NC0025135_ARO_GWDataHistorical_20190204

1
Micha,
William 6.,
North Carolina Department of Environment and i
r
Alan W. Klimek, .
Division of Wo
Coleen H. Sullins, Deputy.
Division of Water Q.
GROUNDWATER SECTION
September 23, 2003
Mr. Lee T. Huffman
Huffinan Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffinan:
Subject: Groundwater Monitor Well Analytical Results
Huffinan Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization To Construct
Caldwell County, North Carolina
Enclosed for your information are copies of the analytical results for samples collected by
this office from the groundwater monitor wells on August 19, 2003. Also enclosed is a copy of
the NC DENR/DWQ Chemistry Laboratory Data Qualifier Codes sheet for reference.
If you have any questions, please contact me at [phone]
/ar /
Enclosures
Sincerely,
Ann C. Rumbough
Environmental Technician
F WIM,
*A-
N. C. Division of Water Quality / Groundwater Section
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 FCustomer Service
Phone: [phone] Faxr(828) 251-6452 Internet: http://gw.ehnr.state.nc.us 1-877-623-6748

41TOR WELL SAMPLING FIELD LOG
Date: August 19, 2003
Facility: Huffman Finishing Company
County: Caldwell
Contact: Lee Huffman
Well #
Depth (ft)
SWL (ft)
Amt. Bailed/Pumped
Time
Remark
MW-2
K72g2
30
5.65
Bailed 12 gal.
1050
Water dingy.
TEMP: 200 C
pH: 5.0
Spec. Cond.: 20 at 25' C
MW-3
K72g3
15
7.1
Bailed 4 gal.
1110
Water clear.
TEMP: 180 C
pH: 6.0
Spec. Cond.: 80 at 250 C

0F W � Michat
0� OG
William G. Ross, Jr., Sec.
North Carolina Department of Environment and Natural Resoul,
`C Alan W. Klimek, P.E. Directoi..
Division of Water Quality
Asheville Regional Office
GROUNDWATER SECTION
September 30, 2002
Mr. Lee T. Huffman
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization To Construct
Caldwell County, North Carolina
Enclosed for your information are copies of the analytical results for samples collected by this
office from the groundwater monitor wells on August 20, 2002. Also enclosed is a copy of the NC
DENR/DWQ Chemistry Laboratory Data Qualifier Codes sheet for reference.
If you have any questions, please contact me at [phone].
Sincerely,
C.
Ann C. Rumbough
Environmental Technician
/af
Enclosures
A5MR—R
Groundwater Section, 59 Woodfin Place Asheville, NC 28801-2414 Telephone: [phone] Customer Service
Fax: [phone] 623-7748

MONITOR WELL SAMPLING FIELD LOG
Date: August 20, 2002
Facility: Huffman Finishing Company
County: Caldwell
Contact: Lee Huffman
well #
Depth
(ft)
SWL (ft)
Amt.
Bailed/Pumped
Time
Remark
MW-2
K72g2
30
10.8
Bailed 10 gala
1040
-Water dingy.
TEMP: 19.70 C
PH: 6.16
Spec. Cond.: 30.3 at
250 C
MW-3
K72g3
15
8.7
Bailed 3 gal.
1105
Water clear.
TEMP• 21.40 C
PH: 5.98
Spec. Cond.: 151.5 at
250 C

l \
Michael F. Easle,
�0� WA , William G. Ross Jr.,
QG North Carolina Department of Environment and Natural Re.
y Gregory J. Thorpe, F,
r- Acting Direci.
"i Division of Water Quality\,
.r
GROUNDWATER SECTION
August 17, 2001
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Enclosed for your information are copies of the analytical results for samples collected by this
office from the groundwater monitor wells on June 18, 2001. Also enclosed is a copy of the NC
DENR/DWQ Chemistry Laboratory Data Qualifier Codes sheet for future reference.
If you have any questions, please contact me at [phone].
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
Enclosures
N
Customer Service Division of Water Quality / Groundwater Section
1 800 623-7748 1636 Mail Service Center Raleigh, NC 27699-1636
Phone: [phone] Fax: [phone] Internet: hftp://gw.ehnr.state.nc.us

IFS B. HUNT.jRr',I
IERNOR
NORTH CAROLINA DEM:'
ENVIRONMENT AND NATURAL K
DIVISION OF WATER.
ASHEVILLE REGIONAL
hr
GROUNDWATER SECTION
August 11, 2000
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical
results for samples collected by this office from the groundwater
monitor wells on June 12, 2000.
If you have any questions, please contact me at
[phone].
Sincerely,
Ann C. —bough
Environmental Technician
/acr
Attachments
INTERCHANGE, BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NC 28801-2414
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

NORTI -.AROLINA
ENVIRONMEN' AND NATURAL\.
DIVISION OF WATE,
ASHEVILLE REGIONAL
GROUNDWATER SECTION \
August 26, 1999
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
t
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical
results for samples collected by this office from the groundwater
monitor wells on June 15, 1999.
If you have any questions, please contact me at
[phone].
Sincerely,
C.
Ann C. Rumbough
Environmental Technician
/acr
Attachments
INTERCHANGE BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NC 28801-2414
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

NORTH CAROLINA DEPARTM',
ENVIRONMENT AND NATURAL RESOD.
DIVISION OF WATER QUAk.,
AOLzw,triI I C Mwr--vANAI nfrirl't
GROUNDWATER SECTION

ate of North Caroli(
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
A. Preston Howard, Jr., P.E., Director
Asheville Regional Office
GROUNDWATER SECTION
October 20, 1997
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Compliance Monitoring Reports
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Permit No. NCO025135 Authorization to Construct issued on June 5, 1989,
requires Huffman Finishing Company to sample groundwater monitor wells K72g2
(MW-2) and K72g3 (MW-3) for Volatile Organic Compounds (VOC's) in November of
each year. This letter is a reminder that the report of laboratory analyses
for VOC's should be attached to each Groundwater Compliance Report Form (GW-
59) when it is submitted to the Raleigh office.
Attached for your information is a copy of the new policy on approved
laboratory analyses for determination of VOC's in groundwater.
If you have any questions, please contact me at [phone].
Sincerely,
C'
Ann C. Rumbough
Environmental Technician
/acr
Attachment
cc: Shuford Wise
Betty Wilcox
Interchange Building, 59 Woodfin Place�® FAX [phone]
Vf
Asheville, North Carolina 28801 An Equal Opportunity/Affirmative Action Employer
Voice 704-251-6208 - 50% recycles/10°%o post -consumer paper

State of North Carolina r
Department of Environment,
Health and Natural Resources 4 • •
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B, Howes, .Secretary
A. Preston Howard, Jr., P.E., Director FD FE H N FZ
Asheville Regional Office
GROUNDWATER SECTION
July 23, 1997
Mr. A. W. Huffman, Jr.
Huffman Finishing. Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the groundwater monitor wells on
June 17, 1997.
If you have any questions please contact me at [phone]
Sincerely,
�L----
Ann C. Rumbough
Environmental Technician
/acr
Attachments
Interchange Building, 59 Woodfin Place W_ FAX [phone]
Asheville, North Carolina 28801 C An Equal Opportunity/Affirmative Action Employer
Voice 704-251-6208 50% recycles/ 10% post -consumer paper

Facility:
County:
Contact:
MONITOR WELL SAMPLING FIELD LOG
Date: June 17, 1997
Huffman Finishing Company
Caldwell
Lee Huffman
well #
Depth
(ft)
SWL (ft)
Amt.
Bailed/Pined
Time
Remark
MW-2
K72g2
30
7.62
Bailed 3-1/2
gal.
10:20 AM
Water dingy.
MW-3
K72g3
15
7.85
Bailed 1-1/4
gal.
10:30 AM
Water clear.

.F '
State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Asheville Regional Office
GROUNDWATER SECTION
October 21, 1996
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Compliance Monitoring Reports
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Permit No. NCO025135 Authorization to Construct issued on June 5, 1989,
requires Huffman Finishing Company to sample groundwater monitor wells K72g2
(MW-2) and K72g3 (MW-3) for Volatile Organic Compounds (VOC's) in November of
each year. This letter is a reminder that the report of laboratory analyses
for VOC's should be attached to each Groundwater Compliance Report Form (GW-
59) when it is submitted to the Raleigh office.
If you have any questions, please contact me at [phone].
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
cc: `Shuford Wise
Beaty Wilcox
Interchange Building, 59 Woodfin Place
Asheville, North Carolina 28801
Voice 704-251-6208
FAX [phone]
An Equal Opportunity/Affirmative Action Employer
50% recycles/10o/. post -consumer paper

-AA
State of North Carolina
Department of Environment,
Health and Natural Resources
Asheville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary IDIEHNF;Z
DIVISION OF WATER QUALITY
GROUNDWATER SECTION
August 1., 1996
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the grow)dwater monitor wells on
June 17, 1996.
If you have any questions, please contact me at (704) 251--6208.
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
Attachments
Interchange Building,
59 Woodfin Place, N"WfC
Asheville, North Carolina 28801
Voice 704-251-6208 FAX [phone],1,52
An Equal Opportunity Affirmative Action FrTiployer
5.0% recycled/ 1 Cr/. post -consumer paper

FIELD LOG
rlvivllvn WELL SAMPLING
Date: June 17, 1996
Facility: Huffman Finishing Company
County: Caldwell
Contact: Lee Huffman
Well
Depth
(ft)
SWL (ft)
Amt.
Bailed/Pumped
Time
Remark
MW-2
K72g2
30
8.15
Bailed 3-1/2
gal.
10:20 AM
Water clear.
MW-3
K72g3
15
8.3
Bailed 1 gal.
10:40 AM
Water clear.
I

State of North Car zAina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor G H F1
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
GROUNDWATER SECTION
October 30, 1995
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Compliance Monitoring Reports
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Permit No. NCO025135 Authorization to Construct issued on June 5, 1989,
requires Huffman -Finishing Company to sample groundwater monitor wells K72g2
(MW-2) and K72g3 (MW-3) in March, July, and November of each year. This
letter is a reminder that the report of laboratory analyses for sampling of
VOC's in November should be attached to each Groundwater Compliance Report
Form (GW-59) when it is submitted to the Raleigh Office.
If you have any questions, please contact me at [phone].
Sincerely,,
/mac
Ann C. Rumbough
Environmental Technician
/acr
cc: Shuford Wise
Betty Wilcox
Interchange Building, 59 Woodfin Place, Asheville,N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50%recycled/ 10% post -consumer paper

State of North Cal ._ ;i�a
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr„ Governor
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
m
GROUNDWATER SECTION
August 8, 1995
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the groundwater monitor wells on
June 19, 1995.
If you have any questions, please contact me at [phone].
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
Attachments
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% past -consumer paper

Facility:
County:
Contact:
MONITOR WELL SAMPLING FIELD LOG
Date: June 19, 1995
Huffman Finishing Company
Caldwell
Lee Huffman
Well #
Depth
(f t)
SWL (f t)
Amt.
Bailed/Pumped
Time
Remarks
MW-2
K72q2
30
11.6
Bailed 3 gal.
10:50 AM
Water clear.
MW-3
K72q3
15
11.5
Bailed 1 gal.
10:30 AM
Water dingy at first-
then cleared up.
NOTE: BAIL FIRST

State of North Carolina
Department of Environment,
Health and Natural Resources i
Division of Environmental Management
A milli
James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary [D F H N p1
Nann B. Guthrie, Regional Manager
Asheville Regional Office
GROUNDWATER SECTION
October 28, 1994
Mr. A. W. Huffman, Jr.;
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Compliance Monitoring Reports
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Permit No. NCO025135 Authorization to Construct issued on June 5, 1989,
requires Huffman Finishing Company to sample groundwater monitor wells K72g2 and
K72g3 for Volatile Organic Compounds (VOC's) in November of each year. This
letter is a reminder that the report of laboratory analyses for VOC's should be
attached to each Groundwater Compliance Report Form (GW-59) when it is submitted
to the Raleigh office.
If you have any questions, please contact me at [phone].
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
cc: Betty Wilcox
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment,
Health and Natural Resources A�j
•
Division of Environmental Management
James B. Hunt, Jr., Governor AdIbbodUmm
® � I N
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
GROUNDWATER SECTION
August 24, 1994
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NC0025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the groundwater monitor wells on
June 27, 1994.
If you have any questions, please contact me at [phone].
Sincerely,
Ann C. Rumbough
Environmental Technician
/acr
Attachments
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

MONITOR WELL SAMPLING FIELD LOG
Date: June 27, 1994
Facility: Huffman Finishing Company
County: Caldwell
Contact: Lee Huffman
Vell
t
I (ft)
| Pumped
Time
Remarks
(7252
30
| 1.0.5
| Bailed 9-1/2 gal.
| 11:05 AM
| Water dingy.
(MW-2)
92q3
| 15
| 11.5
| Bailed 1-1/2 gal.
AN
| Water dingy at
"MW-a)
|
|
| first -then cleared
|
|
|
|UP.
!NOTE: BA T L FIRST

140MITOR WELL sAMPLIENG FIELD LOG
Date: June 8, 1993
Facility: Huffman Finishing Company
County* Caldwell
Contact: Lee Huffman
Depth SWL
Well # (ft) k ,f
t
- - -I.
K72q2 1 30 8.4
(MW-2) ii
K72q3 115 10.6
(MW-3)
Amt. Bailed/
Pumped
Bailed 10 gal.
Bailed 3 gal.
Time
10: 25 AN
10:45
Remarks
Water very turbid.
ater turbid at first -
hen cleared up.
[OTE: BAIL FIRST

State of North Ca,,�lina ,
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
August 18, 1993
Mr. A. W. Huffman, Jr.
Huffman Finishing Company -
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. N00025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the groundwater monitor wells on
June 8, 1993.
If you have any questions, please contact me at [phone].
Sincerely,
G
Ann C. Rumbough
Environmental Technician
ACR/gc
Attachments
I11tc0lanpc Ruil(linp, 51)'N�"1fin f lacc, C(). Ijut 170, A4imille, N.C. 2RR020370 0 Tcicphone 704-29-6208
An t?gnal Oprxntunity ,Af(innativ�A� tk�n FmpL,ycr

I l
i
i
MONITOR WELL SAMPLING FIELD LOG
Date: Mav 18, 1992
Facility: Huffman Finishing Company
County: Caldwell
Contact: Lee Huffman
Shuford Wise
Depth I SWL
Well (ft) � (ft)
Amt. Bailed/
Pumped Time
K72g2 30 10.75 9 gallons
(qW,-2
K72g3 15 18.85
1
(MW-3) 1
3 ,gallons
11:15 AMI
11:55 AM
Remarks
Water turbid.
Water turbid.

STAtt o ,y
`r ii `.
State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
Jaines Q. Hunt, Jr., Governor Ann B. Orr
Jonathan R Howes, SecretaryDIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION Regional Manager
March 1, 1993
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
P 411 632 903
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Notice of Violation
Huffman Finishing Company
Permit No. N00025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Permit No. NCO025135 Authorization to Construct issued on June 5, 1989,
requires Huffman Finishing Company to take samples of groundwater, analyze
those samples and report the results 'of analyses to the Division of
Environmental Management.
Permit No. N00025135 Authorization to Construct stipulates that the
analytical methods used for TOX must be capable of detecting the total of all
halogenated organic compounds present at a concentration of 5.0 parts per
billion (ppb) or greater. In the event that a TOX concentration of 5.0 ppb or
greater is detected, any individual halogenated organic compound(s) present at
a concentration at or above the method detection limit (MDL) must be identified
and quantified utilizing EPA Methods 601, 602, 604, and 611.
Review of compliance monitoring data reported for the November 17, 1992,
sample date indicates TOX concentrations of 39 ug/l for monitor well K72g2 and
26 ug/l for monitor well K72g3. You are in violation of Permit No. NCO025135
Authorization to Construct in that individual halogenated organic compounds
were not identified.
hrterchangr Building, 59 WwAfin Place, Asheville, N.C. 28801 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

4"
State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James G. Martin, Governor Ann B. Orr
William W. Cobey, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
July 15, 1992
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Groundwater Monitor Well Analytical Results
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for your information are copies of the analytical results for
samples collected by this office from the groundwater monitor wells on May 18,
1992.
If you have any questions, please contact me at [phone].
ACR/gC
Attachments
Sincerely,
Ann C. Rumbough
Environmental Technician
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28861 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

WELL DATA TABULATION
POLLUTION SOURCE MONITORING SITE
Facility Name: -H"/--/--/'1/4,,V r11V151411VG Col- PA^ly _County: CA L L9 WE' -
Pollution Source (lagoon, landfill, etc.) 1-14GOC>�
Latitude: 35
Permit No: Longitude: 9/0 3 3-5
Non -Discharge: NPDES: AJ C 0 0 -2 � / 2S-
Wel I Const. 4: 1-3- 0 / f 0 -- w/w - o o 6 o DHS: Quad No: K 7 ;7- 1.2, i 3
Sampled By: 6,6M GR-0"A1,Qv,1A-7-6R -5-T,41--W
Well No.
Date
Installed
Total
Depth
(ft)
Diam.
(in)
Screen(S)/
Open hole.
(OH)
(ft-ft)
Grout
Interval
(ft-ft)
Gravel/Sand
Pack
interval
(ft-ft)
Remarks
2
.2-:2 0-17,2
30
2,
:sZ-2 0 -30
o -
20- 30
1,('7-?X- 3
Draw a diagram on the reverse side of this form showing map location of the site and the
location (direction and distance) of each well with respect to the pollution source and to
each other. Indicate sampling schedule, parameters and any changes to schedule.
GW-51
Revised 8/20/84

s CALDWELL COUNTY
' p
HUFFMAN FINISHING
Tl
GRANITE
FALLS UNNAMED TRIBUTARY
TO CATAWBA RIVER
RHODHISS \
BURKE COUNTY
HICKORY B
LONGVI EW
��l . U.S. 641, 70, 3ZI
CATAWBA COUNTY
01,0*0
fT PLANT
MW3

State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James G. Martin, Governor DIVISION OF ENVIRONMENTAL MANAGEMENT Ann B. Orr
William W. Cobey, Jr., Secretary GROUNDWATER SECTION
Regional Manager
May 27, 1992
Mr. A. W. Huffman, Jr.
Huffman Finishing Company
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
Subject: Compliance Monitoring Reports
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
Attached for future reference are copies of Compliance Monitoring Report
Forms containing information that is to be provided in compliance monitoring
reports submitted to the Groundwater Section. Also., information requested in
the highlighted areas is to be provided.
Note that well identification numbers have been assigned to each well. It
is necessary to use the numbers provided as they relate to our data entry
records. The previous well identification number, in parenthesis, is given for
reference. If there is any discrepancy between this information and your
records, please notify me so that any future confusion may be eliminated.
Please refer to the subject Authorization to Construct for requirements on
groundwater monitoring.
If you have any questions or comments regarding compliance monitoring,
please contact me at [phone].
Sincerely,
C%`' 7'L'' 1�� l� /`L--LL.?7.L�1..—Cv c,-c_-c'�•
Ann C. Rumbough
Environmental Technician
ACR/gc
Attachments
cc: Blue Ridge Labs
Betty Wilcox
Interchange Building, 59 V ibodfin I'lace, Asheville, N.C. 28801 • Telephone [phone]
An Fgird 011pwimity A(lirntative At firm FmldoNri-

m
J
l
t-�(ncn-vm) >o-�� o 200
v m D. sv :3Cl D) CD �— 0 0 o C7
y0CD0(1)8 i'a z
z 3 �, CD
?� 0 -n -n
(n
ipn E
D
CL
c°D C c ca o
m 33,333333393 003
Z(D (a 0 co ca co Up c� 3 c3 ;: c0 3 3 ca
0
8 W =(D =7��°��zz
C: o, $aa.
0-2
R� E 0 2 c3c2n00
.3 073 30m
3
v zz
'0 333333333333333
Lo
g l0 co (D (a (a (D (a (acacacacacacacaca
=r C
_g (D
c �N�z
x I Q.N�z
O n (D 0 Q m
Q a Zip a
OOc oN
't In �n c � ? 0 N�
0.
: m
N a y M 0
�FL
v cfl ccn cD ca
¢+ � ���
-.;
o
�, a
3
-.
0
n
a)
z
0
I
I
fin
I
R
0
R
r
r
m
mm
� c
m -6O z
0o�
0m m
I �
M'm�CDc
O nl
m
z
m
z
G
I z
0
o

m=
0
-,
!<
3 -o
(D
U)
o
U)
CD
m
z
v
c
v
�mcn�0= �0�0 �.� ��Z�
mawm50,..,9) � �
� m� 8D5 Oz OO o 'g4 r D�
52 B. Zorn** -a 2 _
weQ-�m
-I
S 6'
-Ti -n
e
33=73333333S3
003
cn ca 0 (a tD cD ca c� a c0 = (a
3 3 c�
ZKK7�cax �zz
c KKJF" �� C o OZ
�o
w P -v 3 c'j v2i z0
3.3`z 0�33oW.�'
3Zz
�l
hum
333333333333333
(a (a (a (a (a (a (a (a (a (a (a (0 (a (a (a
������»����»Z-2
3V5 M C-yZ
r- z
0 � n Q m
3
c
a QOL
cn
cfl co (a cn ca cfl
a
z
z
0
-,0
_�. r �0
-0
3 C
3
FL U
CL
2A W
£3
rr
0
0
to
C
�c
n
Ia
Z
m
m m 70
vow, C
-0
C m
nm m
u' mm Q c
o� ° �o m
�O
z � v
cz
o�
FA
s
z
O
m
3
rn.
m �r
lE 9 °
y zo I D
a
m
m
0
z

DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
May 27, 1992
MEMORANDUM
TO: Bob Cheek, Groundwater Section
Raleigh Central Office
FROM: Ann Rumbough 6')
Asheville Regional Office
SUBJECT: Additions to the Compliance Monitoring Network
Two new compliance monitor wells located at Huffman Finishing Company in
Caldwell County should be added to the compliance monitoring network. Well
numbers K72g2 (MW-2) and K72g3 (MW-3) were constructed to comply with Permit
No. NC0025135 Authorization to Construct dated June 5, 1989.
Data on the new wells is attached.
ACR/gc
Attachments

OW(`OF NATURAL RESOURCES AND C�Y DEVEIAPMEI,
DIVISION OF EwiRONwYrAL mANAC ttENT
WELL AND PUMP INSPECTION REPORT
Date 1 Y-
/
Well location !-1/V>7 FALLS i\lC Area
(Town, Comm., Subdivision and Lot No.) County GAS DwEc �.
Owner /_1 L.i FFMA,,V ,*iA11 _51411V G C aMla/,A/�`i
Road/Street
Address 13d X f `70 Quad No.
6 30 Serial No. /3-6-0 -311
A�
3-6-
Lat.® ong.
WELL CONSTRUCTION
tie/
L L w i'u i�'I ,r' 3 37
Drilling Contractor. �14KE%�'S PI G�MOA Address Reg. 46
Name
Meets Min. Standards
Measure
Yes No
Remarks
Permit
------
Location
Distance from
1
✓
Pollution source
— -,
Other location standardsTotal
3 0 '------
Depth
Casin
Depth
,!
Diameter
Weight/thickness '
40
� ----
/
Height
NIA
Drive shoe
_:Alm___
Exception approved by owner
Grout:
C6Miff aT
Type
Thickness
Depth
a o- 3p
Screens
IV114
Development
%1 /
�l G L ►N� S D K G D
I. D. Plate
N
.�
HAD v,IAi?".,Af6 LA 136
Abandonment ( temporary/permanent)
Water lever
/i,/�/�
Well test
— .=---
IVLA
Chlorination
Cuttings
Reports
Weser _ia"le (appearance)

cPfCRTMENT OF NATURAL RE , ^URCES AND COMMUNITY DEVELOPMENT
FOR OFFh
,dOF ENVIRONMENTAL MANAGEN GROUNDWATER SECTIONS
'P.O. BOX 27887 - RALEIOH,N.C. 278;q , PHONE [phone] Qull NO?� ✓;'
�gg2 Lat. S `f 6 i3 Long.
MAR 1 Minor Basin
WELL CONSTRUCTION RECOilb Basin Code
4 z
Header Ent. GW-1',
DRILLING CONTRACTOR Baker's Piedmont Well& Pump /�
STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER 339 PERMIT NUMBER: 13-0110-0-060
WELL LOCATION: (Show sketch of the location below)
Nearest Town: Granite Falls County: Caldwell
(Road, Community, or Subdivision and Lot No.)
OWNER Huffman Finishing Co.
ADDRESS P O BOX 170
granite Fa(,Sirset or RouteNCo.) 28630
City or Town State Zip Code
DATE DRILLED 2-20-92 USE OF WELL Monitor
TOTAL DEPTH 30 ' CUTTINGS COLLECTED ❑ Yes O No
DOES WELL REPLACE EXISTING WELL? ❑ Yes ® No
STATIC WATER LEVEL: 20 FT. O above TOP OF CASING,
M below
TOP OF CASING IS 1.5 FT. ABOVE LAND SURFACE.
YIELD (gpm): NA METHOD OF TEST
WATER ZONES (depth):
9. CHLORINATION:
Type
Amount
10. CASING:
Wall Thickness
Depth
Diameter or Weight/Ft. Material
From 0
To
20
Ft.
2" #4.0 pvc
From
To
Ft.
From
To
Ft.
1. GROUT:
Depth
Material Method
From 0
To
18
Ft:
cement pour
From 18
To
20
Ft.
Bentonite pour
2. SCREEN:
Depth
Diameter Slot Size Material
From 20
To 30 Ft.
2" in. .010 in, PVC
From
To
Ft.
in. in.
From
To
Ft.
in. in.
3. GRAVEL PACK:
Depth
Size Material
From 20
To_
30
Ft.
ASTM sand
Depth DRILLING LOG
From To Formation Description
V"
nco
►�i� t-_�41�`i,
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State Roads,
or other map reference points)
Hwy 321 North
to Granite Falls
Huffman
Finishing
Xwell
Hwy 321 South
From To Ft. C '/ �- To Hickory & I-4'0
4. REMARKS: T� _ ' /l/( Q121115-
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
SIGNATURE OF CONTRACTOR OR AGENT DATE
�W-1 Revised 11/84 Submit original to Division of Environmental Management and copy to well owner.

