.0
R D
10/08/2018 14:00
SM-2540G
Total Kjeldahl Nitrogen
0.73
7270
50.0
R D
10/09/2018 09:00
SM-4500-NH3C-TKN
Phosphorus
0.20
2020
50.0
KKM
10/12/2018 23:17
6010D
Potassium
0.01
127
50.0
KKM
10/12/2018 23:17
6010D
Sulfur
1.35
13500
50.0
KKM
10/12/2018 23:17
601 OD
Calcium
0.18
1800
100
KKM
10/12/2018 23:17
601 OD
Magnesium
0.04
418
50.0
KKM
10/12/2018 23:17
601 OD
Sodium
0.03
345
250
KKM
10/12/2018 23:17
601 OD
Iron
24000
50.0
KKM
10/12/2018 23:17
601 OD
Aluminum
179000
500
JTR
10/14/201816:05
6010D
Manganese
5200
50.0
JTR
10/14/201816:05
6010D
Copper
54.9
2.50
KKM
10/12/2018 23:17
6010D
Zinc
162
5.00
KKM
10/12/2018 23:17
6010D
Ammonia Nitrogen
0.10
1020
50.0
R D
10/09/2018 09:00
SM-4500-NI3C
Organic N
0.63
6250
50.0
10/09/2018 09:00
CALCULATION
Nitrate+Nitrite-N
<2.29
2.29
MMT
10/10/201812:36
4500NO317-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our leports and leUers are lorthe exclusive find confidet)Yaf use car our chants, and tray rot be reproduced i , stihote orpart. Po!iriay 8(V refere,%V be made Pauric McGroary
'.0 the 4vork, th" it.su ts. or the co,; poesy in arty Pdvett iing, P.pws release, or ofhC•er 1'wbfic annolirtwementi wit,010 o; taming ourpt"ror'wfitton authorization,
Agronomist

Report Number: 18-281-0200
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Wayp i nt
ANALYTICAL
7621 Whitepine. Road, Richmond, VA 23237
Main $04-743-9401 ° Fax $04-271-6446
www.waypointanalydcal.com
Project: Lake Kirby WTP 2018
REPORT OF ANALYSIS Date Sampled: 10/6/2018 09:30:00
Lab Number: 63041 Date Received: 10/08/2018 00:00
Sample Id : 3 Date Reported: 10/17/2018
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio
Comments:
<1.00
1.00
KKM
10/12/2018 23:1 t
buluu
153
2.50
KKM
10/12/2018 23:17
6010D
11.5
2.50
KKM
10/12/2018 23:17
6010D
10.1
3.00
KKM
10/12/2018 23:17
601 OD
11.2
5.00
KKM
10/12/2018 23:17
6010D
0.0243
0.0155
KKM
10/11/201813:04
SW-7471B
<5.00
5.00
KKM
10/12/2018 23:17
601 OD
7.1
1.0
R D
10/09/2018 09:00
9045D
3.70 37000
2500
R D
10/12/2018 09:30
AOAC 955.01
48.36 483600
100.0
R D
10/08/2018 14:00
SM-2540G
<2.50
2.50
KKM
10/12/2018 23:17
601 OD
1.90
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Jjrr jvpo :s ar:d fetfers are for the exclusive and confidentialuse of ourcheats. and!vayTrot be reproduced in whole oe part, nor ri?ay any re-ference be made
to the work the resuits. or the company any in any -'.dv riif"ing, news na ease; of C;ther i'rGiNk announcements i"Tthou! obtaining our prior Written BFJthor7Zat on.
Pauric McGroary
Agronomist

W�pointNALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 904-741-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-281-0200
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
40 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F— High concentration container (48 hr) F— Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: IBrandi Watson Date & Time: 10/08/2018 13:05:54

