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NC0056928_GroundwaterCompleteFileC_02052019
I HaRnsa CA C/) s��=� o g0 -i8 o�0 Na -''® -CD Ua ?<� Zan w 0 :3 CL 30CL 0�z�� 0. a O a m -n -n ,. W 0N Ngo On d CL3 O ip COD W m to O 3 — w c CD 33 33333353 003 `► `� Cocflc;cn(acmco =cn 3 3 a c r. :CII Ip CD c O' C2 SD 2)7;:7- 2� co t 0 Q. 03 M CDn O� 3 3 �'N C ZO 03 42 �0333c�_�O m CD 0 3 sv cn c �3 0) �wUZ — Z n' I z O m CL c� a p, = m 3 333333cl cQ cn c� cn � cfl cn cQ � a CL ODN13r I` .. 3 =3CcD —. c 3 N r— Z -< w(D .0CD � CA Z o O I3 m C a � N w 7 cx 0 n m w : 1 1 1 1 a 3 3 3 3 KV r AaceAna1ytjca1' www. pacelabs. corn i Pace Sample No: 93718773 Client Sample ID: W5 Pace An,6 980 Kim ,, Hun�e�s, Phone /104.0, Fax 704 81.5 x, DATE: 11/30/00 PAGE: 3 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Date Collected: 11/15/00 Matrix: Water Date Received: 11/15/00 Parameters Resutts Units PRL APP OF Analyzed Analyst CAS# Footnotes -------- ----- GC Volatiles GC VOCs in Water ND Method- SM 6230D ug/L 0.5 1.00 Prep Method: SM 11/29/00 MAG 6230D 75-71-8 Dichlorodifluoromethane ug/l 0.5 1.00 11/29/00 MAG 74-87-3 Chloromethane Vinyl Chloride ND ND ug/t 0.5 1.00 11/29/00 MAG 75-01-4 Bromomethane ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 74-83-9 75-00-3 Chloroethane Trichlorofluoromethane NO ND ug/l ug/l 0.5 1.00 11/29/00 MAG 75-69-4 1,1-Dichloroethene ND ug/L 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 75-35-4 75-09-2 Methylene Chloride trans-1,2-Dichloroethene ND NO ug/L ug/l 0.5 0.5 1.00 11/29/00 MAG 156-60-5 1,1-Dichloroethane ND ug/L 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 75-34-3 156-59-2 cis-1,2-Dichloroethene ND ug/l ug/L 0.5 1.00 11/29/00 MAG 74-97-5 Bromochloromethane NO NO ug/l 0.5 1.00 11/29/00 MAG 67-66-3 Chloroform 2,2-DichLoropropane ND ug/L 0.5 1.00 11/29/00 MAG 594-20-7 107-06-2 1,2-Dichloroethane ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 71-55-6 1,1,1 -Trichloroethane NO ND ug/L ug/L 0.5 1.00 11/29/00 MAG 563-58-6 1,1-Dichloropropene Carbon Tetrachloride NO ug/l 0.5 1.00 11/29/00 MAG 56-23-5 Dibromomethane ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 74-95-3 78-87-5 1,2-Dichloropropane ND NO ug/L ug/L 0.5 1.00 11/29/00 MAG 79-01-6 Trichloroethene Bromodichloromethane ND ug/l 0.5 1.00 11/29/00 MAG 75-27-4 cis-1,3-Dichloropropene ND ug/L 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 10061-01-5 10061-02-6 trans-1,3-Dichloropropene ND ND ug/L ug/t 0.5 1.00 11/29/00 MAG 79-00-5 1,1,2 -Trichloroethane ug/t 0.5 1.00 11/29/00 MAG 142-28-9 1,3-Dichloropropane ND NO ug/l 0.5 1.00 11/29/00 MAG 124-48-1 Dibromochloromethane NO ug/l 0.5 1.00 11/29/00 MAG 106-93-4 1,2-Dibromoethane NO ug/l 0.5 1.00 11/29/00 MAG 127-18-4 Tetrachloroethene 1,1,1,2 -Tetrachloroethane ND ug/l 0.5 1.00 11/29/00 MAG 630-20-6 Chlorobenzene ND ug/L 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 108-90-7 75-25-2 Bromoform 1,1,2,2 -Tetrachloroethane ND ND ug/l ug/t 0.5 1.00 11/29/00 MAG 79-34-5 1,2,3-Trichloropropane ND ug/L 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 96-18-4 108-86-1 Bromobenzene NO ug/l 0.5 1.00 11/29/00 MAG 95-49-8 2-ChLorotoluene ND ug/L Lab°ratDry Certification IN REPORT OF LABORATORY ANALYSIS Lib rat r ertificatio NC Wastewater 12 KY Drinking Water090 NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 Pace Allo, 91300 Kiirch__ Humes. P10oll1 1-04.i,. DATE: 11/30/00 PAGE: 4 Pace Project Number:' 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718773 Date Collected: 11/15/00 Matrix: Water Client Sample ID: W5 Date Received: 11/15/00 Results Units PRL App. of Analyzed Analyst CAS# Footnotes Parameters ---------- -------- ------- 4-Chlorotoluene ---------- ND --------- ug/l 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 106-43-4 541-73-1 1,3 -Dichlorobenzene ND ND ug/L ug/l 1 1 1.00 11/29/00 MAG 106-46-7 1,4 -Dichlorobenzene ND ug/l 1 1.00 11/29/00 MAG 95-50-1 1,2 -Dichlorobenzene 1;2-Dibromo-3-Chloropropane ND ug/t 2 1.00 11/29/00 MAG 96-12-8 1,2,4-Trichlorobenzene ND ug/l 2 2 1.00 1.00 11/29/00 11/29/00 MAG MAG 120-82-1 87-68-3 Hexachloro-1,3-butadiene ND ug/l ug/L 2 1.00 11/29/00 MAG 87-61-6 1,2,3-Trichlorobenzene ND ug/l 0.5 1.00 11/29/00 MAG 1634-04-4 Methyl-tert-butyl Ether ND ND ug/L 0.5 1.00 11/29/00 MAG 108-20-3 Isopropyl Ether ND ug/L 0.5 1.00 11/29/00 MAG 71-43-2 Benzene ND ug/l 0.5 1.00 11/29/00 MAG 108-88-3 Toluene Ethylbenzene ND ug/L 0.5 1.00 11/29/00 MAG 100-41-4 m&p-Xylene ND ug/t 0.5 1.00 11/29/00 MAG 7816-60-0 100-42-5 Styrene ND ug/L ug/L 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 95-47-6 o -Xylene (1,2 -Dimethylbenzene) ND ND ug/L 0.5 1.00 11/29/00 MAG 98-82-8 Isopropylbenzene (Cumene) ND ug/l 0.5 1.00 11/29/00 MAG 103-65-1 n-Propylbenzene 1,3,5-Trimethylbenzene. ND ug/l 0.5 1.00 11/29/00 MAG 108-67-8 tert-Butylbenzene ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 98-06-6 95-63-6 1,2,4-Trimethylbenzene ND ug/t ug/L 0.5 1.00 11/29/00 MAG 135-98-8 sec-Butylbenzene ND ND ug/L 1 1.00 11/29/00 MAG 99-87-6 p-isopropyttoluene 1.4 ug/L 1 1.00 11/29/00 MAG 104-51-8 n-Butylbenzene ND ug/l 2 1.00 11/29/00 MAG 91-20-3 Naphthalene 1-Chloro-2-fluorobenzene (S) 75 % 1.00 11/29/00 MAG 348-51-6 Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS KY o ware ifi�ati9r NC Wastewater 12 This report shall not be reproduced, except in full, TN UST List NC Drinking Water 37706 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 Sc 99006 C5 m x X z x N x x O a n a w O .w a a z z 0 0 C 3 T y 0 d z 5 o 0 x r 0 0 oC A n a o O �. 7 ❑. R o m H x o n �. o m 7 gL 0 V 'P N C rn V 13 fn (n cn cn E iA rn o y 7 n n O C O � A n d n y c 0 N S o x o� n: o O uli V x (n V �° m a o 0 CC C oW 9 B 9 w is in 9 B 9 3 9 3\ 9 r 3 3 oq r r r r r r o 7 00 C5 m x X z x N x x O a n a w O .w a a z z 0 0 C 3 T y 0 d z 5 o 0 x r 0 0 oC A n a o O �. 7 ❑. R o m H x o n �. o m 7 gL 0 V 'P N C rn V o� (n cn cn t�ii iA rn o y 7 n n O C O � A n d n n m c 0 N o� o O V (n V CC C 3 9 B 9 9 9 B 9 3 9 3\ 9 r 3 3 oq r r r r r r 7 3 N C5 m [ � m w z z N x x O a n a w O N a a d a z c tm z 5 0 N r 0 0 oC X o O �. 7 ❑. R o m H x n �. o m 7 gL 0 V 'P N C rn V o� (n cn cn t�ii iA rn y 7 n n O C O � A n d n n m O V (n V CC C r r r C5 m [ � m w n• ^`7 ^"y Z m n n E C o a O a z O O °p d a z c tm z 0 N r 0 0 X o O �. S o x n �. o m 7 gL 0 A N y 7 n n O C O � A n d n n m C5 m [ � m w n• ^`7 ^"y Z m n n E C a O a .. O W °p d a z c tm z N r x O � c m w n• ^`7 ^"y Z m n n E C e O W l X > v v v m A n c zp ........ c 3 n S m 0 n o Z D O N(n N :9 W CL Z 3 0+ O o cn cn cn -a S S 2 v n O o o O Q o D v 3 C -h C-0 D ° m ° - I w Zcz, o Q p -pi �c p �c p p N + 0 N' a 6 n i p O- v v p co y` 3 ° N 3 l0 O- 3 (0 Od U1 0 N p Z Z y 3 m- cin A 0m 00 3 3 w s 3 > 4 rn r m 3 rn A p 0, w M 0 X •p Ja O O o' .A s N V O' P O wLm w 0, Z � N �' N Ul. C.1 3, c z. O rn O 3 O_ 0 v v 01 � �Ul v to l4 todc 03 T T n %O ? O y D V N ^ -mss < cm :E Zm O S 2 p m C p o a 0 o m W W O C m r H C m m m C to C to C m m m m m N Ul m w Lin p a. N N crO in o o O (0 N D N 3 3 3 3 3 3 3 c,p s 3 3 o coo Ln a coI I I O 3 N C% C -� p� W D O, (T 0 N o %0 %O A C O '1 �S s N my o O LM S n � C1 C 0 v S Q O G p = — w 3 A 3 O (0 N C -� cn °a m 0 v O O N m O Ln O vi n F � 3 c H 3 v N 3 N O _ Ln cn s 0 y -r hx X p O N N N ° g -3 m f< m 3. m 3 R % Q n -n+ s m m 0 v n L m 0- n v n -+ N 0 0 0N 3 m 0 c N vO v a r q VI q N Z v N 3 n S m 0 n o Z D O N(n N :9 Z -1 Z 3 0+ O � �-+ cn cn cn -a S S T v n co O Z _ W ° 3 o t°i = 'o 3 C -h C-0 n n p d p C O y H .P p N + 0 N p m 3 in C p O- 1p p co y` 3 ° N 3 l0 O- 3 (0 Od U1 0 N Q Z Z y 3 m- cin A n p H N'0 3 0_ 4 •P 3 rn A 3 0, v w Uri •p rn N aLyl o' .A s P O CNn O 0, •N � N 0 N U C.1 N o o� Lp O Z 01 � �Ul to l4 todc 03 O %O y V N 3 m lC m < cm a p p CC U3 m W W O C m 3 m C m m m C to C to C m m m m m O m m p N crO O (0 N D N 3 3 3 3 3 3 3 c,p 3 3 3 3 m m m m m Lo m \Lo to U3 to O Ed A Ln a coI I I O 3 N C% C -� p� W D O, (T 0 N o %0 %O A C O '1 �S s N my o O LM S n � C1 C 0 v S Q O G p = — w 3 A 3 O (0 N C -� cn °a m 0 v O O N m O Ln O vi n F � 3 c H 3 v N 3 N O _ Ln cn s 0 y -r hx X p O N N N ° g -3 m f< m 3. m 3 R % Q n -n+ s m m 0 v n L m 0- n v n -+ N 0 0 0N 3 m 0 c N vO v a r --0 Z p� 3 n S m 0 n o Z D O N(n N cn ? 3 0+ � �-+ c� i fl o Q o y a a �o �' n co 0 x Ln ° °- ° 3 o t°i 'o 3 v o a 3 n E N 'o �o .P C• C p m 3 in C C V �. C• 3 3 C 3 Ol rn 0 C y 3 m- cin A 3 3 p v 3 rn 4 •P 3 rn A 3 0, v w Uri •p rn Lm aLyl o' .A s 0 0 LM CJI 0, •N � �O 00 0 N U LM UI N OD rte+ Lp O' 01 � �Ul to l4 todc 03 O %O y V N 3 m lC m < cm a N CC U3 m C m C m 3 m C m m m C to C to C m m m m m m m m Ln a coI I I O 3 N C% C -� p� W D O, (T 0 N o %0 %O A C O '1 �S s N my o O LM S n � C1 C 0 v S Q O G p = — w 3 A 3 O (0 N C -� cn °a m 0 v O O N m O Ln O vi n F � 3 c H 3 v N 3 N O _ Ln cn s 0 y -r hx X p O N N N ° g -3 m f< m 3. m 3 R % Q n -n+ s m m 0 v n L m 0- n v n -+ N 0 0 0N 3 m 0 c N vO v a r o v m v m 0 n Z O O 7 O O �0 'o 0 ffi X 0 C m- v 0 o S 0 3 m to o s 0 0 c 0 m o rn ^ a to l4 todc 03 y N 3 m lC m < N O Ul A p N crO (0 D N Ln a coI I I O 3 N C% C -� p� W D O, (T 0 N o %0 %O A C O '1 �S s N my o O LM S n � C1 C 0 v S Q O G p = — w 3 A 3 O (0 N C -� cn °a m 0 v O O N m O Ln O vi n F � 3 c H 3 v N 3 N O _ Ln cn s 0 y -r hx X p O N N N ° g -3 m f< m 3. m 3 R % Q n -n+ s m m 0 v n L m 0- n v n -+ N 0 0 0N 3 m 0 c N vO v a r v m v c 0 o < v m 1 J� :71"- P_ 3 o r 0 0 p v OO (Nn S C7 v � O G S O C O !l+ 3 'n 3 O m C r m c (np i _< m c m 0 0 y 3 o c a v ^ .M 0 m 3 EA t0 $ 3 m ^ 3 O En m p N C Ln X + _n � 3 m v m La3 2. cm m 3 m 3 i 0 S O m 3 *r S m m m 0 y m 3 3 v v O p v o o m p m a m Z c p - m 6 p c NV Ir T _ 3 O' Z G 'a f0 H 3 m S f0 O '• p x q N x xD Z -i Z o c O O z.. c( (1 QW a m v o T v, -F 3 Z CF c C% t0 C7. D D "a 7v --� -j !7 f� f� f� p D 3 p o N N v o{ Q -t w Z m_ s s p n p a = o m e On o o O O D �� D ti Q Z --1 to o S 3 0 o v a n C7 o a s o c v v w Oi y' 'V y N ' S A mp W . -.a 3 0 3 3 3 W aOD - , - S p Ol p M(Il m O � " Cn m m o_ o +- v X 0 3 3 F s 6= LM (n D N A= o X m m - O O rn T T.91 W WZ C to rn(n N C tp , � a Q W p c 00 .A v v LM � O * - i+ x O m S o m O o w m o n Vii 0 N A< 3 3 w 3 3 a 3 3 r c 3 3 3 3 m to to tp N LM o ��, W w W o. � — (Jl LO I- O n0 tp I- I I S m a I I f 'T1 ---I 0 O rn r w H s r ms n. fly C ,J v N oZ p 3 3 t\ 3 t\ 3 t\ 3 t\ 3 3 t\ 3 2 33 \ C t\ O O 3 3 t\ t\ n o -�. a W c n p rn cn W w LM N I'a %O 10 O C Q y, 3 o r 0 0 p v OO (Nn S C7 v � O G S O C O !l+ 3 'n 3 O m C r m c (np i _< m c m 0 0 y 3 o c a v ^ .M 0 m 3 EA t0 $ 3 m ^ 3 O En m p N C Ln X + _n � 3 m v m La3 2. cm m 3 m 3 i 0 S O m 3 *r S m m m 0 y m 3 3 v v O p v o o m p m a m Z c p - m 6 p c NV Ir T 3 O' Z G 3:tq 3 m C 7 a c p N q N 7 Z -i Z o c O O z.. c( (1 v s f7 S S T v, -F 3 p Z W y p 3-0 y' fl n 3 Q In d c o N N rn G Z N N m_ m 3 3 CO m 3_N O m N N a O cn C), ti Q Z Z -3 S tun a n C7 N '•"- y m t0 Cn 'V WLM N Q` m rn A mp W ? •A (M Lnn N 3 C tou a ti N Ol p M(Il m O � " Cn m m O 3{ v O Co C N Ol Ul LM (n N ID a w m m C tp C tp Ol W C to C to 3 C to C tp C is C m C tp C tp p c 00 to S � O m O O 0 N m 3 3 3 3 3 3 3 c c 3 3 3 3 to to tp to ka q tp � to , � — tp LO I- m �:: tp I- I I I I I I f iLL ---I n 3 o r 0 0 p v OO (Nn S C7 v � O G S O C O !l+ 3 'n 3 O m C r m c (np i _< m c m 0 0 y 3 o c a v ^ .M 0 m 3 EA t0 $ 3 m ^ 3 O En m p N C Ln X + _n � 3 m v m La3 2. cm m 3 m 3 i 0 S O m 3 *r S m m m 0 y m 3 3 v v O p v o o m p m a m Z c p - m 6 p c NV Ir T 3 O' Z G 3:tq 3 m C 7 a c p N m co fl Z' o o c O tp 'H z.. A ° (1 n G. f7 W D 7-- D cn -F 3 p n y = 3-0 o O 3C m m -3 m rn 3 A 3 m_ m 3 3 3_N 3 rn cn C), tun ? Q -3 S tun a 0, o, to y O, � Cn O1 U m rn A „V,, �o W Cu71 N 'p (M Lnn N m to CM tou N OLo m r%n3 � " Cn to m p v Co C N m Ea LM (n N m m C tp C tp C tp C to C to 3 C to C tp C is C m C tp C tp C tp c C m 3 o r 0 0 p v OO (Nn S C7 v � O G S O C O !l+ 3 'n 3 O m C r m c (np i _< m c m 0 0 y 3 o c a v ^ .M 0 m 3 EA t0 $ 3 m ^ 3 O En m p N C Ln X + _n � 3 m v m La3 2. cm m 3 m 3 i 0 S O m 3 *r S m m m 0 y m 3 3 v v O p v o o m p m a m Z c p - m 6 p c NV Ir T S= o 3 n n Z O O = °O n o a ao 4l -F p < o y = �p o 0 n Q S S S 3 p O N OLo m r%n3 to to m p Co C N m Ea Q N m m p to S N m O O m 3 o r 0 0 p v OO (Nn S C7 v � O G S O C O !l+ 3 'n 3 O m C r m c (np i _< m c m 0 0 y 3 o c a v ^ .M 0 m 3 EA t0 $ 3 m ^ 3 O En m p N C Ln X + _n � 3 m v m La3 2. cm m 3 m 3 i 0 S O m 3 *r S m m m 0 y m 3 3 v v O p v o o m p m a m Z c p - m 6 p c NV Ir T 0 C zr O N CD i p� CD m 2 C0 m m O 05 C m z 0 C m Z 0 m 0 O AQ1 y N G. O TL 0 '' �a n �OS-a a. -0 C w -O Qpnym Qw o O— p p Q 0 O� O n -n � o i 33�3333333c3 003 cc cc O cQ to cn cQ cc c0 cQ cc 3310 zKK;rll=TOOROwD3z`Z CD CD K K0 CO RE-00WCO--Z c�� �j�833E'3' .(ZO) 3 m 42 W. �D33 03 3 N0 ZZ w R O 33333333333333`3 c0(a(a(aca(accc0cacQcn(a(0c0(a � m CT �.En NrOz o CDU) O Q -m 3 o m C -s C 0 Q 1:Zt ' c r, -2 014 c .c c � °B cn c0 c0 c0 c0 r p �tC N Q n C*—D C�D CCD cnDN 4ao "' o cQ a: 0 w O mo-o`�y� � ti� .1 w (D 3,D o P- g % .43 ci cD o � lir 3 CD 3 C1 lr p `Q c Ul Lk cn ZD- cD — cD DC O l O CD o OL a �O a o p► z O D a) 0 w m 20 0 CIO s E cr c 3 O O im CL D� Q Z a P, CD 4 -a - m DO z C: K co m �o M D c m v Pace Anay, /� 9800 Kincey AvL,. ce Analytical Huntersville;,, Pace Sample No: 93419463 Client Sample ID: W5 Tel: 704-875=5, Fax: 704 -875 -9091 - DATE: 12/09/99 PAGE: 3 Pace Project Number: 9210415 Client Project ID: James&James-939533 Date Collected: 11/29/99 Matrix: Water Date Received: 11/30/99 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane ND ug/l 0.5 1.00 12/08/99 KST 75-71-8 Chloromethane ND ug/l 0.5 1.00 12/08/99 KST 74-87-3 Vinyl Chloride ND ug/L 0.5 1.00 12/08/99 KST 75-01-4 Bromomethane ND ug/1 0.5 1.00 12/08/99 KST 74-83-9 Chloroethane ND ug/l. 0.5 1.00 12/08/99 KST 75-00-3 Trichlorofluoromethane ND ug/t 0.5 1.00 12/08/99 KST 75-69-4 1,1-Dichloroethene ND ug/l 0.5 1.00 12/08/99 KST 75-35-4 Methylene Chloride ND ug/L 0.5 1.00 12/08/99 KST 75-09-2 trans-1,2-Dichloroethene ND ug/l 0.5 1.00 12/08/99 KST 156-60-5 1,1-Dichloroethane ND ug/l 0.5 1.00 12/08/99 KST 75-34-3 cis-1,2-Dichloroethene ND ug/l. 0.5 1.00 12/08/99 KST 156-59-2 Bromochloromethane ND ug/L 0.5 1.00 12/08/99 KST 74-97-5 Chloroform ND ug/t 0.5 1.00 12/08/99 KST 67.66-3 2,2-Dichloropropane ND ug/L 0.5 1.00 12/08/99 KST 594-20-7 1,2-Dichloroethane ND ug/l 0.5 1.00 12/08/99 KST 107-06-2 1,1,1 -Trichloroethane ND ug/t 0.5 1.00 12/08/99 KST 71-55-6 1,1-Dichloropropene ND ug/1 0.5 1.00 12/08/99 KST 563-58-6 Carbon Tetrachloride ND ug/L 0.5 1.00 12/08/99 KST 56-23-5 Dibromomethane ND ug/l 0.5 1.00 12/08/99 KST 74-95-3 1,2-Dichloropropane ND ug/t 0.5 1.00 12/08/99 KST 78-87-5 Trichloroethene ND ug/1 0.5 1.00 12/08/99 KST 79-01-6 Bromodichloromethane ND ug/l 0.5 1.00 12/08/99 KST 75-27-4 cis-1,3-Dichloropropene ND ug/1 0.5 1.00 12/08/99 KST 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.5 1.00 12/08/99 KST 10061-02-6 1,1,2 -Trichloroethane ND ug/1 0.5 1.00 12/08/99 KST 79-00-5 1,3-Dichloropropane ND ug/l 0.5 1.00 12/08/99 KST 142-28-9 Dibromochloromethane ND ug/t 0.5 1.00 12/08/99 KST 124-48-1 1,2-Dibromoethane ND ug/l 0.5 1.00 12/08/99 KST 106-93-4 Tetrachloroethene ND ug/1 0.5 1.00 12/08/99 KST 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/l 0.5 1.00 12/08/99 KST 630-20-6 Chlorobenzene ND ug/t 0.5 1.00 12/08/99 KST 108-90-7 Bromoform ND ug/t 0.5 1.00 12/08/99 KST 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/l 0.5 1.00 12/08/99 KST 79-34-5 1,2,3-Trichloropropane ND ug/l 0.5 1.00 12/08/99 KST 96-18-4 Bromobenzene ND ug/l 0.5 1.00 12/08/99 KST 108-86-1 2-Chlorotoluene ND ug/L 0.5 1.00 12/08/99 KST 95-49-8 Laboratory Certification IDs Laboratory C erl fiCatlon IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS Drinking Water 90090 TN NC Drinking Water 37706 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analy, 9800 Kincey Avt,. A n n l Vt 1[_ A l Huntersville Tel: 704-875 Fax: 704-875-909) DATE: 12/09/99 PAGE: 4 Pace Project Number: 9210415 Client Project ID: James&James-939533 Pace Sample No: 93419463 Date Collected: 11/29/99 Matrix: Water Client Sample ID: W5 Date Received: 11/30/99 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes --------------------------------- 4-Chlorotoluene ---------- ND --------- ug/1 ---------- 0.5 1.00 12/08/99 KST 106-43-4 1,3 -Dichlorobenzene ND ug/1 1 1.00 12/08/99 KST 541-73-1 1,4 -Dichlorobenzene ND ug/l - 1 1.00 12/08/99 KST 106-46-7 1,2 -Dichlorobenzene ND ug/l 1 1.00 12/08/99 KST 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/l 2 1.00 12/08/99 KST 96-12-8 1,2,4-Trichloro,benzene ND ug/L 2 1.00 12/08/99 KST 120-82-1 Hexachlorobutadiene ND ug/l 2 1.00 12/08/99 KST 87-68-3 1,2,3-Trichlorobenzene ND ug/l 2 1.00 12/08/99 KST 87-61-6 Methyt-tert-butyl Ether ND ug/l 0.5 1.00 12/08/99 KST 1634-04-4 Isopropyl Ether, ND ug/l 0.5 1.00 12/08/99 KST 108-20-3 Benzene ND ug/l 0.5 1.00 12/08/99 KST 71-43-2 Toluene ND ug/L 0.5 1.00 12/08/99 KST 108-88-3 Ethylbenzene ND ug/1 0.5 1.00 12/08/99 KST 100-41-4 m&p-Xylene ND ug/l 0.5 1.00 12/08/99 KST 7816-60-0 Styrene ND ug/l 0.5 1.00 12/08/99 KST 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/1 0.5 1.00 12/08/99 KST 95-47-6 Isopropylbenzene (Cumene) ND ug/l, 0.5 1.00 12/08/99 KST 98-82-8 n-Propylbenzene ND ug/L 0.5 1.00 12/08/99 KST 103-65-1 1,3,5-Trimethylbenzene ND ug/1 0.5 1.00 12/08/99 KST 108-67-8 tert-Butylbenzene ND ug/1 0.5 1.00 12/08/99 KST 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 1.00 12/08/99 KST 95-63-6 sec-Butylbenzene ND ug/L 0.5 1.00 12/08/99 KST 135-98-8 p-isopropyltoluene ND ug/L 1 1.00 12/08/99 KST 99-87-6 n-Butylbenzene ND ug/L 1 1.00 12/08/99 KST 104-51-8 Naphthalene ND ug/1 2 1.00 12/08/99 KST 91-20-3 1-Chloro-3-fluorobenzene (S) 104 % 1.00 12/08/99 KST 625-98-9 Laboratory Certification ID Laboratory Certification IDs N DUST List water 9009 NC Wastewater 12 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37706 VA Drinking Water 213 SC 99006 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. r -j bona' 7 k % k m a z Nn nnam k > y v. eW 0 .. 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M (aO � a N A A (D CL W Cd n .� o 3 W a �o W a 0 D rn L= 3 C) c 3 3 3 3 3 3 c 3 z 3 0 0 3 3 3 h vz z O cntncn v22�0 o O = m c C w �� ? w o. w° o. c v; y w+ w a a C _ o c w w a cn oz N y w co (Dp rn w Ca71 In O 0 O N) W O O � y �4 M PL a CA Z �`°" m m c w a' o o co N 3 B 3 3 3 3 y c 3 3 3 Nfn'v z z T.2-nC)nnC)w>>> o (D Cr -` w O to (D c o w w y N to o ? C) a _ a (D (D n— o � 0 o O w d v �' c 3 = vwyi o O C f° Obi U1 7 y. `� 0 w a c 3 c• 3 3 I acn v 4m pAj y (D c 3 a M (n cf v' A A A o IM oai Q1i, � rn rn cn W W N c m N M CD N CD CWJ1 cm C71 C V M cn A c c c 3 c 3 3 c c c c c'3 c c c c 0 Z O O M 2= M 0 m = (D A a o 3 w G) (D 0o y m o 0 -► as O XOAw n w y° — m O o. a D)L� W CD O to y n0 (D < w O y (D i0 o yn' w m D y n: Oi 0 �j y (D (p CL (D w DR) In mm 3 c m v w - m w r- -m > m n a z Dm- mA taco mo ?cn� IOD c -0o 0> r -m bo CL co o D<o D � o w .. Qy DZ � o � CO Ig 0 c n � � D cn cn Ik Z = -n o D^^° `D O ^^ `D C1 li 1. �w 1 7 C' C7 ` c O m c� a Q (A0,6 A m m O O 0 - O m ID p p 5.3 o p -° -44 n � 3 3 p 0 p co cD x 5 �. M (aO n CL 3 n .� 3 a �o 0 D L= DR) In mm 3 c m v w - m w m m n a z mrc IOD c o co CD3 C � y � O CD c 1 7 C' CL c� vv -v <m z3 fD 0a Dm MS z woo JO y D (D -% <� Q �? o Zo.o 0 Z 0 Dc -4 mm N M 0 o m Zy -I CD C/) -0 qv o —ro 0-2 0 0 0 �o� c ��, =02�; 0 0 0 0 Z� 0 v CD 2) C7^ cn m =•: p 3 0 o CD CD CD 3 Z�� CL So -n -n .Q 0 —m "yCA N0CD CLm n CL � � CD ? to — � r cr CL 3 A m A C 33�33�333�3 003 �. co co o co ca ca co co cc ,_. ca 3 3 ca a c 3 ���2-nc�c�c�c�o»O'aZZ r(aCDC�QSVSv`,CL ��......:�p W ca C CD o 0 �• iv A� C C? 9^ CaQ c." �'0 Q�•a �•� I Z0 0)CDa� o..3c3��a0" -< � c3`c �0�3 3-��M cD�— N �ZZ CAo .D Z O 00 G. m T �D rn C. m 33 33333333a ca to ca co ca ca to n• a <MN O ODN o•? O CD 3 O A+n CD 3N r- ? -C am .� o —• 0 • m cn n x. n CD sun0CD n Z C. Q• si o C I � 43 0 CD nCD 0 3 3 Ca CL CL CO 7 O y 7• �. 5 2 7 aC.n. `D� a v� n 86 n n u Q o 0 1: Who 1 3 O 3 3 r I C oa � c3333 `� v Pace Analytical'., 54 Ravensct, Asheville, NC 26. Tel: 704-254-7176 Fax: 704-252-4618 DATE: 11/17/98 PAGE: 3 Pace Project Number: 931990 Client Project ID: Kenmure Monitoring Wells Pace Sample No: 9392267 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE W5 Date Received: 11/03/98 Parameters --------------------------------- Results Units ------------------- PRL ---------- Analyzed -------- Analyst CAS# ----- ---------- Footnotes ---------- Field Services Monitoring Well Data Method: Prep Method: Field pH 5.1 Std. Units 11/03/98 MPS Field Temperature 17 deg C 11/03/98 MPS Depth of Water 8.16 feet 0 11/03/98 MPS Well Volume Purged 1.50 No units 0 11/03/98 MPS Wet Chemistry Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1 Total Dissolved Solids 53 mg/L 1 11/06/98 MAA Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3 Chloride 5.4 mg/L 1 11/12/98 JGJ Ammonia Method: EPA 350.3 Prep Method: EPA 350.3 Nitrogen, Ammonia ND mg/L 0.1 11/06/98 KMH 7727-37-9 Nitrogen, Nitrate Method: EPA 352.1 Prep Method: EPA 352.1 Nitrogen, Nitrate 0.62 mg/L 0.1 11/05/98 TRW Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060 Total Organic Carbon 3.4 mg/L 0.5 11/12/98 KEK 7440-44-0 Fecal Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Fecal Coliform <1.1 1 11/03/98 MLP Total Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Total Coliform <1.1 1 11/03/98 MLP Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical 9800 Kincey Avenue, Analytical Huntersville, NC k' Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 3 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186642 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE - W5 Date Received: 11/04/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ----------------------------- -------- --------------- ---------- GC -- Volatiles Halogen. & Aromatic Vol. Orgs. Method: SM 6230D Prep Method: EPA 8021 Dichlorodifluoromethane ND ug/L 0.5 11/13/98 CLL 75-71-8 Chloromethane ND ug/L 0.5 11/13/98 CLL 74-87-3 Vinyl Chloride ND ug/L 0.5 11/13/98 CLL 75-01-4 Bromomethane ND ug/L 0.5 11/13/98 CLL 74-83-9 Chloroethane ND ug/L 0.5 11/13/98 CLL 75-00-3 Trichlorofluoromethane ND ug/L 0.5 11/13/98 CLL 75-69-4 1,1-Dichloroethene ND ug/L 0.5 11/13/98 CLL 75-35-4 Methylene Chloride ND ug/L 0.5 11/13/98 CLL 75-09-2 trans-1,2-Dichloroethene ND ug/L 0.5 11/13/98 CLL 156-60-5 1,1-Dichloroethane ND ug/L 0.5 11/13/98 CLL 75-34-3 Bromochloromethane ND ug/L 0.5 11/13/98 CLL 74-97-5 Chloroform ND ug/L 0.5 11/13/98 CLL 67-66-3 2,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 594-20-7 1,2-Dichloroethane ND ug/L 0.5 11/13/98 CLL 107-06-2 1,1,1 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 71-55-6 1,1-Dichloropropene ND ug/L 0.5 11/13/98 CLL 563-58-6 Carbon Tetrachloride ND ug/L 0.5 11/13/98 CLL 56-23-5 Dibromomethane ND ug/L 0.5 11/13/98 CLL 74-95-3 1,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 78-87-5 Trichloroethene ND ug/L 0.5 11/13/98 CLL 79-01-6 Bromodichloromethane ND ug/L 0.5 11/13/98 CLL 75-27-4 cis-1,3-Dichloropropene ND ug/L 0.5 11/13/98 CLL 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.5 11/13/98 CLL 10061-02-6 1,1,2 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 79-00-5 1,3-Dichloropropane ND ug/L 0.5 11/13/98 CLL 142-28-9 Dibromochloromethane ND ug/L 0.5 11/13/98 CLL 124-48-1 1,2-Dibromoethane ND ug/L 0.5 11/13/98 CLL 106-93-4 Tetrachloroethene ND ug/L 0.5 11/13/98 CLL 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 630-20-6 Chlorobenzene ND ug/L 0.5 11/13/98 CLL 108-90-7 Bromoform ND ug/L 0.5 11/13/98 CLL 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 79-34-5 1,2,3-Trichloropropane ND ug/L 0.5 11/13/98 CLL 96-18-4 Bromobenzene ND ug/L 0.5 11/13/98 CLL 108-86-1 2-Chlorotoluene ND ug/L 0.5 11/13/98 CLL 95-49-8 4-Chlorotoluene ND ug/L 0.5 11/13/98 CLL 106-43-4 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY N t DUST List 90090 NC Drinking Water 37706 Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. i ! PaceAnalyticai= 9800 Kincey Avenue, ical Huntersville, NCL-- Tel: 704-875-9092-,, Fax: 704-875-9091 DATE: 11/16/98 PAGE: 4 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186642 Date Collected: 11/03/98 Matrix: Water Client SampLe ID: KENMURE - W5 Date Received: 11/04/98 Parameters Results Units --------- PRL ---------- Analyzed Analyst CAS# Footnotes --------------- ---------- --------------------------------- 1,3-Dichlorobenzene ---------- ND ug/L 0.5 -------- 11/13/98 CLL 541-73-1 1,4 -Dichlorobenzene NO ug/L 0.5 11/13/98 CLL 106-46-7 1,2 -Dichlorobenzene NO ug/L 0.5 11/13/98 CLL 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 0.5 11/13/98 CLL 96-12-8 1,2,4-Trichtorobenzene NO ug/L 0.5 11/13/98 CLL 120-82-1 Hexachlorobutadiene ND ug/L 0.5 11/13/98 CLL 87-68-3 1,2,3-TrichLorobenzene NO ug/L 0.5 11/13/98 CLL 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 11/13/98 CLL 1634-04-4 Isopropyl Ether ND ug/L 0.5 11/13/98 CLL 108-20-3 Benzene ND ug/L 0.5 11/13/98 CLL 71-43-2 Toluene ND ug/L 0.5 11/13/98 CLL 108-88-3 Ethylbenzene ND ug/L 0.5 11/13/98 CLL 100-41-4 m&p-Xylene NO ug/L 0.5 11/13/98 CLL 7816-60-0 Styrene NO ug/L 0.5 11/13/98 CLL 100-42-5 o -Xylene (1,2 -Dimethylbenzene) NO ug/L 0.5 11/13/98 CLL 95-47-6 Isopropylbenzene (Cumene) ND ug/L 0.5 11/13/98 CLL 98-82-8 n-Propylbenzene NO ug/L 0.5 11/13/98 CLL 103-65-1 1,3,5-Trimethylbenzene NO ug/L 0.5 11/13/98 CLL 108-67-8 tert-Butylbenzene ND ug/L 0.5 11/13/98 CLL 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 95-63-6 sec-Butylbenzene ND ug/L 0.5 11/13/98 CLL 135-98-8 p-Isopropyltoluene ND ug/L 0.5 11/13/98 CLL 99-87-6 n-Butylbenzene ND ug/L 0.5 11/13/98 CLL 104-51-8 Naphthalene ND ug/L 0.5 11/13/98 CLL 91-20-3 1-Chloro-3-fluorobenzene (S) 91 % 11/13/98 CLL 625-98-9 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN2 KY Drinking Water 90090 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. 0 n � =rw w �c o � 3 o 0 o Q N C,CD = a x CDA o cn 11 ■ ®m D <Tu -o m s o�� m \ Cl) o 3 r co -° m o 33 > _ --q -it,0n0m O� wo 0o a mac. 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' S m D a m p CD vm, aEn f <I y w m r% ra CO o � Zm V1'nrO 6c: O 'n `-+ b O r O g~ 5 m cD o w w Q D m -4° r m m CL m e 7m:; CD m o l< m LD. 3 o C) c3 cn m p7 m h rD- ''11 l c a 2 „CD w Z m m w t'� Ow Za° i C ` 3 aC Zw w = W -Di o " 3 SS m m In O �_ O -c_+ 0 m o CD O z (A Cal m < m 1 O CD v, CD 3 CD (D o ico co i cc w� m c m Cr (D 3� cX CD O a� C CD A O O m T. 0 O 0 O CL a N w Q (D V-n rm Z 0 CD O 0 O � N O C) = O O O = 0 O' 7 0 "* O Q V) N O cD m ** a CJ 0 O aCL os 7: -I -i Cl) Cn -D 2,. 