NC0000337_AROFileDWRCorrespondence_20190207

Dexter R. Matthews, Director Division of Waste Management Michael F Easley, Go,lernor
William G. Ross.Jr., Secretary
June 16, 2006
MEMORANDUM
TO: Landon Davidson, Regional Supervisor
Asheville Regional Office
North Carolina Aquifer Protection Section
FROM: Mark Wilkins, Hydrogeologist MAW
Facility Management Branch
North Carolina Hazardous Waste Section
RE: Oversight of Aeration and Biosolids Digestion Basins (SWMU 4)
Dupont/AGFA — Brevard Facility
Brevard, North Carolina
EPA ID # NCD 003152329
Dear Mr. Davidson:
The Hazardous Waste Section has reviewed the October 31, 2005 letter from the Aquifer
Protection Section (APS), regarding sampling at the closed Aeration and Biosolids Digestion
Basins (SWMU 4) at the Dupont facility. The Section will include your recommendations in the
sampling program that will be required at SWMU 4 as part of the RCRA Corrective Action
process. In addition, as you requested, the Section will copy the Asheville Regional Office of the
APS on all future correspondence and analytical results generated during the RCRA Corrective
Action process at SWMU 4. If you have any questions or comments, please contact Mark
Wilkins at [phone].
cc: Brent Burch re: Vance Jackson
Mark Wilkins
1646 Mail Service Center, Raleigh, north Carolina 27699-1 46
Phone [phone] FAX 91-715-S00 \Internet htt o'1Ahrastenotnc.or
An Equal Oppor Liil.ity i A`tirriiative Action 'Employer— Printed on Dial Purpose Recycled taper
CA\ine1\1naw\oversight of swmu4 APS.doc

April 14, 2006
Mr. Roger C Edwards_
NCDENR Ashville Regional Office
Division of Water Quality
2090 US Highway 70
Swannanoa, North Carolina 28778
Rescission of NPDES General Stormwater Permit
Agfa Corporation — Transylvania County
Dear Mr. Edwards:
Agfa Corporation
P.O. Box 267
Staton Road
Brevard, NC 28712-0267
RECEIVED
1 r;
AF,heville Regional Office
ri, ifor Protection I/
The purpose of this letter is to communicate a request that the Agfa Brevard site
participation in the General Stormwater Permit NCG 030057 coverage be rescinded and
removed from the list of active sites. We wish to inform you of the present status of the
Agfa Corporation, Brevard Site, manufacturing operation and wastewater treatment
system as part of the NPDES closure process:
• The site is not currently. discharging process wastewater, and does not have any -
surface water discharges.
• The manufacturing areas, and wastewater treatment plants have been shutdown
and demolished in accordance with the closure plan filed with the state:
• The sewers have been pressure washed and the manholes filled and sealed.
• The site is currently conducting demolition and grading of the site under the
active permit for Erosion and Sediment Control Plan filed with the NCDENR
Ashville Regional office.
• At the closure of the E&SC Plan the site will have no surface water outfalls or
exposure to manufacturing related materials or equipment as referenced in the
NPDES (stormwater) permit defmitions.
We believe this site, Agfa Brevard, is completely inactive as a manufacturing facility and
no longer requires coverage under an industrial stormwater permit.
We would like to thank you and your staff for your help on the closure of the stormwater
permit coverage. Any discussions and/or guidance provided by the Ashville Regional
staff would be extremely helpful and appreciated.
C. L. Mel er
-T-
Facilities Manager
Brevard Site
Agfa Corporation
4/13/2006

CC: Charles H. Weaver Jr., NCDWQ, Surface Water Permitting, Raleigh, NC
G. Landon Davidson, Ashville Regional Office, Aquifer Protection
Roy Davis, Asheville Regional Office, Water Quality Section
Aisha Lau, Asheville Regional Office, Water Quality Section
Jamie Vanbuskirk, DuPont Corporate Remediation, Charlotte, NC
David Epps, DuPont Corporate Remediation, Charlotte, NC
Mark Wilkins, NCDENR, Solid Waste Management Division
Roger Galloway, Agfa Corporation, Brevard Site, WWT ORC
Michael E. Gell, Environmental Contractor, Waxhaw, NC
2 4/13/2006

03/14,12006 14: 22
9197153605
D41
March 14, 2006
TO: Bev NCe, AShQViH0 Regional OffiCe
[phone]
FROM; Mark Wilkins
RE: Memo for transfer Gfjwisdiction of sludge basins
Bev,
The memo fTom Landon transferring jurisdiction is attached. Ut me know if you need a reply.
Mark Wilkins
IAtjv;&&d Aa'-�
101 1 / 0 �
/VV&0-Vc.
PAGE 01/82
C, V'�tp(y.

03/14,12006 14:22 9197153605 D41 PAGE 02/02
rJFicttdpel F-Easley
Gorernar
William G, Bass, Jr., Secrelary
_ North Carolina Depoetment of Envlrcnment and Natural R4sour*m
Alan W. Kfirnok, P.E., Director
Dlvlsion of theater quality
Asheville Regional UlTlce
MEMORANDUM
TO: Ellzabeth Cannon., Cbief
North Carolina Hazardous Waste Section
FROM: Landon Davids � o
October 31, 2005
I
c,i �r'imus t�ll��'g -
1`'� Section
Supervisor— Aquifer Protection, Section (APS) \ Y :. ' ,.
RE: Oversight of Aeration and Biosolida Digestion Basins (SV'rW
Brevard Facility
Dupou1VAgfa Incorporated
13revard, North Carolina
EPA ID 4 NCD 003152329
4) at Dupont/AGFA.
On September 7, 2005, the Division of Wafter Quality (DWQ) received a closure plan and sampling
results regarding the closure of the sludge basin and polishing pond at DapontrAGFA. DWQ staff ma
with AGFA representatives on September 15, 2005 to discuss various aspects of the closure plan. Based
upon that meeting and subsequent discussions between AGFA representatives and Mark Wilkins of'your
staff', the Aquifer Protection Section has determined that the responsible party would be best served in this
matter by dealing with a single agency, DWM. We feel that the environmental issues (i.e., soil sampling,
potential additional sludge disposal, long-term groundwater monitoring etc.) will be adequately addressed
wider the RCRA Corrective Action program, The A.PS would recommend sampling of soils that underlie
the baslas as well as continued monitoring of the R87 series knells, MW-209 wells and MW-2.10 wells.
Analytical parameters could remain the same as those required in the NPDES permit. We would ask that
DuponVAGFA, copy the ARC? APS on all future correspondence and analytical results generated by the.
closure and long-term monitoring requirements.
If you bave any questions or cornffients, please contact Landon Davidson at 828-2964680.
M. Mark Wilkins —HWS
Roger Edwards — SWP ARC}
Chet Meinzer — AGFA
Jamie tVanbusskirk - Dupont
>a�°ne ai na MCOO R
,,�Vrtturr�ll�
Aquifer Protection Section, 2090 U_S- Highway 70, surannanoo. N.C. 2877E Teiephona; 82W98-4809 Customer 5ervim
Fax: 828129$-7043 4-877-6'1 6748

RECEIVED
FEB 22 2006
February 20 2006 Asheville n'
uder
Mr. Roger C Edwards
NCDENR Ashville Regional Office
Division of Water Quality
2090 US Highway 70
Swannanoa, North Carolina 28778
Rescinding of NPDES Permit NC0000337
Agfa Corporation — Transylvania County
Dear Mr. Edwards:
�
AGFA
Agfa Corporation
P.O. Box 267
staton Road
Brevard, NC 28712-0267
The purpose of this letter is to communicate a request that the NPDES Permit No.
NC0000337 be rescinded and removed from the list of active permits. We wish to inform
you of the present status of the Agfa Corporation, Brevard Site, manufacturing operation
and wastewater treatment system as part of the NPDES closure process:
• The site is not currently discharging process wastewater, and will not have any
surface water discharges from NPDES outfall 001 in the future.
• The manufacturing areas, and wastewater treatment plants have been shutdown
and demolished in accordance with the closure plan filed with the state. _
• The sewers have been pressure washed and the manholes filled and sealed.
• The discharge line from the clarifier was partially removed after it was flushed
and the temporary clarifier discharge line was dismantled rendering the system
inoperable.
• The site is currently conducting the final stage of demolition and grading under
the active permit for the Erosion & Sediment Control Plan filed with the
NCDENR Ashville Regional office.
• At the closure of the E&SC Plan the site will have no surface water outfalls.
Agfa will move forward with the closure of the wastewater treatment facility in
preparation for the property transfer to E. I. DuPont de Nemours Co. Inc. who will be
responsible for the future management of this Solid Waste Management Unit under their
RCRA corrective action plan.
We would like to thank you and your staff for your help on the closure of the wastewater
treatment facility. The discussions and guidance provided by the Ashville Regional staff
were extremely helpful and aEpreciated.
C. L. Meinzer
Facilities Manager
Brevard Site
Agfa Corporation
1 2/20/2006

CC: Paul E. Rawls, NCDWQ, Surface Water Permitting, Raleigh, NC
G. Landon Davidson, Ashville Regional Office, Aquifer Protection
Larry Frost, Asheville Regional Office, Water Quality Section
Keith Haynes, Asheville Regional -Office, Water Quality Section
Jamie Vanbusldrk, DuPont Corporate Remediation, Charlotte, NC
David Epps, DuPont Corporate Remediation, Charlotte, NC
Mark Wilkins, NCDENR, Solid Waste Management Division
Roger Galloway, Agfa Corporation, Brevard Site, WWT ORC
Michael E. Gell, Environmental Contractor, Waxhaw, NC
2 2/20/2006

,,$) closure question
Subject: AGFA sludge basin(s) closure question
From: Landon Davidson <[e-mail]>
Date: Mon, 10 Oct 2005 11:36:15 -0400
To: [e-mail], [e-mail]
CC: [e-mail], [e-mail]
Kim/Rick-
The APS ARO is planning on transferring jurisdiction of the closure of a sludge and
aeration basin at the former AGFA plant (formerly Dupont) to the RCRA/Haz. Waste
program. The closure plan submitted by AGFA does not satisfy the APS's closure policy
(A.M. memo of Aug. 18, 2003) for these types of treatment units. AGFA has removed a
significant amount of sludge but has not sampled the material beneath the unlined
ponds nor performed any modeling to determine if an impact to groundwater is
probable. The SWP agreed verbally.to AGFA's closure plan about a year ago (right at
the re-org. time in July) which involved sludge removal, sampling of the sludge left
in place followed by applying a 503 residuals argument to allow them to incorporate
the remaining sludge into new fill material. I met with AGFA to express my concerns
which include:
1) The lack of soil sampling beneath the basin floor (these are unlined) and
therefore the lack of any modeling to determine potential impact to groundwater.
2) The fact that the floor of the basin and the remaining sludge are probably below
the existing water table.
3) The fact that impact to groundwater was observed in the past in monitoring wells
adjacent to these units (ammonia)..... so we know there is a hydraulic connection
between groundwater and the basin.
I get the sense that AGFA feels that DWQ moved the target on them in regards to
closure, even though AGFA was given our closure policy in writing over a year ago.
One option I see is to transfer the closure issue over to RCRA Haz. Waste since they
will be managing this site and these basins are considered SWMUs. Mark Wilkins (RCRA
Haz. Waste) has agreed to take over the closure aspect (as he has taken over issues
from Solid Waste at this site).His program would require sampling of soil beneath the
basins as well as long-term groundwater monitoring (which we would establish). One
reason I wanted to run this past you is that this site will ultimately be owned by
the State of North Carolina as part of the Dupont State Forest. Just email me if you
have concerns, otherwise I'll prepare a letter from me to Mark that gives them full
jurisdiction on the issue of basin closure on Friday of this week. Thanks.
Landon
Landon Davidson - [e-mail] ....
North Carolina Dept. of Environment and. Natural Resources
Asheville Regional Office
Division of Water Quality - Aquifer Protection Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Landon Davidson <Landon Davidson ancmail.net>
NC DENR - Asheville Regional Office
Division of Water Quality - Groundwater Section
3/10/2006 8:23 AM
1 of 1

R closure]
Subject: [Fwd: Brevard WWTP closure]
From: Landon Davidson <[e-mail]>
Date: Mon, 26 Sep 2005 08:32:54 -0400
To: [e-mail], [e-mail], [e-mail]
fyi
Landon Davidson - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality — Aquifer Protection Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Subject: Brevard WWTP closure
From: Jamie A Vanbuskirk <[e-mail]>
Date: Thu, 22 Sep 2005 17:55:35 -0400
To: [e-mail], [e-mail]
CC: [e-mail], David E Epps <[e-mail]>
Mark/Landon:
An issue has come to my attention that I am looking for assistance with.
During a recent meeting (9/15) with AGFA and State representatives
discussing the WWTP closure plan at the Brevard facility, differences were
noted concerning the type of pre -closure sampling that was being required
by the State. For several years both AGFA (responsible for the closure)
and DuPont (future owner of the facility) have been working with
representatives within the State to work on an acceptable closure plan.
Guidance was provided that discussed sampling of underlying soils to
predict the potential for adverse impact to groundwater after closure was
complete. Subsequent meetings with State officials re -iterated their
desire to see that what was left would not pose a threat to groundwater.
For these reasons, many samples of the materials that are being left in the
ponds (it is not practical to remove all of the material) have been
sampled. The data has been supplied to the State and consensus has been
reached that it does not appear that these materials will be a future
threat to groundwater.
It was pointed out to AGFA at the 9/15 meeting that despite this,
insufficient sampling has occurred since samples of "underlynig soils" has
not occurred and therefore approval of the closure is not possible.
Notwithstanding the arguments of whether the sampling conducted thus far is
adequate to meet the mutually agreed upon sampling goal, I would like to
ask that this issue be addressed under the RCRA Corrective Action Program
and not delay approval of the Closure. I base this request on the
following:
1) It is obvious that these units are regulated under more than one
regulatory program, including the RCRA HSWA Corrective Action Program (SWMU
4). The RCRA CA Program has the broad regulatory authority to address
3/10/2006 8:15 AM
1 of 2

1P closure]
groundwater protection issues which will adequately ensure that the closed
ponds do not pose a threat to human health and the environment (including
potential future impacts of the materials already sampled and determined to
meet current criteria).
2) There is already a vast network of downgradient monitoring wells that do
not indicate a significant impact on groundwater from the ponds. Past
groundwater impacts are trending downward after earlier corrective measures
taken at the facility and further downward trending is anticipated after
removal of the large amounts of sludges and removal of the surface water
head during recent closure activities.
3) Continued monitoring of downgradient groundwater is anticipated to occur
for many years for the WWTP area and the site as a whole. Any future
remediation decisions at the site due to potential impacts to groundwater
should be made based on this site -wide monitoring.
In order for AGFA to proceed with the closure in a timely manner, we would
like the State to recognize that it is in the best interests of all parties
that the final disposition of this unit can and should be handled under the
RCRA CA program. Please let me know if additional information is
necessary. Your prompt response to this request is appreciated.
This communication is for use by the intended recipient and contains information that
may be privileged, confidential or copyrighted under applicable law. If you are not
the intended recipient, you are hereby formally notified that any use, copying or
distribution of this e-mail, in whole or in part, is strictly prohibited. Please
notify the sender by return e-mail and delete this e-mail from your system. Unless
explicitly and conspicuously designated as "E-Contract Intended", this e-mail does
not constitute a contract offer, a contract amendment, or an acceptance of a contract
offer. This e-mail does not constitute a consent to the use of sender's contact
information for direct marketing purposes or for transfers of data to third parties.
Francais Deutsch Italiano Espanol Portugues Japanese Chinese Korean
http://www..upont.com/cor /email disclaimer.html
......... _.......... ___...........
Landon Davidson <Landon.Davidsonna ncmail.net>
NC DENR - Asheville Regional Office
Division of Water Quality - Groundwater Section
Content -Type: message/rfc822
WWTP closure'!
Content -Encoding: 7bit
2 of 2
3/10/2006 8:15 AM

,$) closure question
Subject: AGFA sludge basin(s) closure question
From: Landon Davidson <[e-mail]>
Date: Mon, 10 Oct 2005 11:36:15 -0400
To: [e-mail], [e-mail]
CC: [e-mail], [e-mail]
Kim/Rick-
The APS ARO is planning on transferring jurisdiction of the closure of a sludge and
aeration basin at the former AGFA plant (formerly Dupont) to the RCRA/Haz. Waste
program. The closure plan submitted by AGFA does not satisfy the APS's closure policy
(A.M. memo of Aug. 18, 2003) for these types of treatment units. AGFA has removed a
significant amount of sludge but has not sampled the material beneath the unlined
ponds nor performed any modeling to determine if an impact to groundwater is
probable. The SWP agreed verbally to AGFA's closure plan about a year ago (right at
the re-org. time in July) which involved sludge removal, sampling of the sludge left
in place followed by applying a 503 residuals argument to allow them to incorporate
the remaining sludge into new fill material. I met with AGFA to express my concerns
which include:
1) The lack of soil sampling beneath the basin floor (these are unlined) and
therefore the lack of any modeling to determine potential impact to groundwater.
2) The fact that the floor of the basin and the remaining sludge are probably below
the existing water table.
3) The fact that impact to groundwater was observed in the past in monitoring wells
adjacent to these units (ammonia)..... so we know there is a hydraulic connection
between groundwater and the basin.
I get the sense that AGFA feels that DWQ moved the target on them in regards to
closure, even though 'AGFA was given our closure policy in writing over a year ago.
One option I see is to transfer the closure issue over to RCRA Haz. Waste since they
will be managing this site and these basins are considered SWMUs. Mark Wilkins (RCRA
Haz. Waste) has agreed to take over the closure aspect (as he has taken over issues
from Solid Waste at this site).His program would require sampling of soil beneath the
basins as well as long-term groundwater monitoring (which we would establish). One
reason I wanted to run this past you is that this site will ultimately be owned by
the State of North Carolina as part of the Dupont State Forest. Just email me if you
have concerns, otherwise I'll prepare a letter from me to Mark that gives them full
jurisdiction on the issue of basin closure on Friday of this week. Thanks.
Landon
Landon Davidson - [e-mail]
.....................................................................................................
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Aquifer Protection Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Landon Davidson <Landon.Davidson crncmail.net>
NC DENR - Asheville Regional Office
Division of Water Quality - Groundwater Section
12/1/2005 7:35 AM
1 of 1

.evard WWTP Closure]
Subject: [Fwd: Re: AGFA Brevard WWTP Closure]
From: Kerry Becker <[e-mail]>
Date: Thu, 29 Sep 2005 10:26:52 -0400
To: Bev Price <[e-mail]>
Kerry Becker - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Subject: Re: AGFA Brevard WWTP Closure
From: Forrest Westall <[e-mail]>
Date: Mon, 04 Oct 200414:53:49 -0400
To: Shannon Mohr Thornburg <[e-mail]>
CC: Kerry Becker <[e-mail]>
Shannon, I reviewed the plan with Kerry and Pm thinking that we sent out a letter of approval (Pve slept
since then). I will copy this to Kerry and make sure. In any event, the plan was to approve an acceptable
Closure plan with the understanding that long term issues would be addressed by DWM in the overall
site managment plan. Thanks. Forrest
Shannon Mohr Thornburg wrote:
Forrest - I was just organizing some paperwork in my office and came across my AGFA Brevard
WWTP Closure file. Is there anything required of me at this point in terms of follow-up, review,
etc.? I was just wondering if I should go ahead and send my file to SWPS Central Files or not.
Thanks for any guidance that you are able to provide!
Shannon
Shannon Mohr Thornburg, Environmental EngineerMailing Address:
Land Application Unitl636 Mail Service Center
Aquifer Protection SectionRaleigh, NC27699-1636
NCDENR-DWQ�sical Address.
Telephone:[phone] C61672728 Capital Boulevard, Room No. 1C 130
Fax:[phone]Raleigh, NC27604
shannon thoinburg(a),ncmail nethttp•//h2o.enr.state.nc.us/ndpu
Forrest Westall - [e-mail]
North Carolina Dept. of Environment and Natural Resources
9/29/2005 10:47 AM
1 of 2

1
29 100'S
fbiect:Fw: AGFABre nrd Site Man
m: "Michael Gelt" tngeIl@eamlwatrconv
To::"Shannon Mohr Thornburg'. <sh�nnon•thor°b"rSC�n llcb 1
Shannon,
at \ �, •.
I ending this. I got a -deliverable on th� first
Mike.
Original Message ----
From: .'Michael Gell'<[e-mail]@ncma'l.net>
To:. 'Shannon Mohr Thornburg'.
Cc: 'Rsy Dechant' <kay [e-mail]>
Sent: Friday, June O4,.20D9 8:2, A.M
Subject: Fw: AGFA Brevard Site Map
Shone n,
The tt..hed Excel spreadsheet contains the analytical results on the P
sng les taken from the polishing pond and
a
the approximate locations. In general four samples were taken from each 9
quadrant and conposited into
the sample. analyzed. The organics. reported were for duplicate composite s
samples of pond .ediment.
not. I le. attached a word. document that contain. the body of she original ' -)
ent to Kim'and Chet .the AGFA
"ant Manager. I chink I have corrected Kay Dechant's email address and _
included her or. the cc list.
Best Regards,
Mike Gell
Environmental Contractor
8709 Kentucky Derby Dr.
Waxhaw; MC 28173
704-843-5756 (home/office/fax) 8 T
Mobile [phone]
Original Message -
! From: -Michael Ge11• y 11@^arolin -J -
To: 'Rim Cols K loon@na+arl t
cc: 'Roger Gall - y el low @ g{ Ray Dech [
k.d.chant@.—il.nec-Ke--ry Beck r rv.becker@hema 1 'chet �) _
Mernzer' < [e-mail]; ] anbus;.rrk@usa. Dupont. com>; -
•David E Epps• <Danzd E.EppB@USA,dupont.Co - m> r
Sent. Tuesday, May IS, 2004 8:54 AM
Subject: AGFA Brevard Site Map
Kim,
Fh tos of the polishing pond and pdf site map( groundwater monitoring
wells) for .the AGFA Brevard site. _ p
,Mike Dell
zV
6/1 £/2004 2:
-,f 3

imap://shannon.thornburg%40dwq.denr.ncmai l . net @ cros.ncmail.net:

Metals &Nitrogen Loadings
.,tCNAME DATESMPL
P-1 1/27/200467
Those
CCA4--a,e a denm oe'dudoB" at 2 feet In me uo IshLna pond
C
ANALYTE
ACETONE
RESULT
11700
MDL
1120
PQL
360
UNIT
UG/KG
DRY
D
%H20 dll
0.75
'
Pounds
Total
AVERAGE
Total
Ib.JAc.
Kg/ha
P_2 1/27/2004
CP-1 1/27/20047
67
ACETONE
ARSENIC
1740
10.0
34
2.49
=. 97
4.98
UG/KG
MG/KG
D
D
0.75
79.90%
61.0
CP-2 1
CP-3 1/27/20047
CP-4 1/27/2DD4
p_1 1/27/2004
/27/2DD4 7
7
ARSENIC
ARSENIC
71 BENZENE
4.72
7.57
ARSENIC 5.87
16
1.98
1.95
1.21
9
3.97
3.89
2.42
89
MG/KG
MG/KG
MG/KG
UG/KG
D
D
D
D
1
75.30%
74.30%
58.70%
0.75 1
35.4
59.0
73.5
U.
57.2
12.2
13.7
P-2 1
CP-1 1/27/2DD47
CP-2
CP-3
CP-4
/27/2004
1/27/20047
1/27/2004
1 /27/20D4
71
7
7
BENZENE 14
CADMIUM 10.4
CADMIUM 5.59
CADMIUM 8.99
CADMIUM
2
0.269
0.210
2.33 0.131
!24
;2.49
11.98
1,95
1.21
UG/KG
D
MG/KG D
MG/KG D
MG/KG
MG/KG
D
D
0.75
79.90%
75.30%
74:30%
58.70%
0.1
63.4
41.9
70.1
29.2
51.1
10.9
12.2
P-1
P_2
1/27/2004
1/27/2004
751
751
CARBON DISULFIDE
CARBON DISULFIDE
83 18
47
189
5 24
UG/KG
UG/KG
D
D
0.75
0.75
0.6
0.4
CP-1
1/27/20047
CHROMIUM
651
4.98 12.4
MG/KG
D
79.90%
3968.8
CP-2
1/27/20047
CHROMIUM
230
0.794 1.98
MG/KG
D
75.30%
1723.1
CP-3
CP-4
1/27/20047
1/27/20047
CHROMIUM
CHROMIUM
508
147
3.89 9.73
0.484 1.21
MG/KG
MGJKG
D
D
74.30%
58.70%
3959.9
1841.4
28733
611.3
687.8
CP-1
CP-2
1/27/2004
1/27/20047
7
COPPER
COPPER
380
202
0,945 4.98
0.754 13.97
MG/KG
MG/KG ID
D
79.90%
75.30%
2316.7
1513.3
CP-3
CP-4
1/27l20047
1 /27/2004
7
COPPER
COPPER
216 10.739
114
'3.89
0.460 12.42
MG/KG
MG/KG
D
D
74.30%
58.70%
1683.7
1428.0
1735A
369.2
415.4
P-2
1 J27l2004
FLUORANTHENE
560
410 14100
UG/KG
D
0.75
4.2
CP-1
1 /27/2004
74
LEAD
82.5
3.93 '9.95
MG/KG
D
79.90%
503.0
!
CP-2
CP-3
CP-4
1 /27/2004
1 /27/2004
1/27/2004
7
7
74
LEAD
LEAD
LEAD
35.4
47.0
57.9
3.14
3.07 7.78
1.91
7.94
4.84
MG/KG
MG/KG
MG/KG
D
D
D
75.30%
74.30%
58.70%
265.2
366.4
725.3
465.0
98.9
111.3
CP-1
1/27/20047
MERCURY
1.45
0.0139
0.491
MG/KG
D
79.90%
8.8
CP-2
1/2712004
74
MERCURY
0.920
0,0113 10.400
MG/KG
D
75.30%
6.9
CP-3
CP-4
1/27/2004
1/27/20047
74
MERCURY
MERCURY
0.468
0,438 10.0065
0.0109 10.384
10.228
MG/KG
MGJKG
D
D
74.30%
58.70%
3.6
5.5
6.2
1.3
1.5
P-1
1 /27/2D04
78
METHYL ETHYL KETO
260
71 I
180
UG/KG
D
0.75
2.0
P-2
1/27/200478
METHYL ETHYLKETO
130
19 148
UG/KG
D
0.75
1.0
CPA1/27/2D0474
MOLYBDENUM
12.5
0.896
4.Yt
MG/KG
D
79.90%
76.2
CP-2
1/27/2004
74
MOLYBDENUM
7.65
0.714
3.97
MG/KG
D
75.30%
57.3
CP-3
CP-4
1 /27/2004
1/27/2004
74
7
MOLYBDENUM
MOLYBDENUM
5.10
3.65
0.700 13.89
0.436
2.42
MG/KG
MG/KG I
D
D
74.30%
58.70%
39.8
45.7
54.7
11.6
13.1
CPA
1/27/20047
NICKEL
126
0.995
4.98
MG/KG
D
79.9p%
768.2
CP-2
1/27/20047
NICKEL
23.2
0.794
3:97
MG/KG
D
75.30%
173.8
CP-3
CP-4
1/27/20047
1/27/20047
NICKEL
NICKEL
38.3
37.3
0.778
0.484 12.42
3.89
MG/KG
MG/KG
D
D
74.30%
58.70%
298.5
467.2
426.9
90.8
102.2
P-2
CPA
1/27/2D04
1/27/200477
1
PYRENE
SELENIUM
430
3.07
410 14100
2.34 14.98
VG/KG
MG/KG
D
D
0.75
0.75
3.3
23.3
23.3
5.0
5.6
CP-1
1/27/20047
SILVER
1290
3.73
12.4
MG/KG
D
79.90%
7664.4
CP-2
1 /27/2004
7
SILVER
736
2.98
9.92
MG/KG
D
75.30%
5513.9
CP-3
CP-4
1/27/20047
1/27/20047
SILVER
SILVER
625
530
2.92
1.82
9.73
16.05
MG/KG
MG/KG
D
D
74.30%
58.70%
4871.9
6639.1
6222.3
1323.9
1489.4
P-2
1/27/200410
TOLUENE
12
5
124
UG/KG
D
0.75
0.1
CP-1
1/27/2004
7
ZINC
1850
4.48
149.8
MG/KG
D
79.90%
11278.5
CP-2
1/27/20047
7JNC
751
3.57
'39.7
MGJKG
D
75.30%
5626.2
CP-3
CP-4
1/27/20047
1/27/2D047
ZINC
ZINC
1490
479
3.50
2.18
j38.9
124.2
MG/KG
MG/KG
D
D
74.30%
58.70%
11614.5
6000.2
8629.9
1836.1
2065.7
CP1
1/27/2004
Coliform, Fecal
37500
1
I
C/Gm
Soil
0.00
1
CP2
1/27/2004
Conform, Fecal
3896.10
1
1
C/Gm
Soil
0.00
1
CP3
1/27/2004
Coliform, Fecal
146052.63
1
C/Gm
Soil
0.00
1
CP4
CPI
1/27/2004
1/27/2004
Coliform, Fecal
Nitrate as N
151204.28
<64
1
641
1
IC/Gm
mg/kg
Soil
Soil
0.00
79.90%
1
61
<390
CP2
1/27/2004
Nitrate as N
<49
491
mg/kg
Soil
75.30%
5
<300
CP3
CP4
1/27/2004
1127/20D4
Nitrate as N
Nitrate as N
1 <29
<28
1 29I
281
mg/kg
!mg/kg
Soil
ISoil
74.30%
58.70%
3
<175
3 <170
<234
1
CPI
1/27/2004
Nitrate-Nifrite (as N)
89
164.
Img/kg
(Soil
79.90%
6 542.6
CP2
1/27l2004
Nitrate -Nitrite (as N)
74
49.
1
mg/kg
Soil
75.30%
CP3
CP4
1/27/2D04-
1/27/2004
Ntrate-Nitrite (as M
NitrateNitite (as N)
49
45
29.
28.
1
mg/kg
mg/kg
Soll
Soil
74,30%
56.70%
ff
510.7
108.E 122.2
CPl
1/27/2004
Nitrogen.total
16153
16.2
mg/kg
Soil
79.90%
6 98476.2
CP2
1/27/2004
Nitrogen,total
12096
6.5
1
Imglkg
Soil
75.30%
6 90634.3
CP3
CP4
1/27/2DD4
1/27/2004
Nitrogentotal
Nitrogen total
6174
8673
13.3
13.0
1
mg/kg
mg/kg
Soil
Soil
74.30%
5B.70%
3 48126.2
3 108642.9
86470
18398 I 20698
CPI
1/27/2004
Nitrogen. Ammonia
11200
56.
I
mg/kg
Soil
79.90%
6 7315.8
CP2
1 /27/2004
Nitrogen, Ammonia
1300
55.
mg/kg
Soil
75.30%
5 9739.2
CP3
CP4
CPI
1/27/2D04
1/27/2004
1/27/2004
Nitrogen,Ammonia
Nitrogen, Ammonia
Nitrogen, Kjeldahi,
320
1200
T 16000
129.
33.
46.
i
1
mg/kg
mg/kg
mg/kg
Soil
Soil
Soil
74.30%
58.70%
79.90%
3 2494.4
3 15031.9
51 97543.4
8645
1839 2069
CP2
1/27/2004
Nitrogen, Kjeldahl,
T 1200D
63.
mg/kg
Soil
74.30%
6
CP3
CP4
1 /27/2004
1/27/2004
Nitrogen, Kle ahl,
Nitrogen, Kjeldohl,
T 6100
T 8600
36.
31.
!
mg/kg
mglkg
Soil
Soil
58.30%
58.70%
47549.1
4 47 728.
3 107728.5
85680
!
16230 20509
CPI
1/27/2004
Percent Moisture
79.90%
%
Sotl
1
CP2
1/27/2004
Percent Moisture
75.30%
%
Soil
1
CP3
1/27/2004
Percent Moisture
74.30%
%
Soil
1
CP4
1 /27l20D4
Percent Moisture
58.70%
%
Sol[
1
((2ft'43560sgft/ac'4.7acres/27cu.ft/cu.ydJ'2DMbs./cu.Yd'(1-J5 %sofids)/10A6)'E5concentration In pounds per million pounds
Assumptions are: 2 ft depth and 2000Ibs.NdA3 to get to a total pounds of material.
Page 1