.. '
WELL NO.: K72q2 HUFFMANFINISHING- COMPANY
^
\
\�
�
COUNTY: CALOVVL
DATE SAMPLED
ALUMINUM
BARIUM
BERYLLIUM
CALCIUM
CARBONATE
CHROMIUMJOTAL
COBALT
UOLIFORM, FECAL
COLIFORM, TOTAL
CYANIDE
DISSOLVED SOLIDS
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
6-
0- 0'�z u
NITROGEN, KJELDAHL
NITRATE & NITRITE
ORGANIC SCAN
ORTHOPHOSPHATE
0,
PHENOLS
PHOSPHORUS, TOTAL
0.
POTASSIUM
SELENIUM
SILVER
TOX
TSS
VOC
Red |nk=Sannp|mtaken byfacility

.i
WELL NO.: K72g2 HUFFMAN FINISHING COMPANY COUNTY: CALDWE,
DATE SAMPLED
ALKALINITY,TO pH 4.5
ALKALINITY,TO pH 8.3
ALUMINUM
ARSENIC
D.v/G�t �fl.�te) c� • jig 0. Of c7 O.0/G, � [900�0
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE 3
CHROMIUM,TOTAL 10
COBALT
COD
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
CYANIDE
o. 00 Ss'
a• 0 f o
< ®. v r o
0. oo to -
0. 0a75
0. o /
0. oa-3
DISSOLVED SOLIDS
a
, f 0
� ^ 0
�
a1z
`gym
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
NITROGEN, KJELDAHL
0.100
O, s
©"
NITRATE & NITRITE
ORGANIC SCAN
Nd3` �
nr� 0 /0
/,,630�
o•
®� l0
ORTHOPHOSPHATE
C0.�
d,
U• SO
pH
PHENOLS
5 ' KS�
PHOSPHORUS, TOTAL
!,
POTASSIUM
SELENIUM
SILVER
SODIUM
SPECIF. CONDUCTANCE
� . 3
% . �9
� l . �
/ ,
j • I �
j ,
/, a2 �
SULFATE
S`LI
c • 0
S-- S D
9. /,S
30
SLf
g.
TOC (UNFILTERED)
0. -70
p, p
0. s 0
--a
TuxT©.iidb
v®
VOC
ZINC
STATIC WATER LEVEL
0Co3ly
g7
O'ols
0<,5 L
0.0Ao x
r
o' oas
0.00
0. 0 C
v.s"u t
0. 0-
o
,
/�
/G v
Red Ink=Sample taken by facility
�y
•I` L413 �IL�IE'O/2 _ /CEf a? s^ct� ALLCMiGtM 11vsT,'F7'rR0 O F Ags&,v ic-

DATE SAMPLED
ALKALINITY, TO pl14.5
ALKALINITY, TO pl1 8.3
ALUMINUM
ARSENIC
c O. oos-
v. ® p
BARIUM
BERYLLIUM
FBICAI]WOENATEEEE
CALCIUM
CARBONATE
CHLORIDE
/s-
CIIROM IUM, TOTAL
COBALT
COD
sgg
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
CYANIDE
DISSOLVED SOLIDS
D�
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
RCd Ink = Ssimnlp tnitnn by f.nn
M—

DATE SANIPLEU
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
4 n, �—
NITROGEN, KJELDAI-IL
NI'IRATE & NITRITE
/VL'j y
O •�
NO3
ORGANIC SCAN
PHENOLS
PHOSPHORUS, TOTAL
POTASSIUM
SELENIUM
SILVER
SODIUM
SPECIE. CONDUCTANCE
SULFATE
O �1
TOC (UNFILTERED)
� J
r p 2
TOX
TSS
VOC
ZINC
0.. of %
0 /
Oki NoP140-5PPA T E
o. /
D. /
STATIC WATER LEVEL
Red Ink = Sample taken by facility

'
t'
WELL NO. k 7 ,C a -2
COUNTY: C A L D Vt%& L L
DATE SAMPLED
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC < ©. ®! C 4. UDC t o ov
v� '
a° c C�. 01
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
o r
CHROMIUM, TOTAL
COBALT
COD
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER 0. UD % 0. OA
®. O/ 7
a° ®OA
CYANIDE
DISSOLVED SOLIDS
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

DATE SAMPLED
_ /S =�
%-/'ll'
�� `�i
-
.ors
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
0.01
� U f j.
� C> , !�
,�, L7 , S
®,
O, 0.6
NITROGEN, KJELDAHL
NITRATE & NITRITE
O' S9
�`
D a
NO3
"�°3
40.01
�03
O eiL�
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS, TOTAL
0,09
POTASSIUM
SELENIUM
SILVER
SODIUM
, j
0 . g�
/. /
l .
�• .S
SPECIF. CONDUCTANCE
SULFATE
G S®
0. 3
• 3 -7
la - 3 0
TOC (UNFILTERED)
< /, a
1, 0
zt,
TOX
L ® o
TSS
VOC
A z-c�Err
s HEE T
ZINC
of odq
0,007
t 0..00A
o, 0Al
©, ®a'%
C7. t 13
OR-TrIoPgosPN4A C
.<o, r©
<®, io
' o,S`
CJ.
STATIC WATER LEVEL
/f
, p�
' YJ

DATE SAMPLED
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
v, 0o l
< 0. 006,<
0. o 1
UGC
4 0, 006
< 0- oos`"
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
,IJ�
CHROMIUM, TOTAL
COBALT
COD
o
-7
do, 0
z '70. d
'10. 0
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
0. 0 /.3
< 0, v®�2
. v. Uo�
4 0. 00.2
0. oo*
CYANIDE
DISSOLVED SOLIDS
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
n a T_11- —cl-- '
.�. u 1•••• — oampie Laken by iacuity

COUNTY: C AL D W'e L. L
DATE SAMPLED
/f m � � n
J-/ I- R y
G -- y - l
'74- 7y-
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
lJ • �'
o • o 6
o• .6
NITROGEN, KJELDAHL
NITRATE & NITRITE
� 3 >�
•
a
0•7D
®•98
ORGANIC SCAN
pH
`�
i
S o
C/o
PHENOLS
PHOSPHORUS, TOTAL
0, 0,2
POTASSIUM
SELENIUM
SILVER
SODIUM
q
SPECIE. CONDUCTANCE
SULFATE
/
.3, o
j
Cv. �'
®. n
o" S6
TOC (UNFILTERED)
, 1
6
/ • eO
.�
TOX
TSS
VOC
•c
l3A�
0,25 u L
o. 6-0u9/
ZINC
0,016
O. 0r'
0.073
0-008
0- v/A
6,013
0/e-rgo P/1os P/-IATG
0,061
Q. 0 ,
0.03
G 0. / 0
4 0,03
STATIC WATER LEVEL
Red ink = .q-tm ip fnLn , h- f-;1;1-.,
2, 5 J
, S
7• 7-0-7
7 °

DATE SAMPLED
10-/7..9G
7-/7--76
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
0 . U l D
� O < UDC
� O. 00.6
-4 0.006
0 0 ® 5
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
410,0
—3, `7
• /
/ a G�
CHROMIUM, TOTAL
COBALT
COD
G S
G ®
a J
!/r 5, 3
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
D< o
D . O3 7
Q . Oea
O, oo
CYANIDE
DISSOLVED SOLIDS
j
f/ �,
�
7 `, 0
4
3 7,
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
icea inx = aampie taken by facility

WELL NO. �S 7,2 el j
ESAMPLED
FSNESIUM
�-
i7
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
NITROGEN, KJELDAHL
NITRATE & NITRITE
/V°3
'v03
110.3
N0 P
ORGANIC SCAN
PH
PHENOLS
PHOSPHORUS, TOTAL
POTASSIUM
0.01
SELENIUM
SILVER
SODIUM
SPECIE. CONDUCTANCE
SULFATE
TOvvC (UNFILTERED)
!j
<; / , O
1/G , 7
AID
L 3 v
a , 3
TOA
Ve'
TSS
VOC
ZINC
®. O
o C v 16
- C/-2
!? . 00,710,
O (
V . 00
O. 0a
C), a'/
0. ®(o
®. p
STATIC WATER LEVEL
pi'd Inlr = Cam.. 1- —1_ j_. r _!v!
-
s

DATE SAMPLED
1/'/.� %
�' %�
!� / 9 L✓
7_ fly
I/ /' `3��-�',
ALKALINITY, TO PH 4.5
ALKALINITY. TO pH 8.3
ALUMINUM
ARSENIC
G f�, G� lad°
G 0. l`11a 3
L p , C� %
L CJ s 00
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CAALCIUM
CARBONATE
CHLORIDE ,
3,
CHROMIUM., TOTAL
COBALT
33.3
COD
' 01 U
(o a.
,?o , 0
COLIFORM. FECAL
COLIFORM, TOTAL
COPPER
0, O;�
6 3
t 0, 02
A 0. 00 .7,
0 , 00
CYANIDE
DISSOLVED SOLIDS
J.-% �;
� / • �
�� O
FLUORIDE
HARDNESS CaCo,,
—
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility-

DATE SAMPLED
7- /Y-
MBAS
"LNGNTE S I UM
MANGANESE
MERCURY
NICFEL
NITROGEN, AMMONIA
C), 0
'e 0
4
NITROGEN, KJELDAHL
NITRATE & NITRITE
'v
-4.00
A
tvo.3
/Vo -3
ORGANIC SCAN
PEI
PHENOLS
PHOSPHORUS, TOTAL
POTASSILT',ki
SILVER
SODIUM
SPECIFIC CONDUCTANCE
SULFATE
2.0
3,-o
/0-6-
4 3,0-
TOC (UNFILTERED)
.4 /-o
TON'.
0. 0/0
TSS
IOC
0. 0 co) 0
z I N C
0 v
0. 0A
0.0&9
a.o,),
o . () 0 ('
o o o
cR -r i-io P H o s,01414 -rc
0. 0-5
0.03.
0.63
'o. -f 7
0,0/
STATIC WATERLEVEL2,
t, 50,01UM Lem r of-,V 41"E -;re� or vvlse,

DATE SAMPLED
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
/ CI
0- 00.6-
4 4? "�'�
� 0 0 i0
BARIUM
BERYLLIUM
-BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
CHROMIUM, TOTAL
COBALT
COD
Z 5
/ .S`
`. ©o C?
„ %, j)
COLIFORM, FECAL
COLIFORM,,TOTAL
COPPER
• L /%
0.03
(9. 0 1
0t 0.2
� � 0.0G
G 0 . 0_7
CYANIDE
DISSOLVED SOLIDS
'
° ,3
,9
10,9
=�
FLUORIDE
HARDNESS CaCU,
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

NO
GdtJNTY C :,4 L... 'ol\\
DATE SAMPLED
7-.? %- 3
11- 3 - i.
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICI:EL
NITROGEN, AMMONIA
0. C -f
� � � �
� U � ��
.4 0. 5-
0. o
NITROGEN, KJELDAHL
NITRATE & NITRITE
CJ
3
ORGANIC SCAN
PH
PHENOLS
PHOSPHORUS, TOTAL
0,0
0. 0.,7,
POTASSIUM
SELENIUM
SILVER
SODIUM
r
.3. o
2,
3, ox,
SPECIFIC CONDUCTANCE
SULFATE
+C
G �. U U
.� ✓
+►
L
43,0
TOC (UNFILTERED)
TON
TSS
VOC
ZINC
%�. D �V6
U• 07-/
®, U'ef6
0• 0*7
®, t-/ f
o, o &
'/s'.7140 -P i•1y S P i-/r4 rE
0. D �
tip
10,
0.03
STATIC 14ATER LEVEL
Y, `T
�y• �
to
� �
>
,

COUNTY
G
L 0 VV
L
DATE SAMPLED
-t.2
._ 1,7 _ rf 7,
ALKALINITY, TO pH 4.
ALKALINITY, TO pH 8.3
_
ALUMINUM
---- _-
ARSENIC
0 . 0 0 /
L. O, 0 / O
BARIUiM
BERYLLIUM
BICARBONATE
_ ---
CADMIUM
CALCIUM
CARBONATE
—
CHLORIDE
CHROMIUM, TOTAL
-
COBALT
_
COD
go
S'
7,0_
0.0
COLIFOR.M, FECAL
COLIFORM, TOTAL
,
COPPER
0- 0 D /
0- ooZ -2
0, U / 6
� �.
0 ,2,
0. 0 -3__..
CYANIDE
DISSOLVED SOLIDS
41,0
d
r
/00
FLUORIDE
HARDNESS CaCo,
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

DATE SAMPLED�,2®-9,
MBAS
MAGNESIUM
5-/l--502
7.3 1
-7-�
MANGANESE
MERCURY
NICKEL
NITROGEN, Ai`IMONIA
NITROGEN, KJELDAHL
NITRATE & NITRITE
ORGANIC SCAN
H
6-2
PHENOLS
PHOSPHORUS, TOTAL
v, U
POTASSIUM
SELENIUM
SILVER
SODIUM
SPECIFIC CONDUCTANCE
$•
SULFATE
S�
TOG (UNFILTERED)
TOE
TSS
VOc
ZINC
09-TN0PH0sPyA -rr--
/V!7
o ®r
I
j:
Iro Z)
0,
d. oy
AIA U,,? G,4 J i c-
STATIC WATER LEVEL
t
.7 . `- 5
3,10
� J, o
q reyA
0,0-371 oaf
c

COUNTY: CA L D WC —
DATE SAMPLED
U C��
v1 d
?"o L 4e c n��
o.
d. 9
�-r)qy

-j-icncn-oO�
oop
c�Zn3DCD
3
C
3
m
no-
=
=c3�CD�
a�
....
o°
a
w�zK
K
a
O_
�°m-n
T
cn
Q
O CD
cn
w
N
CD c
w n
w
CL °
- °'
�?
-m
F
.�
o
0
n
o
a
n
ni
I
ro
N
N
o
m
o
CD
c
o
3 3 s3 3 3 3 3 3� 3
6c)
CD
Cc Cc O cc UD (o cc co (o =n
3 3 10cD
o
c
0C-)CvDpSvZZ
�
Dco i cc (D c Qm a —
'
0
CD
_
o
Q3 0C-)CO -0 c�
CD
o � cv sv a� �a
x
3��.
-Oczco:/C 03E3c'•�O
-��3 C��Nm
(DC
O
v ill
(D 3
Rl
—
O � cn
Z Z
cn
z
O
^
d
0
ZD
cn
I_
n
3 3 3 3 3 3 3 3 3 3 3 3
3 3 3
2
(c
(n q
a
(D
a
O CD
O n
D
y� _Z
n
=0
r
aCL
.. .. .. -< E n
3 3 3 P
oo
tt
a a a^ D m
:it :tt -+ w n
u n u 0
z-
cD
v
O>Nmz Ix
53 :3u-.
(D
O Nr-Z <
CD M
-0 n M (n
(D (D
0 Z -
�c -
0 p
o �
3 cD
- c
O z
O
0
N
w
o_
0 ^
0
0
CD A CD
Q
o' L
c3333
CD CO 0 CD 0 �,I-,/(D
ao CO� cD =-
y S � a
w O $ a•o 71
ca _
m CD
= '0 CD �
<
(p N cr
CD
cnQ w M
Co • (? NI NI
to cn o
a
0cn�
+ D O Q CD O CD
Cr o
° 0 m (D � _
C) 3 w 3 0 ,_
o=vQti 3
° 3
I (o c c
j Co
n (a N
CCD D 0 I NJ0
CD
w
3
S 0
CD ❑ ❑ " c�
n
o�
m =
m CD
C
A7 S
c:
N
CD (D
p O
3
(D co
CD
N
<D
3
fJf
o cD 0
0 0
0
O
(D :D
m
zt n
o
0'
CD N :�
Co (D
CD �
LL
N �
J
T T ,
D z Z
a 3 °' Co
CD m m
N r-.
N Q.
w
o
3 0
z
m
Z v
o m
r
N
m
T
w
w o w
m
0
o d
O o
w
T
s
i
Z n
0CD
m w
w
o
=
w N
O
o
D
n o
�
a
-
N
cD
a
C
n
a
c
D
r O 0 cn
a
0
mCD -
--CD
O
(n
z l
x
- zee
o M
I
m
zu
a
D
to
'm
p
N y
o
r
a
3
7l
CD
3
O
m
m rlCD
°'
CD
CD
z
x
o
�cn
•
C D
v j
CD
wCL
o•
z
3
0
=
O
Z�
CD
w
w
0
o•
O
iD
€
o
o
w
m
sFn
CD
m
.�
0
mi
o.
_
Ol N
u

?ESEAR'ch . NAlyTICAt
AEIORATORI S ``c
L
INC. =�h NctY3,
Analytical/Process consultations
0 ANP���
'heroical Analysis for Selected Parameters and Water Sample Identified as Huffinan Finishing
4 {rater Tech Labs Inc. Pro'ect collected 10 November 2003
Volatile Organics Quantitation MW02 MW03
EPA Method 6210 D Limit
Parameter (RRh
I,I-Dichloroethane 0.5 BQL BQL
2,2-Dichloropropane 0.5 BQL BQL
Chloroform 0.5 BQL BQL
l,l,l-THchloroethane 0.5 BQL BQL
1, 1 -Dichloropropene 0.5 BQL BQL
Carbon Tetrachloride 0.5 BQL BQL
Benzene 0.5 BQL BQL
1,2-Dichloroethane 0.5 BQL BQL
Trichloroethene 0.5 BQL BQL
1,2-Dichloropropane 0.5 BQL BQL
Dibromomethane 0.5 BQL BQL
Toluene 0.5 0.9 0.8
1,1,2-Trichloroethane 0.5 BQL BQL
1,3-Dichloropropane 0.5 BQL BQL _
Tetrachloroethene 0.5 BQL BQL
1, 1, 1,2-Tetrachloroethane 0.5 BQL BQL
1,1,2,2-Tetrachloroethane 0.5 BQL BQL
1,2,3-Trichloropropane 0.5 BQL BQL
Hexachlorobutadiene 0.5 BQL BQL
Bromobenzene 0.5 BQL BQL
Ethylbenzene 0.5 0.9 0.6
Styrene 0.5 BQL BQL
Bromoform 0.5 BQL BQL
p-Isopropyltoluene 0.5 BQL BQL
N-Butylbenzene 0.5 BQL BQL
Naphthalene 0.5 BQL BQL
1,3,5-Trimethylbenzene 0.5 BQL BQL
1,2,4-Trimethylbenzene 0.5 BQL BQL
1,2,4-Trichlorobenzene 0.5 BQL BQL
1,2,3-Trichlorobenzene 0.5 BQL BQL
Chlorobenzene 0.5 BQL BQL
2-Chlorotoluene 0.5 BQL BQL
4-Chlorotoluene 0.5 BQL BQL
Tert-Butylbenzene 0.5 BQL BQL
Sec-Butylbenzene 0.5 BQL BQL
1,4-Dichlorobenzene 0.5 BQL BQL -
1,2-Dichlorobenzene 0.5 BQL BQL
Total Xylenes 0.5 0.8 0.6
I-Propylbenzene 0.5 BQL BQL v
N-Propylbenzene 0.5 BQL BQL
1,3-Dichlorobenzene 0.5 BQL BQL i -
Dibromochloromethane 0.5 BQL BQL
Dichlorod ifluoromethane 0.5 BQL BQL
Chloromethane 0.5 BQL BQL
Vinyl Chloride 0.5 BQL BQL
Bromomethane 0.5 BQL BQL
Chloroethane 0.5 BQL BQL t
Trichlorofluoromethane 0.5 BQL BQL CAD o
1,1-Dichloroethene 0.5 BQL BQL
Methylene Chloride 0.5 3.8 3.0
Trans- l,2-Dichloroethene 0.5 BQL BQL i
Cis-1,2-Dichloroethene 0.5 BQL BQL i
Bromodichloromethane 0.5 BQL BQL
s ��
Bromochloromethane 0,5 BQL BQL ma:_
Cis-1,3-Dichloropropene 0.5 BQL BQL
Trans-1,3-Dichloropropene 0.5 BQL BQL
Methyl-Tert-Butylether (MTBE) 0.5 BQL BQL
Isopropyl ether (IPE) 0.5 BQL BQL
Dilution Factor I I
Sample Number 490827 490828
Sample Date - 11/10/03 11/10/03
Sample Time (hrs) 0750 0830
Sample Analyzed 11/18/03 11/18/03
Time Analyzed 2332 2056
BQL = Below Quantitation Limits ppb parts per billion

x x
r"
c �onz
yQRoodo00
9 a; g
z
�
CA
Ln No
c c
5
m
O
x
EFF
° °g�9
a
z
za
n
cn
C
ry
d
�
m
e
rr
y
m
ElC
y
�
z
0
n
a
�
c
m
�e
H
�
n m
m X1A z
W
two

n U1
A
0 s
co
O
O d
y
w `I
I
NIN
x '
r
0
m
p
3
x
y
;r
m
m
co
I
r_-
v J' .p - � w 6� O` CT 0 O� O•
1p
~'
y
s
v
Cr
P O, L O N O 0 N co C.n 01 _
O O V
C71
—
?
GM
N
D
... _ LM
S
to
-F
to
C1
H
rL
c3o
0
O
c3o
O
Q m
G
T
-.
_ O.
p
S A -+ O'
-pig
co to {0 3 ,p 3 s c c c c c 3 c c c c
to t\ t\ t\
m
o
cr m c
<
\
m
m
=
Z
A
<
a
A
.0
_
'a
r+
�
QA
G
p
o
Z
a
v o o v co n Z O O
(A
o
Z
N
La
0
W
o o "' 2 0 0 0
a
m
X o z m -. s s
i-•i
m
v
N C p A N tpii O'
m
�. j y t0 lO u10i nrn
-4
•'h
�
Yl
v
O
o_
v