9 C) �-o z 0 () C) X0-0 C: M =),O =gin ° 000 2) :5 (/) Z) M. h o c 00 Z 3 C7 (n 0_ 0 0-i Q- w (nz0 CD a 0 CD n aoo �� CD Q a N 33 =r3333333:33 003 (Q (Q O CQ (Q (Q (Q (Q (Q (Q CQ 3 3 (Q ZKKT"=M0000w>mZZ 0 W w E CCD O O 3 -www C� N (D O (0 O Q n �- O� z Z W CD c CCD -- C -o 3O 3 c cn ,o CD--3`� 033 30 CD3 —�'Z -Z w c 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 co (Q (Q (Q (Q c0 c0 c0 co c0 (Q cQ cO cQ (0 m C) 0 CD CDCD 0' m 3 O c CL cn w a -ON -UZ CD's 0- �. m ct � 0' O Z o (D n Q. CCD -0 2 O c CD cr CLcn CDC7 Q. c c c 3 (Q (Q (Q CQ (Q (Q �0(DnoCl) °___ D= c� O a r- :3 r w 0 • o w o 0 m° 3 0 0= o w o o mzm�-' '0wCD o 3 a m= ro m o CD _0 CD m 3 m Zc 3 � a C CT cn ,�(n N G y 41� ~�3 m cum 7o a (D m cn C:7 - C) -» en r Q F� o O cr 0 n r CD O O N r 0 w 0 ot m n w CD 0 0 3 CD a I Q�.aw m c cn 0 .� C wM,� z ¢; w (O w rCD _� O p-' -I wD 07 a .. A m mCD m v _ o D CD c m v COD 7 '1I w C -0 O v Q CD 7 t11 r � n v - o00 n �n O mm a o w C) 73z O Z _0 Q CD w I w O 0 Ari -p N CD o w a o ICL v o 0-a �! N CD CL 6 O : 0 c CL n NO O CD m w 0 D� c- z m 3 C'm w M m c0 mmz o -v aFn0 -Vm O� (n D r O M 0 z CA m z O z a c oCD h M �� ov CD �0 r- 0 � w T N CD N a CD 0 m -o m z C: K ou m �o m O c m m v Mr. Harry James Page 3 Client Reference: J&J Kenmore PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units PRL ORGANIC ANALYSIS Pace 9800 Kincey Hun Tel: 704 Fax: 704-871 December 02, 1997 PACE Project Number: A711,, 93 0487718 11/17/97 11/19/97 Kenmore MW W5 METHOD DATE ANALYZED VOLATILE ORGANICS Dichlorodifluoromethane ug/L 0.5 NO 6230D 11/25/97 Chloromethane Chloroethene (Vinyl chloride) ug/L ug/L 0.5 0.5 ND NO 11/25/_97 11/25/97 Bromomethane ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 Chloroethane Trichlorofluoromethane ug/L 0.5 NO 11/25/97 1,1-Dichloroethene ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 Dichloromethane trans-1,2-Dichloroethene ug/L 0.5 NO 11/25/97 1,1-Dichloroethane ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 cis-1,2-Dichloroethene ug/L 0.5 NO 11/25/97 2,2-Dichloropropane Chloroform ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 Bromochloromethane 1,1,1 -Trichloroethane ug/L 0.5 NO 11/25/97 1,1-Dichloro-l-propene ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 Carbon tetrachloride 1,2-Dichloroethane ug/L 0.5 NO 11/25/97 t,A, O richloroethene ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 4,j2 -Da hloropropane Bromo` chloromethane ug/L ug/L 0.5 NO 11/25/97 ,Dibrokðane ug/L ug/L 0.5 0.5 NO NO 11/25/97 11/25/97 cis;-1,� Dichloro-l-propene 'trans-1,3-Dichloro-l-propene ug/L 0.5 NO 11/25/97 11,2 Tt4ichloroethane ug/L 0.5 NO NO 11/25/97 11/25/97 1,3--Di4) oropropane ug/L 0.5 NO 11/25/97 Tetrachloroethene ug/L ug/L 0.5 0.5 NO 11/25/97 Dibromochloromethane ug/L 0.5 NO 11/25/97 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane ug/L 0.5 NO 11/25/97 Bromoform �% ug/L 0.5 NO 11/25/97 ,SAN - I 81998 IDs Laboratory Certification IDs NC Wastewater 12 G e �t �� L ORATORY ANALYSIS I aborato[y c Prtification KY Drinking Water 90090 TN UST List NC Drinking Water 37706 AS e Sc 99006 o _I T �i e This report sha not be reproduced, except in full, VA Drinking Water 213 g without the written consent of Pace Analytical Services, Inc Mr. Harry James Page 4 Pace i1, 9800 Kincey, Huntersu, J Client Reference: J U Kenmore Tel: 704-b Fax: 704-875 December 02, 1997 PACE Project Number: A711, PACE Sample Number: 93 0487718 Date Collected: 11/17/97 Date Received: 11/19/97 Client Sample ID: Kenmore MW Parameter Units PRL W5 METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 6230D 1,1,2,2 -Tetrachloroethane ug/L 0.5 NO 11/25/97 1,2,3-Trichloropropane ug/L 0.5 ND 11/25/97 Bromobenzene ug/L 0.5 ND 11/25/97 2-Chlorotoluene ug/L 0.5 NO 11/25/97 4-Chlorotoluene ug/L 0.5 NO 11/25/97 1,3 -Dichlorobenzene ug/L 0.5 ND 11/25/97 1,4 -Dichlorobenzene ug/L 0.5 NO 11/25/97 1,2 -Dichlorobenzene ug/L 0.5 NO 11/25/97 1,2-Dibromo-3-chloropropane ug/L 0.5 NO 11/25/97 1,2,4-Trichlorobenzene ug/L 0.5 NO 11/25/97 Hexachlorobutadiene ug/L 0.5 NO 11/25/97 1,2,3-Trichlorobenzene ug/L 0.5 NO 11/25/97 Benzen ug/L 0.5 NO 11/25/97 Toluet�t ug/L 0.5 NO 11/25/97 Ch1'oro#enzene ug/L 0.5 ND 11/25/97 Et:hylbiflizene ug/L 0.5 NO 11/25/97 Xy�enes�(total) ug/L 0.5 NO 11/25/97 Styrenec:F Y ug/L 0.5 NO 11/25/97 IsdpropyDenzene ug/L 0.5 NO 11/25/97 n-R.r6pyl benzene ug/L 0.5 NO 11/25/97 1,3,5=Tri4khylbenzene ug/L 0.5 NO 11/25/97 t -Butyl -benzene ug/L 0.5 NO 11/25/97 1,2,4-Trimethylbenzene ug/L 0.5 NO 11/25/97 s-Butylbenzene ug/L 0.5 NO 11/25/97 4-Isopropyltoluene ug/L 0.5 NO 11/25/97 n-Butylbenzene ug/L 0.5 NO 11/25/97 Naphthalene O ug/L 0.5 NO 11/25/97 JAN - 81998 Groundwater Section Asheville Regional Once Laboratory Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS Laboratory certification IDs Drinking Water 90090 NC Drinking Water 37706 Sc 99006 This report shall not be reproduced, except in full, TN TN UST List VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc y 'ea�m f� iC i! 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(Ci) a'm 0 , c 0 c za Fax NO.: 704 252 4618 12p31-9 Pace Aran b AN 5A Ravel,_ rw Asheville Nk, Tel 734.254-71 Fax; 71514-252-461b Mr. Harry vanes December 04, 1996 Page 9 PACE Project Number: A61120b\ Client Reference° J and J Kenmore PACE Sample Number: 93 0305946 Date Collected: 11/20/96 Date Received: 11/21/96 Client Sample 10: Kenmore Parameter Units PRL ids METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Dichlorodifluoromethane ug/L 1.0 ND 12/01/96 Chloromethane ug/L 1.0 ND 12/01/96 Chloroethene (Vinyl chloride) ug!L 1.0 ND 12/01',196 Bromomethane ug/L 1.0 NO 12!01/96 Chloroethane ug"'L 1.0 NO 12/011196 Trichlorofluoromethane ug/L 1.0 NO, 12/01;96 1,1-Dichloroethene ug/L 1.0 NO 12/01//96 Dichloromethane ug/L 1.0 NO 12 O1 96 / trans-1,2-Oichloroethene ug/L 1.0 NO 12/01/96 1,1-Dichloroethane ug/L 11.0 NO 12/01/96 cis-1,2-Dichloroethene, ug/L 1.0 NO, 120196 2,2-Dichloropropane ugjL 1.0 NO 12/01/96 Chloroform NO 12/01/96 Bromochlgromethane uq J 1.0 12/0!/96 1,1,1 -Trichloroethane ugJ 1.0 NO 12,01/96 1,1-Dichloro-1-propene ug/L 1.0 NO 12/01/96 Carbon tetrachloride tag/L 1.0 ND 12/01/96 1,2-0ichloroethane ag/L 1.0 NO 12,P01/96 1,1,2 -Trichloroethene ug/L 1.0 NO 12/01/96 1,2-Dichloropropane ug,/L 1.0 NO 12/01/96 Bromodichloromethane ug/L 1.0 ND 12/01/96 Dibromomethane ug/L 1.0 NO 12/01/96 cis-1,3-Dichloro-l-propene ug/L 1.0 NO 121101/96 trans-1,3-Dichloro-l-propene ug/L 1.0 ND 12/01/96 1,1,2 -Trichloroethane ug/L 1.0 ND 12/01/96 1,3-Dichloropropane ug/L 1.0 NO 12/01/96 Tetrachloroethene ug/L 1.0 NO 12/01/96 Dibromoch?oromethane ug/L 1.0 NO 121'01/96 1,1,1,2 -Tetrachloroethane ug/L 1,0 NO 1241/96 Bromoform ug/L 1.0 ND 12/Oi/96 1,1,2,2 -Tetrachloroethane ug/L 1.0 NO 12/01/96 REPORT OF LABORATORY ANALYSIS This repot! shall not be reproduced exmpl ir, full wrnout the wrten-nnsent of Pare Anayl!cal Serviceg� inc FAX NO.; 704 252 4618 0 Mr, Harry James Page 10 Client Reference- J and J Kenmore 12-31-96, Ox* Anal,,tt—, SA pjve�--, A&PiOf,% N(,, aax f04-2524618 December 04, 1996 PACE Project Number: A611206L PACE Sample Number- 93 0305946 Date Collected: 11/20/96 Date Received: 11/21/96 Client Sample ID: Kenmore Parameter Units -PRL WS METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 1,2,3-Trichloropropane uq/L 1.0 NU 12/01,96 Bromobenzene 2-Chlorotoluene ug ug/�L L 1.0 1.0 ND NO 12/01'/96 4-Chlorotoluene u 9'! L 1.0 IND 12/01/96 12/01/96 1,3 -Dichlorobenzene uq,/L 1.0 ND 12/01/196 1,4 -Dichlorobenzene ug"'L 1.0 ND 12/101/96 1,2 -Dichlorobenzene Ug,/L 1.0 ND 12/01/96 112-Dibromo-3-chloroproparie ug/L 1.0 ND 12/01/96 102,4-Trichlarobenzene ug,(L 1.0 ND 12/01/96 Hexachlorobutadiene Ug/L 1.0 NO 12101196 1,2,3-TrichlorobenZGnO Benzene uq'iL ugJ 1.0 1.0 ND 12/01/96 NO 12/01/96 196 Toluene Chlorobenzene ug/L uq/L 1.0 1.0 ND ND .12/01/96 Ethylbenzeneug/'L 1.0 ND 12/01/96 12/01!96 Xylenes, (total) Styrene ug/L 1.0 ND 12/01/96 Isopropylbenzene ug/L ug)L 1.0 1'0 ND ND 12/01/96 12/01/96 n-Propylbenzene 1,3,5-Trimethylbenzene uqiL ug/L 1.0 110 ND NO 12/01/96 t-Butylbenzene u 10 NO 12/01/96 12/01/95 1.2,4-Trimethylbeozene ug/Lg/L 1.0 ND 12J0I/96 s-Butylbenzene 4-1sopropyltoluene Ug/L uq/L 1.0 1.0 NO ND 12/01/96 12/01/96 n-Butylbenzene Naphthalene uq1L 1,0 ND 12/01196 ug/L 110 ND 12/01"/96 REPORT OF LABORATORY ANALYSIS This repon shelf not be -'ar-odt;ced excephr, fLM ,wilhcQt ipie *titte!(, consent cl Pace AnWylical Servicp_s Inc 'O '9 z ^7 Z a°Doi co m _v{ 0 3 D n a w a» $ e o s T v, M �N o n c O e'i V -1 C ^n n Z o 0 0 o R g w x S o a A o 0 0 a 0 0 v z F O O m � C ❑m z 1 � O O ^ b N 6 o � o V O J z c b � ti e w e 3 3 e c c c p ec 3 c c c e � 3 3 3 3 3 w 3 3 3 3 3 c c 3 3 3 3 ►rC z n 3 fr 3 [W" 3 3 3 3 c' t' cam`-' 3 9 z 3 o e 3 3 3 3 3 A °' . �' O L ^ 'O '9 z ^7 Z 3 m _v{ 0 3 D n a w a» 'z D w v, M �N m Z e'i V -1 C ^n n r 3 Z z m � C ❑m z 1 � O O ^ b N 6 o � o V O J z c b � ti e w e 3 3 e c c c p ec 3 c c c e � 3 3 3 3 3 w 3 3 3 3 3 c c 3 3 3 3 3 N A c z d 3 a m D n a w a» 'z D w v, M �N m m 0 -1 C ^n n r 3 Z z m � C ❑m z 1 � O ^ 6 V O J z c c e ti e 3 e 3 3 e c c c p ec 3 c c c e a s o a D D e Ol C zn 'z a v, M a 'o m 0 -1 C ^n n r 3 Z z m � C ❑m z 1 � O ^ 6 z = n D � o r� w o m z a s o a D D e Ol C zn 'z a v, M O m m 0 -1 C ^n n r 3 Z z m � C ❑m z 1 � z = n r� z ^a cp o a D e Ol c�nnnn o o o Fr CD 2 N --I C' C N CD 00 0 0 CO CLx CD A Ul N C � i cp :9c 3 3 3 3 3 3 0 113 Z;0 0 0 3 3 1 cn cC co co m cn cp cfl co 0 cD A' CL m CD 0 3 O p 9.� O o a� m _O cN) 0 C7 � mcn0rp cD N �3A)CDCO, = O D In b w a �. �'. CD 'C N0F m N :3o O D m % o I a 3 R1 O m m 3 a; -a m t� cc Co ` o m S. � p �o ST 00 Z r R, o ,... n 0 p y � r Z Q 3 n 1 y R13 , me 0 0 r N tA-u s �' Q 13 �•it (D. tD Al fD <D �m M m Z a n 0 a -CD 0 .a d O o 4 CD 0- T m <- CCD c � Z Ku3 a coDC-0 mm m � 2) a � 5 a0 O° o"o'0O0 � co O � O D^ a o 0 �n CAD Zv `� N Vi � i cp :9c 3 3 3 3 3 3 0 113 Z;0 0 0 3 3 1 cn cC co co m cn cp cfl co 0 cD A' CL m CD 0 3 O p 9.� O o a� m _O cN) 0 C7 � mcn0rp cD N �3A)CDCO, = O D In b w a �. �'. CD 'C N0F m N :3o O D m % o I a 3 R1 O m m 3 a; -a m t� cc Co ` o m S. � p �o ST 00 Z r R, o ,... n 0 p y � r Z Q 3 n 1 y R13 , me 0 0 r N tA-u s �' Q 13 �•it (D. tD Al fD <D �m M m Z a n 0 a -CD 0 .a d O o 4 CD 0- T m <- CCD c � Z Ku3 a a m C N CL 5 a0 O° o"o'0O0 N D 00 O D^ a o 0 �n CAD Zv `� N Vi cn CD q 0 3 3 0 cfl * 1 y D co r �1 r z eff F s o �\ y$ m� _ n c� (� C7 D D SD m m 3 w y 5 0 0 3 D Cl)m 32= „O c� CL m 3 � d w m Z o -a la_ �' CD U c ��� a CD 3- "� 0 3 �' c D n n a� r Ct) (n CLCD �' A 51r w A _ oCD O 0 o T A 3 ' °' CD m A o �� A) c co rn � i cp :9c 3 3 3 3 3 3 0 113 Z;0 0 0 3 3 1 cn cC co co m cn cp cfl co 0 cD A' CL m CD 0 3 O p 9.� O o a� m _O cN) 0 C7 � mcn0rp cD N �3A)CDCO, = O D In b w a �. �'. CD 'C N0F m N :3o O D m % o I a 3 R1 O m m 3 a; -a m t� cc Co ` o m S. � p �o ST 00 Z r R, o ,... n 0 p y � r Z Q 3 n 1 y R13 , me 0 0 r N tA-u s �' Q 13 �•it (D. tD Al fD <D �m M m Z a n 0 a -CD 0 .a d O o 4 CD 0- T m <- CCD c � 0 m !�1 v_ O Z 0 nm m� <3 z a m 7 z<_z a0 O D� zr- x m E m?o Z, Z ;{ate C)ZG1 O� C c m_ vm n0 m� m 0 1 O z Z Ku3 A = a m C C Ia 0 w N D OZi cn 4 fp 3 r z eff F o 0 _ n c� (� C7 D D SD m m 0 m !�1 v_ O Z 0 nm m� <3 z a m 7 z<_z a0 O D� zr- x m E m?o Z, Z ;{ate C)ZG1 O� C c m_ vm n0 m� m 0 1 O z Z Ku3 CL a m C n Ia 0 w N D OZi cn - fp 3 r z o 0 _ n 0I (� C7 D D SD m m a- 2S w y m o 0 3 iQ 0 0 �• m 3 � w m c c cn CD 3- �3• C 0 3 �' c p�rnj m CLCD �' A w A d T A 3 A CD m A 3 A� rn Q Q N AIC, ((" L� Ln N W m C. t C - Im I n V 0 m !�1 v_ O Z 0 nm m� <3 z a m 7 z<_z a0 O D� zr- x m E m?o Z, Z ;{ate C)ZG1 O� C c m_ vm n0 m� m 0 1 O z CL a J cn i I m 3 m 0 0 0 0 a m a- 2S m w CD z 3 a -n atom � � y o C3 G .. C o_ m w m o v o my x O Q D SS 0� x C r fp I n _ N N O 0 m 0 O y S C. N N y n. ° •V co N N fD CDD O N n' D N o. CD co a CD (D 0 N 0 m !�1 v_ O Z 0 nm m� <3 z a m 7 z<_z a0 O D� zr- x m E m?o Z, Z ;{ate C)ZG1 O� C c m_ vm n0 m� m 0 1 O z CL a J cn i I m 3 m a m CD -n � � y o x 0� r I I I"\o _ 0 m !�1 v_ O Z 0 nm m� <3 z a m 7 z<_z a0 O D� zr- x m E m?o Z, Z ;{ate C)ZG1 O� C c m_ vm n0 m� m 0 1 O z CCD OOOOO v O m 0 Dr cTo Q7 Q m 3> WOaa-O 77 0 c p c. OD�'-�$ �a CD M-i-�O000m 14. z Wz,� �c 0 0 ? c O Vl0 w CD Q CD 5F 5F_ N z M c O o L 00 6' O 0_0 3.a0'w n gm 2' �,w o m3ZO cam om CD a 00� G 0 CD :;ic 0 CD fD = a y .0 6NL� D00OmNCE �0 -CM l O CD W N O m O A O? O N a O O O CL Q. 06 Cl) QVi � 0 z W w 0 O CD O O _• cn IOOO O X . co � O m CD O mcyl n O s W C1� =3 CD O ID �: N ell a N o. F 0 fD 0 > CA CD n Icn W R O c 3 �� o.� ❑Z O N o a cfl � m r M = CD y��OT G Q' a N t� § (D CD m m W e CD N Cm -� a3N, m � r -� r s i cIZE 3 3 m Lnr 3 c Z 3 0 oi3 3 06 o m= 'o cn� v O m 0 Dr cTo Q7 Q m 3> m O ° 77 0 c p c. OD�'-�$ �a CD CO 14. z Wz,� �c 0 0 ? 6 o CD Vl0 N. CD Q CD cl c N z a a 6' 0 n D.. o m3ZO om CD w o m 0 G z 0 CD cnM o O 6NL� D00OmNCE �0 -CM l 1i1 O o � N a O fQ CL Q. 06 (DX � 0 z e CD �V O _• = IOOO . N.. . O CD �: ell F 0 fD 0 > CA CD n Icn t, R O c 3 �� o.� ❑Z N o a cfl � m r M = CD y��OT G Q' a N t� § (D CD m m W e CD N Cm -� a3N, m cn -� r rnAC) Pz O ° m o m= 'o cn� v O m 0 Dr cTo Q7 Q m 3> m O ° 77 0 c p c. OD�'-�$ �a CD O 14. z Wz,� �c D ? 6 o CD Vl0 N. CD Q CD cl Z-11 N a 6' 0 n D.. m3ZO om G z 0 CD cnM o O 6NL� O -CM l 1i1 O � N a O fQ _ Q. 06 o � 0 z e CD �V CD ell 0 Icn j, R �cnor0 � CD 00 2 CD c 3 �� o.� ❑Z N o a A, = m r M = CD y��OT G D Q m m W e Cm -� a3N, m cn -� r rnAC) Pz O ° m Lnr cn 0 3 CD m (1 vi CD CD CD c Q T CD CL W m c Q CD 0 v v O v r = m C3. z CD = c o CD CD Q CD cl `c a 6' 0 n l CD O _ G Q DD CID v se0 zv O' " �m m� z3 <m z- C 7 z<_z a o 0 r= Z -^ 0m n mdd C- M. O C) d 6t O� c a - z —: «, M m N N m n O z t 1 m g D o �o 0 •c 0 G 61 A w -I�u)Cn-01 Df0-��2�0 TZ �m�;CDC) '�O „ O aw(D0 -0 ooh -. CDD 0 (CD �, Q_ cin D� CDQ � Z oo �a �• Q 0 � s 3 33533333333 00 c= cQ ca o ca co ca cQ cQ ;: c.Qmcc�09) Q Q� � = o 1 1 1 CD mmO Ko cc'0n i c _ Z �� mQ-03cl—o -- 0 3�'CDCD c333—IW X33 3 5.`�� Z Z FED IUD) 333333333.333333 cQ cQ ca ca cc ca ca cQ cQ ca cQ ca ca ca ca o (� Cr m mm '11 1 rZ O CD n �a; m c oC c �o Q� c CD $ m � Q. U SLa A ,. f C c C 3 3 3 rp_r, m cn> o ro cQ � N 3 $_m ro oma' mm CD — _ CD < m�Zo C ro ogo= C cnmo� ��y. I- m cn o m c 0 v, m _Q o.CD m 5. z cns a) z G) I, I z p cn O co 108 INV, CD OL a o 0 0 Z' 01) D CD CDD m m mm m�Zo ogo= C cnmo� ��y. I- m m c ' m z a) z G) I, I z p cn O 108 yy �rr U7 C LL ,10 10:20 ID:PACE INC. ace A►l!lYticel Mr, Harry James Page 12 Client Reference: James & James PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALY5I5 �4if�+I�tL TEL N0:252 4618 #t5_ Pus AnaO &W NMwa. Ike. Tal: 704-194.1170 Fow 704-151-4016 February 07, 1996 PACE Protect Number: A6012260C 93 0171969 01/22/96 01/23/96 Q85 W5 Units MDL #Wa DATE ANALYZED 1.2,3-Trichloropropane ug/L 1.0 NO 01/24/96 Bromobenzene ug/L 1.0 NO 01/24/96 2-Chlorotoluene ug/L 1.0 NO 01/24/96 4-Chlorotoluene ug/L 1.0 NO 01/24/96 1,3-Olchlorobenzene ug/L 1.0 NO 01/24/96 1,4 -Dichlorobenzene ug/L 1.0 NO 01/24/96 1,2-01chlorobenzene ug/L 1.0 ND 01/24/96 1,2-Dibromo-3-chloropropane ug/L 1.0 NO 01/24/96 1,2,4-Trichlorobenzene ug/L 1.0 NO 01/24/96 Hexachlorobutadiene ug/L 1.0 ND 01/24/96 1,2,3-Trichlorobenzene ug/L 1.0 ND 01/24/96 Benzene ug/L 1.0 NO 01/24/95 Toluene ug/L 1.0 NO 01/24/96 Chlorebenzene ug/L 1.0 NO 01/24/96 Ethylbenzene u9/L 1.0 ND 01/24/95 Xylenes ug/L 1.0 NO 01/24/96 Styrene ug/L 1.0 NO 01/24/96 Isoprepylbenzene ug/L 1.0 NO 01/24/96 n-Propylbenzene ug/L 1.0 NO 01/24/96 1,3,5-Trimethylbenzere ug/L 1.0 NO 01/24/96 t•Butylbenzene ug/L 110 NO 01/24/96 1,2,4-Trimethylbenzene ug/L 1.0 NO 01/24/96 s-Butylbenzene ug/L 1.0 NO 01/24/96 4-Isapropyltoiuene ug/L 1.0 NO 01/24/95 n-Butylbenzene ug/L 1.0 NO 01/24/96 Naphthalene ug/L 1.0 NO 01/24/96 ea <o 000woD?>= 70-1-1ooC)l� W c 7 0 S L A C C) O O 0 0 m-i�•asa$ '••3� f'"' 3 3 o o �- o m= x m p° v c '9rt o x a S co �T o- W cn 1 J UI O G 131111110111M�In- R -M IN V (n DZ Z $ 7C 2" 0 0 0 0 w D D D w o w w e c. w w CO y r Z to O oCD a ?.a o 0 o o 0u D C (n w w ° o n. w �. CD 3 Y 3' c w gi' g A w 3. c' 3 3. `° J A a 3 W A 3 3 p A A 3 46 i o U icn fi n• BA r— ch mo w c < Q 4 O 0 D m Z (3Ln co) CD Q w �0 �= O w `2 0 ( m W CA 0 7D CL i2. C (D ° O 9_) N 1 O {G) D D ' c 0-0 6,ZO0 ��� -I 2 " Q :3 .Q 0 IZA o CDm 7D ao O o N = c ml N a n CMD 0 m UN Z _ 0 O ��oo `D a LU in 1 a w p a y w a m O L) (D NSO co ,� a 0 (,. m Qr O D R 0 El 0 M _� b m � 0 �'' �03m m Z oz El m O �• n3 W� c m rn�X0'��m� SZ CA � -4 i XanPs ra a Rio U icn CD t�3 w c < Q 4 CD o' wu cu � D m m Z CD CD Q w �0 �= O w `2 LD. ( m W co �q CL i2. C (D ° O 9_) N 1 O {G) G- ' Dell -I 2 " Q :3 .Q li �• 7D w �. c ml N 2 -u n m D 0 O `D a in 1 a w p a y a W (D co U icn CD t�3 c 4 cu � Q m c CL CCD o `2 LD. ( m W �q CL O. 9_) N 1 O G- Dell -I 2 " -n 0 .Q G c n n m 0 O c CD a w p a a O O Z 0 CD n •g m� z� o� z °. C 3 z5.z A o 0 ate? �o MM w M. O e CL OZw, Oc C vm -1 c m �a m 9 O z `n z 1>11>11 x x < -] rn x D z O O O 0 C" z o z N lax n a E4 o s s n.. °z �cD—• �D—c x c0 n o? w O ° 0 0 0 to Q s $' M M O d d O ri d R 'O . U % � �+ : c0 A A d c p 3 c g 3 c D\ O c c c O c c c c O Nd e4 b N = y O O O O o a *rC 3 N WE 1>11>11 x x < -] rn D z O O O 0 z o z N lax n Crl E4 °z z w w O ° s 9 'O U A c c p 3 c g 3 c D\ O c c c B c c c c e4 b N 00 w O O O O o 3 N -i •3 < -] rn D z O O O 0 z o z N lax n Crl °z z w w O ° s 9 'O y, J c c c c 3 c g 3 c e c c c B c c c c -i •3 < -] rn D z O O O 0 z o z N lax n Crl °z z w w O ° s 9 'O w o O O 0 z o z N lax n Crl °z z w w O ° s 9 'O p O g-- g N a� .p N p n = o O o D I C7 D v Cr r- CD o CL 0 0 CD CL -Z- CD o w_ y D 0 7.1 W ? fD o m a �' __ y rn T N c o -< � n � U1 x o ° a m ZZ o M A 03 ;A CD O D Cn - � is w a e+_ Z o v �Z Q 1J1 4 -1 D n2 D FD r � 0 Ill o rn O y � ca pi �l -n {? a o M � Z nl 1! �A o0(0� r o 2. Ln 33 O S C C 0 (=D N 0 0 O N W -O �: T o n m 00 = o- CL �. 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A O CD cD 0 d ,. m 3 fD C 0 =-c r.r N 0 m n =m 3 < m NZ _c Q CD _TI N fl2 C U) "S o Q o N CO @ * P, 3 M c:) Q N rn 0 (D O r n o CD cr CD O CD r � �: o cn 0 w < 0 � (D CD Cmc o 70 a -i m z3 n = (D sa N 3 v Cc = cQ c CD Z �� z w(0 CD w r CD o m cr m m w CD cr `° v 3 o o z CD c CD (D 0 m� v > �' � f7ffin N 0_0 -i v CD QCD n v Fn v 0 i n m rl a M N 0 A. ci w 0 z 0 z D O V (D 0 :01:1O cD a CcO 0. °0 0 :3 0. a o :3 m D� Q- z CD E3 CD C:) C+ c+ O O X 0 U7 7C w V Wo 0 0 c M 2 m CD 5 V 0 b TI DO fJ � c � T71zzz Ti o�K � 0M0W C/)v,'m n M Z 0, — 000� 0 m cn c N M OO v z c m Z O Z O m 0 0 C,) r C N d M. i �0 2t v p � f m u �. _TI N fl2 C cD m D� Q- z CD E3 CD C:) C+ c+ O O X 0 U7 7C w V Wo 0 0 c M 2 m CD 5 V 0 b TI DO fJ � c � T71zzz Ti o�K � 0M0W C/)v,'m n M Z 0, — 000� 0 m cn c N M OO v z c m Z O Z O m 0 D R 0f L 0 G I C 1 N COMPANY NAME: COMPANY PROJECT NUMBER: HYDROLOGIC PROJECT NUN3ER: HYDROLOGIC SAMPLE NUMBER: HYDROLOGIC LAB I.D.#: SAMPLE IDENTIFICATION: DATE SAMPLED: DATE EXTRACTED: DATE/TIME ANALYZED: Hydrologic -Asheville, Inc IMMURE MWS EL9433991 33993 399 Q85W5 11/15/94 N/A 11/18/94 METHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT ( ug/1) ( ug/1) Benzene 71-43-2 1.0 BDL Bromobenzene 108-86-1 1.0 BDL Bramochloranethane 74-97-5 1.0 BDL Bromodichloranethane 75-27-4 1.0 BDL Bronoform 75-25-2 1.0 BDL Brcmamethane 74-83-9 1.0 BDL n-Butylbenzene 104-51-8 1.0 BDL sec-Butylbenzene 135-98-8 1.0 BDL tert-Butylbenzene 98-06-6 1.0 BDL Carbon tetrachloride 56-23-5 1.0 BDL Chlorobenzene 108-90-7 1.0 BDL Chloroethane 75-00-3 1.0 BDL Chloroform 67-66-3 1.0 BDL Chloromethane 74-87-3 1.0 BDL 2-Chlorotoluene 95-45-8 1.0 BDL 4-Chlorotoluene 106-43-4 1.0 BDL Dibrariochloramethane 124-48-1 1.0 BDL 1,2-Dibrano-3-chloropropane 96-12-8 1.0 BDL 1,2-Dibramanethane (EDB) 106-93-4 1.0 BDL Dibramamethane 74-95-3 1.0 BDL 1,2 -Dichlorobenzene 95-50-1 1.0 BDL 1,3 -Dichlorobenzene 541-73-1 1.0 BDL 1,4 -Dichlorobenzene 106-46-7 1.0 BDL Dichlorodifluoromethane 75-71-8 1.0 BDL 1,1-Dichloroethane 75-34-3 1.0 BDL 1491 Twilight Traif 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 L 0 G I C I N Page 2 continued COMPANY NAME: Hydrologic -Asheville, Inc COMPANY PROJECT NUMBER: KENMURE NWS HYDROLOGIC PROJECT NUMBER: EL9433991 HYDROLOGIC SAMPLE NUMBER: 33993 SAMPLE IDENTIFICATION: Q85W5 DATE SAMPLED: 11/15/94 METHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT ug/1) ug/1) 1,2-Dichloroethane 107-06-2 1.0 BDL 1,1-Dichl-oroethene 75-35-4 1.0 BDL cis-1,2-Dichloroethene 156-59-4 1.0 BDL trans-1,2-Dichl-oroethene 156-60-5 1.0 BDL 1,2-Dichloropropane 78-87-5 1.0 BDL 1,3-Dichlorapropane 142-28-9 1.0 BDL 2,2-Dichloropropane 590-20-7 1.0 BDL 1,1-Dichloropropene 563-58-6 1.0 BDL cis-1,3-Dichloropropene 10061-01-5 1.0 BDL trans-1,3-Dichl-oropropene 10061-02-6 1.0 BDL Ethylbenzene 100-41-4 1.0 BDL Hexachlorobutadiene 87-68-3 1.0 BDL Isopropylbenzene 98-82-8 1.0 BDL p-Isopropyltoluene 99-87-6 1.0 BDL Methylene Chloride 75-09-2 1.0 BDL Naphthalene 91-20-3 1.0 BDL ri�-Propylbenzene 103-65-1 1.0 BDL Styrene 100-42-5 1.0 BDL 1,1,1,2 -Tetrachloroethane 630-20-6 1.0 BDL 1,1,2,2 -Tetrachloroethane 79-34-5 1.0 BDL Tetrachloroethene 127-18-4 1.0 BDL Toluene 108-88-3 1.0 BDL 1,2,3-Trichlorobenzene 87-61-6 1.0 BDL 1,2,4-Trichlorobenzene 120-82-1 1.0 BDL 1491 Twilight TrailU Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 U M Page 3 continued l J 01 I �1� W �x" k.La1�.IC alp 0 L 0 G I C, HYDROLOGIC PROJECT NUMBER: HYDROLOGIC SAMPLE NUMBER: SAMPLE IDENTIFICATION: DATE SAMPLED: ANALYSIS 1,1,1 -Trichloroethane 1, 1, 2 -Trichloroethane Trichloroethene Trichlorof luoranethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride Xylenes (total) Dichloranethane Hydrologic -Asheville, Inc KENMURE MWS EL9433991 33993 Q85W5 11/15/94 N=OD EPA 502.2 CAS NO. SDL ( ug/1) 71-55-6 1.0 79-00-5 1.0 79-01-6 1.0 75-69-4 1.0 96-18-4 1.0 95-63-6 1.0 108-67-8 1.0 75-01-4 1.0 1330-20-7 1.0 75-09-2 1.0 BDL = Below Sample Detection Limit SDL = Sample Detection Limit COMMENTS: ( ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1491 Twilight Trail Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 o_ =' � 0 W n D D= o 0 c m CL N O = p X O A-0 "O p CD O A 0"__ X 0 p W '(moi, N 000m 0 o 0 00 0 Cl.rn = (D 0 3 3 0 i ( 0)W S p A O o (D p O 0 C w w CL a 1 Ln w rn o .ar "m C e;CA LMA CD a m c a -n CD a m v m o >' Co 0 m � A2 �a M z c -o o CDcD 0 wo Q -a o Q O W Z � `< w _= T o m 0 3 a D v oc0cfl Z s o o co C` O i w v mO O 3 S W m G) SU (D O t :W n -n N CD O o cnat86 m 320 _ - m m O X U p > n m .moi. o 86- C a K (D S S o R r cf)i G (fl Owl N A� N f1a y a y.. 70 Z D QAD � O a 0 C �] A) (D n O * 0 \ n p Oo w OCD = N N �. 77 D o w a � g � O � n d CD m D y .ar "m C e;CA LMA CD a m c a -n CD a m v m o >' Co 0 m � A2 �a M z c -o o CDcD 0 wo Q -a o Q O W Z � `< w D^ T o 0 D v Z s o co C` O i r- C ?p N mO O 3 S Cf) t :W n -n 0 > cnat86 m 320 _ - m m O U p > n m 0 o 86- C a K E m _ R r cf)i G Owl N A� f1a y a y.. 70 Z D QAD � O a 0 C �] O * \ Oo w o O n mcn0r-O D CD W CD 0 N "a (D F]� Z r No- 0 m u) CD 0 - C D Z m El n ?`Q� � 3 �' w° c C m --I p ro o• R? m m0 z .ar "m C e;CA LMA CD a m c a -n CD a m v m In Fn r v O v ZEN O Z v 0 m� m� z3 <0 Fa= O Z- 9m m 7 z<_.z no 0 r0 n 7 S Z=" 2 n m d m_ o ? 0 1a3 O Z m O� c C m vM a o 1a M - >, 0 (n H m 0 O z m w m m � ci Q z c -o o (mD 0 (o 3 Cr m W s �cl O i T1 O 3 S 0 c X 0 (u 0 E m _ w D a G m In Fn r v O v ZEN O Z v 0 m� m� z3 <0 Fa= O Z- 9m m 7 z<_.z no 0 r0 n 7 S Z=" 2 n m d m_ o ? 0 1a3 O Z m O� c C m vM a o 1a M - >, 0 (n H m 0 O z - T1 D -1 �l o CA D m cD = o =r 3 T1 0 j ari �. 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County eut"i /�' Road/Street Quad No. V Serial No. IS -37S41 Lat. 1-6-: I 17 Long. 15a R6 12- Well Construction Name Address Reg. # Check Items Meets Min. Standards Remarks Measured Yes No Permit Required ? (Y/N) I .................. - (Permit No. Location . Distance From: ................... Water Tight Sewagetwaste collection... , Waste disposal (septic tank drain field) e Other r Po II. Source Other Poll. Source in Cas( Type...................................................... Depth.................................................... Weight/thickness .................... Height (A.L.S.) ... ......... ........ ....... SSR 2'l. Other ( ) .. 4 Drilling Fluids/Additives Type................... .................. ............... Grout Type.................................................... Thickness ............................................. rf Depth.................................................... r .J/ Other ( ) •• Screens Screened interval ....................." r t Other ( 1 .. Development ......................................... Total Suspended solids .................... Turbidity ........................................... Settleable Solids ................................ . I.D. Plate Well Contractor ..................................... Abandonment Temporary ............................................ (Circle one) i Galy. Stain. St. Other_ aajov/ " Permanent ............................................ Applies to wells constructed after December 1, 1992 GW -36 Rev. 10/92 (Cont. on Reverse) ~-ARTMENrorNATURAL AND COMMUNITY DEVELOPMENT ~.^orENVIRONMENTAL MANAGEMENT GROUNDWATER SECTION po.BOX vrvo,-n^Lcmuw.o.xrm,.PHONE m`mron-oo1 � WELL CONSTRUCTION RECORD DR|LLI08CONTRACTORov-4 ` FOR OFFICE USE 01,, Quad. No. V 9 Serial No. STATE YVl=LLCONSTRUCTION ' DRILLER REGISTRATION NUMBER 1045 Minor Basin ` ouom oouo ` Header Ent. GW—1 Ent.— DR|LLI08CONTRACTORov-4 ` ` STATE YVl=LLCONSTRUCTION ' DRILLER REGISTRATION NUMBER 1045 PERMIT NUMBER: 44-0210-WM-0112 1. WELL LOCATION: (Show sketch orthe location below) ' Nearest Town: Flat Rock, 0C County: Henderson (South of Hendersonville, NC) oonm DRILLING LOG (nvuu.Community, n,Subdivision and Lot mvl From To Tn pomnunnn 000vrinnon e. ovvmsn Kerimute Properties, LID xoonson DS Highway 25 0 91 Alluvium - Tan Sand)r Silt (Street or Route No.) Flat Rock, NC 28731 Containing subrounded Gravel. City n,Town State Zip Code n.DATE DRILLED 5/25/93 USE OpWsLL9' - 15' Brown Micaceous Sandy Silt *. TOTAL DEPTH 15' CUTTINGS COLLECTED C0Yom El No s oosa WELL REPLACE EXISTING WELL? 91 Yes Fl No 51 G. STATIC WATER LEVEL: Fr. 0 above TOP OpCAGwG. Om�uw �p TOP OFCASING |G_____ ---'FT. ABOVE LAND SURFACE. 7.YIELD (opm): METHOD OFTEST o.WATER ZONES 0unnthl: 51 9. CHLORINATION: Type _���-_--__ Amnunt --- 1o.CASING: space is needed use bat4 of If Wall Thickness additional ownm Diameter mWokghuFt. Mamno| LOCATION SKETCH From 0 To 5 Ft. 2" SCB 40 PVC (Show oir0000" and distance from utleast two Gtum n««u«. From -To -____-Ft.______ __-_-_. o, other mop ,n,e,onoe points) From -To _------F\.--_____ 11GROUT: Donm Material Method From --_10___ rn2-__-Ft. SACKCRETE HAND From 2ToFt. BENTONITE HAND 12. SCREEN: oonm Diameter Slot Size wutenu| From 5 Tv_-lSFt. _2m`O.<}1--in. PlCL_-_ F,om ro-_____Ft. in. in. From __-To- Ft. in. in. ' 13.GRAVEL PACK: .' Depth From --37o_15Ft. rrom________rn_____ p�� 2 2 qTAN ARDS, AND THAT A CO Y OF T1,4 'CORD R 0 E WELL OWNER. 4 1994 SIGNATURE OF CONTRACT61`1 OR AGENT �ATE 011 R Submit oriqinal to Division of Environmental Management and copy to well ownpi i �'� - � �..' ;. .' � `t ate- - \ •.� •v �.� �� r� ,i �• /. .. aI dli V. 