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basin and process filtrate for disposal through aeration and
through the aeration basin clarifier
until final grading is Let the PP dry, manage StormH20 to
complete process sewer.
Start addding soils
and add mix as
haracteriz
needed to achieve
Remaining
fixing of the solids
solids
and bringing the area
to final grade.
Start dewatering the Aeration basin and
process filtrate through the clarifier.
Characterize the remaining solids.
Commence -final grading
empty
Emergency Diversion Basin
Remove sediments.
j Sample and test liner
Fill and grade
Final Grading and Disposal of Removed
Decommission the clarifier Rsiduais

mailbox:///Cl/Documents%20and%20Settings/shannon_thornburg/A.
Subject: AGFA Brevard WWTP Closure _
From: Shannon Mohr Thornburg <[e-mail]> _
Date: Thu, 30 Sep 2004 09:25:29 -0400
To: Forrest Westall <[e-mail]>
Forrest - I was just organizing some paperwork in my office and came across my AGFA Brevard
WWTP Closure file. Is there anything required of me at this point in terms of follow-up, review, etc.?
I was just wondering if I should go ahead and send my file to SWPS Central Files or not.
Thanks for any guidance that you are able to provide!
Shannon
Shannon Mohr ThornbUrg, EnvironrTiental Engineer
Land Application Unit
Aquifer Protection Section
\ CDENNR-D WQ
Telephone: [phone]I67
13()
Fax: [phone]
shannon.thomburg(),ncmail.net
V.
Mailins) Address
1636 Mail. Service Center
Ralei.ah, NC 27699-1636
Pvsical Address:
277 '28 Capital Boulevard,1?.c+om :No. 1 C"
Raleigh, NC" 2 6004
http://h2o.enr.state.nc.us/ndpu
9/30/2004 9:25 A?

imap://shannon. [e-mail]
Subject: Re: AGFA Brevard WWTP Closure
From: Forrest Westall <[e-mail]>
Date: Mon, 04 Oct 2004 14:53:49 -0400
To: Shannon Mohr Thornburg <[e-mail]>
CC: Kerry Becker <[e-mail]>
Shannon, I reviewed the plan with Kerry and I'm thinking that we sent out a letter of approval (I've
slept since then). I will copy this to Kerry and make sure. In any event, the plan was to approve an
acceptable closure plan with the understanding that long term issues would be addressed by DWM in
the overall site managment plan. Thanks. Forrest
Shannon Mohr Thornburg wrote:
Forrest - I was just organizing some paperwork in my office and came across my AGFA Brevard
WWTP Closure file. Is there anything required of me at this point in terms of follow-up, review,
etc.? I was just wondering if I should go ahead and send my file to SWPS Central Files or not.
Thanks for any guidance that you are able to provide!
Shannon
�itin�?`.rnon hct �}n;�r1Addles,
Land Application Unit 1€i 6 Mail Seri, -ice Center
Aquifer Protection SectionlZaaki-g.h. NC2-699-1€')6
NCDENR-Tit%QP y sical Address:
I'elephone.(919) 15-6i672728 Capital Boulevard, R.00ni tio. IC 130
Fax:(919)'15_tt;1 Ralei>=h.?tii:4''004
shannon.thomburg(a).ncmail.nelhttp://h2o.enr.state.nc.us/ndpu
Forrest Westall - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Forrest Westall <Forrest.Westall(qncmail.net>
NC DENR - Asheville Regional Office
Division of Water Quality - Water Quality Section
10/11/2004 9:51
of 1

irnap://shannon.thomburg%40dwq. [e-mail]'.
Subject: Re: AGFA Brevard WWTP Closure
From: Forrest Westall <[e-mail]>
Date: Mon, 11 Oct 2004 12:40:3 7­0400
To: Shannon Mohr Thornburg <[e-mail]>
CC: Kerry Becker <[e-mail]>
Thanks. Kerry reminded me that a letter had gone out on our approval of the plan and referenced
DWM for any long term issues. Take care. Forrest
Shannon Mohr Thornburg wrote:
Thanks, Forrest!!! I am going to send all of my files to Surface Water Protection Section -Central
Files!!!
Shannon
Forrest Westall wrote:
Shannon, I reviewed the plan with Kerry and I'm thinking that we sent out a letter of approval
(I've slept since then). I will copy this to Kerry and make sure. In any event, the plan was to
approve an acceptable closure plan with the understanding that long term issues would be
addressed by DWM in the overall site managment plan. Thanks. Forrest
Shannon Mohr Thornburg wrote:
Forrest - I was just organizing some paperwork in my office and came across my AGFA
Brevard WWTP Closure file. Is there anything required of me at this point in terms of
follow-up, review, etc.? I was just wondering if I should go ahead and send my file to SWPS
Central Files or not.
Thanks for any guidance that you are able to provide!
Shannon
Shannon �tol,, 7 i1c p)bur_; Environmental : rn7ineer ��lailing�dclress
Land Applicatmn L r t; 6 6 Mail Se,-VicSe,-Vicee Center -----
Aquifer Protection sectionRaiei`h, N- C-27 699-163-6
NCDEN, R-MVQPhysical _'Address:
Telepbone:t 9191 7 15-61672 7 28 Capital Boulevard, Root n No. 1 C 130
Fax:(919) 7. U 8SRa1ei,_xh. \C2-76`.i4
shannon thomburg(a,,ncmail nedittp•//h2o.enr.state.nc.us/ndpu
Forrest Westall - Forrest.Westall(ancmail.net
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
of 2
10/11/2004 2:101

(W
&kL"
TO:��
FRON(
SUBJECT: Guidelines for the Closure of Treatment Ponds and Lagoons
zgust 18, 2003
L11
Purpose: The purpose of these guidelines is to protect the quality of the groundwater resources
of the state while accomplishing the closure of a treatment pond or lagoon.
Background: Man-made treatment ponds and lagoon type structures are used to contain fluids
and semi-solidsfor a variety of reasons. As these ponds and lagoons become no longer
necessary, the structure needs to be abandoned in an environmentally friendly manner. The
Groundwater Section's major.concern with the elimination of these structures is that
groundwater remains protected both during and after abandonment. Each structure must be
considered for its unique circumstances on a case -by -case basis.
Regulations relevant to the abandonment of ponds and lagoons for ground waters of the state
include the Classifications and Water Quality Standards found in Title 15A NCAC 2L. Other
be found in the DENR Land Resources regulations
pertinent standards and regulations may
pertaining to Sedimentation and Erosion Control and Dam Safety, the DENR Waste
Management regulations pertaining to the disposal of wastes and sludge, and the NCDOT
regulations pertaining to transportation of materials on public highways. Lagoons` for animal
waste are regulated under the federal NRCS Standards.
Recommended Procedure:
The major elements of pond and lagoon structures include the contents, the walls, the floor and
the liner, if one exists. Each element must be characterized for its quantity and material
properties in order to prepare a closure plan. Guidelines for the preparation of this plan are
described in the following steps:
1) Collect and assemble field information by characterizing the structural elements and
liquid contents, including bottom sludge in the impoundment. Sampling will be required
in most situations, and the types of sampling and analyses will depend on factors such as
what the lagoon was used for, its construction materials (earthen, concrete, natural or
synthetic liner), and size. The samples must be representative of the medium sampled,
and the rationale for the depths, locations and number of samples should be justified and
documented in preparation of being legally defensible. The sampling must be performed
Lagoon Closure final.doc Page 1 of 3

Upon completion of the closure, the owner should submit documentation to the DWQ regional
office with the following:
1) A description of all actions taken and dates relative to the abandonment.
2) Copies of all pertinent correspondence with private, local, state and/or federal agencies.
3) Ultimate disposal sites with weigh tickets or processing verifications, as appropriate.
4) Certification by a Professional Engineer (PE) or Professional Geologist (PG) if the pond or
lagoon:
a) is greater than five (5) acres in total area,
b) contains hazardous substances as defined by TCLP tests, or
c) involves a breaching of a dam, which could impose a safety hazard to persons or property
below it.
Lagoon Closure final.doc Page 3 of 3

Mr. Roger C. Edwards
Agf
P.O.OCorporation
PBox 267
NCDENR
_
Brevar� 47
Division of Water Quality
-
i 1
Surface Water Protection
2090 U.S. Highway 70Cn
m i k_
Swannanoa, NC 28778
September 6, 2005
v
k
4
Re: Wastewater Treatment Closure
U
Dear Mr. Edwards:
The purpose of this letter is to follow up on the closure plan agreement reached in our
July 2004 meeting and documented in my letter to Kerry Becker, NCDENR August
26, 2004. The Agfa Brevard site, NC NPDES #NC0000337, will move forward with
the closure of the wastewater treatment facility in preparation for a property transfer
to E.I. DuPont de Nemours Co. Inc., who will be responsible for the future
management of this solid waste management unit (SWMU) under their RCRA
corrective action plan.
• The site has completed the biosolids removal phase for these basins using a barge -
mounted diesel dredge. The removed solids were filtered and landfilled in a
Subtitle D landfill. This was the only practical removal method and achieved
approximately 90% removal of the solids.
• In accordance with the closure plan we have calculated the volume of solids
remaining in the basins based on depth measurements for the biosolids, an
estimated area and the percent solid of the biosolids samples.
o Approximately 250 tons of biosolids remain in the basins; approximately
2,520 tons of solids were removed and landfilled off -site.
• Samples of the residual basin material were collected at locations shown in
Enclosure 1. Analytical results are provided as Enclosure 2. The purpose of the
sampling effort was to characterize the post dredging materials with respect to
contaminants regulated by 503 rules and other potential contaminants based on
the NPDES permit limitations.
• Based on the analytical results and the calculated mass we believe the remaining
materials meet the 503 regulations for the environmentally sound use as a one-
time amendment for the reclamation of the site.
• The site will now proceed with the final grading of these basins in accordance
with the E&SC plan approved by the NCDENR Division of Land Management,
Land Quality Section, in October 2004.
9/6/2005

DISCUSSION:
vsing Ulc analyses Ul uic coiilposited biosolids acid water sarripleS taken from the oasins
we have calculated the mass and estimated loading of the pollutants of interest based on
the 503 biosolids disposal regulations. The estimated mass loadings of the pollutants of
interest are presented in Table i, which also lists the loading of the compounds when
spread over the six (6) acres available, and the 503 limits for comparison. The table
provides the following information.
• Compound or element of interest
• The concentration of that compound in the site biosolids samples.
• The maximum biosolids concentration allowed in the 503 regulations.
• The per -acre loading of the compound in pounds based on the calculated mass of
the compound in the remaining biosolids and the six (6) acres available for
grading the material.
• The final column presents the potential loading allowed for each compound over
the life of a biosolids application under the 503 regulations.
The sample locations for the grab and Encore samples locations are shown on Enclosure
No.1, the wastewater treatment area sketch. The samples were taken in March and May
of this year after completion of dredging operations. Copies of laboratory reports for the
samples in our analysis of the sludge removal process are included in Enclosure No. 2 as
PDF files.
Based on the sampling program initiated at the basins and subsequent analysis using appropriate
guidance, AGFA believes the residuals present in the remaining biosolids represent an
acceptable level for all pollutants during the closure of the wastewater treatment basins.
Several constituents that have been detected in samples collected, but do not have 503
limitations. An evaluation of the potential for impact by these constituents is provided below.
Metals:
The NPDES permit limited the discharge of metals form the process areas and these were
removed before the water was sent to the wastewater treatment system. Any trace metals
that went to the WWT system were chemically bound or in an insoluble matrix. In
sampling the biosolids for the 503 constituents Silver was added since it was limited in
the permit.
Silver - A concentration of 1900 mg/kg was detected in the composite sample collected from
the residual basin material in March of 2005. Since 503 rules do not limit for Silver a risk based
residential soil exposure level of 390 mg/kg was used for calculating an acceptable loading.
Based on this calculation the concentration of silver present in the residual basin material would
not exceed an acceptable loading as shown in Table 1. In addition, ground water samples
collected during 2004 from wells located downgradient of the basins did not detect silver above
laboratory practical quantitation limits (e.g., 5ug/1). We believe these results validate the
calculation assumptions used for the 503 evaluations that silver concentrations present in the
basin material have not impacted shallow ground water.
9/6/2005

Appendix IX Organics
Samples of the biosolids were analyzed for the RCRA Appendix IX constituents and the
results are attached. Two types of samples were taken from the residual biosolids: a set of
standard grab samples and a set of Encore (closed tube core sampler) method samples.
The samples were taken on 5/3/05 and analyzed by Pace Labs.
The grab samples had one occurrence of an organic compound present, Toluene at 84 ug/l, which
we have attributed to the presence of the diesel dredge in the basins, and the possible contamination
of the material in the basin with the exhaust products from the dredge. We do not believe this
concentration of a biodegradable organic represents a significant obstacle to the closure process.
This constituent was not detected in samples collected in 2004 from down gradient monitoring
wells above laboratory practical quantitation limits (e.g., 0.5 ug/1)
The Encore samples were collected using SW846 Method 5035 and laboratory preserved
using methanol. This type of sampling limits potential loss of highly volatile organic
compounds into the headspace of conventional sampling containers. Results of the analysis
are provided in Enclosure 2, a more detailed discussion of the results as they pertain to the
closure of the basins is provided below.
• Acetone was present in four samples at an average of 1037 ug/kg in
the sludge samples. We believe the presence of a very volatile and
biodegradable organic solvent in the biosolids is questionable. This
compound has never been detected in the OCPSF sampling conducted
by the site, but it is a common analytical artifact. In addition, the
average concentration of this compound is below the NCDENR
regulatory guidance for soil to ground water migration of 2,810 ug/kg.
Based on this data, the detection of this constituent in the residual
basin materials should not be considered significant to closure of the
basins and was not detected in 2004 samples from down gradient
monitoring wells above laboratory practical quantitation limits (e.g., 3
ug/1)
• Naphthalene was also detected in four samples at an average
concentration of 75 ug/kg, and again, an OCPSF regulated compound
that has never been detected in the years of sampling under the
NPDES program was found in the biosolids. We believe that, if
present the naphthalene does not present a danger to the ground water
or to the closure or the basins if incorporated into the basin closure
grading materials. The average concentration of this compound is
9/6/2005

below the NCDENR regulatory guidance for soil to ground water
t' of 285 ug/k Based on this data the detection of this
migra ion g•
constituent in the residual basin materials should not be considered
significant to closure of the basins. in addition, iris constituent was not
detected in samples collected in 2004 from down gradient monitoring
wells above laboratory practical quantitation limits (e.g., 1 ug/1)
• 2-Butanone (MEK) at 1,700 ug/kg was present in one sample and we
find its presence in the biosolids questionable based on the operational
history of the wastewater treatment system given it is a biodegradable,
volatile organic and that we have no known source on site for this
organic. This constituent was not detected in samples collected in 2004
from down gradient monitoring wells above laboratory practical
quantitation limits (e.g., 5 ug/l)
• 1,2,3 Trichlorobenzene was present in one sample at 33 ug/kg and
this constituent has a high affinity for adsorption to soil (Koc of 589)
therefore will not readily partition to water given its log octanol/water
partitioning coefficient of 4.05. This constituent has not been detected
in ground water samples collected from downgradient wells. Based on
the fate and transport characteristics of this constituent and the
concentration detected it is unlikely that this constituent would impact
shallow ground water underlying the basins and therefore should not
be considered significant to closure of the basins.
In conclusion, we believe we have met the conditions agreed to in our closure agreement with the
State of North Carolina and will now proceed with the completion of this phase within 30 days.
We request that we meet and review this data with you within the next two weeks, so that we may
immediately remedy any concerns, and then proceed with the closure within our business driven
timeline.
Chet Meinzer
cilities M a
Fa er g
CC: Kerry Becker - DWQ
Keith Haynes — DWQ
Larry Frost - DWQ
Landon Davidson — DWQ
Charlene Graff — Agfa
Jamie Van Buskirk — DuPont
David Epps — DuPont
Michael Gell WWT Consultant
Roger Galloway - Agfa
9/6/2005

AGFA Letterhead from: Chet Meinzer to Roger C. Edwards, NCDENR Surface Water Group,
NPDES
The purpose of this letter is to follow up on the closure plan agreement reached in our
July 2004 meeting and documented in my letter to Kerry Becker, NCDENR August
26, 2004. The Agfa Brevard site, NC NPDES #NC0000337, will move forward with
the closure of the wastewater treatment facility in preparation for a property transfer
to E.I. DuPont de Nemours Co. Inc., who will be responsible for the future
management of this solid waste management unit (SWMU) under their RCRA
corrective action plan.
• The site has completed the biosolids removal phase for these basins using a barge -
mounted diesel dredge. The removed solids were filtered and landfilled in a
Subtitle D landfill. This was the only practical removal method and achieved
approximately 90% removal of the solids.
• In accordance with the closure plan we have calculated the volume of solids
remaining in the basins based on depth measurements for the biosolids, an
estimated area and the percent solid of the biosolids samples.
o Approximately 250 tons of biosolids remain in the basins; approximately
2,520 tons of solids were removed and landfilled off -site.
• Samples of the residual basin material were collected at locations shown in
Enclosure 1. Analytical results are provided as Enclosure 2. The purpose of the
sampling effort was to characterize the post dredging materials with respect to
contaminants regulated by 503 rules and other potential contaminants based on
the NPDES permit .limitations.
• Based on the analytical results and the calculated mass we believe the remaining
materials meet the 503 regulations for the environmentally sound use as a one-
time amendment for the reclamation of the site.
• The site will now proceed with the final grading of these basins in accordance
with the E&SC plan approved by the NCDENR Division of Land Management,
Land Quality Section, in October 2004.
9/6/2005

DISCUSSION:
Using the analyses of the composited biosolids and water samples taken from the basins
we have calculated the mass and estimated loading of the pollutants of interest based on
the 503 biosolids disposal regulations. The estimated mass loadings of the pollutants of
interest are presented in Table I, which also lists the loading of the compounds when
spread over the six (6) acres available, and the 503 limits for comparison. The table
provides the following information.
• Compound or element of interest
• The concentration of that compound in the site biosolids samples.
• The maximum biosolids concentration allowed in the 503 regulations.
• The per -acre loading of the compound in pounds based on the calculated mass of
the compound in the remaining biosolids and the six (6) acres available for
grading the material.
• The final column presents the potential loading allowed for each compound over
the life of a biosolids application under the 503 regulations.
The sample locations for the grab and Encore samples locations are shown on Enclosure
No.1, the wastewater treatment area sketch. The samples were taken in March and May
of this year after completion of dredging operations. Copies of laboratory reports for the
samples in our analysis of the sludge removal process are included in Enclosure No. 2 as
PDF files.
Based on the sampling program initiated at the basins and subsequent analysis using appropriate
guidance, AGFA believes the residuals present in the remaining biosolids represent an
acceptable level for all pollutants during the closure of the wastewater treatment basins.
Several constituents that have been detected in samples collected, but do not have 503
limitations. An evaluation of the potential for impact by these constituents is provided below.
Metals:
The NPDES permit limited the discharge of metals form the process areas and these were
removed before the water was sent to the wastewater treatment system. Any trace metals
that went to the WWT system were chemically bound or in an insoluble matrix. In
sampling the biosolids for the 503 constituents Silver was added since it was limited in
the permit.
Silver — A concentration of 1900 mg/kg was detected in the composite sample collected from
the residual basin material in March of 2005. Since 503 rules do not limit for Silver a risk based
residential soil exposure level of 390 mg/kg was used for calculating an acceptable loading.
Based on this calculation the concentration of silver present in the residual basin material would
not exceed an acceptable loading as shown in Table 1. In addition, ground water samples
collected during 2004 from wells located downgradient of the basins did not detect silver above
laboratory practical quantitation limits (e.g., 5ug/1). We believe these results validate the
calculation assumptions used for the 503 evaluations that silver concentrations present in the
basin material have not impacted shallow ground water.
9/6/2005

Appendix IX Organics
Samples of the biosolids were analyzed for the RCRA Appendix IX constituents and the
results are attached. Two types of samples were taken from the residual biosolids: a set of
standard grab samples and a set of Encore (closed tube core sampler) method samples.
The samples were taken on 5/3/05 and analyzed by Pace Labs.
The grab samples had one occurrence of an organic compound present, Toluene at 84 ug/l, which
we have attributed to the presence of the diesel dredge in the basins, and the possible contamination
of the material in the basin with the exhaust products from the dredge. We do not believe this
concentration of a biodegradable organic represents a significant obstacle to the closure process.
This constituent was not detected in samples collected in 2004 from down gradient monitoring
wells above laboratory practical quantitation limits (e.g., 0.5 ug/1)
The Encore samples were collected using SW846 Method 5035 and laboratory preserved
using methanol. This type of sampling limits potential loss of highly volatile organic
compounds into the headspace of conventional sampling containers. Results of the analysis
are provided in Enclosure 2, a more detailed discussion of the results as they pertain to the
closure of the basins is provided below.
• Acetone was present in four samples at an average of 1037 ug/kg in
the sludge samples. We believe the presence of a very volatile and
biodegradable organic solvent in the biosolids is questionable. This
compound has never been detected in the OCPSF sampling conducted
by the site, but it is a common analytical artifact. In addition, the
average concentration of this compound is below the NCDENR
regulatory guidance for soil to ground water migration of 2,810 ug/kg.
Based on this data, the detection of this constituent in the residual
basin materials should not be considered significant to closure of the
basins and was not detected in 2004 samples from down gradient
monitoring wells above laboratory practical quantitation limits (e.g., 3
ug/1)
Naphthalene was also detected in four samples at an average
concentration of 75 ug/kg, and again, an OCPSF regulated compound
that has never been detected in the years of sampling under the
NPDES program was found in the biosolids. We believe that, if
present the naphthalene does not present a danger to the ground water
or to the closure or the basins if incorporated into the basin closure
grading materials. The average concentration of this compound is
9/6/2005

below the NCDENR regulatory guidance for soil to ground water
/ migration of 285 ug/kg. Based on this data, the detection of this
constituent in the residual basin materials should not be considered
significant to closure of the basins. In addition, this constituent was not
detected in samples collected in 2004 from down gradient monitoring
wells above laboratory practical quantitation limits (e.g., 1 ug/1)
• 2-Butanone (MEK) at 1,700 ug/kg was present in one sample and we
find its presence in the biosolids questionable based on the operational
history of the wastewater treatment system given it is a biodegradable,
volatile organic and that we have no known source on site for this
organic. This constituent was not detected in samples collected in 2004
from down gradient monitoring wells above laboratory practical
quantitation limits (e.g., 5 ug/1)
• 1,2,3- Trichlorobenzene was present in one sample at 33 ug/kg and
this constituent has a high affinity for adsorption to soil (Koc of 589)
therefore will not readily partition to water given its log octanol/water
partitioning coefficient of 4.05. This constituent has not been detected
in ground water samples collected from downgradient wells. Based on
the fate and transport characteristics of this constituent and the
concentration detected it is unlikely that this constituent would impact
shallow ground water underlying the basins and therefore should not
be considered significant to closure of the basins.
In conclusion, we believe we have met the conditions agreed to in our closure agreement with the
State of North Carolina and will now proceed with the completion of this phase within 30 days.
We request that we meet and review this data with you within the next two weeks, so that we may
immediately remedy any concerns, and then proceed with the closure within our business driven
timeline.
9/6/2005

Compound
Arsenic
Cadmium
Chromium
Lead
Nickel
Selenium
Zinc
Silver
Aluminum
Calcium
Potassium
Sodium
Nitrogen, T
PAN Nitrogen
Fecal Coliform
Table I
Brevard Site WWTP Biosolids Residuals
Residual Solids Biosolids
t h/Ar• 5(I3,. ,hi�/ac)
uoncentratiun
ND-mg/Kg
.7VJ l 16; .ri-
75 mg/Kg
< 2@
36.5
7.9
85
0.68
34.7
620
3000
54
2670
340
4300
29
1335
44
840
3.7
267
ND
57
<0.02
15.1
5.3
75
0.47
16
39
420
3.5
374
ND
100
< 2
89
1200
1900
7500
390*/1370**
105
165
2240
1 226****
32000
None
2,794***
None
5700
None
497
None
2800
None
243
None
2900
None
253
None
ND
None
None
None
623
None
55
None
• 11,000
3,400
None
None
960
296
None
None
ND
<1000MPN/g
ND
@ Based on the detection limit listed by the lab
* Residential limit for ingestion by child soil concentration
* * Industrial Brownfield silver limit in soil.
*** Normal soil concentrations 20,000 to 50,000 mg/kg
* * * * 390 mg/kg to a depth of one foot
9/6/2005

Enclosure No.1
Basin Sample Locations
Sludge MGM # 1 [A]
Sludge MGM #2 [B]
Equal -Aeration #3 [C]
Equal -Aeration #4 [D]
Waste Treatment Sludge [E]
Sludge MGM # 1(ENCORE) [F]
Sludge MGM #2(ENCORE) [G]
Equal -Aeration #3 (ENCORE) [H]
Equal -Aeration #4(ENCORE) [I]
9/6/2005

Enclosure No.2
Pace Labs Report Project
No.9293484
No. 9291307
No. 9290415
Demolition Samples
Sludge Lagoon and Aeration Basin
All as .pdf files
9/6/2005

Enclosure No.3
Groundwater Section Guidelines for the
Investigation and Remediation of
Soil and Groundwater
Table 3
Contaminated Soil Clean-up Levels
9/6/2005

Enclosure NO. 1 Basin Sample Locations
Data From Roger Galloway 8/11/2005 MEG
MW-109A
R87—S6
MW-109B
to
R87—S7
MW —209B
MW-209A
R87—S3
7
T� -S4 A, R87
12B &A 2C
SWMU 12A
R87-S5
A
jp
�Rn
TV, W
T, _j I-
j 10,
WIT, -ilivr
6 7
1, �,,
.. . . ....
U;
'q
L
Tz
Ark;
_QN!,
R
-,ff,
...... . . . ......
P
T�l
C',
-211E
M-21 1 C
MW —21 1A
mh
1M,
'alvAli"A Y,

i
Enclosure No.3 Excerpted from the
GROUNDWATER SECTION GUIDELINES FOR THE
INVESTIGATION AND REMEDIATION OF
SOIL AND GROUNDWATER
STATE of NORTH CAROLINA
DEPARTMENT of ENVIRONMENT and NATURAL RESOURCES
DIVISION of WATER QUALITY
GROUNDWATER SECTION
http://gw.ehnr.state.nc.us
July 2000
Table 3
Contaminated Soil Clean -Up Levels
Compound
CAS #
Soil to GW
(mg/kg)*
Acenaphthene
83-32-9
8
Acenaphthylene
208-96-8
11
Acetone
67-64-1
2.81
Anthracene
120-12-7
995
Barium
7440-39-3
848
71-43-2
0.0056
Benzene
56-55-3
0.34
Benzo(a)anthracene
Benzo(b)fluoranthene
205-99-2
1
Benzo(g,h,l)perylene
191-24-2
6720
Benzo(k)fluoranthene
207-08-9
12
50-32-8
0.091/0.088**
Benzo(a)pyrene
65-85-0
112
Benzoic acid
Bis(chloroethyl)ether(BCEE)
111-44-4
0.0002
n-Butylbenzene
104-51-8
4
Sec -Butyl benzene
135-98-8
3
Tert-Butylbenzene
104-51-8
3
Carbon
75-15-0
4
Chloromethane(methyl chloride)
74-87-3
0.02
Chromium III
16065-83-1
27
Chromium VI
18540-29-9
27
Chrysene
218-01-9
38
Dibenzo(a,h)anthrace ne
53-70-8
0.17/0.088**
Dibenzofuran
132-64-9
4.7
Dibromochloromethane
124-48-1
0.002
1,2-Dibromoethane (ethylene dibromide; EDB)
106-93-4
0.00000197
1,2-Dichlorobenzene
95-50-1
7
1,3-Dichlorobenzene
541-73-1
24
1,4-Dichlorobenzene
106-46-7
1
1,1-Dichloroethane (1,1-DCA)
75-34-3
4