SAMPLE T
18-261-0260
7621 White?pine Road Richmond VA 2323 Donau 4Nater 1394:26. rEaie � alcnsEern.ce�na
Lake Krrlav VVtTP 2018
Submitted By
Jeff Re zke/ppnal Water O, DEW
35 freshmer:-t- Place .....
Decatur, AL 3.560:1
Project I Lake Kilby WTP 2018 3L&.,;r e , 6
Lab Number
Sample ID {Lab Use
only).
4
Cctlt�dtlr�n Inforrrtatlon
Tyler
Tate
Time I
0
Crala
1 0/6/18
9:30
)Osil e
Grab
10/6/1$
3GSiE�
Grab
1 1p � 1(�1TUffT13Li0[T
arzlainer lnit�rma#i';t�rl
Please:(
Ues
_ Type
Valume
SOSL2
503
trletals.
Class
oz
y Plastic
---pint
cat
Class
eiret
X plastic
Glass
oz
Plastic
P
Class
------ .pz
plastic
,g
_
Test Package Details
1 1: Total ."xr,.i'ids `lttisturr}'I"oral Kie1dahi Nrswgan, 111110splivn* and Pssw ivm, 1:2i Blwl� im, SL I PW,-, ", Fl u,:, t"z. vuun, Mwn rhVnn> :Maflganvss , Copper eiudrZinc
03 Metals- Arsenic;, Cadmium, ChromiumMercury, Molybdenum. Lead. Nickel Selenium.
(Capper & Zinc included in SL2)
ftroeen Spriest'T"t+W jolsiahl, A mon4wn, Mtrate & Orgpni-. `:ilroge:t.
;CE: Calcium Car boriate Equivalent or Total neutralization Value (For lR me Treated Sludge).
Copy To
j eff . ret zke6LiE,i2q17.+imteM , ce
jeff Is e? : 256 ,503.43 t70
k D6sired Tuts
saea p� CCE leg1.
Gl
dies
---------------
nlatile Uthers
Inflits
d S.A. R.
tameras above.

WaypA CAL.
10/17/2018
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 18-281-0201
Project Description: Lake Kirby WTP 2018
7621 Whiteptne ftad, ftichroond, VA 232�1
Mdin 904-743-6461 ° Fai 804-271-6446
wuuw.WaVpdtntanbtytiitm.con
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. P a7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
r�

Way i
ntie
T621 Whitepane lipad, Rlchrnond, VA 2320
Main.804-743-94i#1 �' Fax 8fi4-271-6A45
www waypmiritenalotal c,0—
Client: Denali Water CASE NARRATIVE
Project: Lake Kirby WTP 2018
Lab Report Number: 18-281-0201
Date: 10/17/2018
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 63041
Analyte: Nitrate+Nitrite N
QC Batch No: E66337
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.