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COUNTY: HENDERSON' DATE SAMPLED ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE tid CHROMIUM,TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL G A COPPER CYANIDE DISSOLVED SOLIDS FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM M BAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA o p i ,s v, f NITROGEN, KJELDAHL NITRATE & NITRITE p. b/ (.[ '~O` 0. I ORGANIC SCAN ORTHOPHOSPHATE pH �• G� PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE TOC (UNFILTERED) j TOX TSS VOC ZINC STATIC WATER LEVEL Red Ink=Sample taken by facility DATE SAMPLED ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE .CHLORIDE CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL , COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS 36 76 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM Ked ink = sample taken by facility i WELL NO. C, J! V COUNTY: DATE SAMPLED MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA 0,0/ b, /o NITROGEN, KJELDAHL NITRATE & NITRITE o 3 7�O ORGANIC SCAN pH S• x,16 PHENOLS PHOSPHORUS, TOTAL 0. POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE ol3 3 SULFATE TOC (UNFILTERED) -30 TOX TSS voc ZINC STATIC WATER LEVEL nea inx = ;niamp►e taken Dy mcnity DATE SAMPLED jj�/ %- 77 1/ • 17- -77 11-3-7 $ //.5 ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE, A J j CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL j , f I 1A f, % COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS /00 60 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM Red Ink = Sample taken by facility WELL NO. Q 8-S v 9 COUNTY: /-/& /V'o & 2 S c?r/ DATE SAMPLED //-3-y5' //-,1- MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA 0.0S ®. J o . ®(, U ! L ®, 01 40,1 NITROGEN, KJELDAHL & NITRITE © - 0 3 �0 3 , i 0,07 � O • 1 f �. © It ivoNITRATE b. Q ORGANIC SCAN PH .5 . 5 ' • J ��. �o ��o PHENOLS PHOSPHORUS, TOTAL 0. OA o• /if D • /f POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS yL ZINC STATIC WATER LEVEL 5� �/ D 5 . �J . %-5 C3 ,4 0 Red Ink = Sample taken by facility COUNTY 1-� ov D 6R -To DATE SAMPLED //LL �S' %`� /"I - / �'q� .� o�.`� 914 IW,��' `//O fl-a�� `j /l -.,2A- J("' ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE T -3 ,2 76 ig J,K `tea S CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL 4 COPPER CYANIDE DISSOLVED SOLIDS % pp// 1� —�- FLUORIDE HARDNESS CaCol HARDNESS, NON -CARBONATE IRON LEAD LITHIUM Red Ink = Sample taken by facility DATE SAMPLED MBAS 1 MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN,AMMONIA ®, /® Z 0. 1 0.03 L 0. i NITROGEN, KJELDAHL k _3 a NITRATE & NITRITE 0. 0 1 N e- U° /0 � � Nt�3�, r� � Q � ORGANIC SCAN PH PHENOLS O, PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIFIC CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS VOC A/o %° 0a C lU G{ L r !y v/1- ZINC STATIC WATER LEVEL -i-�U)cn-0G)> connOv Te�0 � = =(n'� D o v c Z 5; CD iv (D w m O C7 ^ to R Ei: 0 D y�;m ° m F)'n- n < A 3 m. CD CD CD Z3 0 D w �z KK m Q 0 � O A it -n (n n Cl) N Q o O CD d A� 0- I o Sv v 0 o ^�CD a M c N _ 0 3 33 3 3 3 3 3 3 003 Cn co O Cn cQ cQ cm cn CO -•c03 co cD cn = C cn O C DI O 3(n a 0 CD OQ 3 C W W C � 0 CCD O W CDC -• W c',Z �c'3 3 �O m 0 3 0�wCn sv mE �3 — _ Z cn z sv I z A O i`. CL 3333333333333332• co cn cn Cn cn (a cn co n n cfl cn cn cQ ce a• CL OCD a 60 I'D G) D.. 0.y+ n CD a " 0.3 n m CD o 3 3 3 w a. cp c� u Cn 0 0 o I�D = CL CL CL :m- =4: n n II II II S + (9 t 13 C) QDN-0Z Ir m 0 Nr— m 0 W X 0 1 zj; Z o O 3m o z CL Q -noK (D N N'00 (OQD (D CD Q O N CD _ 03 Cn v 0 CDm m co wo. cD m w w o. _rw 7 CD 3: C: _Sa0.y o cr C7 Cn CD Oao CD o w CD- v m m m3 M. a 0 (n "',v .. G9 a w3 3 Q � a CAm CD m o < D v v� .O CD LSU CD < T 7 Cn CD O w CD 3 o -a CD m - a O w ❑ CCD 0 m -� c CD CD ,+ cn C: (0 m `i 0 w C) r O CD Ww o W O 3 b':2 -a F o w w � w 0 0�14 o ai o a CL N Gf N A::ro 0 0 rL 3 '9 m rt 0 3 a. N (n N 0 m CL ,v M IQ m 0 :3 or n -` w m o ID Z' � A _ N 0 O C 0 �G O m � _ m: o cn CD QQ 3` CD ski n ID 0 n -n \/ Li r: Z n ,= O �7 V w 3 '0 C CD Z h Z -u v m D n m mm m z m O CA 0O 0Er 5-900-0 D ..j :- r ° 7 m 7J -n -G o F Q Q m Z_ �C, o --I v 0 O� Cp z^ Cq L J O m v M rc� M M�� O 2Cm Z m N < ,z,-�'ZO z � -4 Z P. vZ -+ c mm mD cn r m� 0m N Z C M n m N -4z zm '0 -u v m mm 0K O CA (n --j 0Er 5-900-0 :- CD z -n ° 7 m 7J (a c3 m a o F Q m �C, o v O� D v CD m O m a ? m Z X U � w v o W M_ w 0 Z n > 0 o = 0 Z z Cn' a o -I O D m CD wCD m = CD v C O m v M rc� M M�� O 2Cm Z m N < ,z,-�'ZO z � -4 Z P. vZ -+ c mm mD cn r m� 0m N Z C M n m N Date: 11/28/01 borato Certification IDs _ REPORT OF LABORATORY ANALYSIS NC Wastewater 12 NC Drinking Water 37706 This report shall not be reproduced, except in full, Sc 99006 without the written consent of Pace Analytical Services, Inc. Page: 9 Laboratory Certification IDs KY Drinking Water 90090 VA Drinking Water 213 FL NELAP E87627 Pace Analytft., 9800KinceyAvb. . �1������ j� A J Huntersville.. Phone. 704.87,).., vrvnv. pasetabs.com Fax: 704.875.9b, Lab Project Number: 9227835 Client Project ID: James&James 9324890 -------------------------------------------------------------------------------------------------------------------- Lab Sample No: 931042980 Project Sample Number: 9227835-005 Date Collected: 11/13/01 12:05 Client Sample ID: V8 Matrix: Water Date Received: 11/13/01 14:03 Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Lim ,GC Volatiles GC VOCs in Water Prep/Method: SM 6230D / SM 6230D Benzene ND ug/l 0.50 1.0 11/27/01 22:06 KST 71-43-2 Bromobenzene ND ug/l 0.50 1.0 11/27/01 22:06 KST 108-86-1 Bromochloromethane ND ug/l 0.50 1.0 11/27/01 22:06 RST 74-97-5 Bromodichloromethane ND ug/l 0.50 1.0 11/27/01 22:06 KST 75-27-4 Bromoform ND ug/l 0.50 1.0 11/27/01 22:06 RST 75-25-2 Bromomethane ND ug/1 0.50 1.0 11/27/01 22:06 KST 74-83-9 n-Butylbenzene ND ug/l 1.0 1.0 11/27/01 22:06 RST 104-51-8 sec-Butylbenzene ND ug/l 0.50 1.0 11/27/01 22:06 KST 135-98-8 tert-Butylbenzene ND ug/l 0.50 1.0 11/27/01 22:06 KST 98-06-6 Carbon tetrachloride ND ug/l 0.50 1.0 11/27/01 22:06 RST 56-23-5 Chlorobenzene ND ug/l 0.50 1.0 11/27/01 22:06 KST 108-90-7 Chloroethane ND ug/l 0.50 1.0 11/27/01 22:06 RST 75-00-3 Chloroform ND ug/l 0.50 1.0 11/27/01 22:06 RST 67-66-3 Chloromethane ND ug/l 0.50 1.0 11/27/01 22:06 RST 74-87-3 2-Chlorotoluene ND ug/l 0.50 1.0 11/27/01 22:06 RST 95-49-8 4-Chlorotoluene ND ug/l 0.50 1.0 11/27/01 22:06 RST 106-43-4 1,2-Dibromo-3-chloropropane ND ug/l 2.0 1.0 11/27/01 22:06 KST 96-12-8 Dibromochloromethane ND ug/l 0.50 1.0 11/27/01 22:06 RST 124-48-1 1,2-Dibromoethane (EDB) ND ug/l 0.50 1.0 11/27/01 22:06 RST 106-93-4 Dibromomethane ND ug/l 0.50 1.0 11/27/01 22:06 KST 74-95-3 1,2 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 22:06 RST 95-50-1 1,3 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 22:06 KST 541-73-1 1,4 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 22:06 RST 106-46-7 Dichlorodifluoromethane ND ug/l 0.50 1.0 11/27/01 22:06 KST 75-71-8 1,1-Dichloroethane ND ug/l 0.50 1.0 11/27/01 22:06 KST 75-34-3 1,2-Dichloroethane ND ug/l 0.50 1.0 11/27/01 22:06 KST 107-06-2 1,1-Dichloroethene ND ug/l 0.50 1.0 11/27/01 22:06 RST 75-35-4 cis-1,2-Dichloroethene ND ug/l 0.50 - 1.0 11/27/01 22:06 KST 156-59-2 trans-1,2-Dichloroethene ND ug/l 0.50 1.0 11/27/01 22:06 KST 156-60-5 1,2-Dichloropropane ND ug/l 0.50 1.0 11/27/01 22:06 KST 78-87-5 1,3-Dichloropropane ND ug/l 0.50 1.0 11/27/01 22:06 KST 142-28-9 2,2-Dichloropropane ND ug/l 0.50 1.0 11/27/01 22:06 KST 594-20-7 1,1-Dichloropropene ND ug/l 0.50 1.0 11/27/01 22:06 RST 563-58-6 cis-1,3-Dichloropropene ND ug/1 0.50 1.0 11/27/01 22:06 KST 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.50 1.0 11/27/91 22:06 KST 10061-02-6 Diisopropyl ether ND ug/l 0.50 1.0 11/27/01 22:06 KST 108-20-3 Date: 11/28/01 borato Certification IDs _ REPORT OF LABORATORY ANALYSIS NC Wastewater 12 NC Drinking Water 37706 This report shall not be reproduced, except in full, Sc 99006 without the written consent of Pace Analytical Services, Inc. Page: 9 Laboratory Certification IDs KY Drinking Water 90090 VA Drinking Water 213 FL NELAP E87627 14dAnaliftal' mvm. pacelabs.com Lab Sample No: 931042980 Client Sample ID: V8 Pace Analytit., 9800 Kincey A�, Huntersvillb,. Phone: 704.8i�,. FaX 704.875.,4. Lab Project Number: 9227835 Client Project ID: James&Jamas 9324890 Project Sample Number: 9227835-005 Date Collected: 11/13/01 12:05 Matrix: Water Date Received: 11/13/01 14:03 Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Lim Ethylbenzene ND ug/l 0.50 1.0 11/27/01 22:06 AST 100-41-4 Bexachloro-1,3-butadiene ND ug/l 2.0 1.0 11/27/01 22:06 AST 87-68-3 Isopropylbenzene (Cumene) ND ug/l 0.50 1.0 11/27/01 22:06 RST 98-82-8 p-Isopropyltoluene ND ug/l 1.0 1.0 11/27/01 22:06 RST 99-87-6 Methylene chloride ND ug/l 2.0 1.0 11/27/01 22:06 RST 75-09-2 Methyl-tert-butyl ether ND ug/l 0.50 1.0 11/27/01 22:06 AST 1634-04-4 Naphthalene ND ug/l 2.0 1.0 11/27/01 22:06 AST 91-20-3 n-Propylbenzene ND ug/l 0.50 1.0 11/27/01 22:06 RST 103-65-1 Styrene ND ug/l 0.50 1.0 11/27/01 22:06 AST 100-42-5 1,1,1,2 -Tetrachloroethane ND ug/l 0.50 1.0 11/27/01 22:06 AST 630-20-6 1,1,2,2 -Tetrachloroethane ND ug/l 0.50 1.0 11/27/01 22:06 RST 79-34-5 Tetrachloroethene ND ug/l 0.50 1.0 11/27/01 22:06 RST 127-18-4 Toluene ND ug/l 0.50 1.0 11/27/01 22:06 RST 108-88-3 1,2,3-Trichlorobenzene ND ug/l 2.0 1.0 11/27/01 22:06 AST 87-61-6 1,2,4-Trichlorobenzene ND ug/l 2.0 1.0 11/27/01 22:06 RST 120-82-1 1,1,1 -Trichloroethane ND ug/l 0.50 1.0 11/27/01 22:06 AST 71-55-6 1,1,2 -Trichloroethane ND ug/l 0.50 1.0 11/27/01 22:06 AST 79-00-5 Trichloroethene ND ug/l 0.50 1.0 11/27/01 22:06 SST 79-01-6 Trichlorofluoromethane ND ug/l 0.50 1.0 11/27/01 22:06 AST 75-69-4 1,2,3-Trichloropropane ND ug/l 0.50 1.0 11/27/01 22:06 RST 96-18-4 1,2,4-Trimethyibenzene ND ug/l 0.50 1.0 11/27/01 22:06 RST 95-63-6 1,3,5-Trimethylbenzene ND ug/l 0.50 1.0 11/27/01 22:06 RST 108-67-8 Vinyl chloride ND ug/l 0.50 1.0 11/27/01 22:06 AST 75-01-4 m&p-Xylene ND ug/l 0.50 1.0 11/27/01 22:06 AST o -Xylene ND ug/l 0.50 1.0 11/27/01 22:06 AST 95-47-6 1-Chloro-3-fluorobenzens (S) 115 % 1.0 11/27/01 22:06 RST 625-98-9 Date: 11/28/01 Page: 10 Laboratory Certification IDSREPORT OF LABORATORY ANALYSIS L aboratory Certification IDs NO Wastewater 12 KY Drinking Water 90090 NO Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 SC 99006 without the written consent of Pace Analytical Services, Inc. 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S O m 3 O 0 m N p H m° y ff a O C m m m to m G O N y H m to A 0p 3D CL toQ O N m O � H 0 O 0 m O 0 r n Q' m 0 m a m Z 0 3 N C S ' mcr o_ 00 N d P 0 O m O 0 r n Q' m 0 m a m Z 3 N C 0 Ir mcr o_ c. F 3 December 11,2001 MEMORANDUM TO: Data Users From: Cindy Green, DWQ Che istry Labe Through: Lang Ausley Subject: TOC Samples with data qualifier code The TOC analysis requested on this sample set was not performed due to an administrative decision to discard a set of TOC samples received during this period due to an unforeseen problem with the analytical instrument. Samples appropriately preserved with sulfuric acid have been causing cumulative degradation of the analyzer. This effect was previously unknown. The Laboratory Section has issued guidance to preserve subsequent TOC samples with concentrated phosphoric acid in an attempt to resolve this issue. We apologize for any inconvenience caused by this necessary action. If you have any questions please contact Cindy Green or Larry Ausley at 733-3908. -1-1CACA'UnDn-/-iv pi 000 To-vc=r-.@�'O=viO oop Zc�o(D��oC):E000p Z.0 -0C°-0 m CDa�33 I.M 3 O Q sv �z Cl = 0 3 -n -n W C .0 Ll z `� CD o !� N U)oa — o m Q�o M C CD — � r O 3 Q CD d a /� m J to m m 33K333333 3 003 w a:) cm ocncccmcaCam =Ca 3 3ca (D _ c w KMT:c-noOC')Ow>O-OZZ 0 to to (D C ?a.M 0 � a =; %d. c ' o ' ' ' 0 (n w -� KKO 9:::703 00M CD CD �cQ cin �-0 a a -n ='3 0 o ZZ ca a �.a �,c � N c 00 0 CO W CD r � 0� 3 3 -i`� CO N a� CD sv cD N Z — SD Z CD C I z O m CL 2. Cn 333333333333333c) ca ca ca ca ca CQ ca Ca ca ca ca ca ca Ca a CD CL OCD - no a a. D z ��cn �a a3 �o .. -< 5 3 CD a ol�ni Z Q '� Q 1 VCD aI 0 v O3 N -OZ I r= a a' _. cD 3 1 1 ' oNr—Z 0 c o zl ri Pace Analytical... � yt www.pacelabs.com Pace Analyi,, 9800 Kincey'h. Huntersm,., Phone. 704. Fax. 704.&" DATE: 11/30/00 PAGE: 9 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718849 Date Collected: 11/15/00 Matrix: Water Client sample 1D: V8 Date Received: 11/15/00 Parameters --------------------------------- Results ---------- Units --------- PRL ---------- App. Df -------- Analyzed -------- Analyst CAS# Footnotes ----- - GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane ND ug/t 0.5 1.00 11/29/00 MAG 75-71-8 Chloromethane ND ug/L 0.5 1.00 11/29/00 MAG 74-87-3 Vinyl Chloride ND ug/l 0.5 1.00 11/29/00 MAG 75-01-4 Bromomethane ND ug/L 0.5 1.00 11/29/00 MAG 74-83-9 Chloroethane ND ug/l 0.5 1.00 11/29/00 MAG 75-00-3 Trichlorofluoromethane ND ug/t 0.5 1.00 11/29/00 MAG 75-69-4 1,1-Dichloroethene ND ug/l 0.5 1.00 11/29/00 MAG 75-35-4 Methylene Chloride ND ug/1 0.5 1.00 11/29/00 MAG 75-09-2 trans-1,2-Dichloroethene ND ug/t 0.5 1.00 11/29/00 MAG 156-60-5 1,1-Dichloroethane ND ug/t 0.5 1.00 11/29/00 MAG 75-34-3 cis-1,2-Dichloroethene ND ug/l 0.5 1.00 11/29/00 MAG 156-59-2 Bromochloromethane ND ug/l 0.5 1.00 11/29/00 MAG 74-97-5 Chloroform ND ug/L 0.5 1.00 11/29/00 MAG 67-66-3 2,2-Dichloropropane ND ug/t 0.5 1.00 11/29/00 MAG 594-20-7 1,2-Dichloroethane ND ug/1 0.5 1.00 11/29/00 MAG 107-06-2 1,1,1 -Trichloroethane ND ug/l 0.5 1.00 11/29/00 MAG 71-55-6 1,1-Dichloropropene ND ug/l 0.5 1.00 11/29/00 MAG 563-58-6 Carbon Tetrachloride ND ug/l 0.5 1.00 11/29/00 MAG 56-23-5 Dibromomethane ND ug/l 0.5 1.00 11/29/00 MAG 74-95-3 1,2-Dichloropropane ND ug/l 0.5 1.00 11/29/00 MAG 78-87-5 Trichloroethene ND ug/l 0.5 1.00 11/29/00 MAG 79-01-6 Bromodichloromethane ND ug/l 0.5 1.00 11/29/00 MAG 75-27-4 cis-1,3-Dichloropropene ND ug/1 0.5 1.00 11/29/00 MAG 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.5 1.00 11/29/00 MAG 10061-02-6 1,1,2 -Trichloroethane ND ug/t 0.5 1.00 11/29/00 MAG 79-00-5 1,3-Dichloropropane ND ug/l 0.5 1.00 11/29/00 MAG 142-28-9 Dibromochloromethane ND ug/1 0.5 1.00 11/29/00 MAG 124-48-1 1,2-Dibromoethane ND ug/l 0.5 1.00 11/29/00 MAG 106-93-4 Tetrachloroethane ND ug/l 0.5 1.00 11/29/00 MAG 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/t 0.5 1.00 11/29/00 MAG 630-20-6 Chlorobenzene ND ug/1 0.5 1.00 11/29/00 MAG 108-90-7 Bromoform ND ug/l 0.5 1.00 11/29/00 MAG 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/1 0.5 1.00 11/29/00 MAG 79-34-5 1,2,3-Trichloropropane ND ug/t 0.5 1.00 11/29/00 MAG 96-18-4 Bromobenzene ND ug/1 0.5 1.00 11/29/00 MAG 108-86-1 2-Chlorotoluene ND ug/l 0.5 1.00 11/29/00 MAG 95-49-8 Laboratory Certification IDs KY REPORT OF LABORATORY ANALYSIS I ihnrafy (ertificatio IG NC Wastewater 12 Drinking Water 90,09 NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 Laborator ertification los REPORT OF LABORATORY ANALYSIS Lab rafr ertificati ►o NC Wastewater 12 KY DrinkirYg Water X009! NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 Pace Anafy,,, Analytical r 9,100 Kincey , Hu , -,,,,�Ace Phhoneone.+ 704.E www.pacelabs.coni Fax 704.61., DATE: 11/30/00 PAGE: 10 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718849 Date Collected: 11/15/00 Matrix: Water Client Sample ID: V8 Date Received: 11/15/00 Parameters Results Units PRL --------. App. DF Analyzed Analyst CAS# Footnotes --------------------------------- 4-Chlorotoluene ---------- ND --------- ug/l 0.5 1.00 11/29/00 MAG 106-43-4 1,3 -Dichlorobenzene ND ug/1 1 1.00 11/29/00 MAG 541-73-1 1,4 -Dichlorobenzene ND ug/L 1 1.00 11/29/00 MAG 106-46-7 1,2 -Dichlorobenzene ND ug/t 1 1.00 11/29/00 MAG 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 2 1.00 11/29/00 MAG 96-12-8 1,2,4-Trichlorobenzene ND ug/t 2 1.00 11/29/00 MAG 120-82-1 Hexachloro-1,3-butadiene ND ug/L 2 1.00 11/29/00 MAG 87-68-3 1,2,3-Trichlorobenzene ND ug/l 2 1.00 11/29/00 MAG 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 1.00 11/29/00 MAG 1634-04-4 Isopropyl Ether ND ug/L 0.5 1.00 11/29/00 MAG 108-20-3 Benzene No ug/l 0.5 1.00 11/29/00 MAG 71-43-2 Toluene ND ug/l 0.5 1.00 11/29/00 MAG 108-88-3 Ethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 100-41-4 m&p-Xylene ND ug/l 0.5 1.00 11/29/00 MAG 7816-60-0 Styrene ND ug/l 0.5 1.00 11/29/00 MAG 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/l 0.5 1.00 11/29/00 MAG 95-47-6 Isopropylbenzene (Cumene) ND ug/l 0.5 1.00 11/29/90 MAG 98-82-8 n-Propylbenzene ND ug/t 0.5 1.00 11/29/00 MAG 103-65-1 1,3,5-Trimethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 108-67-8 tert-Butylbenzene ND ug/t 0.5 1.00 11/29/00 MAG 98-06-6 1,2,4-Trimethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 95-63-6 sec-Butylbenzene ND ug/1 0.5 1.00 11/29/00 MAG 135-98-8 p-Isopropyltoluene ND ug/L 1 1.00 11/29/00 MAG 99-87-6 n-Butylbenzene ND ug/t 1 1.00 11/29/00 MAG 104-51-8 Naphthalene ND ug/1 2 1.00 11/29/00 MAG 91-20-3 1-Chloro-2-fluorobenzene (S) 71 % 1.00 11/29/00 MAG 348-51-6 Laborator ertification los REPORT OF LABORATORY ANALYSIS Lab rafr ertificati ►o NC Wastewater 12 KY DrinkirYg Water X009! NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 t.3 3 r 7 �7 � \ \ \ { \ � & � F x C',n h n W c a D O S S O D -! " � � z �• � d 3 0 �y v m N N O `•C o -. N ? p Q p X Q -. O 3 $ t4 S S o c c~Qu -P 1a c nn Linto o a c U3 m x y -! v m o 3 o c nn iv a 0 8 v M y o -t a= y p j 0 C a (A o 3 c Z 3 g �o A ,� a to r v •• .� c LM -n�� ° a A2 -n - Z v Ol m ° -i o Dca 35-10- C d o n r \ m w w 3 LM ° n °• �+ o c s c � 0 a m o0 N v a to 3 - 3 - a o ti A W 14CO A In N c Q I � r C O 7 W W N 7 O U 2 f0 N 3 OQ a v o aIn c p O N V N b -I Cn a O C% i ov 3 C% v s° c x p r En -1 ¢ �o i-3 �o �n m (n O v r O l0 O 3 z . m yi n 3 = L h N 3 N 3 ,�roa :rte Smu �w 3 7 V •LnF OS O N N N 3 ° A ° ° 10 m Jr W 1 H D D o O Z p. M n r T o a C (_n 7 w - 3: 3 N S O .p n i (°71 C', Lr N p g. `G O N W Lm (ill 0 3 o N A �! 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N y 3 3 3 3 3 3 3 c c 3 3 3 3 — — — — — t\ to t\ t\ t\ to to — O y — — — — 3 A 3 0 N 0 tJl fl 1111- N (n o Z m v IM m III m y a D rn = Z n 3 to c tc m e s a o c o a n too o o O. o � o n 3:18 n N f) 3 d N tp l0 N 7 3 V O 3, CL 3 ^ a a (31C' 3 rn a y 3 c' C 3 C - t0 3 C' 3 -3 1� (' 3 v 3 rn v a, M 3 � 14 L" � rn A � rn � y= OO y �Ln ZS o N (iii c N co� t? E 3 A a tr Ul O to V = UI U7 .P 3 fo A ti N c Lo c to c to c m 3 to c to La 3-3 to to c m c I c OIT c to c to 3 c to c to 'c m c to A 3 0 N 0 tJl fl o nv N o cpo fl n S n N S Q c m v p t m 3 m U, m Z = 2 fl too � n 3:18 n n r y � a a x m - 7 3 v a oa n to N A m N02 y= OO y n tD o - Q{ N t? S 0 3 A to = 3 fo A ti N D O N n y A l0 p. y l0 �+ A 3 0 N 0 tJl fl o nv N o cpo fl n S n N S Q c m v p t m 3 m U, m Pace Analytica,., 9800 Kincey Avenlir, ; "Ce Afla�j(t�Cal Huntersville, NC Tel: 704-875-90; Fax: 704-875-909'1. DATE: 12/09/99 PAGE: 9 Pace Project Number: 9210415 Client Project ID: James&James-939533 Pace Sample No: 93419497 Date Collected: 11/29/99 Matrix: Water Client Sample ID: V8 Date Received: 11/30/99 Parameters Results Units PRL App. OF Analyzed Analyst CAS# Footnotes --------------------------------- ------------------- ---------- ------- -------- ---------- ---------- GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane NO ug/l, 0.5 1.00 12/08/99 KST 75-71-8 Chloromethane NO ug/t 0.5 1.00 12/08/99 KST 74-87-3 Vinyl Chloride NO ug/1 0.5 1.00 12/08/99 KST 75-01-4 Bromomethane NO ug/1 0.5 1.00 12/08/99 KST 74-83-9 Chloroethane NO ug/l 0.5 1.00 12/08/99 KST 75-00-3 Trichlorofluoromethane ND ug/l 0.5 1.00 12/08/99 KST 75-69-4 1,1-Dichloroethene NO ug/l 0.5 1.00 12/08/99 KST 75-35-4 Methylene Chloride NO ug/l. 0.5 1.00 12/08/99 KST 75-09-2 trans-1,2-Dichloroethene ND ug/l 0.5 1.00 12/08/99 KST 156-60-5 1,1-Dichloroethane NO ug/l 0.5 1.00 12/08/99 KST 75-34-3 cis-1,2-Dichloroethene NO ug/l 0.5 1.00 12/08/99 KST 156-59-2 Bromochloromethane NO ug/l 0.5 1.00 12/08/99 KST 74-97-5 Chloroform NO ug/1 0.5 1.00 12/08/99 KST 67-66-3 2,2-Dichloropropane NO ug/l. 0.5 1.00 12/08/99 KST 594-20-7 1,2-Dichloroethane NO ug/1 0.5 1.00 12/08/99 KST 107-06-2 1,1,1 -Trichloroethane NO ug/l 0.5 1.00 12/08/99 KST 71-55-6 1,1-Dichloropropene NO ug/l. 0.5 1.00 12/08/99 KST 563-58-6 Carbon Tetrachloride NO ug/t 0.5 1.00 12/08/99 KST 56-23-5 Dibromomethane ND ug/1 0.5 1.00 12/08/99 KST 74-95-3 1,2-Dichloropropane ND ug/l 0.5 1.00 12/08/99 KST 78-87-5 Trichloroethene ND ug/l 0.5 1.00 12/08/99 KST 79-01-6 Bromodichloromethane ND ug/l 0.5 1.00 12/08/99 KST 75-27-4 cis-1,3-Dichloropropene ND ug/l 0.5 1.00 12/08/99 KST 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.5 1.00 12/08/99 KST 10061-02-6 1,1,2 -Trichloroethane NO ug/l. 0.5 1.00 12/08/99 KST 79-00-5 1,3-Dichloropropane NO ug/l. 0.5 1.00 12/08/99 KST 142-28-9 Dibromochloromethane NO ug/1 0.5 1.00 12/08/99 KST 124-48-1 1,2-Dibromoethane NO ug/t 0.5 1.00 12/08/99 KST 106-93-4 Tetrachloroethene NO ug/l. 0.5 1.00 12/08/99 KST 127-18-4 1,1,1,2 -Tetrachloroethane NO ug/1 0.5 1.00 12/08/99 KST 630-20-6 Chlorobenzene ND ug/1 0.5 1.00 12/08/99 KST 108-90-7 Bromoform NO ug/l. 0.5 1.00 12/08/99 KST 75-25-2 1,1,2,2 -Tetrachloroethane NO ug/l 0.5 1.00 12/08/99 KST 79-34-5 1,2,3-Trichloropropane ND ug/1 0.5 1.00 12/08/99 KST 96-18-4 Bromobenzene NO ug/1 0.5 1.00 12/08/99 KST 108-86-1 2-Chlorotoluene NO ug/1 0.5 1.00 12/08/99 KST 95-49-8 Laboratory Certification IDs Laboratory Certifica 1 0D NC DrNC inking Water stewater 37706 REPORT OF LABORATORY ANALYSIS TN Drinking 9009C Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytica .. 9800 Kincey Avenue, ,"ce AnalyfiCal Huntersville, NGS Tel: 704-875-90a Fax: 704-875-9091 DATE: 12/09/99 PAGE: 10 Pace Project Number: 9210415 Client Project ID: James&James-939533 Pace Sample No: 93419497 Date Collected: 11/29/99 Matrix: Water Client Sample ID: V8 Date Received: 11/30/99 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes --------------------------------- 4-Chlorotoluene ---------- ND --------- ug/1 ---------- 0.5 -------- 1.00 -------- 12/08/99 ----- KST -------------------- 106-43-4 1,3 -Dichlorobenzene ND ug/l 1 1.00 12/08/99 KST 541-73-1 1,4 -Dichlorobenzene ND ug/L 1 1.00 12/08/99 KST 106-46-7 1,2 -Dichlorobenzene ND ug/L 1 1.00 12/08/99 KST 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 2 1.00 12/08/99 KST 96-12-8 1,2,4-Trichlorobenzene ND ug/L 2 1.00 12/08/99 KST 120-82-1 Hexachlorobutadiene ND ug/L 2 1.00 12/08/99 KST 87-68-3 1,2,3-Trichlorobenzene ND ug/L 2 1.00 12/08/99 KST 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 1.00 12/08/99 KST 1634-04-4 Isopropyl Ether ND ug/L 0.5 1.00 12/08/99 KST 108-20-3 Benzene ND ug/L 0.5 1.00 12/08/99 KST 71-43-2 Toluene ND ug/L 0.5 1.00 12/08/99 KST 108-88-3 Ethylbenzene ND ug/l 0.5 1.00 12/08/99 KST 100-41-4 m&p-Xylene ND ug/l 0.5 1.00 12/08/99 KST 7816-60-0 Styrene ND ug/l 0.5 1.00 12/08/99 KST 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/t 0.5 1.00 12/08/99 KST 95-47-6 Isopropylbenzene (Cumene) ND ug/1 0.5 1.00 12/08/99 KST 98-82-8 n-Propylbenzene . ND ug/L 0.5 1.00 12/08/99 KST 103-65-1 1,3,5-Trimethylbenzene ND ug/L 0.5 1.00 12/08/99 KST 108-67-8 tert-Butylbenzene ND ug/l 0.5 1.00 12/08/99 KST 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 1.00 12/08/99 KST 95-63-6 sec-Butylbenzene ND ug/t 0.5 1.00 12/08/99 KST 135-98-8 p-Isopropyltoluene ND ug/L 1 1.00 12/08/99 KST 99-87-6 n-Butylbenzene ND ug/L 1 1.00 12/08/99 KST 104-51-8 Naphthalene ND ug/L 2 1.00 12/08/99 KST 91-20-3 1-Chloro-3-fluorobenzene (S) 102 % 1.00 12/08/99 KST 625-98-9 Laboratory Certification IDs Laboratory Certification IDs NC NC Drinking Water tewater '37706 REPORT OF LABORATORY ANALYSIS TN DrinkingSLis water 9°09C TN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. 