NC DENR/DWQ Chemistry Laboratory
Sample Anomaly Report (SAR) ✓
Report to: ARO Metals Fi;.
Lab Number: 3G1188 Sample ID: 2
Station Location: Huffman Finish County: Caldwell Region: ARO
Sample Type: Water Priority: Routine Collector: T. Minnick
Date collected: 8/19/03 Date received: 8/21/03 Date analyzed: 09/ 0 / 03
Affected Parameters : .Zane
Analytical Area (check one):
❑ WCH QX METALS ❑ VOA
❑ SVOA
❑ NUT ❑ MICRO ❑ PEST
The
following anomalies occurred (check all that apply):
Samples
Improper container used
Quality Control
Instrument failure — no reportable results
VOA vials with headspace
Analyst error — no reportable results
Sulfide samples with headspace
Surrogates
Samples not received, but listed on fieldsheet
None added
Samples received, but not listed on fieldsheet
Recovery outside acceptance limits
Mislabeled as to tests, preservatives, etc.
S ike recovery
Holding time expired
None added
Prior to receipt in lab
After receipt in lab
Recovery outside acceptance limits
Insufficient quantity for analysis
Failed to meet criteria for precision
Internal standards
Sample exhibits gross non -homogeneity
X
Blank contamination
Sample not chemically preserved properly
QC data reported outside of controls (i.e. QCS, LCS)
pH out of range (record pH):
Incorrect procedure used
Improper chemical
Residual chlorine present in sample
SOP intentionally modified with QA and Branch Head approval
Color interference
Invalid instrument calibration
Heavy emulsion formed during extraction
Elevated detection limits due to
Insufficient sample volume
Sample bottle broken in lab - no reportable results
Other (specify):
Comments: Zinc concentration for LRB is 29 µg/L for associated sample Value of LRB is NOT subtracted from sample value.
1n ,yakoc _ 10�
Corrective Action:
Samples were rejected by DWQ Lab. Authorized by: Date:
Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
Sample(s) on hold until:
x Sample reported with qualification. Data qualification code used: L.V
Other (explain):
Notification Required (check one)? YesFJ No ❑X
Person Contacted:
by:
Date:
Date: c�
Lead Chemist Review (initial):
❑O hBI�OTALS
CHEM SA(J SVOA
ranch Head Review (initial • s
QA/QC Review (initial
Logged into databa
1 se by (initial) r
�;
QATormsV.aboratory\SAR - -
L......._.:e._ 06112/03RWB

r
A
W
f
MX
FO CD
m C7
fTi 00
Cn
b n Lae!
O -_i c8?
T �
0
0
o
p
o
p
We
57
2
M
O
o
0
0
0
0
v
NO
r
3
m
c
o
0
3
3
E
s
c
0
S
O
x
O,
m
.p
1�
o
o
c"
u�
�
T
3
T
w
w
A
O
m
x
.p
-v
S
.II
S
=
o
m
u
0
0
0
00?
a
p
g
W.
N
C71
LJ
(71
N
—
W
W
t71
O
W
0
(31
OA
O`
Q
3
�
n
C
�w
3
3
to
3
to
3
tm
3
to
3=
Lo
3
\
Z
3
�
o
o
3
3
3
m
ti
C
o
o
\�
X
:4
Z
-i
z
(n
(n
(n
'o
S
2
'?1
P
C.
a.
+
+
p
°
i
n
4
C
a
0
n�p
O
IA
Z
O
in
N
O_
(0
N
n
N
N
IA
c%
2-
rn
rn
A
DW
C.,
v
A
n
Q
0
p
a`
z
N
0
C7
W
kO
%0
w
O
O
p
O
10
O
N
M
�
m
3
3
3
3
3
3
3
c
c
3
3
3
3
3
�
3
m
Z
o3:
cp
a
o
o
y
N
(n
Z
rt
to
m
H
m
N
c
W
3
0•
n
3
0
m
L
3
c°n
3
i'o
3
'c
0,
A
3
3
A
A^
3
rn
V
.p,
Q•
N
Q`
U1
J
W
(P7I
'p
P
C�77
LA
kmO
-P
�p
N
P
CP
N
UI
rn
O
0
%0
V
rr
�
C
e
10
lc
W 0
C
W
o
C
wp
C
io
C
10
C
Uo
C
LO
C
M
C
W
0
0
m�
v
n
s
X
.
m
=!
�
v
o
_m
On
y
3
0
0
art
s
O
p
°
n
3
to
o
to
N
n
n
(0
N
3
N
N
G
ro
p
uz
O
!
Q
oa
m
D 77�
T
A
A
No
o
vmi
N
�
n
O
�
h (n
)7.
o
, ,
-tea m
f
O
l
y �
a
o
�
3 �
W Q.
z
p (n I w p
o
n N
w
C1 C "� P w > W
3 v 3 { C '� a w
Q to!? m O cn
co c n w
� O
Z Qo p 0 O
° cn
(D O N O C A
n �
v O
Cl.
N �
0 3
C -h l0
�nX
Ln1 4 LJ.LJ
0
l0
� O
y Ll
A (n P r
3 y ^ O m 3 0°
p .a q m' 3
-. O Y -f l0 3
A
m N O
Q 0 a m X
O p z
� 3 A
v
i
c
v C 2
°•
' v c
m m { �*
a 3 s
u m p p
-3r zl
s
m { �
P a o
m 3
rt �
°
-+, 3 P P p v P r-
m P T (l m Q
A
CO
a
t�

--� -i C/) C/) C) C) C) C�
Zno�i Dc(DC U'= °OO
—oS1i�woo(�.-.cnm =-p
D=;6o(n° �ocoo
0 —CD n'CL C <(A " -I
Z3C-) = m ja�3. m
m
O o m m-n
C? FJT N ° o O CD
CD CD 0 w
n a. a)
0, 'D
CD '--•' s fD
e O
c
n n cr
'+
owom �E
• 00 CA N 4?
O Ul Ul O m O to
N O Ul
O 0 CD
CD
o
3 3 3 o 00 F
E 3 D 3 3°� 0C:)
cn Cc o cry uc aD cn cn (0 CD
CL
��T2TiC�C�C�C�07D0ZZ cD
C co t� (II O C O Q iv ,� C == G
W LI W co\V Q ° C• W w C 0 T `V
W CD C CD 3 3 C C— O CO Z O
�C/) -,o 333ac„�vm
cn W W O
cnO�Cn
sn Z Z
cn
cn
O
O w
cn
it CD
a
3 3 3 3 3 3 3 3 3 3 3 3
cn co cn cp cr.] cn c° cp cQ cp cn cn cn Cn csa a
a
C = (n O
00 o
�- D
.. Z
«CD
^r C/)^
/ ^►
CDaO
•� 3 n
CD
3 3 ° a 3:
r=•=
D =
t at at
It II =0
Z
Q'
O �
0
O
o�
9
R
on
6ODNMZ x
0 53 : C-
G�oNrZm
_ ^ TT
C
- Z —
`C
C) p
On
3 (D
O z
� O
O.
N
m
a
0 ^
Ulci
h0;,
g c 3 3 3 3
CD W CD
CD
0 N p� m co
CD
0 " ? = a
iD Q 7 Q. `Op M
cD (D
CD
(D N c
u, ° 3
P.w
CD -,
a 0
n cf) Ft, v
0 Iv Q _ CC (D
d n. O O CD O G
< O (D 3
n'
0 3 5-3
�
CD w
z: a D)
In
c a cD
(Dww i= CD j
CD �' O N
D NIA
N
AOi Ln
1
m
S
0 CD
CD ❑ ❑ c
O c
(D
C C d
ti o CD CD
w
D CD 3
Coco
N n
N
0 r- 0
(D Q. m
O (D
o w
= o
Z CD
aD) 0
3 0
(7
Q.
• 1
m3
\V
w
P7
0
O pCj
o CD
a cn
m �
0
0 0
C
0 a
:3 -,
(D
n
Iy.
H a
N
0
CD
goo a
CD
0 a
0co
X
O O
I. CD
m
N �y
a�V 0
oow
o
0 0ZS
�-
0
o'
o
CD r
z
w (D
CD
x
� >r
At �
mw
rt m
F'!
n
b
N
w c�
rt r C
8
o o
O D
C S �
CD
G �
C ^
1 J
O
Q• CO Cz
O N
wW ao (D
w�- 1-
'o H
CD w
a �
m
vktb
w � z
D Z
1' a � w
o m CD
a
O-zo
m:ou
m
Cl)cn
_0
'�
m w
w
o
Yt
1
<
�
o
.
(
y
T.
CD_
Q
_
o`
c
N
o
O
w
m
�
lI
I m
wCC
D
�
o
a
0
m z
X
w
3 �
n -�
�,
0
z
g
= O
cn
°' z
y
c
0 -1
0
m
m
w �
C7
z
O
A
r:
2 X'O.Z...
0Lnnm ,
4m�.n
rn 6:m
ro m�
o c.

z o :3 CD = Q m
�z
} O 3 "n -n
-n
(D Q a O 0
w
Ll o o M
_
mm 1
CD
.A
o
c 3
CD
a
A V1 A �
N °1 N N
A 3o p
. w
o CD
c o
0
c� cn 0 co cn cc cc cc cc = cn 0 C a
c
���=TC�nC)C�ODDQ�ZZ c�
C co c0 CD C C- Q w Iy7 C = COC
CzD
n
oom>o WD_
D Q c Cp
Bc
CCoc033COcOz
ll (D . C� O1wcmx cn
(D 60 cn
v zz
� I �
Z
O
C1
•_ a
a
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
0 cn cn cn cn cc cc cQ (a cn cn cn cc cQ a
cD
a
0 M�
n o o
-D
z
CD
Co w (n
?CD _
Qa O
J 3 P
cD
Er C7
3 3 ccn CL
cD o
n. CL
n
n u =r
oZ q t„1
v
V
0> NAZ5S
I
O E- cr
C(D
P- a N r— Z -<
rco
z3=cD m
CD cD
2• Z —
O
3
o z
Z O
a
w
o n O
w 2 cn w
.•� �F 1
N
0
3 3 3
TOK0cn,�C�
CD w cD co 0 m m"
_
a o
cD o
_ °
cn°
::r cD
w ° /a o Q• '0
-.
0 -0f�
w = n
j
w op m CD
w
V1
: o
= c <
Z
m
o
3
aa)
P—
w
CD
cD
L,
c
n
o
�
cn.
CD CD Q CD
0 iF < a
CD
;b
m
w w 3
=`
0 CD
° o. w
3
a N Cc:
m
w�
vco
Aco
CD o
CD
D
o
o m
CDCD
aCDi
o
0 m
�. o
D
CD
rn
o
O c
p
m� a
0-
3
a
ca Ca
cn
N
3
o
I.
�
3 '
n r- p
CD cr w
o (D
0 a
m
21 o m
o' � -°
o
m
w Z N
°
c
CD
0 3 o
a
0
CD c
°'
N
n
n
o
a
°
0
c
a
CD
CD
I
w
�
CD
r.
w
0
[v
:3
a
\
fA
O
y
w
°
Z
p
a
w
CD
:3
to
n.
d cD W
= 3 -=
q =
Z
a B 3
(D
a
m
CD
x
s✓
rn
w
N•
u o
m
m o
y.
m w
w o
w
o
co
a
-
@r
c
0
O
v
I
I I
m
m
w
a
CD (D
( OZ
D
m
m
nai• o p
o=
z
C D
o
O
o
O
Z
w Z_
D
C
a
O
=
m
C
CD
M
_ m
o
CD p
re,
n
A
m
--i
M'm
m.
.D
O
.0
Q
Z
0;
C
C
0
z
O
z
m
r
O
D
e
O
z
r
I N,: -. C�. 11
ZN

y DI
i ) -1'0 .Z l) l) L Jtv
Cf)
o
w -,
D
�0=� m o 0 0
o0
�
c�
.a ���
CD ocnm �3
r1
2
0 z
o
w
__
v o -n -n
O
d
rA'
O
(ND G n
CL aw
—
TI
rn
CD
s f0A
O
4
c
o^
a CD
O
y ^ w
m N
o
� �
w
C)
m (D
= m
C
0
Q(0 O(ncocc
C 0 0 n
nccto 3
(o
a
c
��T2-rtC�C�C�C�(z7D0-pZZ
9c
(n �cn o
c n_w w n
03C-)
-4..o -•_'
o
>oNw_ID a
w c w m C)O
• m LU w C�� CD
an-�c'3.00ZZ
�c
cn�N�
33 _.
((DD
C•3�C
o
=.. OO m
cn
CD
3
w
—
o�cn
w ZZ
w
�
I
'U
Z
O
A
O
w
C)
o
a
(nLrl
C)
(D
a
3 3 3 3 3 3 3 3 3 3 3
cn cn (n (n cn (n (Ez: cn (o (n
Eln (n (o (n (n cca
= = =
cD
a
00CDD
a
ODN t7Z Ix
n
O o
=i Q
_ D
-. 3
o NrZ
n
= w
Z
_
0
p-a G�
n o
•J 3 .�
9
I
CAD
-< S CD 0 _n
7 S S
i°an°
=
tt :tt
n
i n
n
Q
N
Z t:
O
o
oNQ11
d
I
O.r
©MH
' 3 3 9
(a (Q (0 (a
z
O
v
c�dmCD
p o w O m (D
w
CL
°' o 0 a D
NC
ti CD = 1 W �.
(D D 'D y (D W W p
= C < N C
CD
— CD c
CD
CD o
a
ri02'.F p3
0_ (C-D CD
(D o (D . G
< o 3
0 ai w —
0� aw a)
C (p C Cc:
O
N
m o
D = I
(D
CD
Cal
0 ?
❑Q��c
O c
m m
ch > CD
cu
(0 Co
a
� 3
y �
a y 3
m0) C)
w
Cr
cc
o W-
3 omo <
U_ o p1
Z N p C
0 CD
0 3 o m 0
m =N
0 n S
W m °
Ln a
c
(su
C)rt (oD
1 `D
4+ (D
(D a
Cl N y
Cl)
0
E
CD
w caCL
(n n.
o
-n
CD
w
N
Q.
-' O
00 m
O O
N N
c
owr
0zs.A
o CD r
� o R
h
CD p
w r
CD
1-3
ro m r;
Z (n n 0
o D C
0
CD m
ti n
0 f-
ol
co
c�
a
i
171
N•
r'-
N•
Z
—Z-0
0
-7 m
m
o
0 o
w
m
a
m w
w
o
w
0
p
n
o
(D
a
a�
C
0
1
O
I
I
m
I m
m
D
a
CD
3
3 O
Z
m
•�
?
�
0
g co
x
�
�.
0'
o. m
C
Z
D
m
� �
n �
:3
O
o
p
z
C
Z
c
a
? -1
p
>
CD
w m
m
CD 0
�n

` RESEA►.. � & ANAIyTICAI
LabO�ATORIES, INC.
ti
�y ti
..t+
g.
e % NG �371b�
Analytical/Process'Consultations
Volatile Orl anic Analysis from Selected Sampling Locations Identified as Huffman Monitoring Neils #2 & #3
(A Water T,4ch Labs, fne. Project, 06 November 2002)
Volatile Organic„
Ouantitation
EPA Method 621OD
Limit
Well
2 Well #3
Parameter
itp-61
IEUB
(PPB)
1,1-Dichloroeth .lie ... , ,
, ... , 0.5 ..
, , BQL ..
, BQL
2,2-Dichloropro lane , , ..
, , ... 0.5 , ,
, , SQL ,
, , BQL
Chloroform , . . , . . , .
, .. . 0.5 ...
, SQL ..
, BQL
1,1,1-TrichtorceThane ........
0.5 ..
, . SOL .
, . SQL
1,1-DichiorEprol:one .........
0.5 ....
BQ!. .
, , SOL
Carbon Tatrach' )ride ......
, . 0.5 . ,
, . BQL .
, , BQL
Sen2ene . . . . ...........
0,5 , ,
, . SOL ,
, . SOL
1,2•Dichioroeth, ne ..........
0,5 ..
, . SQL ,
.. SOL
Trichioroethena .....
, .... 0,5 ..
BQL
, BQL
1,2-Dichiorop(Q, One , ..
. , .. 0.5 .
BQL ,
. , BQL
Dibromomethan, ...........
0.5 . ,
, , BQL ...
SQL
Toluene .... .....
, ... 0.5 . ,
.. SQL .
, . SOL
1,1,2-Tr;chioroe hane , , ...
, . , 0.5 , ,
, , SOL
SOL
1,3•Dichiorop(olane , . , ,
. , , , 0.5 , ,
, . SOL ,
, , SOL
Tetrachloroothei a ... , ,
, . , .. 0,5 ...
, BQL ...
BQL
1,1,1,2•Te1r4uh5roethane
... , 0.5 ....
BQL ..
, BQL
1•,1,2,2•Tetrachl sroathane
, .. , 0,5 ..
, , BQL .
, , SOL
1,2,3•Trich)orop,opane ..
, .. , . 0.5- .
, , BQL .
, , BQL
Nexach;orobutad one .. ,
, , ... 0,6 . ,
, . BQL ..
, BQL
Bromobenzene . ....
. 0,5 ....
SOL ,
.. BQL
Ethytbenzene ... . . ... .
. . .. 0.6 ....
SQL ...
BQL
Styrene ........ .........
0,5 .
.. SOL ...
SQL
Brcmoform ... . , . ,
, ... 0,5 , ,
.. BQL
. BQL
p•Isopropyltoluena ......
. .. , 0,5 , ,
. , SOL ...
BQL
N-Sutylbenzene . .. , . ,
, , , , 0,5 ...
, BQL ,
. , BQL
Naphthalene .. ........
. . . 0.5 ....
SQL ...
SOL
M•Xylene .... ...........
0.5 ....
BQL ...
BQL
1,3,5-Trimethytb,nzene .
, .... 0,5 , .
, . SQL ...
BQL
1,2,4-Trimethyth nzene ..
, . , . 0,5 ..
, . BQL .
, . SOL
1,2,4-Trichiorobe lzene .......
0.5 . ,
.. SOL ,
, . SQL
1,2,3•Trichlorobe:,zene , ..
, , , , C.5 ..
, . SQL ...
SOL
Dilution Factor . ...... .. . . . . . ... 1 , , ... 1
Sample Numbor
Sample Date
Sample Time
Date Analyzed
Time Analyzed
453628 453629
1 1106/02 11106/02
OSCO 0840
111141C2 11114/02
1236 1259
Volatile Org,: nits (CONTINUED) Quantitation
EPA Method 6210D
Limit
Well x2
Weil >a5
Parameter
P?l
E-6
riPP3
Chlorolnenze,re . , ..... ..
0.5 ....
SOL , ..
SOL
2-Chlorotolu-.ne , . , ... , .. , ..
0.5 ....
BQL ...
BQL
4-Chlorotoluono ...... , . ,
. 0,5 , , ..
SOL , .
, BQL
Tert- Butyl be; .... , , ...
0.5 ....
SOL ...
BQL
Sec-Butyibenzene ...........
0.5 . , ,
. BQL ..
, SOL
1,4-Diehlorol-en4ene . . , , ...
0,5 . , ..
BQL
, SOL
1,2-0ichloron•enzene , , , .. , ,
. 0.5 , , ,
, BQL ...
BOL
P•Xylene . ........ . . .
. 0.5 , . ,
. SOL . ,
. BQL
0-Xylene . . . . . . .. ... .
. 0.5 , .
. SOL ...
BQL
-Propylbenzene . , . , .... , . ,
. 0.5 ....
SQL
, BQL
N•Propy!ber.:r one , , . , , ..
, 0.5 .. ,
, SOL . ,
. SOL
1,3-Dichlorotenzene , .......
, 0.5 , , ,
, BQL ...
SOL
Dibromochlor methane , . , .. ,
, 0.5 . , ,
, SOL , ,
, SOL
Dichlorodifluoromethane , , , , ..
QA , .
, 8OL , ,
, BQL
Chloromethare .... , , , ....
0.5 ....
BQL . ,
, SQL
Vinyl Chlorid,: .............
0.5 , ...
13QL ..
, SQl-
Sromomethe to ...... , . , ..
0,5 ....
SOL , .
, SOL
Chloroethane ,, , , , ,, , , , , ,,
0.6 , . ,
. BQL
, SQL
Uchlorofiuoromethane ... , ...
0.5 ....
SOL ...
BQL
1 A-Dichloroe' hens ...... , , ,
. 0.e . ...
BQL ...
6QL
Methylene Ch oride , .... , , ,
. 0.$ ....
BQL , ..
SOL
Trans •1,2-Dicnloroethena , ,
. 0.5 . , ..
BQL . ,
, SOL
Ci4-1,2•Dichloroathene .... , ..
0.5 , , ..
SOL ..
, SOL
Bromod;chloremethane . , . , , ,
. 0,5 ....
BQL ..
, SO
Dromochloron-ethane .. , , , ...
0.5 , ..
, BQL ...
BQL
Cis•1.3-Dichlo-opropone . , ....
0.5 ...
,'SOL ...
BOL
Trans•1,30chlaropropens , , ,
. 0.5 .. ,
._SOL ...
8QL
Methyl•Tert-S� tyl other (MTBE)
. 5.0 ....
SOL ...
BQL
Isopropyl ethc (1PE) ..... , ...
5.0 . , ,
. SOL ..
, BQL
Dilution Factor . . . ..... . ......
. .
. 1 .....
1
Sample Numb,:. r
453629
453629
Sample Date
11106/02 11/08i02
Sample Time
0800
C640
Date Analyzed
11/14/02 11!14102
Time Analyzeci
1236
1259
PC). lcx 473 • 106 Short Street • Kerner5viila, North Carolina 27234 • ;136•3SG.2641 • =ax 336.996-0326
BQL = Mow Q11tntitation Limits PPS Parts Per Bill.or,
pECEowE
JAN - 8 2003
GROUNDWATER SECTION
ASHEVILLE REGIONAL OFFICE
., v1120Tf CH'