Waypol t
ANALYTICAL
76211 thit+'pine Road, Richmond, VA 23237
Main 804=743-9401fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 18-281-0201
Client Project Description: Lake Kirby WTP 2018
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63042
4
Solids
10/06/2018 09:45
10/08/2018
63042
4
Solids
10/06/2018 09:45
10/08/2018 SW-7471B WTN
63042
4
Solids
10/06/2018 09:45
10/08/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-281-0201
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63042
Sample Id: 4
7623 Whitepine Road, Rlchmond; VA 23237
Main 804-743-9401 °lax $04-271-6446
www.waypointanalytical.com
Project: Lake Kirby WTP 2018
REPORT OF ANALYSIS
Date Sampled: 10/6/2018 09:45:00
Date Received: 10/08/2018 00:00
Date Reported: 10/17/2018
Total Solids
14.88
148800
100.0
R D
10/08/2018 14:00
SM-2540G
Moisture *
85.12
100.0
R D
10/08/2018 14:00
SM-254OG
Total Kjeldahl Nitrogen
0.72
7190
50.0
R D
10/09/2018 09:00
SM-4500-NH3C-TKN
Phosphorus
0.18
1830
100
JTR
10/15/2018 21:28
601 OD
Potassium
0.01
136
100
JTR
10/15/2018 21:28
601 OD
Sulfur
1.39
13900
100
JTR
10/15/2018 21:28
601 OD
Calcium
0.19
1880
200
JTR
10/15/2018 21:28
601 OD
Magnesium
0.04
422
100
JTR
10/15/2018 21:28
601 OD
Sodium
<0.05
<500
500
JTR
10/15/2018 21:28
601 OD
Iron
25200
100
JTR
10/15/2018 21:28
601 OD
Aluminum
183000
1000
KKM
10/16/201813:13
601 OD
Manganese
5440
10.0
JTR
10/15/2018 21:28
6010D
Copper
49.3
5.00
JTR
10/15/2018 21:28
6010D
Zinc
161
10.0
JTR
10/15/2018 21:28
6010D
Ammonia Nitrogen
0.11
1140
50.0
R D
10/09/2018 09:00
SM-4500-NH3C
Organic N
0.61
6050
50.0
10/09/2018 09:00
CALCULATION
Nitrate+ N itrite-N
<2.29
2.29
MMT
10/10/201812:39
4500NO3F-2011
All values are on a dry weight basis
except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B-Analyte detected in blank
H -Beyond Holding
Time
PC
Our reports ar:d iatfers are fbr itta exclusive and ccn¢)dential use ofour r clients, arcs may not be reproduced in lwhole orpad.. ncrntay any reference be made
Pauric MCGroary
to ff?9 'stiC,P)f, the r£.^�uits. or the COr rr7r3,)y in arty a f vedis"ing, P,F, vvs release, cr c)Tf? r
z?:;bfrc a±il? un-.-r^f?7E nts
ir7° ,,)uf obmining our pilmr
�ivit!en auth .rizar`ion.
Agronomist

Report Number: 18-281-0201
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63042
Sample Id: 4
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio
Comments:
0 0
Waypol t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804 743-9401 ° Fax [phone]
www.waypoi6tanatytical.com
Project: Lake Kirby WTP 2018
REPORT OF ANALYSIS
Date Sampled: 10/6/2018 09:45:00
Date Received: 10/08/2018 00:00
Date Reported: 10/17/2018
<2.00
2.00
JTR
10/15/2018 21:28
601 OD
157
5.00
JTR
10/15/2018 21:28
601 OD
11.3
5.00
JTR
10/15/2018 21:28
601 OD
8.10
6.00
JTR
10/15/2018 21:28
601 OD
<10.0
10.0
JTR
10/15/2018 21:28
6010D
0.0242
0.0150
KKM
10/11/201813:06
SW-7471B
<10.0
10.0
JTR
10/15/2018 21:28
601 OD
7.0
1.0
R D
10/09/2018 09:00
9045D
3.45 34500
2500
R D
10/12/2018 09:30
AOAC 955.01
48.65 486500
100.0
R D
10/08/2018 14:00
SM-2540G
<5.00
5.00
JTR
10/15/2018 21:28
601 OD
2.70
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
lour le' tarts af"d !alters an. IGr it?8 eyclusive and confidei iiial use v oar LhentS, art! ?ray riot be .''epnodoceU i i whole or part, nor may & re?ererice be Made
to the work, the ;-eswlts. it the company in aoy r:C)mfising, nemvs nelea^se, or tither i?;.itb6 . fi??f?ouncementS vVlthout Obtaining our prior i,vi ttett 8E1thC:rtZ3:`7;11?.
17
Pauric McGroary
Agronomist

Way.�. n
PARTICAL
,7621 Whitepine•Road, Richmond, VA 23137
Main 804-743-9401 '0 Fax $04-271-6446
www.wtaypointanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-281-0201
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
40 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F High concentration container (48 hr) [— Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: IBrandi Watson Date & Time: 10/08/2018 13:08:51