' 1,2-Dichloroethane (ethylenedichloride;1,2-DCA)
107-06-2
0.0018
1,2-Dichloroethene (cis)(cis-1,2-DCE)
156-59-2
0.35
1,2-Dichloroethene (trans) (trans-1,2-DCE)
156-60-5
0.38
1, 1 -Dichloroethane (1,1-DCE)
75-35-4
0.045
1,2-Dichloropropane
78-87-5
0.0029
1,3-Dichloropropene (cis and trans)
542-75-6
0.0009
2,4-Dimethylphenol
105-67-9
0.9
Ethyl acetate
141-78-6
11
Ethylbenzene
100-41-4
0.24
Fluoranthene
206-44-0
276
Fluorene
86-73-7
44
Hexachlorobutadiene
87-68-3
0.26
2-Hexanone
591-78-6
1.9
Indeno(1,2,3-cd)pyrene
193-39-5
3
Isopropyl benzene (cumene)
98-82-8
2
Isopropyl ether (diisopropylether)
108-20-3
0.37
Lead
7439-92-1
270
Methanol
67-56-1
14
Methylethylkeytone (2-Butanone; MEK)
78-93-3
0.69
Methyl tert-butyl ether (MTBE)
1634-04-4
0.92
Methylene Chloride
75-09-2
0.02.
2-Methylnaphthalene
91-57-6
3
Naphthalene
91-20-3
0.58
Phenanthrene
85-01-8
60
n-Propylbenzene
103-65-1
2
Pyrene
129-00-0
286
1,1,2,2-Tetrachlorethane
79-34-5
0.001
Tetrachloroethylene (PCE)
127-18-4
0.0074
1,2,4-Trichlorobenzene
120-82-1
2.6
1,2,4-Trimethylbenzene
95-63-6
8
1,3,5-Trimethylbenzene
108-67-8
7
Toluene
108-88-3
7
Xylenes (mixed)
1330-20-7
5
Notes * If the soil contaminant concentration is less than the method detection limit,
the maximum soil concentration should be set at the level of the
method detection limit.
** Residential Level
July 2000

Table I
Brevard Site WWTP Biosolids Residuals
Residual Solids Biosolids
�._•� �_ i_ e� ! 7 ,,7 ,+oa T h/An Cfl2 T,h_/ac_
l,Om ounu
Arsenic
t vticcuu auvn
ND-mg/Kg
75 mg/Kg
< 2@
36.5
Cadmium
7.9
85
0.68
34.7
Chromium
620
3000
54
2670
Copper
Lead
340
44
4300
840
29
3.7
1335
267
Mercury
Molybdenum
Nickel
ND
5.3
39
57
75
420
<0.02
0.47
3.5
15.1
16
374
Selenium
Zinc
Silver
ND
1200
1900
100
7500
390*/1370**
< 2
105
165
89
2240
1,226****
Aluminum
32000
None
2,794***
None
Calcium
5700
None
497
None
Magnesium
Potassium
2800
2900
None
None
243
253
None
None
Sodium
ND
None
None
None
Phos hate
623
None
55
None
Nitrogen, T
PAN Nitrogen
11,000
3,400
None
None
960
296
None
None
Fecal Coliform
ND
<1000MPN/
ND
@ Based on the detection limit listed by the lab
* Residential limit for ingestion by child soil concentration
** Industrial Brownfield silver limit in soil.
*** Normal soil concentrations 20,000 to.50,000 mg/kg
**** 390 mg/kg to a depth of one foot ,, e

L11V loi J't,�ily V.1
Basin Sample Locations
Sludge MGM # 1 [A]
Sludge MGM #2 [B]
Equal -Aeration #3 [C]
Equal -Aeration #4 [D]
Waste Treatment Sludge [E]
Sludge MGM # 1(ENCORE) [F]
Sludge MGM #2(ENCORE) [G]
Equal -Aeration #3 (ENCORE) [H]
Equal -Aeration #4(ENCORE) [I]
9/6/2005

Enclosure NO.1 Basin Sample Locations
Data From Roger Galloway
sn liaoos MEG
..
MW-109A
R87-S6' MW-109B
1 R87-S7'�.
r 7
4
f
A o MW-2096
Ltd F, MW-209A
e �q
-s
`�s � ` R87-$3
MaN 20 ` f
w
NOV �5 (�
_ A
y,— ppy E b4a'
Hi
i
R87-S4
}t't a S "
e
C Jd MWi
uNI17� 2248 f ! R87-S5
MW-224A Vie'xl
r
�9y
V =
x.
YiYie _ f
: � B
,MW-211C
MW-211A
d
r gj
�Anra 4%ir,�-.P ��t1L.li9/J>tE7`

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
malXical w Phone: [phone] Phone. [phone]
wwwpaceiabs,cam Fax: 704.875,9091 Fax. • 828.252.4618
May 13, 2005
Mr. Roger Galloway
AGFA Corporation
P.O. Box 267
Brevard,NC 28712 _
RE: Lab Project Number: 9293484
Client Project ID: Demolition
Samples
Dear Mr. Galloway:
Enclosed are the analytical results for
sample(s) received by the laboratory on May 3,
2005. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of
the report.
If you have any questions concerning
this report please feel free to contact me.
Sincerely,
R
4d Ph
Lorri Patton
[e-mail]
Project Manager
Enclosures
Asheville Certification los
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater 40
This report shall not he reproduced, except in full,
NC Wastewater 12
NC Drinking Water 37706
NC Drinking Water 57712
without the written consent of Pace Analytical Services, Inc.
SC 99006
SC Environmental 99030
*�� /+�
FL NELAP E87627
FL NELAP E87648
���'y�Q

Solid results are reported on
vBenzo(k)fluoranthene
Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
Biphenyl (Diphenyl)
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
Date: 05/13/05
Lab Project Number: 9293484
Client Project ID: Demolition Samples
ght basis
Project Sample Number: 9293484-001 Date Collected: 05/03/U5 12:z5
Matrix: Water Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Prep/Method:
EPA 3510 / EPA 8270
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
5000
ND
ug/l
1000
ND
ug/l
2000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
2000
ND
ug/l
2000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
2000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
1000
ND
ug/l
5000
ND
ug/l
5000
l
05/12/05 01:56 BET 83-32-9
05/12/05 01:56 BET 208-96-8
05/12/05 01:56 BET 62-53-3
05/12/05 01:56 BET 120-12-7
05/12/05 01:56 BET 207-08-9
05/12/05 01:56 BET 205-99-2
05/12/05 01:56 BET 56.55-3
05/12/05 01:56 BET 65-85-0
05/12/05 01:56 BET 191-24-2
05/12/05 01:56 BET 100-51-6
05/12/05 01:56 BET 50-32-8
05/12/05 01:56 BET 92-52-4
05/12/05 01:56 BET 101-55-3
05/12/05 01:56 BET 85-68-7
05/12/05 01:56 BET 59-50-7
05/12/05 01:56 BET 106-47-8
05/12/05 01:56 BET 111-,91-1
05/12/05 01:56 BET 111-44-4
05/12/05 01:56 BET 39638-32-9
05/12/05 01:56 BET 91-58-7
05/12/05 01:56 BET 95-57.8
05/12/05 01:56 BET 7005-72-3
05/12/05 01:56 BET 218-01-9
05/12/05 01:56 BET 53-70-3
05/12/05 01:56 BET 132-64-9
05/12/05 01:56 BET 95-50-1
05/12/05 01:56 BET 541-73-1
05/12/05 01:56 BET 106-46-7
05/12/05 01:56 BET 91-94-1
05/12/05 01:56 BET 120-83.2
05/12/05 01:56 BET 84-66-2
05/12/05 01:56 BET 105-67-9
05/12/05 01:56 BET 131-11-3
05/12/05 01:56 BET 84-74-2
05/12/05 01:56 BET 534-52.1
05/12/05 01:56 BET 51-28-5
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030
FL_NEL AP E87648
Page: 1 of 55
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NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FI Nn nn F�7�n7
nTl Hr

Lab Sample No: 925584591
Project Sample
Number: 9293484-001
Date Collected: 05/03/05 12:25
Client Sample ID: SLUDGE MGM°1
Matrix: Water
Date Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
ByCAS
No.
Qual RegLmt
2,4-Dinitrotoluene :.
ND
ug/l
1000
05/12/05
01:56
BET
121 14 2
2,6-Dinitrotoluene :r
ND
ug/1
1000
05/12/05
01:56
BET
606-20 2
Di-n-octylphthal�te
ND
ug/1
1000
05/12/05
01:56
BET
117-84-0
1,2-Diphenyl'hydrazine
ND
ug/l
2000
05/12/05
01:56
BET
122-66-7
bis(2-Ethyl iiexyl)phthalate
ND
ug/1
1000
05/12/05
01:56
BET
117-81-7
Fluoran "e
ND
ug/l
1000
05/12/05
01:56
BET
206-44-0
Fluorene
ND
ug/l
1000
05/12/05
01:56
BET
86 73 7
0exachioro-1,3-butadiene
ND
ug/l
1000
05/12/05
01:56
BET
87 68 3
Hexachlorobenzene
ND
ug/1
1000
05/12/05
01:56
BET
118 74 1
Hexachlorocyclopentadiene
ND
ug/l
1000
05/12/05
01:56
BET
77-47-4
Hexachloroethane
ND
ug/l
1000
05/12/05
01:56
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
1000
05/12/05
01:56
BET
193-39-5
Isophorone
ND
ug/l
1000
05/12/05
01:56
BET
78-59-1
2-Methylnaphthalene
ND
ug/l
1000
05/12/05
01:56
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
1000
05/12/05
01:56
BET
95-48-7
3&4-Methylphenol
ND
ug/l
1000
05/12/05
01:56
BET
Naphthalene
ND
ug/l
1000
05/12/05
01:56
BET
91-20-3
2-Nitroaniline
ND
ug/l
5000
05/12/05
01:56
BET
88774-4
3-Nitroaniline
ND
ug/l
5000
05/12/05
01:56
BET
99-09-2
4-Nitroaniline
ND
ug/l
5000
05/12/05
01:56
BET
100-01-6
Nitrobenzene
ND
ug/l
1000
05/12/05
01:56
BET
98-95-3
2-Nitrophenol
ND
ug/l
1000
05/12/05
01:56
BET
88-75-5
4-Nitrophenol
ND
ug/l
5000
05/12/05
01:56
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
1000
05/12/05
01:56
BET
62-75-9
1,2
N-Nitroso-di-n-propylamine
ND
ug/l
1000
05/12/05
01:56
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
1000
05/12/05
01:56
BET
86-30-6
Pentachlorophenol
ND
ug/l
5000
05/12/05
01:56
BET
87-86-5
Phenanthrene
ND
ug/l
1000
05/12/05
01:56
BET
85-01-8
Phenol
ND
ug/l
1000
05/12/05
01:56
BET
108-95-2
Pyrene
ND
ug/l
1000
05/12/05
01:56
BET
129-00-0
1,2,4-Trichlorobenzene
ND
ug/1
1000
05/12/05
01:56
BET
120-82-1
2,4,5-Trichlorophenol
ND
ug/l
5000
05/12/05
01:56
BET
95-95-4
2,4,6-Trichlorophenol
ND
ug/l
1000
05/12/05
01:56
BET
88-06-2
Nitrobenzene-d5 (S)
18
%
05/12/05
01:56
BET
4165-60-0
3
2-Fluorobiphenyl (S)
35
%
05/12/05
01:56
BET
321-60-8
Terphenyl-d14 (S)
50
%
05/12/05
01:56
BET
1718-51-0
Phenol-d5 (S)
8
%
05/12/05
01:56
BET
4165-62-2
4
2-Fluorophenol (S)
9
%
05/12/05
01:56
BET
367-12-4
4
2,4,6-Tribromophenol (S)
51
%
05/12/05
01:56
BET
Page: 2 of 55
Date: 05/13/05
REPORT OF LABOATO ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IDs
NO Wastewater
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without the written consent of Pace Analytical Services, Inc.
NO Wastewater
12
NO Drinking Water
37712
N A��oRo
° ' """
NO Drinking Water
SC
37706
99006
SC Environmental
99030
�� "g
ol;w: ct-
FF"dELAp
C476.27
,
ELAv�u
FL N P
Eg7Fnn

aceAnalytical
www.pacelabs.com
Lab Sample No: 925584591
Client Sample ID: SLUDGE MG
Date Extracted
1,4-Dioxane by 8270�SIM
1,4-Dioxane (p Dioxane)
Date Extracted
/MS'`k'Vol ati 1 es
;G%MS VOCs by 8260, low level
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
Date: 05/13/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
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Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-001
Matrix: Water
Date Collected: 05/03/05 12:25
Date Received: 05/03/05 15:42
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
05/09/05
05/09/05
Prep/Method:
EPA 3510 /
EPA 8270
ND
ug/l
60.
05/11/05
15:46
BET
123-91-1 2
05/09/05
05/09/05
Method: EPA
8260
ND
ug/l
10.
05/06/05
22:07
MSF
71-43-2
ND
ug/l
10.
05/06/05
22:07
MSF
108-86-1
ND
ug/l
10.
05/06/05
22:07
MSF
74-97-5
ND
ug/l
10.
05/06/05
22:07
MSF
75-27-4
ND
ug/l
10.
05/06/05
22:07
MSF
75-25-2
ND
ug/l
10.
05/06/05
22:07
MSF
74-83-9
ND
ug/l
10.
05/06/05
22:07
MSF
104-51-8
ND
ug/l
10.
05/06/05
22:07
MSF
135-98-8
ND
ug/l
10.
05/06/05
22:07
MSF
98-06-6
ND
ug/l
10.
05/06/05
22:07
MSF
56-23-5
ND
ug/l
10.
05/06/05
22:07
MSF
108-90-7
ND
ug/l
10.
05/06/05
22:07
MSF
75-00-3
ND
ug/l
10.
05/06/05
22:07
MSF
67-66-3
ND
ug/l
10.
05/06/05
22:07
MSF
74.87-3
ND
ug/l
10.
05/06/05
22:07
MSF
95-49-8
ND
ug/l
10.
05/06/05
22:07
MSF
106-43-4
ND
ug/l
10.
05/06/05
22:07
MSF
96-12-8
ND
ug/1
10.
05/06/05
22:07
MSF
124-48-1
ND
ug/l
10.
05/06/05
22:07
MSF
106-93-4
ND
ug/l
10.
05/06/05
22:07
MSF
74-95-3
ND
ug/l
10.
05/06/05
22:07
MSF
95-50-1
ND
ug/l
10.
05/06/05
22:07
MSF
541-73-1
ND
ug/l
10.
05/06/05
22:07
MSF
106-46-7
ND
ug/l
10.
05/06/05
22:07
MSF
75-71-8
ND
ug/l
10.
05/06/05
22:07
MSF
75-34-3
ND
ug/l
10.
05/06/05
22:07
MSF
107-06-2
ND
ug/1
10.
05/06/05
22:07
MSF
75-35-4
ND
ug/l
10.
05/06/05
22:07
MSF
156-59-2
ND
ug/l
10.
05/06/05
22:07
MSF
156-60-5
ND
ug/l
10.
05/06/05
22:07
MSF
78-87-5
ND
ug/l
10.
05/06/05
22:07
MSF
142-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
y ACCpgO
ar``
Page: 3 of 55
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37706
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c" IIM AI
1 L IV LLn
E87627

Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2,2-Dichloropropane
ND
ug/l
10.
05/06/05
22:07
MSF
594-20-7
1,1-Dichloropropene
ND
ug/l
10.
05/06/05
22:07
MSF
563 58 6
Diisopropyl eiher,�
ND
ug/1
10.
05/06/05
22:07
MSF
108-20-3
Ethyl benzene a-
ND
ug/l
10.
05/06/05
22:07
MSF
100 41 4
Hexachlord--4,3-butadiene
ND
ug/l
10.
05/06/05
22:07
MSF
87 68 3
Isopropylbenzene (Cumene)
ND
ug/l
10.
05/06/05
22:07
MSF
98 82 8
p Isopropyltoluene
ND
ug/l
10.
05/06/05
22:07
MSF
99 87 6
=:Methylene chloride
ND
ug/l
20.
05/06/05
22:07
MSF
75-09-2
Methyl -test -butyl ether
ND
ug/1
10.
05/06/05
22:07
MSF
1634-04-4
Naphthalene
ND
ug/l
10.
05/06/05
22:07
MSF
91-20-3
n-Propylbenzene
ND
ug/l
10.
05/06/05
22:07
MSF
103-65.1
Styrene
ND
ug/1
10.
05/06/05
22:07
MSF
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/l
10.
05/06/05
22:07
MSF
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/l
10.
05/06/05
22:07
MSF
79.34.5
Tetrachloroethene
ND
ug/l
10.
05/06/05
22:07
MSF
127-184
Toluene
84.
ug/l
10.
05/06/05
22:07
MSF
108-88-3
1,2,3-Trichlorobenzene
ND
ug/l
10.
05/06/05
22:07
MSF
87-61-6
1,2,4-Trichlorobenzene
ND
ug/l
10.
05/06/05
22:07
MSF
120-82-1
1,1,1-Trichloroethane
ND
ug/1
10.
05/06/05
22:07
MSF
71-55.6
1,1,2-Trichloroethane
ND
ug/l
10.
05/06/05
22:07
MSF
79-00-5
Trichloroethene
ND
ug/l
10.
05/06/05
22:07
MSF
79-01-6
Trichlorofluoromethane
ND
ug/l
10.
05/06/05
22:07
MSF
75-69.4
1,2,3-Trichloropropane
ND
ug/l
- 10.
05/06/05
22:07
MSF
96-18-4
1,2,4-Trimethylbenzene
ND
ug/l
10.
05/06/05
22:07
MSF
95-63-6
1,3,5-Trimethylbenzene
ND
ug/1
10.
05/06/05
22:07
MSF
108-67-8
Vinyl chloride
ND
ug/1
10.
05/06/05
22:07
MSF
75-01-4
m&p-Xylene
ND
ug/l
20.
05/06/05
22:07
MSF
o-Xylene
ND
ug/1
10.
05/06/05
22:07
MSF
95-47-6
Toluene-d8 (S)
103
%
05/06/05
22:07
MSF
2037-26-5
4-Bromofluorobenzene (S)
96
%
05/06/05
22:07
MSF
460-00-4
Dibromofluoromethane (S)
90
%
05/06/05
22:07
MSF
1868-53-7
1,2-Dichloroethane.d4 (S)
89
%
05/06/05
22:07
MSF
17060-07-0 5
Page: 4 of 55
Date: 05/13/05
Asheville Certification IN This report shall not be reproduced, except in full,
NO Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NO Drinking Water 37712 " "
SC Environmental 99030
FL NELAP E87648
Charlotte Certification IDs
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NO Drinking Water 37706
SC 99006
F1 INF! AP Fn7[)%7

Lab Sample No: 925584609
Client Sample ID: SLUDGE MG
GUMS Semi vol ati
semi vol atile Orgam
Acenaphthene,,
Acenaphthylenea'
Aniline
Benib(k)fluoranthene
,' Benzo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
Biphenyl (Diphenyl)
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
Date: 05/13/05
Project Sample Number: 9293484-002 Date Collected: Ub/U3/Ub iz:4b
Matrix: Water Date Received: 05/03/05 15:42
Results.
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Prep/Method:
EPA 3510
/ EPA 8270
ND
ug/l
1000
05/12/05
01:22
BET
83-32-9
ND
ug/l
1000
05/12/05
01:22
BET
208-96-8
ND
ug/l
1000
05/12/05
01:22
BET
62.53-3
ND
ug/l
1000
05/12/05
01:22
BET
120-12-7
ND
ug/l
1000
05/12/05
01:22
BET
207-08-9
ND
- ug/1
1000
05/12/05
01:22
BET
205-99-2
ND
ug/l
1000
05/12/05
01:22
BET
56-55-3
ND
ug/l
5000
05/12/05
01:22
BET
65-85-0
ND
ug/l
1000
05/12/05
01:22
BET
191-24-2
ND
ug/l
2000
05/12/05
01:22
BET
100-51-6
ND
ug/1
1000
05/12/05
01:22
BET
50-32-8
ND
ug/l
1000
05/12/05
01:22
BET
92-52-4
ND
ug/l
1000
05/12/05
01:22
BET
101-55-3
ND
ug/l
1000
05/12/05
01:22
BET
85-68-7
ND
ug/l
2000
05/12/05
01:22
BET
59-50-7
ND
ug/l
2000
05/12/05
01:22
BET
106-47-8
ND
ug/l
1000
05/12/05
01:22
BET
111-91-1
ND
ug/l
1000
05/12/05
01:22
BET
111-44-4
ND
ug/l
1000
05/12/05
01:22
BET
39638-32-9
ND
ug/l
1000
05/12/05
01:22
BET
91-58-7
ND
ug/1
1000
05/12/05
01:22
BET
95-57-8
ND
ug/l
1000
05/12/05
01:22
BET
7005-72-3
ND
ug/1
1000
05/12/05
01:22
BET
218-01-9
ND
ug/l
1000
05/12/05
01:22
BET
53-70-3
ND
ug/l
1000
05/12/05
01:22
BET
132-64-9
ND
ug/l
1000
05/12/05
01:22
BET
95-50-1
ND
ug/1
1000
05/12/05
01:22
BET
541-73-1
ND
ug/l
1000
05/12/05
01:22
BET
106-46-7
ND
ug/1
2000
05/12/05
01:22
BET
91-94-1
ND
ug/l
1000
05/12/05
01:22
BET
120-83-2
ND
ug/1
1000
05/12/05
01:22
BET
84-66-2
ND
ug/l
1000
05/12/05
01:22
BET
105-67-9
ND
ug/l
1000
05/12/05
01:22
BET
131-11-3
ND
ug/l
1000
05/12/05
01:22
BET
84-74-2
ND
ug/l
5000
05/12/05
01:22
BET
534-52-1
ND
ug/1
5000
05/12/05
01:22
BET
51-28-5
ND
ug/l
1000
05/12/05
01:22
BET
121-14-2
l
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
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L NELAP E87648::�!'.1C'
Page: 5 of 55
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E87627
FL N€LAP

l
ce Analytica
www.pacelabs.com
Lab Sample No: 925584609
Client Sample ID: SLUDGE MG
2,6-Dinitrotolu
Di-n-octylphtha
1,2-Diphenylhyd
bis(2-Ethyl
hexy
Fluoranthene
Fluorene`
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-002 Date Collected: 05/03/05 12:4b
Matrix: Water Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
�e ND ug/l 1000 05/12/05 01:22 BET 606 20 2
ate ND ug/l 1000 05/12/05 01:22 BET 117 84 0
azne ND ug/l 2000 05/12/05 01:22 BET 122-66 7
)phthalate ND ug/l 1000 05/12/05 01:22 BET 117-81-7
He " loro-1,3-butadiene
.�Hexachlorobenzene
Hexachlorocyclopentadien
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-Cresol
3&4-Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
-
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylami
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date Extracted
Date: 05/13/05
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NC Drinking Water
37712
SC Environmental
99030
FL NELAP
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ND
e
ug/l
1000
05/12/05
01:22
BET
206-44-0
ND
ug/l
1000
05/12/05
01:22
BET
86-73.7
ND
ug/l
1000
05/12/05
01:22
BET
87-68-3
ND
ug/l
1000
05/12/05
01:22
BET
118.74-1
ND
ug/l
1000
05/12/05
01:22
BET
77-47-4
ND
ug/l
1000
05/12/05
01:22
BET
67-72-1
ND
ug/l
1000
05/12/05
01:22
BET
193-39-5
ND
ug/l
1000
05/12/05
01:22
BET
78-59-1
ND
ug/l
1000
05/12/05
01:22
BET
91-57-6
ND
ug/l
1000
05/12/05
01:22
BET
95-48-7
ND
ug/l
1000
05/12/05
01:22
BET
ND
ug/l
1000
05/12/05
01:22
BET
91-20-3
ND
ug/l
5000
05/12/05
01:22
BET
88-74-4
ND
ug/l
5000
05/12/05
01:22
BET
99-09-2
ND
ug/l
- 5000
05/12/05
01:22
BET
100-01-6
ND
ug/l
1000
05/12/05
01:22
BET
98-95-3
ND
ug/l
1000
05/12/05
01:22
BET
88-75-5
ND
ug/l
5000
05/12/05
01:22
BET
100-02-7
ND
ug/l
1000
05/12/05
01:22
BET
62-75-9 1,2
ne ND
ug/l
1000
05/12/05
01:22
BET
621-64-7
ND
ug/l
1000
05/12/05
01:22
BET
86-30-6
ND
ug/l
5000
05/12/05
01:22
BET
87-86-5
ND
ug/l
1000
05/12/05
01:22
BET
85-01-8
ND
ug/l
1000
05/12/05
01:22
BET
108-95-2
ND
ug/l
1000
05/12/05
01:22
BET
129-00-0
ND
ug/l
1000
05/12/05
01:22
BET
120-82-1
ND
ug/l
5000
05/12/05
01:22
BET
95-95-4
ND
ug/l
1000
05/12/05
01:22
BET
88-06-2
36
%
05/12/05
01:22
BET
4165-60-0
60
%
05/12/05
01:22
BET
321-60-8
69
%
05/12/05
01:22
BET
1718-51-0
21
5.1
05/12/05
01:22
BET
4165-62-2
29
%
05/12/05
01:22
BET
367-12-4
64
%
05/12/05
01:22
BET
05/09/05
05/09/05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inca
N ACCpR
Page: 6 of 55
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ceAnalytical°
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Lab Sample No: 925584609
Client Sample ID: SLUDGE MG
1,4-Dioxane by 8270 SIM,�'
1,4-Dioxane (p Dioxane)
Date Extracted
GUMS Vol at I es
GC/MS,,,V by 8260, low level
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Date: 05/13/05
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-002 Date Collected: 05/03/05 12:45
Matrix: Water Date Received: 05/03/05 15:42
_ Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Prep/Method:
EPA 3510 /
EPA 8270
ND
ug/l
60.
05/11/.05
14:31
BET
123-91-1 2
05/09/05
05/09/05
Method: EPA
8260
ND
ug/l
10.
05/06/05
22:33
MSF
71-43-2
ND
ug/i
10.
05/06/05
22:33
MSF
108-86-1
ND
ug/l
10.
05/06/05
22:33
MSF
74-97-5
ND
ug/l
10.
05/06/05
22:33
MSF
75,27-4
ND
ug/l
10.
05/06/05
22:33
MSF
75-25.2
ND
ug/l
10.
05/06/05
22:33
MSF
74-83-9
ND
ug/1
10.
05/06/05
22:33
MSF
104-51-8
ND
ug/l
10.
05/06/05
22:33
MSF
135-98-8
ND
ug/1
10.
05/06/05
22:33
MSF
98-06-6
ND
ug/l
10.
05/06/05
22:33
MSF
56-23.5
ND
ug/l
10.
05/06/05
22:33
MSF
108-90-7
ND
ug/l
10.
05/06/05
22:33
MSF
75-00-3
ND
ug/l
10.
05/06/05
22:33
MSF
67-66-3
ND
ug/1
10.
05/06/05
22:33
MSF
74-87-3
ND
ug/l
10.
05/06/05
22:33
MSF
95-49-8
ND
ug/l
10.
05/06/05
22:33
MSF
106-43-4
ND
ug/1
10.
05/06/05
22:33
MSF
96-12-8
ND
ug/l
10.
05/06/05
22:33
MSF
124-48-1
ND
ug/l
10.
05/06/05
22:33
MSF
106-93-4
ND
ug/1
10.
05/06/05
22:33
MSF
74-95-3
ND
ug/l
10.
05/06/05
22:33
MSF
95-50-1
ND
ug/l
10.
05/06/05
22:33
MSF
541-73-1
ND
ug/1
10.
05/06/05
22:33
MSF_
106-46-7
ND
ug/l
10.
05/06/05
22:33
MSF
75-71-8
ND
ug/1
10.
05/06/05
22:33
MSF
75-34-3
ND
ug/l
10.
05/06/05
22:33
MSF
107-06-2
ND
ug/l
10.
05/06/05
22:33
MSF
75-35-4
ND
ug/l
10.
05/06/05
22:33
MSF
156-59-2
ND
ug/l
10.
05/06/05
22:33
MSF
156-60-5
ND
ug/1
10.
05/06/05
22:33
MSF
78-87-5
ND
ug/l
10.
05/06/05
22:33
MSF
142-28-9
ND
ug/l
10.
05/06/05
22:33
MSF
594-20-7
ND
ug/1
10.
05/06/05
22:33
MSF
563-58-6
-r,EPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
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��
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37706
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E87627

aceAnalW cal°
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Lab Sample No: 925584609
Client Sample ID: SLUDGE MG
Parameters
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3 bgtadiene
Isopropylbenzene(Cumene
p-Isopropy1toluene
Methy166e' chloride
Meths -tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 05/13/05
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-002 Date Collected: 05/03/05 12:45
Matrix: Water Date Received: 05/03/05 15:42
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
ND
ug/l
10.
05/06/05
22:33
MSF
108-20-3
ND
ug/l
10.
05/06/05
22:33
MSF
100-41-4
ND
ug/l
10.
05/06/05
22:33
MSF
87-68-3
ND
ug/l
10.
05/06/05
22:33
MSF
98-82-8
ND
ug/l
10.
05/06/05
22:33
MSF
99-87-6
ND
ug/l
20.
05/06/05
22:33
MSF
75-09-2
ND
ug/l
10.
05/06/05
22:33
MSF
1634-04-4
ND
ug/l
10.
05/06/05
22:33
MSF
91-20-3
ND
ug/l
10.
05/06/05
22:33
MSF
103-65-1
ND
ug/l
10.
05/06/05
22:33
MSF
100-42-5
ND
ug/l
10.
05/06/05
22:33
MSF
630-20-6
ND
ug/l
10.
05/06/05
22:33
MSF
79-34-5
ND
ug/l
10.
05/06/05
22:33
MSF
127-18.4
ND
ug/l
10.
05/06/05
22:33
MSF
108-88-3
ND
ug/l
10.
05/06/05
22:33
MSF
87-61-6
ND
ug/l
10.
05/06/05
22:33
MSF
120-82-1
ND
ug/l
10.
05/06/05
22:33
MSF
71-55-6
ND
ug/l
10.
05/06/05
22:33
MSF
79-00-5
ND
ug/l
10.
05/06/05
22:33
MSF
79-01-6
ND
ug/l
10.
05/06/05
22:33
MSF
75-69-4
ND
ug/l
10.
05/06/05
22:33
MSF
96-18-4
ND
ug/l
10.
05/06/05
22:33
MSF
95-63-6
ND
ug/l
10.
05/06/05
22:33
MSF
108-67.8
ND
ug/l
10.
05/06/05
22:33
MSF
75-01-4
ND
ug/l
20.
05/06/05
22:33
MSF
ND
ug/l
10.
05/06/05
22:33
MSF
95-47-6
102
%
05/06/05
22:33
MSF
2037-26-5
96
%
05/06/05
22:33
MSF
460-00-4
94
%
05/06/05
22:33
MSF
1868-53-7
85
%
05/06/05
22:33
MSF
17060-07-0 5
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NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
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al °
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Benzo(k)f1uoranthene
Ben zo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
Biphenyl (Diphenyl)
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene,
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
Date: 05/1V05
Asheville Certification IDS
NC Wastewater
40
6NVC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-003 Date Collected: 05/03/05 12:05
#3 Matrix: Water Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Prep/Method:
EPA 3510
/ EPA 8270
NO
ug/l
67.
05/11/05
05:26
BET
83-32-9
NO
ug/l
67.
05/11/05
05:26
BET
208.96-8
NO
ug/l
67.
05/11/05
05:26
BET
62-53-3
NO
ug/l
67.
05/11/05
05:26
BET
120-12-7
NO
ug/l
67.
05/11/05
05:26
BET
207-08-9
NO
ug/l
67.
05/11/05
05:26
BET
205-99-2
NO
ug/l
67.
05/11/05
05:26
BET
56-55-3
NO
ug/l
330
05/11/05
05:26
BET
65-85-0
NO
ug/l
67.
05/11/05
05:26
BET
191-24-2
NO
ug/l
130
05/11/05
05:26
BET
100-51-6
NO
ug/l
67.
05/11/05
05:26
BET
50-32-8
NO
ug/l
67.
05/11/05
05:26
BET
92-524
NO
ug/l
67.
05/11/05
05:26
BET
101-55.3
NO
ug/l
67.
05/11/05
05:26
BET
85-68-7
NO
ug/l
130
05/11/05
05:26
BET
59-50-7
NO
ug/l
130
05/11/05
05:26
BET
106-47-8
NO
ug/l
67.
05/11/05
05:26
BET
111-91-1
NO
ug/l
67.
05/11/05
05:26
BET
111-44-4
NO
ug/l
67.
05/11/05
05:26
BET
39638.32-9
NO
ug/l
67.
05/11/05
05:26
BET
91-58-7
NO
ug/l
67.
05/11/05
05:26
BET
95-57-8
NO
ug/l
67.
05/11/05
05:26
BET
7005-72,3
NO
ug/l
67.
05/11/05
05:26
BET
218-01-9
NO
ug/l
67.
05/11/05
05:26
BET
53-70-3
NO
ug/l
67.
05/11/05
05:26
BET
132-64-9
NO
ug/l
67.
05/11/05
05:26
BET
95-50-1
NO
ug/l
67.
05/11/05
05:26
BET
541-73-1
NO
ug/l
67.
05/11/05
05:26
BET
106-46-7
NO
ug/l
130
05/11/05
05:26
BET
91-94.1
NO
ug/l
67.
05/11/05
05:26
BET
120-83-2
NO
ug/l
67.
05/11/05
05:26
BET
84-66.2
NO
ug/l
67.
05/11/05
05:26
BET
105-67-9
NO
ug/l
67.
05/11/05
05:26
BET
131-11.3
NO
ug/l
67.
05/11/05
05:26
BET
84-74-2
NO
ug/l
330
05/11/05
05:26
BET
534-52-1
NO
ug/l
330
05/11/05
05:26
BET
51-28-5
NO
ug/l
67.
05/11/05
05:26
BET
121-14.2
Page:
9 of 55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Charlotte Certification IDs
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37706
r qy
SC
99006
NFL L LH
FL nice A
E87627