Cf)
r7l
�
CD
\
■
}
0
.
\ 6
9 ±
\ }
k
)
q \0
) R
}
ƒ
\
(
.G�
\
:
ƒ
�\
G2i§q
o
ƒ\�
0
_ \<
ttl
§
0
)j
>&
2 .
/
.
0
;
.
19
❑
E
\
(
\ m�
/
2
,
0
&
/
/
/
❑
f
*
\
n
t2l
#
\
r)
®
[
\
.
�
�
}
o
#ƒ{[
&�Km,
.. ..�
.. .. .. ..
/�\))

/
m
7`
\
?
»
/
t » c
(
_
\ &
°
70 q
2 °
p
M \
(
§
®toto
®
.
.
7
-
0
&
m
.
oa
00 /
7
m
'
r
.
;
\
r
/ ƒ f
0
3
C' �Ln
j
m
ƒ
( / \ / }
ƒ �
-
(A.
\
-
® -
%
x
CX §
\
\
$
�2
a
m a
.
z
k
E
2 ° ` m r-
q
&
ƒ c./ /
m
R c
S.
ƒ
-
m
�!
z
2
..
•� �
k
$
�
Q
I
2
�
�
E
e
�
�
(
.
Im
�
a
;
L,
-n
}
\
!
z
p
$
m

Cn Cn 17/ _ 0/-)0
Q O O
Z W o m 0 cn N m o
cn O _ ^" _. a
u O O
00
a
cvUjz
coo 3 -t7-i1
N
N as Own
w
7
(D
Q w
°
cD
O
0
�m
m
0
c
�
c
a
m
H
m
�
y
n
o
n
m
m
CD
ry
3 3= 3 3 3 3 3 3 S 3 003
0
(O CO O (O (O (O (O c0 (O - c0 (0
cD
CL
��T.2'rtC�C�C�C�[T�DQ'oZZ
�
� (o CDC =r CL W W -L =- — —•
r
�
=-0
C7CAD- -0 CD (D
cv S1) Sv w C = =. _
n._ ,.._ n 3 p O z Z
3 cz
3
=r �
3�0cn�
m
r�
N
w ZZ
Yf
T�
V
Z
O
m
m
A
O
m
=
a
1
a
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
c0 (0 (0 (0 cn co (o cn c0 c0 cO (0 (0 (0 cO
n
a
QCD -v M
oD= az
�—D
r
�p NrZ-<
D Z
cn3.=a0i0 Umi
y 0
(n
(AD CD
0 Z
0w
CD
l O
,«
o O
•J 3 n
3 CD
m O
0 = Z
CD a C)
= O
a
c3D33
0 M. =r _
a 00. Dnr-
w
a
0-
(��
'IIJ II�� NI `fl Jib Y
CD
'D
I
c 3 3 3
O
y ` (S` (m (o
m w
m (D 0 m m
d O
y
D) m
0 7 0 n
o m m m
w 0
:3
w 0 0
cy_n' obi
=
o CD
cCD m
D)
CD
N m
?.
p
3
m
N=
CD
3
m
cr
I�
IJ
n
C-�
3
Ic>cn$••
v
•n
0.
_
w ra• m
0 CD 0
CD
O
0 w
0
m
�~
O -0
m —
= m
o.w
w
3
c
w
c c m
CD Cc
m
O_ IN
D
c�D
•'
w
1
w_
S-
CD
1
❑❑� 0
O c
m°C
w
0
C CD
co CD
N
to co fD
rn
N
N
CD 11) C)
w
0 m
2 w a m
0
0��_ o_m
Z pzi m O C
0 3 o a cmn
m (fl N
0 n =r
0 0
c
0 a
cn m
cn O w m
0' c�
\= o
O
o a_
\ to N
O N
N O
m
w
wQ00 m
a
Om
Xw
t-h �
O�
!'i m
�a
C) CD
0 v
O -�
Ln -1
O
0 n
w �
0 y
0
CD
z
w
3
CD
o � n
0
(D C
O -0
0
Q
(D
CD
(n :tt
0
0-
(D
cn Do
w
3
m
3a I
3
-n -o
n. - 0,
Z
w
a 3
m m m
Vi a
i CD
rlz
6.,
CD
z
Z -0
m
0 m
m
m0
O
n
o
CD w
m
z
w
.�
•�
o
ca
o
w
(D
a
—
IQ
Q
c
0
O
JI
D
m
a
C
m
Z
X
s
w
m
C
w
o
Z
G)
D
n =I
c
0
o
w
O
z
O
c
w
'�
O
D
4
m
fO
CD
w
M
O

OO
Z-0a)=3noto0n—cnm —._0
—0 a)
6o� � M.
E D
CD
o c O O
m
Z"<
S n
m
>
oD3
>QK
T -m
�m
Q
0
v o m
Icn
0
�,'
a s
N a n
Cl)
n)
0
-
0
a0
a
CD
Q
�m
C4
o
e
n
o
n
•Ul
C
a
(D
�_
Ln
O
-'
0N3
O
j.
N
� m
b
n
N N
O
O
m
O y
• CD
O CD
3 3
5'3 3
(n O (0 U]
3 3 3 3 a 3 003
(c co (D {Q
O _.=:zmt
c
-OZZ
�cn �cncDc==rCLvcu—
�K0 ::7
c�OM-L>o "' �'
CD�svwCCD�3��,s�o=.�-o.-.
003
a— 3a
3�
X
Dc0
D 3•("p0
C Z3 O N 'G
nC.3`<
033
3..�.,m''
--� n, cn
0 3
w
°'
m ZZ
cu
I
2
0
A
O
•
O
N
41
o
U
Ln
-"
a
33333333333333�0
cn cn (n (o to a:) (n (n (o (n cc (n (n a
(n (n
a
<m
O�
O to
cnpDN-oZ
IDc
�.D
a=D
o3ncr
s
P-�3NrZ-<
CD
CO
�n
n)MC�
o cn
(°o
L). Z
(D
=
n
I
0 o
Cl. 'n
•�
3
I
0
�5 n
-o 5
°CD
Z
0
3 m cn a�
c
a
O
c3o
0 0 0
I NO
0
0
o~
9
mh
�T•333

- --i Cl) U) � O n -i ce C�
cn O
Z E C CD (D _' — = m O O O
o
CD cn
06�
C,)>= �m-'c�:��0a
n n cD
a
Z3o
=
=a?�3
>_>
a
Boa ��
. n.
iU
Q
�, a
0
N Cl) c O�
N
m
=
CD a r. n
�
0
CD
0
-�
Sv ,a
N
o
`
3
r
a
n
n
p
•
O
In
a
m
00�
n
N
N
N
O
cD
�O
O
Ul
00
Ul
Cl
A
C
� �
O
33=333333S3 003
can O cn cn zz.cn cn cn cn —•cn
CD
a
C
a
��T.2TC�C�C�C")07DQ�ZZ
�
:3 cn i cQ CD C a. CO su ' �• — —
o �O �_.
cD (D
o
a
W CD0 W¢ W C=
-��ann_o=.3ooZZ
x
_
*3c3•
CD _0a0Q
cnm3
03
3�
-'M
CD
mCnZZ
cn
z
O
a
o
m
n
O
CL
o
cn
o
o,
933333333333333
cc CO cn cn cn cn cn an cn cn cn cc cn ca cn
o•
co
CL
O.o co
C7 00 +�
D
.. z
_D
CD
o m fn
as
•� 3 n
c°
933c
CD na�
m m
c2D;
0 0
�D _
a CL
—
o_01,
Al
v
�
0
00-9 'UZIx
DCCLo3 a I•
_�CD
>v37N
CD CD
`-' z -
n o I
o cp
3 CD
o z
O
a
m
a
-' o o O
7
Oo� Ul0
o N
4 p
0
Q q 3 3 3 3
o Gm a
o 0..
c
co
0
0
z
I
r
m
D
v
m
X
0
z
r

RESEARCh1 & ANA1yTICAL •° °,.
LABORATORIES, INC.
w iy NC7i3T1.
r
Analytical/Process Consultations a• QRECIo�`�
ED AN���e•�.
Volatile Organic Analysis from Selected Sampling Locations Identified as
Huffman Monitoring Wells #2 & #3 (A Water Tech Labs, Inc. Project, 07 November 2000)
Volatile Organics Quant. Volatile Organics (CONTINUED)
EPA Method 6210D Limit MW #2 i�IW #3 EPA Method G210D Quant.
Parameter PPB Limit MW #2 MW #3
�� PPB �� Parameter PPB) (PPB) (PPB
I,I-Dichloroethane ..... Q
0.5 .... B L ... BQL Chlorobenzene ..... ,
2,2-Dichloropropane .... 0.5 Q
0.5 .. , . BQL .... BQL
... BQL ... BQL 2-Chlorotoluene .... ,
Chloroform ..:.::.... ........ 0.5 .... Q
BQL B L
0.5 , . , ,BQL ... BQL 4-Chlorotoluene ..... .
I,1,1-Trichloroethane . 0.5 . 05 BQL • BQL
• • ... BQL .. ,BQL Tert-Buty!benzene .. , .. , , 1,1-Dichloropropene .... 0.5 .... 0.5 .... BQL .... BQL
BQL ... BQL Sec -Butyl benzene ..... .
Carbon Tetrachloride ... 0.$ • • • • • . • 0.5 .Q
Q BQL .... BQL
• • ... BQL ... BQL i,4-Dichlorobenzene ...... , .
Benzene Q ... 0.5 .... BQL .... BQL
'S ..... BQL ... BQL 1,2-Dichlorobenzene ........
1,2-Dichloroethane Q 0.5 .... BQL .`.. BQL
0.5 ..... BQL ... BQL P-Xylene ......... .
Trichloroethene ....... 0.5 .... B Q
BQL .... BQL
0.5 .... BQL ... BQL O-Xylene ..... .
1,2-Dichloropropane 0.5 ...... BQL .... BQL
Q 0.5 ....
... BQL ... BQL I-Propylbenzene . . , . ,
Uibromornethane ... , , • • • • • • • • 0.5 . , , , Q Q
Q B L ;... B L
0.5 ..... B L ... $QL N-Propylbenzene .... ,
Toluene ............ 0.5 ..... 0.5 .... BQL . . BQL
• . , ,BQL ... BQL 1,3-Dichlorobenzene ....
1,1,2-Trichloroethane • . • • • . 0.5 Q Q
Q BQL .... BQL
0.5 ..... BQL .. ,BQL Dibromoc!,loromethane . , . , , , , , ,
1,3-Dichloropropane 0.5 BQL 0.5 .... BQL .... BQL
' ' ' ' ' Q • • •BQI- Dichlorod!fluoromethane ... , , ,
Tetrachloroethene ...... Q • • 0.5 • ... BQL .... BQL
0.5 ..... BQL ...BQI_ Chloromcthane ..... .
1,1,1,2-Tetiachloroethane . 0.5 ..... ..... 0.5 .... BQL • • • • BQL
1 I > > BQL ... BQL Vinyl Cl-.I-,ride .............. • 0.5 .... Q Q
Tetrachloroethane . 0.5 ..... BQL ... BQL. BQL • • • BQL
Bmmomcthane ............... 0.5 ... • Q
1,2,3-'Frichloropropane .. 0.5 BQL BQL • RQL
BQL Chlorocthane O.S . BQL BQL
Hexachlotobutadiene 0.5 Q � ' ' ' ' ' ' '
' ' ' B L • . • BQi- TrichIorofluoromethane ......... Bromobenzene ...:.. Q 0.5 .... BQL .... BQL
. 0.5 ..... BQL ... BQI. 1,1-Dichloroethene ....
Ethylbenzene ....... 0.5 BQL BQL
.. 0:5 .... BQL , . ,BQL Methylene Chloride
Styrene .. .. Q Q
.... 0.5 ... 0.5 BQL .... BQL
BQL ... BQL Trans- l,2-T)ichloroethene . . . ,
Bromoform 0.5 • . BQL .... BQL
,. ...;. 0.5 ,.... BQL ... B L �_,� r '
Q Cis -I,_ f rloroethene ......... Q
p-Isopropyltoluene ..... 0.5 Q 0.5 .... BQL .. BQL
.. • .. BQL ...BQL Broinodir!�lorornethane ....... .
N-Butylbenzene ....... 0.5 O.S BQL . BQL
...: BQL ...BQL Bromoch! �-methane .... .
Naphthalene .. , 0.5 BQL .... 0.5 BQL . BQL
..... . Q ... RQL Cis•1,3-f� lrloropropcnc 0.5
N Xylene ........... 0.5 ... B( I. .... BQ1. BQL
1 BQi- Tana-I,'-Oichloropropcnc ... 0.5 BQL .... 13QL
1,3 5-'frimcthylbcnzcne • . 0.5 Q
B [. BQL h1cthyl-I'C t-Butyl ether (MTBE) . 5.0 . B L .
I? t--frimethylbenzene .. 0.5 ..... Q Q ... BQL
B L ... BQL Isopropyl c1her (IPE .... .
1,2,4-Trichlorobenzene .. 0.5 . , . BQL ...) 5.0 BQL ...: BQL
BQL
1,2,3-Trichlorobenzene 0.5 ..... BQL . , . BQL
Dilution I",ctor ................ .....
Dilution Factor I ....
Sample Number' Sample ::r 4 436185 436186
436185 436186 Sample 1
Sample Date 11/07/01 11/07/01 6�a 11/07/01 11/07/01
Sample Time Sample "1 . 1 0940 1025
0940 1025 Date An . z Date Analyzed 11/20/01 11/:!0/01 Time An: r d 1 ?M' 11/20/01 11/2oro1
Time Analyzed
1419 1451 cr, !rand,. tF, Seraian 1419 1451
Asb{ , ,,,, -,- ,,t !lEttrO
BQL _ Below Quantitation Limits
PPB Parts Per Billion
PO. Box 473 • 106 Short Street Kernersville. North Carolina 27284 336-996-2841 Fax [phone] s\62wowioTecrt621

C/) C '� -. .= 0 -O, GC �,
Z (01) C=D —lz 9 1 (o') 00 :1
m
CO) > Eii o ch 0-6
0 CD a- =r
CD CD C<D
3 a ic
0 0 :3 03 :3
:3 CX. 0 C/) zo m
CL 0 ol -n -n
c a 9 --1 -n
0 cn N O(D
CID
0
CD
m w
CL
C) co
C) 0
C: 0
335-K 33933353 003o
a:) 0 (a (D to (m (a (o =(OcD
cn cn z-�
3 10
co M c =r a m In @
3 C) 0 M -00 CD
ca In In CD 0 0 -1 m m ca C =r —
CO " =3 -0 C: a — " 3 o 2 Z
0 -0 3 3 Q- F-- s' 0
CD - - — C: cn 200
--j a -0 CA3 to
03 3 - —
L C: -j� M
o
0 cn U)
2L Z Z
LU
:cl
O
o
A
o C)
CD
3 3 3 D 3 3 3 3 3 3 3 3 3 3 3
<m- o
> N Z
0 CD M
0-0 3 m cr
0.0 (Do
0 0 6j CD E3 I I
> i.- " o z
z t::; -C � 2.
E3 'D rl)
0 CD CD
(1) 9. z
0 03 ..
=r = —
(D r-L G)
0
P 3
-0 :3
0 z
CD o 0
3 3 3 ch 0. a
0 0 0 > 0.
0- a Cl 1--, — A
4t 4t 0
0 C)
00 :3 - CD
0 Ln
z CD
L
0 cr rl
3 333
to
C:) z::%
co
0
cD 0
,U

M.
W
y
a
a
O
X
as
o
C
x
k
o
N
IN
e
-
a
k
m
w>
T
x
o
0
n
n
n
n
m
w
m
o,
w
_
a
a,
n
o
o
O
O
O
o
s
o=
a
a
o
0o
a
a
6
In
ly
�
�
rn
a
a
a
3
�_
a
3
z
Ol
a
g
9
rl
r=
r
—
r
a
L
r=
r
C
OA.
-✓
mr OO
®
OZ
m
nH
H
zH
O ••�
OH
O
v.
Cl)
o
c
n
O
O t Z H Z o 0 o O c c a x S
a:
a 3 w a
_. •• n c h
p N Z w .� O n
� C O ..
U
n
a
a
3
a
,
ur,
z
z D
r
�
n
a
G
�
i�
r
°a�
.�
b
�_—
�� a• a ��� a a a a rn a U
rn
vUi v O O
17
W
v 0)
< W
C
aeo\ aeo\ aea\ aeon vo 3 0. a aeo ace aco a w o w acv
r r r r r r r r r r r r r r r
p
ro
ro
o
M
C
Y
z
O
O
kv W `®..
H
y
d
w
x
l
a
X
O
c,
a.
L°
c,
a•
..
�
y
O
jCSJ
P
O
m
IL
pro
O
n
M
rf
A=

Zm
N
w`
J
O
o
n
n
3
•�
C
'�
C
A
In
a
Q
C1
�.
_
O
O
O
C?
N
c
3
o
c
c
c
w
c
n_
Q`
o
n
n
3
F
Q
Q
o
a
a
v
a
y°
T
A
X
N.
_
S
N
_•I.
-nQ
O
O
O
coA
G
-o.
n
N
Lit
U7
m
N
°
R.
A
A
d
(
W
W
UI
O
W
Qua,
3
r'l
cIQ
3
3
3
3
3
3
c
-3
33
101.1-01
ICIZ
3
-
—
'
m
D
O
y
m
D
r
A.
yh
�•
N N
U1
(A
D
V
3
a
a
.
o
r
O (A
o
CL mr
w
O
v
n
_ Off. W
3
W
W
CL
-r -.70
0
0
p
O
A
7p
I oz
m e AO S S
Ul °D ° Lin= \ a
X
X
X
Q
M�
X
-1
Q71Z
G
z
N
_
po
N
z
O•
'.
A
A
N
P
m
N
o
N.
UI
a
0
too
ti..
P
z..�
m
V
UI
�p
O
O
V
O
O
O
pp
"1
Q
N
is
m
�0
3
3
3
c
3
3
3
3
o
3
1C
X
i
X
x
xx
Z
o:
c
n
c
o
9
a
D
L14
(AZ
{
o
�3
�o
is
T
o
0
02
N
D
t0
.N@°
$
$�
o
e
3
O
3
3^
c
3
tPi(3
P
3
umi
3
c
rn
UI
3
3
3
3
2.
3
P
V
P
A
A
P
UI
umi
m
A
C'
3
A
P
V
P
W
.p
Cy,A
P
0,U
A
P
U
U
P
Ul
A
P
UI
P
OU
P
P
u
O
N
cm
N
UI
co
w
P
P
Q
Q
V
Ul
A
to
to3�
t°
3
3
c
(o
c
to
c
(°
c
�c
c
(n
3
c
c
c
c
_
_
i°
(c
is
W
--------------------
------------------
2
2
c
N
a
z
0
0
=3
W
n'n
to
U3
v
o
�
_
°
O
m
o
O
o`
o
0
^
s
to
to
0
m
m
m
C
m
3
m
y
N
O
^
N
F
Q
(A
m
A
co
o
a
F
N
m
1n
W
P
N
O
..
o
0
3
O
N
3
On
ci
1
`%
CEFTX
N
O
A
O
m
m ;a
O p
3
n
o
C, c
3
Z
m
o.
m X -
O
c
O
O N
d °
m
CL
N
Ll
Li
_+
^
�.
c
c3o
m
n
CO
i
V 7
—
N
C
S n ti Q
m m
m
T
R C
D
a
«
m
o'
Z
c
m
p
=
O
m
m
4
a
a
A
_
C A
z
m
m
�
cn
m
O
N
T
O
N
O
0
3
Z
W
4Cf
0
'
m

NC DENR/DWQ Chemistry Laboratory
i Sample Anomaly Report (SARR)
'Lab Number: Sample
P Type:
� Priority: C
t x Sampled: (' d1� lb1
Date of Analysis: —
Affected Parameters:
Analytical Area (check one):
❑ WCH
Cr'METALS
❑ NUT ® MICRO
Cl VOA ❑ SVOA
❑ PEST
The following anomalies occurred (check all that apply):
❑ Samples
❑ " Improper container used
❑ Quality Control
❑ Data flag may be needed.
❑ VOA vials with headspace
❑ No trip blank. included w/ VOA samples
❑ Sulfide samples with headspace
❑ Instrument failure - no reportable results
❑ Samples not received, but listed on freldsheet
Q Analyst error — no reportable results
❑ Samples received, but not listed on fieldsheet
p Surrogates
❑ Mislabeled as to tests, preservatives, etc.
❑ None added
❑ Holding time expired
0 Prior to receipt in lab
❑ Recovery outside acceptance limits
❑ After receipt in lab
❑ Spike recovery
❑ None added
❑ Insufficient quantity for analysis
❑ Recovery outside acceptance limits
❑ iSarnple exhibits gross non -homogeneity
❑ Internal standards
C] Sample not chemically preserved properly
Blank contamination
❑ pH out of range (record pH):
❑ QC data reported outside of controls
13 Improper chemical
- ❑ Incorrect procedure used
❑ Residual chlorine present in sample
❑ SOP intentionally modified with QA and Branch Head
❑ Color interference
approval
El Heavy emulsion formed during extraction
❑ Invalid instrument calibration
❑ Elevated detection limits due to:
❑ Sample matrix — does not have high analyte content
❑ Insufficient sample volume
❑ Other (specify):
Comments:
c�na\4ai * L-� 6 3 v c) C',�-X 's�/