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J c3333 Co CQ CC Cov Pace Analytical Ser,, naly ocal 54 Ravenscrotr,, Asheville NC 28& Tel: 704-254-7176 Fax: 704-252-4618 DATE: 11/17/98 PAGE: 6 Pace Project Number: 931990 Client Project ID: Kenmure Monitoring Wells Pace Sample No: 9392317 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE V8 Date Received: 11/03/98 Parameters --------------------------------- Results Units ---------- --------- PRL ---------- Analyzed -------- Analyst CAS# ----- ---------- Footnotes --------- Field Services Monitoring Well Data Method: Prep Method: Field pH 5.2 Std. Units 11/03/98 MPS Field Temperature 17 deg C 11/03/98 MPS Depth of Water 5.95 feet 0 11/03/98 MPS Well Volume Purged 2.00 No units 0 11/03/98 MPS Wet Chemistry Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1 Total Dissolved Solids 47 mg/L 1 11/06/98 MAA Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3 Chloride 2.4 mg/L 1 11/12/98 JGJ Ammonia Method: EPA 350.3 Prep Method: EPA 350.3 Nitrogen, Ammonia ND mg/L 0.1 11/09/98 JGJ 7727-37-9 Nitrogen, Nitrate Method: EPA 352.1 Prep Method: EPA 352.1 Nitrogen, Nitrate 0.11 mg/L 0.1 11/05/98 TRW Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060 Total Organic Carbon 6.5 mg/L 0.5 11/12/98 KEK 7440-44-0 Fecal Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Fecal Coliform <1.1 1 11/03/98 MLP Total Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Total Coliform 1.1 1 11/03/98 MLP Laboratory Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 IDs REPORT OF LABORATORY ANALYSIS TN Drinking g WaterCertiat'on 02980 This report shall not be reproduced, except in full, FL Environmental 96317 without the written consent of Pace Analytical Services, Inc. Pace Analytical Se,, 9800 Kincey Avenue, Su Huntersville, NC 28a, Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 9 Pace Project Number: 922633 Ctient Project ID: J&J - 931990 Pace Sample No: 92186691 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE - V8 Date Received: 11/04/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ---------- --------------------------- ----- ---------- ---------- GC -- Volatiles Halogen. & Aromatic Vol. Orgs. Method: SM 6230D Prep Method: EPA 8021 Dichlorodifluoromethane ND ug/L 0.5 11/13/98 CLL 75-71-8 Chloromethane ND ug/L 0.5 11/13/98 CLL 74-87-3 Vinyl Chloride ND ug/L 0.5 11/13/98 CLL 75-01-4 Bromomethane ND ug/L 0.5 11/13/98 CLL 74-83-9 Chloroethane ND ug/L 0.5 11/13/98 CLL 75-00-3 Trichlorofluoromethane ND ug/L 0.5 11/13/98 CLL 75-69-4 1,1-Dichloroethene ND ug/L 0.5 11/13/98 CLL 75-35-4 Methylene Chloride ND ug/L 0.5 11/13/98 CLL 75-09-2 trans-1,2-Dichloroethene ND ug/L 0.5 11/13/98 CLL 156-60-5 1,1-Dichloroethane ND ug/L 0.5 11/13/98 CLL 75-34-3 Bromochloromethane ND ug/L 0.5 11/13/98 CLL 74-97-5 Chloroform ND ug/L 0.5 11/13/98 CLL 67-66-3 2,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 594-20-7 1,2-Dichloroethane ND ug/L 0.5 11/13/98 CLL 107-06-2 1,1,1 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 71-55-6 1,1-Dichloropropene ND ug/L 0.5 11/13/98 CLL 563-58-6 Carbon Tetrachloride ND ug/L 0.5 11/13/98 CLL 56-23-5 Dibromomethane ND ug/L 0.5 11/13/98 CLL 74-95-3 1,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 78-87-5 Trichloroethene ND ug/L 0.5 11/13/98 CLL 79-01-6 Bromodichloromethane ND ug/L 0.5 11/13/98 CLL 75-27-4 cis-1,3-Dichloropropene ND ug/L 0.5 11/13/98 CLL 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.5 11/13/98 CLL 10061-02-6 1,1,2 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 79-00-5 1,3-Dichloropropane ND ug/L 0.5 11/13/98 CLL 142-28-9 Dibromochloromethane ND ug/L 0.5 11/13/98 CLL 124-48-1 1,2-Dibromoethane ND ug/L 0.5 11/13/98 CLL 106-93-4 Tetrachloroethene ND ug/L 0.5 11/13/98 CLL 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 630-20-6 Chlorobenzene ND ug/L 0.5 11/13/98 CLL 108-90-7 Bromoform ND ug/L 0.5 11/13/98 CLL 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 79-34-5 1,2,3-Trichloropropane ND ug/L 0.5 11/13/98 CLL 96-18-4 Bromobenzene ND ug/L 0.5 11/13/98 CLL 108-86-1 2-Chlorotoluene ND ug/L 0.5 11/13/98 CLL 95-49-8 4-Chlorotoluene ND ug/L 0.5 11/13/98 CLL 106-43-4 Laboratory Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090 TN UST List This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services. Inc. v Pace Analytical Seg 9800 Kincey Avenue, Sur,, �,� Ar1a�Vt�Ca� Huntersville NC 2M Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 10 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186691 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE - V8 Date Received: 11/04/98 Parameters --------------------------------- Results ---------- Units --------- PRL Analyzed Analyst CAS# 1,3-Dichlorobenzene ND ug/L ---------- 0.5 -------- 11/13/98 ----- CLL ---------- 541-73-1 1,4 -Dichlorobenzene ND ug/L 0.5 11/13/98 CLL 106-46-7 1,2 -Dichlorobenzene ND ug/L 0.5 11/13/98 CLL 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 0.5 11/13/98 CLL 96-12-8 1,2,4-Trichlorobenzene ND ug/L 0.5 11/13/98 CLL 120-82-1 Nexachlorobutadiene ND ug/L 0.5 11/13/98 CLL 87-68-3 1,2,3-Trichlorobenzene ND ug/L 0.5 11/13/98 CLL 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 11/13/98 CLL 1634-04-4 Isopropyl Ether ND ug/L 0.5 11/13/98 CLL 108-20-3 Benzene ND ug/L 0.5 11/13/98 CLL 71-43-2 Toluene ND ug/L 0.5 11/13/98 CLL 108-88-3 Ethylbenzene ND ug/L 0.5 11/13/98 CLL 100-41-4 m&p-Xylene ND ug/L 0.5 11/13/98 CLL 7816-60-0 Styrene ND ug/L 0.5 11/13/98 CLL 100-42-5 o -Xylene (1,2-Dimethy(benzene) ND ug/L 0.5 11/13/98 CLL 95-47-6 Isopropylbenzene (Cunene) ND ug/L 0.5 11/13/98 CLL 98-82-8 n-Propylbenzene ND ug/L 0.5 11/13/98 CLL 103-65-1 1,3,5-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 108-67-8 tert-Butylbenzene ND ug/L 0.5 11/13/98 CLL 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 95-63-6 sec-Butylbenzene ND ug/L 0.5 11/13/98 CLL 135-98-8 p-Isopropyltoluene ND ug/L 0.5 11/13/98 CLL 99-87-6 n-Butylbenzene ND ug/L 0.5 11/13/98 CLL 104-51-8 Naphthalene ND ug/L 0.5 11/13/98 CLL 91-20-3 1-Chloro-3-fluorobenzene (S) 90 % 11/13/98 CLL 625-98-9 Footnotes Laboratory Certification IDs Laboratory Certification IDs NC Wastewater NC Drinking Water 3TN706 REPORT OF LABORATORY ANALYSIS Drinking Water 90090 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Se,. 9800 Kincey Avenue, Su Huntersville, NC Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 11 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186709 Date Collected: 11/03/98 Matrix: Water Client Sample ID: TRAVEL BLANK Date Received: 11/04/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ---------- --------------------------- ----- ---------- ---------- GC -- Volatiles Halogen. & Aromatic Vol. Orgs. Method: SM 6230D Prep Method: EPA 8021 Dichlorodifluoromethane ND ug/L 0.5 11/13/98 CLL 75-71-8 Chloromethane ND ug/L 0.5 11/13/98 CLL 74-87-3 Vinyl Chloride ND ug/L 0.5 11/13/98 CLL 75-01-4 Bromomethane ND ug/L 0.5 11/13/98 CLL 74-83-9 Chloroethane ND ug/L 0.5 11/13/98 CLL 75-00-3 Trichlorofluoromethane ND ug/L 0.5 11/13/98 CLL 75-69-4 1,1-Dichloroethene ND ug/L 0.5 11/13/98 CLL 75-35-4 Methylene Chloride ND ug/L 0.5 11/13/98 CLL 75-09-2 trans-1,2-Dichloroethene ND ug/L 0.5 11/13/98 CLL 156-60-5 1,1-Dichloroethane ND ug/L 0.5 11/13/98 CLL 75-34-3 Bromochloromethane ND ug/L 0.5 11/13/98 CLL 74-97-5 Chloroform ND ug/L 0.5 11/13/98 CLL 67-66-3 2,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 594-20-7 1,2-Dichloroethane ND ug/L 0.5 11/13/98 CLL 107-06-2 1,1,1 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 71-55-6 1,1-Dichtoropropene ND ug/L 0.5 11/13/98 CLL 563-58-6 Carbon Tetrachloride ND ug/L 0.5 11/13/98 CLL 56-23-5 Dibromomethane ND ug/L 0.5 11/13/98 CLL 74-95-3 1,2-Dichloropropane ND ug/L 0.5 11/13/98 CLL 78-87-5 Trichloroethene ND ug/L 0.5 11/13/98 CLL 79-01-6 Bromodichloromethane ND ug/L 0.5 11/13/98 CLL 75-27-4 cis-1,3-Dichtoropropene ND ug/L 0.5 11/13/98 CLL 10061-01-5 trans-1,3-Dichtoropropene ND ug/L 0.5 11/13/98 CLL 10061-02-6 1,1,2 -Trichloroethane ND ug/L 0.5 11/13/98 CLL 79-00-5 1,3-Dichloropropane ND ug/L 0.5 11/13/98 CLL 142-28-9 Dibromochloromethane ND ug/L 0.5 11/13/98 CLL 124-48-1 1,2-Dibromoethane ND ug/L 0.5 11/13/98 CLL 106-93-4 Tetrachloroethene ND ug/L 0.5 11/13/98 CLL 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 630-20-6 Chlorobenzene ND ug/L 0.5 11/13/98 CLL 108-90-7 Bromoform ND ug/L 0.5 11/13/98 CLL 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 79-34-5 1,2,3-Trichloropropane ND ug/L 0.5 11/13/98 CLL 96-18-4 Bromobenzene ND ug/L 0.5 11/13/98 CLL 108-86-1 2-Chtorotoluene ND ug/L 0.5 11/13/98 CLL 95-49-8 4-Chlorotoluene ND ug/L 0.5 11/13/98 CLL 106-43-4 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS Drinking Water 90090 TN NC Drinking Water 37706 TN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. ;u Pace Analytical Ser, 9800 Kincey Avenue, Sut,. Analytical Huntersville, NC 28U, Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 12 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186709 Date Collected: 11/03/98 Matrix: Water Client Sample ID: TRAVEL BLANK Date Received: 11/04/98 Parameters --------------------------------- Results ---------- Units --------- PRL Analyzed Analyst CAS# Footnotes 1,3-Dichlorobenzene ND ug/L ---------- 0.5 -------- 11/13/98 ----- CLL ---------- ---------- 541-73-1 1,4 -Dichlorobenzene ND ug/L 0.5 11/13/98 CLL 106-46-7 1,2 -Dichlorobenzene ND ug/L 0.5 11/13/98 CLL 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 0.5 11/13/98 CLL 96-12-8 1,2,4-Trichlorobenzene ND ug/L 0.5 11/13/98 CLL 120-82-1 Hexachlorobutadiene ND ug/L 0.5 11/13/98 CLL 87-68-3 1,2,3-Trichlorobenzene ND ug/L 0.5 11/13/98 CLL 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 11/13/98 CLL 1634-04-4 Isopropyl Ether ND ug/L 0.5 11/13/98 CLL 108-20-3 Benzene ND ug/L 0.5 11/13/98 CLL 71-43-2 Toluene ND ug/L 0.5 11/13/98 CLL 108-88-3 Ethylbenzene ND ug/L 0.5 11/13/98 CLL 100-41-4 m&p-XyLene ND ug/L 0.5 11/13/98 CLL 7816-60-0 Styrene ND ug/L 0.5 11/13/98 CLL 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/L 0.5 11/13/98 CLL 95-47-6 Isopropylbenzene (Cunene) ND ug/L 0.5 11/13/98 CLL 98-82-8 n-Propylbenzene ND ug/L 0.5 11/13/98 CLL 103-65-1 1,3,5-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 108-67-8 tert-Butylbenzene ND ug/L 0.5 11/13/98 CLL 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 95-63-6 sec-Butylbenzene ND ug/L 0.5 11/13/98 CLL 135-98-8 p-Isopropyltoluene ND ug/L 0.5 11/13/98 CLL 99-87-6 n-Butylbenzene ND ug/L 0.5 11/13/98 CLL 104-51-8 Naphthalene ND ug/L 0.5 11/13/98 CLL 91-20-3 1-Chloro-3-fluorobenzene (S) 89 % 11/13/98 CIL 625-98-9 Laboratory Certification IDs Laboratory Certification IDs NC DrinkingTN g Water 37706 REPORT OF LABORATORY ANALYSIS Drinking Water 90090 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Sere. 54 Ravenscroh . AnalVtiCa� Asheville NC 288x. Tel: 704-254-7176 Fax: 704-252-4618 DATE: 11/17/98 PAGE: 7 Pace Project Number: 931990 Client Project ID: Kenmure Monitoring WeLls PARAMETER FOOTNOTES ND Not Detected NC Not Calculable PRL Pace Reporting Limit LaboratoryCertification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services.. Inc. Pace Analytical Sego,. /� 9800 Kincey Avenue, Suiit, G Analytocal Huntersville, NC 2801, Tel: 704-875-9092 Fax: 704-875-9091 DATE: 11/16/98 PAGE: 13 Pace Project Number: 922633 Client Project ID: J&J - 931990 PARAMETER FOOTNOTES ND Not Detected NC Not Calculable PRL Pace Reporting Limit (S) Surrogate Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS Drinking Water 90090 TN NC Drinking Water 37706 TN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. r y x x x -4 -a r + a ---IZ 00 z o x •o rO ZO -i W o o N X F9 z o x m z m n � 3 Q > a o C g g rn 3 N—� S = � � c pp� ,••� b O N 2 3 m a c � g•. z b U y rt 00 E x A U T U � A U p a H p 10 1S g S � 0 o 2 A x N H o o O O N w A 4 OOi ^ n 3 3 3 e e 3 f c , 3 ,-- 3 c e e e c 3 e e c c N 6 w W W N O U � 3 3 3 3 c 3 3 7a. 3= � 3 g 3 3 t'' t� t'' e' e' e� t� c� N [' ['' C 3 e�• t�- C' r y x x x -4 -a r + a ---IZ 00 z o o •o rO ZO -i W o o N X F9 z o x $ z � n � 3 Q > o C G b rn 3 N—� S � � c pp� ,••� b �• 3 3 3 0. �• A z b U O rt 00 3• v A U T U � A U p a H p 10 1S g S � U A N H VPUi O O O A 4 OOi ^ n 3 3 3 e e 3 f c , 3 ,-- 3 c e e e c 3 e e c c n N r y ado c. n7 � -4 -a r + a ---IZ 00 z o o O � d 9 w> n m 9 w a x x F9 z o x $ z � n � 3 Q > o C G b rn 3 N—� S � � c pp� ,••� b �• 3 3 3 0. �• A z b QQ� 00 3• v A U T p A A U p a H � U A V�Ui H VPUi T ^ n c c e e 3 f c , 3 ,-- 3 c e e e c 3 e e c c r y ado c. n7 � -4 -a r + a ---IZ 00 z o o O � d 9 n m a x x F9 z o x $ z � n � 3 Q > o C G b S z ,••� b � �' o �• C z b C 0 00 On � to rt � � C ^ n R r y ado c. n7 � n 0 + vOi ---IZ 00 O O � d 9 n m O 3 Pifl F9 z o x z � n � 3 Q > o C G b S z ,••� b � �' o �• C z b C 0 00 a o s o 3 0 y S n7 � m o rn N m z O � d 9 n m O 3 Pifl F9 z o x n � 3 z > o C G b S tf ,••� b � �' 3 �• C z b C 0 � � C 77 1-1 y n7 � cn w m z n m z o x n � 3 C G b K y cn w U C CD r- -n --i -a dam �0 3 mm � CD ODS= O° 0 CD O o o "Z v 0 Q D� Q o �o —moi N C Z's�c O r ca a O \ OQ O O n n O m n D D 'o -1 --10 0 0 „ O �' S w n w �- _ o ��� m a CD C R Cn O O O O p 0 p w Q ID N a =' �0 w r nc - Q A M CD o o m o CD w .� .� K o 3* O N m 3 a oa cn 0 _W O O m O = o x a CD A .O .0 N eC c y TI Ti w - A 0 x m O 0 = = 3 'D n O 0 O cn n O CD w a M W 3 o� r -13 3 w o co A 0 N G S 1 m O_ CD y (7 Na = o A_ CD a C13 w O =r CL to :a U O O W O i. 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CL CDc CL z cD 3' co m c 0 9 0) J1 m 1� 1 (Q (Q (Q CQ (Q (Q corpT`�„,;zo Q O0 CL z cD 3' co m c 0 9 0) J1 m 1� 1 O corpT`�„,;zo Q O0 o D� w m w m m m m m m Mo w -•o W(D 0 O -P cn cn °� 0 (D conn,<-a� w cO m z-0 O� �; wo CD3 w o m w -Do w O o w. r o m r- 0 CD =a c m O mim 3 m =c CD I I D r O_� %Q > �^ 3 cn U)m A c m w m a m c 0 , 0 Oyn. CD W Cr cr m /9 T� r COAD �0 O n o 3 3 a -q = -0 m m c C)cn Cc j� W:3 5- :2 > W Z CD p> w _ r m o_ -rl m 070 m cn w m c v 3 o p CD ,< Z m c m -n-0 v D •�" mCl)° oma Z r p rev -I a mall -a -= a n mm CL z cD 3' co m c 0 9 0) J1 m 1� 1 O M N CA Q O0 o 0 v C m -0: w D -� O -P cn cn Dm 0 (D O c v cO n a z W -Do w mp-Uo'C m z o m r- 0 �omoM O m 21 CD I I N a > �^ O �CD m o o � mm v C w 0- O D -� O -P cn cn N 0 (D O c v O'.. n a z W -Do w o o m r- 0 z O -P cn cn O -a c CD :0�� ° m -Do w v r- 0 m 21 N m N a CD Mr. Harry James Page 9 Client Reference: J&J Kenmore PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS Pace An,,, 9800 Kinsey A, Hunter: TO 704-8,, Fax: 704-8754), December 02, 1997 PACE Project Number: A7111, 93 0487742 11/17/97 11/19/97 Kenmore MW Units PRL V8 METHOD DATE ANALYZED VOLATILE ORGANICS 6230D Dichlorodifluoromethane ug/L 0.5 NO 11/26/97 Chloromethane ug/L 0.5 NO 11/26/97 Chloroethene (Vinyl chloride) ug/L 0.5 NO 11/26/97 Bromomethane ug/L 0.5 NO 11/26/97 Chloroethane ug/L 0.5 ND 11/26/97 Trichlorofluoromethane ug/L 0.5 NO 11/26/97 1,1-Dichloroethene ug/L 0.5 NO 11/26/97 Dichloromethane ug/L 0.5 NO 11/26/97 trans-1,2-Dichloroethene ug/L 0.5 NO 11/26/97 1,1-Dichloroethane ug/L 0.5 ND 11/26/97 cis-1,2-Dichloroethene ug/L 0.5 ND 11/26/97 2,2-Dichloropropane ug/L 0.5 NO 11/26/97 Chloroform ug/L 0.5 NO 11/26/97 Bromochloromethane ug/L 0.5 NO 11/26/97 1,1,1 -Trichloroethane ug/L 0.5 NO 11/26/97 1,1-Dichloro-l-propene ug/L 0.5 NO 11/26/97 Carbon tetrachloride ug/L 0.5 NO 11/26/97 1,2-Dichloroethane ug/L 0.5 NO 11/26/97 1,1,2 -Trichloroethene ug/L 0.5 NO 11/26/97 1,2-Dichloropropane ug/L 0.5 NO 11/26/97 Bromodichloromethane ug/L 0.5 NO 11/26/97 Di omomethane ug/L 0.5 NO 11/26/97 ,cis:1,3-Dichloro-l-propene ug/L 0.5 NO 11/26/97 :trate-1,3-Dichloro-l-propene _. ug/L 0.5 NO 11/26/97 1�1,A- Trichloroethane ug/L 0.5 NO 11/26/97 _1,3-[fthloropropane ug/L 0.5 NO 11/26/97 Jetrae.hloroethene ug/L 0.5 NO 11/26/97 IDI-b�rorffik, h1oromethane ug/L 0.5 NO 11/26/97 Dib-ro%moethane ug/L 0.5 NO 11/26/97 1,1;'J' 'Tetrachl nM N g T -11 ug/L 0.5 NO - 11/26/97 Brornoform ug/L 0.5 NO 11/26/97 .. �a�,14� � 8 1998 t aboratocy Certfication IDs uruur,73' , t7n Laboratory Certification IDs NC Wastewater 12 ¢fir'° "s ' � F LABORATORY 7 ANALYSIS KY Drinking Water 90090 NC Drinking Water 3706 TN LIST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc Mr. Harry James Page 10 Client Reference: J&J Kenmore Pace Aria, 9800 Kincey A,. Huntersvih . Tel: 704-8t, Fax: 704-875-9L December 02, 1997 PACE Project Number: A7111, PACE Sample Number: 93 0487742 Date Collected: 11/17/97 Date Received: 11/19/97 Client Sample ID: Kenmore MW Parameter Units PRL V8 METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 0.5 ND ug/L 6230D 1,1,2,2 -Tetrachloroethane ug/L 0.5 NO 11/26/97 1,2,3-Trichloropropane ug/L 0.5 ND 11/26/97 Bromobenzene ug/L 0.5 NO 11/26/97 2-Chlorotoluene ug/L 0.5 NO 11/26/97 4-Chlorotoluene ug/L 0.5 NO 11/26/97 1,3 -Dichlorobenzene ug/L 0.5 NO 11/26/97 1,4 -Dichlorobenzene ug/L 0.5 NO 11/26/97 1,2 -Dichlorobenzene ug/L 0.5 NO 11/26/97 1,2-Dibromo-3-chloropropane ug/L 0.5 ND 11/26/97 1,2,4-Trichlorobenzene ug/L 0.5 NO 11/26/97 Hexachlorobutadiene ug/L 0.5 ND 11/26/97 1,2,3-Trichlorobenzene ug/L 0.5 NO 11/26/97 Benzene ug/L 0.5 ND 11/26/97 Toluene ug/L 0.5 ND 11/26/97 Chlorobenzene ug/L 0.5 ND 11/26/97 Ethylbenzene ug/L 0.5 NO 11/26/97 Xylenes, (total) ug/L 0.5 NO 11/26/97 Styrene ug/L 0.5 NO 11/26/97 Isopropylbenzene ug/L 0.5 NO 11/26/97 n-Propylbenzene ug/L 0.5 ND 11/26/97 1,3,5-Trimethylbenzene ug/L 0.5 NO 11/26/97 t-Butylbenzene ug/L 0.5 ND 11/26/97 1,2,4-Trimethylbenzene ug/L 0.5 NO 11/26/97 s-Butylbenzene ug/L 0.5 ND 11/26/97 4.-I sxTropyltoIuene 4 :� n- B 1 benzene =`AY�nhi�'�l rnc Laboratofy Certification IDs NC Wastewater 12 NC Drinking Water 37706 Sc 99006 D JAN- 8 1998 Groundwater Section Asheville Re Tonal Office ug/L 0.5 ND ug/L 0.5 NO ug/L 0.5 NO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 11/26/97 11/26/97 11/26/97 Laboratory Certification IDs KY Drinking Water 90090 TN UST List VA Drinking Water 213 111 IIII!II( I I l I �I I 1 I i 13 i _ Y z z- G _ n z n L I I z p� J _ I I � I J N 111 IIII!II( I I l I �I I 1 I i 13 i _ Y z z- G _ n z n - z p� J _ J N — tn P_ Cn = J A? - A W O Z?, 7 _— - - - - k r� O O j O O O ; O N w U 7 i = 111 IIII!II( I I l I �I I 1 I i 13 i _ J N Cn = J A? - A Z?, 7 - - - - 111 IIII!II( I I l I �I I 1 I i 13 i _ D D --i a I� n cn a m O= C,m ! 07 a = 75 7 o O v «� ID O — LQ - -i C7 h '7 0 CO C7 D I D � ' '17 ; —I 0 0 C7 � 0 17 7 i 1 O Q CD z Q wly = o olc D o j njc c Iz - w w IJ O n D cU-3 77 I ✓ �I `� I` ,i'7 -r Ix o o —,Y) V1 rol I'D ✓y I Iii � ', j i I I i � � I I� i �� � I On ISI w to v j = h 'Ic rD h. h iU h jM 11 n ��� � � io r- � �� z Imo. I^ s - 1:1 El n It�Jn ^io o o j �J Cn r O _Q (n CD ( o O CO h: _ C-) m m h I ClVj. I I I N — r QL cD Ir M I � I zl�I��12 C7 SIC 'Cui DIDF>11� On I� io �� �� in IO, I�� Im i� cn + �• �tj lz C;lIco m ID � rn ' c i I ' I i I m Ti m r r co 3 3 CD �I D n C C c 0 3 o M o. n CD r r t n30'0� o A m -a �2y 0 a. 3 �i 3 3 n wo 3 - � r wZ :3O w w ?o O CL :: cn 0 C)0 o C 0 0 w m �� 0, 3 y 3 Z 0 ro 3 o U� -Q 00000 D. o D C 0 co n D D •0 U)U) ��� m -4 -i o o 0 a l< o s 2• w c, w x T = 7m0 �• c CL m m C O o 0 O O O o 0 o I0 w o w w w a Q Q n o o C7 C7 D n 3. a° _ Q o >> N W m p C a rn CJ7 r m m c -+ ' w O Z a m ' 3 o 3 3 o o w v C 3 oa m w m 2 M -4 n m my o O Co O = O X m A .� w CD N 0 Z 41 x m A ,p O � OD A m Q Z O m (D' G) N is in a w w N j 1 m a o� 0 Ut 3 n c C I 3 cQ 3 � 3 3 co 3 3 co C = -c 1.3 2 -I 3 j1 0 3 0 3 3 co= 3 3 O Ul T Z Z Q (n Cn (n = 2 n C7 0 O = G 0� c c N w a w Q o to w+w a a m CD o� oa cn w Z O o Z A A u, y m 0 C m aa'° v a) ' ° m a Cl) o= 0-1 -4 mw y Ch Ch co O?WW v' Z o 0 o 0 CA) CD co o N � R c G 0 3 3 3 3 3 3 3 3 Z c 3 3 3 3 N fA 'v Z Z T. 2 m 0 n n n W D D D = m Q w= co m e a w w y Z o - n n Oo D C fn o N CD CD 0 N w_° 0 =r 0 0 0 w• m 3. m c' c� 3 c Cl) i� rn 3 rn A w m c' 3 w a 3 3 0 V - m 3 rn m cn P,4 a.. cOn vii m rn N Ln cn 0 N N W Oi V1 v Ln c c c 3 c 3 3 c c c c c 3 c c c C 22w 23 Waococo po 0 =m w 0 w 0 ooG�`D CD -�y O co ' Q.�� X o -w -2. cu . m c o O (D N 5- n m w N m 0 u) N = f0 w N o C "CI O' C O N n. w W �° R 2 CD D cn a a Ol 0 C1 CD to m n m u1 3 o M o. n CD r r t n30'0� o A m -a �2y 0 a. 3 �i 3 3 n wo 3 - � r wZ :3O w w ?o O CL :: cn 0 C)0 o C 0 0 w m �� 0, 3 y 3 Z 0 ro 3 o U� -Q cc D. o D C 0 O0 -n 0 D U)U) ��� -nCD 0 vC� � D 0 a � r- (n 1. m m a �] c 7m0 �• c CL m v 0 o � l< m 3 Cl)CL 0,6 o o o O �� m �' D E: o (D O w w a 0 n W �2o n m (n d N m p ^�1 �j20 o CJ7 3 o M o. n -i r r t 3 �2y �l N Co m 0 O 3 �i 3 3 n wo 3 - � o v :3O S � 1 p C 0 0 w m �� 0, 3 y 3 Z n ro .3 w= c cc D. o D O u) 0 Cl) o O C7 m a �+ �+ E;n m w CT D > 7 3 o M r� U r r t �2y �ei"� N3 3 yrs 3 - � o v m � 1 C 0 0 3 o M C) 3 o v C 0 p3 Z C 0 Cl) o O C7 m a �+ �+ E;n m w CT D > 7 m m a �] c 7m0 �• c CL m v 0 o � l< m 3 A = m c m W m m �' D E: a +c a a �2o n m (n d CL �j20 o C�- -+ ' �" O Z a 3 J � 0) �° O W m CD 2 M n m my C n C CD Z 41 w � = Q (D' CD Cn � --I V) Cl) -U y --l7) D C) �70 2 t) t / \ J _0 %070 C � W - =0=�'o 000 D~:C o CD CD �.Q zro y do z30 n CD E c CD CD CD 33 < o 3 w -nzm �.�� w CD o 7o CD3 Q- P. r - o 00—� mm = C:< 3 �z D a -0 CD c 3 ra cnIn 1- Cf CD N �? 0 O n 3 m CD a 7o 0 a CD m 0 - n O CD W o- 0 Cr CD @ �_ O O O CD r m n' n w CD 0 o 3 U 3 m CD a W l 0 Z ^' 0 0 CO CD CD CD o r cr mm m �, m m v3 w CL D D z CD O CD T a , D 9:cn TI 3 C ca m O v QCD `Q 3 0 ® "n T ro 3 3 3 3 3 3 3 3 3 .1 .L 53 C)03 CQ CO O CS] (Q CQ (Q CQ CQ (Q r r CCZ 3 3 cc ZKKT2-nC�000WD-Uzz W �(Q (Q CD o —bra KK� K� O w C: 0CCD Q w (Q w n O-oc-o 3 a O , _3 O z Z WCD= co ��c 3C: (n 3 O3 m33� acl'zZ — w cnP N'o 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3� co cQ cQ co � cQ co co co co cQ cQ cQ cv cQ � 00 O O CD D cn O CD � n z M. o o 3 O C: a co Q -UN-0Z CD =3 CT —. CD = , o NrZ CD 0 O (D C7 Q CSD "O CO CD =3 CY- uCi O 3 3 3 CQ (Q (Q (Q (Q (Q /O 0 DW CD W 07 -O CD CD CD CD E m � o O < o 3 w -nzm �.�� w CD o 7o CD3 o a P. r - o mm = C:< 3 �z D a -0 CD c 3 ra cnIn 1- Cf CD 3 m CD a 7o a CD m n O CD `° !R W o- 0 Cr CD @ �_ O O O CD r m n' n w CD 0 o 3 U 3 m CD a W l 0 Z ^' 0 0 CO CD CD CD o r cr mm m �, m m v3 w m V, 0 D D z CD O CD T a , D 9:cn TI 3 C m O v QCD `Q 3 0 ® "n T ro m v n m a M N o w O z O Z D O CD CD w O 0 w o nri CD w a w 0 O D Q m 0 0 0 CL Co0 O -u U) co CD ° C CD c' N 7 lC] C n p °i w -00 0 "r t 0 � w 71 N m 0 a CD 0- Z m 3 N CD N 7D < m m c0 mo-uoc v 0 M a) 0Cf) n M D y� r Om m m c M� ._� o 0 z m z 0 CA K 0 z O x m 0 Mr. Harry James Page 11 FPX NO.i 704 252 4618 12-31--96 Park kQtfv-ai Aslwoilke, NC Client Refclrence, J and J Kenmore Tei -CA-254-7176' Fax 7D4-2524618 December 04. 1996 PACE Project Number: A61120600 PACE Sample Nimber: 93 0305954 Date Collected: I M Mr. Harry James Page 11 FPX NO.i 704 252 4618 12-31--96 Park kQtfv-ai Aslwoilke, NC Client Refclrence, J and J Kenmore Tei -CA-254-7176' Fax 7D4-2524618 December 04. 1996 PACE Project Number: A61120600 PACE Sample Nimber: 93 0305954 Date Collected: 11/20/96 Date Received: 11/21/96 Client Sample 10: Kerifficre Parameter Units PRL V8 METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Dichlorodifluoromethane ug/L 1.0 ND 12/01/96 Chloromethane uq/L 1.0 N1 12/01/96 Chloroathene (Vinyl chloride) ug/L 1.0 NO 12/01/96 Bromomethane uq/L 1.0 NO 12/01/96 Chlaroetharle uq/L 1'0 NO 12/01/96 Trichlorofluoromethane ug/L 1.0 NO 12/01196 1,1-Dichloroethene ug/L 1.0 NO 12/01/96 Dichloromethane Ug/L 1.0 NO 12/01/96 trans-1,2-Dichloroethene uq1L 1.0 NO 12/01/196 1,1-Dichloroethane uq/L 1.0 NO 12/01/96 cis-1,2-Dichloroethene, ug /L 1.0 NO 12/01/96 2,2-Dichloropropane U9,21 1.0 NO 12/01/96 Chloroform ug/L 1.0 NO 12/01/96 Bromochloromethane ug/L 1,0 NO 12/01/96 1,1,1 -Trichloroethane ug/L 1.0 NO 12/01/96 1,1-Dichloro-l-propene uq/L 1,10 No 12/01/96 Carbon tetrachloride ug/L 1.0 NO 12/01/96 1,2-Dichloreethane ug/L 1,10 NO 12/01/96 1,1,2 -Trichloroethene ug/L 1.0 NO 12/01/96 1,2-Dichlorapropane uq/L 1.0 NO 12/01/96 Bromodichloromethane, ug/L 1'0 NO 12JOI/96 Dibromomethane ug/L 1.0 NO 1.2/01/96 cis-1,3-Dichloro-l-propene ug/,L 1.0 NO 12/01/96 trans-1,3-Dichloro-1-propene ug / IL 1.0 No 12/01/96 1,1,2 -Trichloroethane ug/L 1.0 NO 12/01/96 1,3--Dichloropropane ug/L 1.0 ND 12/01/96 Tetrachloroethene Ug/ L 1.0 NO 12/01/96 Dibromochloromethane ug/L 1.0 NO 12/01/96 1,1,1,2 -Tetrachloroethane ug/L 1.0 NO 12/01/96 Bromoform uq/ L 1.0 NO 12/01/96 1,1,2,2 -Tetrachloroethane ug/L 1.0 NO 12/01/96 REPORT OF LABORATORY ANALYSIS This rerory shat not be reproduced except in full without Viewrilien consent of Face Analytcai Se!Ces Inc mL FPX NO. 704 252 4618 12-31-96 Pace Analytical Sc. -2 A54 Ravens,. A=x wtical Asheville, NC 28o, Mr. Harry Jamez Page 12 Client Reference: J and J Kenmore Tel: 704-254-17176 Fax. 704-2524618 December 04, 1996 PACE Project Number: A61120600 PACE Sample Number; 93 0305964 Date Collected: 11/20/96 Date Received; 11/21196 Client Sample ID: Kenmore Parameter Units PRL V8 METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 1,23-Trichloropropane ug/L 1.0 No 12/01/96 Bromoberzene uq/L 1.0 NO 12/01/96 2-Chlorotoluene uqlL 1.0 NO 12/01/96 4-Chlorotoluene ug/L 1,0 NO 12/01/96 1,3-Dichlorobenzere ug/L 1.0 NO 12/01/96 1,4 -Dichlorobenzene ug/L 1.0 NO 12/01/96 1,2 -Dichlorobenzene Ug/L. 1.0 NO 12/01/96 1,2-Dibromo-3-chloropropane Uq/L 1.0 ND 12/01/96 1,2,4-Trichlcrobenzene ug/L 1.0 NO 12/01/96 Hexachlcrobutadiene uq/L 1.0 NO 12/01/96 1,2,3-Trichlorobenzene ug/L 1.0 NO 12/01'/96 Benzene uq1L 1.0 NO 12/01/96 Toluene ug/L 1.0 NO 12/01/96 Chlorobenzene ug/L 1.0 ND 12/01/96 Ethylbenzene ug/L 1.0 NO 12/01/96 Xylenes, (total) ug/L 1.0 NO 12/01/96 Styrene ug/t. 1.0 NO 12101/96 Isopropylbenzene ug/L 1.0 NO 12/01/96 n-Propylbenzene ug/L 1.0 NO 12/01/96 1,3,5-Trimethylbenzene uq/L 1.0 NO 12/01/96 t-Butylbenzene uq/L 1.0 NO 12/01/96 1,2,4-Trimethylbenzene ug/L 1.0 NO 12/01/96 s-Butylbenzene uq1'L 1.0 ND 12/01/96 4-Isopropy'ltoluene uq/L 1.0 NO 12/01/96 n-Butylbenzene ug/L 1.0 ND 12/01/96 Naphthalene U911- 1.0 NO 12/011/96 REPORT OF LABORATORY ANALYSIS Tris rsapnrl st-11 not oe e&prcdoced ma ept n full w0o,.,t the wro!!er, 'onsenl of Pace Analv!icai Semces Inc 0 m 2 O 7 r c lona ton i y - �-4 Or; C O C a 9 a 0 D� D O O � IN A C w IF G ' tan O N A wD H �- ? c' ry 9 m N � v �' -• c � 3 C7 m F O a� n c a. v o r QBEG 'n" Z O 7 z ..I z z ',A O y - O — � C C 9 S S 6 S 6 � IN A C w IF G ' tan S N A wD H �- ? c' ry 9 m N � v �' -• c � 3 C7 m F O a c a. v QBEG 'n" U W 5' w b to n Ol O N O `b' O O A 0 O O p U A o ry a H r m r rp r (e- Is- � Q* -3 r" Q.- 3 3 r r r r r r r N 3 N c m o- Z z= n ',A S A f7 n a m © 1p a Y IN 2 IF wD �- ? c' ry 9 m N � v �' -• c � 3 C7 m F a c a. v 'n" 5' w O p U A o ry a H � rt rt c n ',A a ?oo C7 m F a c a. v 'n" 5' w A o ry a H � rt rt c n d rt, n _0 3 m 0 0 0 o Ci 0 c� w 0 0 a0 ) D7 �_ m 0° 0 0o0' ° o 0 0 d- w g? w v ?.� A T. c cr a� 0= ° ° o (D �3.a= a 0 a �' `c m o.. 3 r= ca C C X w W 14 OI �= O c T. W A X A O CO .ja CD O CD o t1l is in a w ni N A A a w cn O Ln O A 0 �e 0 a 3(3( _ CQ -= 3 (:, B = m 0 0 o = _ m Ig• a- o- o y, + N a m m O ° m M a cn W Z O Z A p n o N w N rn m o a cn cn O v vcoi N a)N O O Al ° W (.nZ � o 0 W 6 0 m 0 N C 0 3 3B 3 3 3 o nc 3 k 3 — M Z y K x = a m c 0 ai D D (D K a) m Nr (n m Z o° o n? m w D (n 3 A7 m °- = A7 0 o 0 o a o ww m 3 < m E- CCD C m c' c 3 o c a CD 3 G N C A �! 14 A cn A ccn CD 3 . O ((n m d. a) �+ C" c71 M °f 0. CA. 0 cn 0 0 N (071 0 N CO 0 V co A c c c c 3 c 3 3c c c c c 3 c c c c 0 v o m Z o O O 2 2 m 3 °-o o m CD CDD CDD O O M m 0 m & -0 = � ° (DN� w m w a CD C D ?- CDCD 0 0- V1 N y D m CO0 n a CD m cD r T D--0 CCCD M j�CA� cA �Dmmoa.00 rU .i wCL 03 o=D v Q oDcc O ro Do. W ro �c r- (c D (nm32� �p z -0 t�, ro �O.R O CD ro a M 0 ��� c QLA m a n Q z QA 0 mm0 °eo c o 0 U 0 7.7 1 =r U °Q C 0 0 =7(n0r0 CD R D a33�W CD A 0 Z r S� _ m O3 rl -nm m w� C m -� m� 3 � ri IN 4 SCD O 0 Z n v .) t 3 r 3 m0."vc Z. -A �' m m cr c Zv C m o LD Q 1 ' T -t CCD c CD a lc (n m 3 v c o �J 3 n. G Q 0 i U C 0 ro !t 0 C= CIO4 v_ N O z v 0 m� z3 C 0 w 0 z0. mm m= z<_z noo r� Z X- �(D md� Mss M- o CL �zm o� C v( A aW m� mA c� m 0 1 O z CD cn Al A oho cD o co Q 3 co co �• co I C I IcQ c� r- TI D --i -a C/) f D -0 m Sdo� c C ' c o D moQ p o a O �o > � Z � o a, in >S o S y SZo m - :0 �Z D cn 32 ; m O D cin t�- " P, r- R, -CD r� i < n p 7 - Cn Oo to�W CL :]maA v o O 0 a 0 4 � 2 O -g : o :o ka V' SD CD o �� Ln ell �c 0 cnor0 m CA U)c CD p o \ �Z r Q o o = m m KN D m SL z w � o m �� O❑ Q a 3 (1\ Tt m �• �Z w-0 C m cc O 3 - o 'a Udo m m C) z r � � �I It o Ni I c, I Z „< CD OD Q �mc 2 c� plo 0 0 0 0 Ao .511 I CD o 0'000 CD a y a a � o' o (D 2 �, C v 0 3 0 1 V CA rn 3 ? c N w A C � O_CD -A s Ln O CD 0 i t r i :3 CD c Al A oho cD o co Q 3 co co �• co I C I IcQ c� r- TI D --i -a C/) f D -0 m Sdo� c C ' c o D moQ p o a O �o > � Z � o a, in >S o S y SZo m - :0 �Z D cn 32 ; m O D cin t�- " P, r- R, -CD r� i < n p 7 - Cn Oo to�W CL :]maA v o O 0 a 0 4 � 2 O -g : o :o ka V' SD CD o �� Ln ell �c 0 cnor0 m CA U)c CD p o \ �Z r Q o o = m m KN D m SL z w � o m �� O❑ Q a 3 (1\ Tt m �• �Z w-0 C m cc O 3 - o 'a Udo m m C) z r � � �I It o Ni I c, I Z -1112 „< CD OD Q �mc .511 I o si m m CD a y L O m o (� (D 2 �, C v a Q •c 0. 1 V CA T CD 3 CD m l N -1112 „< n3 Q �mc .511 I si m m n. (D ::3 2,- O m o (� 2 �, C v a Q •c 1 V CA T CD 3 CD m l C -A s i t r i 'D71 a W ED m 1 ` 1 0 0 G\ VLZ = C °1 CCIL v m v_ 0 z O� „m m� z� 5 CD S 7 0 Z -. C m zsz Doo r� w D = S D~ S n and m M7 m_ o aM d 0 O� C cm z— v M, . m --i C M -� m� (� m 0 O z a \ CD z 0 4- (A N � C Q 2 O 7 �N r B' O � Q 0 .5 m m m O m z v n C ■ �* oCf) c -0 7 D��2Pc S O 3•mmo��o� o6 W. 0 RD 8 2-Q. O o -�CL Cl)z TT 335333333353 003 co Co ocQcococccccccc ;: cc 3 aCC zKK;=TOOROF>Tzz w0cs? 0= o o cn m 007� o Z Wmc�C: `. X333 om` w z z EnD T 333333333333333 co co co CC co co cc cQ cQ co cn co cQ co to -0N-0Z CD O Cy (n �.NrCD Z O CD 0 CW)_ (D 3 -- 0 C=D C -c uCL, 0 C CD rA C C C CQ CC.0 3 3 3 CQ CQ C� Om c 70;Z2 m -D o p 0 0 SO wm_� 0 0 S CD m o i 0 c m o` z Ln p ocn 9)s s. 