Lab Sample No: 925584633
Client Sample ID: EQUAL-AER
Project Sample Number: 9293484-003 Date Collected: 05/03/05 12:05
Matrix: Water Date Received: 05/03/05 15:42
rameters
Results
Units
Report Limit
Analyzed
By
CAS No. Quay Re4Lmt
2,6 Dinitrotoluene F
ND
ug/1
67.
05/11/05
05:26
BET
606 20 2
Di-n-octylphthalate-
ND
ug/l
67.
05J11/05
05:26
BET
117 84 0
1,2-Diphenylhydrazine
ND
ug/l
130
05/11/05
05:26
BET
122-66-7
bis(2-Ethylhekyl)phthalate
ND
ug/l
67.
05/11/05
05:26
BET
117-81-7
Fluoranthene
ND
ug/l
67.
05/11/05
05:26
BET
206-44-0
ND
ug/l
67.
05/11/05
05:26
BET
86-73.7
oro-1,3-butadiene
5orobenzene
ND
ug/l
67.
05/11/05
05:26
BET
87-68-3
ND
ug/l
67.
05/11/05
05:26
BET
118-74-1
Hexachlorocyclopentadiene
ND
ug/l
67.
05/11/05
05:26
BET
77-47-4
Hexachloroethane
ND
ug/l
67.
05/11/05
05:26
BET
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/l
67.
05/11/05
05:26
BET
193-39-5
Isophorone
ND
ug/l
67.
05/11/05
05:26
BET
78-59-1
2-Methylnaphthalene
ND
ug/l
67.
05/11/05
05:26
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
67.
05/11/05
05:26
BET
95-48-7
3&4-Methylphenol
ND
ug/l
67.
05/11/05
05:26
BET
Naphthalene
ND
ug/l
67.
05/11/05
05:26
BET
91-20-3
2-Nitroaniline
ND
ug/l
330
05/11/05
05:26
BET
88-74-4
3-Nitroaniline
ND
ug/l
330
05/11/05
05:26
BET
99-09.2
4-Nitroaniline
ND
ug/l
330
05/11/05
05:26
BET
100-01-6
Nitrobenzene
ND
ug/l
67.
05/11/05
05:26
BET
98-95-3
2-Nitrophenol
ND
ug/l
67.
05/11/05
05:26
BET
88-75-5
4-Nitrophenol
ND
ug/l
330
05/11/05
05:26
BET
100-02-7
N-Nitrosodimethylamine
ND
ug/l
67.
05/11/05
05:26
BET
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/l
67.
05/11/05
05:26
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/1
67.
05/11/05
05:26
BET
86-30-6
Pentachlorophenol
ND
ug/l
330
05/11/05
05:26
BET
87-86-5
Phenanthrene
ND
ug/l
67.
05/11/05
05:26
BET
85-01-8
Phenol
ND
ug/l
67.
05/11/05
05:26
BET
108.95-2
Pyrene
ND
ug/l
67.
05/11/05
05:26
BET
129-00-0
1,2,4-Trichlorobenzene
ND
ug/l
67.
05/11/05
05:26
BET
120-82-1 2
2,4,5-Trichlorophenol
ND
ug/l
330
05/11/05
05:26
BET
95-95-4
2,4,6-Trichlorophenol
ND
ug/l
67.
05/11/05
05:26
BET
88-06.2
Nitrobenzene-d5 (S)
35
%
05/11/05
05:26
BET
4165-60-0
2-Fluorobiphenyl (S)
36
%
05/11/05
05:26
BET
321-60-8
Terphenyl-d14 (S)
66
%
05/11/05
05:26
BET
1718-51-0
Phenol-d5 (S)
18
%
05/11/05
05:26
BET
4165-62-2
2-Fluorophenol (S)
24
%
05/11/05
05:26
BET
367-12-4
2,4,6-Tribromophenol (S)
69
%
05/11/05
05:26
BET
Date Extracted
05/05/05
05/05/05
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
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Lab Sample No: 925584633
Client Sample ID: EQUAL AERATION,'�3
1,4-Dioxane by 8270 t,),1K:'
1,4-Dioxane (p Dioxane)
Date Extracted4"T"�"�,02
GUMS Vo 'at l es
GC/MS 1iCs by 8260, low level
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Date: 05/13/05
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-003 Date Collected: 05/03/05 12:05
Matrix: Water Date Received: 05/03/05 15:42
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Prep/Method:
EPA 3510
/ EPA 8270
ND
ug/l
60.
05/11/05
15:21
BET
123 91 1 2
05/09/05
05/09/05
Method: EPA
8260
ND
ug/l
10.
05/06/05
22:59
MSF
71-43-2
ND
ug/l
10.
05/06/05
22:59
MSF
108-86.1
ND
ug/l
10.
05/06/05
22:59
MSF
74-97.5
ND
ug/l
10.
05/06/05
22:59
MSF
75-27-4
ND
ug/l
10.
05/06/05
22:59
MSF
75-25-2
ND
ug/l
10.
05/06/05
22:59
MSF
74-83-9
ND
ug/l
10.
05/06/05
22:59
MSF
104-51-8
ND
ug/l
10.
05/06/05
22:59
MSF
135•98-8
ND
ug/l
10.
05/06/05
22:59
MSF
98-0& 6
ND
ug/l
10.
05/06/05
22:59
MSF
56-23-5
ND
ug/l
10.
05/06/05
22:59
MSF
108-90-7
ND
ug/l
10.
05/06/05
22:59
MSF
75-00-3
ND
ug/l
10.
05/06/05
22:59
MSF
67-66-3
ND
ug/l
10,
05/06/05
22:59
MSF
74-87-3
ND
ug/l
10.
05/06/05
22:59
MSF
95-49-8
ND
ug/l
10.
05/06/05
22:59
MSF
106-43-4
ND
ug/l
10.
05/06/05
22:59
MSF
96-12.8
ND
ug/l
10.
05/06/05
22:59
MSF
124-48.1
ND
ug/l
10.
05/06/05
22:59
MSF
106-93-4
ND
ug/1
10.
05/06/05
22:59
MSF
74-95-3
ND
ug/l
10.
05/06/05
22:59
MSF
95-50-1
ND
ug/l
10.
05/06/05
22:59
MSF
541-73-1
ND
ug/l
10.
05/06/05
22:59
MSF
106-46-7
ND
ug/l
10.
05/06/05
22:59
MSF
75-71-8
ND
ug/l
10.
05/06/05
22:59
MSF
75-34-3
ND
ug/1
10.
05/06/05
22:59
MSF
107-06-2
ND
ug/l
10.
05/06/05
22:59
MSF
75-35-4
ND
ug/l
10.
05/06/05
22:59
MSF
156-59-2
ND
ug/l
10.
05/06/05
22:59
MSF
156-60-5
ND
ug/l
10.
05/06/05
22:59
MSF
78-87-5
ND
ug/l
10.
05/06/05
22:59
MSF
142-28-9
ND
ug/l
10.
05/06/05
22:59
MSF
594-20-7
ND
ug/l
10.
05/06/05
22:59
MSF
563-58-6
• • 1` • 1 ' ( ' 1 1
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Lab Sample No: 925584633
Client Sample ID: EQUAL-AER
Diisopropyl ether
Ethylbenzene
Hexachloro-1„3 butadiene
Isopropylberl.2ene (Cumene)
p- Isopropyl -toluene
MethylYene chloride
Meth-yl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane_(S)
1,2-Dichloroethane-d4 (S)
Date: 05/13/05
Project Sample Number: 9293484-003 Date Collected: 05/03/05 12:05
Matrix: Water Date Received: 05/03/05 15:42
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
ND
ug/l
10.
05/06/05
22:59
MSF
108-20-3
ND
ug/l
10.
05/06/05
22:59
MSF
100-41-4
ND
ug/l
10.
05/06/05
22:59
MSF
87-68-3
ND
ug/l
10.
05/06/05
22:59
MSF
98-82-8
ND
ug/l
10.
05/06/05
22:59
MSF
99-87-6
ND
ug/l
20.
05/06/05
22:59
MSF
75-09-2
ND
ug/l
10.
05/06/05
22:59
MSF
1634.04.4
ND
ug/l
10.
05/06/05
22:59
MSF
91-20-3
ND
ug/l
10.
05/06/05
22:59
MSF
103-65-1
ND
ug/l
10.
05/06/05
22:59
MSF
100-42-5
ND
ug/l
10.
05/06/05
22:59
MSF
630-20-6
ND
ug/l
10.
05/06/05
22:59
MSF
79-34-5
ND
ug/l
10.
05/06/05
22:59
MSF
127-18-4
ND
ug/l
10.
05/06/05
22:59
MSF
108-88-3
ND
ug/l
10.
05/06/05
22:59
MSF
87-61-6
ND
ug/l
10.
05/06/05
22:59
MSF
120-82.1
ND
ug/l
10.
05/06/05
22:59
MSF
71-55-6
ND
ug/l
10.
05/06/05
22:59
MSF
79-00-5
ND
ug/l
10.
05/06/05
22:59
MSF
79-01-6
ND
ug/l
10.
05/06/05
22:59
MSF
75-69-4
ND
ug/l
10.
05/06/05
22:59
MSF
96-18-4
ND
ug/l
10.
05/06/05
22:59
MSF
95-63-6
ND
ug/l
10.
05/06/05
22:59
MSF
108-67-8
ND
ug/l
10.
05/06/05
22:59
MSF
75-01-4
ND
ug/l
20.
05/06/05
22:59
MSF
ND
ug/l
10.
05/06/05
22:59
MSF
95-47-6
103
%
05/06/05
22:59
MSF
2037-26-5
96
%
05/06/05
22:59
MSF
460.00-4
92
%
05/06/05
22:59
MSF
1868-53-7
89
5.1
05/06/05
22:59
MSF
17060-07-0 5
REPORT OF LABORATORY ANALYSIS
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Lab Sample No: 925584641
Client Sample ID: EQUAL-AERAI,
GUMS Semi vol at
Semivolatile Organ-,
t;
Acenaphthene k
Acenaphthylene= '��
Aniline
Anthra, ne
Benzo'tk)fluoranthene
Ben zo(b)fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g,h,i)perylene
Benzyl alcohol
Benzo(a)pyrene
Biphenyl (Diphenyl)
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
Date: 05/13/05
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-004 Date Collected: 05/03/05 11:50
Matrix: Water Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Prep/Method:
EPA 3510
/ EPA 8270
NO
ug/l
50.
05/11/05
06:04
BET
83-32-9
NO
ug/l
50.
05/11/05
06:04
BET
208-96-8
ND
ug/l
50.
05/11/05
06:04
BET
62-53-3
NO
ug/l
50.
05/11/05
06:04
BET
120-12-7
ND
ug/l
50.
05/11/05
06:04
BET
207-08.9
NO
ug/1
50.
05/11/05
06:04
BET
205-99.2
NO
ug/l
50.
05/11/05
06:04
BET
56-55.3
NO
ug/l
250
05/11/05
06:04
BET
65-85-0
NO
ug/l
50.
05/11/05
06:04
BET
191-24-2
NO
ug/l
100
05/11/05
06:04
BET
100-51-6
NO
ug/l
50.
05/11/05
06:04
BET
50-32.8
NO
ug/1
50.
05/11/05
06:04
BET
92-52-4
ND
ug/l
50.
05/11/05
06:04
BET
101-55-3
NO
ug/l
50.
05/11/05
06:04
BET
85-68-7
ND
ug/l
100
05/11/05
06:04
BET
59-50-7
NO
ug/l
100
05/11/05
06:04
BET
106-47-8
ND
ug/l
50.
05/11/05
06:04
BET
111-91-1
NO
ug/l
50.
05/11/05
06:04
BET
111-44-4
NO
ug/l
50.
05/11/05
06:04
BET
39638-32-9
NO
ug/1
50.
05/11/05
06:04
BET
91-58-7
ND
ug/l
50.
05/11/05
06:04
BET
95-57-8
NO
ug/l
50.
05/11/05
06:04
BET
7005-72-3
NO
ug/l
50.
05/11/05
06:04
BET
218-01-9
NO
ug/1
50.
05/11/05
06:04
BET
-53-70-3
NO
ug/l
50.
05/11/05
06:04
BET
132-64-9
NO
ug/l
50.
05/11/05
06:04
BET
95-50-1
NO
ug/l
50.
05/11/05
06:04
BET
541-73-1
NO
ug/l
50.
05/11/05
06:04
BET
106-46-7
NO
ug/l
100
05/11/05
06:04
BET
91-94-1
NO
ug/l
50.
05/11/05
06:04
BET
120-83-2
ND
ug/l
50.
05/11/05
06:04
BET
84-66-2
NO
ug/l
50.
05/11/05
06:04
BET
105-67-9-
NO
ug/l
50.
05/11/05
06:04
BET
131-11-3
NO
ug/l
50.
05/11/05
06:04
BET
84-74-2
NO
ug/l
250
05/11/05
06:04
BET
534-52-1
NO
ug/l
250
05/11/05
06:04
BET,
51-28-5
NO
ug/l
50.
05/11/05
06:04
BET
121-14-2
REPORT OF LABORATORY ANALYSIS
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anQ q n�l 'n�'®
liC� Hl t l�
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Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax:[phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Lab Sample No: 925584641
Project Sample
Number: 9293484-004
Date Collected: 05/03/05 11:50
Client Sample ID: EQUAL AERAT;30N'#4
Matrix: Water
Date Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2;6 Dinitrotoluene
ND
ug/l
50.
05/11/05
06:04
BET
606 20 2
Di-n-octylphthalate.>'3
ND
ug/l
50.
05/11/05
06:04
BET
117-84-0
1,2-Diphenylhydraz ne
ND
ug/l
100
05/11/05
06:04
BET
122-66 7
„.., ._
bis(2-Ethylhexyl)phthalate
ND
ug/1
50.
05/11/05
06:04
BET
117-81-7
Fluoranthene
ND
ug/l
50.
05/11/05
06:04
BET
206-44-0
P
FIuor ne
ND
ug/1
50.
05/11/05
06:04
BET
86 73 7
Hexachloro-1,3-butadiene
ND
ug/l
50.
05/11/05
06:04
BET
87 68 3
Hexachlorobenzene
ND
ug/1
50.
05/11/05
06:04
BET
118 74 1
Hexachloro cyclopentadiene
ND
ug/1
50.
05/11/05
06:04
BET
77 47 4
Hexachloroethane
ND
ug/l
50.
05/11/05
06:04
BET
67 72 1
Indeno(1,2,3-cd)pyrene
ND
ug/l
50.
05/11/05
06:04
BET
193-39-5
Isophorone
ND
ug/l
50.
05/11/05
06:04
BET
78-59-1
2-Methylnaphthalene
ND
ug/l
50.
05/11/05
06:04
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/l
50.
05/11/05
06:04
BET
95-48-7
3&4-Methylphenol
ND
ug/l
50.
05/11/05
06:04
BET
Naphthalene
ND
ug/l
50.
05/11/05
06:04
BET
91-20-3
2-Nitroaniline
ND
ug/l
250
05/11/05
06:04
BET
88-74-4
3-Nitroaniline
ND
ug/l
250
05/11/05
06:04
BET
99-09-2
4-Nitroaniline
ND
ug/l
250
05/11/05
06:04
BET
100-01-6
Nitrobenzene
ND
ug/l
50.
05/11/05
06:04
BET
98-95-3
2-Nitrophenol
ND
ug/l
50.
05/11/05
06:04
BET
88-75-5
4-Nitrophenol
ND
ug/1
250
05/11/05
06:04
BET
100-02.7
N-Nitrosodimethylamine
ND
ug/l
50.
05/11/05
06:04
BET
62.75-9
N-Nitroso-di-n-propylamine
ND
ug/l
50.
05/11/05
06:04
BET
621-64.7
N-Nitrosodiphenylamine
ND
ug/l
50.
05/11/05
06:04
BET
86-30-6
Pentachlorophenol
ND
ug/l
250
05/11/05
06:04
BET
87-86-5
Phenanthrene
ND
ug/l
50.
05/11/05
06:04
BET
85-01-8
Phenol
ND
ug/l
50.
05/11/05
06:04
BET
108-95-2
ND
ug/l
50.
05/11/05
06:04
BET
129-00-0
Pyrene
1,2,4-Trichlorobenzene
ND
ug/l
50.
05/11/05
06:04
BET
120-82-1 2
2,4,5-Trichlorophenol
ND
ug/l
250
05/11/05
06:04
BET
95-95-4
2,4,6-Trichlorophenol
ND
ug/l
50.
05/11/05
06:04
BET
88-06-2
Nitrobenzene-d5 (S)
33
%
05/11/05
06:04
BET
4165-60-0
2-Fluorobiphenyl (S)
36
%
05/11/05
06:04
BET
321-60-8
Terphenyl-d14 (S)
57
%
05/11/05
06:04
BET
1718-51-0
Phenol-d5 (S)
15
%
05/11/05
06:04
BET
4165-62-2
2-Fluorophenol (S)
19
%
05/11/05
06:04
BET
367-12-4
2,4,6-Tribromophenol (S)
65
%
05/11/05
06:04
BET
Date Extracted 05/05/05
05/05/05
Date: 05/13/05
,EPORT OF LABORATORY ANALYS101;
Asheville Certification IN This report shall not be reproduced, except in full,
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Lab Sample No: 925584641
Client Sample ID: EQUAL-AER
1,4-Dioxane by 8270 ,STM:�"`�
1,4-Dioxane (p DOX-4fle)
Date Extracted,, -
GUMS Vol A l es
GUMS.,-,V6Cs by 8260, low level
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2•Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Date: 05/13/05
Project Sample Number: 9293484-004 Date Collected: 05/03/05 11:50
Matrix: Water Date Received: 05/03/05 15:42
Results
Units
Report Limit
Analyzed
By
CAS No. Quay RegLmt
Prep/Method:
EPA 3510 /
EPA 8270
ND
ug/l
60.
05/11/05
14:56
BET
123-91-1 2
05/09/05
05/09/05
Method: EPA
8260
ND
ug/1
1.0
05/07/05
13:55
BCK
71-43-2
ND
ug/l
1.0
05/07/05
13:55
BCK
108-86-1
ND
ug/l
1.0
05/07/05
13:55
BCK
74-97.5
ND
ug/1
1.0
05/07/05
13:55
BCK
75-27-4
ND
ug/l
1.0
05/07/05
13:55
BCK
75-25-2
ND
ug/l
1.0
05/07/05
13:55
BCK
74-83-9
ND
ug/l
1.0
05/07/05
13:55
BCK
104-51-8
ND
ug/l
1.0
05/07/05
13:55
BCK
135-98-8
ND
ug/1
1.0
05/07/05
13:55
BCK
98-06-6
ND
ug/l
1.0
05/07/05
13:55
BCK
56-23-5
ND
ug/l
1.0
05/07/05
13:55
BCK
108-90-7
ND
ug/1
1.0
05/07/05
13:55
BCK
75-00-3
ND
ug/l
1.0
05/07/05
13:55
BCK
67-66-3
ND
ug/l
1.0
05/07/05
13:55
BCK
74-87-3
ND
ug/l
1.0
05/07/05
13:55
BCK
9549-8
ND
ug/l
1.0
05/07/05
13:55
BCK
106-43-4
ND
ug/l
1.0
05/07/05
13:55
BCK
96-12-8
ND
ug/1
1.0
05/07/05
13:55
BCK
_124-48-1
ND
ug/l
1.0
05/07/05
13:55
BCK
106-93-4
ND
ug/l
1.0
05/07/05
13:55
BCK
74-95-3
ND
ug/1
1.0
05/07/05
13:55
BCK
95-50-1
ND
ug/l
1.0
05/07/05
13:55
BCK
541-73-1
ND
ug/l
1.0
05/07/05
13:55
BCK
106-46-7
ND
ug/1
1.0
05/07/05
13:55
BCK
75-71-8
ND
ug/1
1.0
05/07/05
13:55
BCK
75-34-3
ND
ug/1
1.0
05/07/05
13:55
BCK
107-06-2
ND
ug/l
1.0
05/07/05
13:55
BCK
75-35-4
ND
ug/l
1.0
05/07/05
13:55
BCK
156-59-2
ND
ug/l
1.0
05/07/05
13:55
BCK
156-60-5
ND
ug/l
1.0
05/07/05
13:55
BCK
78-87-5
ND
ug/l
1.0
05/07/05
13:55
BCK
142-28-9
ND
ug/l
1.0
05/07/05
13:55
BCK
594-20-7
ND
ug/l
1.0
05/07/05
13:55
BCK
563-58-6
Page: 15 of 55
REPORT OF LABORATORY ANALYSIS
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99030
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i�"'1'e1act.
Sc
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99006
E87627
FL VELAP
E87648

aceAnalytical°
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Lab Sample No: 925584641 Project Sample Number: 9293484-004 Date Collected: 05/03/05 11:50
Client Sample ID: EQUAL AERAT20N 14 Matrix: Water Date Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Diisopropyl ether
ND
ug/1
1.0
05/07/05
13:55
BCK
108 20 3
Ethylbenzene
ND
ug/1
1.0
05/07/05
13:55
BCK
100-41-4
Hexachloro-1,3 butadiene
ND
ug/l
1.0
05/07/05
13:55
BCK
87-68-3
Isopropylbenzene�(Cumene)
ND
ug/1
1.0
05/07/05
13:55
BCK
98-82-8
p-Isopropyltoluene
ND
ug/1
1.0
05/07/05
13:55
BCK
99-87-6
Methy7erib chloride
ND
ug/l
2.0
05/07/05
13:55
BCK
75-09-2
dwlMettil -tert-butyl ether
ND
ug/l
1.0
05/07/05
13:55
BCK
1634-04-4
,Na °phthalene
ND
ug/l
1.0
05/07/05
13:55
BCK
91-20-3
n-Propylbenzene
ND
ug/l
1.0
05/07/05
13:55
BCK
103-65-1
Styrene
ND
ug/1
1.0
05/07/05
13:55
BCK
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/l
1.0
05/07/05
13:55
BCK
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/1
1.0
05/07/05
13:55
BCK
79-34-5
Tetrachloroethene
ND
ug/l
1.0
05/07/05
13:55
BCK
127-18-4
Toluene
ND
ug/l
1.0
05/07/05
13:55
BCK
108-88-3
1,2,3-Trichlorobenzene
ND
ug/l
1.0
05/07/05
13:55
BCK
87-61-6
1,2,4-Trichlorobenzene
ND
ug/l
1.0
05/07/05
13:55
BCK
120-82-1
1,1,1-Trichloroethane
ND
ug/l
1.0
05/07/05
13:55
BCK
71-55-6
1,1,2-Trichloroethane
ND
ug/1
1.0
05/07/05
13:55
BCK
79-00-5
Trichloroethene
ND
ug/l
1.0
05/07/05
13:55
BCK
79.01-6
Trichlorofluoromethane
ND
ug/1
1.0
05/07/05
13:55
BCK
75-69-4
1,2,3-Trichloropropane
ND
ug/1
1.0
05/07/05
13:55
BCK
96-18-4
1,2,4-Trimethylbenzene
ND
ug/l
1.0
05/07/05
13:55
BCK
95-63-6
1,3,5-Trimethylbenzene
ND
ug/1
1.0
05/07/05
13:55
BCK
108-67-8
Vinyl chloride
ND
ug/1
1.0
05/07/05
13:55
BCK
75-01-4
m&p-Xylene
ND
ug/l
2.0
05/07/05
13:55
BCK
o-Xylene
ND
ug/l
1.0
05/07/05
13:55
BCK
95-47-6
Toluene-d8 (S)
102
%
05/07/05
13:55
BCK
2037.26-5
4-Bromofluorobenzene (S)
99
%
05/07/05
13:55
BCK
460-00-4
Dibromofluoromethane (S)
93
%
05/07/05
13:55
BCK
1868-53-7
1,2-Dichloroethane-d4 (S)
93
%
05/07/05
13:55
BCK
17060-07-0
Date: 05/13/05
■ ■ (i'■ 'mi ' ■ 1 ' ■ 1 1 "1
Page: 16 of 55
Asheville Certification IN
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Charlotte Certification IDs
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
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NC Drinking Water
37712
NC Drinking Water
37706
SC Environmental
99030
��^^ `;'yF
Sc
99006
L NELAP
E87548
W� nct-
n'�LAP
I L I U E. /11
E87627

Lab Sample No: 925584674 Project Sample Number: 9293484-005 Date Collected: 05/03/05 12:5U
Client Sample ID: WASTE TREATMENT"SLUDGE Matrix: Water Date Received: 05/03/05 15:42
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals TCEIi Leach. Prep/Method: EPA 3010 / EPA 6010
Arsenic ND mg/1 0.025 05/05/05 19:53 ALV 7440-38-2
Barium 0.18 mg/l 0.025 05/05/05 19:53 ALV 7440-39-3
Cadmium - 0:016 mg/l 0.0050 05/05/05 19:53 ALV 7440-43-9
Chromium 0.016mg/l 0.010 05/05/05 19:53 ALV 7440 47 3
Leadb" ND mg/1 0.025 05/05/05 19:53 ALV 7439-92-1
Selenium ND mg/l 0.025 05/05/05 19:53 ALV 7782-49-2
Silver ND mg/1 0.010 05/05/05 19:53 ALV 7440 22 4
Date Digested 05/05/05 02:00 05/05/05 02:00
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Date Digested 05/04/05 06:15 05/04/05 06:15
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Mercury ND mg/1 0.00020 05/05/05 07:03 ALV 7439-97-6
P
Date: 05/13/05 age: 17 of 55
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N a oqo NC Drinking Water 37706
qy SC Environmental -99030 r Sc 99006
1 n £ FL NELAP E89.27
FL NELP.P E87648 a:_.. iSwrw -.—.__ ��,

Pace Analytical Services, Inc,
2225 Riverside Drive
�nQ H n����tC�'O
Asheville, NC 28804
Phone: [phone]
www.pacelabs.com
Fax: [phone]
Lab Project Number:
9293484
Client Project
ID:
Demolition
Samples
Lab Sample No: 925584732
Project Sample
Number: 9293484
006
Date Collected: 05/03/05 12:25
Client Sample ID: SLUDGE MGM#1 TENCORE)
Matrix: Soil
Date
Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
ByCAS
No.
Quay Reg Lmt
Wet Chemistry
Percent Moisture Method: i Moisture
Percent Moisture °`
64.6
%
05/04/05
10:49
TNS
GUMS Vol Ai l es
GC/MS UQCt 5035/8260 low level Method: EPA 8260
Acetone
530"
ug/kg
280
05/09/05
18:36
MSF
67-64 1
Benzene
ND
ug/kg
14.
05/09/05
18:36
MSF
71-43-2
Bromobenzene
NO
ug/kg
14.
05/09/05
18:36
MSF
108 86 1
Bromochloromethane
NO
ug/kg
14.
05/09/05
18:36
MSF
74 97 5
Bromodichloromethane
NO
ug/kg
14.
05/09/05
18:36
MSF
75-27-4
Bromoform
NO
ug/kg
14.
05/09/05
18:36
MSF
75-25-2
Bromomethane
ND
ug/kg
28.
05/09/05
18:36
MSF
74-83-9
2-Butanone (MEK)
NO
ug/kg
280
05/09/05
18:36
MSF
78-93-3
n-Butylbenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
104-51-8
sec-Butylbenzene
NO
ug/kg
14.
05/09/05
18:36
MSF
135-98-8
tert-Butylbenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
98-06-6
Carbon tetrachloride
ND
ug/kg
14.
05/09/05
18:36
MSF
56-23-5
Chlorobenzene
NO
ug/kg
14.
05/09/05
18:36
MSF
108-90-7
Chloroethane
ND
ug/kg
28.
05/09/05
18:36
MSF
75-00-3
Chloroform
NO
ug/kg
14.
05/09/05
18:36
MSF
67-66-3
Chloromethane
NO
ug/kg
28.
05/09/05
18:36
MSF
74-87-3
2-Chlorotoluene
NO
ug/kg
14.
05/09/05
18:36
MSF
95-49-8
4-Chlorotoluene
ND
ug/kg
14.
05/09/05
18:36
MSF
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
14.
05/09/05
18:36
MSF
96-12-8
Dibromochloromethane
NO
ug/kg
14.
05/09/05
18:36
MSF
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
14.
05/09/05
18:36
MSF
106-93-4
Dibromomethane
ND
ug/kg
14.
05/09/05
18:36
MSF
74.95.3
1,2-Dichlorobenzene
NO
ug/kg
14.
05/09/05
18:36
MSF
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
541.73.1
1,4-Dichlorobenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
106-46-7
Dichlorodifluoromethane
ND
ug/kg
28.
05/09/05
18:36
MSF
75-71-8
5,6
1,1-Dichloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
75-34.3
1,2-Dichloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
107-06-2
1,1-Dichloroethene
NO
ug/kg
14.
05/09/05
18:36
MSF
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
14.
05/09/05
18:36
MSF
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
14.
05/09/05
18:36
MSF
156-60-5
1,2-Dichloropropane
NO
ug/kg
14.
05/09/05
18:36
MSF
78-87-5
1,3-Dichloropropane
ND
ug/kg
14.
05/09/05
18:36
MSF
142-28-9
Page: 18 of 55
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report
shall not be reproduced,
except in full,
Charlotte Certification IDs
NC Wastewater 40
without the
written consent of Pace Analytical Services,
Inc.
NC Wastewater 12
a
NC Drinking Water 37706
NC Drinking Water 37712
N �oRa
Sc 99006
SC Environmental 99030
FI NIFI AP F87627
FL "dELAP E87648