Jeff e-zke enali Water PODEW
35 Refreshment Pl c
�akki Xi lby WTP 2018 3&A Of 6
Sample [nforrnati6h
Lab Number Contamer Into ation
ern# #
(tab Use
Orly)
Type
Date "
Time
hSora b
iSf.C3ittt#��
Type
Volume:
Ll
U
�a��
3�etals:
Grab
10J6118.
UO
_ Glass
X �j S
X Plastic
'-�--�-`P;n
Composite
Gmb
10/6/18
[y a
9 X45
_ Glass
'X east.Pint
e' 0z
Composite
— Gratz
#ass
-----• oz
in
—plastic
Cara
lass
oZ
Plastic
pint
J-0f f Is Cell. 2,56.5 3.4�00
ed Tests
Volatile
pH CCE h.9C 1 Cli#t�f
Safift
and. S, a'§.. R ;
game as above I�
{
T

Waypoln.-I,
..
ANALYTICAL
7671 Whitep ite Read; 8ichiiw6d, l A 23217
main.$04-743-9461 ° Fax [phone]' 6
wv+ruvvvaypainta�alytical.cvtri
Client: Denali Water CASE NARRATIVE
Project: Lake Kilby WTP 5 of 6
Lab Report Number: 18-297-0202
Date: 11 /5/2018
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 63282 (5)
Analyte: Nitrate+Nitrite N
QC Batch No: E66539/E66516
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Metals Analysis Method 6010D
Sample 63289
Analyte: Aluminum
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Copper
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L406330
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.

Waypol.nt.
-
ANALYTICAL
1621 Whitepine Road, Wchm nd,Va 2387
Main 804-743- Oft ° Fax $Q4-271 644£
wwviiwaypmintana[ytical.coi
Analyte: Manganese
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method SW-7471 B
Sample 63285
Analyte: Mercury
QC Batch No: E66590
MS/MSD Recovery failed, PDS confirmed matrix interference

7621 Whit+epine Road, Richmond, VA BZ37
Waypoint Main 804=743-9401 *'Fax 804-271-W6
ANALYTICAL www.waypointanalydcal.com
Sample Summary Table
Report Number: 18-297-0202
Client Project Description: Lake Kilby WTP 5 of 6
Lab No Client Sample ID
Matrix Date Collected Date Received Method Lab ID
63282
5
Solids
10/23/2018
11:10
10/24/2018
63282
5
Solids
10/23/2018
11:10
10/24/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-297-0202
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63282
Sample Id: 5
A
Waypoint'.
ANALYTICAL
7621 Whitepine. Road, Richmond, VA 23237
Main 804.743-9401 ° Fax [phone]
www.waypointan aiyticaLcom
Project: Lake Kilby WTP 5 of 6
REPORT OF ANALYSIS
Date Sampled: 10/23/2018 11:10:00
Date Received: 10/24/2018 00:00
Date Reported: 11/05/2018
Total Solids "
14.80
148000
100.0
JM
10/24/2018 14:40
SM-254OG
Moisture "
85.19
100.0
JM
10/24/2018 14:40
SM-2540G
Total Kjeldahl Nitrogen
0.78
7770
50.0
R D
10/25/2018 08:45
SM-4500-NH3C-TKN
Phosphorus
0.15
1520
50.0
KKM
10/29/201817:56
601OD
Potassium
0.02
214
50.0
KKM
10/29/201817:56
601OD
Sulfur
1.31
13100
50.0
KKM
10/291201817:56
601OD
Calcium
0.20
1970
250
KKM
10/29/201817:56
601OD
Magnesium
0.06
637
50.0
KKM
10/29/201817:56
6010D
Sodium
0.04
400
250
KKM
10/29/201817:56
6010D
Iron
19600
50.0
KKM
10/29/201817:56
601OD
Aluminum
188000
500
BKN
10/30/201813:11
.601OD
Manganese
6050
50.0
BKN
10/30/201813:11
6010D
Copper
87.2
2.50
KKM
10/29/201817:56
6010D
Zinc
255
5.00
KKM
10/29/201817:56
6010D
Ammonia Nitrogen
0.09
945
50.0
R D
10/25/2018 08:45
SM-4500-NH3C
Organic N
0.69
6825
50.0
10/25/2018 08:45
CALCULATION
Nitrate+Nitrite-N
<2.37
2.37
MMT
10/26/201810:14
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding
Time
Folit,
fillo 7,1000
V, 10
01U ±'eports aafd letters ata tb±'the exclusive anal ronffdenUal use of outchet?ts, art! traynot be reproduced
in whole or part; nor'may atly reference be n?atie
Pauric McGroary
%o ti?C: 'rL'CiflS, tik'?{ S{l'tF..OP!`h,f;Co„rp81}dill?,7y;C}lt;{?ii.±7Q,nF;4„ir:?.c�as<�,rr<3tf?::rx,uh.±Gannouncementsi".itli0lii
A.'?ialnii?q our p{;or
�writfe:n aufb0±iz?U0l?.
Agronomist