'R- F m � ac g. mo o v � m c a m m DO z c K co m �o 70 m fJ C M m O v Om c 70;Z2 m -D o p 0 0 SO wm_� 0 0 S CD m o i 0 c m o` z Ln p ocn 9)s s. 'R- F m � ac g. mo o v � m c a m m DO z c K co m �o 70 m fJ C M m O -10.21 ID:PACE INC. TEL NO:252 4618 ® e� Ra+wna s� t+�or AnMpliOol 9elrvtaa, ►s 4� I ca l nlR0M ha SNC !9101 Tel. 704-l94-7170 i®t: 104.2$1-+919 Mr. Harry James Page 14 Client Reference: James 6 James February 07, 1996 PACE Project Number:'A6012260 FACE Sample Numbers 93 0173677 Date Collected: 01/22/96 Date Received: 01/23/96 C1 iant Sample I6: Qgg V$ Parameter Units MDL #V6_ DATE ANALYZED 1,2,3-Trichloropropane ug/L 1.0 NO 01/24/96 6romobenzene ug/L 1.0 ND 01/24/96 2-Chlorotoiuene ug/L 1.0 NO 01/24/96 4-Chlorotoluene ug/L 1.0 NO 01/24/96 1,3 -Dichlorobenzene ug/L 1.0 ND 01/24/96 1,4 -Dichlorobenzene ug/L 1.0 ND 01/24/96 1,2 -Dichlorobenzene ug/L 1.0 ND 01/24/96 1,2-Dibromo-3-chloropropane ug/L 1.0 ND 01/24/96 1,2,4-Trichlorobenzene ug/L 1.0 NO 01/24/96 Hexachlorobutadiene ug/L 1.0 NO 01/24/96 1,2,3-Trichlorobenzene* ug/L 1.0 ND 01/24/96 Benzene ug/L 100 NO 01/24/96 Toluene ug/L 1.0 NO 01/24/96 Chlorobenzene ug/L 1.0 NO 01/24/96 Ethylbenzene wg/L 1.0 ND 01/24/96 Xylenes ug/L 1.0 NO 01/24/96 Styrene ug/L 1.0 NO 01/24/96 Isopropylbentene u9/L 1.0 ND 01/24/96 n-Prcpylbenzene ug/L 1.0 NO 01/24196 1,3,5-Trimethylbenzene ug/L 1.0 ND 01/24/96 t-Butylbenzene ug/L 1.0 NO 01/24/95 1,2,4-Trimethylbenzene ug/L 1.0 NO 01/24/96 s-Butylbenzene ug/L 1.0 NO 01/24/96 4-Isopropyltoluene ug/L 110 ND 01/24/95 n-Butylbenzene ug/L 1.0 NO 01/24/96 Naphthalene ug/L 1.0 NO 01/24/96 MAR 1 31996 �]nwp biz -. vvDN0 x 133 1 s o � W D Z�cn W :3 -C 3 2 0 -n ` D �P U � � b CD n Z w c � � =• � 0 n a 7t7 Z O A w 0 33 O o40 Z 1 m_ ➢a � g IS, U CD p33 �W CD 0 0 N O �. 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Q N 3 �,O Qs o = mcn o 1 Q cncr w`to z z z o -n crN • w, v M CD � 0 cn m r-'• Q OD 0 m 7C w m C/) 07 ,. m m o c n CD o 0� 0 Co := z w Q= r =• (D o N CD � t m n < o ro (D - � c m O N v n3 av a z cc) ?5' m ° Q � OD o �' 0 cQ CD 0_ Z A O :3 O ro ro z •pro ®, m c cn — g n mphi N CD 0 3 0 0 CLc _0_ CD CD z z CD c y I z 0 � K w • _ -n N O -i � Fn z w — O CL 0 --j v, Q3 c�D •o Cl) D M o �_ � v � N aQ C n m N vLn 0 � n f mm JI Q (D O 9 0) m m CL V N cn cn --4.o m 0 m v 0 CD ID M o = c-� 03m z z z o v -o :?� 0 � D z O � M 0 c cn6,m CD 0 � D w A o m m o c ro w a w o y UT M D � -n � c m O N v �. a z ?5' m OD o W m O :3 O z CLc CD I z p •o Cl) M �_ � � N aQ C n m N f w m T! N CD C E W D R 0 L O G COMPANY NAME: COMPANY PROJECT NUMBER: HYDROLOGIC PROJECT NUMBER: HYDROLOGIC SAMPLE NUNBER: HYDROLOGIC LAB I.D.#: SAMPLE IDENTIFICATION: DATE SAMPLED: DATE EXTRACTED: DATE/TIME ANALYZED: Hydrologic -Asheville, Inc KE''NLU URE MWS FL9433991 33992 399 Q85V8 11/15/94 N/A 11/18/94 NETHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT ( u9/1) ( u9/1) Benzene 71-43-2 1.0 BDL Branobenzene 108-86-1 1.0 BDL Bromochloranethane 74-97-5 1.0 BDL Bromodichloramethane 75-27-4 1.0 BDL Bramoform 75-25-2 1.0 BDL Bramanethane 74-83-9 1.0 BDL n-Butylbenzene 104-51-8 1.0 BDL sec-Butylbenzene 135-98-8 1.0 BDL tert-Butylbenzene 98-06-6 1.0 BDL Carbon tetrachloride 56-23-5 1.0 BDL Chlorobenzene 108-90-7 1.0 BDL Chloroethane 75-00-3 1.0 BDL Chloroform 67-66-3 1.0 BDL Chloromethane 74-87-3 1.0 BDL 2-Chlorotoluene 95-45-8 1.0 BDL 4-Chlorotoluene 106-43-4 1.0 BDL Dibromochloranethane 124-48-1 1.0 BDL 1,2-Dibrano-3-chloropropane 96-12-8 1.0 BDL 1,2-Dibrothane (EDB) 106-93-4 1.0 BDL Dibrancmethane 74-95-3 1.0 BDL 1,2 -Dichlorobenzene 95-50-1 1.0 BDL 1,3 -Dichlorobenzene 541-73-1 1.0 BDL 1,4 -Dichlorobenzene 106-46-7 1.0 BDL Dichlorodifluoromthane 75-71-8 1.0 BDL 1,1-Dichloroethane 75-34-3 1.0 BDL 1491 Twilight Tra '❑ Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 5 1491 Twilight Tra '❑ Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 D R 0`y L 0 G I C I N Page 2 continued COMPANY NAME: Hydrologic -Asheville, Inc COMPANY PROJECT NUMBER: KENMURE MWS HYDROLOGIC PROJECT NUMBER: EL9433991 HYDROLOGIC SAMPLE NUMBER: 33992 SAMPLE IDENTIFICATION: Q85V8 DATE SAMPLED: 11/15/94 METHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT ( ug/1) ( u9/1) 1,2-Dichloroethane 107-06-2 1.0 BDL 1,1-Dichloroethene 75-35-4 1.0 BDL cis-1,2-Dichloroethene 156-59-4 1.0 BDL trans-1,2-Dichloroethene 156-60-5 1.0 BDL 1,2-Dichloropropane 78-87-5 1.0 BDL 1,3-Dichloropropane 142-28-9 1.0 BDL 2,2-Dichloropropane 590-20-7 1.0 BDL 1,1-Dichloropropene 563-58-6 1.0 BDL cis-1,3-Dichloropropene 10061-01-5 1.0 BDL trans-1,3-Dichloropropene 10061-02-6 1.0 BDL Ethylbenzene 100-41-4 1.0 BDL Hexachlorobutadiene 87-68-3 1.0 BDL Isopropylbenzene 98-82-8 1.0 BDL p-Isopropyltoluene 99-87-6 1.0 BDL Methylene Chloride 75-09-2 1.0 BDL Naphthalene 91-20-3 1.0 BDL n-Propylbenzene 103-65-1 1.0 BDL Styrene 100-42-5 1.0 BDL 1,1,1,2 -Tetrachloroethane 630-20-6 1.0 BDL 1,1,2,2 -Tetrachloroethane 79-34-5 1.0 BDL Tetrachloroethene 127-18-4 1.0 BDL Toluene 108-88-3 1.0 BDL 1,2,3-Trichlorobenzene 87-61-6 1.0 BDL 1,2,4-Trichlorobenzene 120-82-1 1.0 BDL 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 R 0 L 0 G Page 3 continued COMPANY NAME: Hydrologic -Asheville, Inc COMPANY PROJECT NUMBER: KENM1W MWS HYDROLOGIC PROJECT NUMBER: FL9433991 HYDROLOGIC SAMPLE NUMBER: 33992 SAMPLE IDENTIFICATION: Q85V8 DATE SAMPLED: 11/15/94 F=0D EPA 502.2 ANALYSIS CAS NO. SDL RESULT ug/1) ug/1) 1,1,1 -Trichloroethane 71-55-6 1.0 BDL 1,1,2 -Trichloroethane 79-00-5 1.0 BDL Trichloroethene 79-01-6 1.0 BDL Trichlorofluoromethane 75-69-4 1.0 BDL 1,2,3-Trichloropropane 96-18-4 1.0 BDL 1,2,4-1Trimethylbenzene 95-63-6 1.0 BDL 1,3,5-Trimethylbenzene 108-67-8 1.0 BDL Vinyl Chloride 75-01-4 1.0 BDL Xylenes (total) 1330-20-7 1.0 BDL Dichloromethane 75-09-2 1.0 BDL Ell 9 W, R Ar BDL = Below Sample Detection Limit SDL = Sample Detection Limit COMMENTS: 1491 Twilight Traill,0 Frankfort, KY 40601 ❑ 502/223-0251 ❑ FAX 502/875-8016 ❑ Toll Free 1-800/728-2251 3 0 11 r-nD-�� vv o O cn m o m - CD ch 0 CD g Oa r p Q O o z -c S S m a 10 ZOO 3 0 a 0 o. co LIN t < -O Z z � z o • 70 Cl) Cn Cl) -0 S= CD T g o r- 3 o s s ' co C) D D-0 � rn W --1-i w+ n n C) n W �' o m :3 CD m o. m m w_ m A a w w Z O Ono v, Z 0 00 O cfl 3 w o 0 0 6 (D (O o T G) > O o ? cn cn 0 7 CL _ 3 a 0 o U) °' O a s o 2) (cDi W O O O (D O C O 7 N .0 .� O m 7 `G O 3 O O (p w o V7 V N C (D N cQ a o c0 A d O a CD O O CD O - (n v CF) U) a S O m o` a O W o S o X O A-0-0 3 3 g �m C T T W v' p R, �z�N `° X 0m m a S S � 0 N T o CD A O OD (D U v O (D o co„ is cn a m T N (D ` 1 CJ cn o w A N 0 3 3 3 O 3 W o 3 3 3 -r CD fi N Cn Z z T. 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O O O (D O. 7 CD Df -0 O �. 3 (D 8- M a) = m m m m (D m m m ° a m m CD m 3 5 =- � m y m m mCD m m m m m m > > > CD m m 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 O O U Cn (Nn (Nn CCn of Cn (Nn (Nn CNn r C." CNn (Nn. (Nn CJn Ln Ln 0 (Nn m (NJi C" CVn O U cccccccccccCccccccccccccccc CO O CO W O (O O O to 00 0 O O J W O O N m (O O A O CO 00 A (O Cn (n07 W W W9 TO O W— A J J O W Ln W— W (n W W N j m O m m m A A W A m A O 66 & L Cn A V A A m L O V W W W J Ut N N V Oo W W A T OD N N O 07 W W (O W O z 7 a (n — m— 7 N w 3 m --I 07 = O W Vi C1 N W '� C .m-.. N k N N N A W Ci Ci O N '00 W A W Cn O (D `C X ry N ,L co v A o o o 3 W N O" 4 `a0 (D m 0 CD m CD(D m m O O S S S O O IOD' n CD CD 'v O m 0 0 0 0 0= 3 Ort 7 S C 7' N= N 7 iT 0 6' 0 0 5- (T O' m m (D O 7 N K N `G m N CD C O C O W m. m m 7 3= 0 CD CD m (D 7 (D `G 6 N ZT 7 0 7 m m (D -O O m m m m m m m 7 CD �' 7 CD 3 CD m m. O mN Er N N N O m m m CD CD (D m -O m 0 a m CD 0 0 0 0 0 0 0 0 0 cn N N N N N N N _. -� s � � � � � — — N— -•— Cn Cn Cn C -+ m n .07 Cn Cn MCn " Cn C C C C C C C C C C C C C C C C C C C C C C C C C C C < 0 r- > m -r m D F z zD m r D C7 < r r D O c r D N O X 0 m cn =z c D m m 0 0 D Fn o� m —1 0 <-<mx A to z 0 a O V ao (n \Y A to z 0 a O V ao (n OF NATtXiA i. ,'..*8 AND COMMUNITY DEVELOPMENT .41RONMENTAL MANA(i GROUNDWATER SECTION SOX 27687 - RALEIGKN.C. 27611, PHONE (919) 733-5088 WELL CONSTRUCTION RECORD I FOR OFFICL. Quad. No. Se Lat.Long. � . Minor Basin Basin Code Header Ent. GW -1 Ent._ DRILLING CONTRACTOR: F r o e ii l i n s' and Roo e r t s on, I n c STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER 4 2 1 PERMIT NUMBER: 4 4- J 210 - .J ri- J J 3 2 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: Flat Rock County: ti e n d e r s o n Depth DRILLING LOG (Road, Community, or Subdivision and Lot No.) 2. OWNER Kenmure Properties, Inc. ADDRESS Post Office Box 537 (Street or Route NoJ Flat Rock 'QC 28731 City or Town State Zip Code 3. DATE DRILLED 3-23-87 USE OF WELL. 10n1 for 4. TOTAL DEPTH 55' CUTTINGS COLLECTED ❑ Yes Q No 5. DOES WELL REPLACE EXISTING WELL? Q Yes ❑ No 6. STATIC WATER LEVEL: 41 FT. 0 above TOP OF CASING, abelow Ground Level TOP OF CASING IS 2 FT. ABOVE LAND SURFACE. 7. YIELD (gpm): T A A METHOD OF TEST ii 1A 8. WATER ZONES (depth): 41 ' t o J51 9. CHLORINATION: Type .d A Amount i4 /A 1o. CASING: Wall Thickness Depth Diameter or Weight/Ft. Material 40 � From +2 To �_' Ft. ' SCa ( ' VC From To Ft. From To Ft. 11. GROUT: Depth Material Method From J To -33' Ft. Cemeat From To Ft. 12. SCREEN: I DO HEREBY CERTIFY THAT THIS WELL STANDARDS, AND THAT A COPY OF THIS From To Formation Description of fine mica if 5' Cregisa tan SILT, some fine mica, trace of fine sand 5' S5' Greyish -brown SILT, a. little fine sand, trace of fine mica If additional space is needed; use' -back of farm. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) TED IN-ACQOF)0A NCAC 2C, WELL CONSTRUCTION SIGNATURE OF CON FRACTOORA E , DATE GW -1 Revised 11/84 Submit original to Division of n on ntal Management and copy to well owner. Depth Diameter Slot Size Material e From - 3 5 To - � � 11 Ft. 2 in. . J 1 J in. ;' VC From To _ Ft. in. in. From To Ft. in. in. 13. GRAVEL PACK: Depth Size Material From -34 To -5�' Ft. 2S Sand From To Ft., bentonite seal above grav 0pa( 14. REMARKS:12" I DO HEREBY CERTIFY THAT THIS WELL STANDARDS, AND THAT A COPY OF THIS From To Formation Description of fine mica if 5' Cregisa tan SILT, some fine mica, trace of fine sand 5' S5' Greyish -brown SILT, a. little fine sand, trace of fine mica If additional space is needed; use' -back of farm. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) TED IN-ACQOF)0A NCAC 2C, WELL CONSTRUCTION SIGNATURE OF CON FRACTOORA E , DATE GW -1 Revised 11/84 Submit original to Division of n on ntal Management and copy to well owner. ~' \ 11(ENMURE1 nL�� 'SEm^"=°^- mmn*^�~- ' August� 3, l?U��� \ [MD Groundwater Section P.O. Box 27687 Raleigh, N.C. 27611 DEM ND Department of NR0D P.O. Box 27687 Raleigh, N'C' 27611 Subjects Authorized Age|'t Wastewater Disposal Monitoring Kenmure Henderson County, N.C. Dear Si/s: &� This leiter is written to identify Jon H. Laughter as Autho- rized Vent for the purpose of reviewing and signing the fol-, lowing [ormsz l' GW -59 Revised 7/85, entitled Compliance Monitoring Report Form' 2' DEM Form MR -1 (11/84), entitled Effluent If problems opour in the rePortinn procedures or the quality of our ground and surface waters, Please contact Mr' Laughter and myself' Respectfully submitted, Kenmure Properties Ltd' KENxxooErmzpsazzEs crn *POST opRcEBOX 5a7°FLAT ROCK, mozracamzUoNAzo7a1 ° 704/6930481 This leiter is written to identify Jon H. Laughter as Autho- rized Vent for the purpose of reviewing and signing the fol-, lowing [ormsz l' GW -59 Revised 7/85, entitled Compliance Monitoring Report Form' 2' DEM Form MR -1 (11/84), entitled Effluent If problems opour in the rePortinn procedures or the quality of our ground and surface waters, Please contact Mr' Laughter and myself' Respectfully submitted, Kenmure Properties Ltd' KENxxooErmzpsazzEs crn *POST opRcEBOX 5a7°FLAT ROCK, mozracamzUoNAzo7a1 ° 704/6930481 x -a "Carolina - Departrneat of Env(mnrnm wd Natural Resources - Division of Water Quality - Cmin iwater Section - 1636 Mail -Sorvia Ccnta -lta *h.NC 27699.1639 - Phone No. (919) 733-3221 WELL ABANDONMENT RECORD WELL CONTRACTOR WELL CONTRACTOR CRRTLPICATION err 1. WELL USE (Cluck Applicable $o#: Residential 13 Municipal ❑ Industrial Q Agricultural 0 Monitoring fi7' Recovery 0 Heat Pump Water Injecdon.0 Other 0 20ther, List Use: 2. WELL LOCATION. ( o a inch of the location an back of form.) f Nearest Town • t' CF, County ' Pt r &ywn (Road Name and Number, == t6 Subdivision, -Lot No.) - Quadrangle No. �(/� t 3. OWNER. Ke-r)m(47— 1 4. ADDRESS: S. TOPOGRAPHY: draw,o�;)hilltop, valley, flat / (circle one) J 6. TOTAL DEPTH: S -7 D*L MEEM a 7. CASING REMOVED: 71 S. DISINFECTION: (Amount of 70% hypochlorite used.) 9. SEALING MATERIAL: Neat CCment -Sand .etnent bags of cement bags of cement_ gallons of water gallons of water--7— Type ater Type material Amount r �. r 1 s r I 1' � M 1 a � �• . WMtRINFAR WELL DIAGRAM: Draw a detailed sketch of the weu sheaving told depdh. dtrpth wad diameter of screens musdomg.ia••thc well, gWMI ictetvai, intervals of lasing pofoations, and depths and types of frli uhatexianls used. 11. DATE WELL ABANDONED b 3 I do hereby certify that this well was abandoned in accordance with _ 15A NCAC 2C, well construction standards, and that a copy of ft record has been,to the ll owner. f Signature of person abandoning the well ba,� WELL LOCATION: Draw a location skmteh an the =iniac of this sheet, showing the direction and distance of the well to at least two (2) nearby reference points such as roads, intcrsectians and smims. Identify roads with State Highway road identification numbers. Submit original to tate Division or Water Quality. Groundwater Section, one copy to the owner within 30 days from completion of z6andonment. GW -30 Revised 12/99 I KENMURE PROPERTIES, INC. COUNTY: HENDERSOI\ DATE SAMPLED 11-13-01 it -i3 "0d ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE 1z�o S' CHROMIUM,TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL j. I COPPER CYANIDE DISSOLVED SOLIDS �� 0 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA p• 01 L•( NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN ORTHOPHOSPHATE pH (�. i .7 • !� PHENOLS PHOSPHORUS, TOTAL o- 3,� POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE j SULFATE TOC (UNFILTERED) '7— TOX TSS VOC �, 3 ZINC y STATIC WATER LEVEL Red Ink=Sample taken by facility WELL NO./ COUNTY: /V'o t = 12 S U r1 DATE SAMPLED ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE I a CHROMIUM, TOTAL COBALT -CJD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS 7 36 �tS� 33 6 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM Red Ink = Sample taken by facility COUNTY: / L /az)t-- DATE SAMPLED /1-3--`I� f�"�'`�� '999 f1 � l-�df jj_,g;Nao MBAS MAGNESIUM MANGANESE MERCURY' NICKEL NITROGEN, AMMONIA d o / 0, d < p. o/ ® 1 > O f U, d NITROGEN, KJELDAHL NITRATE &' NITRITE o- ORGANIC SCAN pH Via. .� 5 , ® S� S,7 7 PHENOLS PHOSPHORUS, TOTAL p . /5 O, /� 0.01 POTASSIUM SELENIUM SILVER SODIUM SPECIE CONDUCTANCE („ SULFATE TOC (UNFILTERED) ,L S r 0 TOX TSS ZINC STATIC WATER LEVEL 1 41 , j o, Ked Ink = Sample taken by facility DATE SAMPLED /— 9G %—s,22 9(1 %/-gyp %% ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE • , °G 0,/ CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL J r/ COPPER CYANIDE DISSOLVED SOLIDS / 76 / .3 o FLUORIDE HARDNESS CaCo,, HARDNESS, NON-CARBONATE IRON LEAD LITHIUM Red Ink = Sample taken by facility f COUNTY�lJL DATE SAMPLED MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN. AMMONIA 010 3 1 0,03 NITROGEN, KJELDAHL NITRATE & NITRITE • / 0./(, 0 • ORGANIC SCAN pH_ �•� �• ,.� ��.0 PHENOLS PHOSPHORUS, TOTAL 0. 03 0, O �L POTASSIUM SELENIUM SILVER SODIUM SPECIFIC CONDUCTANCE SULFATE TOC ( UNFILTERED) 4�� ,� , a S _5 3.o T'0 TSS VOC ' �+ a 051L % 4 / . 0 V jL G lla J� UJA ZINC STATIC MATER LEVEL , I • �� ` 7 ' i, 3g, D , P'ER /q7)A,`,"r �vze�ll in/�li' i'� _Eta �iMPC DATE SAMPLED 6 ' 1 i/-,? 7- 7,;- ,2ALKALINITY, ALKALINITY,TO pH 4.5 ALKALINITY. TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE ° 3, 30 CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL-'� / ° 4 - COLIFORM, TOTAL COLIFORM, '7 X31 3 y 6 / • f- �° j COPPER CYANIDE DISSOLVED SOLIDS FLUORIDE HARDNESS CaCo. HARDNESS, NON -CARBONATE IRON LEAD LITHIUM i COUNTY JqEA1.06k 5 e) .. DATE SA14PLED/—.2 i- ri �...: . MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA d � , �V.-, .4 0.03 0.1 NITROGEN, KJELDAHL �, � C). NITRATE & NITRITE 01/0 0.0-6 C) • � `% ORGANIC SCAN pH C, 39 s 3,5r 6. PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIFIC CONDUCTANCE SULFATE TOC ( UNFILTERED) z -3,2 ZINC .vOae oC 74CC `rE SeE ATTAc'+�� KE��eT ` /may V V G 4pM,' O_ -Tee rE c-EA?rgcHEd .PFPae-r /� tri p iJ /.�' L. t ice- A/0 v STATIC WATER LEVEL `� Al V -G . 7 + 7 c:),j I r ss�J DATE SAIPLEn % -f ALKALINITY TO PH 4.5 I ALKALINITY, TO PH 8.3 r ALUMINUM - _ ARSENIC BARIUM I BICARBONATE CADMIUM CALCIUM MRBONATE �HLORIDE :HROMIUM, TOTAL :OD 'OLIFORM, FECAL i a_ D L �D s�� To � G l of ;OLIFORM, TOTAL TOPPER I ;YANIDE lISSOLVED SOLIDS iI. 6 � 2,0 95.G �is ` '�7• G� %r � $. LUORI DE ARDNESS, CaCO ARDNESS NON -CARBON A RON q EAD BAS AGNESI M .WGANESE 3RCURY EGKLE r (Continued) 'AfE SA"1PLEn _ NITRO X17. � � � G � .�- C3 . f d ©•' > . NITROGEN KJELDAH NITRATE & NITRITE- 1,77- r r ti 0 IIZ I 0.97 ORGANIC SCAN H G , o .S / �� 6, D S. c� ' 6,-0 S , -2- .PHENOLS PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM - SPECIFIC CONDUCTANCE SULFATE t - 'TOC (UNFILTERED) � O. SD # �i• Z � � • // �. �l 5 ZINC .� 11 I, I I e ALKALINITY CaCO3) To PH- 8.3 To PH 4.5 77— 51.7-91ff 64*6 7-11-ff A - Al umi n um Arsenic Bicarbonate Cadmium Calcium 0. Carbonate 4 TZ Chl ori de 174. Chlorinated Hydrocarbon Chromium, Hexavalent Chromium, Total COD Coliform, Fecal Coliform, Total Cyanide Dissolved Solids 93 1�4zo Vj- 36' Fl uori de } �` Hardness as CaCO 3 Hardness, Non -carbonate <1 LJ I ron Lead Lithium WAS Magnes i um Manganese Mercury rkp I R -34' �9z e, 2_//� // 7Ammnia y.^ I Ni trogen, Kjeldahl'"` 65.0 Z, Ni trate & Ni tri te_ Organic Scan Phenols'�t Phosphorus, Total Potassi um Selenium Silicm Siiver� Sodium. `' •s. Specifi c Conductance SulfUte Sulfite Ii nc j Barium j I- --j --- i Cf) (n -0 G) > 0 --1-0 0 -2 Q () Q -0 A 0 -0 a :T --% "I ::r 0 2� a 0 > 0 Z — CD CD ID CD0 In — =4 W W D— 0 CL zr Z z30 CD CD m 3 m 0 w (nz 0 :3 CL m :3 0 F1 C/) CL 0 c 2L = a ---i -n 0 cn '< 0- = 0 CD ch N U) 0 o w 0 Q.-10 " � E W 3 :3 13 0 0 - CD 2: 0 CCD CL CD O C� 0 m ,35,33,33S:3 c) a 3 co (0 0 (a (c (a co co� (a = (!Z W CL r_ KK;r,,:z-nooOC)oj>o-uzz m Co (o CD c: ZY 0- W CD ZY 0 0 c(D n 0 E:Ko-3Z:703 0003> =r — SD CD -a =. 3. :37 0 Al C 0 z (:n (0 (,ncc,)) 2: oz 0 W CD r- :3 (n 3 cD E 0 cin z(n c(DD 3 0) 0 cn z 0) w Ci) (D Z 0 w CL CL 3333333333333332• co (o (o n (a (o (o (o to co n (o (a (o ca CL 0'0 (D(D 3 EJ'—' I o o CD 3 z :z 0 (D 5' M > cf) (D CD 0 U) Z (D 0CD . . U) =r :3 CLCD CLO 0 ,33 C) 3 CD O 0 z =r 0 a 0 3 3 3 CL CD CD CD I�D :*L 2)0 0 0CL CL 0- CL z 6 0 CD C) 90 cn c co 71 0 0 z m 0 m x 0 z ww3epacelabs.Com Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Attn: Ms. Beverly Grinstead Phone: (828)254-7176 --------------------------- Lab Sample No: 931042949 Client Sample ID: W2 Pace Ana., J 9800 Kincr,, Hunter.. Phone: Ia Fax: 704.61. Lab Project Number: 9227835 Client Project ID: James&James 9324890 Project Sample Number: 9227835-001 Date Collected: 11/13/01 10:40 Matrix: Water Date Received: 11/13/01 14:03 Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Lim GC Volatiles GC VOCs in Water Prep/Method: SM 6230D / SM 6230D Benzene ND ug/l 0.50 1.0 11/27/01 19:02 KST 71-43-2 Bromobenzene ND ug/l 0.50 1.0 11/27/01 19:02 KST 108-86-1 Bromochloromethane ND ug/l 0.50 1.0 11/27/01 19:02 KST 74-97-5 Bromodichloromethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 75-27-4 Bromoform ND ug/l 0.50 1.0 11/27/01 19:02 KST 75-25-2 Bromomethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 74-83-9 n-Butylbenzene ND ug/l 1.0 1.0 11/27/01 19:02 RST 104-51-8 sac-Butylbenzene ND ug/l 0.50 1.0 11/27/01 19:02 KST 135-98-8 tert-Butylbenzene ND ug/l 0.50 1.0 11/27/01 19:02 KST 98-06-6 Carbon tetrachloride ND ug/l 0.50 1.0 11/27/01 19:02 RST 56-23-5 Chlorobenzene ND ug/l 0.50 1.0 11/27/01 19:02 KST 108-90-7 Chloroethane ND ug/l 0.50 1.0 11/27/01 19:02 KST 75-00-3 Chloroform ND ug/l 0.50 1.0 11/27/01 19:02 KST 67-66-3 Chloromethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 74-87-3 2-Chlorotoluene ND ug/l 0.50 1.0 11/27/01 19:02 KST 95-49-8 4-Chlorotoluene ND ug/l 0.50 1.0 11/27/01 19:02 RST 106-43-4 1,2-Dibromo-3-chloropropane ND ug/l 2.0 1.0 11/27/01 19:02 KST 96-12-8 Dibromochloromethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 124-48-1 1,2-Dibromoethane (EDB) ND ug/l 0.50 1.0 11/27/01 19:02 KST 106-93-4 Dibromomethane ND ug/l 0.50 1.0 11/27/01 19:02 KST 74-95-3 1,2 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 19:02 KST 95-50-1 1,3 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 19:02 KST 541.73-1 1,4 -Dichlorobenzene ND ug/l 1.0 1.0 11/27/01 19:02 RST 106-46-7 Dichlorodifluoromethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 75-71-8 1,1-Dichloroethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 75-34-3 1,2-Dichloroethane ND ug/1 0.50 1.0 11/27/01 19:02 KST 107-06-2 1,1-Dichloroethene ND ug/l 0.50 1.0 11/27/01 19:02 KST 75-35-4 cis-1,2-Dichloroethene ND ug/l 0.50 1.0 11/27/01 19:02 RST 156-59-2 trans-1,2-Dichloroethene ND ug/l 0.50 1.0 11/27/01 19:02 KST 156-60-5 Date: 11/28/01 Page: 1 C Waste atCertification IDS REPORT OF LABORATORY ANALYSIS Laboratory Drinking Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627 Pace Ana,, ,._ 9800 Kinn.; V ea, CNNPhone: Itr. wwpacefabCom Fax 704.b w. s�, Lab Project Number: 9227835 Client Project ID: James&James 9324890 --------------- --------------------- Lab Sample No: 931042949 Project Sample Number: 9227835-001 Date Collected: 11/13/01 10:40 Client Sample ID: W2 Matrix: Water Date Received: 11/13/01 14:03 Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Lim 1,2-Dichloropropane ND ug/l 0.50 1.0 11/27/01 19:02 SST 78-87-5 1,3-Dichloropropane ND ug/l 0.50 1.0 11/27/01 19:02 RST 142-28-9 2,2-Dichloropropane ND ug/l 0.50 1.0 11/27/01 19:02 RST 594-20-7 1,1-Dichloropropene ND ug/l 0.50 1.0 11/27/01 19:02 RST 563-58-6 cis-1,3-Dichloropropene ND ug/l 0.50 1.0 11/27/01 19:02 RST 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.50 1.0 11/27/01 19:02 RST 10061-02-6 Diisopropyl ether ND ug/l 0.50 1.0 11/27/01 19:02 SST 108-20-3 Ethylbenzene ND ug/l 0.50 1.0 11/27/01 19:02 SST 100-41-4 Rexachloro-1,3-butadiene ND ug/l 2.0 1.0 11/27/01 19:02 RST 87-68-3 Isopropylbenzene (Cumene) ND ug/l 0.50 1.0 11/27/01 19:02 SST 98-82-8 p-Isopropyltoluene ND ug/l 1.0 1.0 11/27/01 19:02 SST 99-87-6 Methylene chloride ND ug/l 2.0 1.0 11/27/01 19:02 SST 75-09-2 Methyl-tert-butyl ether ND ug/l 0.50 1.0 11/27/01 19:02 RST 1634-04-4 Naphthalene ND ug/l 2.0 1.0 11/27/01 19:02 SST 91-20-3 a-Propylbenzene ND ug/l 0.5D 1.0 11/27/01 19:02 SST 103-65-1 Styrene ND ug/l 0.50 1.0 11/27/01 19:02 RST 100-42-5 1,1,1,2 -Tetrachloroethane ND ug/l 0.50 1.0 11/27/01 19:02 SST 630-20-6 1,1,2,2 -Tetrachloroethane ND ug/l 0.50 1.0 11/27/01 19:02 AST 79-34-5 Tetrachloroethene ND ug/l 0.50 1.0 11/27/01 19:02 SST 127-18-4 Toluene ND ug/l 0.50 1.0 11/27/01 19:02 SST 108-88-3 1,2,3-Trichlorobenzene ND ug/l 2.0 1.0 11/27/01 19:02 SST 87-61-6 1,2,4-Trichlorobenzene ND ug/l 2.0 1.0 11/27/01 19:02 RST 120-82-1 1,1,1 -Trichloroethane ND ug/l 0.50 1.0 11/27/01 19:02 RST 71-55-6 1,1,2 -Trichloroethane ND ug/l 0.50 1.0 11/27/01 19:02 SST 79-00-5 Trichloroethene ND ug/l 0.50 1.0 11/27/01 19:02 SST 79-01-6 Trichlorofluoromethane ND ug/l 0.50 1.0 11/27/01 19:02 SST 75-69-4 1,2,3-Trichloropropane ND ug/l 0.50 1.0 11/27/01 19:02 RST 96-18-4 1,2,4-Trimethylbenzene ND ug/l 0.50 1.0 11/27/01 19:02 RST 95-63-6 1,3,5-Trimethylbenzene ND ug/l 0.50 1.0 11/27/01 19:02 RST 108-67-8 Vinyl chloride ND ug/l 0.50 1.0 11/27/01 19:02 SST 75-01-4 m&p-Xylene ND ug/l 0.50 1.0 11/27/01 19:02 SST o -Xylene ND ug/l 0.50 1.0 11/27/01 19:02 RST 95-47-6 1-Chloro-3-fluorobenzene (S) 95 % 1.0 11/27/01 19:02 RST 625-98-9 Date: 11/28/01 Page: 2 NG Wast certification IN REPORT OF LABORATORY ANALYSIS Laboratory Drinking ertification 90 NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627 z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El b 77, Xi, x 1 z z x x x- o n n n eo x D a D z x o d ir- b w z o' oL/� O 3 c c m ux C m i > a co z z3 O o 0 0 0 0 C OQ O O H m O io v d O r'Te 0 c o N p z z n cn to A D` n N ti U On to N V ^ O O N a O a � � y r 5 r r= x n x oa x A na o o u o w < N w N co 6 w O N W N �a W Q N O N 8 3 3 6' 3 3 3 3 3 c W 3 3 B 3 ° w w w w w ow \ w w� w 9 w w w x H z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El b y pn x x z z x x x- o n n n eo c H cn D a D z x p d p b 0- z o' oL/� O 3 c c m ux C m i > a co z z3 O tv a o o C OQ O O H m O io v d O r'Te � c o N p z z n cn to A D` n N ti U On to N V ^ O O N a O a � � y r 5 r r= 0 N w < N w co N O 3 8 3 3 6' 3 3 3 3 3 c W 3 3 B 3 ° w w w w w ow \ w w� w 9 w w w x H III z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El b y pn .on ? z z no x x x- o n n n eo c H cn D a D z p p d O y n e m i > a co z z3 O tv a o o C OQ O O H m O io v d O r'Te � c o � n 3 H A to to cn to A D` � o � On to N V ^ O O N a O a � � y r 5 r r= z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El b y pn .on � w��. D no x �. n c H o b c H cn D z p p O -C O n e m i > a co z z3 O tv a o o C OQ O O H m O io v d O r'Te � c o o � � o � M N m z a � � y r 5 w < w w ° a z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El b y pn .on � w��. D no x �. n c oz c H cn z to HO O -C O n m i > a co z z3 O tv a o o C � z z a d O a z d d o p A m3 � 4 n :� ❑ � ° o N T - o v .. 