Pace Analytical Services, Inc.
2225 Riverside Drive
®
Asheville, NC 28804
ace Ana lytical
Phone: [phone]
www.pacelahs.com
Fax: [phone]
Lab Sample No: 925584732
Client Sample ID: SLUDGE MGM,#lf('ENC0RE)
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-006 Date Collected: 05/03/05 12:25
Matrix: Soil Date Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2,2-Dichloropropane;=_ �
ND
ug/kg
14.
05/09/05
18:36
MSF
594-20-7
1,1-Dichloropropene.
ND
ug/kg
14.
05/09/05
18:36
MSF
563-58.6
cis-1,3-Dichloropropene
ND
ug/kg
14.
05/09/05
18:36
MSF
10061-01-5
trans-1 3 DJ6hloropropene
ND
ug/kg
14.
05/09/05
18:36
MSF
10061-02-6
Diisopropyh ether
ND
ug/kg
14.
05/09/05
18:36
MSF
108-20-3
Ethylbenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
100.41.4
Hexachloro-1,3-butadiene
ND
ug/kg
14.
05/09/05
18:36
MSF
87-68-3
Hexanone
ND
ug/kg
140
05/09/05
18:36
MSF
591.78.6
Isopropylbenzene (Cumene)
ND
ug/kg
14.
06/09/05
18:36
MSF
98 82 8
p-Isopropyltoluene
ND
ug/kg
14.
05/09/05
18:36`MSF
99 87 6
Methylene chloride
ND
ug/kg
14.
05/09/05
18:36
MSF
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
140
05/09/05
18:36
MSF
108-10.1
Methyl-tert-butyl ether
ND
ug/kg
14.
05/09/05
18:36
MSF
1634-04.4
Naphthalene
130
ug/kg
14.
05/09/05
18:36
MSF
91-20-3
n-Propylbenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
103-65.1
Styrene
ND
ug/kg
14.
05/09/05
18:36
MSF
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
79=34-5
Tetrachloroethene
ND
ug/kg
14.
05/09/05
18:36
MSF
127-18-4
Toluene
ND
ug/kg
14.
05/09/05
18:36
MSF
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
120.82-1
1,1,1-Trichloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
14.
05/09/05
18:36
MSF
79-00-5
Trichloroethene
ND
ug/kg
14.
05/09/05
18:36
MSF
79-01-6
Trichlorofluoromethane
ND
ug/kg
14.
05/09/05
18:36
MSF
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
14.
05/09/05
18:36
MSF
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
14,
05/09/05
18:36
MSF
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
14.
05/09/05
18:36
MSF
108-67-8
Vinyl acetate
ND
ug/kg
140
05/09/05
18:36
MSF
108.05.4
Vinyl chloride
ND
ug/kg
28.
05/09/05
18:36
MSF
75-01-4
Xylene (Total)
ND
ug/kg
14.
05/09/05
18:36
MSF
1330-20-7
m&p-Xylene
ND
ug/kg
28.
05/09/05
18:36
MSF
o-Xylene
ND
ug/kg
14.
05/09/05
18:36
MSF
95-47-6
Toluene-d8 (S)
78
%
05/09/05
18:36
MSF
2037-26-5 4
4-Bromofluorobenzene (S)
56
%
05/09/05
18:36
MSF
460.00-4 4
Dibromofluoromethane (S)
114
%
05/09/05
18:36
MSF
1868-53.7
1,2-Dichloroethane-d4 (S)
119
%
05/09/05
18:36
MSF
17060-07-0
Page: 19
of 55
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report
shall not be reproduced,
except in full,
Charlotte Certification IDs
NO Wastewater 40
without the
written consent
of Pace Analytical Services, Inc.
NC Wastewater
12
NO Drinking Water
37706
NO Drinking Water 37712
19"�F
Sc
99006
SC Environmental .99030
r
FL NELAP
E87627
FL NELAP E87648�:�`

Pace Analytical Services, Inc.
0 2225 Riverside Drive
e'eAnalyfical Asheville, NC 28804
Phone: [phone]
www. pacelabs.com Fax: 828,252.4618
Lab Sample No: 925584740
Client Sample ID: SLUDGE MGM
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-007 Date Collected: 05/03/05 12:45
Matrix: Soil Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Wet Chemistry
Percent Moisture V
Method:
% Moisture
Percent Moisture, �
76.0
%
05/04/0510:49
TNS
GC/MS Vol a'`1 es
GC/MS Cs 5035/8260 low level
Method:
EPA 8260
Acetone -
740
ug/kg
340
05/09/05
18:53
MSF
67-64-1
'Benzene
ND
ug/kg
17.
05/09/05
18:53
MSF
71-43-2
Bromobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
108 86 1
Bromochloromethane
ND
ug/kg
17.
05/09/05
18:53
MSF
74-97-5
Bromodichloromethane
ND
ug/kg
17.
05/09/05
18:53
MSF
75-27-4
Bromoform
ND
ug/kg
17.
05/09/05
18:53
MSF
75-25-2
Bromomethane
ND
ug/kg
34.
05/09/05
18:53
MSF
74-83-9
2-Butanone (MEK)
ND
ug/kg
340
05/09/05
18:53
MSF
78-93-3
n-Butylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
104-51-8
sec-Butylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
135-98-8
tert-Butylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
98-06-6
Carbon tetrachloride
ND
ug/kg
17.
05/09/05
18:53
MSF
56-23-5
Chlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
108-90-7
Chloroethane
ND
ug/kg
34.
05/09/05
18:53
MSF
75-00-3
Chloroform
ND
ug/kg
17.
05/09/05
18:53
MSF
67-66-3
Chloromethane
ND
ug/kg
34.
05/09/05
18:53
MSF
74-87-3
2-Chlorotoluene
ND
ug/kg
17.
05/09/05
18:53
MSF
95-49-8
4-Chlorotoluene
ND
ug/kg
17.
05/09/05
18:53
MSF
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
17.
05/09/05
18:53
MSF
96-12-8
Dibromochloromethane
ND
ug/kg
17.
05/09/05
18:53
MSF
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
17.
05/09/05
18:53
MSF
106-93-4
Dibromomethane
ND
ug/kg
17.
05/09/05
18:53
MSF
74-95.3
1,2-Dichlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
106-46-7
Dichlorodifluoromethane
ND
ug/kg
34.
05/09/05
18:53
MSF
75-71-8
1,1-Dichloroethane
ND
ug/kg
17.
05/09/05
18:53
MSF
75-34-3
1,2-Dichloroethane
ND
ug/kg
17.
05/09/05
18:53
MSF
107-06-2
1,1-Dichloroethene
ND
ug/kg
17.
05/09/05
18:53
MSF
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
17.
05/09/05
18:53
MSF
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
17.
05/09/05
18:53
MSF
156-60-5
1,2-Dichloropropane
ND
ug/kg
17.
05/09/05
18:53
MSF
78-87-5
1,3-Dichloropropane
ND
ug/kg
17.
05/09/05
18:53
MSF
142-28-9
Date: 05/13/05
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NO Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCpRo
neiac:
5,6
Page: 20 of 55
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12
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37706
SC
99006
FL 1`.1E1.AP
11:87627

Lab Sample No: 925584740
Project Sample
Number: 9293484-007
Date Collected:
05/03/05 12:45
Client Sample ID: SLUDGE MGM k, (ENCORE)
Matrix: Soil
Date Received:
05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual
RegLmt
2,2 Dichloropropane.; ``
ND
ug/kg
17.
05/09/05
18:53
MSF
594 20 7
1,1 Dichloropropene,'
ND
ug/kg
17.
05/09/05
18:53
MSF
563 58 6
cis-1,3-Dichloropropene
ND
ug/kg
17.
05/09/05
18:53
MSF
10061-01-5
trans-1 1 3 Dlchloropropene
ND
ug/kg
17.
05/09/05
18:53
MSF
10061 02 6
Diisopropyl ether
ND
ug/kg
17.
05/09/05
18:53
MSF
108 20 3
Ethylbe zene
ND
ug/kg
17.
05/09/05
18:53
MSF
100-41-4
H,exacloro-1,3-butadiene
ND
ug/kg
17.
05/09/05
18:53
MSF
87-68.3
:`2-Hexanone
ND
ug/kg
170
05/09/05
18:53
MSF
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
17.
05/09/05
18:53
MSF
98-82-8
p-Isopropyltoluene
ND
ug/kg
17.
05/09/05
18:53
MSF
99-87-6
Methylene chloride
ND
ug/kg
17.
05/09/05
18:53
MSF
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
170
05/09/05
18:53
MSF
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
17.
05/09/05
18:53
MSF
1634-04-4
Naphthalene
- 67.
ug/kg
17.
05/09/05
18:53
MSF
91-20-3
n-Propylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
103-65-1
Styrene
ND
ug/kg
17.
05/09/05
18:53
MSF
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
17.
05/09/05
18:53
NSF
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
17.
05/09/05
18:53
MSF
79-34-5
Tetrachloroethene
ND
ug/kg
17.
05/09/05
18:53
MSF
127-18-4
Toluene
ND
ug/kg
17.
05/09/05
18:53
MSF
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
120;82-1
1,1,1-Trichloroethane
ND
ug/kg
17.
05/09/05
18:53
MSF
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
17.
05/09/05
18:53
MSF
79-00-5
Trichloroethene
ND
ug/kg
17.
05/09/05
18:53
MSF
79-01-6
Trichlorofluoromethane
ND
ug/kg
17.
05/09/05
18:53
MSF
_75-69-4
1,2,3-Trichloropropane
ND
ug/kg
17.
05/09/05
18:53
MSF
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
17.
05/09/05
18:53
MSF
108-67-8
Vinyl acetate
ND
ug/kg
170
05/09/05
18:53
MSF
108-05.4
Vinyl chloride
ND
ug/kg
34.
05/09/05
18:53
MSF
75-01-4
Xylene (Total)
NO
ug/kg
17.
05/09/05
18:53
MSF
1330-20-7
m&p-Xylene
ND
ug/kg
34.
05/09/05
18:53
MSF
o-Xylene
ND
ug/kg
17.
05/09/05
18:53
MSF
95-47-6
Toluene-d8 (S)
78
%
05/09/05
18:53
MSF
2037-26-5 4
4-Bromofluorobenzene (S)
55
%
05/09/05
18:53
MSF
460-00-4 4
Dibromofluoromethane (S)
124
5.1
05/09/05
18:53
MSF
1868-53-7
1,2-Dichloroethane-d4 (S)
133
%
05/09/05
18:53
MSF
17060-07-0
Page: 21 of 55
Date: 05/13/05
;, •
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030
QQ
FL INELAP 1:8764U
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP
EQ7627

Lab Sample No: 925584757
Client Sample ID: EQUAL AERATTOOe#3 (ENCORE)
Parameters
Wet Chemistry
Percent Moisture
Percent Moistur
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-008 Date Collected: 05/03/05 12:05
Matrix: Soil Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: % Moisture
87.1 %
05/04/05 10:50 TNS
GC/MS Vol,ati1es
GC/MS VOCs75035/8260 low level
Method:
EPA 8260
AFetone
1900
ug/kg
740
05/09/05
19:11
MSF
67-64-1
-Benzene
NO
ug/kg
37.
05/09/05
19:11
MSF
71 43 2
Bromobenzene
ND
ug/kg
37.
05/09/05
19:11
MSF
108-86-1
Bromochloromethane
NO
ug/kg
37.
05/09/05
19:11
MSF
74-97-5
Bromodichloromethane
NO
-ug/kg
37.
05/09/05
19:11
MSF
75-27-4
Bromoform
NO
ug/kg
37.
05/09/05
19:11
MSF
75-25-2
Bromomethane
ND
ug/kg
74.
05/09/05
19:11
MSF
74-83-9
2'-Butanone'(MEK)
1700
ug/kg
740
05/09/05
19:11
MSF
78-93-3
n-Butylbenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
104-51-8
sec-Butylbenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
135-98-8
tert-Butylbenzene
ND
ug/kg
37.
05/09/05
19:11
MSF
98-06-6
Carbon tetrachloride
NO
ug/kg
37.
05/09/05
19:11
MSF
56-23-5
Chlorobenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
108-90-7
Chloroethane
NO
ug/kg
74.
05/09/05
19:11
MSF
75-00-3
Chloroform
NO
ug/kg
37.
05/09/05
19:11
MSF
67-66.3
Chloromethane
NO
ug/kg
74.
05/09/05
19:11
MSF
74-87-3
2-Chlorotoluene
ND
ug/kg
37.
05/09/05
19:11
MSF
95-49-8
4-Chlorotoluene
NO
ug/kg
37.
05/09/05
19:11
MSF
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/kg
37.
05/09/05
19:11
MSF
96-12-8
Dibromochloromethane
NO
ug/kg
37.
05/09/05
19:11
MSF
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
37.
05/09/05
19:11
MSF
106-93-4
Dibromomethane
NO
ug/kg
37.
05/09/05
19:11
MSF
74-95-3
1,2-Dichlorobenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
37.
05/09/05
19:11
MSF
541-73-1
1,4-Dichlorobenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
106-46-7
Dichlorodifluoromethane
ND
ug/kg
74.
05/09/05
19:11
MSF
75-71-8 5,6
1,1-Dichloroethane
ND
ug/kg
37.
05/09/05
19:11
MSF
75-34-3
1,2-Dichloroethane
_ NO
ug/kg
37.
05/09/05
19:11
MSF
107-06-2
1,1-Dichloroethene
NO
ug/kg
37.
05/09/05
19:11
MSF
75-35-4
cis-1,2-Dichloroethene
NO
ug/kg
37.
05/09/05
19:11
MSF
156-59-2
trans-1,2-Dichloroethene
NO
ug/kg
37.
05/09/05
19:11
MSF
156-60-5
1,2-Dichloropropane
ND
ug/kg
37.
05/09/05
19:11
MSF
78-87-5
1,3-Dichloropropane
ND
ug/kg
37.
05/09/05
19:11
MSF
142-28-9
Date: 05/13/05
nny
Page: 22 of 55
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NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
b A o9p
NC Drinking Water
37706
99006
SC Environmental
99030
°�'
Sc
FL JUL MI
E87648
= ac
__
FI NFI AP
E87621

Cr H,1 fi�a'o
ac Ana
www.pacelabs.cnm
Lab Project Number:
Client Project ID:
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax:[phone]
9293484
Demolition Samples
Lab Sample No: 925584757
Project Sample
Number: 9293484
008
Date Collected: 05/03/05 12:05
Client Sample ID: EQUAL-AERAT.ION,.`#3
(ENCORE)
Matrix: Soil
Date Received: 05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2,2-Dichloropropane , °
NO
ug/kg
37.
05/09/05
19:11
MSF
594 20 7
1,1-Dichloropropenew'
NO
ug/kg
37.
05/09/05
19:11
MSF
563 58 6
cis-1,3-Dichlo.r6propene
NO
ug/kg
37.
05/09/05
19:11
MSF
10061-01-5
trans-1 3 D,cfnToropropene
ND
ug/kg
37.
05/09/05
19:11
MSF
10061-02-6
Diisop ropyl ether
NO
ug/kg
37.
05/09/05
19:11
MSF
108 20 3
,
Ethyl benzene
NO
ug/kg
37.
05/09/05
19:11
MSF
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
37.
05/09/05
19:11
MSF
87-68-3
2'=Hexanone
NO
ug/kg
370
05/09/05
19:11
MSF
591 78 6
Isopropylbenzene (Cumene)
ND
ug/kg
37.
05/09/05
19:11
MSF
98 82 8
p-Isopropyltoluene
NO
ug/kg
37.
05/09/05
19:11
MSF
99-87-6
Methylene chloride
ND
ug/kg
37.
05/09/05
19:11
MSF
75-09-2
4-Methyl-2-pentanone (MIBK)
NO
ug/kg
370
05/09/05
19:11
MSF
108-10-1
Methyl-tert-butyl ether
NO
ug/kg
37.
05/09/05
19:11
MSF
1634-04-4
Naphthalene =
60.
ug/kg
37.
05/09/05
19:11
MSF
91.20-3
n-Propylbenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
103-65-1
Styrene
NO
ug/kg
37.
05/09/05
19:11
MSF
100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/kg
37.
05/09/05
19:11
MSF
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
37.
05/09/05
19:11
MSF
79-34-5
Tetrachloroethene
ND
ug/kg
37.
05/09/05
19:11
MSF
127-18.4
Toluene
NO
ug/kg
37.
05/09/05
19:11
MSF
108-88-3
1,2,3-Trichlorobenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
37.
05/09/05
19:11
MSF
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
37.
05/09/05
19:11
MSF
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
37.
05/09/05
19:11
MSF
79-00.5
Trichloroethene
NO
ug/kg
37.
05/09/05
19:11
MSF
79-01-6
Trichlorofluoromethane
ND
ug/kg
37.
05/09/05
19:11
MSF
75-69-4
1,2,3-Trichloropropane_
NO
ug/kg
37.
05/09/05
19:11
MSF
96-18-4
1,2,4-Trimethylbenzene
NO
ug/kg
37.
05/09/05
19:11
MSF
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
37.
05/09/05
19:11
MSF
108-67-8
Vinyl acetate
NO
ug/kg
370
05/09/05
19:11
MSF
108-05-4
Vinyl chloride
ND
ug/kg
74.
05/09/05
19:11
MSF
75-01-4
Xylene (Total)
NO
ug/kg
37.
05/09/05
19:11
MSF
1330-20-7
m&p-Xylene
NO
ug/kg
74.
05/09/05
19:11
MSF
o-Xylene
ND
ug/kg
37.
05/09/05
19:11
MSF
95-47-6
Toluene-d8 (S)
83
i
05/09/05
19:11
MSF
2037-26-5
4-Bromofluorobenzene (S)
60
i
05/09/05
19:11
MSF
460-00-4 4
Dibromofluoromethane (S)
112
i
05/09/05
19:11
MSF
1868-53-7
1,2-Dichloroethane-d4 (S)
114
05/09/05
19:11
MSF
17060-07-0
Date: 05/13/05
Asheville Certification IDS
NO Wastewater
40
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37712
SC Environmental
99030
FL NELAP
E87648
Page: 23 of 55
REPORT OF LR ATOP ANALYSIS
This report shall not be reproduced, except in full,
Charlotte Certification IDs
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
a
NC Drinking Water
37706
H oRo
SC
99006
FI "IF AP
FR7S:7

Lab Sample No: 925584765
Client Sample ID: EQUAL-AER
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax. [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Project Sample Number: 9293484-009 Date Collected: 05/03/05 11:5U
(ENCORE) Matrix: Soil Date Received: 05/03/05 15:42
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Wet Chemistry
Percent Moisture
Method: Method:
i Moisture
Percent Moist
83.2
%
05/04/05
10:50
TNS
GC/MS Vol at 1 es
GC/MS=UOCs 5035/8260 low level
Method:
EPA 8260
Acetone
980
ug/kg
570
05/09/05
19:28
MSF
67-64-1
-Benzene
NO
ug/kg
28.
05/09/05
19:28
MSF
71-43-2
Bromobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
108 86 1
Bromochloromethane
NO
ug/kg
28,
05/09/05
19:28
MSF
74 97 5
Bromodichloromethane
NO
ug/kg
28.
05/09/05
19:28
MSF
75-27-4
Bromoform
NO
ug/kg
28.
05/09/05
19:28
MSF
75-25-2
Bromomethane
NO
ug/kg
57.
05/09/05
19:28
MSF
74-83-9
2-Butanone (MEK)
NO
ug/kg
570
05/09/05
19:28
MSF
78-93-3
n-Butylbenzene
ND
ug/kg
28.
05/09/05
19:28
MSF
104-51-8
sec-Butylbenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
135-98-8
tert-Butylbenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
98-06.6
Carbon tetrachloride
NO
ug/kg
28,
05/09/05
19:28
MSF
56-23-5
Chlorobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
108-90-7
Chloroethane
NO
ug/kg
57.
05/09/05
19:28
MSF
75-00-3
Chloroform
NO
ug/kg
28.
05/09/05
19:28
MSF
67-66.3
Chloromethane
NO
ug/kg
57.
05/09/05
19:28
MSF
74-87-3
2-Chlorotoluene
NO
ug/kg
28.
05/09/05
19:28
MSF
95-49-8
4-Chlorotoluene
NO
ug/kg
28.
05/09/05
19:28
MSF
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/kg
28.
05/09/05
19:28
MSF
96-12-8
Dibromochloromethane
ND
ug/kg
28.
05/09/05
19:28
MSF
124-48-1
1,2-Dibromoethane (EDB)
NO
ug/kg
28.
05/09/05
19:28
MSF
106-93-4
Dibromomethane
NO
ug/kg
28.
05/09/05
19:28
MSF
74-95-3
1,2-Dichlorobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
95-50-1
1,3-Dichlorobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
541-73-1
1.4-Dichlorobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
106-46-7
Dichlorodifluoromethane
NO
ug/kg
57.
05/09/05
19:28
MSF
75-71-8 5,6
1,1-Dichloroethane
ND
ug/kg
28.
05/09/05
19:28
MSF
75-34-3
1,2-Dichloroethane
NO
ug/kg
28.
05/09/05
19:28
MSF
107-06-2
1,1-Dichloroethene
NO
ug/kg
28.
05/09/05
19:28
MSF
75-35-4
cis-1,2-Dichloroethene
NO
ug/kg
28.
05/09/05
19:28
MSF
156-59-2
trans-1,2-Dichloroethene
NO
ug/kg
28.
05/09/05
19:28
MSF
156-60-5
1,2-Dichloropropane
NO
ug/kg
28.
05/09/05
19:28
MSF
78-87-5
1,3-Dichloropropane
NO
ug/kg
28.
05/09/05
19:28
MSF
142-28-9
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
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Lab Sample No: 925584765
Project Sample
Number: 9293484.009
Date Collected:
05/03/05 11:50
Client Sample ID: EQUAL AERATION'#4
(ENCORE)
Matrix: Soil
Date Received:
05/03/05 15:42
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual
RegLmt
2,2-Dich1oropropane.
NO
ug/kg
28.
05/09/05
19:28
MSF
594.20-7
1,1-Dichloropropene ��
NO
ug/kg
28.
05/09/05
19:28
MSF
563 58 6
cis-1,3-Dichl&6*bpene
ND
ug/kg
28.
05/09/05
19:28
MSF
10061-01-5
trans-1 3 D1�6'hloropropene
ND
ug/kg
28.
05/09/05
19:28
MSF
10061-02-6
Diisoprop�, ether
NO
ug/kg
28.
05/09/05
19:28
MSF
108-20-3
Ethylb h2ene
NO
ug/kg
28,
05/09/05
19:28
MSF
100 41 4
Hexaehloro-1,3-butadiene
NO
ug/kg
28.
05/09/05
19:28
MSF
87-68-3
2�Hexanone
ND
ug/kg
280
05/09/05
19:28
MSF
591-78-6
Isopropylbenzene (Cumene)
NO
ug/kg
28.
05/09/05
19:28
MSF
98-82-8
p-Isopropyltoluene
NO
ug/kg
28.
05/09/05
19:28
MSF
99-87-6
Methylene chloride
NO
ug/kg
28.
05/09/05
19:28
MSF
75-09-2
4-Methyl-2-pentanone (MIRK)
NO
ug/kg
280
05/09/05
19:28
MSF
108-10-1
Methyl-tert-butyl ether
NO
ug/kg
28.
05/09/05
19:28
MSF
1634-04.4
Naphthalene'"
45.`
ug/kg
28.
05/09/05
19:28
MSF
91-20-3
n-Propylbenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
103-65-1
Styrene
NO
ug/kg
28.
05/09/05
19:28
MSF
10.0-42.5
1,1,1,2-Tetrachloroethane
NO
ug/kg
28.
05/09/05
19:28
MSF
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
28.
05/09/05
19:28
MSF
79-34-5
Tetrachloroethene
NO
ug/kg
28.
05/09/05
19:28
MSF
127-18-4
Toluene
NO
ug/kg
28.
05/09/05
19:28
MSF
108-88-3
1,2;3-Trichlorobenzene
33.
ug/kg
28.
05/09/05
19:28
MSF
87-61-6
1,2,4-Trichlorobenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
120-82-1
1,1,1-Trichloroethane
NO
ug/kg
28.
05/09/05
19:28
MSF
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
28.
05/09/05
19:28
MSF
79-00-5
Trichloroethene
ND
ug/kg
28.
05/09/05
19:28
MSF
79-01-6
Trichlorofluoromethane
NO
ug/kg
28.
05/09/05
19:28
MSF;
75-69-4
1,2,3-Trichloropropane
NO
ug/kg
28.
05/09/05
19:28
MSF
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
28.
05/09/05
19:28
MSF
95-63-6
1,3,5-Trimethylbenzene
NO
ug/kg
28.
05/09/05
19:28
MSF
108-67-8
Vinyl acetate
NO
ug/kg
280
05/09/05
19:28
MSF
108-05-4
Vinyl chloride
NO
ug/kg
57.
05/09/05
19:28
MSF
75-01-4
Xylene (Total)
ND
ug/kg
28.
05/09/05
19:28
MSF
1330-20.7
m&p-Xylene
NO
ug/kg
57.
05/09/05
19:28
MSF
o-Xylene
NO
ug/kg
28.
05/09/05
19:28
MSF
95-47-6
Toluene-d8 (S)
84
%
05/09/05
19:28
MSF
2037-26-5
4-Bromofluorobenzene (S)
64
%
05/09/05
19:28
MSF-
460-00-4 4
Dibromofluoromethane (S)
101
%
05/09/05
19:28
MSF
1868-53-7
1,2-Dichloroethane-d4 (S)
109
%
05/09/05
19:28
MSF
17060-07-0
Date: 05/13/05
Page: 25 of 55
REPORT OF LABORATORY ANALYSES
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NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
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FL NELAP E87648 'E1en t
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NC Wastewater 12
NC Drinking Water 37706
Sc 99006
F-i NFi AP F°7527

PARAMETER FOOTNOTES
Inorganic We C}emistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method 071E modified to use ASE.
Al.l pH, free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended,immediate
time.
ND Not detected at or above adjusted reporting limit
ANC Not Calculable
,l Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
[11 The sample extract could not be concentrated to the normal final volume. This resulted in an elevated
reporting limit."
[21 The sample was diluted to reduce matrix interference, resulting in elevated reporting limits.
[31 Base/neutral surrogate recovery outside of control limits. The data was accepted based on valid recovery of
remaining two base/neutral surrogates.
[41 The surrogate recovery was outside QC acceptance limits due to matrix interference.
151 Insufficient sample available for re -analysis.
[61 Results for this sample may be biased high due to matrix interference.
P
Date: 05/13/05 age: 26 of 55
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NO Wastewater
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without the written consent of Pace Analytical Services, Inc.
NO Wastewater
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37712
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37706
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99030
�� 9"
'
SC
99006
FL hvELAID
E87648
`/� £
el^
e' V.�Y/i
FL nin n o
VLL II
E87627

Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
aceAnalytlCal° Phone:828.254J176
www.pacelads.com QUALITY CONTROL DATA Fax:[phone]
QC Batch: 127415
QC Batch Method: EPA 35
Associated Lab Samples;'.
Lab Project Number: 9293484
Client Project ID: Demolition Samples
Analysis Method: EPA 8270
Analysis Description: Semivolatile Organics
925584633 925584641
METHOD BLANK:::=925593345
Associated Lab Samples: 925584633
925584641
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
°"Acenaphthene
ug/1
ND
10.
Acenaphthylene
ug/l
NO
10.
Aniline
ug/l
NO
10.
Anthracene
ug/l
NO
10.
Benzo(k)fluoranthene
ug/l
NO
10.
Benzo(b)fluoranthene
ug/l
NO
10.
Benzo(a)anthracene
ug/l
NO
10.
Benzoic acid
ug/1
NO
50..
Benzo(g,h,i)perylene
ug/l
NO
10.
Benzyl alcohol
ug/l
NO
20.
Benzo(a)pyrene
ug/l
NO
10.
Biphenyl (Diphenyl)
ug/l
NO
10.
4-Bromophenylphenyl ether
ug/l
NO
10.
Butylbenzylphthalate
ug/l
ND
10.
4-Chloro-3-methylphenol
ug/l
NO
20.
4-Chloroaniline
ug/l
NO
20.
bis(2-Chloroethoxy)methane
ug/1
ND
10.
bis(2-Chloroethyl) ether
ug/l
NO
10.
bis(2-Chloroisopropyl) ether
ug/1
NO
10.
2-Chloronaphthalene
ug/l
NO
10.
2-Chlorophenol
ug/l
NO
10.
4-Chlorophenylphenyl ether
ug/l
ND
10.
Chrysene -
ug/1
NO
10.
Dibenz(a,h)anthracene
ug/l
NO
10.
Dibenzofuran
ug/l
ND
10.
1,2-Dichlorobenzene
ug/l
ND
10.
1,3-Dichlorobenzene
ug/l
NO
10.
1,4-Dichlorobenzene
ug/1
NO
10.
3,3'-Dichlorobenzidine
ug/l
NO
20.
2,4-Dichlorophenol
ug/l
ND
10.
Diethylphthalate
ug/l
ND
10.
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
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NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
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37712
s a u. oqy
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99030
F
FL NELAP
E87648
act -
Page: 27 of 55
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METHOD BLANK: 925593345
Associated Lab Samples
925584633
925584641
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
2,4-DimethylphOno �
ug/-1
NO
10.
Di methyl phthalate
ug/l
NO
10.
Din butylphthalate
ug/l
NO
10.
4 6„tro-2-methylphenol
ug/l
ND
50.
�,2.,4-Din1trophenoi
ug/l
NO
50.
2,4-Dinitrotoluene
ug/l
NO
10.
_ 2,6-Dinitrotoluene
ug/l
NO
10.
Di-n-octylphthalate
ug/l
NO
10.
1,2-Diphenylhydrazine
ug/l
NO
20.
bis(2-Ethylhexyl)phthalate
ug/l
NO
10.
Fluoranthene
ug/l
ND
10.
Fluorene
ug/l
NO
10.
Hexachloro-1,3-butadiene
ug/l
NO
10.
Hexachlorobenzene
ug/l
ND
10.
Hexachlorocyclopentadiene
ug/l
ND
10.
Hexachloroethane
ug/l
NO
10.
Indeno(1,2,3-cd)pyrene
ug/l
NO
10.
Isophorone
ug/l
NO
10.
2-Methylnaphthalene
ug/l
NO
10.
2-Methylphenol (o-Cresol)
ug/l
NO
10.
3&4-Methylphenol
ug/l
NO
10.
Naphthalene
ug/l
NO
10.
2-Nitroaniline
ug/l
ND
50.
3-Nitroaniline
ug/l
ND
50.
4-Nitroaniline
ug/l
NO
50.
Nitrobenzene
ug/l
NO
10.
2-Nitrophenol
ug/l
ND
10.
4-Nitrophenol
ug/l
NO
50.
N-Nitrosodipethylamine
ug/l
NO
10.
N-Nitroso-di-n-propylamine
ug/l
NO
10.
N-Nitrosodiphenylamine
ug/l
ND
10.
Pentachlorophenol
ug/l
ND
50.
Phenanthrene
ug/l
NO
10.
Phenol
ug/l
ND
10.
Pyrene
ug/l
NO
10.
1,2,4-Trichlorobenzene
ug/l
NO
10.
Date: 05/13/05
Page: 28 of 55
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NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N.A� oRo
NC Drinking Water
37706
99006
SC Environmental
99030
�`�` \.9�
SC
FL NELAD
E87648
, �Pa� £
■ ■ `e:-�
FL NELAP
E87527