Z;r0-n= rC)—�a pz
,a;CDD=CDcn`'6=rO=via 00
cn o �j 0 �'�� 0 a 0 0�
Zen _ ?am m.... m
Q O mom -nT
0 UTN QI cn
O �.
(D a CD
0 � O � O �
_z
m
0
_ 1
C
c
G n
Ln N ce
3 o (a
C)
c
3333333�� oo��
co cn 0 cn co cn cn cn cn — cQ C c CD
C
CL
0
-n 0 c') 0 0 >0-0ZZ
0cn cn m c �aa� w 0'- _ o
C�Q >0 a' a
w W !v CD 0 O C S11 N N c a 0 (D
w CD CD � c' � 5* cj) 0 x
ccDC�`� o =..ca—m
m 3 o cn cn
cn
m Zz
cn
c I
.Z
0
0
o n.
a
3 3 3 3 3 3 3 3 3 � 3 3 3 3 0
co co cc co to co co co co cn co co co co cn a
co
CA.
< m in 0
0 CD
Z7
C7 O coi
=D
D� Z
CD
c x a
n
3 3 3 con a K
o I cn
T o o 2
CL CA. 0 0
na
jd Cr'?
Z�
O Q'
C
I ,a
0
o�
)ODNaZ
O p• —•
3 ,
0 N r- Z
CD � m
00 0 —
� cD
O
c
m
o.
0 JA
o•
�j I
m o
a�
00 1 1 1 1
c3333
�• � co co co
Ix
m
cn
Z
0
-nG)K�
0
y
C ? o p
0 ° n." CD
O
ty w
O F
m O
ZO)
�
M
fD
N CDO.
CD
--
z
�TT
l-
CD
W V
w.
�\
F
a
1
0
3
n co
F
0 (CD
_ << -Oi
CD
(SOD
O57
0 0' m
G
m m 3
0 D
fl w a)
C c0
N
G C f3D
� (D
1
m
cc
C
0
o_
v
a
m
m
m
`D
0F]c
CD
c
�
= = d
s
CD CD co
y
>
d
ca aw
fn 3
3 a
N
o m o
o D C
0
0
(D
N :rt
O
CD
v)
m
•0
aI
m z
7M CDt0
D aZi Z
to 3 3
D m m (D
`J y o
J CD
J 1
ip
y En I-f�
)o W
rn �
(D
tw En.
� N
0 r p
o N
p 0 m
3 0 o
5,42 -0 O d
T7
m C)
n' -{
Z aZi o 0
o
N
030 aconcc
O
n
o
o cD
n Q
B
w
a
O
= E
w" 0 a
c
uNi
rt D
(D -•
w
=
co
m
cn
' o�
II
m
I >
o a
N cn
r
�
D
� _i
o
a
CD
CD o Z
ij
m
m
g
_a. m
-0m
p
'o
w'
o
>
c" m
> Z
77
C D
a
n
m
3
0
= 0
o
z
m z
o
N(9133S
CD
.N31
QNn
ate! a
rn
0
w
110
rD- o.p •�
mCDccn'
�csz
z(D>-n
m0-
" �.A
m m m
ro �
o �n
c.
to O A I

CD
16
c`n
co
Zw CD m CD CD o Ch m a2.
o � o (n o_ ;.n� 0 0 0 0
co
3o•m—moCD mmm 33
Z3 n 0) .o Cr....
.a 0 M_.m
>y0 cn (�D N
.+ N CD0 0 O0m
0 �O� �N �
CDCA
?
—m
S O
0
n —+ OCS1 NC, N3
Ln OC N:D
l0 O CL m
w cn m to
v �
m
a
33�333333=3 003 0.
co cQ o ca co to to to (0 —•cn 3 3 as CD
;== =0� Q.
c
���2"nC�C)C�C7Q]Dp't7ZZ
o(0 (n CDC: maw 0 —1? m
S'S0 0 C-)3 nC)ca—'-0-0 CD O
Ca (� �• n �C3 C2 n �• �• O O� Z Z
O CD C (0D ' • �• � 3 ' '6 � 0NO -G
(D C 3 O 3 3 M --1 ~ 0 CA
CD 3 rn N N
tv Z Z
a) I
z
0
o O p m
o cn cn
a
333333333BC2
cocnCOcncncncn(0cn� a
a
cn
ODZ
Oo-0 M
nn
Q3o�o
�>
CD3 -t
^oNZ
Z
�.CD
0X-WDCD
m w 0
CD
Q. z CD
nCD
O O
•J n
3
3 3 3 CD cL
CL
�0 U)
a
0 0 x D
I
CL
a n CL =
3t * 4t — m . C7
,�
-� C) n CD
II It II .. 0
• 7 O
_a A . p
N Z �,
O
to : cn -'
o I C',
O
c3333
�-
C5
2. cn cn ct�

4.
RESEARCh & ANA1 TI A ���
Y C RECEIWEDIOENR3°
LABORATORIES, INC. DWO G�ROUNDI'WER Ste 10V* NC#37701
i,
..;. l
- Analytical/Process Consultations 00 OEC 20 AM 11: �, 9 ..,,,,•,•.. � ,�
��ED *0 AN��
Volatile Organic Analysis from Selected Sampling Locations Identified as Huffman Monitoring Wells #2 & #3
(A Water Tech Labs, Inc. Project, 9 November 2000)
Volatile Organics
Quantitation
EPA Method 6210D
Limit
Well
#2
Well #3
Parameter
PPB
PPB
(PPB)
1,1-Dichloroethane ..........
0,5 ....
BQL
...
BQL
2,2-Dichloropropane .........
0.5 ....
BQL
...
BQL
Chloroform ...............
0.5 ....
BQL
...
BQL
1,1,1-Trichloroethane ........
0.5 ....
BQL
...
BQL
1, 1 -Dichloropropene .. ... .
0.5 ....
BQL
...
BQL
Carbon Tetrachloride ........
0.5 ....
BQL
...
BQL
Benzene .................
0.5 ....
BQL
...
BQL
1,2-Dichloroethane ..........
0.5 ....
BQL
...
BQL
Trichloroethene ...........
0.5 ....
BQL
,
BQL
1,2-Dichloropropane .........
0.5 ....
BQL
...
BQL
Dibromomethane .........
0.5 ....
BQL
...
BQL
Toluene .................
0.5 ....
BQL
...
BQL
1,1,2-Trichloroethane ........
0.5 ....
BQL
...
BQL
1,3-Dichloropropane ..........
0.5 ....
BQL
...
BQL
Tetrachloroethene .......
0.5 ....
BQL
.
BQL
1,1,1,2-Tetrachloroethane ....
0.5 ....
BQL
...
BQL
1,1,2,2-Tetrachloroethane ....
0.5 ....
BQL
...
BQL
1,2,3-Trichloropropane .......
0.5 ....
BQL
...
BQL
Hexachlorobutadiene ........
0.5 ....
BQL
...
BQL
Bromobenzene .............
0.5 ....
BQL
...
BQL
Ethylbenzene ..............
0.5 ....
BQL
...
BQL
Styrene ..................
0.5 ....
BQL
...
BQL
Bromoform ...............
0.5 ....
BQL
...
BQL
p-Isopropyltoluene ..........
0.5 ....
BQL
...
BQL
N-Butylbenzene ............
0.5 ....
BQL
...
BQL
Naphthalene ..... . ........
0.5 ....
BQL
...
BQL
M-Xylene ................
0.5 ....
BQL
...
BQL
1,3,5-Trim ethylbenzene ......
0.5 ....
BQL
...
BQL
1,2,4-Trimethylbenzene ......
0.5 ....
BQL
...
BQL
1,2,4-Trichlorobenzene .......
0.5 ....
BQL
...
BQL
1,2,3-Trichlorobenzene .......
0.5 ....
BQL
...
BQL
Dilution Factor .................... 1 ..... 1
Volatile Organics (CONTINUED)
Quantitation
EPA Method 621OD
Limit
Well
#2
Well #3
Parameter
PPB
PPB
(PPB)
Chlorobenzene .............
0.5 ....
BQL
...
BQL
2-Chlorotoluene ............
0.5 ....
BQL
...
BQL
4-Chlorotoluene ............
0.5 ....
BQL
...
BQL
Tert- Butyl benzene ..........
0.5 ....
BQL
...
BQL
Sec-Butyibenzene ...........
0.5 ....
BQL
...
BQL
1,4-Dichlorobenzene .........
0.5 ....
BQL
...
BQL
1,2-Dichlorobenzene .........
0.5 ....
BQL
...
BQL
P-Xylene .................
0.5 ....
BQL
.
BQL
0-Xylene . . ............
0.5 ....
BQL
...
BQL
I-Propylbenzene ............
0.5 ....
BQL
...
BQL
N-Propylbenzene ...........
0.5 ....
BQL
...
BQL
1,3-Dichlorobenzene .........
0.5 .....
BQL
...
BQL
Dibromochloromethane .......
0.5 ....
BQL
...
BQL
Dichlorodifluoromethane ......
0.5 ....
BQL
...
BQL
Chloromethane ............
0.5 ....
BQL
...
BQL
Vinyl Chloride ...........
0.5 ....
BQL
...
BQL
Bromomethane ............
0.5 ....
BQL
...
BQL
Chloroethane ..............
0.5 ....
BQL
...
BQL
Trichio..ofiuorcmethar.e .......
0.6 ....
BQL
...
BQL
1,1-Dichloroethene ..........
0.5 ....
BQL
...
BQL
Methylene Chloride .........
0.5 ....
BQL
...
BQL
Trans- l,2-Dichloroethene .....
0.5 ....
BQL
...
BQL
Cis-1,2-Dichloroethene .......
0.5 ....
BQL
...
BQL
Bromodichioromethane .......
0.5 ....
BQL
...
BQL
Bromochloromethane ........
0.5 ....
BQL
...
BQL
Cis- 1,3-Dichloropropene ......
0.5 ....
BQL
...
BQL
Trans- l,3-Dichloropropene ....
0.5 ....
BQL
...
BQL
Methyl-Tert-Butyl ether (MTBE) .
5.0 ....
BQL
...
BQL
Isopropyl ether (IPE) .........
5.0 ....
BQL
...
BQL
Dilution Factor .................... 1 ..... 1
Sample Number
406902 406903
Sample Number
406902 406903
aample Date
11/09/00 11/09/00
Sample Date
11/09/00 11/09/00
Sample Time
0815 0900
Sample Time
0815 0900
Date Analyzed
11/15/00 11/15/00
Date Analyzed
11/15/00 11/15100
Time Analyzed
1119 1201
Time Analyzed
1119 1201
BQL = Below Quantitation Limits PPB = Parts Per Billion
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone] Fn"�h2'TECH s

� - co
Z r"• CD , c=D to N 0 p= co m O O p fl. o -Cp �w t9 cfl
CDO•c2�SOa O�v y CD CD o''�"�
30 no mmm 33 ty a0 O o.� ' z
Zan �t1.3o y��m���' a�°•�°'
p t2 W (/) z ;r; m o c� CD = o~ m m m
^' Cn o n 3 m • •CD co
>y D 0 3 3 — c z CA D
CD -« cD Cp CD CD 1'lisL
o CD o
C N CD
C7'�t�D�
a ^►
Ln In cr '. CD
O O NO N O (DCL
tD O „zr,c
O A O O y< -gym �
Ai 3 (D �J
cn c oj� n.y 3;.
$CD
c oo CD ��••�FrC � n�Z
33�333333a3 003
to ca o co co to cc cn ca =q co `°
==o 3 Q. o rt s Q
C m � = r
3• v Z -i (� �
O N O O $3 g
�'S�=-nc�c�c�c�map-azZ o p h x
O to i to CD C S t2 O ? ._« r.: t0 N.�
p i SO ram^.' C. m n 17 O
Dorn o �� �� b K
CO CD 0 n tD
aca�3-30-��3o�ZZ' oc o.
ca c� m 3.c �'cpp a n
sn CD3O-0yW v-t c cD �zx
�`a3`� 033 3� c a v,�f
CA c r. —1 m� o cD CD m
CD 3 1� CD N y' -i h s°c
0
Z d
iii tD CL
3
cn tC co a "
cn
Z xs>-k
O tD �"L xs f3
.: o m
0 0 CL m 1, z z -0
�o� 'morn
O fl. 33
ani O aNi m m o •
33333333333333-3 In ��� o °C--' o0 0 -n �.
to ca cc ca to co to co co tQ to cn ca co to a z w CD O � = � w o � -
CD 3 — 0 -n. � cD
C. cD o ? `D —
a
'�� o =
Ln c br
O' ct cD a z C
O O
.� 0
o
0 A
w y . ► .....tr A
y N �
C] y N r 70 31 °gym m
N L O
O O L3 Z X Qk1 4�
• �.
CD
co ia C13 -0
C• c °^ rn oa az� u
07
C.
3 O Z
�-h cD Cl)
nmGS.S i`l 4 !;
a,y mk;
w
0 0
p co -a ?]
n�� D
n Z_
d 0
C.) Cn
.CD CL "
Q�
CD 0
B39CnC.�
f-�� r
Z v.
O t
I �
0
^a
C5
coo >N'nZ
oEF3:31
a CD 3 t
N� O Nrz
Z 2.cai��
m sv cD
A ca
0 o
v m
o a
c
CL
� n
-� Q- O
_, o 0
o Ln
m
Ln
c3333
Ca cc
to
� D d
a
to
c
03
0
0
z
rim
.D
D
m
O
z

o
�
OC,
x
Z
°
3
+._.
�',
o
�•
o;.
?
o
c;
o,
�i
O
O
O
0
Otz
0
/ m r
Q
mp x
�
3
�
n
•e
_
'2
y
�
�
�
�
S.
�
a
\,:,� rn z.
m. Q-
'rn
c
x
n
�
c
r
r 7
►c
v� o
� C
1.
l
�
3
3:
o•
x
O
�.0 c O �.
H
o
z
z
�_
y
to
W
p
n
b
a
N
o
^
o
> n O
C
0
3
3
3
3
0
3
B
3
3
3
3
c
c:3'33
3�
m p m
C
m
3• �
t�
Co
w CM0
x
x
x
x
m.y
y_
a
�
�
A
G"
A
fD
�
w
w
°
•O
°
c
°
c �
�
3
J
A
b
O
C•
A.
�
V�.
�
N
A
�,
�`
�
U
U
O
A
�
0
0
k
w
�
o•
A
e
o
�.
�'
o
_
aq
m
�
�
O
m
O
�
m
a
y
z
a
x
r
A
x �

f) � fn'
�'
o C
COa CD �-o% o
o0�w
�0000w20 00 a�o
Omam > Zy
CO
o
3
o
0
w to D o �
W
' 3C �,
m3Zo °� r
o�No
N
D
C,
z O CD
tit
w
�" /CD
_ { M O CCD :X)
A^�
a
O
Cn 0 r
� or m
O� oo��
Q a 03 (D (D 0 ` r
O _ v
z 3
0
0
3
3
3 O �,
CD O p 03
-n
Ga
O O
(n
w
u=i
o
t
p O _
vi
CD
u'
CD
o
o
N O
Cn
D
n
O
ti
Q.
(p O
C)
"o
-I�
y 3 ❑0ED
Qo0E
W 3M�ooO� 0co
CD
0- N(D O m
r
o
m "a CD
o a .�
N
��o�
y (Q -�
j O m
r K - o 0)
(nm
o �-
yoy�� a 0,
D
a � 0 ❑P-0
w- � 3 = �
�co O
=
=
n CD
CL
`<(93
0.
. .
�" o ,C
w+y,,, o
`1,
Q)
0
0
D
D
D (-h
a
w
w
m
T x
r w
o
w
D
�
y T
• C
C
O•
C•
�. O
A O
i 3
A
rn
3
C
�� cnm
T
�o
�'�N��
�=h 0
�,
j co
�,
N
�,
V
3 m R� CD 3
!!�• z
OmC O 3
3 Q -.(D m O
O �m
�3. y3�� �0��C� n�
CL z msz
0
CD CD
_
m CD �»
o
M
(
zooMM
_
_
=
3
�0
COCL
p
co
co
_
(D
p
a
m(D
w
o
w
0
-+
w
0
co
?�
c=
o
o
x
c
w
m
0
D
o
0
CD
O
mCA
w
<
to
w
N
v)
C
to
CD
CD
m
w
0
U)
n
a
w
Q
O
n
'N
t(D
co
CDc
a
(�
CD
z
cn
w
1
a
CD
�..,
0
=�O
Z CL
1
y
c
o
Z Q CO
�w
y
z
w
0
�
c
-4
CD
x-
"
9
m
m °c
d
Q
c
1
Q
� 1
CD
A
CD
z N
(Al
w
?p
a

m
co
n
n
b
K
I
O
3
n
n
Q
00
m
0
D
D
am
--A
�
n
n
n
0
co
3
<
o�
o
=1
o
o
m
n�
=
m
�
O
o
0
0
0
O
o
Q
Al
w
A
Q
CL
y
c
C
Q.
W
?)
r
t0
w
V.
O
CD
-
X
m
A
O
O
cn
.O
K
K
w
w
O
CD
2
p
0-
A
A
O
D
T1
TI
Vw
A
Xcn
(D
A
CT
S
S
'D
-
O
A
O
90
A
(D
O
w
N
j
l
a
G1
O
w
O
A
W
O
T
13101,Q-.1313L�1313131-1 . I A I- L I:M Ic L31
'T_7D-
(D CD` 1
ammo
T O
rm
CC
<
cn
(D
=.
�o
-0
0 o
O
o
a
D o.
°
o.
to CD
CA
Z
D
o
03
a3
N^^
Al)
.
p
Cl)1
V/
3:k
o
-
m
Z o
X
C
Ui
Q �
-
O
0 CD
m
P
7
O
Q
JCL
O
I..--
�'
r
QA
0 01
0
m
�o
o
m
0
°'
w
�Ea�
�o
w
o
N
Q
CD
o
O
O
0
-i
3
a
(D
ocnG
Vmwmo*
n
3
v a
m
b
❑
r
o
CD
n
--�
<
�m (A
m
o
a
�s
y Q�
O
C
�
CD
O
�o
m
�oCD
SD
coca
=
Iar�
aZo
rh
b
3
000m
00
m
m
m m
m �
a
m
z
CD
Q
m
Z
3
o
m_
m
m
Q
CD
o.
�
�
O
CN
a
m
c
CD
Jj
lCDz
o
vv
<(D
a
v� m
Z3
cD
Oo
Dm
3
m<_z
mco
fJ 3
Dm
r ^,
�X o
y v
M?o
c�—
Z CL
vZcu
Dc
m a�
m_
CO N
mo
Om
zy

-1 —i V3 C/) -0s7 �F
—1'c p Z 0 0 0
�0-a a =r ; �'0a:
0) CD CD
O O O
N D=~C�D CD
?CD
O O O
3A
�nCD
mm33�
m
Z3 0
a
0 �z ��
�mm
- CL
��
O
fD = m -n
IN
�a50CD
N � 0 .. C)
CD
QD o
CD
S
y
—m
�
0,
3
Q
�
�P
tJI
a
N m
m
N
dlD
00
�
OD
V
W
M
N
m
O
33�333333�3
CD
003 2
CO CO O ca co co co cO
cD
cn —•co 33(, o CL
c
Z
KKT2-mC)000m>omZZ
ocn I(nCDC =-aIDM—p=r
-.
K K� �0 0 3_ 00� �� ScQ
w CD
n�-6 c an
3 o O
zZ �C
cn
W CD c�
.3
�� 3 c BCD �o m
3
(D
O 3
Nr. -1 CO N
�3
at
CD UZ
— Z
�
Cn
I
�D
Z
O
o
A
o
•
O
o
cn
�
a
v
cn
o
c�
a
m
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 c'
co cO co (c cc to cQ cQ cc cc cn cc cn cn co a
c�
a
<� O
w
ODN-OZ
O
o
-3c�_.
0 a C) D
a'
� 3C) m
D Z
�z
Cn3.O " cn
d u n
(D
�• Z
CD
0.
CD
o
I
n
co
CD
-< n
°c
CD o
3 3 3 0 CL
n.
0
m
0 o
o( D=
a
o
aaa^�
n
�t �� v m n
II 11 II ?
o
n
o
N
CD
J
Z01
Q
c�
o'
O
a 333
_
__ cn cn_ an co
..a
{--,

--1 fn co 'O
-ra 0,2 C) C) C)
Zw m =cD m cn '0=v; m 000
n�pccn:3=. �Ooa
OO
a=CND;m
Zan m :3nmCO= a wcn
_Oo. Oo3 T1-n
0 sv — m
O00-. cn NN C OCD Cl)
a —n m
CD o o
CD
—m
s CA
� 3
a �
Co N H
CD
A
335-333333c3 o03
cc cn O cn ca co co (n cc -- (n 3 3 cn �
c
KyT,::-poC)C)C" m>o-DZZ 9
nca = m c =o.M cu —;:L_-
0 0 w C� =
�a:) m . 3 c-n n'm' 00
33330..{Oa� ro
m0Mc
m ZZ
0
z
O
m
n G
O
c�
o a
333333333333333a
cn cn cn cn to co cn cn cn co co co co cn co a
c�
a
N
ti
CD
O

SPECIALIZED ASS.tY" '* M.
2966 Foster Creighton Dr.
P 0, 33ox 40566
Nasbville, TN 37204-0566
1'hotte 1-615-726-0177
BLJRLIs4GTON RESEARCH, INC 2140
WAYNE ALTHOUSE
1302 BELMON T ST
BLFRLIF4G T ON, NC 2721 `.a
Project:
Pro jeft Name: BURLINGTON RESEARCH, INC
Sampler: S. C.
Ah1A1-YT I 4C AI___
Report Ouan
1lnal a Result Units Limit Limit
e►,1DLATILE GRGAPICS by Mw
Lab Number: 73-A167372
Sample ID: 9K 1 QQ-441
Sample Type: Water
Site ID:
Date
Collected:
ll/ 3/99
Time
Collected:
8:50
Date
Received:
1I/ 5/9S
Time
Received:
4:00
Dil
Factor Date Time Analyst nethod Batch
senze*e
PD
ug/l
9.1
0.1
1
11/12/79
23:48
1t. Himelick
MUM
5426
I romGkenzene
kD .
ug/I
0.1
0.1
1
11/12/79
23:48
11. Himelick
MUM
5426
n-[{ut it xzene
XD
us/1
0.3
0.1
1
11/12197
23:48
n. Himelick
MUM
5426
sec- :€11Lenze€>e
HD
ugll
0.1
0.1
1
11112/99
23:48
fl. Himelick
MUM
5426
tert-Butylbenzebe
HD,
ug/l
0.1
0.1
1
11/12/99
23:48
". Himelick
MUM
5426
Chlorebenzece
HD
u9/1
0.1
0.1
1
11/12199
23:48
n.Himelick
MUM
5426
2-chlorottiuene
HD
U911
0.1
0.1
1
11/12/79
23:48
11. Himelick
MUM
5426
4-C?tlarotoluene
HD
ug/l
0.1
0.1
1
11112179
23:48
M. Himelick
MUM
5426
1,2-#f j larubenz¢ne
No
ssg/I
0.1
0.1
1
11/12/77
23:48
ft. Hinelick
M62300
5426
1,3-l;ishlorobeazpne`
NO
Sign
0.1
0.1
1
11/12/99
23:48
1l.Hineliek
MUM
54226
I,4-t�i.hlaroGenzeae
ND
ug/l
0.1
0.1
1
11/I2/99
23:48
ilMmelick
Si4UM
5426
Ethgl3+enzeae
RD
u9/1
0.1
0.1
1
11112179
23:48
n.Himelick
M6230D
5426
Isopropylbenzeae
ND
ug/i
0.1
0.1
1
ll/12/9q
23:48
tl.HinelLek
MGM
5426
4-Isopropyltoluerse
RD
u9/1
0.1
0.1
1
11/12/99
23:48
11. Flineliek
MUM
5426
#apht:alette
RD
ug/l
0.1
0.1
1
I1/12/99
23:48
!!.Himelick
M6230D
5426
B-Propglbenzene
RD
u9/1
0.1
0.1
1
11/12/79
23:48
11. Himellck
Sit6230D
5426
Styrene
HD
ug/l
0.1
0.1
1
11/12179
23:48
tt.Himelick
M6239D
5426
Toluene
0.3
eg/l
0.1
0.1
1
11112/99
23:48
lt.tlineliek
Sii62300
5426
1,2,3-Trichlorobenzene
HD
u9/1
0.1
0.1
1
11/12179
23:48
11.HImelick
M6230D
M26
1,2,4-Trichlorobenzene
ND
u1/1
0.1
0.1
1
11112/79
23:48
It. Himelick
M6230D
5426
1,2,4-Trimethylbeazene
ND
ug/l
0.3
0.1
1
11/12/99
23:48
tt. Hinelick
Stt62300
5426
1,3,5-Trimethylbenzene
Nil
ag/l
0.1
0.1
1
11/12/99
23:48
lt.Hineliek
SH62300
5426
m,p-Xgllenes
HD
u9/1
0.2
0.1
1
11/12199
23:48
H. Himelick
MUM
5426
0-Xylene
RD
u9/1
0.1
0.1
1
11/12179
23:48
1t.Hinelick
aM230D
5426
Nexachlorobutadiene
RD
ug/l
0.1
0.1
1
11112/79
23:48
tt.Himelick
Stt6230D
5426
i rowhloratlethane
NU
v9/1
0.1
0.1
1
11/12/99
23:48
H.Hitteliek
MUM
5426
Dromodickloronethane
ND
ug/l
0.1
0.1
1
11112/97
23:48
i1.Hinelick
MUM
5426
Pronoform
ND
u9/1
0.1
0.1
1
11/12199
23:43
H.Himelick
06230D
5426
Bromomethane
HD
ug/l
0.1
0.1
1
11/12/79
23:40
11.Himelick
MUM
5426
Carboa tetrachloride
no
u9/1
0.1
0.1
1
11/12/99
23:48
!!.Hinelick
SttUM
5426
Chloroethat}e
ND
u9/1
0.1
0.1
1
11/12/79
23:48
lt.Ilineliek
062300
5426
Chloroforn
HD
ug/l
0.1
0.1
1
11/12/79
23:48
1I.Himelick
MUM
5426
Chloronethane
Nil
ug/I
0.1
0.1
1
11/12199
23:46
11.H1meliek
SiF62300
5426
D1bromochlorometnane
RD
ug/1
0.1
9.1
1
11/12/99
23:43
li.Himeliok
SR6230D
5426
- 1,2-Dibrrtwetbane
ND
ug/l
0.1
0.1
1
11/12/99
23:48
11.Himelick
S1i6230D
5426
Dibrot methane
Nli
tl4/1
0.1
0.1
1
11/12/99
23:48
!!.Hinelick
S116230D
5426
COPY 1