3 n ac v El r � w��. D no x �. n c D c H cn z z D n m i O O o D b z a a � � � o � M N m z a � � y r 5 r � w��. `A '•v z C w �. n c f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 3( X X Z X ° � 3 0 A c cii n c c w O X N CL � - Z -i X , O m D N v S 0 n m O n Z t M. N _ O "h o 3 3.. O C n o ul 8 m C N n ao ° a 5F: a x s O c v 3 o 3m c w 4 Z O Z D o 0- �n OH wc7 pZOaa o o to n p H w mtA N 00 - C, rn O. < p wLyl �cr T` Ln = V 0 -� a w rn N cn -s -] 0 t71 L71 m 0 N u - O 3 .. V O < ° n w LM LT, A p to w cr c w N c to o aO wn`N 3 m 2 X 3 m- A o o c tO Cm 3 0 c tc 04' c to o T T Lt'4 O p- -- , , w ° 00 'a CL p O 41-0 n O a LM r t0 w O- N z to OD A fl. n O n I{ F O O 0 N n N I m 3 3 to 3 -33 3 c c 3 3 3LM 3 to f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 3( X X Z X ° � 3 0 A c cii n c c w O X N CL N :? Z -i Z , O m cn C ul c Cn -a S 0 to n m O n Z t M. N _ O "h o 3 3.. O C n C O ul m C N H w a ° _ m c O 3 O c '�` ° n 3 NLa 3m c w 4 Z O Z Z cwo 3 P v V to n w w H w mtA N 00 - C, rn O. p wLyl (0 71 Ln = V = -� a w rn N cn O O` LM -Al � t71 L71 m 0 N u - O 3 o V O o ° n w LM LT, A to m to w c w c to c to w to 3 m c to 3 3 c W c to c tO c tO Cm 3 0 c tc 10 c to o O O p- -- , , w p O n O a t0 w O- to cr O n I{ m O N n m 3 3 3 3 -33 3 c c 3 3 3 3 to to tO to to w to Ic f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 3( p v Z o ° � 3 0 A c cii n c c w O la N CL N oma m Z (n3 , 3i m o so0 W 0 to n m a� O o M. N O v o 3 �' c' two -3 m m e 3 o, w C ° _ m c N O 3 NLa to c S 4 X o a cwo 3 P v a T . P 3 l0 wLyl c°il a' ca n to U1 t71 O` y p tP ol O` LM -Al � t71 L71 c 0 N u u to N00 CL m w �_ V m o ° n w LM LT, A to m to w c c to c to cc to to 3 m c to 3 3 c W c to c tO c tO c to 3 0 c tc c tO c to o c to p- -- , , w o- n f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 0 p v v o ° � 0 N c U3 s w 1p n Z O O N CL oma 2 2 a ty SB m W _'moo o W{ O O w O m w m N O NLa to O S X o O N T s O 3 l0 l0 n m w � y p c 0 CL m w �_ o m o ° n w to m to w c m m � 3 co O w n O a w O- to cr n ti m O m w f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 0 p t0 ° � 0 N c U3 s w 1p A n < N CL oma f> c =j p ON o y V o 3 c p w a o to rn !" O w Oo to o C% ao m A j- w v N mi O O � ... o_ o C7 m o o O tNit � 3- ri � 0 v s �c �p m N m U1 O N o m 0 O m A 0 3 3 ° � n � 3 3 i o' cn s °, 0- X X ' o w O- O T v CL f - m m' I m - < A 3 m = H 3 t0 - :+ = m 11 m 0 T Q 1 o M m W A s � N O S 0 a a 0 S Lo m m 3 O C7 p t0 ° � m N c A w A n < oma L m -n H m r v r a W -n M 9-: I M J December 11,2001 MEMORANDUM TO: Data Users From: Cindy Green, DWQ Che istry LabG�' Through: Larry Ausley Subject: TOC Samples with data qualifier code The TOC analysis requested on this sample set was not performed due to an administrative decision to discard a set of TOC samples received during this period due to an unforeseen problem with the analytical instrument. Samples appropriately preserved with sulfuric acid have been causing cumulative degradation of the analyzer. This effect was previously unknown. The Laboratory Section has issued guidance to preserve subsequent TOC samples with concentrated phosphoric acid in an attempt to resolve this issue. We apologize for any inconvenience caused by this necessary action. If you have any questions please contact Cindy Green or Larry Ausley at 733-3908. =-i -i fA vi '0 O D . 1 -Iv p �a C� n C� Tov c �-+ @ 2-02F; x 0 00 E; Z co = CD CID m o (fir. cn ®=» =« p w 0 0 Z300o0 0 CDam 30 .a O cu o M -4- iv N Q a O Cl) 0 � CIDQ 22 c 3 a A) m A 33�333333�3 003 .°• con o cn to cfl tQ cn to =0 3 3 a3 c r. KKAMMOOC Ow>O-ZZ * =30 to EDC ? t2 >y >v �. C' r: m -p o ' ' ' D o N a. wMW K0 0 3.w w w ca �gCD� Mca�W„ �vCa=.3oozZ (a =3 �33.�3cwa00-� �v 3a X033 3�••w---N �� Zz C I m 3n33 3333330 tQ n tC (a (a cC a a <M0 -Fn- O ODN-OZ -=T3 :3 cr nD m Z30NrZ .e D = ch 3. n v iDi 0 M CD ? - Z %<;= 0m N � 0 c a3 n 0. 3D CD a� ......-tc�-� 3 3 3 cn a a c� co m 0 0 0 `D = n. an.OL, o It n n ? LA. /2 Zm 0 `D 30 NI C c3333 0 v �-- a 0 ace Analytical "' www. pacelabs. coni i James & James Environmental Mgmt. 814 B. Kanuga Street Hendersonville, NC 28739 / 1 � Pace Anar,, 9800 Kince). Phone_ 7N,_ rax 704.x;. DATE: 11/30/00 PAGE: 1 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Attn: Mr. Harry James Solid results are reported on a dry weight basis Pace Sample No: 93718765 Date Collected: 11/15/00 Matrix: Water Client Sample ID: W2 Date Received: 11/15/00 Parameters --------------------------------- Results ---------- Units --------- PRL ---------- App. OF -------- Analyzed -------- Analyst CAS# Footnotes ----- GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane ND ug/L 0.5 1.00 11/29/00 MAG 75-71-8 Chloromethane NO ug/l 0.5 1.00 11/29/00 MAG 74-87-3 Vinyl Chloride NO ug/L 0.5 1.00 11/29/00 MAG 75-01-4 Bromomethane NO ug/l 0.5 1.00 11/29/00 MAG 74-83-9 Chloroethane NO ug/L 0.5 1.00 11/29/00 MAG 75-00-3 Trichlorofluoromethane NO ug/1 0.5 1.00 11/29/00 MAG 75-69-4 1,1-Dichloroethene ND ug/L 0.5 1.00 11/29/00 MAG 75-35-4 Methylene Chloride ND ug/l 0.5 1.00 11/29/00 MAG 75-09-2 trans-1,2-Dichloroethene ND ug/L 0.5 1.00 11/29/00 MAG 156-60-5 1,1-Dichloroethane NO ug/l 0.5 1.00 11/29/00 MAG 75-34-3 cis-1,2-Dichloroethene ND ug/L 0.5 1.00 11/29/00 MAG 156-59-2 Bromochloromethane ND ug/1 0.5 1.00 11/29/00 MAG 74-97-5 Chloroform NO ug/L 0.5 1.00 11/29/00 MAG 67-66-3 2,2-Dichloropropane ND ug/L 0.5 1.00 11/29/00 MAG 594-20-7 1,2-Dichloroethane ND ug/1 0.5 1.00 11/29/00 MAG 107-06-2 1,1,1 -Trichloroethane ND ug/L 0.5 1.00 11/29/00 MAG 71-55-6 1,1-Dichloropropene ND ug/t 0.5 1.00 11/29/00 MAG 563-58-6 Carbon Tetrachloride ND ug/L 0.5 1.00 11/29/00 MAG 56-23-5 Dibromomethane ND ug/1 0.5 1.00 11/29/00 MAG 74-95-3 1,2-Dichloropropane ND ug/L 0.5 1.00 11/29/00 MAG 78-87-5 Trichloroethene No ug/l 0.5 1.00 11/29/00 MAG 79-01-6 BromodichLoromethane ND ug/L 0.5 1.00 11/29/00 MAG 75-27-4 cis-1,3-Dichloropropene ND ug/l 0.5 1.00 11/29/00 MAG 10061-01-5 trans-1,3-Dichloropropene NO ug/L 0.5 1.00 11/29/00 MAG 10061-02-6 1,1,2 -Trichloroethane NO ug/1 0.5 1.00 11/29/00 MAG 79-00-5 1,3-DichLoropropane NO ug/L 0.5 1.00 11/29/00 MAG 142-28-9 Laboratory Certification IDsREPORT OF LABORATORY ANALYSIS I aboratory Certification ID' NC Wastewater 12 KY Drinking Water 9009' NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 r- --'-1--..)aceAnalyticaF' www. pacelabs. coni i -' Pace Ana., .9800 Kincey. H;nt&s, Phone- 704 Fax. 704.8 DATE: 11/30/00 PAGE: 2 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718765 Date Collected: 11/15/00 Matrix: Water Client Sample ID: W2 Date Received: 11/15/00 Parameters Results Units PRL App. DF -------- Analyzed -------- Analyst ----- CAS# Footnotes ---------- ---------- --------------------------------- Dibromochloromethane ---------- ND --------- ug/l ---------- 0.5 1.00 11/29/00 MAG 124-48-1 1,2-Dibromoethane ND ug/1 0.5 1.00 11/29/00 MAG 106-93-4 Tetrachloroethene ND ug/l 0.5 1.00 11/29/00 MAG 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/l 0.5 1.00 11/29/00 MAG 630-20-6 Chlor6benzene ND ug/l 0.5 1.00 11/29/00 MAG 108-90-7 Bromoform ND ug/l 0.5 1.00 11/29/00 MAG 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/t 0.5 1.00 11/29/00 MAG 79-34-5 1,2,3-Trichloropropane ND ug/t 0.5 1.00 11/29/00 MAG 96-18-4 Bromobenzene ND ug/l 0.5 1.00 11/29/00 MAG 108-86-1 2-Chlorotoluene ND ug/l 0.5 1.00 11/29/00 MAG 95-49-8 4-Chlorotoluene ND ug/t 0.5 1.00 11/29/00 MAG 106-43-4 1,3 -Dichlorobenzene ND ug/t 1 1.00 11/29/00 MAG 541-73-1 1,4 -Dichlorobenzene ND ug/l 1 1.00 11/29/00 MAG 106-46-7 1,2 -Dichlorobenzene ND ug/t 1 1.00 11/29/00 MAG 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/1 2 1.00 11/29/00 MAG 96-12-8 1,2,4-Trichlorobenzene ND ug/t 2 1.00 11/29/00 MAG 120-82-1 Hexachloro-1,3-butadiene ND ug/l 2 1.00 11/29/00 MAG 87-68-3 1,2,3-Trichlorobenzene ND ug/1 2 1.00 11/29/00 MAG 87-61-6 Methyl-tert-butyl Ether ND ug/l 0.5 1.00 11/29/00 MAG 1634-04-4 Isopropyl Ether ND ug/l 0.5 1.00 11/29/00 MAG 108-20-3 Benzene ND ug/l 0.5 1.00 11/29/00 MAG 71-43-2 Toluene ND ug/l 0.5 1.00 11/29/00 MAG 108-88-3 Ethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 100-41-4 m&p-Xylene ND ug/1 0.5 1.00 11/29/00 MAG 7816-60-0 Styrene ND ug/l 0.5 1.00 11/29/00 MAG 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/t 0.5 1.00 11/29/00 MAG 95-47-6 Isopropytbenzene (Cumene) ND ug/l 0.5 1.00 11/29/00 MAG 98-82-8 n-Propylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 103-65-1 1,3,5-Trimethylbenzene ND ug/t 0.5 1.00 11/29/00 MAG 108-67-8 tert-Butylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 98-06-6 1,2,4-Trimethylbenzene ND ug/1 0.5 1.00 11/29/00 MAG 95-63-6 sec-Butylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 135-98-8 p-Isopropyltoluene ND ug/l 1 1.00 11/29/00 MAG 99-87-6 n-Butylbenzene ND ug/1 1 1.00 11/29/00 MAG 104-51-8 Naphthalene ND ug/l 2 1.00 11/29/00 MAG 91-20-3 1-Chloro-2-fluorobenzene (S) 93 % 1.00 11/29/00 MAG 348-51-6 NC Wastewater IDS REPORT OF LABORATORY ANALYSIS Laboratory v Ceratei cati�� NC Wastewater 12 KY Drinking Water 9009 NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List SC 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 e Analytical " www. pacelabs. com ��✓ PaceAna.. 9800 Kincc,, Hunler�, Phone: 70* Fax. 704.1x, DATE: 11/30/00 PAGE: 11 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718856 Date Collected: 11/14/00 Matrix: Water Client Sample ID: TRAVEL BLANK Date Received: 11/15/00 Parameters --------------------------------- Results ---------- Units --------- PRL ---------- App. DF -------- Analyzed -------- Analyst CAS# Footnotes ---- GC Volatiles GC VOCs in Water Method: ND SM 6230D ug/l 0.5 1.00 Prep Method: SM 11/29/00 MAG 6230D 75-71-8 Dichlorodifluoromethane Chloromethane ND ug/l 0.5 1.00 11/29/00 MAG 74-87-3 Vinyl Chloride ND ug/l 0.5 1.00 11/29/00 MAG 75-01-4 Bromomethane ND ug/l 0.5 1.00 11/29/00 MAG 74-83-9 Chloroethane ND ug/l 0.5 1.00 11/29/00 MAG 75-00-3 Trichlorofluoromethane ND ug/t 0.5 1.00 11/29/00 MAG 75-69-4 1,1-Dichloroethene ND ug/l 0.5 1.00 11/29/00 MAG 75-35-4 Methylene Chloride ND ug/l 0.5 1.00 11/29/00 MAG 75-09-2 156-60-5 trans-1,2-Dichloroethene ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 75-34-3 1,1-Dichloroethane cis-1,2-Dichloroethene ND ND ug/l ug/l 0.5 1.00 11/29/00 MAG 156-59-2 Bromochloromethane ND ug/l 0.5 1.00 11/29/00 MAG 74-97-5 Chloroform ND ug/l 0.5 1.00 11/29/00 MAG 67-66-3 2,2-Dichloropropane ND ug/l 0.5 1.00 11/29/00 MAG 594-20-7 1,2-Dichloroethane ND ug/t 0.5 1.00 11/29/00 MAG 107-06-2 1,1,1 -Trichloroethane ND ug/l 0.5 1.00 11/29/00 MAG 71-55-6 1,1-Dichloropropene ND ug/l 0.5 1.00 11/29/00 MAG 563-58-6 56-23-5 Carbon Tetrachloride ND ug/t ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 74-95-3 Dibromomethane 1,2-Dichloropropane ND ND ug/l 0.5 1.00 11/29/00 MAG 78-87-5 Trichloroethene ND ug/t 0.5 1.00 11/29/00 MAG 79-01-6 Bromodichloromethane ND ug/t 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 75-27-4 10061-01-5 cis-1,3-Dichloropropene ND ND ug/l ug/l 0.5 1.00 11/29/00 MAG 10061-02-6 trans-1,3-Dichloropropene 1,1,2 -Trichloroethane ND ug/l 0.5 1.00 11/29/00 MAG 79-00-5 1,3-Dichloropropane ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 142-28-9 124-48-1 Dibromochloromethane ND ND ug/l ug/t 0.5 1.00 11/29/00 MAG 106-93-4 1,2-Dibromoethane Tetrachloroethene ND ug/l 0.5 1.00 11/29/00 MAG 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/l 0.5 1.00 11/29/00 MAG 630-20-6 108-90-7 Chlorobenzene ND ug/t 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 75-25-2 Bromoform 1,1,2,2 -Tetrachloroethane ND ND ug/l ug/l 0.5 1.00 11/29/00 MAG 79-34-5 1,2,3-Trichloropropane ND ug/l 0.5 0.5 1.00 1.00 11/29/00 11/29/00 MAG MAG 96-18-4 108-86-1 Bromobenzene 2-Chlorotoluene ND ND ug/l ug/l 0.5 1.00 11/29/00 MAG 95-49-8 Laboratory iKY ertificaton IDs REPORT OF LABORATORY ANALYSIS Laboratory Drinking Water ertificati�_n l[?_ NC Wastewater X009 TN UST List NC Drinking Water 37706 This report shall not be reproduced, except in full, 'Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 21 Inalytical rM www.pacelabs.com Pace Aria.. 9800 Kinct, Hunter,.. Phone: 70ti. Fax: 704.b,. DATE: 11/30/00 PAGE: 12 Pace Project Number: 9218626 Client Project ID: James&James-9316553 Pace Sample No: 93718856 Date Collected: 11/14/00 Matrix: Water Client Sample ID: TRAVEL BLANK Date Received: 11/15/00 Parameters Results Units PRL ---------- App. DF -------- Analyzed -------- Analyst ----- CAS# Footnotes ---------- ---------- --------------------------------- 4-Chlorotoluene ---------- ND --------- ug/l 0.5 1.00 11/29/00 MAG 106-43-4 1,3 -Dichlorobenzene ND ug/l 1 1.00 11/29/00 MAG 541-73-1 1,4 -Dichlorobenzene ND ug/l 1 1.00 11/29/00 MAG 106-46-7 1,2 -Dichlorobenzene ND ug/l 1 1.00 11/29/00 MAG 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 2 1.00 11/29/00 MAG 96-12-8 1,2,4-Trichlorobenzene ND ug/l 2 1.00 11/29/00 MAG 120-82-1 Nexachloro-1,3-butadiene ND ug/L 2 1.00 11/29/00 MAG 87-68-3 1,2,3-Trichlorobenzene ND ug/L 2 1.00 11/29/00 MAG 87-61-6 Methyl-tert-butyl Ether ND ug/l 0.5 1.00 11/29/00 MAG 1634-04-4 Isopropyl Ether ND ug/L 0.5 1.00 11/29/00 MAG 108-20-3 Benzene ND ug/L 0.5 1.00 11/29/00 MAG 71-43-2 Toluene ND ug/l 0.5 1.00 11/29/00 MAG 108-88-3 Ethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 100-41-4 m&p-Xylene ND ug/l 0.5 1.00 11/29/00 MAG 7816-60-0 Styrene ND ug/t 0.5 1.00 11/29/00 MAG 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/l 0.5 1.00 11729/00 MAG 95-47-6 Isopropylbenzene (Cumene) ND ug/l 0.5 1.00 11/29/00 MAG 98-82-8 n-Propylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 103-65-1 1,3,5-Trimethylbenzene ND ug/t 0.5 1.00 11/29/00 MAG 108-67-8 tert-ButyLbenzene ND ug/l 0.5 1.00 11/29/00 MAG 98-06-6 1,2,4-Trimethylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 95-63-6 sec-Butylbenzene ND ug/l 0.5 1.00 11/29/00 MAG 135-98-8 p-Isopropyttoluene ND ug/L 1 1.00 11/29/00 MAG 99-87-6 n-Butylbenzene ND ug/l 1 1.00 11/29/00 MAG 104-51-8 Naphthalene ND ug/t 2 1.00 11/29/00 MAG 91-20-3 1-Chloro-2-fLuorobenzene (S) 71 % 1.00 11/29/00 MAG 348-51-6 Laboratory Certification IDsREPORT OF LABORATORY ANALYSIS L aboratory Certification IQ NC Wastewater 12 KY Drinking Water X9090 NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List y Sc 99006 without the written consent of Pace Analytical Services, Inca VA Drinking Water 21 x x x an. 2 Z3 � 2 �w N a n n n r r• t n Y Y "'� m H C ''3 p ccpp ° s y . = o o O d O 0 O d m H �• � a� y� 7 0 a"� O 3 °r x o X �• 7 0 o ^yn-' T; N• n a n p ,��, .,y o O x G. ° Y L. c "l1 Tl N iP 7 7 V1 O 0. 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L r (n s 0 m �o X= x O O n m- n o: 3 v S o S z to co m fn O N p 3 O O O -f O N m n m mm= yin y O rn o 3 D rn { o to m O r. rn m y_ Z Q00 N O O n N o Q $uoi p O p m o n m ^ � O W z O O y N � -i• O o 3 0 P -C o O (71 s n n 0 n Q (n �.(n �' 3 s -r• o 0 o I P 3 O � m N C C + (n C m G m r O y f17 O O 0 w f { c o v °r N IZ 3 y �• 3 ' N No. l0 { n V 371{� O m (A(cn S -11,O-+ O 0 { + m V { 1p p m — uf0i F m y � 11 N to p O o O { n O 0 M 00 +0 Gtm y s coco (7 v o A(7 r 3 Cul- to- O S n. N A m v A c ° '< m m mm a ' w (JI CT I � 3 W H r .1 n v o9 o, CL 0 0 " w Z 0 U1 v °I r LM S D w Q S O A W n D N m � L O � 3 � 4 a. L r (n s 0 m �o Z Q00 N O O n N o Q $uoi p O p m o n m ^ � O W z O O y N � -i• O o 3 0 P -C o O (71 s n n 0 n Q (n �.(n �' 3 s -r• o 0 o I P 3 O � m N C C + (n C m G m r O y f17 O O 0 w f { c o v °r N IZ 3 y �• 3 ' N No. l0 { n V 371{� O m (A(cn S -11,O-+ O 0 { + m V { 1p p m — uf0i F m y � 11 N to p O o O { n O 0 M 00 +0 Gtm y s coco (7 v o A(7 r 3 Cul- to- O S n. N A m v A c ° '< m m mm a ' w (JI CT I � 3 W H r .1 I—ICn(A�1 �''DC�—I� Oz ��C� f7 ` 0c:w@(i; 02: 0 m =::9 C�-mo o 0 0 0 �_ ND�CD���Dc�-R ���j1 CD c3� o 00 �0- cnZ -n -n DSO 0-i -n -� `� CDC = s cno m o N C CD m 3353333'333S3 oo3 to (a o cc cc ca cc cc cc cc ,..F cc cc _ _ � z n z'KK;r,m moo o -70zz Ci o r� m 3 D CDS o , �zz u `21 NG Itlolld?��Z+ f , c c' To cn c� cQ Q We CD .w ,-cT C N N w mao�r.— C:Cn y cn M. Q r ID " o co A z�6 w Y 0 n N CD o -® r I .w =Q �' m Cf)g---V -V "c i m 0 3 3 v a CD_ m a o; C a c3 c3 c3 ca c3 cQ cQ c3 cQ cQ cQ C) -0 N T Z o 'K'cD cn CD D C- ch o go3 � Mo co D C Z9.NrZ o ��w _ o� om0Q0 3 E 3 r _M m c m m 2 O (D w m C f oO c. o 0.. M: z Q n � in 21 z c (D Z --I CL 'O 0 m `21 NG Itlolld?��Z+ f , c c' To cn c� cQ Q We CD .w ,-cT C N N w mao�r.— C:Cn y cn M. Q r ID " o co A z�6 w Y 0 n N CD o -® r I .w =Q �' m 0 u 0 0 z 0 D CD w w A D CL CB Cf)g---V -V "c i m 0 3 3 v a CD_ m a o; C cn C m ooC cn v go3 � Mo co D C o ��w m' 3 E r _M m 0 u 0 0 z 0 D CD w w A D CL CB m i m m m m' m ooC v go3 � Mo co ��w m' DAsi r _M m m m cn w m C Imm o 0.. M: z � in 21 z Z --I Q 'O 0 m (A F 0 0 (� c a m j Pace Analy,, 9800 Kincey Ave, ,nalvti�a� Huntersville; , Tel: 704-875. DATE: 12/q -9104-875-9ft PAGE: 1 James & James Environmental Mgmt. Pace Project Number: 9210415 814 B. Kenuga Street Client Project ID: James&James-939533 Hendersonville, NC 28739 Attn: Mr. Harry James Solid results are reported on a dry weight basis Pace Sample No: 93419448 Date Collected: 11/29/99 Matrix: Water Client Sample ID: w2 Date Received: 11/30/99 Parameters Results Units PRI, App. OF Analyzed Analyst CAS# Footnotes GC Volatiles GC VOCs in Nater Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane NO ug/1 0.5 1.00 12/07/99 KST 75-71-8 Chloromethane NO ug/l 0.5 1.00 12/07/99 KST 74-87-3 Vinyl Chloride ND ug/l 0.5 1.00 12/07/99 F KST 75-01-4 Bromomethane ND ug/l 0.5 1.00 12/07/99 KST 74-83-9 Chloroethane NO ug/l 0.5 1.00 12/07/99 KST 75-00-3 Trichlorofluoromethane NO ug/t 0.5 1.00 12/07/99 KST 75-69-4 1,1-Dichloroethene NO ug/l 0.5 1.00 12/07/99 KST 75-35-4 Methylene Chloride ND ug/l 0.5 1.00 12/07/99 KST 75-09-2 trans-1,2-Dichloroethene NO ug/1 0.5 1.00 12/07/99 KST 156-60-5 1,1-Dichloroethane NO ug/l 0.5 1.00 12/07/99 KST 75-34-3 cis-1,2-Dichloroethene NO ug/l 0.5 1.00 12/07/99 KST 156-59-2 Bromochloromethane ND ug/l 0.5 1.00 12/07/99 KST 74-97-5 Chloroform NO ug/L 0.5 1.00 12/07/99 KST 67-66-3 2,2-Dichloropropane NO ug/l 0.5 1.00 12/07/99 KST 594-20-7 1,2-Dichloroethane NO ug/l 0.5 1.00 12/07/99 KST 107-06-2 1,1,1 -Trichloroethane ND ug/1 0.5 1.00 12/07/99 KST 71-55-6 1,1-Dichloropropene ND ug/L 0.5 1.00 12/07/99 KST 563-58-6 Carbon Tetrachloride NO ug/t 0.5 1.00 12/07/99 KST 56-23-5 Dibromomethane NO ug/l 0.5 1.00 12/07/99 KST 74-95-3 1,2-Dichloropropane ND ug/l 0.5 1.00 12/07/99 KST 78-87-5 Trichloroethene NO ug/l 0.5 1.00 12/07/99 KST 79-01-6 Bromodichloromethane NO ug/l. 0.5 1.00 12/07/99 KST 75-27-4 cis-1,3-Dichloropropene NO ug/l 0.5 1.00 12/07/99 KST 10061-01-5 trans-1,3-Dichloropropene NO ug/l 0.5 1.00 12/07/99 KST 10061-02-6 1,1,2 -Trichloroethane ND ug/l 0.5 1.00 12/07/99 KST 79-00-5 1,3-Dichloropropane ND ug/t 0.5 1.00 12/07/99 KST 142-28-9 LaboratoryCertification 1Da NC Wastewater 12 NC Drinking REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs N Drinking Water 90090 Water 37706 T TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analy,, 9800 Kincey Ave,., e Analytocal Huntersville,, Tel: 704-875=:., Fax: 704-875-90k, DATE: 12/09/99 PAGE: 2 Pace Project Number: 9210415 Client Project ID: James&James-939533 Pace Sample No: 93419448 Date Collected: 11/29/99 Matrix: Water Client Sample ID: W2 Date Received: 11/30/99 Parameters Results Units PRL App. OF Analyzed Analyst CAS# Footnotes Dibromochloromethane NO ug/l 0.5 1.00 12/07/99 KST 124-48-1 1,2-Dibromoethane NO ug/l 0.5 1.00 12/07/99 KST 106-93-4 Tetrachloroethene NO ug/t 0.5 1.00 12/07/99 KST 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/t 0.5 1.00 12/07/99 KST 630-20-6 Chlorobenzene ND ug/l 0.5 1.00 12/07/99 KST 108-90-7 Bromoform ND ug/l. 0.5 1.00 12/07/99 KST 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/1 0.5 1.00 12/07/99 KST 79-34-5 1,2,3-Trichloropropane NO ug/L, 0.5 1.00 12/07/99 KST 96-18-4 Bromobenzene ND ug/1. 0.5 1.00 12/07/99 KST 108-86.1 2-Chlorotoluene ND ug/1 0.5 1.00 12/07/99 KST 95-49-8 4-Chlorotoluene NO ug/l 0.5 1.00 12/07/99 KST 106-43-4 1,3 -Dichlorobenzene ND ug/l 1 1.00 12/07/99 KST 541-73-1 1,4 -Dichlorobenzene NO ug/l 1 1.00 12/07/99 KST 106-46-7 1,2 -Dichlorobenzene NO ug/t 1 1.00 12/07/99 KST 95-50-1 1,2-Dibromo-3-Chloropropane NO ug/l 2 1.00 12/07/99 KST 96-12-8 1,2,4-Trichtorobenzene NO ug/l 2 1.00 12/07/99 KST 120-82-1 Hexachlorobutadiene NO ug/t 2 1.00 12/07/99 KST 87-68-3 1,2,3-Trichlorobenzene ND ug/l 2 1.00 12/07/99 KST 87-61-6 Methyl-tert-butyl Ether NO ug/l. 0.5 1.00 12/07/99 KST 1634-04-4 Isopropyl Ether ND ug/L 0.5 1.00 12/07/99 KST 108-20-3 Benzene ND ug/l. 0.5 1.00 12/07/99 KST 71-43-2 Toluene NO ug/1 0.5 1.00 12/07/99 KST 108-88-3 Ethylbenzene NO ug/l 0.5 1.00 12/07/99 KST 100-41-4 m&p-Xytene NO ug/l 0.5 1.00 12/07/99 KST 7816-60-0 Styrene NO ug/t 0.5 1.00 12/07/99 KST 100-42-5 o -Xylene (1,2 -Dimethylbenzene) NO ug/l 0.5 1.00 12/07/99 KST 95-47-6 isopropylbenzene (Cunene) NO ug/l 0.5 1.00 12/07/99 KST 98-82-8 n-Propylbenzene NO ug/l 0.5 1.00 12/07/99 KST 103-65-1 1,3,5-Trimethylbenzene ND ug/l 0.5 1.00 12/07/99 KST 108-67-8 tert-Butylbenzene NO ug/l 0.5 1.00 12/07/99 KST 98-06-6 1,2,4-Trimethylbenzene NO ug/l 0.5 1.00 12/07/99 KST 95-63-6 sec-Butylbenzene NO ug/1 0.5 1.00 12/07/99 KST 135.98-8 p-Isopropyttoluene NO ug/l. 1 1.00 12/07/99 KST 99-87-6 n-Butylbenzene ND ug/1 1 1.00 12/07/99 KST 104-51-8 Naphthalene ND ug/t 2 1.00 12/07/99 KST 91-20-3 1-Chloro-3-fluorobenzene (S) 103 % 1.00 12/07/99 KST 625-98-9 Laboratory Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS aboratory Qertification IDs N Drinking 90090 NC Drinking Water 37706 Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. 6 acndr O w i NLn y— p -�t a N 0 z o o 08 v x v T x , C - � O N O o � M.0 x o m 7 O O ,P .w.. + v C Z m p 6• or G ry n � w � m ^ �, r ° N x •°. n 0 y O O _ a o N V W O r O 0 w V C C C C py C- 3 C C C G C C C o H W w O w O ry o C. 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G ry n � w � m ^ �, r ° N x •°. n 0 y O _ a o N V W O O 0 V C C C C py C- 3 C C C G C C C C H w O ry n A Iq 6 acndr O w i y— p -�t a N 0 z o o 08 v x v T x , C - � H y O o � M.0 x m 7 m v C Z ,fir O w � w � m ^ �, r ° N x •°. n 0 y O _ a o y 0 'n. 7 H w O ry n A 6 acndr O w i m N 0 H � � o o 08 v v C - � z o � n m v C Z ,fir O � n 0 y O 6 acndr O w i N 0 H � � o o v v ?t D -n o cn 37 (D 'D (D 0 T cD iU. p 3 ., m(q Deo po CL O Z� 0 D y Q ° �0 CA (D D ca C13 I— 3WOO� U��n cn 12°c m m 3 °' =. (D CD ° ° r a c7 �R= M 0 m a Z a 77 O j' aT. 7 Q O 1 CD Z aC o m n� Er o �' n o� vW o Lm 0 wNCn Q Or ° fD 0 N 3 B L w= , n Sa.m r CO cn n ° d m (n �, a 4 O y 0 S CL ❑� A S m c m n cp w 0 m= r i g a �n 3 ' SD o m�' ZAP - A r 3 W 41. '1 y W 0 cn 0 i 0 0 0:0 (D <D 0) cDC Z ss M m :17] c CD J \ CL CD 0 m CA m cn m CD CD 1 <D fh -{ -n cD Nn c Ra CD 1 I CD L` 0 W C, CD C� v_v cm � c 03 z 03 n O Dm m4z X00 D :r -mac 0 CD 0�03 om— a 0 C.= OzCl) Dc 1 m m 1) n 0 i 1 50 Z W m Q w n >>> ° -• w o cp ccDD c a 0 m co D =i c (D a°i a ° a w w w y w o ° 0 V ° w a 0 w N (D c C. C� A 3 A. C C m. fD C"C. 3 N (D C ID A 0 C A V pW.. A Im cn N C A W G7 N 3 A 3 A A W 01 N A CT CDcn os m U1 cn W G CO cn V ?t D -n o cn 37 (D 'D (D 0 T cD iU. p 3 ., m(q Deo po CL O Z� 0 D y Q ° �0 CA (D D ca C13 I— 3WOO� U��n cn 12°c m m 3 °' =. (D CD ° ° r a c7 �R= M 0 m a Z a 77 O j' aT. 7 Q O 1 CD Z aC o m n� Er o �' n o� vW o Lm 0 wNCn Q Or ° fD 0 N 3 B L w= , n Sa.m r CO cn n ° d m (n �, a 4 O y 0 S CL ❑� A S m c m n cp w 0 m= r i g a �n 3 ' SD o m�' ZAP - A r 3 W 41. '1 y W 0 cn 0 i 0 0 0:0 (D <D 0) cDC Z ss M m :17] c CD J \ CL CD 0 m CA m cn m CD CD 1 <D fh -{ -n cD Nn c Ra CD 1 I CD L` 0 W C, CD C� v_v cm � c 03 z 03 n O Dm m4z X00 D :r -mac 0 CD 0�03 om— a 0 C.= OzCl) Dc 1 m m 1) n 0 i 1 50 Z W CD -n O 0 N CA O CD CL D w Cl) y G Q 3 CD CD C1 w 3 a (D Al �i Q i cu 0 Cr 0 0 0 > Dcni— 7o s 5 M 07 a i` :; FT1 = o O m � r w Di nD O n cr w CD o C b1° IA -.�w (D v, 0 z.. ° -°• D .G 3 CD o l< CD o- c�D 0C) CD a 0 0 0 CD a D D o CD 7] -I -i n n n C1 m w o== 0 m 0 w O 2 m D 0 00 CD 0 0 O! O CL O . O O 3 p O N Q Q 0== N N A 0 W y a Q n 0 0 c 0 =. O 0 v v 2) o CD O CD R! R O 5D `c o 3 (c ro OC co 2 0 x CD o o C w a (n G 14 w W w J o c X CD a a �+ t3 O 2 2 Cl) --f -n- �' A o a O �A "o CD Cl) 0 CD W CA) cn N d Q W w or /r�_ V' m w 0 ° O CD CT O cn CA �3 3 8 0) 72. - 2 .CD O A 13cD coo m T .3 d w Cc O = c 0 O ° CA O d m m o N 1� o � 1 3 3 co n� c 3 3 3 3 3 3 G 3 z3 N o 0 3 3 3 RI co -= \ - ca co = cQ ^ cQ =c -1 3 CD = \ - C7 �C0 yrnrh r A z Z 0 O 07 C a C w n Q C N + Z w CA d CD V N Cp ^' A O N N Cn C=D m = CD CD O N O z L) CD 0 wwp m O In a1 Of CD a w 0 0 V 0)Z Cil O co C W o w o 0 CD w o o m N 41,C 3 3 3 3 3 3 G S 3 3 _ 2S m y T ncwami DD - cD (a CD o w y cn ami = m w 0 O ami w C C _• < QAi _ c A __ GCD ? O N La. c C ", 0, c B 3 C. 3 3 R. CD 3� CD y C d w am 3 3 a rn 3 conn m 3 rn m CD c" m rn CD T� CA O N (r cn N cn V V7 O CO L a C C Cc 3 G 33 C C C G C 3 C G C C — _ a' _ f9 a -a m cn C) O O M S S o w CD 2 Z 3 mn a o a m v CD v 2 CO CD CD C o 7 0 mN 0 Com ��_ k L7 C > > A CD O C1 m O ^ •0 . O c O 0 Cn. n O m d 0 cD c w < O an Cn CA CD -0 2 m Q Cj w a o y ca mCD (D co > Dcni— 7o s 5 M 07 a i` :; FT1 = o O m � r w Di nD O n cr w CD o C b1° -.�w (D v, 0 z.. ° -°• D .G 3 CD o l< CD o- c�D CD a CD a CL CD 2n0 -n z 9-� 0 Ix . � -n m O D O CD onm a K1r ` fA \j O � a cn CCD 7 _• f° v � m CI) a a A 2) o m 0M CD �Q O O dJ m O C w a O ° �w p� +V O "o Cl) �O W or /r�_ V' m w 0 ° O CD cn �3 3 8 0) 72. - 2 .CD = 13cD coo m T .3 d w Cc O = 0 ° O d m m o N 1� o � 1 3 ci ® n 3y c) m-0 w e N m�-0 o r a (� �o RI _• N 0 %< ID Ca Lot t+ m CD C7 �C0 yrnrh r A r. cn w 3 (D m m Q6 Ln 3 1 me O m 0 r w CD O m CD b w CD z C CD 0 c C .G 3 CD o l< CD o- c�D CD a CD a CL -n CD 9-� ` \j O CCD � y C7 CD O G m a 0 4a ""i CA CI)Z7� ?\p"O' C S� n SQ2�j w 0 0 0 O >0 w..p N a =. (aa0cD `°�:0 C 00 mmm 33 0 CL cn zO u ��. CL. 0CD Q o m -n w N No CD CL CD CO) m aoo C '� o tN _ -4 3 Q n o w I` f • m 3 CL SNii m O 1 sAr �C a! 3335,333333 9 009 A i n cc 0 cc cc cc cc to cc N cc .00 ?. c c 3 y ��%=Tn�nnmDQ�ZZ _r +D i7 t�D an CD m ' + �+'+ + p + + SO��,a m 2)CD2) c�=r p � w caSD �. � 0 3 3 Q �. CA -1 0 33:7.. mw3 —M CO cv C Cj)CA —Z v 1 1 7 J, ` m F 1 o a 0 m a w, 33:43`3333333338 a 0` Ka ca to alca'co ca to co to ca ca co co ca Z a I I 0DN-13 �3=�� CD a Nr-Zcn -t � w�wm N Z O co O I c p Z CL .O N Q1 CL l l� 0.110 8 n CD 1S i Vi Oi� iO 01 c3333 w j y Pace Ar AL ■ .