Report Number: 18-297-0202
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63282
Sample Id : 5
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio
Comments:
Wayp int,'O
ANALYTICAL
7611 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Lake Kilby WTP 5 of 6
REPORT OF ANALYSIS
Date Sampled: 10/23/2018 11:10:00
Date Received: 10/24/2018 00:00
Date Reported: 11/05/2018
<1.00
1.00
KKM
10/29/201817:56
601OD
135
2.50
KKM
10/29/201817:56
601OD
12.8
2.50
KKM
10/29/201817:56
6010D
11.8
3.00
KKM
10/29/201817:56
6010D
7.18
5.00
KKM
10/29/201817:56
601OD
<0.400
0.400
MMT
10/31/201811:11
SW-7471B
<5.00
5.00
KKM
10/29/201817:56
6010D
7.3
1.0
R D
10/25/2018 08:45
9045D
1.29 12900
2500
R D
10/25/2018 13:00
AOAC 955.01
47.61 476100
100.0
JM
10/24/201814:40
SM-2540G
<2.50
2.50
KKM
10/29/201817:56
601OD
2.00
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
Our 1'erorts aad iBlters are for the eY.clusive* and confidenl,'al use Of ow cheats. and tT:ay'io" be izdproduced in E,VfiUl$ or part nor n:ay any reference be made
to the i!"GP?f, ti7c, i &il!ts. or thFT f.0±:ifh2.}y 1,} any a0'Ngtililt}g� n�+ws nolvaso'. cr other R:CiNic announcce^f7 e!f I i "ili-o t L ix fining our p for �N7it!on autho!TZat. n.
Pauric McGroary
Agronomist

Want:,,
�iALYTICAL
7621 Whitepine Road;. Richmond, VA 23237
Main 904-7.43-9441 ° Fax [phone]
www"aypo➢ntanalytical.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-297-0202
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 Other:
UPS 0 Client 0 Courier
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
-All-samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr)
F— Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Imorgan Tichacek I Date & Time: 10/24/2018 13:16:36

SAMPLE,
7621 WhitopinoRmul Richmond Donah.Water
Lake Kilby VVTP 5 of 6
-Submitted 8}
Jeff Retzke/Denali Water PO
35 Refreshment Place
Decatur, AL 35601
Project Lake Kilby WTP 2018 3 & 6 cif 6
Sample Informai
Leib Number Collaction.1niOnnallon Container infer
USTODY
Jeffle C411: 256.503.4300 1,
Qqm" Ct (Lab . 0 Number Type Volume S
Only) Type Date Time of O I SL9 '03 JN'trogao p. I S I Aq: 1'�oiafite
Uetgta Series CC Cl AnItAft
,Amunt #
,Others
Grab COMPOO,
Glass- ect
Plastic
Composite and S.A.A.
x sint
Grab oz
—Glass. same. as above
Plastic
19gMP-ai fte W, At
I— Grab 0-Ii—I I . Ox
SU; UWo Test SLI plus Sulfur, Calciusi , Mepcsjum,Sadium, trcrn, Airuirittttuf, manpl�% COPW And Zinc
$03 Metals: Arsenic, Cadmium, Chromium; MarcuryMolybdenum, Lead, Nickel, Selenium,
(Copper & Zinc Included in W)
Nilralita Series- Foie! Kjoidahl, Ammonitun, Nitraw & Orgmiic Nhmveo.
CCE: Calcium Carbonate Equivalent �or Total neutralization Value (For Ume Treated Sludge)

iay
po'_
ANALYTICAL
11/5/2018
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 18-297-0203
Project Description: Lake Kilby WTP 6 of 6
7621 whitepine`Rod, f ichmandi VA 2181
Main 804-743-946i ° Fax 8-o4»27i-6446
wnnrvi+ waypaintana[ydcal,t&i
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/24/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample -analysis time for confirmation of holding time compliance. -
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. 0 ea?-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007