VECIAUZED ASSAY`F X.
160 Foster Creighton Dr.
D. Wix 40566
ishviile, T\ 37204-0566
me 1-615-726-0177
AIVPrI_YT I C Pit_ Fi lEt=0 C3Fk
Laboratory Number: 49-AI6?378
Sample ID: 9K100-001
Page 2
Report
Juan
Dil
aalga
Result
Units
Lit11t
Littit
Factor Date
Tine
Analyst
itethod
catch
1,2,3Iriciloroprtspane
RD
u511
0.1
0.1
1
11/12/99
23:48
t1.Hinelick
SH6230D
5426
G! D91 yhlorl de
PD
u9/1
0.1
0.1
1
11/12/77
23: 48
11. Hinellck
06230D
5426
Gicblc,radifluorwthaee
NO
u9/i
0.1
0.1
1
11112177
23:48
t4.Hitielick
MGM
5426
i'l-O&Woroethahe
NO
ugll
8.1
0.1
1
11112177
23:48
if. Hinelick
MUM
5426
1,2-01ybloroethate
RD
ug/l
0.1
0.1
1
11112/79
23:48
n.Hinelick
M6239D
5426
i,l-DgC-LloroetbeKe
RD
ug/l
0.1
0.1
1
11/12/99
23:48
n.Hinellck
06230D
5426
cis-I,2-Dlclloroetbene
ND
sg11
0.1
0.1
1
11112/99
23:48
M ffinelick
Sit62M
5426
trans-2,2-0101aroethese
No
ug11
0.1
0.1
1
11112135
23:48
11. Hlttellck
S11623M
3426
1,2-0ithloropropaae
NO
u911
0.1
0.1
1
11/12177
23:48
1t.Hittelick
SUM
5426
1,3-Dirhloropropaw
RD
ug/l
0.1
0.1
1
11/12197
23:48
ti.HinelIok
Stl6230D
5426
2,2-OLChloropropane
ND
U111
U.1
0.1
1
1111MY
23:48
"Mnelick
S116^c30D
5426
1,1-Vichioropropese
no
ug11
0.1
0.1
1
11112199
23:48
n.Hittelick
S,16230D
5426
cis-1,3-Dicbloropropene
ND
U911
0.1
0.1
1
11112199
23:48
n.Ninelick
SUM
5426
trans-3,3-Dichloropropene
RD
u9/1
U.1
U.1
1
U/12/99
23:48
M.HInelick
M623DD
5426
tiethglene chloride
RD
09/1
0.5
0.1
1
11/12199
23:48
".Hinelick
MUM
5426
1,1,1,2-Tetrachloroethane
NO
ug/l
0.1
0.1
1
11/12199
23:48
n.Hinelick
Sn6230A
5426
1,1,2,2-Tetrachloroethalne
NO
u911
0.1
0.1
1
11/12199
23:48
t#.Hinelick
SitUM
5426
Tetrxkloroethene
ND
u9/1
8.1
0.1
1
11112199
23:48
i1.Hinelick
M6230D
5426
1,1,1-Trichloreethare
RD
u9/1
0.1
0.1
1
11112199
23:48
M.Hinelick
SN623DD
5426
1,1,2-Trickloroethane
NO
ug11
0.1
0.1
1
11112199
23:48
it.Hinelick
S1t6230D
5426
Tricbloroetbene
ND
U911
0.1
0.1
1
11112199
23:48
n.Hinelick
SH62300
5426
Tricklorofluoronethane
RD
09/1
8.1
0.1
1
11/12199
23:48
".Hinelick
SN623DD
5426
1,2-1librono-3-cbloropropane
ND
u5/1
0.3 -
0.1
1
11112/99
23:48
N.Hinelick
Si162300
5426
."ISC�AEMS MI-ITRY-11
Total ilrgaeic Carbon
ND
ttgli
1.0
1.0
1
11.115/99
21:50
A Hardison
415.1
6373
Total iirganic Halogens
ND
t1g11
0.010
0.010
1
11120199
11:27
A Hardison
90200
3360
HD = *Dt detected at the report linit.
Surrogate
7.
Recoverg
Target
Range
53011M Surrogate t2
501/M Surrogate 93
97.
63. - 122.
59. - 117.
COPY 1

SPECIALIZED ASSAY' PVC.
2960 Foster Creighton Dr.
P O. Box 40566
Nashville, TN 37204-0566 A"^ LL Y T I C ALL FR � F' F,
Phone [phone]
Laboratory Number: 99—A169378
Sample ID: 9K100-001
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in Mull and with
permission of the laboratory.
Report Approved By: Report Date: 11/22/99
Theodore J. Duello, Ph.D., Lab Director
Michael H. Dunn, M. S. , Technical Director
Johnny A. Mitchell, Dir. Technical Services
Eric Smith, Assistant Technical Director
Gail A Lage, Technical Services
Laboratory Certification Number: 387
COPY 1

-a -icn cn 7 -ice
p z C� n n
�0�ccom y'O=vim 00p
0-2.
cD
=m0o0—En
o = c 00 0
a.
CD n•
z3n
— CD 0—
m cn
0• < o -, -%
0aM33
00
=CL
n.
mCoz�
-n'n
O
003
Sv 0
O•
N o O Q O
Cl)
CD a 0
CD
ro
^�`�
0
'7
L•
^
^
C
a
N
o
�
^
Un
Wu
O
In
01
ip
CD
CD
33s33333303
A
003
E
cn ca cs�
cn cn cn cn co ca 3
a
c
��T,='rtC�C�C�C�D7DpZ7ZZ
�
0c0 i ca
CD CLM W
obi nM m CD0
=Z0a�-00CL--•3o0^Z
oo-•m m 2)c ==r0
cnM,c
M3�02ZO
CD
cn
Z ZZ
v
z
0
^
0
^
0
o
.a
m
w
0
0
..
N
M
a
333333333333333a
tta cs� cn t:o
cn cn cn cn c0 cn co co c0 cp c0
a
O=-
no 0
a=z D
D .. Z_
v n
�ro N
CD ^
Qro 0
..... -CCD 0
SC)
3 3 3 co CL
co c>~ ro C5
nL CL CL — �
Ott qt --` d C7
II It II 0
S
Z
O rr
1
I ro
0
0
cD
\� a
03 = O,CD Z
�o' '
Nr-Z•t
m
3.0M�-N
CD m
00 I
o n
v CD
0 z
a
0
N
7
a
n
0
m
1 1 1 1
c3333

x
nnn
nay
o
m
r
~o�nnoo�
7
A.
^I
-
�
O
a
m
�
A
O•
7
d
<
�
...
N
O-
W
r
W
n
Ln
r
r
i
C
ayOm
0
�y
►C'
v
�
G
�
C
n
x
x
x
1>1
.-j
p
O
N
x
Z
.x
C
m
to
d
w
G
!n
�'.
+
m
m
w
p
¢•
In
A
n
H
a
m
o
to
.p
W
T
�
N
.•y
V
-
p
N
N
7
W
O
N
N
C
O
00
O
O
O
n
000
L
o
crn
3
3
raj
\
q
n
X
X
X
X
z
w
x
F
n�
y
y
a
a
f�
5
a
m
H"
V
N
(OII
N
N
V
O
a`
O
V
V
n
N
�O
cn
O
O
F
C
F
G
G
C
C
C
G
C
=
G
L
G
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
x
x
m
x
3
a
z
O
O
a
o
w
w
o
a
x
o
g
yO
Q
`m
.�..
y
O
O'
7
N
O
n
O
A
m
A
7
m
ii
o
�
a
c
P:
„
CL
H
O
n
y
n
Q
C:
b
a
a
T
O
3
n
"'
C
O
�
O
b
O
z
0
�
C
h9
�
q
r
A
C
"qq'�Or
N A
N
O A A
wO
d�.r
v
r

0
3
°
O
0
0
0
0
0
co
0DD-0
C)C)IC)m
m
nr
o
=
=
61
G7
S
(D
y
=
O
O
C
_'voQ
O
O
O
D
a
o
a
o
Qm
°
�w
°
crC)-
cD
:;4_
a
(D
d
g
3
O
w
O
iu
(=D
..
a
C
O
p
O
p
p
cn
cn
'S
w
J
O
m
O
o
=
O
C
a
'Q
c
'n
'11
�
o
X
CD
A
o
(n
S
S
p
O
T
(D
o
A
0
rn
CD
is
A
in
CL
°'
w
D
Z
Na
CD
C
Co
Cn
j
O
Cn
CJ
cn
A
O
m
(n
C
(a
(o
u�
(n
p
?.
(c
C
Ei
=
=
=
IS,
=
=
II
Pin
°I-1I
I�I
I
I
Z
Z
O
w
w
w
m
S
S
m
Q
p
a
C7
(D
U.
(D
7
w
C
O
O.
O
C
N
V1
y
+
(D
O.
(D
(D
o
O
((DD
(p
O.
CA
G1
C)
O
m
Z
A
d
n
cj
y
to
CD
O
y
-�23
�
Cn
Cn
p
FLW
N
0
0
Cn
+-
y
y
O
O=
N
W
3
�n
Z
o
W
Ea
rn
a
�
y
N
o
3
3
3
3
y=
3
3
n
Sal,
N
W
Q-
Z
K
K
7=
c
o
o
ID
c
y
D
D
c
(p
0
Co
a
n
d
w
y
y
C
CL
C
p=
y
CR
n0.
O0
a
°
3
n.
C
Co
C
=•
CCD
m
cn
CD
y
T.
w
3
3
A
a)CD
g
s
"4
t71
m
C1
(O
0)
C)
QAf
((A
Ul
Zn
C�J1
CA
O
m e
m
(n`n
a�
Cn
A
3
n�
Llc
c
c
a
c
0
9
c
c
c
c
c
c
c
c
c
�-a&
m
FEZ-
ra
a
_
a
M
c
(D
n
S
Z
O
O
Z
2=m
23
mc.o(t
Q
W
O
y
=
CD
(D
93
o
O
-4d
O
(o
°7
Qc
?_
+
k
a
_03
to
(o
°
a^o
�
N
°
�
(�
y
H
fD
y
Ci
t0
Q
00
O
O
<
O
(D
C�'
y
y
y
y
(�
(D
C
n
N
3
(G
C
O
(D
.y..
y
Iv
-n>-i-o
m-0 =
-�
Tn �
mo =
* m
�70
D CD
`OD
O
o
o Q
(n (D
y'
Z
D w
+
�
Cl)In
Zy
o
OC�
'ncn
--
(D
o
�
-a+
m
o (D
n
o
=
�
_
O
�
cc �
n
ao
Q^�
o
m
m
� ooCD
r
�O
O
:]3
vi
4
O
❑D
3
r
CD
o cn
El
y (�
�o
= °
U
m
y of (D
a 3
3'
0.
p
n
n
y
m�
c
mM
3
n
3
co =
r
m
CD
to
CO CD
rh
o
CD
a
(D
cn
a
TI
(D
SR
D�
C
O
s
CD
1
0
0 0
m
a r
7
3
0
l<
CD o
m
4
OJ
<

0
y
0
O
CD
a
D
d
N
N
y
C
C7
(D
Co
a
N
w
3'
CD
w
=
a
1�.
I
T
LA0
cu
0
n
n
00
W
n
D
D'O
17
m
-1
c
-1
O
n
o
n
n
n
Ov
W
3
3
o
o
0
0
w
0.
0
w
w
Q
x.5F=
w
w
�'
a
0-
-'
o
o
D
"�
3.
C
a
p,
7
w
G.
W
O
W
O
mCL
CD
C
CD
tQ
W
NO.
(D
AO
X.
(D
A
O.
O
O
W
W
O
NCD
Ala
_
_
e
TI
M
'7�
Cn
A
O
x
o
'0
-1
D
A
co
A
(Dw
n
z
N.W,,
Ww
D
fT
O
A
O
O
y^
V,
k,
3
o
e
3
3
3
3
3
3
c
3
Z
3
0
0
3
3
3
to
C
to
to
I
�
T
to
c
_
3
3
co
U
-yz0
O
cncnWTmMmv
-•4
=
C
'"
C0
S
j
0
a
w
n
C
y
O
Al
+
w
=
(1
°
CVD
y
.o
CD
N
O
y
ri
A
t00
a
0
or
N
y
N
CD
CCO
0.
a
U7
N
O
d
N
O
a
CAO
O
C)
Cl)
O
O
O
=i
W
CD
W
o0
Cn
Z
Ul
®
r
O
W
O
O
N
e
0
3
3
3
3
3
3
o
e
3
3
3
Nfn-uzzKKx=m0000
W
DDD
=
CD
?r
w=
to
m
e
a
w
w
N
!n
Z
o
o
O
m
N
c
U)
o
m
w
x
a
p1
O
=
o
a
in
A
R.
A
C
=
N.
C
T
N
3
C
Cj'
C
A
T.
d
f7f
a
d
A
O
O
3
cn
c
i r"
Acn
CD
3
.�.�
U7
M
rn
Cl)
0
T
a
cm
0
W
o
O
N
fT
a,
Cn
N
CA
.
r,
tin
o
CO
c
e
c
3
c
3
3
c
c
c
c
c
3
c
c
c
c
xxw
=CD
3
anoaocoto
co
o
=
m
cD
w
0
w
0
Wm
O
�
w
Q-0=2'
o
w
a
s
cNo
0
a
O
e'
CD
o0i
fA
W
O
C
3
cow
rA
CA
m
R30
m
m
so
D
Q
C4
� .
w
to
c
CD
CD
C)
N
O
N
-n 3y (D
�,—O
3p�370
U) tD
am
D r
(D
o
O =
Gv
_ Mo
w
a
Dv c
X
lw o
< o
m
Z
ui
w
..
D
r
3 y
:I
�?C
O.
m
Q�
n (
-
��
Q Kcn
17
O O
C
�.
CL
p
oQo
a�
O
(D
O
v �
61CD
CD
0
W
l
1
O
a)
CD 0
N
o
_
3
cn
❑ ® D
CD m (D
3 3 n
n
w=
o
o ? 2. w r
ro m
. (D
(,
—1
cn
O
m
-1 ®
�
�
O pj
CL
CD
Z
N
❑ a
�I
(1
3
Ire c�
,3i
co v
uw,
4�
3 Ci 'moo
coo m
cn
w
m
N
l`
W
O
3CD0
z0
3
v
o
v
w
— m
0a
w
w w
CD
SD(
n.
CD Z
m
(D
m:r1
c
ID 3
o
m a
CD
CD
t
s
3
Q
�
U
W
O
(D
N
w
�nh
a
00
;z CD
z3
m
>m
m<z
O C
D m
r�
km o
y/ re 1
M?o
O m —_
Z rL
pZw
Dc
m
MM
a) N
mo
0
1
O�
z to

-,� , I "1 -11 G) >
;r\ 0 -0 = =- --i -0 0 a C) C) C-)
ZE;CD =lD 0 C 0
> 0
0 CD 0, a CDCD <
CD 23
Q
0 CL z
:3 o -n -n
CL 0 Cf)
FT c
C) C/) N 0 0 CD Cl)
CD Ci- Q
CL
C)
CD
m
ra to
CD
Coll
to ^
C) El NJ
�j 72, OD -q m
o
0
33 333333 3 0 o CD
5 5 3S!
cocz C(mn(mCon = =ED cp
a:) CD =rCLM W —0-ozz cl)
E3 r.L
0
K �L R: .0-0 — CD
co m w o D) C: CD
(m (D CCDCD CL F 0 C —2 Z
cc cn C)
M CD C: = C)"
CD
= 3 cn (nw —
m
—.�
cn C: 09 W= — M cn
m cn CD 9 co
RLZZ
z
0
CD to
o CL
0 co
D9323S33333SB932
co cry co co cn co con 5 In m m ca
2:
F
CL
<m— C)
0 CD Cj) a�3N�?ix
-0="D
C) 0 0 > (D 3 N
z
o
z CD
> 0
CD �l o ;)�- Ch
CD
E z I
Oo
r7
.93
�l CD
CD
(o
i
z
0
I
lllj'l 11
= m
CD
3 3
0
cnCDCL
CD CD CD
00.
COL COL
it 4t
Z 2)
rr
0
0
C)
ifil

7 0-0 c 3 _Nf, C7 --j'a 02
Zai CD =Cq CD i 'o O=N m
o
Z00 Q_ 003
.a Q M —m
N0 N Ntp.o
a
CO3 a O
CD
—m
s
C
c
a
A Iwoo m
O • �
O l0 rn
Ln lfl
C
33=r333333cc3
CO CO O 0 t0 CO CO c0 CO .=: t0
oop
00
B3
n -n
0 CD CO) d
cD
W
O
3
n�
N
a CD
3 c.
��T2'r1C�C�C�nODDQ't7ZZ
-p ' ` ' ' o ' ' �- O N - a
KKO K0 n3 00100 -fl'Na Cp CD
X
n� 0) sv CD 0 - sv In 0) = =��
ca�Ca,00�3�0��ooZZ
ca
Ca
aL Z Z
sv
N
Z
O
0 0
to
o � �
0 o Q'
rn �
Cs
333333333333333a
cO cO cO �O cO c0 cO cO cO cO cO cO cO cO cQ a
—CD
C•
Ora
n C
n
a.. z
CD 0
C L °.
.a 3 n
.... '< o
CD 0
chr.L�n
°a a a D r-
* * *moo Cl)
It a it ?
Z
o a.
a
0
cD 0 Nr2 -t
.0.atmN
0z —
�
o O 1 D
rn
C
Z
m 0
Cl
03
a.
Uy' •F • ?. ! '7 r
= 0 -- L w
CD _a
7
0
3333

'�menw
I N O R P O R A T E D
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
23600 8K165-001
Analyte Method
6230D (GC/MS CONFIRMED AQ) 6230D
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
2-Chloroethyl vinyl ether
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3--Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
trans-1,4-Dichloro-2-butene
Result
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
11/04/1998 09:30
Rep.
Limit Units Flags
Date
Analyzed
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1996
<0.50
0.50
ug/L
11/12/1996
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
<0.50
0.50
ug/L
11/12/1998
Page 26 of 31
1491 TWILIGHT TRAIL. / FRANKFORT. KY 40601 / 502-223-0251 / FAX: [phone]

i N C 0 RP.O RA T c D
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
2360031C165-001
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
11/04/1998 09:30
Rep.
Date
Analyte Method
Result
Limit
Units Flags
Analyzed
1,1-Dichloroethane
<0.50
0.50
ug/L
11/12/1998
1,2-Dichloroethane
<0.50
0.50
ug/L
11/12/1999
1,1-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
cis-1,2-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
trans-1,2-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
1,2-Dichloropropane
<0.50
0.50
ug/L
11/12/1998
1,3-Dichloropropane
<0.50
0.50
ug/L
11/12/1998
2,2-Dichloropropane
<O.50
0.50
ug/L
11/12/1998
1,1-Dichloropropene
<0.50
0.50
ug/L
11/12/1993
cis-1,3-Dichloropropene
<0.50
0.50
ug/L
11/12/1996
trans-1,3-Dichloropropene
<0.50
0.50
ug/L
11/12/1998
Ethylbenzene
<0.50
0.50
ug/L
11/12/1998
Hexachlorobutadiene
<0.50
0.50
ug/L
11/12/1996
Isopropylbenzene
<0.50
0.50
ug/L
11/12/1998
Isopropryl ether (IPE)
<0.50
0.50
ug/L
11/12/1998
p-Isopropyltoluene
<0.50
0.50
ug/L
11/12/1998
Methylene chloride
<0.50
0.50
ug/L
11/12/1998
Methyl-tert-butyl ether (MTBE)
<0.50,
0.50
ug/L
11/12/1998
Naphthalene
<0.50
0.50
ug/L
11/12/1998
n-Propylbenzene
<0.50
0.50
ug/L
11/12/1998
Styrene
<0.50
0.50
ug/L
11/1.2/1998
1,1,1,2-Tetrachloroethane
<0.50
0.50
ug/L
11/12/1998
1,1,2,2-Tetrachloroethane
<0.50
0.50
ug/L
11/12/1998
Tetrachloroethene
<0.50
0.50
ug/L
11/12/1998
Toluene
<0.50
0.50
ug/L
11/12/1998
1,2,3-Trichlorobenzene
<0.50
0.50
ug/L
11/12/1998
1,2,4-Trichlorobenzene
<0.50
0.50
ug/L
11/12/1998
Page 27 of 31
1491 TWILIGHT TRAIL / FRANKFORT, KY 40601 / 502-223-0251 / FAX: [phone]