■ ■ November 17, 1998 Mr. Harry James James&James Environmental Mgmt 814 B Kanuga St. Hendersonville, NC 28739 RE: Pace Project Number: 931990 Client Project ID: Kenmure Monitoring Wells Dear Mr. James: 54 Ravena, Asheville. N Tel: 704-254-71 i, Fax: 704-252-4618 Enclosed are the results of analyses for samples) received by the laboratory on November 3, 1998. If you have any questions concerning this report, please feel free to contact me. Sincerely, Jennifer Jones Project Manager Enclosures Laboratory Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Sertices, Inc. Laboratory Certification IDs TN Drinking Water 02980 FL Environmental 96317 Pace Analyticu, 54 Raven,, knalvticat Asheville, NGS James&James Environmental Mgmt 814 8 Kanuga St. Hendersonville, NC 28739 IGI. / Ulf -";J4-1 I T Fax: 704-252-4618 DATE: 11/17/98 PAGE: 1 Pace Project Number: 931990 Client Project ID: Kenmure Monitoring Wells Attn: Mr. Harry James Phone: (704)697-0063 Solid results are reported on a wet weight basis Pace Sample No: 9392259 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE W2 Date Received: 11/03/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ------------------- ------------------ ----- ---------- ---------- Field Services Monitoring Well Data Method: Prep Method: Field pH 5.5 Std. Units 11/03/98 MPS Field Temperature 13 deg C 11/03/98 MPS Depth of Water 49.20 feet 0 11/03/98 MPS Well Volume Purged 1.00 No units 0 11/03/98 MPS Wet Chemistry Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1 Total Dissolved Solids 36 mg/L 1 11/06/98 MAA Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3 Chloride 1.5 mg/L 1 11/12/98 JGJ Ammonia Method: EPA 350.3 Prep Method: EPA 350.3 Nitrogen, Ammonia ND mg/L 0.1 11/06/98 KMH 7727-37-9 Nitrogen, Nitrate Method: EPA 352.1 Prep Method: EPA 352.1 Nitrogen, Nitrate ND mg/L 0.1 11/05/98 TRW Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060 Total Organic Carbon 2.2 mg/L 0.5 11/12/98 KEK 7440-44-0 Fecal Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Fecal Coliform <1.1 1 11/03/98 MLP Total Coliform MPN Water Method: SM 9223 Prep Method: Standard Methods Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 FL Environmental 96317 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Inc. Pace Analytif ��e� Analytical A Raven, Asheville Nu, Tel: 704-254-71-, Fax: 704-252-4618 DATE: 11/17/98 PAGE: 2 Pace Project Number: 931990 Client Project ID: Kenmure Monitoring Wells Pace Sample No: 9392259 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE W2 Date Received: 11/03/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes ---------------------------------------------------------------------- ----- ---------- ---------- Total Coliform <1.1 1 11/03/98 MLP Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37712 SC Environmental 99030 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Laboratory Certification IDs TN Drinking Water 02980 FL Environmental 96317 Pace Analytica, 9800 Kincey Avenue;., Analytical Huntersville, Nu, James & James Environmental Mgmt. 814 B Kanuga St. Hendersonville, NC 28739 Attn: Mr. Harry James Tel: 704-875-909. Fax:704-875-9091 DATE: 11/16/98 PAGE: 1 Pace Project Number: 922633 Client Project ID: J&J - 931990 Solid results are reported on a dry weight basis Pace Sample No: 92186618 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE - W2 Date Received: 11/04/98 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ---------- ------------------- -------- --------------- ---------- GC -- Volatiles Halogen. & Aromatic Vol. Orgs. Method: SM 6230D Prep Method: EPA 8021 Dichlorodifluoromethane NO ug/L 0.5 11/13/98 CLL 75-71-8 Chloromethane ND ug/L 0.5 11/13/98 CLL 74-87-3 Vinyl Chloride ND ug/L 0.5 11/13/98 CLL 75-01-4 Bromomethane NO ug/L 0.5 11/13/98 CLL 74-83-9 Chloroethane NO ug/L 0.5 11/13/98 CLL 75-00-3 Trichlorofluoromethane NO ug/L 0.5 11/13/98 CLL 75-69-4 1,1-Dichloroethene NO ug/L 0.5 11/13/98 CLL 75-35-4 Methylene Chloride NO ug/L 0.5 11/13/98 CLL 75-09-2 trans-1,2-Dichloroethene NO ug/L 0.5 11/13/98 CLL 156-60-5 1,1-Dichloroethane NO ug/L 0.5 11/13/98 CLL 75-34-3 Bromochloromethane NO ug/L 0.5 11/13/98 CLL 74-97-5 Chloroform ND ug/L 0.5 11/13/98 CLL 67-66-3 2,2-DichLoropropane ND ug/L 0.5 11/13/98 CLL 594-20-7 1,2-Dichloroethane NO ug/L 0.5 11/13/98 CLL 107-06-2 1,1,1 -Trichloroethane NO ug/L 0.5 11/13/98 CLL 71-55-6 1,1-Dichloropropene ND ug/L 0.5 11/13/98 CLL 563-58-6 Carbon Tetrachloride ND ug/L 0.5 11/13/98 CLL 56-23-5 Dibromomethane NO ug/L 0.5 11/13/98 CLL 74-95-3 1,2-Dichloropropane NO ug/L 0.5 11/13/98 CLL 78-87-5 Trichloroethene NO ug/L 0.5 11/13/98 CLL 79-01-6 Bromodichloromethane ND ug/L 0.5 11/13/98 CLL 75-27-4 cis-1,3-Dichloropropene ND ug/L 0.5 11/13/98 CLL 10061-01-5 trans-1,3-Dichloropropene NO ug/L 0.5 11/13/98 CLL 10061-02-6 1,1,2 -Trichloroethane NO ug/L 0.5 11/13/98 CLL 79-00-5 1,3-Dichloropropane NO ug/L 0.5 11/13/98 CLL 142-28-9 Dibromochloromethane NO ug/L 0.5 11/13/98 CLL 124-48-1 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN2 KY Drinking Water 90090 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytica, 9800 Kincey Avenue, tza Analytocal Huntersville, NC Tel: 704-875-909, Fax: 704-875-9091 DATE: 11/16/98 PAGE: 2 Pace Project Number: 922633 Client Project ID: J&J - 931990 Pace Sample No: 92186618 Date Collected: 11/03/98 Matrix: Water Client Sample ID: KENMURE - W2 Date Received: 11/04/98 Parameters --------------------------------- Results ---------- Units --------- PRL Analyzed Analyst CAS# Footnotes 1,2-Dibromoethane NO ug/L ---------- 0.5 -------- 11/13/98 ----- CLL -------------------- 106-93-4 Tetrachloroethene ND ug/L 0.5 11/13/98 CLL 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/L 0.5 11/13/98 CLL 630-20-6 Chlorobenzene NO ug/L 0.5 11/13/98 CLL 108-90-7 Bromoform NO ug/L 0.5 11/13/98 CLL 75-25-2 1,1,2,2 -Tetrachloroethane NO ug/L 0.5 11/13/98 CLL 79-34-5 1,2,3-Trichtoropropane ND ug/L 0.5 11/13/98 CLL 96-18-4 Bromobenzene NO ug/L 0.5 11/13/98 CLL 108-86-1 2-Chlorotoluene NO ug/L 0.5 11/13/98 CLL 95-49-8 4-Chlorotoluene NO ug/L 0.5 11/13/98 CLL 106-43-4 1,3 -Dichlorobenzene ND ug/L 0.5 11/13/98 CLL 541-73-1 1,4 -Dichlorobenzene NO ug/L 0.5 11/13/98 CLL 106-46-7 1,2 -Dichlorobenzene NO ug/L 0.5 11/13/98 CLL 95-50-1 1,2-Dibromo-3-Chtoropropane NO ug/L 0.5 11/13/98 CLL 96-12-8 1,2,4-Trichlorobenzene NO ug/L 0.5 11/13/98 CLL 120-82-1 Hexachlorobutadiene NO ug/L 0.5 11/13/98 CLL 87-68-3 1,2,3-Trichlorobenzene NO ug/L 0.5 11/13/98 CLL 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 11/13/98 CLL 1634-04-4 Isopropyl Ether ND ug/L 0.5 11/13/98 CLL 108-20-3 Benzene NO ug/L 0.5 11/13/98 CLL 71-43-2 Toluene NO ug/L 0.5 11/13/98 CLL 108-88-3 Ethylbenzene ND ug/L 0.5 11/13/98 CLL 100-41-4 m&p-Xylene NO ug/L 0.5 11/13/98 CLL 7816-60-0 Styrene NO ug/L 0.5 11/13/98 CLL 100-42-5 o -Xylene (1,2-Dimethytbenzene) ND ug/L 0.5 11/13/98 CLL 95-47-6 Isopropylbenzene (Cumene) NO ug/L 0.5 11/13/98 CLL 98-82-8 n-Propylbenzene NO ug/L 0.5 11/13/98 CLL 103-65-1 1,3,5-Trimethylbenzene NO ug/L 0.5 11/13/98 CLL 108-67-8 tert-Butylbenzene NO ug/L 0.5 11/13/98 CLL 98-06-6 1,2,4-Trimethylbenzene ND ug/L 0.5 11/13/98 CLL 95-63-6 sec-Butylbenzene NO ug/L 0.5 11/13/98 CLL 135-98-8 p-Isopropyltoluene NO ug/L 0.5 11/13/98 CLL 99-87-6 n-Butylbenzene NO ug/L 0.5 11/13/98 CLL 104-51-8 Naphthalene NO ug/L 0.5 11/13/98 CLL 91-20-3 1-Chloro-3-fluorobenzene (S) 92 % 11/13/98 CLL 625-98-9 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. r y ro ca x x �J x r^m�0 rrj HHH yy kk� 0 O i x a N OAf �3 z r y ro ca x x d x r^m�0 b m Q00 Im 3 0 O i x a F+ 'O O ;•J z Q ,•i Z z W on 07 y0 4 n n n n m a o 3 a o c g vi O d G> D A c n o o• O O O r z z- 7 o Z to m n y y H A O o_ c o x^ T o o C n rt c OR O v U m O% ro T �i ° O S S R 8• � �• ..� .O U O O g N O Oe A �• 6 U O W W 3 0 3 0 �3a X30 c X30 �3a r�3 @3 3 W O 3 ° o L T p� 3 t�3 X30 N N n � m � r y ro ca x x d x r^m�0 b m Q00 Im 3 0 O i bi N A N W a F+ 'O O ;•J z Q ,•i Z z W on 07 y0 4 Iz O O g vi O d G> D A C a S rt r z z- 7 a o� Z m n y y H A O c o ►tea v� T •G n C n rt U OR O v U m ro T �i a\ N O A R r �• O � � � = J O g O n b N 3 0 3 0 �3a X30 c X30 �3a r�3 @3 3 3 3 ° ° t3� 3 t�3 X30 A N r y ro ca bona 3D0� '0, cL d ro r^m�0 b m Q00 Im 3 0 O i bi N A N W a F+ I_ N� Iz O g vi y n m C a S rt r ° 7 a o� Z m C7 Elm o 0 c n ►tea v� n C n � OR � y r O J g n r y ro ca bona 3D0� '0, cL d ro r^m�0 b m Q00 Im 3 0 O i bi N A N W a F+ Iz O g vi y n m C a S rt r ° 7 a o� Z m C7 Elm o 0 c n ►tea v� n C n � OR � y r g n n � m � r y ro ca bona 3D0� '0, cL d ro r^m�0 b m Q00 Im 3 0 O i bi N A N W a F+ Iz O g vi r ° 7 a o� Z m C7 Elm c n ►tea v� n C n � o' m O rn d o 0 n a fA S � O. 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CD CD (D CD M o m Q o 0 a n. �w w>mc �Q� mow��' 0wCDo ca< a� °(0 *(D az CL °' n -0 w 0w 2.6 0 0 CcD 3 (n CD -Vo 3 m `E r Q " a r CA ra � Ami f LI). -03' m 0 `-o m � C7 O ZCD O o U m m �: m �o rr, 0 m cD m 0 o 3 m , m Dlob — PD CD s v (flcn c CD z m m o m 6 - n m U) m m = C ® a o O w Z m Cr-: m -n -0 D w T1 W a --j I7I u 1 N � Q CD cQ L4, 1A 0 �3 ® 0n O Q- 0 D a 0 CD su 7 0 CD C/) nri 0 (D Q _0C/) -o �y c0 c r- w u 0 CD r- 0 r0 CD c m 0 70 < m pm c0 m o -o o C V om00o O(DU m D ,s.. O m m 0 p m c �L v 0 z� m IV z PQ 0 E O z q CD X m w SD m' CL James & James Environmental Mgt. P. 0. Box 1354 Mountain Home, NC 28758 Attn: Mr. Harry James Client Reference: J&J Kenmore PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS Q ` L� JAN11 - 8 1998 Groundwater Section Asheville Regional Oftice Units PRL / ^ 9800 Hu Tel: ib-. Fax: 704-8, December 02, 1997 PACE Project Number: A71`i 93 0487700 11/17/97 11/19/97 Kenmore MW W2 METHOD DATE ANALYZED VOLATILE ORGANICS 6230D Dichlorodifluoromethane ug/L 0.5 ND 11/25/97 Chloromethane ug/L 0.5 ND 11/25/97 Chloroethene (Vinyl chloride) ug/L 0.5 ND 11/25/97 Bromomethane ug/L 0.5 ND 11/25/97 Chloroethane ug/L 0.5 ND 11/25/97 Trichlorofluoromethane ug/L 0.5 ND 11/25/97 1,1-Dichloroethene ug/L 0.5 ND 11/25/97 Dichloromethane ug/L 0.5 ND 11/25/97 trans-1,2-Dichloroethene ug/L 0.5 ND 11./25/97 1,1-Dichloroethane ug/L 0.5 ND x'1/25/97 cis-1,2-Dichloroethene ug/L 0.5 ND 11/25/97 2,2-Dichloropropane ug/L 0.5 ND 11/25/97 Chlororm ug/L 0.5 ND 11/25/97 B,romocW, romethane ug/L 0.5 ND 11/25/97 1,1;::1-T�"ichloroethane ug/L 0.5 ND 11/25/97 1,-Dicoro-l-propene ug/L 0.5 ND 11/25/97 Carbon tetrachloride ug/L 0.5 ND 11/25/97 1x2-Dichgoroethane ug/L 0.5 ND 11/25/97 1,,;`2 Tr hloroethene ug/L 0.5 ND 11/25/97 1,2-D-chropropane ug/L 0.5 ND 11/25/97 Bromodichloromethane ug/L 0.5 ND 11/25/97 Dibromomethane ug/L 0.5 ND 11/25/97 cis-1,3-Dichloro-l-propene ug/L 0.5 ND 11/25/97 trans-1,3-Dichloro-l-propene ug/L 0.5 ND 11/25/97 1,1,2 -Trichloroethane ug/L 0.5 ND 11/25/97 1,3-Dichloropropane ug/L 0.5 ND 11/25/97 Tetrachloroethene ug/L 0.5 ND 11/25/97 Dibromochloromethane ug/L 0.5 ND 11/25/97 Laboratory Certification IDs Laboratory Qertification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water 37706 TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Mr. Harry James Page 2 Client Reference: J&J Ke PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS 00000�- 1[5 JAN - 8 1998 Pact. 9800 Kine., Hunte. Tel: Ao Fax: 704-b,. December 02, 1997 PACE Project Number: A71 93 0487700 11/17/97 11/19/97 Kenmore MW PRL W2 METHOD DATE ANALYZED VOLATILE ORGANICS 1,2-Dibromoethane ug/L 0.5 ND 6230D 11/25/97 1,1,1,2 -Tetrachloroethane ug/L 0.5 ND 11/25/97 Bromoform ug/L 0.5 ND 11/25/97 1,1,2,2 -Tetrachloroethane ug/L 0.5 ND 11/25/97 1,2,3-Trichloropropane ug/L 0.5 ND 11/25/97 Bromobenzene ug/L 0.5 ND 11/25/97 2-Chlorotoluene ug/L 0.5 ND 11/25/97 4-Chlorotoluene ug/L 0.5 ND 11/25/97 1,3 -Dichlorobenzene ug/L 0.5 ND 11/25/97 1,4 -Dichlorobenzene ug/L 0.5 ND 11/25/97 1,2 -Dichlorobenzene ug/L 0.5 ND 11/25/97 1,2-Dibromo-3-chloropropane ug/L 0.5 ND 11/25/97 1,2,4-Trichlorobenzene ug/L 0.5 ND 11/25/97 Hexachlorobutadiene ug/L 0.5 ND 11/25/97 1,2,3-Trichlorobenzene ug/L 0.5 ND 11/25/97 Ben4ene ,.n ug/L 0.5 ND 11/25/97 Toluene ug/L 0.5 ND 11/25/97 C qo ob(izene ug/L 0.5 ND 11/25/97 Ethylben ene ug/L 0.5 ND 11/25/97 Xylenes,'total) ug/L ug/L 0.5 0.5 ND ND 11/25/97 11/25/97 Styrene IsoRropylnzene ug/L 0.5 ND 11/25/97 n-Prbpylbgflzene ug/L ug/L 0.5 0.5 ND ND 11/25/97 11/25/97 1,3,5=Trimethylbenzene t-Butylbenzene ug/L ug/L 0.5 0.5 ND ND 11/25/97 11/25/97 1,2,4-Trimethylbenzene s-Butylbenzene ug/L 0.5 ND 11/25/97 4-Isopropyltoluene ug/L 0.5 ND ND 11/25/97 11/25/97 n-Butylbenzene Naphthalene ug/L ug/L 0.5 0.5 ND 11/25/97 t aboratoly Certification IDs NC Wastewater 12 REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs Drinking Water 90090 TN UST List TN NC Drinking Water 37706 Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. _ n. 77 7r— = I\ i > >s S _ I Fl. 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CD CD r =CD � ma D r v m �' 3 < m — z �� (t)m D z 0 3 U ® '�,� -n„ 0 3CD m m m� Q vO CD m� C O n Q 6 CSD - CD CD O < � � . O m n w CD CD Ca 0 o 3 U 3 m cr -� -a m Q " Q- 0 7 0i cQ � � � � -6C- C - O ® w w 0 w _ -a Z m e Cf) � a n CD CD (D o = PL) W N Fn r r w r v CD Q 3 `< (t)m z �� m U ® '�,� -n„ 0 3CD ® O 0 CD ,G -a Z m e Cf) � a m v = PL) W N Fn Z,n CO o o r v CD Q 3 `< 0 �� ® '�,� -n„ vO Am e0 �T M0—D v�o " Um O Cn 02 O o w a m m ]7 D D f� O T N o m O Q O 6 � C O 7 0 �n I 0 � S C 6 DD O co fp C 2 rw v m 0 m (A CD r w 0 0 7 z 0 O z q cf, 0 CD X w w m' CL Mr. Harry James Page 5 4L FPX NO 704 252 4618 9.2-31 Pace Ara:y,, 54 Rav, Asheo#e 'el. 704-2%,,,, Far 744-252-469h_ December 04, 1996 PACE Project Number, A611206, Client Reference: J and J Kenmcre PACE Sample Number: 93 0305920 Date Collected: Date Received: 111,20/96 Client Sample ID: 111121/96 Kenmore Parameter Units PRL W2 METHOD DATE ANALYZEO ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Dichlorodifluoromethane Ug"'I 1-0 NO 12/01/96 Chloromethane Chloroethene (Vinyl chloride) Ugr(L ug /'L 1.0 1.0 NO ND 12/01/96 Bromomethane u94 1,10 NO 12/01/96 12JUJ/96 Chloroethan2 Trichlorofluoromethane UVL Ug/L 1.0 1.0 NO NO 12/01/96 12/01/96 1,1-Dichloroethene Dichloromethaneg ug/1- "L 1,0 NO 12/01/96 trans-1,2-Dichloroethene u ug"L 1.0 1.0 NO NO 12/01/963 12/0]/96 1,1-Dichloroethane uq/L 1.0 ND 12/01/96 cis-1,2-Dichloroathene 1 Lg/L i_0 NO 12101/96 2,2-Dichloropropane ug/L 1.0 NO 12101196 Chloroform Bromochloromethane ug/L ug/L LID 1,0 NO NO 12/01/96 1,1,1 -Trichloroethane Ug/L 1.0 NO 12101/96 12j01/96 IJ-Dichloro-1-propene Uq/L 1.10 NO 12/01/96 Carbon tetrachloride 1,2-Dichloroethane ug/L ug/L 1.0 1.0 ND 12/01/96 NO 12/01 ' /96 1,1,2 -Trichloroethene ug/L 110 NO 12/01/96 1,2-Dichlcropropene ug,/L 1,0 NO 12/01/96 Bromodichloromethane ug/L 1,0 NO 12/01/96 Dibromomethane cis-1,3-Dichloro-l-propene ug/L ug/L 1.0 1.0 NO NO 12/01/96 trans-1,3-Dichloro-l-propene ug/L 1.0 NO 12/01/96 12/01/96 1,1.1 -Trichloroethane Ug/L 1.0 NO 12/01/96 1.3-Dichloropropane uq/L 1.0 ND 12/01/96 Tetrachloroethene ug/'L 1.0 NO 12/01/96 Dibromochloromethane uq/L 1-0 NO 12/01196 1,1,1,2 -Tetrachloroethane ug/L 1.0 NO 12/01'96 Bromoforin ug/L 1.0 NO 12/01/96, 1,11,2,2 -Tetrachloroethane Ug/L 1.0 NO 12/01/96 REPORT OF LABORATORY ANALYSIS TAis report SM111 riot be teproducm, except in full w#�Oul IMe Wlter conAent of Pace Anat)eiQai Serv�;eS. Ino s14i_ F A X bi 0 704 252 4618 12-31 Pace Ar4,i, 54 a,3ti, 4ST,*Ole T ,el 1".4-254-', , �ax 252 5! Mr. Harry James December 04, 1996 Page 6 PACE Project Number: A6112060L Client Reference: J and J Kenmore PACE Sample Number: 93 0305920 Date Collected: 111120/96 Date Received: 11/21/96 Client Sample ID: Kormore Parameter Units PRL W2 METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANIC:S 502.2 1,2,3-Trichloroppropane Ug/L 1.0 NO 12/01/96 Bromobenzene 2-Chlorotoluene uglL ug / L, 1.0 1.0 ND ND 22/01/96 4-Chlorotoluene ugjl 1.0 NO 12/01/96 12/01/96 1,3 -Dichlorobenzene J gj L 1.0 N0 12/01/96 1 . 4 -- D i c ti I o r o b e n z. e n e Ug/L 1.0 NO 12/01/96 1,2 -Dichlorobenzene ug/L 1.0 ND 1241/96 1,2-Dibromo-3-chloropropane U9/L 1,0 ND 12/01/96 1,2,4-Trichlorobenzene uqlL 1.0 ND 12/01/96 Hexachicrobutadiene Ug/L 1 NO 12/01/96 1,2,3-Trichlorob�enzene lig/1_ .1.0 NO 12/01/96 Benzene ug;EL 1.0 NO 12/01/96 Toluene Chlorubenzene uq/L ug/L 1.0 1,0 NO NO 12/01/96 12/01/96 Ethylbenzene uq/L I'D Na 12/01/96 Xylenes, (total) ug/L 1.0 ND IZ/01/96 Styrene Isopropylbenzene ug/L ug/L 1.0 1.0 ND ND 12/0/96 12/01/96 n-Propylbenzene ug/L 1,0 NO 12/01/96 193,5-Trimethylbentene ug/L 1.0 ND 12/01/96 t-Butylbenzene ug/L 1.0 NO 12/01/96 1,2,4-Trimethylbienzene ug/L 1.0 NO 12/01/96 s -Bu tyl benzene Ug/L 1.0 ND 12/01/96 4-1sopropyltoluene ug/L 1.0 NO 12/01/96 n-Butylbenzene ug/L 1.0 ND 12/01/96 Naphthalene ug/L 1.0 NO 12/01/96 REPORT OF LABORATORY ANALYSIS TM)s rvgor* snap rofbe leproduced. 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CD a� Z:' n m� d m?o z —_ � rL �zm m Oc cm v m � c m� m cn m 0 1 O z CD �o� c C o �� n �--�Q(WD O®n ®O sv 9O= n Z CD Q mM m m 00 —I Q" Col TT --I � o o CD c m zzz r.. m n �o VOC�m c (D �2: o � � CD L i D �o �n w c �v c 33=333D399S3 ooD w (Q CQ O(Q (Q CQ CO Cit (Q CQ =r(Q CQ C_ ZKK;r"=Moo (D =30 c C O Z 3 D --q � cs c W --CDQ3 o3 zw iD' Z z a: t i} Cu t'(c (Q (Q (Q (Q (Q (Q (Q (Q (Q (Q (Q (Q (Q Q -0 N -U Z (D n U _. c� _N.-1— Z CD o o CD n C X" (D o (D Q. n Q (D (n N 4.aFv c c c 3 33 r ®m ro N C ou' �• O ;CLo 3 w o (�D zUy�$ A' m 0 3 n o (D o -0 �. m - 2 N �Z C N cn _.o�� "m o o m cn m 0 0m a CN 5 A c q CD c Q N o cO� cn N CD C 70 O (Np Q CD '� ri t CD o sv mM m m o --I =r �. c m zzz o v®oma m VOC�m c o � � CD D �o J w c - m w ca m C_ D .0 � � � OO Z Dm CY. g = W m --I =r �. o m o � c °- m , riU 18:14 - -Pace Analytical Mr. Harry James Page 3 I D : PAGE INC. TEL NO: 252 4618 Client Reference: Janes A James PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS Dichlorodifluoromethane Chloromethane Chloroethene (Vinyl chloride) Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichioroethene Dichloromethane trans-1,2-Dichloroethene 1.1-Dichloroethane cis-1,2-Dichloroethene 2,2-Dichloropropane Chloroform Bromochloromethane 144 -Trichloroethane 14-Dichloro-1-propene Carbon tetrachloride 1,2-Dichloroethane 1,1,2 -Trichloroethene 1,2-Dichloropropane Bromodichloromethane Dibromomethane cis-1,3-Dichloro-1-propene trans-1,3-Dichloro-l-propene 1,1,2 -Trichloroethane 1,3-Dichloropropane Tetrachloroethene Dibromochloromethane 1,1,1,2 -Tetrachloroethane Bromoform woa Annywai Mw9vev; 13 Ren nsoroh OAy. Asheville WC 2ml Tel: "4.2"1178 Fax: 704.212-w o February 07, 1995 PACE Project. Number: A6012260 93 0171626 01/22/96 01/23/96 Q85 W2 Units MDL #4% DATE ANALYZED u9/L 1.0 NO 01/24/96 ug/L 1.0 ND 01/24/96 u9/L 1.0 NO 01/24/96 ug/L 1.0 NO 01/24/96 u9/L 1.0 ND 01/24/96 ug/L 1.0 ND 01/24/96 ug/L u91L 1.0 1.0 NO ND 01/24/96 01/24/96 ug1L 1.0 NO 01/24/96 u9/L 1.0 NO 01/24/96 u9/L 1.0 NO 01/24/96 u9/L 1.0 ND 01/24/96 u9/L 1.0 ND 01/24/96 u9/L u9/L 1.0 1.0 NO ND 01/24/96 01/24/96 01/24/96 ug1L 1.0 NO 96 u9/L 1.0 NO 01%24/96 ug/L 1.0 ND 01/24/96 u9/L 1.0 NO 01/24/96 u9/L 1.0 NO 01/24/96 ug/L ug/L 1.0 1.0 NO NO 01/24/96 ug/L 1.0 NO 01/24/96 01/24/96 u9/L 1.0 NO 01/24/96 ug/L 1.0 NO 01/24/96 Ug/L 1.0 NO 01/24/96 ug/L 1.0 NO 01/24/96 u9/L 1,0 NO 01/24/96 u9/L 1.0 NO 01/24/96 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND 01/24/96 306 R Groundwater Section Asheville Re ionel Office -D � o Cl) rD o cu z -- v v v D .� Dcr o:rt l^ w co =r M o In M 3Zo o M w Z Z 0 tDm ,`� r r� t11 O n CL 4. z c( CD O ao Z 1 _ 0 _-nv Fla, CL Q C N CNJ1 - N ( O N N N _i g to C) ��CO (D n m O D El �. 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CD �3 U, W � o -_� r CDA o _TI = c S 3 co < CD NZ = -1 "S O�Q � 0- CD r N 01CD Cl)N C -_n � p C m v � '4 1) 3 ~ m (M N CD I C7 "OOD CD N M 0 CD - Cn N M ro 0 kob 4 ---CD o S @ O O CD _ =;; CD 0 CD CD =r m C, CD n Wro o 0 a v ncQ (n c CD �y C . z Sv (0 TI CD N A ro -0 (O mn m C/ m CD �o v 3 o o D (n CD C 3 y v D S. TI (n 01 0 m O Ln N f U, _TI a 3 0 v -_n � m v � P o I C7 N CS -< 0 10-O M ro -PC2 U)a o sv 0 z 0 V CD sv w CD 0 � a o fN � a o Lnc OL co CD O m Q- Z m 3 N ro -0 ao m z z z -uo c '0M0uj �-)' m w O `°M m > m �_ m O v z m_ z O z O U Cn -p (n C 3 y m m 0 y ID f :v _TI N C y D R 0 COMPANY NAME : COMPANY PROJECT NUMBER: HYDROLOGIC PROJECT NUMBER: HYDROLOGIC SAMPLE NUMBER: HYDROLOGIC LAB I.D.#: SAMPLE IDENTIFICATION: DATE SAMPLED: DATE EXTRACTED: DATE/TIME ANALYZED: ANALYSIS Benzene Bronxbenzene Bramochlorcanethane Bromodichloromethane Bromoform L 0 G I C I N Hydrologic -Asheville, Inc IMMURE FL9434447 34449 399 #54451/Q85W2 11/29/94 N/A 12/5/94 CAS NO. SDL 1.0 ( ug/1) 71-43-2 1.0 108-86-1 1.0 74-97-5 1.0 75-27-4 1.0 75-25-2 1.0 tj 1995 a. 6roruMcIvii,-K to N: s� RESULT Brcmamthane 74-83-9 1.0 BDL n-Butylbenzene 104-51-8 1.0 BDL sec-Butylbenzene 135-98-8 1.0 BDL tert-Butylbenzene 98-06-6 1.0 BDL Carbon tetrachloride 56-23-5 1.0 BDL Chlorobenzene 108-90-7 1.0 BDL Chloroethane 75-00-3 1.0 BDL Chloroform 67-66-3 1.0 BDL Chloromethane 74-87-3 1.0 BDL 2-Chlorotoluene 95-45-8 1.0 BDL 4-Chlorctoluene 106-43-4 1.0 BDL Dibrcanochloranethane 124-48-1 1.0 BDL 1,2-Dibrcano-3-chloropropane 96-12-8 1.0 BDL 1,2-Dibromomethane (EDB) 106-93-4 1.0 BDL Dibromomethane 74-95-3 1.0 BDL 1,2 -Dichlorobenzene 95-50-1 1.0 BDL 1,3 -Dichlorobenzene 541-73-1 1.0 BDL 1,4 -Dichlorobenzene 106-46-7 1.0 BDL Dichlorodifluoromethane 75-71-8 1.0 BDL 1,1-Dichloroethane 75-34-3 1.0 BDL 1491 Twilight Trdi1 ❑ Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 L 0 G I C I N Page 2 continued COMPANY NAME: Hydrologic -Asheville, Inc_4 COMPANY PROJECT NUMBER: KENMCIRE HYDROLOGIC PROJECT NUMBER: EL9434447 HYDROLOGIC SAMPLE NUMBER: 34449 ' i SAMPLE IDENTIFICATION: #54451/Q85W2 w DATE SAMPLED: 11/29/94 dviamr e vaus�srs��.,:«.. METHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT i ug/l) ug/l) 1,2-Dichloroethane 107-06-2 1.0 BDL 1,1-Dichloroethene 75-35-4 1.0 BDL cis-1,2-Dichloroethene 156-59-4 1.0 BDL trans-1,2-Dichloroethene 156-60-5 1.0 BDL 1,2-Dichloropropane 78-87-5 1.0 BDL 1,3-Dichloropropane 142-28-9 1.0 BDL 2,2-Dichloropropane 590-20-7 1.0 BDL 1,1-Dichloropropene 563-58-6 1.0 BDL cis-1,3-Dichloropropene 10061-01-5 1.0 BDL trans-1,3-Dichloropropene 10061-02-6 1.0 BDL Ethylbenzene 100-41-4 1.0 BDL Hexachlorobutadiene 87-68-3 1.0 BDL Isopropylbenzene 98-82-8 1.0 BDL p-Isopropyltoluene 99-87-6 1.0 BDL Methylene Chloride 75-09-2 1.0 BDL Naphthalene 91-20-3 1.0 BDL n-Propylbenzene 103-65-1 1.0 BDL Styrene 100-42-5 1.0 BDL 1,1,1,2 -Tetrachloroethane 630-20-6 1.0 BDL 1,1,2,2 -Tetrachloroethane 79-34-5 1.0 BDL Tetrachloroethene 127-18-4 1.0 BDL Toluene 108-88-3 1.0 BDL 1,2,3-Trichlorobenzene 87-61-6 1.0 BDL 1,2,4-Trichlorobenzene 120-82-1 1.0 BDL 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 L 0 G Page 3 continued COMPANY NAM: Hydrologic -Asheville, Inc COMPANY PROJECT NUMBER: KENMURE HYDROLOGIC PROJECT NUMBER: FL9434447 HYDROLOGIC SAMPLE NUMBER: 34449 SAMPLE IDENTIFICATION: #54451/Q85W2 DATE SAMPLED: 11/29/94 N=OD EPA 502.2 ANALYSIS CAS NO. SDL u9/1) 1,1,1 -Trichloroethane 71-55-6 1.0 1,1,2-yfrichloroethane 79-00-5 1.0 Trichloroethene 79-01-6 1.0 Trichlorofluoranethane 75-69-4 1.0 1,2,3--Trichloropropane 96-18-4 1.0 1,2,4-Trinethylbenzene 95-63-6 1.0 1,3,5-Trimethylbenzene 108-67-8 1.0 Vinyl Chloride 75-01-4 1.0 Xylenes (total) 1330-20-7 1.0 Dichloramethane 75-09-2 1.0 Surrogate Recovery: BFB BDL = Below Sample Detection Limit SDL = Sample Detection Limit COMMENTS: RESULT ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 96% WX 2 7 1995 croup, 1491 Twilight Trall 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 CD _rt D �TI C7 -0 Cl)D;., 0 Q- -1 N c o � m� c�3, o m m o CD o 70 o ._ r p -O m 0 O a � �3W mcn0r-0 0 m ti0 0 m w Z. C 0-0 0 0 ! r r Cn N 5.0 O M C tQ O o h tJ) cD O Q A -Ma roO Z °O o Z -1 0- (n -10- 0Pay o P I 3 m 0 M o R1 vw a � m- n O n n n M n D D 'o n cfl m -A -I n n O n W `G O_ 7' T Al O N ;K- X, m m C O O O O O O j O O O Q- N N N A N a U 0- o o a (D 3. 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Lo a j ✓T ! » O. 0 i h IAC 0 CD 0 m Z co m z G) �QvI• : KM '►4 vi • i• :, is V • f• NO ANALYSIS Branobenzene Brauochlorarethane Bra ndichloranethane BramfOEM Brcum ethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chlorarethane 2-Chlorotoluene 4-Chlorotoluene Dibranochlorarethane 1,2-Dibrcan-3-ch1orcpropane 1, 2-Dibrancmthane ( EDB ) Dibran= ethane 1,2 -Dichlorobenzene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene Dichlorodi.fluorauethane 1,1-Dichloroethane L 0 G Hydrologic -Asheville, Inc FL932774 23254 Kermure NI�1-2 11/8/93 N/A 11/12/93 NETHOD EPA 502.2 CAS N0. SDL 71-43-2 1.0 108-86-1 1.0 74-97-5 1.0 75-27-4 1.0 75-25-2 1.0 74-83-9 1.0 104-51-8 1.0 135-98-8 1.0 98-06-6 1.0 56-23-5 1.0 108-90-7 1.0 75-00-3 1.0 67-66-3 1.0 74-87-3 1.0 95-45-8 1.0 106-43-4 1.0 124-48-1 1.0 96-12-8 1.0 106-93-4 1.0 74-95-3 1.0 95-50-1 1.0 541-73-1 1.0 106-46-7 1.0 75-71-8 1.0 75-34-3 1.0 RESULT ( ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 CCMPANY NAME: ANALYSIS 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- l,2-Dichloroethene 1, 2-Dichloroprcpaie 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichlorcprcpene Ethylbenzene Hexachlorobutadiene Isoprcpylbenzene p-Iscpropyltoluene Methylene Chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2 -Tetrachloroethane 1,1,2,2 -Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorcbenzene 1, 2, 4-IPrichlorcbenzene Hydrologic -Asheville, Inc FL932774 23254 Kemare W--2 11/8/93 NXIC-11 * CAS NO. SDL C ug/1) 107-06-2 1.0 75-35-4 1.0 156-59-4 1.0 156-60-5 1.0 78-87-5 1.0 142-28-9 1.0 590-20-7 1.0 563-58-6 1.0 10061-01-5 1.0 10061-02-6 1.0 100-41-4 1.0 87-68-3 1.0 98-82-8 1.0 99-87-6 1.0 75-09-2 1.0 91-20-3 1.0 103-65-1 1.0 100-42-5 1.0 630-20-6 1.0 79-34-5 1.0 127-18-4 1.0 108-88-3 1.0 87-61-6 1.0 120-82-1 1.0 ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 BDL = Below Sauple Detection Limit SDL = Sample Detection Limit C:O1I5: 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 Page 3 continued CCHPANY NAME: Hydrologic-Asheville, Inc HYDROLOGIC PRWECTT NCAutB,ER: FL932774 HYDROLOGIC SAMPLE NOM6ER: 23254 SAMPLE IDEN`T'IFICATION : Kenmure MW-2 DATE SAMPLED: 11/8/93 NETHW EPA 502.2 ANALYSIS CAS NO. SDL RESULT ( u9/1) ( u9/1) 1,1,1-Trichloroethane 71-55-6 1.0 BDL 1,1,2-Trichloroethane 79-00-5 1.0 BDL Trichloroethene 79-01-6 1.0 BDL Trichlorofluoromethane 75-69-4 1.0 BDL 1,2,3-rrichloropropane 96-18-4 1.0 BDL 1,2,4-Trimethylbenzene 95-63-6 1.0 BDL 1,3,5-Irrimethylbenzene 108-67-8 1.0 BDL Vinyl Chloride 75-01-4 1.0 BDL Xylenes (total) 1330-20-7 1.0 BDL Dichloramethane 75-09-2 1.0 BDL BDL = Below Sauple Detection Limit SDL = Sample Detection Limit C:O1I5: 1491 Twilight Trail 0 Frankfort, KY 40601 0 502/223-0251 0 FAX 502/875-8016 0 Toll Free 1-800/728-2251 �cncn-0g-OD0 0zn O� c �SDCD CD m in.�02 29 0.CDQ) 00 -- jo CD3 0 Z n _ 0 --1 m m CL o m S e a� O •N O n N 33�3333333c3 003 cc ca o ca (Q cc ca ca cc ca :; (a 3 3 cc ZKcnXcflCDc:=r pp�ZEf Z Rw.3 2 ZO C §.3`� -.03 3o�N 3z z O CJt 333333333333333 ca ca cc ca cc cc ca ca ca ca ca to (a ca ca x- 0 0 oM m N N —cn CD= mc C-+ Sf o �Cl- c c c ins 3N�Z nC1CL �Z o (n m 3 CD crCLn CD cn 333 r 2iaU ocqv �� z� p. 3 Cd o _ -0 Z co cn 3 s cn, t� Oc)1 ,fes O N C1J a v to �• i n l0 o N Nn c n o CL CL 5 CA). .