WayPANi4LYTICAL
Client: Denali Water
Project: Lake Kilby WTP 6 of 6
Lab Report Number: 18-297-0203
Date: 11/5/2018
7621 Whitep ne Road, Richmond, VA 23237
Main $04-743-9401 0 Fax $04 271 6446
wuvw:wayperiitana[ytteal.coiri'
CASE NARRATIVE
Nitrate + Nitrite Nitrogen Method 4500NO3F-2011
Sample 63282
Analyte: Nitrate+Nitrite N
QC Batch No: E66539
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Metals Analysis Method 6010D
Sample 63289
Analyte: Aluminum
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Copper
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L406330
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.

W..
PA
NAl:YTIEAL.
7b21 Whitep ne Road, WOO'.
ilA 23237
Main 804-743-9�tii7 ° Fait 804 271-6446
WWW.Waypointana[ytical.cotri
Analyte: Manganese
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L406213
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method SW-7471B
Sample 63285
Analyte; Mercury
QC Batch No: E66590
MS/MSD Recovery failed, PDS confirmed matrix interference

f
Waypoint. 76Z1 Whitepine Road, Richmond, VA 23?.,37
Main 804-743-9401 ° Fax [phone]
ANALYTICAL wwwwaypointainalytical.corn
Sample Summary Table
Report Number: 18-297-0203
Client Project Description: Lake Kilby WTP 6 of 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63283
6
Solids
10/23/2018
11:15
10/24/2018
63283
6
Solids
10/23/201811:15
10/24/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 18-297-0203
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63283
Sample Id : 6
Waypoint,10,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalVtical.com
Project: Lake Kilby WTP 6 of 6
REPORT OF ANALYSIS
Date Sampled: 10/23/2018 11:15:00
Date Received: 10/24/2018 00:00
Date Reported: 11/05/2018
Total Solids
15.13
151300
100.0
JM
10/24/2018 14:40
SM-2540G
Moisture `
84.86
100.0
JM
10/24/2018 14:40
SM-2540G
Total Kjeldahl Nitrogen
0.79
7860
50.0
R D
10/25/2018 08:45
SM-4500-NH3C-TKN
Phosphorus
0.14
1440
50.0
KKM
10/29/201818:01
6010D
Potassium
0.02
168
50.0
KKM
10/29/201818:01
6010D
Sulfur
1.43
14300
50.0
KKM
10/29/201818:01
6010D
Calcium
0.20
1950
250
KKM
10i29/201818:01
6010D
Magnesium
0.07
654
50.0
KKM
10/29/201818,01
6010D
Sodium
0.04
420
250
KKM
10/29/201818:01
6010D
Iron
20400
50.0
KKM
10/29/201818:01
6010D
Aluminum
201000
500
BKN
10130/20181317
6010D
Manganese
6450
50.0
BKN
10/30/201813:17
6010D
Copper
89.4
2.50
KKM
10/29/201818:01
6010D
Zinc
270
5.00
KKM
10/29/201818:01
6010D
Ammonia Nitrogen
0.11
1120
50.0
R D
10/25/2018 08:45
SM-4500-NH3C
Organic N
0.68
6740
50.0
10/25/2018 08:45
CALCULATION
Nitrate+Nitrite-N
<2.33
2.33
MMT
10/26/201810:16
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. nn11
B - Analyte detected in blank H - Beyond Holding Time Fwir' if 6"Wr
Our reports and letters are for the exdusrve and confidential use of cur clients. and may not be reproduced in M;o/e or part, nor may any reference be made Paurlc MCGroary
to the work, the resuits. orthe company in any advertising, news release, orothorpublw announcements without obtaining our prior written authodzatwa Agronomist