IN CORPO RATED
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
23600 8K165-001
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
!1/04/1998 09:30
Rep.
Date
Analyte Method
Result
Limit
Units Flags
Analyzed
1,1,1-Trichloroethane
<0.50
0.50
ug/L
11/12/1998
1,1,2-Trichloroethane
<0.50
0.50
ug/L
11/12/1998
Trichloroethene
<0.50
0.50
ug/L
11/12/1998
Trichlorofluoromethane
<0.50
0.50
ug/L
11/12/1998
1,2,3-Trichloropropane
<0.50
0.50
ug/L
11/12/1998
1,2,4-Trimethylbenzene
<0.50
0.50
ug/L
11/12/1998
1,3,5-Trimethylbenzene
<0.50
0.50
ug/L
11/12/1998
Vinyl acetate
<0.50
0.50
ug/L
11/12/1998
Vinyl chloride
<0.50
0.50
ug/L
11/12/1998
m+p-Xylenes
<0.50
0.50
ug/L
11/12/1998
o-Xylene
<0.50
0.50
ug/L
11/12/1998
SURR: Toluene-d8
79.0
%
11/12/1998
SURR: 1,2-Dichloroethane-d4
72.0
%
11/12/1998
SURR: 4-Bromofluorobenzene
86.0
%
11/12/1998
Page 28 of 31
1491 TWILIGHT TRAIL / FRANKFORT. KY 40601 / 502-223-0251 / FAX: [phone]

X
m
OD
CD
CD
0
D
c
0
N
CD
Q
D
CD
0
C Cl)
t m
3�
6
c -*
(D O
3 7
O. CO)
(D
0 0
3
O fn
T.
Cl)CD
O
0
0)
a
a
(D
0
CA
O
cr
O
(D
n
m
m
--I
2
2
CA
m
0
--I
U)
C
m
D
Z
D
C�
n
C
D
m
Z
O
0 a)
O _
aCA
n :r
O O
� O
Q
7 <C
fl1 CD
o
�a
N Cl)
ui O
CD C
CD CD
� Q
ca
O 0)
rr a
01
0
pr
--I—Icl1CA-0= DC)-+0 02 ciC)n
�070 C =rW� Zr02�, a O O
CD =ti (D CD w �. Cn R =: —
ZA? 0 M Q� cD O n� O O O C,
� D n (D O CD CD C) N (�D CAD ID 33
3 w � Q �
z3 C) � Z) 'o
O O fl � Cl) 3 -n -n
�. Q 00 m
n (p N (n o O CD
0 a w C)
CL — w
ct 0 s
�1 CD N (c
O
(D c
Q n
n d
n �nw-+�n��
O O� Cc)In • • W O
O Ck7 'U
(� oo In O O O
=3 3 3 3 3 3 3 5 3 00
3 33
co o cQ co co cn cQ co cQ =(0 3 3 10
ZKK;r,=m000C m>mzz
w (Q ( CQ O C 0- ill w ( = ;
pt ( '> (0n
0���((DD�o3wwa)C��^
-o 5- m.3oZz
C: (a m �-� -CD 3 z3 c 00
3wCDc ccnW
� c3 033 Sow �'
CD'3 w0Z
—z
w
0
O
ri
rt
sm O, O
o O�
O • O
N �
t�
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
(n co co co co co co co (a co cQ (o co (o (0
nO
n CD
D z
-0
o CD
0
� C7
3
O
C
Q
0
w
0
Q
-0NTZ
CD0-
o =
< Q CD C-)oOnQm
-o m
c o CD
Q n.
CD
cn r
fn r- p 71 ' p
D O W (D '>_ iD CD CD (D CD
o 0 Q o � _ _
gip, (nD0 �0
m 3 w o� 0 3? o9
o w
M z m w -0 w CD � o.
O 2.9 CD 9
C) (D
m CD 2_0 n CD ivy
c <
c 3 m Cn
D lx7 Q 0 3 c*
CD
r Ul Q F-+
fp O v
* u7. ww, r+ 3
rt
M O a CD Oro
M r
0 � = fv rti
CD . CA o �'•'3O CD oomCDmn 3 3mL = w
m C 0 C/' c
C I w
D w (o —
CD CD -0 �c
0Co
�-
m 6 00 a
m Cl oo CDrr
v 3 o
CD
Z m cn
m c) -0 o w
0 Q (D
r
3
n
-n coo
m
v ��
O
M CD va
� � o
0 4-- z
o .D M
z Oo CD
0
Z _
OUl
CD
0
CD
w Q o
,� o
p a T
FJ y a CD
ro 0
r� °
o :3
I D
O
00
ir
sbo
i0o
3 33
(Q (0
O :pc
? -=. CS
CD 7 (n
(D C
vCD
r
CD
c
CD
n
0L
Q z
3
Cl) CD
C
O �-h
. o
CD
Fa W
v0 O
OF• C
Cn 0
� w
'a
O.
cD
3
,o < m
Am K
CO -1
m nzzz
mp-uo c
�mp�
OU)(n m
0
D
r
O CD m
0 A
m C_
D
i m
o
z
m
m_
Z
G)
K
O
Z
O
CD M
a m
o p
w
p
w•
T
CD
a

x
o
A
3
O
0
O
0
�o
o
�
�
N.
0
c,
c•
�
c
E
qs
c
W
W
N
W
O
oN
A
T
a
3^
c
3
3
3
3
3
3
c
3
3
3==
3
3
3
x
x
x
x
O
•o
O
O
N
zy-
o
z
z
n
N
o
(�C
O
t�i�
3
b
b
WW
w
O
P'i
O"
V
N
p
S
3'
0
3
0
3
3
0
330
3
3
3
3
3
V1
3
c
c
3
4
3
3
0
N
x
x
x
I
x
a
n
m
m
H
9
o
�
e•
n
a
m
n
���
a
a
h
c.
m
c�
�
is
�.
H
a
3
�O
H
N
N
tOn
N
N
V
N
O
O
N
P
O
�
N
CO
H
N
V
c
t
c
It
c
t
c
N
3
c
r
3
3
c
c
O
c
c
c
3
c
O
c
c
c
b
b
o
b
a
z
o
o
W
0
m
o
O
a
rt
n
o
m
2
O<
C.y
0
'C OA `.
l
O
tyn
m A
G
{
O- 0
y '
O
3
a
n
b
Z
O
Q
�
r
C
r
°
n
0
v
O
a
c
s �•
d
UQ
9
0
❑
❑
>
x
o
a
r
z
z>
=3
m
Z
N
rzi
n
e
N
F
b
A
b
K
. 3
p• m
W C C
00
b

0
3
CD
0
0 0
0w5F�=
m
c
00
0
000
m
2
c m
a=
w'
.Z
m
,� 0
3
0
N
m
�
A
O
m
m
0
0
(n
14
�
3i
0
O
Co
= o
x
a
a'D
cn
==
13
c
-n
-n
w=
w
O
X
m
A
O
CG
.AM
O
_'I
O
T-
m
O
W
�
W
cn
CL
W
n0i
N
A
CL
Ira
ul
a�
a
O
O
cc
C
c
In
c
co
C
o
3
0
c
3
c3
I3
0
o
al
b
)
_
c
c
p
p
m
m
w
o
w
o.
o
0
ui
o
+
>v
a
a
m
w
co
c>
=
A
>
o
m
m
a�
N
N
O
N
Z
Li
a
a
0
W
vi
fA
O
d
U1
U7
O
=w=
�W
rn
03
o
a
o
rn
cn
Z
co cn
0w
CD
W
w
�o
o
0
0
to
N
c
3
3
3
3
3
30
c
3
3
3
0
-
V1
l/l
In
y't
m
-a-
KK�cp
m
e
oaw0
pZi
w
0
m
o
c
o
c
w
a
w
w
m
0
Rr
w
w
A
R
C
m
3
c
3
w
m
c
C,O
g
3,
C
_
p
taon
�3�
paj
(D
7
Ul
�G
—4(4Cp33a��3�
C
C
3
n
C
A
n
m
3
rn
rn"
A
m
cn
CD
Q)
CA
C
N
N
W
cn
cn
ul W
01
Cn
CA00
CO
`I
cn
A
c
c
c
3
c
3
3
c
c
c
c
c
3
c
c
c c
m
m
o
m
CD m
n
Z
O
O
03
=
3
a) CL
to
W
=
m
0
0
y m
(D
>SD
O
o
m
N
-
y
°'
Q
A
-a
'C
O
y
x
o
�,
30
M
m
m
aD
CO 'n
0,
o
m
O
m
y
m
CCD
'o
O
m
C*
(n
52CL.
(�
CD
0
a
�c
m
m
m
N
0
'n D —I
CD a m =
3
'- o?
m —
m
o '.
w
O > �'�°�
�o
o
°
CL
�0
3)0 ��
m o
D G
Q-
D„
y z
o
u.`
CD
0
°
r-
.CO
<
3Z
o
T%
r
z
��aZ__no
n 0
O`
a
R�
can
u
��
Q
'W..
f°
Z
O'd p
a4 o
0 m
a
0
@
sv
W
�CD
°
o
w�
N)
O
❑�1
3��pa0�
0 CD 5�
3 3
y���o.�
o
❑
��
`°-4
m
f °
n
m
0)
a CDCL 0 N
,�
O
=0
o°.
m
n
CD M
�r
o
t
a�rn
o
000
oor
CD
m
0)M
m
a
m
Z
M
cr
,Q
c
o
m
W
<
a
.,
3
n
c
O
c
<D
CD
7
CL
p
m
gv
<�
L
zop
o
Dm
m : z
moo
D=�
D � �
ym
m
o�'o
Za3
vZm
d
m
Cl) y
mo
��
Z co

0
Z
Q
Q
F
r;
2
'.
Z
O
w
M
s
CD0
3
W
a
o
m
tu
Inv
ro
O
N
ro
M
o
w
n
,;
m
a)0
(D
w
a
o??
x
0
m
a
CD
575
0)
(DN•
0
Cl)
0
(D
C
a
SI)CD
Q.
C
Ur
N
O
0
IC
CD
O
(A
W
-0
ro
=
roin
CD
CD
c
0,
�:
o
cc
Nro
-n D
lD a CD =
D
- O S
CC
G
(D
O
o
D(D
im- (D •-00
37
O�
O
O.
m
O Q.
D=_ Q
_�
o
0
w_m
!n
Z v
>
yMmOW
U,-<z
co
n
-n(\)�
m
Io
-
m
cn
C0 .CCD
� p �
°
K
l)
r- Cm CD
s
o �
oojo
a_
o�
0
r
O
m
D)
�1
o
5o
ww
o
0
0
n
3.
0- -. CD
� .m
O
Elcua
�. 1
(p
n
0
y00
°
CL 3
3
0
O
n �o �3�.y
CL
�5
❑Q In
m3)M
m
o
v o
m
r
('D
m
0) CD
m
m
ci
o
(D
a7
°"
CD
0
.�
m
c
l
co(D
CD
m
CD
q
`�
a
�
�
1
41
o
0
ca
n
F
-�
^
l 1
O
c'
T
W
a
(D
p

Im C
m CD
O
CO
CCD
CD
3
CD
cD
0
D
c
O
N
CD
n_
D
CD
C CD
Cr cD
3 ni
CS w
r M
CD O
d
3:
fl. c
CD O
_0
0 0
n N
0
v
CD
0
O
P.
Iff
a
CD
CD
w
N
O•
O
C
CD
C�
m
M
m
D
—i
2
CA
m
a
m
Cn
C
m
D
z
D
C)
0
C
D
m
r
n
O �_
O O
fl. to
o S
00
= i
:3 m
�_ CD
fn Cl) !
m O
CD
cr
N
0
X
—i
Cl)
-0
D c)
--� -a o Z c-) ()
c)
`—� ••c-)
o0
Z o
C=-
O
O n_ fv
�z-p=,�o
CD O
coo
C7 ^ cn m
o
o0mm�Ca-
goy 00
z 3
C�
(n
CD
CD cD 3
n_
OCL
OD
D
00
O03 TIm
O 0
S1l cn'
.0 Cn 0 O CD
N �?
r.
C
CD a C-)
n �o
�0�
vCD
Q
n
n
C'
i.t
Z,
- is r-= 3
Nam;
—1 1
ooE3
co cn o cn
(c
cQ cQ cn
cn (C)
— cn co
ZKK;;=m )000m>mzz
sv � cQ cn CD zr C_ W M — � ;:W
Q I I ' o " =-
Q O O v 0zr
�cQcnn �nz3oZZ
W m c 3 0 0 3 c r 0
CD 3
cD3 0`n
— Z
Cn
cn cQ n co cn n cn cQ cc co n cn co n cQ
00
O —
CO 0-
a) _0
o m
c �
c `�-
�• n
O
�3
0
c
Z3
a
cn
iv
c
a
c c c
Cn cn Cn
-0 N -0 Z
CD 0 0-
_.
CD Cn i
C _ O O C)
o CD ( O 0- CD
-o =
0
c (D
c is
Q ncn
3 3 D
cn (n (Q
D S
�s
m
m'
Os
m
D
r
m
m
m
n
O
r
r
m
n
-i
m
v
c
z
r
m
m
m
v
D
z
v
m
r
v
D
n
v
m
v
07' ����
T .0 a 0 CD
�CDCL'
(D
;
O
-
D
Qj c cn �- o 0
3 o
0
w
CL
z
-0 CD
y3
pO CD �_
r O
_ cn CCD tQ
; ,
;-r,
CD
•0 3
en
N
G
rn
CI
cr
cn cr
D �J CD W Cr 0
• J
r
G^ n
y
Cn CD 0 CD
CD
`T
LA
W CD
0
fr c -a c CD
r•r
C
a a M =
.
;,^
Cn
p c <CD
C
n o
0
CD CD
r o
w
cr
C 6 CD
3 CD
o
(DCD
.
D cn
"�
y
cn o
�v
N m 3 tv
�
�
W
ry _ -n -n
-
m
a
o
M CD 0-
cn c
O \ :�
z a
0
0
CD
�Cl)
a c
n c
00
�CD
r-
0
i
fn
(n
c
CD
r
m
C)
0
0
: O � m
m-0 :0
Dm;
cO
m0-0o C
0-0� jz
" um00
OU(-/)"m
0
D.—_,�
m
m C
-�{ m
o v
z
m
m
z
O
O
z
O
M
m
0

�
NORTH `..-AROLINA DEPARTN,
ENVIRONMENT AND NATURAL RESO,
DIVISION OF WATER QU}
®
ASHEVILLE REGIONAL OFF,
NCDENC��
R
SECTION
GROUNDWATER
June 26, 1998
JAMES B. HUNTJR.
GOVERNOR -
-.
WAYNEMcDEv1Tr
Mr. A. W. Huffman, Jr.
SECRETARY
Huffman Finishing Company -
Post Office Box 170
Granite Falls, North Carolina 28630
Dear Mr. Huffman:
A. PRESTON HOWARD,JR., `
Subject: Compliance Monitoring Data Review
PE., DIRECTOR
Huffman Finishing Company
Permit No. NCO025135
June 5, 1989 Authorization to Construct
Caldwell County, North Carolina
In reviewing the groundwater compliance monitoring data
submitted for the March 11, 1998, sampling event, it was noted that
no analysis was submitted for COD. Please ensure that the monitor
wells are sampled for COD on all subsequent samples.
Please refer to Permit No. NCO025135 Authorization to Construct
issued on June 5, 1989, for requirements on groundwater monitoring.
If you have any questions, please contact me at [phone].
Sincerely,
45Z-X"'- G . •i
Ann C. Rumbough
Environmental Technician
/acr
CC: Shuford Wise
Betty Wilcox
INTERCH NcE BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NC 28801-2414
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/i 0% POST -CONSUMER PAPER

� c
m
CO
o
rn T
CD
3
O
D
C:
ZT
0
N"
CD
Q
D
(.0
CD
(1) Cl)
C CD
s (D
ni
c' X
c
m 0
Q CO)
(D
0
0 0
n O
O
.a
CD
O
0
3
O
d
CL
CL
CD
CA
CO)
01
Q
O
cD
z
0
O 2)
O C
� O
0
O O
= r-
c0D CL
CD
Cl)
CD
o
..t
=CL
r
Cl) 0
(D CD
4ta
W
0
3 �
cr
Iy
0
��UJCA-0
DC)
-0 CJz C)C)C7
T�0-0
Z�ni�Q�cDoC�^
c
3SL.4 3Q2N'o
0 0
`° -
Q
w opOcn
m—cCDnCDn'c�D
�.
0c Oo
0
z3
U)
mCDm 33
�
n
0
Q�
0
O
-ice
0
w Cl) ��
o
�0
d
wcn
c�
oD
N N a. '0
D
0- l o -
COD
Er
n
a
O
W
O
�
O
N In F-3
o.
I„-o
I n
y
In
'o O r
3 3 zT3
3 3 3 3 3
3 zi 3 003
CQ (0 0 (a
(a
CQ Cc CO (0 (Q
r+Cc 3 3 CQ
(Dc sQ �D�ZZ
Cn-0 K03 0000 -o m m m�o -oQc a 3 0^Z
c(Q(z5 Ln.c-o33cQ
co
cD 3 �' C,
—z
c
0
N
O
O
� o
0
O O
cQcOCQ(QcsocQ(Q(0�c0c0(O(oco(D
e Z_-i- —
00
ZT
CO CD
D -,
w Cf)
0 CD
�• n
O
� 3
O
c
a
O
w
0_
A
-0 N -0 Z
(D :3 CT
CD Cn , s
o_
CDn
0 OnC'm
-a 2
O
C C
0 0-
Q Q
CD
I•
3 "iqq IO
t` cc"c 333
Cnr0T 0���
D �Cr w CD " ✓ CD CD m CD (D
K O O Q p w = = =
0� C/)> � o
p w . O w CD n
m Cn 3 w O w
m z m a w
O w o 0 a
o r o
mn _ c O < IN)z :E�
0- z
m w
cn CDcn
y
Cda
3
COw01
_0
G 3 CD
rt
N
?"C-)-
Q
h- O 0' N\�
P.
r'
bJ I
m
N. N
4 CD 0
w (D
O
m
`� cn o�- `°
O
N
(D �
ri
0
v
0 Q0 CD o a Cr 0
FF--�
m
F-3 1-
O f
m�
n M*m
(D
(D 0 Q
f
(!] -0 CD
f 1
m
(D Cl--Q 3
v
Z) Cn C (D
(D
w � w
rr
0(C)
CD CD 0
'TJ
r
r
c
m
�
wn
m
C)CDm
��
w
_
rt -,
v
3
o
v
D
a
m
CD
ra
®
>
TI
w
m
C
o
W
®
CD CD
n
v
-n
n
m
v
O
x
1
m
CD
0-
Cl)
w O
W
�
o
o
z oo
(D
O
z
D
O
CD
CD
w
c3i
0
o
w
-o ari
(D
w
n
< o
C)
p
o
0
(D
=
n
n
o
�
rt
o
O
I
D
0
-0C/
m
CD
�• y
co c
o
- w
w
�C
r
0
0
�
w
-v
N
YI
si
ry
Q
CD
70 < m
Am
e0
CnO -DoZc
v�0om
OAF m
0 DD
D ON
J
Om
0U-1 A
m F- c_
�� m
0 °
z
m
Z
K
O
z
O
7)
m
0

m
00
(D
CA
C)
m
Mc
cD -n
o -G
-i
CD
-i
m
CD (n
O �7
x
0
M.
o_
(C) C
(D m
D
C)
C
M
D
H
m
n
Z
CO) Cl)
a cD
3. o e
o _.d
�,.0 .M.
pr
r°CD
o
CD 0 Q. Cl)
7 � r CA
3
C1 U 0
CD C
C1
"'! n
0
�0 CD
O to
0) CD
Cl)CD O ^* 7 CZ
N
Cn
o CO) O_
a) m CD
CL a w Q-
tv
CD
N a Q.
w a1
r o
0
5D pq
-IMCIJCn-01 ,ADC)--f�
�C�� c �w �, �0=v'O 0 0 0
z (D = CD -. CD CD O C)
o: N g 0 y 00
(n 0 (D — CD CD c� CD CD CD3 3
z C) 0 0_
O H Q =5 0 3 TI '71
Q 00CD
O CD
N a 0
CD x� w Q•p o
10 •+ 3
WCD
— 3
C
Q
a
A N
O Cn C)-,% C), h—'w
0o h—'y
(r o
O
3 3 =3 3 3 3 3 3 3 0 3 (D03
cc (0 0 (0 (0 (0 (o (o (0 (o ;=�(o 3 3 co
K;r,=- c SQC coD-0ZZ
co w (Sd T I ' O I 1 0 V
CnKo 03 C)C)00 m CD
C. �-o c Q� �.3 O -3
ccoov'.0 �33c33200
3 w CD C -, C Cn
0c,�
CD(`-'3`� 03H 3
0 w 3..0
-
CD — Wz`�z
w
-o
O
H
x
00
v O O ' v
O N
W
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
(o co (o (o (o (o (o (o (o (o (o (o (o (o (o
:---------- --
Cn I
w
0o
OC CD
M -0
O (D
� n
3
O
c
O
a
CD
w
7
Q
-vN -z
-o (DOS_.
CD
o h
c C)-� n
0 CD 0 0-CD
0 CD
Q. CS
co
Q
CD
(n
nw
� o
w
0
® L
a7
CC
m
--I
D
r
c t
C
r
h
mh
0
®�
r�
r
m;
O-I
m;
vi
C i
z
m
m
m
v
D
z
a
2i
m
r
v
D
n
v
23
m
v
I
w m`� ✓m
� m m
m
CD Q O
CnD=)
�?0
0
3 w o
o 3�
w
m cn
w 0
2.6
0 _0'D
_�
Cn CD
NP
w
t-i
m
:
tow
rt
�
CD
(nC
3
m
H.
. Q
C
rr
i7 N
006
w •
w
(D
'
rr
(D
e:rJ
CD
3 \p CD
a �O 0 o
07 CD
H
ri
F-
Cl)
t �I (D
CD
O 00 (OD
(D
_
D " CD
J
CD m
cwr
o 3
3 Q
p a
Q N
rD
c�
D
n
� m
D p�
'' <
N
D 7
n (0
b
00
i CD COD
CD "O
7 r
SCS
O
co
c
CDO CD
o
3
m 0
CD
CD -n70
D
C)
�_ o
N (D
G
Q 3
(D
\
rn
-n -n
N
O
�C)
1��,2
m ((D
Cn \
A �
o \0
0 mo z
z Jm
0
z OD
o 00
all
(D
3
B."
0
Tr
(n
-a =
7 N
(ti C
r w
vCD
v
,o
v
(D
CD
w
o.
>
Qz
m w
3
CD
x
O Cr
� t-h
rr r-n
w
(� H. (D
(D 0
cn C
0 �:Yl N
n
0
�o m
;m
C_0
�IZZz
mo-00 C,
D M 0
OU)� m
D
°�M
r
0 mO
D m
O F�
W
co
m
z
I 0
O
z
(n O
CD m
m
O
I
ID
C7
CD
m.
T