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
METHOD BLANK: 925593345
Associated Lab Samples 925584633 925584641
Blank Reporting
Parameter Units Result Limit Footnotes
2,4,5-Trichlq*enol
ug/l
ND 50.
2,4,6-Trichlorophenol
ug/1
ND 10.
Nitrobenzene-6 (S)
i
65
2 Fluorobiphenyl (S)
%
58
Terphenyl-d14 (S)
%
74
Phenol-d5 (S)
i
30
2-Fluorophenol (S)
i
42
2 4 6-Tribromophenol (S)
i
73
LABORATORY CONTROL SAMPLE: 925593352
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Acenaphthene
ug/l
50.00
27.06
54
Acenaphthylene
ug/l
50.00
27.09
54
Aniline
ug/l
50.00
24.33
49
Anthracene
ug/l
50.00
30.77
62
Benzo(k)fluoranthene
ug/l
50.00
27.31
55
Benzo(b)fluoranthene
ug/1
50.00
29.81
60
Benzo(a)anthracene
ug/l
50.00
29.71
59
Benzoic acid
ug/l
50.00
12.57
25
Benzo(g,h,i)perylene
ug/l
50.00
26.35
53
Benzyl alcohol
ug/1
50.00
16.00
32
Benzo(a)pyrene
ug/l
50.00
28.58
57
4-Bromophenylphenyl ether
ug/l
50.00
30.31
61
Butylbenzylphthalate
ug/l
50.00
29.93
60
4-Chloro-3-methylphenol
ug/l
50.00
32.05
64
4-Chloroaniline
ug/l
50.00
17.22
34
bis(2-Chloroethoxy)methane
ug/l
50.00
26.40
53
bis(2-Chloroethyl) ether
ug/l
50.00
21.32
43
bis(2-Chloroisopropyl) ether
ug/l
50.00
23.81
48
2-Chloronaphthalene
ug/l
50.00
25.78
52
2-Chlorophenol
ug/l
50.00
19.96
40
4-Chlorophenylphenyl ether
ug/l
50.00
29.07
58
Chrysene
ug/l
50.00
28.68
57
Date: 05/13/05
Page: 29 of 55
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37712
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37706
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99030
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E87648
��� f
Fi iu 'ri i+P
P8707

Lab Project Number: 9293484
Client Project ID: Demolition Samples
LABORATORY CONTROL SAMPLE 925593352
Spike
LCS
LCS
Parameter
Units
Conc.
Result
i Rec
footnotes
Dibenz(a,h)anthra`cene
ug/l
50.00
26.56
53
Dibenzofuran
ug/l
50.00
28.43
57
1,2-Dichlorabenzene
ug/l
50.00
17.35
35
1 3- DI, ehl°orobenzene
ug/1
50.00
16.62
33
1 4,Dichlorobenzene
ug/l
50.00
17.33
35
3 3' Di chl orobenzi di ne
ug/l
100.00
15.82
16
1
2,4-Dichlorophenol
ug/l
50.00
26.19
52
Diethylphthalate
ug/l
50.00
30.63
61
2,4-Dimethylphenol
ug/l
50.00
27.56
55
Dimethylphthalate
ug/l
50.00
30.19
60
Di-n-butylphthalate
ug/1
50.00
29.93
60
4,6-Dinitro-2-methylphenol
ug/l
50.00
27.37
55
2,4-Dinitrophenol
ug/l
50.00
21.90
44
2,4-Dinitrotoluene
ug/l
50.00
30.19
60
2,6-Dinitrotoluene
ug/1
50.00
30.32
61
Di-n-octylphthalate
ug/l
50.00
29.89
60
1,2-Diphenylhydrazine
ug/l
50.00
28.43
57
bis(2-Ethylhexyl)phthalate
ug/l
50.00
30.11
60
Fluoranthene
ug/l
50.00
28.56
57
Fluorene
ug/l
50.00
28.46
57
Hexachloro-1,3-butadiene
ug/l
50.00
19.12
38
Hexachlorobenzene
ug/l
50.00
30.37
61
Hexachlorocyclopentadiene
ug/l
50.00
15.09
30
Hexachloroethane
ug/l
50.00
18.02
36
Indeno(1,2,3-cd)pyrene
ug/l
50.00
26.48
53
Isophorone
ug/1
50.00
32.50
65
2-Methylnaphthalene
ug/l
50.00
25.11
50
2-Methylphenol (o-Cresol)
ug/l
50.00
22.24
44
3&4-Methylphenol
ug/l
50.00
22.58
45
Naphthalene
ug/l
50.00
20.69
41
2-Nitroaniline
ug/l
50.00
25.68
51
3-Nitroaniline
ug/l
50.00
27.18
54
4-Nitroaniline
ug/1
50.00
32.04
64
Nitrobenzene
ug/l
50.00
23.92
48
2-Nitrophenol
ug/l
50.00
22.82
46
4-Nitrophenol
ug/l
50.00
6.096
12
N-Nitrosodimethylamine
ug/l
50.00
13.96
28
Date: 05/13/05
Page: 30 of 55
AEPORT OF
LABORATORY I 1 ti
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NC Wastewater
40
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NC Wastewater
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NC Drinking Water
37712
N a oRo
NC Drinking Water
37706
SC Environmental
99030
a F
W
SC
99006
FL NELAP
E87648
'£
■ve vtt
A NFL
E87627

®
l��i /'l� I y lr
ace /� ai tica'
www.pacelabs.cnm
QUALITY
CONTROL
DATA
Lab Project Number:
Client Project ID:
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax. [phone]
9293484
Demolition Samples
LABORATORY CONTROL SAMPLE 92593352
Spike
LCS
LCS
.,
Parameter' Units
Conc.
Result
iRec
Footnotes
N-Nitroso-di-n-propylamine ug/l
50.00
29.76
60
N-Nitrosodlphe ylamine ug/l
50.00
33.21
66
Pentachlorophenol ug/l
50.00
30.05
60
Phenanthrene ug/l
50.00
29.72
59
Phenol '�ug/l
50.00
10.23
20
y' rene ug/l
"1,2,4-Trichlorobenzene
50.00
30.82
62
ug/l
50.00
19.78
40
2,4.5-Trichlorophenol ug/l
50.00
29.89
60
2,4,6-Trichlorophenol ug/l
50.00
30.24
60
Nitrobenzene-d5 (S)
48
2-Fluorobiphenyl (S)
55
Terphenyl-d14 (S)
68
Phenol-d5 (S)
21
2-Fluorophenol (S)
28
2,4,6-Tribromophenol (S)
74
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
925593378 925593386
925586844
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec i
Rec
RPD Footnotes
4-Chloro-3-methylphenol
ug/l
0
100.00
62.85
62.01
63
62
1'
2-Chlorophenol
ug/l
0
100.00
41.37
46.84
41
47
12
4-Nitrophenol
ug/l
0
100.00
13.58
13.73
14
14
1
Pentachlorophenol
ug/l
0
100.00
50.10
61.45
50
62
20
Phenol
ug/l
0
100.00
21.44
24.21
21
24
12
Phenol-d5 (S)
20
24
2-Fluorophenol (S)
29
33
2,4,6-Tribromophenol (S)
58
70
SAMPLE DUPLICATE: 925593360
925586828 DUP
Parameter Units Result Result RPD Footnotes
Pentachlorophenol ug/1 NO ND NC
Phenol-d5 (S) Y. 16 16
Date: 05/13/05 Page: 31 of 55
AEPORT
I LABORATORY
. ) . ) . 1 5
.
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without the written consent of Pace Analytical Services, Inc.
NC Wastewater
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NC Drinking Water
37712
a
NC Drinking Water
37706
SC Environmental
99030
Sc
99006
FL NEL AP
E87648
a ::��C��'=
FI NFI AP
F87 27

Date: 05/13/05
Page:
32 of 55
REPORT OF LABORATORY ANALYSIS
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IN
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NC Wastewater
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NC Drinking Water
37712
a N A� o9a
NC Drinking Water
37706
SC Environmental
99030
'' i qy
¢
SC
99006
GL NELAP
E87648
�'1i�la�°'
■olCli`__
FI P�PI AP
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LUfU f

Lab Project Number: 9293484
Client Project ID: Demolition Samples
QC Batch: 127648 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: Semivolatile Organics
925584591 925584609
Associated Lab Sampled
METHOD BLANK.r.`925606741
Associated -dab Samples:
925584591
925584609
Blank
Reporting
..Parameter
Units
Result
Limit Footnotes
o 'Acenaphthene
ug/l
NO
10.
Acenaphthylene
ug/l
NO
10.
Aniline
ug/l
ND
10.
Anthracene
ug/l
NO
10.
Benzo(k)fluoranthene
ug/l
NO
10.
Benzo(b)fluoranthene
ug/l
NO
10.
Benzo(a)anthracene
ug/l
ND
10.
Benzoic acid
ug/l
NO
50.
Benzo(g,h,i)perylene
ug/l
ND
10.
Benzyl alcohol
ug/l
NO
20.
Benzo(a)pyrene
ug/l
ND
10.
4-Bromophenylphenyl ether
ug/l
ND
10.
Butylbenzylphthalate
ug/l
ND
10.
4-Chloro-3-methylphenol
ug/l
NO
20.
4-Chloroaniline
ug/l
ND
20.
bis(2-Chloroethoxy)methane
ug/l
NO
10.
bis(2-Chloroethyl) ether
ug/l
NO
10.
bis(2-Chloroisopropyl) ether
ug/l
NO
10.
2-Chloronaphthalene
ug/l
NO
10.
2-Chlorophenol
ug/l
NO
10.
4-Chlorophenylphenyl ether
ug/l
ND
10.
Chrysene
ug/1
NO
10.
Dibenz(a,h)anthracene
ug/l
ND
10.
Dibenzofuran
ug/l
ND
10.
1,2-Dichlorobenzene
ug/l
ND
10.
1,3-Dichlorobenzene
ug/l
ND
10.
1,4-Dichlorobenzene
ug/l
ND
10.
3,3'-Dichlorobenzidine
ug/l
ND
20.
2,4-Dichlorophenol
ug/l
ND
10.
Diethylphthalate
ug/l
NO
10.
2,4-Dimethylphenol
ug/l
NO
10.
Date: 05/13/05 Page: 33 of 55
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37712
N A o9p
NC Drinking Water
37706
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_99030
0
Sc
99006
FL NELAP
EnV'7648
.. 0 ■ lac ;'
FI "IF1 An
F07G2-t7

laceAnalyfical °
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828,252.4618
Lab Project Number: 9293484
Client Project ID: Demolition Samples
METHOD BLANK: 925606741
Associated Lab Sample
925584591
925584609
Blank
Reporting
Parameter ..0
Units
Result
Limit Footnotes
Di methyl phthalate
ug/l
NO
10.
Di-n-butylphthalate
ug/l
NO
10.
4,6-Din tro 2-methylphenol
ug/l
NO
50.
2 4 0-161trophenol
ug/l
NO
50.
2 4�-Dinitrotoluene
ug/l
NO
10.
2,6-Dinitrotoluene
ug/l
NO
10.
Di-n-octylphthalate
ug/l
NO
10.
1,2-Diphenylhydrazine
ug/l
NO
20.
bis(2-Ethylhexyl)phthalate
ug/l
ND
10.
Fluoranthene
ug/l
NO
10.
Fluorene
ug/l
NO
10.
Hexachloro-1,3-butadiene
ug/l
NO
10.
Hexachlorobenzene
ug/l
NO
10.
Hexachlorocyclopentadiene
ug/l
NO
10.
Hexachloroethane
ug/l
ND
10.
Indeno(1,2,3-cd)pyrene
ug/l
NO
10.
Isophorone
ug/l
ND
10.
2-Methylnaphthalene
ug/l
ND
10.
2-Methylphenol (o-Cresol)
ug/l
NO
10.
3&4-Methylphenol
ug/l
NO
10.
Naphthalene
ug/l
ND
10.
2-Nitroaniline
ug/l
NO
50.
3-Nitroaniline
ug/l
NO
50.
4-Nitroaniline
ug/l
NO
50.
Nitrobenzene
ug/l
NO
10.
2-Nitrophenol
ug/l
ND
i0.
4-Nitrophenol
ug/l
NO
50.
N-Nitrosodimethylamine
ug/l
ND
10.
N-Nitroso-di-n-propylamine
ug/l
ND
10.
N-Nitrosodiphenylamine ,
ug/l
NO
10.
Pentachlorophenol
ug/l
NO
50.
Phenanthrene
ug/l
NO
10.
Phenol
ug/l
NO
10.
Pyrene
ug/l
ND
10.
1,2,4-Trichlorobenzene
ug/l
NO
10.
2,4,5-Trichlorophenol
ug/l
NO
50.
Date: 05/13/05
Page: 34 of 55
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without the written consent of Pace Analytical Services, Inc.
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NC Drinking Water
37712
N_A� oRo
NC Drinking Water
37706
SC Environmental
99030
'' qy
Sc
99006
FI nin no
L NIE1 11
[o n4
L876YV
{1�F(/''� (/��
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[ In n
I L NLLM
ER76L7

METHOD BLANK: 925606741
Associated Lab Samples,,:
2,4,6-Trichlor6phenol
Nitrobenzene-8(S)
2-Fluorob�phenyl (S)
Terphenyl-d14 (S)
Ph- nol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
84591 925584609
Blank
Units
Result
ug/l
ND
29
30
50
12
18
43
LABORATORY CONTROL SAMPLE & LCSD: 925606758 925606766
Reporting
Limit Footnotes
10.
Spike
LCS
LCSD
LCS
LCSD
Parameter
Units
Conc.
Result
Result
Y. Rec
% Rec
RPD Footnotes
Acenaphthene
ug/l
50.00
25.88
21.76
52
44
17
Acenaphthylene
ug/l
50.00
26.29
21.45
53
43
20
Aniline
ug/l
50.00
28.23
27.90
56
56
1
Anthracene
ug/l
50.00
29.12
22.84
58
46
24
Benzo(k)fluoranthene
ug/l
50.00
30.14
21.91
60
44
32 2
Benzo(b)fluoranthene
ug/l
50.00
27.71
21.50
55
43
25
Benzo(a)anthracene
ug/l
50.00
29.66
22.38
59
45
28
Benzoic acid
ug/l
50.00
12.28
10.61
25
21
15
Benzo(g,h,i)perylene
ug/l
50.00
22.14
17.65
44
35
23
Benzyl alcohol
ug/l
50.00
24.54
22.82
49
46
7
Benzo(a)pyrene
ug/l
50.00
28.50
21.56
57
43
28
4-Bromophenylphenyl. ether
ug/l
50.00
28.44
22.69
57
45
22
Butylbenzylphthalate
ug/l
50.00
30.67
22.72
61
45
30
4-Chloro-3-methylphenol
ug/l
50.00
32.78
27.82
66
56
16
4-Chloroaniline
ug/l
50.00
26.17
23.10
52
46
12
bis(2-Chloroethoxy)methane
ug/l
50.00
25.30
21.55
51
43
16
bis(2-Chloroethyl) ether
ug/l
50.00
19.26
19.27
38
38
0
bis(2-Chloroisopropyl) ether
ug/l
50.00
22.18
22.16
44
44
0
2-Chloronaphthalene
ug/l
50.00
23.72
20.03
47
40
17
2-Chlorophenol
ug/l
50.00
18.55
18.68
37
37
1
4-Chlorophenylphenyl ether
ug/l
50.00
28.85
23.01
58
46
23
Chrysene
ug/l
50.00
28.95
21.63
58
43
29
Dibenz(a,h)anthracene
ug/l
50.00
23.78
18.78
48
38
23
Date: 05/13/05
3' ' ' J ' 1 ' ' ' 1t I I' 1 1ti
Page: 35 of 55
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NC Wastewater
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without the written consent of Pace Analytical Services, Inc.
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NC Drinking Water
37712
NC Drinking Water
37706
SC Environmental
99030
of -�
Sc
99006
FL NELAP
E87648
9 :�.°:��.
FL NFL AP
E87627

Lab Project Number: 9293484
Client Project ID: Demolition Samples
LABORATORY CONTROL SAMPLE &sCCSD: 925606758 925606766
Spike
LCS
LCSD
LCS
LCSD
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
RPD Footnotes
Dibenzofuran
ug/l
50.00
27.48
22.65
55
45
19
1,2-Dichlor0benzene
ug/l
50.00
15.20
15.71
30
31
3
1,3-Dichl_orobenzene
ug/l
50.00
14.72
15.37
29
31
4
1,4-Dichl6robenzene
ug/l
50.00
14.78
15.72
30
31
6
3 3�hlorobenzidine
ug/l
100.00
24.22
19.96
24
20
19
2 4=Dichlorophenol
ug/l
50.00
25.69
21.35
51
43
18
�`Diethylphthalate
ug/l
50.00
30.76
23.37
62
47
27
2,4-Dimethylphenol
ug/l
50.00
28.59
25.26
57
50
12
Dimethylphthalate
ug/l
50.00
29.34
23.14
59
46
24
Di-n-butylphthalate
ug/l
50.00
30.25
22.66
60
45
29
4,6-Dinitro-2-methylphenol
ug/l
50.00
24.20
19.67
48
39
21
2,4-Dinitrophenol
ug/l
50.00
21.96
16.31
44
33
30
2,4-Dinitrotoluene
ug/l
50.00
30.89
23.24
62
46
28
2,6-Dinitrotoluene
ug/l
50.00
29.76
23.56
60
47
23
Di-n-octylphthalate
ug/l
50.00
29.80
22.64
60
45
27
1,2-Diphenylhydrazine
ug/l
50.00
26.14
22.06
52
44
17
bis(2-Ethylhexyl)phthalate
ug/l
50.00
57.81
49.85
116
100
15
Fluoranthene
ug/l
50.00
28.17
21.67
56
43
26
Fluorene
ug/l
50.00
27.77
22.41
56
45
21
Hexachloro-1,3-butadiene
ug/l
50.00
17.39
17.28
35
35
1
Hexachlorobenzene
ug/l
50.00
28.87
22.52
58
45
25
Hexachlorocyclopentadiene
ug/l
50.00
13.71
13.69
27
27
0
Hexachloroethane
ug/l
50.00
15.54
16.44
31
33
6
Indeno(1,2,3-cd)pyrene
ug/l
50.00
23.61
18.47
47
37
24
Isophorone
ug/l
50.00
30.62
26.10
61
52
16
2-Methylnaphthalene
ug/l
50.00
23.08
19.44
46
39
17
2-Methylphenol (o-Cresol)
ug/l
50.00
23.16
20.71
46
41
11
3&4-Methylphenol
ug/l
50.00
21.83
19.25
44
38
13
Naphthalene
ug/1
50.00
18.56
16.90
37
34
9
2-Nitroaniline
ug/l
50.00
24.64
20.04
49
40
21
3-Nitroaniline
ug/l
50.00
30.26
23.51
60
47
25
4-Nitroaniline
ug/l
50.00
39.25
27.53
78
55
35 2
Nitrobenzene
ug/l
50.00
22.42
21.13
45
42
6
2-Nitrophenol
ug/1
50.00
20.27
18.89
40
38
7
4-Nitrophenol
ug/l
50.00
12.70
10.57
25
21
18
N-Nitrosodimethylamine
ug/l
50.00
11.97
14.09
24
28
16
N-Nitroso-di-n-propylamine
ug/l
50.00
28.01
24.36
56
49
14
Date: 05/13/05
1 ■'_ ■ '; LABORATORY 1 i-1
Page: 36 of 55
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40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NO Drinking Water
37712
p q0
NC Drinking Water
37706
SC Environmental
99030
Sc
99006�
cL NFLA°
E87E^8
�■ act-
LA
FL Nei MP
E87627

Pace Analytical Services, Inc.
2225 Riverside Drive
Q/I e o
naly cal
Asheville, NC 28804
aci I lr
Phone: [phone]
www.pacelahs.com
QUALITY CONTROL DATA
Fax:[phone]
Lab Project
Number:
9293484
Client
Project ID:
Demolition
Samples
LABORATORY CONTROL SAMPLE &;LCSD: 925606758
925606766
Spike
LCS
LCSD
LCS
LCSD
Parameter - Units
Conc.
Result
Result i
Rec
% Rec
RPD
Footnotes
N-Nitrosodiphenylamine ug/l
50.00
31.52
25.10
63
50
23
Pentachloroplpp- ug/l
50.00
35.05
27.47
70
55
24
Phenanthrene ug/l
50.00
28.15
21.82
56
44
25
Ph:,g;= ug/l
enol
50.00
9.673
9.509
19
19
2
Pyrene=�� ug/1
50.00
31.99
23.32
64
47
31
2
Trichlorobenzene ug/1
50.00
18.01
16:81
36
34
7
2,4,5 Trichlorophenol ug/l
50.00
28.78
24.70
58
49
15'
_ 2,4,6-Trichlorophenol ug/l
50.00
30.50
25.26
61
50
19
Nitrobenzene-d5 (S)
45
43
2-Fluorobiphenyl (S)
50
43
Terphenyl-d14 (S)
72
53
Phenol-d5 (S)
19
19
2-Fluorophenol (S)
25
27
2,4,6-Tribromophenol (S)
72
58
Date: 05/13/05
Pager
37 of 55
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
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Charlotte Certification
II)s
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
sv
NC Drinking Water
37706
SC Environmental 99030
SC
FL no
99006
E87627
Fl- nP NP Fa7r,48
„I'���a�"£
`y�`y_�!µ
IML Lf1f
UL

QC Batch:
127730
Analysis Method: EPA 8270
QC Batch Method:
EPA 3510
Analysis
Description: 1,4-Dioxane by 8270 SIM
Associated Lab
Samples 925584591
925584609
925584633 925584641
METHOD BLANKr ,1'9'
&8838
Associated Lab"Samples:
925584591
925584609
925584633 925584641
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
°1,4-Dioxane (p-Dioxane)
ug/l
NO
3.0
LABORATORY CONTROL SAMPLE: 925608846
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
1,4-Dioxane (p-Dioxane) ug/l 10.00 11.02 110
Date: 05/13/05
Page:
38 of 55
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN
This report shall not be reproduced, except in full,
Charlotte Certification
IN
NC Wastewater
40
without the written consent of Pace Analytical Services. Inc.
NC Wastewater
12
NC Drinking Water
37712
N A� o9p
NC Drinking Water
37706
SC Environmental
99030°r'"F
0
Sc
99006
G h'FLAP
I L U_
ES'�4°
/ V U
�{�� c
■-a
F nIELnP
I L IVL /1
UI UL/
E87

Pace Analytical Services, Inc.
2225 Riverside Drive
�ce/� naly fica'
Asheville; NC 28804
lri� P'1, I tr
Phone: [phone]
www.pacelabs.com QUALITY CONTROL
DATA
Fax., 828.252.4618
Lab Project Number: 9293484
Client Project ID: Demolition
Samples
QC Batch: 127564
Analysis Method: EPA 8260
QC Batch Method: EPA 8260
Analysis Description: GC/MS VOCs by 8260, low level
Associated Lab Samples 925584591
925584609 925584633
925584641
METHOD B
Associat
14 602997
Samples: 925584591 925584609 925584633 925584641
Blank Reporting
Units Result Limit Footnotes
ug/l ND 1.0
Bromobenzene
ug/l
ND
1.0
Bromochloromethane
ug/l
ND
1.0
Bromodichloromethane
ug/l
ND
1.0
Bromoform
ug/l
NO
1.0
Bromomethane
ug/l
NO
1.0
n-Butylbenzene
ug/l
ND
1.0
sec-Butylbenzene
ug/l
ND
1.0
tert-Butylbenzene
ug/l
ND
1.0
Carbon tetrachloride
ug/l
ND
1.0
Chlorobenzene
ug/l
ND
1.0
Chloroethane
ug/l
ND
1.0
Chloroform
ug/l
ND
1.0
Chloromethane
ug/l
ND
1.0
2-Chlorotoluene
ug/l
ND
1.0
4-Chlorotoluene
ug/l
ND
1.0
1,2-Dibromo-3-chloropropane
ug/l
ND
1.0
Dibromochloromethane
ug/l
ND
1.0
1,2-Dibromoethane (EDB)
ug/l
ND
1.0
Dibromomethane
ug/l
NO
1.0
1,2-Dichlorobenzene
ug/l
ND
1.0
1,3-Dichlorobenzene
ug/l
NO
1.0
1,4-Dichlorobenzene
ug/l
NO
1.0
Dichlorodifluoromethane
ug/l
NO
1.0
1,1-Dichloroethane
ug/l
ND
1.0
1,2-Dichloroethane
ug/l
NO
1.0
1,1-Dichloroethene
ug/l
ND
1.0
cis-1,2-Dichloroethene
ug/l
NO
1.0
trans-1,2-Dichloroethene
ug/l
NO
1.0
1,2-Dichloropropane
ug/l
NO
1.0
1,3-Dichloropropane
ug/l
ND
1.0
Date: 05/13/05
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 10"
SC Environmental 99030
FL NELAP E8lu
7648 ne�aP';
Page: 39 of 55
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NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Lab Project Number: 9293484
ClientProjectID: Demolition Samples
METHOD BLANK: 925602997
Associated Lab Samples<`925584591
925584609
925584633 925584641
Blank
Reporting
Parameter _."�
Units
Result
Limit Footnotes
2,2 Dichloropropane
ug/l
NO
1.0
1
1,1-Dichl9ropropene
ug/l
NO
1.0
DilsoprapyTether
ug/l
ND
1.0
Ethy'T'benzene
ug/l
ND
1.0
=HeXachloro-1,3-butadiene
ug/l
NO
1.0
Lsopropylbenzene (Cumene)
ug/l
NO
1.0
_ p Isopropyltoluene
ug/l
ND
1.0
Methylene chloride
ug/l
ND
2.0
Methyl-tert-butyl ether
ug/l
ND
1.0
Naphthalene
ug/l
NO
1.0
n-Propylbenzene
ug/l
NO
1.0
Styrene
ug/l
ND
1.0
1,1,1,2-Tetrachloroethane
ug/l
ND
1.0
1,1,2,2-Tetrachloroethane
ug/l
NO
1.0
Tetrachloroethene
ug/l
NO
1.0
Toluene
ug/l
ND
1.0
1,2,3-Trichlorobenzene
ug/l
ND
1.0
1,2,4-Trichlorobenzene
ug/l
NO
1.0
1,1,1-Trichloroethane
ug/l
ND
1.0
1,1,2-Trichloroethane
ug/l
NO
1.0
Trichloroethene
ug/l
NO
1.0
Trichlorofluoromethane
ug/l
NO
1.0
1,2,3-Trichloropropane
ug/l
NO
1.0
1,2,4-Trimethylbenzene
ug/l
ND
1.0
1,3,5-Trimethylbenzene
ug/1
NO
1.0
Vinyl chloride
ug/l
NO
1.0
m&p-Xylene
ug/l
NO
2.0
o-Xylene
ug/l
ND
1.0
Toluene-d8 (S)
%
101
4-Bromofluorobenzene (S)
%
97
Dibromofluoromethane (S)
%
93
1,2-Dichloroethane-d4 (S)
%
95
Date: 05/13/05
Page: 40 of 55
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LABORATORY CONTROL SAMPLE11',,=.925603003
Spike _
LCS
LCS
Parameter
Units
Conc.
Result
Y Rec Footnotes
Benzene
ug/l
50.00
50.52
101
Bromobenzene ,1"
ug/l
50.00
50.24
100
Bromochlorombt ane
ug/l
50.00
47.40
95
Bromodichloromethane
ug/l
50.00
47.56
95
Bromoform
ug/l
50.00
51.56
103
,T6o omethane
ug/l
50.00
32.83
66
............ n-Butylbenzene
ug/l
50.00
45.35
91
sec Butylbenzene
ug/l
50.00
49.25
98
tert-Butylbenzene
ug/l
50.00
49.08
98
Carbon tetrachloride
ug/l
50.00
48.31
97
Chlorobenzene
ug/l
50.00
46.83
94
Chloroethane
ug/l
50.00
20.73
42 3
Chloroform
ug/l
50.00
47.06
94
Chloromethane
ug/l
50.00
37.86
76
2-Chlorotoluene
ug/l
50.00
46.57
93
4-Chlorotoluene
ug/l
50.00
48.95
98
1,2-Dibromo-3-chloropropane
ug/1
50.00
61.65
123
Dibromochloromethane
ug/l
50.00
48.78
98
1,2-Dibromoethane (EDB)
ug/l
50.00
49.94
100
Dibromomethane
ug/l
50.00
48.64
97
1,2-Dichlorobenzene
ug/l
50.00
47.64
95
1,3-Dichlorobenzene
ug/l
50.00
45.95
92
1,4-Dichlorobenzene
ug/l
50.00
45.28
91
Dichlorodifluoromethane
ug/l
50.00
34.62
69
1,1-Dichloroethane
ug/l
50.00
44.09
88
1,2-Dichloroethane
ug/l
50.00
48.02
96
1,1-Dichloroethene
ug/l
50.00
47.64
95
cis-1,2-Dichloroethene
ug/l
50.00
46.19
92
trans-1,2-Dichloroethene
ug/l
50.00
48.36
97
1,2-Dichloropropane
ug/l
50.00
48.47
97
1,3-Dichloropropane
ug/l
50.00
48.24
96
2,2-Dichloropropane
ug/l
50.00
50.95
102
1,1-Dichloropropene
ug/l
50.00
48.33
97
Diisopropyl ether
ug/l
50.00
47.35
95
Ethylbenzene
ug/l
50.00
49.10
98
Hexachloro-1,3-butadiene
ug/l
50.00
51.81
104
Isopropylbenzene (Cumene)
ug/l
50.00
53.29
107
Date: 05/13/05
' ' ' ' 11171:111 ' f; V
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SC Environmental
99030
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www.pacelabs.com
QUALITY CONTROL
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
DATA Fax:[phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
LABORATORY CONTROL SAMPLE 92 6b3003
Spike
LCS
LCS
Parameter Units
Conc.
Result
%Rec
Footnotes
p-Isopropyltoluene =' ug/l
50.00
46.07
92
Methylene chlora'de ug/l
50.00
48.31
97
_
Methyl- tert butyl ether ug/l
50.00
46.40
93
Naphthal"-ne ug/l
50.00
47.05
94
n Propyl benzene ug/l
50,00
49.27
98
Styrene ug/l
50.00
50.10
100
`1,1,1,2-Tetrachloroethane ug/l
50.00
48.78
98
1,1,2,2-Tetrachloroethane ug/l
50.00
50.87
102
Tetrachloroethene ug/l
50.00
49.02
98
Toluene ug/l
50.00
49.29
99
1,2,3-Trichlorobenzene ug/l
50.00
53.48
107
1,2,4-Trichlorobenzene ug/l
50.00
51.93
104
1,1,1-Trichloroethane ug/l
50.00
47.54
95
1,1,2-Trichloroethane ug/l
50.00
50.13
100
Trichloroethene ug/l
50.00
45.49
91
Trichlorofluoromethane ug/l
50.00
33.31
67
1,2,3-Trichloropropane ug/l
50.00
48.42
97
1,2,4-Trimethylbenzene ug/l
50.00
45.27
90
1,3,5-Trimethylbenzene ug/l
50.00
44.97
90
Vinyl chloride ug/l
50.00
42.90
86
m&p-Xylene ug/l
100.00
97.43
97
o-Xylene ug/l
50.00
48.12
96
Toluene-d8 (S)
102
4-Bromofluorobenzene (S)
97
Dibromofluoromethane (S)
96
1,2-Dichloroethane-d4 (S)
95
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 925603011 925603029
Parameter
Units
Benzene
ug/l
Chlorobenzene
ug/l
1,1-Dichloroethene
ug/l
Toluene
ug/l
Trichloroethene
ug/l
Date: 05/13/05
925559452
Spike
MS
MSD
MS
MSD
Result
Conc.
Result
Result
% Rec Y.
Rec
RPD Footnotes
152.6
50.00
201.4
202.7
98
100
1
0
50.00
47.84
47.59
- 96
95
1
0.5443
50.00
48.83
50.12
97
99
3
13.20
50.00
59.47
59.86
92
93
1
175.9
50.00
218.6
221.7
85
92
1
' ' ' � ` 1 ' ' 1 ' 1 f r
Page: 42 of 55
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37712
N a �oRo
NC Drinking Water
37706
SC Environmental
99030
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MATRIX SPIKE & MATRIX SPIKE°:QUPLICATE: 925603011 925603029
925559452 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Toluene d8 (S) 96 96
4-13romofluorobdii ne (S) 98 96
Dibromofluoromethane (S) 98 101
1,2-Dichh&oethane-d4(S) 99 101
Date: 05/13/05
Page:
43 of 55
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification
IN
NC Wastewater
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without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
�_a� oRo
NC Drinking Water
37706
SC Environmental
99030
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E87627