« o CD c � � m o o :3 00 NLn Cm' 70 ZZZ CD V 'S m0'o3 C vim -K N 0 � v � .. m N „ -n ip V (D o N o m M v N O s g S C+O 'S z O c 1 1 D� z (D c O (D "'S C C CD No � � m o :3 00 Cm' 70 ZZZ o N m0'o3 C vim -K com � v � .. m n ip w m g (D o o m M v � s g S m z 14 1 1 COMPANY NAME: COMPANY PROJECT: HYDROLOGIC PROJECT NUMBER: HYDROLOGIC SAMPLE NUMBER: SAMPLE IDENTIFICATION: DATE SAMPLED: DATE EXTRACTED: DATE/TIME ANALYZED: ANALYSIS Benzene Bramobenzene Bramochloraffethane Brcutodichloromethane Bromoform Brthane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chlorcanethane 2-Chlorotoluene 4-Chlorotoluene Dibroamchlorcmthane 1,2-Dibramo-3-chloropropane 1,2-Dibrthane (EDB) Dibrcmnethane 1,2 -Dichlorobenzene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene Dichlorodifluoramethane 1,1-Dichloroethane L 0 G I C Hydrologic -Asheville, Inc EL920191 10667 #2-Q85W2 11/27/92 N/A 12/07/92 METHOD EPA 502.2 CAS NO. SDL ( ug/1) 71-43-2 0.5 108-86-1 0.5 74-97-5 0.5 75-27-4 0.5 75-25-2 0.5 74-83-9 0.5 104-51-8 0.5 135-98-8 0.5 98-06-6 0.5 56-23-5 0.5 108-90-7 0.5 75-00-3 0.5 67-66-3 0.5 74-87-3 0.5 95-45-8 0.5 106-43-4 0.5 124-48-1 0.5 96-12-8 0.5 106-93-4 0.5 74-95-3 0.5 95-50-1 0.5 541-73-1 0.5 106-46-7 0.5 75-71-8 0.5 75-34-3 0.5 RESULT ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL A 1003 Twilight Trail • Frankfort, Ky. 40601 • (502) 223-0251 • FAX: (502) 227-9451 • Toll Free: 1-800-728-2251 ® R 0 L 0 G I C I N Page 2 continued COMPANY NAME COMPANY PROJECT: HYDROLOGIC PROJECT NUMBER: HYDROLOGIC SAMPLE NUMBER SAMPLE IDENTIFICATION: DATE SAMPLED: ANALYSIS 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichlorcpropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichlorcpropene trans-1,3-Dichlorcpropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Methylene Chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2 -Tetrachloroethane 1,1,2,2 -Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene Hydrologic -Asheville, Inc EL920191 10667 #2-Q85W2 11/27/92 METHOD EPA 502.2 CAS NO. SDL ( ug/1) 107-06-2 0.5 75-35-4 0.5 156-59-4 0.5 156-60-5 0.5 78-87-5 0.5 142-28-9 0.5 590-20-7 0.5 563-58-6 0.5 10061-01-5 0.5 10061-02-6 0.5 100-41-4 0.5 87-68-3 0.5 98-82-8 0.5 99-87-6 0.5 75-09-2 0.5 91-20-3 0.5 103-65-1 0.5 100-42-5 0.5 630-20-6 0.5 79-34-5 0.5 127-18-4 0.5 108-88-3 0.5 87-61-6 0.5 120-82-1 0.5 RESULT ug/1) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1003 Twilight Trail Frankfort, Ky. 40601 (502) 223-0251 • FAX: (502) 227-9451 Toll Free: 1-800-728-2251 u R 0`4 L 0 G I C µ Page 3 continued COMPANY NAME: Hydrologic -Asheville, Inc COMPANY PROJECT: Keinure HYDROLOGIC PROJECT NUMBER: EL920191 HYDROLOGIC SAMPLE NUMBER: 10667 SAMPLE IDENTIFICATION: #2-Q85W2 DATE SAMPLED: 11/27/92 NETHOD EPA 502.2 ANALYSIS CAS NO. SDL RESULT ( ug/1) ( ug/1) 1,1,1 -Trichloroethane 71-55-6 0.5 BDL 1,1,2 -Trichloroethane 79-00-5 0.5 BDL Trichloroethene 79-01-6 0.5 BDL Trichlorofluoramethane 75-69-4 0.5 BDL 1,2,3-Trichloropropane 96-18-4 0.5 BDL 1,2,4-Trimethylbenzene 95-63-6 0.5 BDL 1,3,5-Trimethylbenzene 108-67-8 0.5 BDL Vinyl Chloride 75-01-4 0.5 BDL Xylenes (total) 1330-20-7 0.5 BDL M BDL = Below Sample Detection Limit SDL = Sample Detection Limit COMMEN'T'S: 1003 Twilight Trail Frankfort, Ky. 40601 • (502) 223-0251 FAX: (502) 227-9451 Toll Free: 1-800-728-2251 0 C O N CQ (D 0� CD \N -ion c �� iDC7-�� _�c PRO \ m in �n�mo2' O= A —�O 0 ooh z3�-�o 0 ~ _ o `�D CD 3 o O �_ -n-n y �� 3. 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Cb m ° z Cffn o o � � f � m Aff-Aff ArAff VC to December 17, 1991 HydroLogic, Inc. 122 Lyman Street Asheville, NC 28801 LABORATORY RESULTS CONTROL #: 6342 RECEIVED : 12/04/91 ANALYZED : 12/05/91 SAMPLED : 11/26/91 METHOD 502.2 PARAMETER BENZENE BROMOBENZENE BROMODICHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE n—BUTYLBENZENE sec—BUTYLBENZENE tert—BUTYLBENZENE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE E. FEB - 6 1 SAMPLE ID: KENMORE #2 MATRIX : WATER METHOD : 502.2 If, AMOUNT UNITS ND<0.009 ND<0.006 ND<0.01 ?1919- ND<0.02 p ND< 1.6 ND< 1.1 ND<O. 02 91 ND<O. 02 is ND<0.06 if ND<O. 0 1 If ND<O. 003 of ND<O. 1 ff ND<O. 02 of ND<.03 it P.O. Box 4204 9 1003 Twilight Trail * Frankfort, Ky 40604 * (502) 223-0251 Work * (502) 223-0454 Mobile #6342 PARAMETER AMOUNT UNITS 2-CHLOROTOLUENE ND<0.01 ug/L 4-CHLOROTOLUENE ND<0.01 It DIBROMOCHLOROMETHANE ND<0.03 it 1,2-DIBROMO-3-CHLOROPROPANE ND< 3.0 if 1,2-DIBROMOETHANE ND<0.8 if DIBROMOMETHANE ND< 2.2 of 1,2-DICHLOROBENZENE ND<0.02 " 1,3-DICHLOROBENZENE ND<0.02 if 1,4-DICHLOROBENZENE ND<0.007 it DICHLORODIFLUOROMETHANE ND<.05 it 1,1-DICHLOROETHANE ND<0.07 it 1,2-DICHLOROETHANE ND<0.03 it 1,1-DICHLOROETHENE ND<0.07 If cis-1,2-DICHLOROETHENE ND<0.02 if trans-1,2-DICHLOROETHENE ND<0.05 to 1,2-DICHLOROPROPANE ND<0.006 if 1,3-DICHLOROPROPANE ND<0.03 1° 2,2-DICHLOROPROPANE ND<0.05 " 1,1-DICHLOROPROPENE ND<0.02 If ETHYLBENZENE ND<0.005 " HEXACHLOROBUTADIENE ND<0.02 " ISOPROPYLBENZENE ND<0.05 p-ISOPROPYLTOLUENE ND<0.01 METHYLENE CHLORIDE ND<0.02 " NAPHTHALENE ND<0.06 " REVIEWED BY #6342 PARAMETER AMOUNT UNITS n-PROPYLBENZENE ND<0.004 ug/L STYRENE ND<0.01 1,1,1,2 -TETRACHLOROETHANE ND<0.005 1,1,2,2 -TETRACHLOROETHANE ND<0.01 TETRACHLOROETHENE ND<0.04 TOLUENE ND<0.01 1,2,3-TRICHLOROBENZENE ND<0.03 1,2,4-TRICHLOROBENZENE ND<0.03 1,1,1 -TRICHLOROETHANE ND<0.03 1,1,2 -TRICHLOROETHANE ND<0.03 TRICHLOROETHENE ND<0.01 It TRICHLOROFLUOROMETHANE ND<0.03 if 1,2,3-TRICHLOROPROPANE ND<0.4 it 1,2,4-TRIMETHYLBENZENE ND<0.05 if 1,3,5-TRIMETHYLBENZENE ND<0.004 VINYL CHLORIDE ND<.02 o -XYLENE ND<0.02 m -XYLENE ND<0.01 p -XYLENE ND<0.01 REVIEWED BY m O -0 m = %v � C: CD CD CD Q' CD 3 a <D cfl v O -n :" Ul ,n n O 3 3 3 3 3 � 3 3�° 3 -f —I cn cn -V= .3 O D C7 � a 0 O C7 O r 0 M O � D cc cc wq p n ° m Cl) w cc cc O cc o o a -CD to w O a CD m m=mMw 1 Z w C,) w c W CD o n O p — o l7 p N — w o 3 3 C7 w Co m ° CD m O a C "� D o 0 0 CO : u' c O 0 3 r cn 3 0 c o cn w '0 m � a 3 3 0 3 o W o n 0 3 D c0� a Z 3 n CD =� o 3 � a N r CD cn w ` ° l cc a c. CD w-= w O O D n o o CD (n o -n -n Z m (D. � o. w m i o ' N W N o w OO -p w < a- (n �. CSD n (n o_ -� o 3 C) c) co D Z" 0 , o c CD m n Q 7 D0. �� p a c �. 3 Z (D O w p C -' cc (fl � 0 n a 3 3 3. c- c W 7 w N O `t� cc - o D 3� n a C -� ° N Z c L U)w a Z CD o O aCD - m rn __ cD c. 3 (D a 3 a 3 c C(D -D cn ao U' rn o N '<• cn 3 CDD CD o uri i O n Q m �C 3 Q C/) CD �- f Q � U' •a O o O °' w c c tc tc � ` c c :3 tc cc cn L 3 O v CD m cn rn cr W N 1 FD* d y r O O N = lD Q CDD ^+ 0i 1 W w 00 A I CD — CD cD N = %v � C: CD CD CD Q' CD 3 a <D cfl v O -n :" Ul ,n n O 3 3 3 3 3 � 3 3�° 3 N 3 cn 3 .3 S 3 3 3 3 3 3 3 c 3 -- o i o 3 � cc \ cc cc wq p n i pD Cl) cc cc \ \ - - cc cc cc cc cc cc cc . to o O cc n 0 ca a c o n p \ \ \ \ w w o 3 3 C7 w 3 Co m CD Z z O a C "� D 0 moo 0 O 3 m 0 c o m '0 fl l ZI f)m Z Z z = . 7C = -n n C7 n 0 00 D m Z Z 0 CL c CD =� o 3 CD a N r CD Z w cc 0 cc m e c. w w-= O O n o co CD (n z � O 7 o l i 0 i i ' N W N o w OO -p w < a- (n �. CSD n (n o_ -� o 3 C) c) co D = 0 , o c CD Q 7 D0. �� p a c �. 3 Z (D O w p C -' cc (fl � 0 n a 3 3 3. c- c Z w N O `t� cc - D 3� c°n c I -� c < 3 c cn U)w a m o O aCD - m rn cD c. 3 (D 0 3 3 w c -D cn ao U' rn o N '<• cn 3 CDD o uri O n Q m �C 3 Q C/) Q � U' •a O o O °' w c c tc tc � c c c c (fl (c cc cc c c :3 tc cc cn 3 cc 3 O 3 fc CD m cn o C FD* d y o N N C a 3 >S 0 a � o (D Cn (D O C 0 fl. 3 � to 0 O N O CL CL cD N fy IS O C w O D a. �Z CD ccn CD l a m Jo D r_ O Z O Z O O r n 0 m m lu --I In m c G ' op `7 r r f < ��% �'• t ^� < 4 CD CD CD Q' CD 3 a <D cfl v O -n :" Ul ,n 3 3 3 3 3 � 3 3�° 3 3 3 3 p 10 I I I m cc cc o cc cc cc cc cc��xc co cc cc \ cc \ cc cc p n Cl) m CO \ \ - - \ - \ - \ \ \ - - - \ - - - \ - \ - O r c o p w o Z z a D 0 moo 0 O 3 m Q '0 f)m Z = . o 6Et 0 CD =� CCD N r CD Z W O 0 � N O� in Qa a Cf)o w c. 7C CD ~ W (n r � O 7 o h o2 i o OO -p Ln < a- (n �. CSD Fl(D m m (D (D D0. �� Q rt m N O C1 a% r-, a CD O I I < U)w a m C °' m o (D CD n w c -D cn ao Cf)CD N '<• CDD n O �C 3 � U' •a O o O °' t� ^ c c tc tc c tc c c c c (fl (c cc cc c c :3 tc cc cn 3 cc 3 O 3 fc CD m cn C FD* d w O D a. �Z CD ccn CD l a m Jo D r_ O Z O Z O O r n 0 m m lu --I In m c MASS SPEC SERVICES INC . Environmental Analytical Laborato 1 1003 Twilight Trail P. O. Box 4204 Frankfort, Kentucky 40604 (502) 223-0251 March 18, 1991 HYDROLOGICS INC. P.O. BOX 18029 ASHVILLE, NC. 28814-0029 LABORATORY RESULTS MSS #: 4953 SAMPLE IDs #2 RECEIVED: 3/11/91 MATRIX: WATER ANALYZED: 3/13/91 METHOD: 8240 PARAMETER AMOUNT UNITS ACETONE ND<100* ug/L ACROLEIN ND<50 it ACRYLONITRILE BENZENE ND< 5 , BROMODICHLOROMETHANE ND< 5 BROMOFORM C- BROMOMETHANE ? _ ND<10 2—BUTANONE ND<10 ED - CARBON DISULFIDE u<a y ND< 5 91 CARBON TETRACBLOR ND< 5 �� CHLOROBENZENE , CHLOROETHANE ND<10 � 2—CHLORO ETHYL VINYL ETHER if CHLOROFORM ND< 5 4 DIBROMOCHLOROMETHANE DIBROMOMETHANE 1,4-DICHLORO-2-BUTANE DICHLORODIFLUOROMETHANE 1,2 -DICHLOROBENZENE 1,3 -DICHLOROBENZENE 1,4 -DICHLOROBENZENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE trans-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE cis-1,3-DICHLOROPROPENE trans-1,3-DICHLOROPROPENE ETHANOL ETHYLBENZENE ETHYL METHACRYLATE 2-HEXANONE IODOMETHANE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE STYRENE 1,1,2,2 -TETRACHLOROETHANE TETRACHLOROETHYLENE TOLUENE 5 ND< 5 if if if ND< 5 it ND<10 it ND< 5 .. if of ND< 5 If VV to to it if of 11 if 0 it of o 0 0 ND<100 if ND< 5 if ND<10 if ND<50 if ND<10 if ND< 5 of ND<50 if ND<10 0 of 0 IV ND< 5 it IV PARAMETER AMOUNT UNITS 1,1,1—TRICHLOROETHANE ND< 5 ug/L 1,1,2—TRICHLOROETHANE of TRICHLOROETHYLENE if TRICHLOROFLUOROMETHANE it VINYL CHLORIDE ND<10 XYLENE (TOTAL) ND< 5 " SURROGATE RECOVERIES 1,2—DICHLOROETHANE—D4 92% TOLUENE-D8 106% BROMOFLUOROBENZENE 91% ANALYSIS BY Ci i REVIEWED BY /7 f 1'irilLiL *SW 846 METHOD 8240 PRACTICAL QUANTITATION LIMITS h -I A o Cl) •o co u c �- 2� � � � _ n C7 C7 r p � � p -n -» Z 0 o°: -Z m CD m �_ sv m moo w 0. 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BOX 27887 - RALEIGH.N.C. 27811, PHONE (919) 733-5083 WELL CONSTRUCTION RECORD FOR OFFICE Ub, Quad.: No. � & Serial 1, Lat. 3 -V IS -Ato Long. oZ -24 Minor Basin Basin Code Header Ent. GW -1 Ent._ DRILLING CONTRACTOR Froehling & Robertson. inc_ STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER 1045 PERMIT NUMBER: 44-0210-WM-0032 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: Flat Rock, N.C. - County: Henderson (Road, Community, or Subdivision and Lot No.) 2. OWNER Kenmure Properties ADDRESS Post Office Box 537 (Street or Route No.) Flat Rock NC 28731 City or Town State Zip Code 3. DATE DRILLED 9-29-89 USE OF WELL. Monitor 4. TOTAL DEPTH 15 n CUTTINGS COLLECTED ❑ Yes ® No 5. DOES WELL REPLACE EXISTING WELL? ❑ Yes O No 6. STATIC WATER LEVEL: Dry FT. ❑ above TOP OF CASING, ❑ below TOP OF CASING IS 2.2 FT. ABOVE LAND SURFACE. 7. 'YIELD (gpm): N/A METHOD OF TEST N/A 8. WATER ZONES (depth): N/A 9. CHLORINATION: Type N/A Amount N/A 10. CASING: Wall Thickness Depth Diameter or Weight/Ft. Material From 0 To -15.0 Ft. 2" S H� D 40 PVC From To Ft. From To Ft. 11. GROUT: Depth Material From 0 To -4 Ft: Cement From To Ft. 12. SCREEN: Method Depth Diameter Slot Size Material From -5 To -15 Ft. 2" in. .010 in. PVC From To Ft. in. in. From To Ft. in. in. 13. GRAVEL PACK: Depth Size Material From -4 To -15 Ft. 30-40 Sand From To Ft.� 14. REMARKS: I DO HEREBY CERTIFY THAT THIS WELL WAS QONS.TRUCTE.0 STANDARDS, AND THAT A COPY OF THIS RE MAR, SIGNATURE OF b GW -1 Revised 11/84 Submit original to Depth DRILLING LOG From To Formation Description 0 17.2 Henderson Gneiss If additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) � !�{ t9'j tzt +2s 1�IONIia(` Nr y 1 S � L/ 41, m WITH 15 NCAC 2C, WELL CONSTRUCTION `L OWNER. TRAC�OR AGEN� DATE ivision-,o-Enxironrrt ntal Management and copy to well owner. I North Carolina - Dep"Unent of gnvironment and Natural Resources - Division of Water Quality - Groundwater Section - 1636 Mail Service Ccmcr _lWeigb, NC 27699.1639 - Phone No. (919) 733-3221 WELL ABANDONMENT RECORD WELL coNTRAcToR WELL CONTRACTOR CERTIFICATION 0 1. WELL USE (Check Applicable Box): Residential Ll Municipal Q industrial E3 Agriculture! O Monitoring Recovery ❑ Heat pump Water Injection ❑ Other 0 If Other, List Use: 2. WELL LOCATI : (Showa tch a location on back of forr) Nearest Town:LL� (Road Name and Number, Co ty, Subdivision , Lot No. Quadrangle No. 3. OWNER: �� mt�r��� WELL DIAGRAM: Draw a detailed sketch of the 4. ADDRESS: Vl" LA�-t r well showing total depth. depth and diameter of semens rernaWns.inithe well, gravel ictmval, S. TOPOGRAPHY: draw slope 'lltop, valley, flat intervals of casing p&&rations, and depths and circlo one) �/ types of fill materials used. 6. TOTAL DEPTH: �� DUM 7. CASING REMOVED: diame aVf ` 8. DISINFECTION: (Amount of 701/b hypochlorite used:) 9. SEALING MATERIAL: Net crmen Sandfxm= bags of cement bags of cement F gallons of water gallons of Qtb= Type material Amount !.IAIN N�ETHOD EMPLA NT OM Foc,trA � ( �v1 '� n 11. DATE WELL ABANDONED =_7D'3 I do hereby certify that this well was abandoned in accordance with 15A NCAC 2C, well construction standards, and that a copy of the record has been proto the well owner. /' Date5*,&� Signature of person abandoning the well -4w) WELL LOCATION: Draw a location sketch on the reverse of this sheet, showing the direction and distance of the well to at least two (2) nearby reference points such as roads, intersections and streams. Identify roads with State Highway road identification numbers. Submit original to the Division of Water Quality, Grouadwater Section, one copy to the owner within 30 days from completion of abandonment. GW -30 Revised 1.2149 95- V 6 KENMURE PROPERTIES, INC. COUNTY: HENDERSON DATE SAMPLED rf��� �� fr••�3•�r ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE CHROMIUM,TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM M BAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN ORTHOPHOSPHATE pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS VOC ZINC STATIC WATER LEVEL Red Ink=Sample taken by facility M/�Lz opo DATV SAMPLVI) ALKALINITY, To pli 4.5 ALKALINITY, TO rll 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE CIIROMIUM, TOTAL, COBALT COU COLIFORM, IiECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS I;LUORIDE HARDNESS CaCo3 HARDNESS, NON CARR IRON LEAD LITHIUM Ri~d Itik = SAmrle taken by ff►culty VVCLL Dr2y WaL DAY WELL NO. Q SS V 6 f ^� COUNTY: H fND cRso.✓ DATE SAMPLED MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIE. CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS VOC ZINC STATIC WATER. LEVEL Red Ink = Sample taken by facility DATE SAMPLED // 17_�� li- 7- 11-3-'19 ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM 9 BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE 7 f CHROMIUM, TOTAL O j COBALT J, J COD -3: COLIFORM, FECAL COLIFORM, TOTAL c l _i I / a COPPER CYANIDE DISSOLVED SOLIDS % a� FLUORIDE HARDNESS CaCo3 HARDNESS, NON CA" i IRON LEAD LITHIUM Red Ink = Sample taken by facility WELL NO. -()9-6V(l COUNTY: 1-1,51v'06Rso1 DATE SAMPLED MBAS 6 MAGNESIUM II MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL II NITRATE & NITRITE ORGANIC SCAN pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM -4 SELENIUM SILVER SODIUM SPECIE CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS VOC ZINC STATIC WATER LEVEL O'l 1, 3 Red Ink = Sample taken by facility Iv.S tx /-- F / C i &-l-J SA M P4- L DATE SAMPLED ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE _ CADMIUM CALCIUM _. CARBONATE - CHLORIDE CHROMIUM. TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS 66 y FLUORIDE HARDNESS CaCo, HARDNESS, NON -CARBONATE IRON -- - LEAD _ ---- -- LITHIUM V Red Ink = Sample taken by facility COUNTY DATE SAMPLED A`7- /�.� - rf� ;/- ?,A '76, 11-20.• MEAS MAGNESIUM 11ANGANESE MERCURI NICKEL _ NITROGEN. AMMONIA I NITROGEN, KJELDAHL NITRATE & NITRITE IV,p3 3 ORGANIC SCAN PH PHENOLS �� Jae � �' 1 °� � �•� PHOSPHORUS, TOTAL _ 0' - — POTASSIUM SELENIUM w _ SILtiER SODIUM SPECIFIC CONDUCTANCE — SULFATE TOC (UNFILTERED) �`• TOX TSS A'OC ZINC _-- STATIC WATER LEVEL i COuwr ..,ATE SAMPLES IIIJIALINITY TO PH 4.5 ALKALINITY, TO PH 8.3 ALUMINUM - `ARSENIC BARI UM ! � I BICARBONATE �ChDMIUM Eu.iLCI UM !CARBONATE 4 CHLORIDE, / d • 3 CHROMIUM, TOTAL COD . COLIFORM, FECAL I COLIFORM, TOTAL / !lt rc COPPER CYANIDE ! F --T DISSOLVED SOLIDS ! 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Fax: 704-875-�, December 02, 1997 PACE Project Number: A7111> PACE Sample Number: 93 0487750 Date Collected: 11/17/97 Date Received: 11/19/97 Client Sample ID: Kenmore MW Parameter Units PRL V6 METHOD DATE ANALYZE[ ORGANIC ANALYSIS VOLATILE ORGANICS 6230D Dichlorodifluoromethane ug/L 0.5 ND 11/26/97 Chloromethane ug/L 0.5 ND 11/26/97 Chloroethene (Vinyl chloride) ug/L 0.5 ND 11/26/97 Bromomethane ug/L 0.5 ND 11/26/97 Chloroethane ug/L 0.5 ND 11/26/97 Trichlorofluoromethane ug/L 0.5 ND 11/26/97 l,l-Dichloroethene ug/L 0.5 ND 11/26/97 Dichloromethane ug/L 0.5 ND 11/26/97 trans-1,2-Dichloroethene ug/L 0.5 ND 11/26/97 1,1-Dichloroethane ug/L 0.5 ND 11/26/97 cis-1,2-Dichloroethene ug/L 0.5 ND 11/26/97 2,2-Dichloropropane ug/L 0.5 ND 11/26/97 Chloroform ug/L 0.5 ND 11/26/97 Bromochloromethane ug/L 0.5 ND 11/26/97 1,1,1 -Trichloroethane ug/L 0.5 ND 11/26/97 1,1-Dichloro-l-propene ug/L 0.5 ND 11/26/97 Carbon tetrachloride ug/L 0.5 ND 11/26/97 1,2-Dichloroethane ug/L 0.5 ND 11/26/97 1,1,2 -Trichloroethene ug/L 0.5 ND 11/26/97 1,2-Dichloropropane ug/L 0.5 ND 11/26/97 Bromodichloromethane ug/L 0.5 ND 11/26/97 Dibromomethane ug/L 0.5 ND 11/26/97 cis-1,3-Dichloro-l-propene ug/L 0.5 ND 11/26/97 trans-1,3-Dichloro-l-propene ug/L 0.5 ND 11/26/97 1,1,2 -Trichloroethane ug/L 0.5 ND 11/26/97 1,3-Dichloropropane ug/L 0.5 ND 11/26/97 Tetrachloroethene ug/L 0.5 ND 11/26/97 Dibromochloromethane ug/L 0.5 ND 11/26/97 1,2-Dibromoethane--- g/L 0.5 ND 11/26/97 1,1,1,2-Tetrachloro TRaq �i� L /L 0.5 ND 11/26/97 Bromoform�� �. $ 1998 /1 0.5 ND 11/26/97 Laboratoryitifi� `ta ton IDs ` C`" . � eville ater nwl--QSecti(1 i. Asheville Re ir�na4 't - Laboratory Certification IDs "C Wastewater :, tz PORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water' 8776' TN UST List SC990bE}`, This report shall not be reproduced, except in full, VA Drinking Water 213 f ' , without the written consent of Pace Analytical Services, Inc Mr. Harry James Page 12 Client Reference: J&J Kenmore PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units PRL ORGANIC ANALYSIS Pace,, An<lr,., 9800 Kincey Avc. Huntersville;, TO 704-875 Fax: 704-8754 December 02, 1997 PACE Project Number: A7111i. 93 0487750 11/17/97 11/19/97 Kenmore MW V6 METHOD DATE ANALYZED VOLATILE ORGANICS 623OD 1,1,2,2 -Tetrachloroethane ug/L 0.5 ND 11/26/97 1,2,3-Trichloropropane ug/L 0.5 ND 11/26/97 Bromobenzene ug/L 0.5 ND 11/26/97 2-Chlorotoluene ug/L 0.5 ND 11/26/97 4-Chlorotoluene ug/L 0.5 ND 11/26/97 1,3 -Dichlorobenzene ug/L 0.5 ND 11/26/97 1,4 -Dichlorobenzene ug/L 0.5 ND 11/26/97 1,2 -Dichlorobenzene ug/L 0.5 ND 11/26/97 1,2-Dibromo-3-chloropropane ug/L 0.5 ND 11/26/97 1,2,4-Trichlorobenzene ug/L 0.5 ND 11/26/97 Hexachlorobutadiene ug/L 0.5 ND 11/26/97 1,2,3-Trichlorobenzene ug/L 0.5 ND 11/26/97 Benzene ug/L 0.5 ND 11/26/97 Toluene ug/L 0.5 ND 11/26/97 Chlorobenzene ug/L 0.5 ND 11/26/97 Ethylbenzene ug/L 0.5 ND 11/26/97 Xylenes, (total) ug/L 0.5 ND 11/26/97 Styrene ug/L 0.5 ND 11/26/97 Isopropylbenzene ug/L 0.5 ND 11/26/97 n-Propylbenzene ug/L 0.5 ND 11/26/97 1,3,5-Trimethylbenzene ug/L 0.5 ND 11/26/97 t-Butylbenzene ug/L 0.5 ND 11/26/97 1,2,4-Trimethylbenzene ug/L 0.5 ND 11/26/97 s-Butylbenzene ug/L 0.5 ND 11/26/97 4-Isopropyltoluene ug/L 0.5 ND 11/26/97 n-Butylben ug/L 0.5 ND 11/26/97 Naphthalen L1 ug/L 0.5 ND 11/26/97 JAN — 81998 Laboratory Certification ll',k Laboratory Certification I s NC WastewaterRESORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water 37706—`e'TN UST List Sc 99006This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services. Inc. n 0 3 3 (D r- f7u, T- cu .° CD �o- I I CD o °. c a h w�o OD^� r -m 00 O �sz� D,c �o C D � ; 0 U'O -•I L m Z .. O D n o o n( coo D D'o Cn -0 0 TID -p 0 0 cn N U) o o• = w 0 w x x S o V s o m Cl) 0 0 0 0 0 o w Q w A a70 0= = 0 0 0 d o 3. a o o>> t _w w o o r 2 0 m w e o, w w -,� ooCD 0 3 N (D A O N p O O 0 0= O o x m O 0 C } w A CD X N A O S S o 'a O —I -n (D 3 w A � w p o 0 m 00 is A in 0 CA (D a O w w _ M M � 3 :3 N(D Ci 1 j K � $ a m (n cD O (n cn S 0 u, o cn co 0 ❑ D e Z3 0 r rq n ca wco o mo . = m � A 0. 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O D o U1 Cn -0 0 -n 1 ? D Zo cn N U) ,, a o D n 0 o V s o m Cl) 0 - Q- Z a70 Z 0,6 o C CD o O t 0 w w -,� ooCD 0 ^ o 3 ❑❑ n w p o 0 m 0 CA (n c' _ M M � 3 :3 Ci -G K � $ m (n cD O (n cn S 0 cn CD 3 n ❑ D e Z3 0 r rq n ca wco o mo . = m �.,0 0. U) Cc 0 y aha o� i r R m =' j' N n3 r � O �13 R, ' 19 1G r' s N3 m .gin G.5' UC m m O o ' Q m =r w m 0 0- z a CL m o M l Q: m, c 3 fn (D W m ^ d (n N S' I -o (D w -. b EO cnc rl 2 0 m Iw CD X y 3 0 (D O C ^ (D Q G m 20 <M 03 Z 0� n am mZ 7v o 0 p� .. D m r� k X o w w O? O cam— Z C. 3 �Z0) w 4c" M °' S (1) (D M 0 00 Z 0 m m Cil ZKK7=MC)000m>-vZZ w �cQ i (D (D c :'QO w i g U) moQ30C)CO--mCD Q=(a C5 �cQ0M.3o"Z W m c� (D 3 3 � 0rQ 0 �c_o l< 01 3 w.� c�nc3 w3 ocnai cD3 – wZZ D cnm 154 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 (O (Q (Q (0 (Q (Q (Q (O (Q (0 (Q (Q (Q (Q (Q i- i-- Z--- Z-- � =--i- 0 � =T A CD C wcn a O (D =3 n z �• n 3 a 0 C Q CD w Q -0 N 73 Z a (D =5 O' o Q =3 CD Z 0 (D f7 Q ( . (D a = 0 CD C � Z Cy Q CDc D CD w (D 0 (D (D (D o 0 Q 0 CMI) 3 W 0= w -n z m a 0 o O �; w 0 m m 2 70 o CD o M06 2_ CD 7 m 3 c D. ( � _ U) -3 m m� t m m �cn 0 CD .= � O (D PL) o ooc> 0 CD m -" CD CD m 0 o 3 3 a m Q Q W, D 0 cc cn C m z M �i w CD CD CD -0 m cr h m WN CD v _0 o 0 N D m c m -n _0 z D� TI N (n "O 0 ® a 5.m r D m m m A 01 CL O cn a m CL v cn o c 6 cc c r, in vCD v CD c CD m w Q- OL z 3 Cn m (D Ch CD d m 3 70 < m O m c0 m nzzz mo -00 C Umo00 O.w y m O C/)' � r m m r v 0 cfl m e: C o D m Q Cl. G ,�....s..-5a+ —I coC!»1L,bDC7—170 0'z C-)00 �o70 C: =7W =rO=v� Zsv o ° 0 0 " E;� E;�p O 0 W � Q� CD 2 C�^� 0 c 00 w M 0 cn (n300 CDCDnCDD CD 33 z3C� �?� CD Z)Q�.... 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G ,�....s..-5a+ -TICAL FAX NO,, 704 252 4618 Mr. Harry James Page 3 Client Reference: J and J Kenmore 12-31-96 Pam Andylcb)" �4 Rayem Fax: '04-2524618 December 04, 1996 PACE Project Number: A61IZ06,9i PACE Sample Number: 93 0305911 Date Collected: 11/20/96 Date Received: 11/21/96 Client Sample 10. Parameter Units PRL Kenmore METHOD V6 DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS Dichlorodifluoromethane Ug / L 1.0 502.2 NO 12/01/'96 Chloromethane Chloroethene (Vinyl chloride) Ug/L ug/L 1,0 1.0 NO ND 12/01/96 12/01/96 Bromomethane UqA 1.0 NU 12/01/96 Chloroethane ug/L 1.0 ND 121'01/96 Trichlorofluoromethane ug/L 1.0 NO 12/01/96 1,1-Dichloroethene ug/L 1'0 NO 12/01/96 Dichloromethane ug/L 1'0 NO 12/01/96 trans-1,2-Dichloroethene Ug/L 1.0 NO 12/01/96 1,1-Dichloroethane ug/L 1.0 NO 12/01/96 cis-1,2-Dichloroethene ug/L uqJL 1.0 1'0 No ND 12/01196 12/01/96 2,2-Dichloropropane Chloroform ug/L 1.0 NO /96 12;01196 Bromochloromethane 1,1,1 -Trichloroethane ug/L ug/L 1.0 1.0 NO ND 12/01/96 12/01/96 1,1-Dichloro-1-propene ug/L 1.0 ND 12/01/96 Carbon tetrachloride uq1L 1'0 NO 12/01/96 1,2-Dichloroethane ug/L 1.0 ND 12i01196 1,1,2 -Trichloroethene ug/L 1.0 ND 12/01/9E 1,2-DichloroPrOane ug/L U9 (L 1.0 1.0 ND NO 12/01/96 121/01/96 Bromodichlorome'thane ' Dibromomethane uq/L I . C, ND 12/cii% cis-1,3-Dichloro-l-propene ug/L 1.0 NO 12/01/96 trans-1,3-Dichlaro-1-propene ug/L. 1.0 ND 12/01/96 1,1,2 -Trichloroethane ug/L 1.0 NO 12/01/9e 1,3-Dichl cropropane fL ug /L 1.0 ND 12101/96 Tetrachloroethene Ug/L 1.0 NO 12/01/96 Dibromochloromethane Ug/L 1.0 NO 12/01/96 1,1,1,2 -Tetrachloroethane ug/L 1.0 NO 12/01/96 Bromoform ug/L 1.0 NO 12/01/96 1,1,2,2 -Tetrachloroethane ugA 1.0 NO 121011`9E REPORT OF LABORATORY ANALYSIS Th;$ reporl Sha�f no,. oe reproduced exceptin furl without the wristen oonSenj at PaCe AnalyllCal SeMrSS inC eTlCqL A v% FAX NO., 704 2112 4618 Mr. Harry James Page 4 Client Refererce: J and J Kenmore 12-31-96 Pact Ariaipicai'., 54 Raver.30,, Asheville, NC "el- 704-254-7176 Fax 704-2624610 December 04, 1996 PACE Project Number: A61120600 PACE Sample Number: 93 0305911 11/20/96 Date Collected: 11/21/96 Date Received: Client Sample ID: Units PRL Kenmore V6 METHOD DATE ANALYZED Parameter ORGANIC ANALYSIS VOLATILE ORGANICS Uq/L 1.0 502.2 NO 12/01/96 1,2,3-Trichloropropane uq/L 1.0 NO 12/01/96 Bromobenzene 2-Chlorot,cluene ug/L 1,0 NO 12/01/96 4-Chlorotoluene ug/L uq/L 1.0 1.0 NO NO 12/01/96 12/01/96 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene ug/L 1.0 NO 12/01/96 1,2 -Dichlorobenzene uq/L ug/L 1.0 1.0 ND NO 12/01/96 12/01/96 1,2-Dibromo-3-chloropropane 1.0 NO 12/01/96 1,2,4-Trichloroberzene Hexachlorobutaidiene ug/L Ug/L 1.0 NO 12J0I/96 1,2,3-Trichlorobenzene ug/L. 1.0 1,0 ND ND 12/01/96 12/01/96 Bianzene uq/L Toluene ug/L ug/L. 1.0 1.0 ND NO 12/01/96 12/01/96 Chlarobenzene Ethylbenzene ug/L 1.0 NO 12/01/96 Xylenes, (total) ug/L uq/L I'D 1.0 NO NO 12/01/96 12J0I/96 Styrene Isopropylbenzene ug/L 1.0 NO 12/01/96 n-Propylbenzene uq/L ug/L 1.0 1�0 NO ND 12/01/96 12/01/96 1,3,5-TrimethylbLanzone ug/L 1.0 NO 121,01/96 t-Butylbenzene 1,2,4-Trimethylbenzenp ug/L 1.0 NO 12101/96 s-Butylbenzene ug/L ug/L 1.0 1.0 NO NO 12/01/96 12/01/96 4 -Isopropyl toluene n-htylbenzene qiL. Lg/L 1.0 1.0 NO NO 12/01/96 12/01/96 Naphthalene REPORT OF LABORATORY ANALYSIS This repair shah nol be reproduced, CACCV( in full. without the written concert of Pace Arisjyt:741! Sevice% inc n d 7r ;F = CD 3 = 0 0 0 0 su v v A N CDCL CD -i c' cp 0 N -4 c c B cD 0 CD o co CD CD Ci. A A 'O 6 i A OD ? N � W W — Ti A -� -o_ �l ;0 0 0 m r n n w & p n O == O �A,'�$ n ;CD o_o (Am m 0 0 3 3 - 2 A� n 0 0 0 a rn o �w N CD CD 0 0 Z.. D w 0 � �p ��w n O W W A O DO CL 3 O Ri -3 O CD z Z3CO 'o D1 — n D7 CD O D co C7 p �no- --jCD M nn �► o.cn — Ti A -� -o_ �l ;0 0 0 m r CD - --:Eo > Q� co M C � � 37 0 a :cn0r-0 �A,'�$ n ;CD o_o (Am m 0 0 3 3 - 2 A� n D v .a- 0 0� 4 o 0 �w N CD CD 0 rN�00tn Z.. D w Cal 0 � cn ��w n O � FN c� ul O DO CL 3 Ri -3 TI m z Z3CO 'o wv LL--. 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No 98e01 TO 704.944.7174 Fax: 704.949.4419 Mr. Harry James February 07, 1996 Page 6 PACE Project Number: A60122601 Client Reference: James & James PACE Sample Number: 93 0171834 Date Collected: 01/22196 Date Received: 01/24/96 Client Sample ID: Q85 U6 Parameter Units MOL #V6 DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANIG5 1,2,3-Trichioropropane ug/L 1.0 ND 01/24/96 Bromobenzene ug/L 1.0 ND 01/24/96 2-Chlorotoluene ug/L 1.0 NO 01/24/96 4-Chlorotoluenef ug/L 1.0 NO 01/24/96 1,3 -Dichlorobenzene ug/L 1.0 NO 01/24/96 1,4-Dichloroberizene ug/L 1.0 NO 01/24/96 1,2 -Dichlorobenzene ug/L 1.0 NO 01/24/96 1,241bromo-3-Chloropropane, ug/L 1.0 NO 01/24/96 1,2,4-Trichlorobenzene ug/L 1.0 NO 01/24/96 Mexachlorobutadiene ug/L 1.0 ND 01/24/96 1,2,3-Trichlorobenzene ug/L 1.0 NO 01/24/96 Benzene ug/L 1.0 ND 01/24/96 Toluene ug/L 1.0 NO 01/24/96 Chlorobenzene ug/L 1.0 ND 01/24/96 Ethylbenzene ug/L 1.0 NO 01/24/96 Xylenes ug/L 1.0 ND 01/24/96 Styrene ug/L 1.0 NO 01/24/96 Isopropylbenzerie ug/L. 1.0 NO 01/24/96 n-Propylbenzene ug/L 1.0 NO 01/24/96 1,3,5-Trimethylbenzene ug/L 1.0 NO 01/24/96 t-6utylbenzene ug/L 1.0 NO 01/24/96 1,2,4-Trimethyllbenzene ug/L 1.0 ND 01/24/96 s-Sutylbenzene ug/L 1.0 NO 41/24/96 4-Isopropyltoluene ug/L 1.0 NO 01/24/96 n-Butylbenzene ug/L 1.0 NO 01/24/96 Naphthalene ug/L 1.0 NO 01/24/96 ndwater D m < m 0) 0_ W CD CD CD 0 D c 0 N CD C1 CD C (D fT fD w fT w o �o tm M 7 C m 0 c. 0 y lD O O 72. fn O 7 0 C. a m N N lv cr C fD m F c m Z 0 Z' O ChD O O c=D N _ w C7 � O O C CD CD rrt ,.p tU c� NO c' U) C% O CD CD W C2 O O O CL a A) n— I-�Cl)Cnti G)>0 To-oc=r �) 2: (fin � 0 CD CD CD n Q z co w 3 n =3 :3 0.0 0 CD -I-v p z 00 CD m 00 �2Un-O. cn P E;: _.: 30 O O CD . 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