Report Number: 18-297-0203
Account Number: 07274
Send To: Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL 35801
Lab Number: 63283
Sample Id : 6
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Sodium Absorption Ratio "
Comments:
W
Waypoint,
ANALYTICAL
7521 Whitepine Road, Richmond, VA 23237
Main 904-743-9461 ° Fax $04-271-6446
wwrw.waypointanalyt caLcom
Project: Lake Kilby WTP 6 of 6
REPORT OF ANALYSIS
Date Sampled: 10/23/2018 11:15:00
Date Received: 10/24/2018 00:00
Date Reported: 11/05/2018
<1.00
1.00
KKM
10/29/201818:01
6010D
140
2.50
KKM
10/29/201818:01
601OD
12.9
2.50
KKM
10/29/201818:01
601OD
13.1
3.00
KKM
10/29/2018 18:01
601 OD
10.5
5.00
KKM
10/29/201818:01
601OD
<0.400
0.400
MMT
10/31/201811:13
SW-7471B
<5.00
5.00
KKM
10/29/201818:01
601OD
7.3
1.0
R D
10/25/2018 08:45
9045D
1.10 11000
2500
R D
10/25/2018 13:00
AOAC 955.01
47.82 478200
100.0
JM
10/24/201814:40
SM-2540G
<2.50
2.50
KKM
10/29/201818:01
601OD
2.09
CALCULATION
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our feparts and letters ani hor the exc?us!'v`B and conf dent i use o ourchelits. and :r.'ay iot be f'E',prodaced in twhole of par$: nor inay i3ny eferen-c e be I?7cFde
to i/h9 Work, the resuiN. oP !hp company in any adve?? sing, t etvs or other k"U is a!iJh3ifncenne!its --without obtaining our Prior gw-itten authorization,
PC,,,�
Pauric McGroary
Agronomist

Wayp_M �ni�IALYTICAL
7621'Whitepine>Road, Richmond; VA 23237
Main 904-743-9401 0 Fax [phone]
www.waypointanalyncal.com
Cooler Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 18-297-0203
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0. No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F— High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: IMorgan Tichacek Date & Time: 10/24/2018 13:23:32

SAINIR,
1621 Whiterina. Roid
Q�20
�IIIlllli�lllll�ll Nnali WOW#
Lake KIIIJY WTP 6 of 6
.'."'USTODY
Copy TO
aeff Retzke/D�anal-' Water,
PO: DEW
_35 Refreahmennt PLace
Deca",-.ur, AIj 35601
PTOJeCt
',ake K'1111b�,, WTP 20�16 5 6 -,f r,
Sample Information
I ab ;Nlurnfter
Collection
Information
Container
. Information
Please
Check Desired
Te�ts.
Sam..Ple ID
(Lab Use
Only)
Type
Dple
1 f me
NurMWr
of
lype
Vaiume
SLI
81.2
503
Nitrogen
pH
COE
Aq
CI
Volatile
. .
Others
et al�
4
Ser"es.
Sofids
5Int
Grob
COO
Mass
Plastic
St-Andari Compou
urn
P 051le
—Y
and S,A.F­
61
Glass
plastic
mits s above
Glass
at.
lComposhe
—Plastic
Int
F—I
Grab
Mass
o'7
Int
Tow So 4" (IN lokw'ao I r k.ldniif Nitrogen, I
x mIron, A'Squlklum, Nlangl,=_e, C;)rper AM
Motals., Arsenic, Cad?u=, ChroMum, Mefc.,wi,, Molybdenum� Lead. Saleniurn,
"Copper & Zinc included in SL2)
Calduni Carbonate Et;0*,,aient Or ­Ot.al n.Pufralizal0l VaW� (Pot U rn�e Tmalad Sludge)