Pace Analytical Services, Inc.
2225 Riverside Drive
ace Analytical
Asheville, NC 28804
y
''
Phone: 828.254, 7176
www.pacelabs.com
QUALITY CONTROL DATA
Fax.,828.252.4618
Lab Project Number:
9293484
Client Project ID:
Demolition Samples
QC Batch: 127600
Analysis Method: EPA 8260
QC Batch Method: EPA 8260
Analysis Description: GC/MS VOCs 5035/8260 low level
Associated Lab Samples 925584732
925584740 925584757 925584765
METHOD BLANK i-;9256056
Associated L:a1S Samples
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropan
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 05/13/05
925584732
e
925584740
925584757 925584765
Blank
Reporting
Units
Result
Limit Footnotes
ug/kg
ND
100
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
NO
10.
ug/kg
ND
100
ug/kg
NO
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
10.
ug/kg
ND'
5.0
ug/kg
NO
10.
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
NO
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
10.
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
NO
5.0
ug/kg
NO
5.0
REPORT OF LABORATORY J
Page: 44 of 55
Asheville Certification IN
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Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inca
NC Wastewater
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NC Drinking Water
37712
N,.A� oqo
NC Drinking Water
37706
SC Environmental
FL niGi no
99030
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99006
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E87627

aceAnalytical °
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone. [phone]
QUALITY CONTROL DATA Fax.,828.252.4618
1
Lab Project Number: 9293484
Client Project ID: Demolition Samples
METHOD BLANK: 925605693
Associated Lab Samples
925584732
925584740
925584757 925584765
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
1,2-Dichloropapane
ug/kg
ND
5.0
1,3-Dichloropr'opane
ug/kg
ND
5.0
212-Dichlor`opropane
ug/kg
ND
5.0
1 1 Difeh1oropropene
ug/kg
NO
5.0
cis''1,3 Dichloropropene
ug/kg
ND
5.0
'trans-1,3-Dichloropropene
ug/kg
ND
5.0
Diisopropyl ether
ug/kg
NO
5.0
Ethylbenzene
ug/kg
ND
5.0
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
2-Hexanone
ug/kg
ND
50.
Isopropylbenzene (Cumene)
ug/kg
ND "
5.0
p-Isopropyltoluene
ug/kg
ND
5.0
Methylene chloride
ug/kg_
NO
5.0
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.
Methyl-tert-butyl ether
ug/kg
ND
5.0
Naphthalene
ug/kg
NO
5.0
n-Propylbenzene
ug/kg
ND
5.0
Styrene
ug/kg
ND
5.0
1,1,1,2-Tetrachloroethane
ug/kg
NO
5.0
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
Tetrachloroethene
ug/kg
ND
5.0
Toluene.
ug/kg
ND
5.0
1,2,3-Trichlorobenzene
ug/kg
NO
5.0
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
1,1,1-Trichloroethane
ug/kg
ND
5.0
1,1,2-Trichloroethane
ug/kg
NO
5.0
Trichloroethene
ug/kg
ND
5.0
Trichlorofluoromethane
ug/kg
NO
5.0
1,2,3-Trichloropropane
ug/kg
ND
5.0
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
Vinyl acetate
ug/kg
ND
50.
Vinyl chloride
ug/kg
ND
10.
Xylene (Total)
ug/kg
ND
5.0
m&p-Xylene
ug/kg
NO
10.'
o-Xylene
ug/kg
ND
5.0
Date: 05/13/05
NEPORT OF LABORATORY ANALYSM
Page: 45 of 55
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37712
N a oR
NC Drinking Water
37706
SC Environmental
99030
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Sc
99006
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ace Analytical
www.paceiabs.com
METHOD BLANK: 925605693
Associated Lab Samples:.,
Parameter_"
Toluene-d8
4-Bromofluorobenzene (S)
Dibrompflluo`'romethane(S)
.,
1 2 D,rcmloroethane-d4 (S)
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
,84732 925584740 925584757 925584765
Blank Reporting
Units Result Limit Footnotes
98
i 96
i 99
i 100
LABORATORY CONTROL SAMPLE: 925605701
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec Footnotes
Acetone
ug/kg
100.00
105.5
106
Benzene
ug/kg
50.00
50.73
101
Bromobenzene
ug/kg
50.00
50.25
100
Bromochloromethane
ug/kg
50.00
49.10
98
Bromodichloromethane
ug/kg
50.00
50.81
102
Bromoform
ug/kg
50.00
51.12
102
Bromomethane
ug/kg
50.00
48.65
97
2-Butanone (MEK)
ug/kg
100.00
99.00
99
n-Butylbenzene
ug/kg
50.00
44.10
88
sec-Butylbenzene
ug/kg
50.00
48.07
96
tert-Butylbenzene
ug/kg
50.00
48.18
96
Carbon tetrachloride
ug/kg
50.00
50.54
101
Chlorobenzene
ug/kg
50.00
48.46
97
Chloroethane
ug/kg
50.00
58.54
117
Chloroform
ug/kg
50.00
49.84
100
Chloromethane
ug/kg
50.00
45.35
91
2-Chlorotoluene
ug/kg
50.00
48.79
98
4-Chlorotoluene
ug/kg
50.00
47.26
94
1,2-Dibromo-3-chloropropane
ug/kg
50.00
55.79
112
Dibromochloromethane
ug/kg
50.00
49.77
100
1,2-Dibromoethane (EDB)
ug/kg
50.00
50.43
101
Dibromomethane
ug/kg
50.00
51.28
103
1,2-Dichlorobenzene
ug/kg
50.00
50.04
100
1,3-Dichlorobenzene
ug/kg
50.00
48.39
97
1,4-Dichlorobenzene
ug/kg
50.00
48.74
98
Dichlorodifluoromethane
ug/kg
50.00
47.70
95
Date: 05/13/05
Page: 46 of 55
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Charlotte Certification IN
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40
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NC Drinking Water
37712
,N A� "
NC Drinking Water
37706
SC Environmental
99030
9"�
SC
99006
FL NELAP
E87648'1P�
1�
FL NELAP
E87627

aceAna,,Iyt cal
www.pacelabs.com QUALITY CONTROL DATA
s' Lab Project Number:
Client Project ID:
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax, 828,252.4618
9293484
Demolition Samples
LABORATORY CONTROL SAMPLE,,',",',',',,5605701
Spike
LCS
LCS
Parameter:
Units
Conc.
Result
Y. Rec Footnotes
1,1-Dichloroethe6e::
ug/kg
50.00
48.53
97
1,2-Dichloroet
ug/kg
50.00
47.35
95
1,1-Dichloroethene
ug/kg
50.00
52.19
104
cis-1,,2DTthloroethene
ug/kg
50.00
48.26
96
trans=l;2-Dichloroethene
ug/kg
50.00
49.12
98
=.1 2-Dichloropropane
ug/kg
50.00
48.22
96
`1,3-Dichloropropane
ug/kg
50.00
48.58
97
2,2-Dichloropropane
ug/kg
50.00
47.56
95
1,1-Dichloropropene
ug/kg
50.00
45.80
92
cis-1,3-Dichloropropene
ug/kg
50.00
48.03
96
trans-1,3-Dichloropropene
ug/kg
50.00
47.60
95
Diisopropyl ether
ug/kg
50.00
50.27
101
Ethylbenzene
ug/kg
50.00
48.67
97
Hexachloro-1,3-butadiene
ug/kg
50.00
54.61
109
2-Hexanone
ug/kg
100.00
109.9
110
Isopropylbenzene (Cumene)
ug/kg
50.00
50.94
102
p-Isopropyltoluene
ug/kg
50.00
44.38
89
Methylene chloride
ug/kg
50.00
47.34
95
4-Methyl-2-pentanone (MIBK)
ug/kg
100.00
107.2
107
Methyl-tert-butyl ether
ug/kg
50.00
50.88
102
Naphthalene
ug/kg
50.00
55.76
112
n-Propylbenzene
ug/kg
50.00
47.77
96
Styrene,
ug/kg
50.00
48.99
98
1,1,1,2-Tetrachloroethane
ug/kg
50.00
50.13
100
1,1,2,2-Tetrachloroethane
ug/kg
50.00
50.12
100
Tetrachloroethene
ug/kg
50.00
46.83
94
Toluene
ug/kg
50.00
49.17
98
1,2,3-Trichlorobenzene
ug/kg
50.00
66.18
132
1,2,4-Trichlorobenzene
ug/kg
50.00
54.94
110
1,1,1-Trichloroethane
ug/kg
50.00
48.47
97
1,1,2-Trichloroethane
ug/kg
50.00
49.86
100
Trichloroethene
ug/kg
50.00
48.64
97
Trichlorofluoromethane
ug/kg
50.00
53.20
106
1,2,3-Trichloropropane
ug/kg
50.00
46.57
93
1,2,4-Trimethylbenzene
ug/kg
50.00
44.51
89
1,3,5-Trimethylbenzene
ug/kg
50.00
44.68
89
Vinyl acetate
ug/kg
100.00
95.49
96
Date: 05/13/05
Page: 47 of 55
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall
not be reproduced,
except in full,
Charlotte Certification IDs
NC Wastewater 40
without the written consent
of Pace
Analytical Services, Inc.
NC Wastewater 12
NC Drinking Water 37712
H A� oRo
NC Drinking Water 37706
SC Environmental 99030
�`
a%
SC 99006
FL ni Gi no EQ7v4Q
ILLLnI
/��
�,�Jmb,y`y'!�
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I L IU L L„ P LVI VLI

LABORATORY CONTROL SAMP
Vinyl chloride,
Xyl ene (Total-1,
m&p-Xylene
"
o-Xylepe
Toluene`='d8 (S)
4 B mofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
MATRIX SPIKE: 925611576
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
QUALITY CONTROL DATA Fax. [phone]
Lab Project Number: 9293484
Client Project ID: Demolition Samples
5701
Spike
LCS
LCS
Units
Conc.
Result
% Rec Footnotes
ug/kg
50.00
51.10
102
ug/kg
150.00
143.6
96
ug/kg
100.00
95.44
95
ug/kg
50.00
48.17
96
101
100
98
98
Parameter
Units
Benzene
ug/kg
Chlorobenzene
ug/kg
1,1-Dichloroethene
ug/kg
Toluene
ug/kg
Trichloroethene
ug/kg
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
925563983
Spike
MS
MS
Result
Conc.
Result
% Rec Footnotes
0
67.45
66.70
99
0
67.45
62.95
93
0
67.45
76.51
113
0
67.45
65.27
97
0
67.45
62.50
93
98
98
99
99
SAMPLE DUPLICATE: 925611584
925584831
DUP
Parameter
Units
Result
Result
RPD Footnotes
Acetone
ug/kg
ND
NO
NC
Benzene
ug/kg
NO
NO
NC
Bromobenzene
ug/kg
NO
NO
NC
Bromochloromethane
ug/kg
NO
NO
NC
Bromodichloromethane
ug/kg
NO
NO
NC
Bromoform
ug/kg
NO
NO
NC
Bromomethane
ug/kg
NO
NO
NC
2-Butanone (MEK)
ug/kg
NO
NO
NC
Date: 05/13/05
Page: 48 of 55
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without the written consent of Pace Analytical Services, Inc.
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NC Drinking Water
37712
9p^9cF
NC Drinking Water
37706
SC Environmental
99030
��/1
SC
99006
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i Hr
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E 62

SAMPLE DUPLICATE: 925611584''
Parameter
Units
n-Butylbenzene
ug/kg
sec -But ylbenzene
ug/kg
,,a
tert-Butylbenzene
ug/kg
Carbon,,aetrachloride
ug/kg
Chlorobenzene
ug/kg
',Chloroethane
ug/kg
Chloroform
ug/kg
Chloromethane
ug/kg
2-Chlorotoluene
ug/kg
4-Chlorotoluene
ug/kg
1,2-Dibromo-3-chloropropane
ug/kg
Dibromochloromethane
ug/kg
1,2-Dibromoethane (EDB) —
ug/kg
Dibromomethane
ug/kg
1,2-Dichlorobenzene
ug/kg
1,3-Dichlorobenzene
ug/kg
1,4-Dichlorobenzene
ug/kg
Dichlorodifluoromethane
ug/kg
1,1-Dichloroethane
ug/kg
1,2-Dichloroethane
ug/kg
1,1-Dichloroethene
ug/kg
cis-1,2-Dichloroethene
ug/kg
trans-1,2-Dichloroethene
ug/kg
1,2-Dichloropropane
ug/kg
1,3-Dichloropropane
ug/kg
2,2-Dichloropropane
ug/kg
1,1-Dichloropropene
ug/kg
cis-1,3-Dichloropropene
ug/kg
trans-1,3-Dichloropropene
ug/kg
Diisopropyl ether
ug/kg
Ethylbenzene
ug/kg
Hexachloro-1,3-butadiene
ug/kg
2-Hexanone
ug/kg
Isopropylbenzene (Cumene)
ug/kg
p-Isopropyltoluene
ug/kg
Methylene chloride
ug/kg
4-Methyl-2-pentanone (MIBK)
ug/kg
Date: 05/13/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NM AP E87648
925584831
DUP
Result
Result
RPD
ND
ND
NC
ND
NO
NC
ND
ND
NC
NO
ND
NC
ND
NO
NC
NO
NO
NC
ND
ND
NC
NO
NO
NC
ND
ND
NC
ND
ND
NC
NO
ND
NC
ND
ND
NC
ND
ND
NC
NO
NO
NC
ND
ND
NC
NO
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
NO
NO
NC
ND
ND
NC
ND
ND
NC
ND
NO
NC
NO
ND
NC
ND
ND
NC
NO
NO
NC
ND
ND
NC
NO
ND
NC
ND
ND
NC
NO
ND
NC
ND
ND
NC '
NO
NO
NC
ND
ND
NC
NO
ND
NC
ND
ND
NC
ND
NO
NC
Footnotes
Page: 49 of 55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, Charlotte Certification IN
without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
N a oqa NC Drinking Water 37706
SC 99006
Q®� FL ni Ei no Ea7907

Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
QUALITY CONTROL DATA Fax, 828.252.4618
Lab Project Number: 9293484
Client Project ID: Demolition Samples
SAMPLE DUPLICATE: 92561158
925584831
DUP
Parameter
Units
Result
Result
RPD Footnotes
Methyl-tert-butyl ,ether
ug/kg
ND
ND
NC
Naphthalene
ug/kg
ND
ND
NC
n-Propylberrzene
ug/kg
ND
ND
NC
Styrene `
ug/kg
ND
ND
NC
1 1 Tetrachloroethane
ug/kg
ND
ND
NC
1„1;2,2-Tetrachloroethane
ug/kg
ND
ND
NC
�Tetrachloroethene
ug/kg
ND
ND
NC
Toluene
ug/kg
ND
ND
NC
1,2,3-Trichlorobenzene
ug/kg
ND
ND
NC
1,2,4-Trichlorobenzene
ug/kg
ND
ND
NC
1,1,1-Trichloroethane
ug/kg
ND
ND
NC
1,1,2-Trichloroethane
ug/kg
ND
ND
NC
Trichloroethene
ug/kg
ND
ND
NC
Trichlorofluoromethane
ug/kg
ND
ND
NC
1,2,3-Trichloropropane
ug/kg
ND
ND
NC
1,2,4-Trimethylbenzene
ug/kg
ND
ND
NC
1,3,5-Trimethylbenzene
ug/kg
ND
ND
NC
Vinyl acetate
ug/kg
ND
ND
NC
Vinyl chloride
ug/kg
ND
ND
NC
Xylene (Total)
ug/kg
ND
ND
NC
m&p-Xylene
ug/kg
ND
ND
NC
o-Xylene
ug/kg
ND
ND
NC
Toluene7d8 (S)
%
102
99
4-Bromofluorobenzene (S)
%
94
96
Dibromofluoromethane (S)
%
92
96
1,2-Dichloroethane-d4 (S)
%
85
108
Date: 05/13/05
Page: 50 of 55
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NO Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NO Drinking Water
37712
N .a oRo
NC Drinking Water
37706
SC Environmental
99030
0
%'
"�
Sc
99006
Fi nisi no
L NLLPII
ra aAQ
LV7V�V
(/�
e� �e act
Ci MM AD
I L IVL -
ER76 7
2.

QC Batch: 127366 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Sample's 925584674
METHOD BLANK `925591844
Associated Lab Samples:
925584674
Blank
Reporting
'Parameter
Units
Result
Limit Footnotes
'Mercury
mg/1
ND
0.0002
LABORATORY CONTROL SAMPLE:
925591851
Spike
LCS LCS
Parameter
Units
Conc.
Result i Rec Footnotes
Mercury
mg/l
0.0025
0.0027 107
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
925591869 925591877
925584674
Spike MS MSD MS MSD
Parameter
Units
Result
Conc. Result Result o Rec i Rec RPD Footnotes
Mercury
mg/l
0
0.0025 0.0024 0.0021 95 82 14
Date: 05/13/05 Page: 51 of 55
REPORT OF LABORATORY ANALYSIS
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NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 H A oqa NC Drinking Water 37706
SC Environmental 99030 0;�; 9yF Sc 99006
FL NELAP E87648 FL NELAP E87627

METHOD BLANK .-`'925592024
Associated Lab` Samples: 925584674
Blank
Reporting
=Parameter
Units
Result
Limit Footnotes
Arsenic
mg/l
NO
0.025
Barium
mg/l
NO
0.025
Cadmium
mg/l
NO
0.0050
Chromium
mg/l
NO
0.010
Lead
mg/l
NO
0.025
Selenium
mg/l
ND
0.025
Silver
mg/l
NO
0.010
LABORATORY CONTROL SAMPLE: 925592032
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec Footnotes
Arsenic
mg/l
2.500
2.215
89
Barium
mg/l
2.500
2.230
89
Cadmium
mg/l
2.500
2.150
86
Chromium
mg/l
2.500
2.180
87
Lead
mg/l
2.500
2.170
87
Selenium
mg/l
2.500
2.165
87
Silver
mg/l
2.500
2.235
89
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
925592040 925592057
925573495
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec 5.1
Rec
RPD Footnotes
Arsenic
mg/l
0.01935
2.500
2.205
2.315
87
92
5
Barium
mg/l
0.7550
2.500
2.940
3.025
87
91
3
Cadmium
mg/l
0.00710
2.500
2.045
2.155
82
86
. 5
Chromium
mg/l
0.00326
2.500
2.060
2.170
82
87
5
Lead
mg/l
0.1325
2.500
2.170
2.295
82
86
6
Date: 05/13/05 Page: 52 of 55
_jEPORT OF LABORATORY ANALYSUP
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Charlotte Certification IDs
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N a o,o
NC Drinking Water
37706
SC Environmental
99030
Sc
99006
I ni
FL
E8764$
£
6 :����� ±
FL NEI _ P
E87627

Pace Analytical Services, Inc.
aceA nianIX cal °
2225 Riverside Drive
Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA
r
Phone: Fax828,252,4618
Fax: [phone]
Lab Project Number:
9293484
Client Project
ID: Demolition Samples
MATRIX SPIKE& MATRIX SPIKE";DUPLICATE: 925592040 925592057
925573495 Spike MS MSD
MS MSD
ParameterUnits Result Conc. Result Result
i Rec Rec RPD Footnotes
Selenium mg/l 0.00026 2.500 —2.170 2.310
87 92 6
Silver mg/l 0 2.500 2.125 2.230
85 89 5
Date: 05/13/05
Page: 53 of 55
REPORT OF LABORATORY ANALYSIS
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Charlotte Certification IDs
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Wastewater 12
NC Drinking Water 37712 N A oA
NC Drinking Water 37706
SC Environmental 99030 `""
o���-
Sc 99006
FI NELAP E87648
IFi INIE n E8p76 7
I LIULLHP LUI V21

QC, Batch: 127319 Analysis Method: i Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated tab Samples 925584732 925584740 925584757 925584765
SAMPLE DUPLICATfE:""925586968
925585580 DUP
Parameter Units Result Result RPD Footnotes
•P.ercent Moisture % 19.90 20.80 4
Date: 05/13/05
Page:
54 of 55
REPORT OF LABORATORY ANALYSIS
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Charlotte Certification
IN
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
N A oR
NC Drinking Water
37706
SC Environmental 99030
ai �9F
SC
99006
FL NEI_AP E87648�l"'�i�.
��:£.
■ !/m■.L�r !_
rri niri n n
1 IVr1 Fir
rro7en�
(1/!]//

QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidel1,nes,"'unrounded concentrations are displayed and have been used to calculate i Rec and RPD values.
LCS(D) Laboratory 'ontrol Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Samphe`Duplicate
ND Not. -detected at or above adjusted reporting limit
NC Not Calculable
J„r3. Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDIL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
[1] The surrogate and/or spike recovery was outside acceptance limits.
[21 RPD value was outside control limits, however both percent recoveries were acceptable. Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data.
[31 The spike recovery was outside acceptance limits for this compound, however, the spike recovery was within
acceptance limits in the MS/MSD.
Date: 05/13/05
."I'EPORT OF LABORATORY ANALYSM
Page: 55 of 55
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Charlotte Certification IN
NC Wastewater
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12
NC Drinking Water
37712
N a oqo
NC Drinking Water
37706
SC Environmental
99030%`'
0
r ,F
Sc
99006
FL NELAP
E87648
v
51—r\
a ■...■!�■6iiea':r
n nisi AP
I L IVLLPI
E87co7
f uL'

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
,e�Wvm, �#acetabs coin HuntersvrNe, NC28078
Phone, 704.875.909
P Fax- 704.875.9091
April 07, 2005
Mr. Roger Galloway
AGFA Corporation
P.O. Box 267
Brevard, NC 28712
RE: Lab Project Number: 9291307
Client Project ID: Sludge Lagoon & Aeration
Dear Mr. Galloway:
Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2005. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of
the report.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
4 ( �
Lorri Patton
[e-mail]
Project Manager
Enclosures
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REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater 40
This report shall not be reproduced, except in full,
NC Wastewater 12
NC Drinking Water 37712
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37706
SC Environmental 99030
Sc 99006
FL NELAP E87648
FL NELAP E87627

Pace Analytical Services, Inc.
laneAnalyticalAshe
Riverside Drive
Asheville, NC 28804
www.pacelabs.com
Phone: [phone]
Fax: [phone]
Lab Project Number:
9291307
Client Project
ID:
Sludge Lagoon & Aeration
Solid results are
reported on a dry weight basis
Lab Sample No:
925465528,'
Project Sample
Number: 9291307-001
Date Collected: 03/21/05 11:45
Client Sample ID:
SLUDGE LatatON"& AERATION BASIN
Matrix: Soil
Date Received: 03/21/05 13:58
Parameters
Results Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Metals
Metals, Trace ICP T Prep/Method: EPA 3050 /
EPA 6010
Chromium
620 mg/kg
1.3
04/07/05 03:06
ALV
7440-47-3
Silver
1900 mg/kg
1.3
04/07/05 03:06
ALV
7440-22-4
Date ted
04/05/05 05:30
04/05/0505:30
WeteChemistry
Percent Moisture
Method:i Moisture
Percent Moisture
84.4 Y.
04/06/05 08:55
TNS
Date: 04/07/05
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37712
0 ,N A oRo
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37706
SC Environmental
99030
5`
��
Sc
99006
FL NELAP
E87648
_ r:enc
P1 KIFI GP
PPQ7A97

Date: 04/07/05
Page:
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REPORT OF LABORATORY ANALYSIS
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NO Wastewater
40
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NO Wastewater
12
NO Drinking Water
37712
a �oqo
NO Drinking Water
37706
SC Environmental
99030
`:\F
SC
99006
FL NELAP
E8764$
FI NIFI AP
FR1927

ace Anal t cal °
J
www,pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9291307
Client Project ID: Sludge Lagoon & Aeration
QC Batch: 125007
Analysis Method: EPA 6010
QC Batch Method: EPA 305u
Analysis
Description: Metals, Trace ICP
Associated Lab Samples
925465528
METHOD BLANK;?925467862
Associated Lit' Samples:
925465528
Blank
Reporting
.Parameter
Units
Result
Limit Footnotes
Chromium
mg/kg
ND
0.20
Silver
mg/kg
NO
0.20
LABORATORY CONTROL
SAMPLE: 925467870
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y Rec Footnotes
Chromium
mg/kg
50.00
44.00
88
Silver
mg/kg
50.00
46.40
93
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
925467888 925467896
925371957 Spike
MS
MSD
MS
MSD
Parameter
Units
Result Conc.
Result
Result
Y. Rec Y
Rec RPD Footnotes
Chromium
mg/kg
85.10 75.99
157.6
127.4
95
58 21 1,2
Silver
mg/kg
0 75.99
68.11
64.59
90
88 5
Date: 04/07/05 Page: 3 of 5
REPORT OF LABORATORY ANALYSIS
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37706
SC Environmental
99030
FL NELAP
E87648
F1 KIPI AP
FR7A97

Percent Moisture
Analysis Method: % Moisture
Analysis Description: Percent Moisture
925465528
925465528 DUP
Units Result Result RPD Footnotes
84.40 83.30 1
Uate: 04/0//Ub
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REPORT OF LABORATORY ANALYSIS
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NC Wastewater
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NC Wastewater
12
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37712
NC Drinking Water
37706
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99030
so
99006
FL NELAP
11:87648
F1 NFI AP
F97627

Pace Analytical Services, Inc.
r 1 2225 Riverside Drive
aceAl lal �/tica'� Asheville, NC 28804
J ` Phone: [phone]
www, pacelabs, com Fax [phone]
Lab Project Number: 9291307
Client Project ID: Sludge Lagoon & Aeration
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guideliaunrounded concentrations are displayed and have been used to calculate i Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix"",, le (Duplicate)
DUP Sample Duplicate
ND Not°detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDLAdjusted Method Detection Limit
RPD Relative Percent Difference
Ill The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
[21 The calculated RPD was outside QC acceptance limits.
Date: 04/07/05
Pager
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REPORT OF LABORATORY ANALYSIS
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40
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NC Wastewater
12
NC Drinking Water
37712
0 ,y A� oqa
NC Drinking Water
37706
SC Environmental
99030
% l 9y
Sc
99006
FL NELAP
E87648
� ��
P1 NIP] AP
GR7907

Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
*lx Hunteisville, NC 28078
l Phone; 704.8759092
u t:9lcpsctabsetim Fax- 704.875.9091
March 29, 2005
Mr. Roger Galloway
AGFA Corporation
P.O. Box 267
Brevard, NC 28712
RE: Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Dear Mr. Galloway:
Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2005. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of
the report.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
P
4')
Lorri Patton
[e-mail]
Project Manager
Enclosures
Asheville certification IN
REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712
This report shall not he reproduced, except in full,
SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Lab Sample No: 9254149
Client Sample ID: SLUDGE.
'arameters
Client Services
Nitrogen, Total :Soil
Nitrogen
Microbiology
Fecal `Coliform MPN Solid
,Col iform, Fecal
Metals
Metals, Trace ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Date Digested
Mercury, CVAAS, in Soil
Mercury
Wet Chemistry
Percent Moisture
Percent Moisture
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252,4618
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Project Sample Number: 9290415-001 Date Collected: 03/21/05 11:45
& AERATION Matrix: Soil Date Received: 03/21/05 13:58
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: SM 4500-CO2 D
11000 mg/kg 7.1 03/29/05 LJP 7727-37-9
Method: SM 9221E
ND
Prep/Method: EPA 3050 / EPA 6010
32000
mg/kg
64.
ND
mg/kg
3.2
7.9
mg/kg
0.64
5700
mg/kg
64.
340
mg/kg
1.3
44.
mg/kg
3.2
2800
mg/kg
64.
5.3
mg/kg
3.2
39.
mg/kg
3.2
2900
mg/kg
640
NO
mg/kg
3.2
ND
mg/kg
640
1200
mg/kg
6.4
03/22/05 04:00
Method: EPA 7471
NO mg/kg
Method: o Moisture
85.9 Y.
03/22/05 09:25 MMG
03/29/05 00:50 ALV 7429-90-5
03/29/05 00:50 ALV 7440-38-2
03/29/05 00:50 ALV 7440-43-9
03/29/05 00:50 ALV 7440-70-2
03/29/05 00:50 ALV 7440-50-8
03/29/05 00:50 ALV 7439-92-1
03/29/05 00:50 ALV 7439-95-4
03/29/05 00:50 ALV 7439-98-7
03/29/05 00:50 ALV 7440-02-0
03/29/05 00:50 ALV 7440-09-7
03/29/05 00:50 ALV 7782-49-2
03/29/05 00:50 ALV 7440-23-5
03/29/05 00:50 ALV 7440-66-6
03/22/05 04:00
0.035 03/29/05 ALV 7439-97-6
Nitrogen, Ammonia Method: EPA 350.1 Modified
Nitrogen, Ammonia 370 mg/kg 70
Total Kjeldahl Nitrogen, Soil Method: EPA 351.2
Nitrogen, Kjeldahl, Total 11000 mg/kg 710
Date: 03/29/05
03/23/05 10:00 TNS
03/29/05 12:51 TMR 7727-37-9
03/25/05 22:00 ARH
Page: 1 of 15
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9y
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37706
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YY
: C
>
l
Sc
99006
FI NFI AP
E87627

rax: tSLfi.LDZ.4b I tS
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Lab Sample No: 925414971
Project Sample
Number:
9290415-001
Date Collected: 03/21/05 11:45
Client Sample ID: SLUDGE LAGOON:&
AERATION
Matrix:
Soil
Date Received: 03/21/05 13:58
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Nitrogen, Nitrate plus Nitrite
Method: EPA
353.2 Modified
Nitrate as N
NO
mg/kg
71.
03/28/05
22:15
JDA1
Nitrate -Nitrite (as N)
NO
mg/kg
71.
03/28/05
22:15
JDAI
7727-37-9
Nitrite as N.
NO
mg/kg
71.
03/28/05
22:15
JDA1
Phosphorus, Total, Soil
Method: EPA
365.2
,Phosphorus
623.
mg/kg
68.2
03/24/05
08:00
TMR
7723-14-0
pH
Method: EPA
9045
pH
7.00
units
03/25/05
10:30
TMR
1
Plant Available Nitrogen
Method:
Nitrogen
3400
mg/kg
1.0
03/29/05
14:55
EWS
7727.37-9
Date: 03/29/05 Page: 2 of 15
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37712
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E87648 ,
act
FI 1IFI AP
E87627

ti. VLV.LJT./ I / V
www, pace a s. cnm Fax: 828,252.4618
I' Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was,.performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method,9071B modified to use ASE.
Ala'pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Nb� Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Ell Analysis conducted in excess of EPA recommended holding time.
Date: 03/29/05
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SC
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f
FI NIFI AP
F87627

Lab Project Niwmher• 9290415
Client Project ID: Sludge Lagoon & Aeration
QC Batch: 124282 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: Mercury, CVAAS, in Soil
Associated Lab Samples, 925414971
METHOD BLANK:`•: 925433781
Associated'°;Lab Samples: 925414971
Mercury
Blank Reporting
Units Result Limit Footnotes
mg/kg ND 0.0050
LABORATORY CONTROL SAMPLE: 925433799
Spike LCS LCS
Parameter Units Conc. Result i Rec Footnotes
Mercury mg/kg 0.0667 0.0691 104
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 925434060 925434078
925414971 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/kg 0 0.4728 0.5050 0.4842 107 102 4
Date: 03/29/05
Page: 4 of 15
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37712
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37706
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99030
�` ` F
SC
99006
FL NIF1 AP
FR7fi4n
l�� �
FI AIFI AP
F87627

QC Batch: 123978
QC Batch Method: EPA 30!
Associated Lab Samples:
925414971
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Analysis Method: EPA 6010
Analysis Description: Metals, Trace ICP
METHOD BLANK.::_925415598
Associated Lab Samples:
925414971
Blank
Reporting
°Parameter
Units
Result
Limit Footnotes
Aluminum
mg/kg
ND
10.
Arsenic
mg/kg
ND
0.50
Cadmium
mg/kg
ND
0.10
Calcium
mg/kg
NO
10.
Copper
mg/kg
ND
0.20
Lead
mg/kg
NO
0.50
Magnesium
mg/kg
ND
10.
Molybdenum
mg/kg
ND
0.50
Nickel
mg/kg
ND
0.50
Potassium
mg/kg
NO
100
Selenium
mg/kg
NO
0.50
Sodium
mg/kg
ND
100
Zinc
mg/kg
ND
1.0
LABORATORY CONTROL SAMPLE: 925415606
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec Footnotes
Aluminum
mg/kg
2000.00
1890
94
Arsenic
mg/kg
50.00
47.50
95
Cadmium
mg/kg
50.00
46.10
92
Calcium
mg/kg
2000.00
1820
91
Copper
mg/kg
50.00
45.10
90
Lead
mg/kg
50.00
42.50
85
Magnesium
mg/kg
2000.00
1820
91
Molybdenum
mg/kg
50.00
49.60
99
Nickel
mg/kg
50.00
45.50
91
Potassium
mg/kg
1000.00
897.0
90
Selenium
mg/kg
50.00
45.40
91
Sodium
mg/kg
1000.00
936.0
94
Date: 03/29/05
Page: 5 of 15
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40
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12
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37706
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F
SC
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E87648
¢1� 'ne a�
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E87627

LABORATORY CONTROL
Zinc
Spike LCS LCS
Units Conc. Result % Rec Footnotes
mg/kg 50.00 48.10 96
MATRIX,SPI`KE & MATRIX SPIKE DUPLICATE: 925415614 925415622
925410748
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD
Footnotes
Aluminum
mg/kg
1492
2869.00
4213
4213
95
104
0
Arsenic
mg/kg
2.333
71.74
62.87
554.2
84
846
159
1,2
Cadmium
mg/kg
0.01530
71.74
60.00
48.78
84
75
21
2
Calcium
mg/kg
471.6
2869.00
2804
2322
81
71
19
1
Copper
mg/kg
0.1605
71.74
59.87
64.69
83
99
8
Lead
mg/kg
1.718
71.74
57.52
54.00
78
80
6
Magnesium
mg/kg
222.0
2869.00
2569
2426
82
84
6
Molybdenum
mg/kg
0.00928
71.74
63.39
50.87
88
78
22
Nickel
mg/kg
0.5844
71.74
60.13
52.04
83
79
14
Potassium
mg/kg
73.62
1435.00
1317
1487
87
108
12
Selenium
mg/kg
0
71.74
58.56
54.52
82
84
7
Sodium
mg/kg
0
1435.00
1262
1295
88
99
3
Zinc
mg/kg
4.828
71.74
65.48
56.87
84
80
14
SAMPLE DUPLICATE: 925415986
925410755
DUP
Parameter
Units
Result
Result
RPD Footnotes
Aluminum
mg/kg
2100
1700
20
Arsenic
mg/kg
2.100
1.500
34
Cadmium
mg/kg
ND
ND
NC
Calcium
mg/kg
740.0
830.0
11
Copper
mg/kg
NO
NO
NC
Lead
mg/kg
1.500
2.200
41
Magnesium
mg/kg
210.0
170.0
24 2
Molybdenum
mg/kg
NO
ND
NC
Nickel
mg/kg
0.6200
ND
NC
Potassium
mg/kg
ND
NO
NC
Selenium
mg/kg
NO
NO
NC
Date: 03/29/05
REPORT OF LABORATORY ANALYSHE
Page: 6 of 15
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40
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12
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37712
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37706
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99030
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99006
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E87648
�:�lac,-
FL NELAP
E87627

Pace Analytical Services, Inc.
laceAnalytical Asheville,
Riverside Drive
NC 28804
SAMPLE DUPLICATE:
Sodium
Zinc
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
925410755 DUP
Units Result Result RPD Footnotes
mg/kg ND ND NC
mg/kg 5.100 3.500 37
Date: 03/29/05
Page:
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REPORT OF LABORATORY ANALYSIS
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37706
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E87648
:����
Fi nIFi AP
P87F;7

QC Batch: 124422 Analysis Method: SM 9221E
QC Batch Method: SM 9221F�.s Analysis Description: Fecal Coliform MPN Solid
Associated Lab Samples. ' 925414971
METHOD BLANKs:._,925440653
Associated Cab Samples: 925414971
Blank Reporting
Parameter Units Result Limit Footnotes
Coliform, Fecal NO
Date: 03/29/05
Page:
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REPORT OF LABORATORY ANALYSIS
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act-
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QC Batch: 124124 Analysis Method: % Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated Lab Samples: 925414971
SAMPLE DUPLICATE:" 925421620
925419533 DUP
Paramet"er Units Result Result RPD Footnotes
Percent Moisture % 24.20 22.60 7
Date: 03/29/05
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REPORT OF LABORATORY ANALYSIS
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H A o
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� �£
SC
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FL NELAP
E87648
ac=
�
FL NELAP
E87627

Date: 03/29/05
Page:
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REPORT OF LABORATORY ANALYSIS
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a N a ogo
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a %' aF
SC
99006
FL NELAP
E87648!��C�
FL NELAP
E87627

ace Analytical °
www.pacelabs.com
I
QC Batch: 124201
QC Batch Method: EPA 36
Associated Lab Samples'
METHOD
Associa
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax- 828,252,4618
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Analysis Method: EPA 365.2
Analysis Description: Phosphorus, Total, Soil
925414971
Samples: 925414971
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Phosphorus
mg/kg
ND
10.0
LABORATORY CONTROL SAMPLE:
925427452
Spike
LCS LCS
Parameter
Units
Conc.
Result % Rec Footnotes
Phosphorus
mg/kg
20.00
22.96 115
MATRIX SPIKE: 925427460
925419947 Spike MS MS
Parameter Units Result Conc. Result Y. Rec Footnotes
Phosphorus mg/kg 2235 1352.00 3740 ill
SAMPLE DUPLICATE: 925427478
925414971 DUP
Parameter Units Result Result RPD Footnotes
Phosphorus mg/kg 623.0 873.0 33 2
Date: 03/29/05
Page: 11 of 15
REPORT OF LABORATORY ANALYSIS
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12
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SC Environmental
37712
99030
N n �oRo
9
NC Drinking Water
37706
FL NELAP
E87648
�. ® �\
Sc
99006
FL NELAP
E87627

ce Analytical
www.pacelabs.com
QC Batch: 124321
QC Batch Method: EPA 35
Associated Lab Samples":t
METHOD BLANK:;, 9254354Z
Associated Lab Samples: 925414971
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrogen, Kjeldahl, Total mg/kg ND 10.
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
QUALITY CONTROL DATA Fax:828.252:4618
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Analysis Method: EPA 351.2
Analysis Description: Total Kjeldahl Nitrogen, Soil
925414971
LABORATORY CONTROL SAMPLE: 925435430
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Nitrogen, Kjeldahl, Total mg/kg 400.00 381.6 — 95
MATRIX SPIKE: 925435448
925414971 Spike MS MS
Parameter Units Result Conc. Result Y. Rec Footnotes
Nitrogen, Kjeldahl, Total mg/kg _11320 2837.00 13050 61 1
SAMPLE DUPLICATE: 925435455
925419947 DUP
Parameter Units Result Result RPD Footnotes
Nitrogen, Kjeldahl, Total mg/kg 270000 300000 9
Date: 03/29/05
Page: 12 of 15
REPORT OF LABORATORY ANALYSIS
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Charlotte Certification
IN
NC Wastewater
40
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NC Wastewater
12
NC Drinking Water
SC Environmental
37712
99030
N a� oRo
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37706
FL NELAP
E87648
N
SC
99006
FL NELAP
E87627

QC Batch: 124480
QC Batch Method: EPA 35
Associated Lab Samplzes:"
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
Analysis Method: EPA 353.2 Modified
ified Analysis Description: Nitrogen, Nitrate plus Nitrite
925414971
METHOD BLANKf-t.925442790
Associated L Samples: 925414971
Nitrate as N
Nitrate -Nitrite (as N)
Nitrite as N
Blank
Reporting
Units
Result
Limit Footnotes
mg/kg
NO
10.
mg/kg
NO
10.
mg/kg
NO
10.
LABORATORY CONTROL SAMPLE: 925442808
Spike LCS LCS
Parameter Units Conc. Result Y. Rec Footnotes
Nitrate -Nitrite (as N) mg/kg 500.00 480.0 96
MATRIX SPIKE: 925442816
925414971
Spike
MS
MS
Parameter Units Result
Conc.
Result
Y. Rec Footnotes
Nitrate -Nitrite (as N) mg/kg 0
3546.00
3617
102
SAMPLE DUPLICATE: 925442824
925419947
DUP
Parameter
Units
Result
Result
RPD Footnotes
Nitrate as N
mg/kg
ND
NO
NC
Nitrate -Nitrite (as N)
mg/kg
NO
ND
NC
Nitrite as N
mg/kg
NO
ND
NC
Date: 03/29/05
Page:
13 of 15
REPORT F LA AT ANALYSIS
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IDs
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40
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NC Wastewater
12
NC Drinking Water
37712
a oR
NC Drinking Water
37706
SC Environmental
99030
Sc
99006
FL NELAP
E87648
.� act-
FL NELAID
E87627

Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
QC Batch: 124500 Analysis Method: EPA 350.1 Modified
QC Batch Method: EPA 350 1`'Modified Analysis Description: Nitrogen, Ammonia
Associated Lab Sam , �`'
pies 925414971
METHOD BLANK`r„925443442
Associated Laab Samples:
925414971
Blank
Reporting
P.ar'ameter
Units
Result
Limit Footnotes
Nitrogen, Ammonia
mg/kg
NO
10.
LABORATORY CONTROL SAMPLE:
925443459
Spike
LCS LCS
Parameter -
Units
Conc.
Result i Rec Footnotes
Nitrogen, Ammonia
mg/kg
100.00
106.2 100
925414971
Spike
MS
MS
Parameter Units Result
Conc.
Result
% Rec Footnotes
Nitrogen, Ammonia mg/kg 366.4
695.30
1120
161
SAMPLE DUPLICATE: 925443475
925419947 DUP
Parameter Units Result Result RPD Footnotes
Nitrogen, Ammonia mg/kg 2500 2700 6
Date: 03/29/05 Page: 14 of 15
SPORT F LA AT Y ANALYSIS
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40
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12
NC Drinking Water
SC Environmental
37712
99030
N a o
".
NC Drinking Water
37706
FL NELAP
E87648
:° _
SC
99006
FL NELAP
E87627

laneAnalytical
www.pacelabs.com ;
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 9290415
Client Project ID: Sludge Lagoon & Aeration
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guldeliPnes`'unrounded concentrations are displayed and have been used to calculate i Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spr`ke (Duplicate)
DOPSample buplicate
ND Not detected at or above adjusted reporting limit
NC iJot Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
<DL Adjusted Method Detection Limit
RPD Relative Percent Difference
[1] The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
[2] The calculated RPD was outside QC acceptance limits,
[31 Analysis conducted in excess of EPA recommended holding time.
Date: 03/29/05
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REPORT OAF LABORATORY AALYSI
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without the written consent of Pace Analytical Services, Inca NC Wastewater 12
N " NC Drinking Water 37706
? \F SC 99006
c EL NELAP E87627

Enclosure No.3
Groundwater Section Guidelines for the
Investigation and Remediation of
Soil and Groundwater
Table 3
Contaminated Soil Clean-up Levels

Enclosure No.3 Excerpted from the
GROUNDWATER SECTION GUIDELINES FOR THE
INVESTIGATION AND REMEDIATION OF
SOIL AND GROUNDWATER
STATE of NORTH CAROLINA
DEPARTMENT of ENVIRONMENT and NATURAL RESOURCES
DIVISION of WATER QUALITY
GROUNDWATER SECTION
http://gw.ehnr.state.nc.us
July 2000
Table 3
Contaminated Soil Clean -Up Levels
Compound
CAS #
Soil to GW
(mg/kg)*
Acenaphthene
83-32-9
8
Acenaphthylene
208-96-8
11
Acetone
67-64-1
2.81
Anthracene
120-12-7
995
Barium
7440-39-3
848
Benzene
71-43-2
0.0056
Benzo(a)anthracene
56-55-3
0.34
Benzo(b)fluoranthene
205-99-2
1
Benzo(g,h,l)perylene
191-24-2
6720
Benzo(k)fluoranthene
207-08-9
12
Benzo(a)pyrene
50-32-8
0.091/0.088**
Benzoic acid
65-85-0
112
Bis(chloroethyl)ether(BCEE)
111-44-4
0.0002
n-Butylbenzene
104-51-8
4
Sec -Butyl benzene
135-98-8
3
Tert-Butylbenzene
104-51-8
3
Carbon
75-15-0
4
Chlorom ethane(m ethyl chloride)
74-87-3
0.02
Chromium III
16065-83-1
27
Chromium VI
18540-29-9
27
Chrysene
218-01-9
38
Dibenzo(a,h)anthracene
53-70-8
0.17/0.088**
Dibenzofuran
132-64-9
4.7
Dibromochlorom ethane
124-48-1
0.002
1,2-Dibromoethane (ethylene dibromide; EDB)
106-93-4
0.00000197
1,2-Dichlorobenzene
95-50-1
7
1,3-Dichlorobenzene
541-73-1
24
1,4-Dichlorobenzene
106-46-7
1
1,1-Dichloroethane (1,1-DCA)
75-34-3
4

1,2-Dichloroethane (ethylenedichloride;1,2-DCA)
1,2-Dichloroethene (cis)(cis-1,2-DCE)
1,2-Dichloroethene (trans) (trans-1,2-DCE)
1,1-Dichloroethane (1,1-DCE)
1,2-Dichloropropane
1,3-Dichloropropene (cis and trans)
2,4-Dimethylphenol
Ethyl acetate
Ethylbenzene
Fluoranthene
Fluorene
Hexachlorobutadiene
2-Hexanone
Indeno(1,2,3-cd)pyrene
Isopropyl benzene (cumene)
Isopropyl ether (d i isopropyl ether)
Lead
Methanol
Methylethylkeytone (2-Butanone; MEK)
Methyl tert-butyl ether (MTBE)
Methylene Chloride
2-Methyl naphthalene
Naphthalene
Phenanthrene
n-Propylbenzene
Pyrene
1,1,2,2-Tetrachlorethane
Tetrachloroethylene (PCE)
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Toluene
Xylenes (mixed)
107-06-2
156-59-2
156-60-5
75-35-4
78-87-5
542-75-6
105-67-9
141-78-6
100-41-4
206-44-0
86-73-7
87-68-3
591-78-6
193-39-5
98-82-8
108-20-3
7439-92-1
67-56-1
78-93-3
1634-04-4
75-09-2
91-57-6
91-20-3
85-01-8
103-65-1
129-00-0
79-34-5
127-18-4
120-82-1
95-63-6
108-67-8
108-88-3
1330-20-7
0.0018
0.35
0.38
0.045
0.0029
0.0009
0.9
11
0.24
276
44
0.26
1.9
3
2
0.37
270
14
0.69
0.92
0.02
3
0.58
60
2
286
0.001
0.0074
2.6
8
7
7
5
Notes * If the soil contaminant concentration is less than the method detection limit,
the maximum soil concentration should be at the level of the
method detection limit.
** Residential Level
July 2000

NOV _ 5 2004 � � Agfa Corporation
P.O. Box 267
Staton Road
WATER QUALITY SECTION Brevard, NC 28712-0267
SHEVILLE REGIONAL OFFICE
To: Bradley Bennett, State of North Carolina, DENR, NPDES Stormwater
From: Chet Meinzer, AGFA Corporation, Brevard Site, Facilities Manager
CC: Charlene Graff, Roger Galloway, Jamie Vanbuskirk, Kerry Becker, Michael E. Gel],
David Epps
Date: 11/4/2004
Re: WWTP Closure: Redirection of Stormwater to a new outfall
Stormwater Redirect to New Outfall
The AGFA Corporation Brevard Site, in Transylvania County, at Staton Road, Brevard, NC 28712, is in
the process of closing the manufacturing site and the industrial wastewater treatment plant.
• All production facilities are currently shutdown and being dismantled. No further
process wastewater will be discharged to the existing wastewater treatment plant.
o The site produced medical X-ray film with a SIC code of 3861 until the
manufacturing area was shut down.
• The closure of the wastewater treatment facility requires that several stormwater drains
be rerouted from the current NPDES outfall to a new stormwater outfall.
• We request that the new outfall (Stormwater outfall 008) be covered by the site's
existing stormwater permit. (General permit # NCG 030057)
o The new stormwater outfall will be located at Latitude N 35011'15"and
Longitude W 82036'51". The outfall is identified on the attached drawing.
(Drawing # D&Z 1000452 Rev. 1)
o The redirecting of stormwater flows will include construction of a wet detention
basin that will contain the 10-year 24=hour rainfall event for the area.
o The new outfall will discharge to the same unnamed tributary of the Little River;
a Class C Trout Stream, which has received the NPDES surface water
discharge flow from Outfall 001. (NPDES Permit 0000337)
o The drainage area of the new outfall is approximately 9.4 acres and is shown
by the shaded area on the attached drawing. The area drained is 70%
impervious. (See drawing D&Z A1000438 Rev 0.)
1

• An Erosion & Sedimentation Control Plan has been prepared for the site demolition
activities. Under the closure plan for the wastewater treatment system, in agreement
with the Ashville Region NPDES group, the basins will be re -graded after they have
been emptied.
o The final grade of the wastewater treatment ponds after closure is shown on
the attached drawings D&Z 1000452 Rev. 1 and D&Z Al 000455 Rev. 1.
• The site contact person for this project will be Roger Galloway the ORC for the
wastewater treatment facility. He can be reached at 828-862-8379 ext. 200
If you have any questions about our request for coverage please call Roger Galloway or me at 828-
862-8379 ext. 100.
Sincerely,
Chet Meinzer
Facilities Manager
• Page 2

P Closure
..bject: Re: AGFA Brevard WWTP Closure
From: Forrest Westall <[e-mail]>
Date: Mon, 04 Oct 2004 14:53:49 -0400
To: Shannon Mohr Thornburg <[e-mail]>
CC: Kerry Becker <[e-mail]>
Shannon, I reviewed the plan with Kerry and I'm thinking that we sent out a letter of approval (I've slept
since then). I will copy this to Kerry and make sure. In any event, the plan was to approve an acceptable
closure plan with the understanding that long term issues would be addressed by DWM in the overall
site managment plan. Thanks. Forrest
Shannon Mohr Thornburg wrote:
Forrest - I was just organizing some paperwork in my office and came across my AGFA Brevard
WWTP Closure file. Is there anything required of me at this point in terms of follow-up, review,
etc.? I was just wondering if I should go ahead and send my file to SWPS Central Files or not.
Thanks for any guidance that you are able to provide!
Shannon
Shannon Mohr Thornburg, Environmental EngineerMailing Address:
Land Application Unitl636 Mail Service Center
Aquifer Protection SectionRaleigh, NC27699-1636
NCDENR-DWQPhysical Address:
Telephone:[phone] Capital Boulevard, Room No. 1C 130
Fax:[phone]Raleigh, NC27604
shannon. thomburg(cb,ncmail.nethttp://h2o. enr. state.nc.us/ndpu
Forrest Westall - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
Forrest Westall <Forrest.Westal.1pncmail.net>
Division of Water Quality - Water Quality Section
NC DENR - Asheville Regional Office
1 of 1 4/13/2006 1:14 PM

Agfa Corporation
P.O. Box 267
Staton Road
Brevard, NC 28712-0267
To: Kerry Becker, State of North Carolina, NCDENR Ashville Region NPDES
From: Chet Meinzer, AGFA Brevard Site Manager
CC: Roger Galloway, Jamie Vanbuskirk, Michael Gell, David Epps
Date: 8/26/2004
Re: WWTP Closure NPDES Permit # NC0000337
Wastewater treatment plant closure
We have attached an engineering drawing of the temporary piping changes required as a first step to
begin dewatering our wastewater treatment facility. We request that you issue a letter approving the
temporary piping modifications so that we may proceed with the closure. During the closure of the
AGFA Brevard Plant wastewater treatment system the site is proceeding with the following steps to
ensure the quality of the surface water discharges to Little River.
• The site has stopped all sanitary flows to the WWTP and is providing portable (Porta -
john) sanitary units for construction crews. In addition, the guardhouse and CTC office
building are connected to a septic system with drain fields.
• All production facilities are currently shutdown and being dismantled. No further
process wastewater will be discharged to the existing wastewater treatment plant.
o All flushing water used to rinse underground sewer lines will be treated and
discharged at outfall 001.
• We have attached an engineering drawing for the piping changes needed to complete
the closure of the wastwater treatment plant. (D&Z Temporary Pump & Piping For
Process Wastewater Pond Closing; drawing # Al000449 Rev.A.)
o The redirecting of flows within the system will provide a mechanism for
discharging the treated water at outfall 001. All of the water discharged during
the closure will meet the current NPDES permit limits.

• The site currently monitors the groundwater down gradient of the WWTP basins. The
site will continue the current monitoring and schedule until the NPDES permit is
i terminated or transferred. The monitoring will then be conducted under the site
corrective action plan and schedule being developed in conjunction with the state
groundwater and corrective action groups.
o The down -gradient monitoring wells (R87 series, MW-108, 109,207,
208,209,210) are shown on the attached DuPont CRG - SWMU 4 pdf file.
• The biosolids dewatering process will be closed loop within the treatment plant area
and all water discharged from the system will meet the NPDES permit limits.
o The removed solids will be landfilled in a Sub -title D facility.
• The solids remaining in the aeration and biosolids digestion basins after the dredging is
complete will be sampled for the 503 and appropriate RCRA Appendix IX constituents.
o An estimate of the mass of biosolids remaining will be made for calculation of
constituent loadings being applied to the area during final grading.
The water in the polishing pond will be discharged at outfall 001 and any water that cannot be directly
discharged will be pumped to the emergency basin and processed through the clarifier for direct
discharge to outfall 001.
• The sediments remaining in the polishing pond will be capped with a textile mat and a
two -foot cover of soil. Responsibility and management of this SWMU (solid waste
management unit) will pass to the RCRA corrective action plan.
• The final grade will be low maintenance cover that will support light vehicular traffic and
have a meadow like appearance.
The stormwater currently passing through the wastwater treatment facility will be managed under the
plant Sediment and Erosion Plans as part of the final grading contract.
The Emergency Diversion basin sediments will be removed after all the water in the system has been
successfully treated and discharged.
• After the sediments are removed and sent to an appropriate landfill the area will be
sampled for the RCRA Appendix IX constituents of interest in that area.
As the closure progresses the site will provide timely and informative updates to the State agencies
involved in the process. The updates will list milestone activities.
Sincerely,
i
Chet Meinzer
0 Page 2

$
M-131
/

To:
Kerry Becker, State of North Carolina, NCDENR Ashville NPDES
Agfa Corporation
From:
Chet Meinzer, AGFA Brevard Site Manager
P.O. Box 267
Staton Road
CC:
Roger Galloway, Jamie Vanbuskirk, Michael Gell
Brevard, NC 28712-0267
Date:
5/6/2004
Re:
Modifications to NPDES Permit # NC0000337
Proposed Permit Modifications NC 0000337
During the closure of the AGFA Brevard Plant wastewater treatment system the site requests the
following modifications be permitted under the current permit for the management of dewatering
filtrates and stormwater influents to the basins.
• Installation of a temporary effluent line from the clarifier overflow to the outfall flume.
The water discharged will be sampled under the conditions and limitations of the
existing permit. This process will include sealing the clarifier discharge to the polishing
pond and sealing the overflow from the polishing pond to outfall 001.
• Install a temporary pump and line from the existing emergency spill basin to the existing
clarifier to manage filtrates and stormwater for discharge to outfall 001. After all process
water has been treated the line from the emergency spill basin pump station to the
equalization -settling section of the aeration basin will be sealed.
• Install a temporary pump and line from the polishing pond to the existing sewer line for
management of the decanted water from the polishing pond and stormwater collected
in the polishing pond.
We have attached a sketch of the temporary piping changes requested and ask that you approve the temporary
modifications so that we may proceed with the closure plan. As part of the plan we will be removing the majority
of the solids from the aeration and sludge digestion basins. Sediments will also be removed from the emergency
spill basin and transported to an appropriate Subtitle - D landfill.
The sediments in the polishing pond are currently being evaluated and an appropriate disposal pathway will be
developed in concert with the NCDER divisions.
1
Sincerely,
Chet Mein er
n E :04
LSLJ
WACTION
ASHEL OFFICE

Brevard Plant Closure Piping modifications
Green for temporary new lines & pumps
Red for temporary valves & plugs
Emergency Spill Basin
Clarifier
�M-=
polymer addition
Sludge Return
Sanitary
Wastewater
Aeration
EQ
Sludge
Digestion
Emergency
Spill Basin
Pump
1200 GPM
Eq & Settling /
Lime Phosphoric addition I
Process
Sewers
Clarifier overflow to
Polishing pond
Polishing Pond
4.5 MG