HYDROLOGIC SAMPLE NUMBER: 9722344
HYDROLOGIC LAB ID #
399
SAMPLE IDENTIFICATION:
7K501-002
A, d
DATE SAMPLED:
11/19/97
DATE EXTRACTED:
N/A
DATE/TIME ANAL=:
11/26/97
bWIi M 6230 D
(GC -MS CCdWn;M=)
ANALYSIS
CAS NO.
SQL
RFcUL,r
--
( ug/ 1)
( ug/1)
Dichlorodifluoromethane
75-71-8
0.5
BDL
Chloromethane
74-87-3
0.5
BDL
Vinyl chloride
75-01-4
0.5
BDL
Bromomethane
74-83-9
0.5
BDL
Chloroethane
75-00-3
0.5
BDL
Trichlorofluoromethane
75-69-4
0.5
BDL
1,1-Dichloroethene
75-35-4
0.5
BDL
Methylene chloride
75-09-2
0.5
BDL
trans -1,2-Dichlorc;ethene
156-60-5
0.5
BDL
1,1-Dichloroethane
75-34-3
0.5
BDL
2,2-Dichlorcprcpane
590-20-7
0.5
BDL
cis-1,2-Dichloroethane
0.5
BDL
Chloroform
67-66-3
0.5
BDL
Bromochloromethane
74-97-5
0.5
BDL
1,1,1-Trichloroethane
71-55-6
0.5
BDL
1,1-Dichloropropene
563-58-6
0.5
BDL
Carbon tetrachloride
56-23-5
0.5
BDL
Benzene
71-43-2
0.5
BDL
1,2-Dichloroethane
107-06-2
0.5
BDL
Trichloroethene
79-01-6
0.5
BDL
1,2-Dichlorcpropane
78-87-5
0.5
BDL
Bromodichloromethane
75-27-4
0.5
BDL
Dibromomethane
74-95-3
0.5
BDL
Toluene
108-88-3
0.5
BDL
1,1, 2-Trichloroethane
79-00-5
0.5
BDL
I fi7gi;��a.
1491 TWILIGHT TRAIL FRANKFORT, KY 40601
502-223-0251 FAX: [phone] / TOLL FREE 800-728-2251

7
n
0
c
—1—iCnCn-u
' ��>0-1-0
pz C)00
;r,,o-0 C
��,_ -� =702F;
o
0 0 0
C)--�
0
CO w 0
—CD CD �,'Q
�ocoo
° 3 3
z3n
c?�
CD CCD
=o�
—10-
z
�oB
00
�.0-
0
��
m
(
O (D
Q
�y�
N a n
W
Q O O
CD
rf 3
w�
—�
A
w
p FP
•CI1
O F -'
F- -A c
O
(Jt
00 CS
0
O C)e
a
O
N
d
a
CD
3 3 =3
3 3 3 3 3
3� 3 003
cQ co 0 c0
c0 cc c0 c0 (a
c0 71:c0 3310
:TQw WD0
w0� �
i 0 O N
CA o n3 QC)WD..O m_
'S��CD i 3
0- (n-o°ea�m.3ozZ
Cco��.� �33�' �c-N0
3WCDc� ��C3 CcnC_.
CD�3 o3 3—Ivcn
w
cD3��Z
— Z
Cn
u
O
Orn
O .
• O Ul
IQF-°
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
co c0 c0 c0 co (a (0 co co c0 c0 e0 c0 (o c0
-0 N -0 Z
0 CD :3 CY -
(D h
����0
OCnQCCDD
3 \
-0 2
C o CD
0 s
a c>:
CD
cn
m
,` H
3 33
co
r-
CAV
Os
�i
m
D
r
cn
m
m
m
0
O
r
r
m
O
1
m
0
z
r
m
m
m
0
D
z'
0
m
m
r
v
D
0
v
TI
m
0
III
m CD m CD CD
r � CD
(D CD
inD�
®Qr
0
w
:3wocQM�
-0 w CD
w
CDO
in. o w
7
Cn
C.)
o. m w
3 C)o
0
D 0
r
D
t/i
a
C
3
<
I
= C
cn
Q
A
Qn CD
i
a'
rt
0-
�L
U) m
�\
F�3
m
m
Q
F
CDO
(D
rt
�
�0
CT
hi
0
� CD
a 0W m
O O CD
A0i
0 ¢,
< CCD)-
63
w 3
�:3
m
-0
Q CD
rF
c c m
N
�0 C
w
w
CD CD
CD -0rt
r
0
CT
00
o
m
w
CD
o
-33
a
CD C
CD
CD -n a
>
p� '
w 0
3
o
0
�
CD
N
CD
W
0
C)
w
0
D�
a z
a w
CD 3
CD
z
0
0
C
n
F�
N
c
0
m
w
�c
C)
N O
CD
oo
N
0
�Z
Dm
¢'
O =i
0
z z z
mo-oo C:z
0
©cn03
omo�
® 00
_0
I
I
I
(n 0
I
Q'
nm m
O
cC>
o
w
a
mo A
w m N C
w
a
o D
-0
I
M
p
oL
F
9
Q
z
Fy
w
W
5
o
m
°
'
z
o
>90
oCD
z
o
��
a m
CD
m
0
r of
N
w
3
0
�2
Al
�
3
T_
y
N
N
C
d
CD

-n D —I -
o cn i� , �� o
m
c0 3 8
m cD
cn
70
0
c,
r. a
w�
p o
<O
O
WZ
��
DN
coo
�1�
r
W I- A3 m °= o
-C��o Q�
m3
cn ,i2 ; -n p
O C �" CR
o
R =
c
0
cn
oCD
Cl
a
c
0-
p
j
0
op0
pM
(�}
s
o
w �,
O
l� C
CD
0
77 Cn r- 0
CD
(D 0 cp O
3 3 w
-o
sv =
j
m
G
y co O
-
0
�m
O
p
S13
cn
(D m
oZ0
-u-
o
co
ZOO
W
m
O
m
(D
O O
O
?:
o
=)
0 o
m
�'
o
m
o
O0
9
s
a
W
Q
CD
m
su
N
CD
c
m
D
�-
�
a
y
B3
:3a
to
CD
m
A
m
a
d
1
icn
O
F-IZ
n m r
a:rn
D
Z❑ m
m0 m O
4 M -
O m
< n
�
:0
mCD
c
'0
-
�?
m
3
O
(D
W
CL
i
'
-�
o
B.
J
co
(D
O
c
r
C
1
�
_
O.
CD
g
0
zQ
ou
m�
z3
0-
Zz0
M
9m
m:3
Z <_. Z
Doo
r�
a�
Z�
mdw
m=0
rL
�Z w
O�
=w
Q 70
Do
-i c
m�
�m
� a
m
n
O
Z

x
° O
O
O
°
rn
��
u
c
3
o
°_'
��
a
3
3 °
rn•
o
0o
A
°
a
o
m
o
N
C
U
W
0
—
0
A
W
—
a
C•
n
3
3
3
3
rq�
3
rq�
3
cam-
w
3
3
z
3
0
0 3
3
3
x
x
x
x
Pn
O
z
zd,
O
W
U
d
N
O
C
O
O
O
n
O
n
co
O
rn
fF
m
m
rm
f3
m
3
7
o
rm
9
�r
to
fF
3
w
3
r
�
f=
r
rr-
r-
ram-
cam-
r-
c
r
y
3
N
N
n
c
Z
Z
g
7
F.
- T
n
n
n
n
V.
>
>
>
a
a
—
U
O
O
rn
V
n
fJl
V
O
T
>
z 0
0
i
-
=
3
rr
fm
m
iC
0
m
'ro
m
rt
�
O
n
-
a
n
f
> p rrnn
v
m rd r 0
Oy
A 1
O O
.
a v o o °
a
3
w
O
v
z
O
_i
O X
A 3 w
� d
m o.
� C
�:a J
e w

m
w�
r
w
a-
0
0
q
3
CD
0
4
o
m
o
z
O O
g
m'
o
_
(D
0 0
F
-am
m En
0
o
cn
g
o
G� CD
O
CD_
�.
2 23
ID
C
_
o'
CD
N CD
<D C
O
m
70
y o:
-• m
o
y
a
CD
co
y
rmD
D a co =
07aC3g
_ o
mm a'
-M
CD
p c;
.r'-C
0
a
O
o
z
:7
D
0
D � Q
—
o
w
U10
n m
Dv
�
ao
r
3 cC0
a
=
v
,
D
cn
m
32
Q-�
0p
M
7]
O
W
Z
0 m
o �,
r
w
c
m
0
a
i 0
a
y
c
z
cl�
oomo
°ao
o
Oar
sCDoo
w
�
o
v
o
�
C
l
V
n
�
mwo0Om
oD
cp
E 3 0 2
-0
0
C
M
W - -
m
r
(n 0
0 0
9a
n
D
m
m
�1
L �o
�-
m
o
z
.
M
�
Q 3
-n
0
3
' -o
c
m
-_�
o
Mm
(n
cn
O
m
3
-
a
R1 'n
ar
i cn
Q
a
CD
Z c
`D
� a
T m
a�
� c
fD
0 z
O
p r
CDA�
, cD
(7p7
A
cmr
cD
CL
Q
z
CD
o
:31
�TT
CD
fD. cc

C)
M
m c
�
m
-
<
coO
(D
2
(D
o
m
D
c
p
0
CD
(n
Q
D
(0
C
C
m
m
0
u
0
c cD
Cr CD
3 c
n
ID
-* n O O
CT — _
O
CD 0 Q.
a0 n C
CD n O C
CL
O 0
n N M (D
T. � n
CD
0 CL
3 N
K ... N
CD o O
(D <
(D
CLW Q.
CD
0 O �
CA CL
D) g
6 2)
O 0
< w
CD v
-� CACn�
DC�-��
0z 0C)0
z mcm-�in��p=��
000
mD��o=3cnDM
�Ocdo�
n30
-cmmm5CD
m� ° 33
Z3C)
�,�
O -C----
00
0-
003 -n -n
a
sv c
0_O
w—CD -i -n
0
—
Q s
N Cn 0 0 CD
CL w
�0
W CD
w co
3
C
Q
Ach
a
A
ACD
3
O
W
N
�N (n -
N
CJ1
O
00
(J7
w
L" . d:
(fI
O'No
c
o`iw
33=73333333Z3
003
(0 (0 0 co
� � w
co
�
co (c n (o cm
� � = � �
� � 3 �
� 0 �
�
e
�cQ cs� (D c zram W -.
o ' O
D-WWWmM-OCO— 0^Z
c'co�L.� �33�c3'�Zp
3WCD 3c�'wp`.
mc n o33 3 `.
cn c - m m
m3 W,
`nz
Z
0
rt
N O
N p m
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
c0 c0 c0 C0 cQ taco c0 c0 cQ c0 e0 cQ c0 (0
C-) p
ZT
CO D m
0
cn
o m
� 0.
C:'G
�- C-)
O
.0
0
c
CL
0
W
Q
W
-UN-UZ
is (D0CT
0 cn
c) N r- Z
o (n n 0-CD
7
O
C CD
CT
a Q
U)
I-EIR
't'3 - wra fo;
CQ (Q CQ
�a
D Q m'=� I(D C m m m
�O m cio a��
W= 0) - s-- Q o
vmi<2 3 w o 3
m
CD
a <
-n z
m 0 m �
CD 3 N� Ln�
cn P. ow w� rn� m
CD
m �C�� Nn
cn
® J N O C' CD
c�
@ m
rr- ch 0. m o o m Z
(D CD w m CD
n' o 3 w 3 Q
c 0� O - w
sv 3• <
m m C)-q W co Q-
m 07 •P � (7
m (n rn m o
v 3 m
a _0 o 0
® > wD
,n O 3'
m _0 o
0 a CD cQ N
D 0a
0 w'
0 N f -Ti TI
:'n- • c.n
v �
0
� n
O
M m a
Cl) = o
0
m
z
0
Z D
O _0
00 m
su
CD
n
N
0
0
m
-0 Cn
� c
io c
r- w
um
0
0
CD
U)
c
CD
n °'
0 6
a�
c
rt
CD
r-r �
(D 3
n CL
acn
rt
M
r�
b
y
m
m-
pm
C: O
m
mo-vo c
M 0 C]o
Ocn M
cp 0
D Zm
O
CD m
N a
M
c
-Di w m
Ul 0
z
m
m
z
O
z
7,
00 m
o p
w
w
m
Q

x
m
C)
f m
v9 �
CO
m
9 V
m
17 -1 �n
2 --A
M
C
m
D
Z
D
C7
C
--I C/)
C/)
C)
-170 ^z C) C)
C)
Z m�.m--'mm--0=cn�
_p
oop
a m o
p O� _O =
C7 _ cn
O c 00
C
_o
(n3nm
Z3 C)
UmimC7CCDD
m
CCDNfD 33
Q'o
00
-
- �
_niU
,<
0 CD
,0
N (n O _
Q
0
n
—
Q
0 o
Li
CD
?
^
n
3
0
OIN
C) Li
a,rnc
C7 , crY Q
�o
w
Ln
J
O J
I-- Ln y
Ui
U'I
o�
a
r
�
3
3353333333C3
o03
(a (v 0
��0
n (v
���;���w
(v (Q (O (sue (v
;� (Q 3 3 (O
Z__
ZKK;; mmmo 7oom>-vZZ
N O(p s (Q m C =y-QW =err
0 i Y Y 0 i i i D(
0 N A) (�0 O W W WC� CAD m
Z3cQ cn I O-0 c 0— m.3 O^Z
CcOO(n �33'v3c0ZO
3 w cD E, -1 c. 03 3 C cn wN
CD 0
C3 w 0cn
—ZZ
m
_ m
1
0
C)
0
0 0
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
�e0 c0 cQ c0 (Q c0 c0 (a cQ (O (0 n cQ
C) p
O
CO CD
Cn
a
O O
7 n
O
C
a
CD
w
D
a
'&5 -0Ni7Z
m CD :3 0- .
cn
o =
o N I- Z
0-) C) Q CD
-O
CD
CO �
O 07
Q 0.
a
CD
cn Y
U)
Ln
OC
.6
?1
j 0-1
rt
cn
1=
C C C
IY
^3 33 3
DCT W CD 96 � CD CD CD CD
o
s a o
w� CD0
N� 3 su o ca < 3 w
'nzm �'.�-0 0 caci'�
00 3 n m :3m(D
CD (D 2 a O (D N 1v
mm
-Zcn
-1 CD a — I--rt
CD n a 3 (D
rLn
M N a,.f_' (D 3 o
m � w o 1-3
coCn CD « N
O (D CS O O 6 CCDD O ¢1
r cnni Ei (D O O COD rt
m C) w m CD N
m Q a0
z � � ni (o
rm- r CD o rt
mcr A '°
m Cl) w m m
v 3 o
D c
z CD v cn D � � s
s
m �- C, -o o w
N
CD CD
n
LrI
m
m
v �
rn o
1n
X �
M CD p
M m\�o-
�o
0
w
0 0
� 8
z
0
z
a
O coUl
I
CD
CD
I
w
CD
°
n
D
v o
0
O
a
Q_
o
D
I�Qm
I I
O -0 Cl) Co
3 d C CD
CD �' CT O
co c ci
co
j.
CD
Cn CD
C �-
CD
m
>y
D�
w
0
3
m _< m
m-0 M
cm
O
mo-uo �.
v uIT] 0CA'
O Cl) 55' mm
..
r (Z')cfl m
O0 CD m
D
IT v
(rI >F- o
0 (wTI
co
m_
z
O
Z
O
m
0

Client :
Burlingan Research, Inc.
1302 Belmont Street
Bur ' NC 27215-6935
Attention:
Mr. WadeEdwards
Date Received:
11/15/96
Report Date:
18-Nov-96 =
Sample Date:
13--No6
SDG #:
SDG-M]614
Lab Sample ID:
LSID83 W e l
v2
Client Sample ID:
6K2 2
Parameter
Result MQL
Unit
Method
Analysis
Time
Analysis
Date
Analyst
Benzene
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Bromobenzene
*
0.5
ug/1
EPA-6230D/5
2:07
11/16/96
_
DRW
Bromochloromethane - *
0.5
ug/l
EPA-623013/5
2:07
11/16/96
DRW
Bromodichloromethane *
0.5
ug/l
EPA-623013/5
2:07
11/16/96
DRW
Bromoforro
*
0.5
ug/1
EPA-6230D/5
2:07
11/16/96
DRW.
Bromomethane
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Butylbenzene, n-
*
0.5
ug/1
EPA-623013/5
2:07
11/16/96
DRW
Butylbenzene, sec-
*
0.5
ug/l
EPA-623013/5
2:07
11/16/96
DRW
Butylbenzene, tert-
*
0.5
ug/1
EPA-623013/5
2:07
11/16/96
DRW
Carbon Tetrachloride
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW.
Chlorobenzene
*
0.5
ugli
EPA-623013/5
2:07
11/16/96
DRW ..
Cliloroethane
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Chloroform ,
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
.
DRW
Chloromethane .
*
0.5
ug(I
EPA-6230D/5
2:07
11/16/96
DRW
Chlorotoluene; 2-
*
0.5
ug/1
EPA-623013/5
2:07
11/16/96
DRW
Chlorotoluene, 4-
*
0.5
ug/1
EPA-6230D/5
2:07
11/16/96
DRW
Dibromo-3-Chloropropane, 1,2-
ug/1
EPA-M,913/5
2:07
11/16/96
DRW
Report' By:
S. Matheson
_
*Coamtrations a low
um Quantification Limit except where noted.
NC Laboratory Certificate No. 275
PIA an 19 of 10

1 3 999 i
r"FEB
k�C ;1
�r
Client :
Burlington Research, Inc.
1302 Belmont Street
Burlington, NC 27215-6935
Attention:
Mr. Wade Edwards
Date Received:
11/15/96
Report Date:
IS-Nov-96 -
Sample Date:
13-Nov 96
SDG #:
SDG-001614
Lab Sample ID:
LSID-009783
Client Sample ID:
6K260-002
Parameter
Result
MQL
Unit Method
Analysis
Time
Analysis
Date
Analyst
Dibromochloromethaane
*
0.5
ug/I EPA-623013/5
2:07
11/16/96
DRW
Dibromoethane, 1,2- (EDB)
*
0.5
ug/l EPA-6230D/5
2:07
11/16/96
DRW
Dibromomethane
*
0.5
ug/I EPA-6230D/5
2:07
11/16/96
DRW
Dichlorobenzene, 1,2-
*
0.5
ug/I EPA-623013/5
2:07
11/16/96
DRW
Dichlorobenzene, 1,3-
*
0.5
ug/I EPA-6230D/5
2:07
11/16/96
DRW
' Dichlorobenzene, 1,4-
*
0.5
ug/l EPA-623013/5
2:07
11/16/96
DRW
Dichlorodifluoromethane
*
0.5
ug/I EPA-6230D/5
2:07
11/16/96
DRW
Dichloroethene, 1,1-
*
0.5
ug/I EPA-623013/5
2`07
11/16/96
DRW
Dichloroethene, 1,2
*
0.5
ug/l EPA-6230D/5
2:07
11/16/96
DRW
Dichloroethene, 1,1-
*
0.5
ug/I EPA-6230D/5
2.07
11/16/96
DRW
Dichloroethene, cis-1,2-
*
0.5
ug/l EPA-6230D/5
2:07
11/16/96
DRW
Dichloroethene, trans-1,2-
*
0.5
ug/l EPA-623013/5
2:07
11/16/96
DRW,
Dichloropropane, 1,2-
*
0.5
ug/l EPA-6230D/5
2:07
11/16/96
DRW
Dichloropropane, 1,3-
*
0.5
ug/I EPA-623013/5
2:07
11/16/96
DRW
Dichloropropane, 2,2-
*
0.5
ug/l EPA-6230D/5
2:07
11/16/96
DRW
Dichloropropene, 1,1-
*
0.5
ug/I EPA-6230D/5
2:07
11/16/96
DRW
Dichloropropene cis-1,3-
*
l ug/I�A-623065
2:07
11/16/96
DRW
Reported By:
S. Matheson
* Concentrations are
a kow Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
PaoP ?0 of 1n
.

FEB1 3 091
Client : Burlington Research, Inc.
1302 Belmont Street
Burlington, NC 27215-6935
Attention: Mr. Wade Edwards
Date Received: 11/15/96
Report Date: 18-Nov-96
Sample Date: I3-Nov-96
SDG #: SDG-001614
Lab Sample ID: LSID-009783
Client Sample ID: 6K260-002
Parameter Result
MQL
Unit
Method
Analysis
Time
Analysis
Date
Analyst
Dichloropropene, trans-1,3-
0.5
ug/I
EPA-623013/5
2:07
11/16/96
DRW
Ethyl Benzene
*
0.5
ug/I
EPA-6230D/5
2:07
11/16/96
DRW
Hexachlorobutadiene
*
0.5
ug/L
EPA-6230D/5
2:07
11/16/96
DRW
- Isopropyltoluene, p-
*
0.5
ug/I
EPA-6230D/5
2:07
11/16/96
DRW
Isopropypbenzene
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Methylene Chloride
*
0.5
ug/I
EPA-6230D/5
2:07
11/16/96
DRW
Naphthalene
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Propylbenzene, n-
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Styrene
*
0.5
ug/I
EPA-6230D/5
2:07
11/16/96
DRW
Tetrachloroethane, 1,1,1,2- ,
*
0.5
ug/I
EPA-6230D/5
2:07
11/16/96
DRW
Tetrachloroethane, 1,1,2,2-
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Tetrachloroethene
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Toluene
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Trichlorobenzene, 1,2,3-
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Trichlorobenzene, 1,2,4-
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Trichloroethane, 1,1,1-
*
0.5
ug/l
EPA-6230D/5
2:07
11/16/96
DRW
Trichloroethane, 1,1,2-
0
ug/l
7A-6230D/5
2:07
11/16/96
DRW
Reported BY:
I( Matheson
* Concentrations are`below Minimum Quantification Limit except where noted.
d.
NC Laboratory Certificate No. 275
Pnoe 11 of '10

r
LQ 7#mr�
Client
Budbgton Research, Inc.
1342 Belmont Street
- gton, NC 27215-6935
Attention:
lam. Wade Edwards
Date Received:
05/96
Report Date:
1 v-96
Sample Date:
13Wov- 96
SDG #:
SDG,001614
Lab Sample ID:
9783
Client Sample ID:
-002
Parameter
Result MQL Unit Method
Analysis
Time
Analysis
Date
Trichloroethene
* 0.5 ug/l EPA-6230D/5
2:07
11/16/96
Trichlorofluoromethaw
* 0.5 ug/1 EPA-623013/5
2:07
11/16/96
Trichloropropane, 1,2,3-
* 0.5 ug/1 EPA-6230D/5
2:07
11/16/96
Trimethylbenzene, 1,2,4-
* 0.5 ug/l EPA-6230D/5
2:07
11/16/96
Trimethylbenzene, 1,3,5-
* 0.5 ug/l EPA-623013/5
2:07
11/16/96
Vinyl Chloride
* 0.5 ug/l EPA-6230D/5
2:07
11/16/96
Xylene, o
* 0.5 ug/l EPA-6230D/5
2:07
-11/16/96
Xylenes, in & p-
* 0.5 ug/1 EPA-623013/5
2:07
11/16/96
Rqwted By:
S. Matheson
J
Cencentrations'are'below Minimum Quantification Lit except where noted.
NC Laboratory Certificate No. 275
Paf7P. 77 of 30
Analyst
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW

m l
e
CD
CD
O
D
C
O
N
CD
Q
cQ
CD
0
CD
t*
(n (n
Qm
o
Q0
((D O
a
CD C
CDn
j
O N
R
N
O
7
0
0
a
a
(D
co
(A
ID
Q
0
5D
m
2
z
CD
m
m
0
m
G
m
D
Z
0
0
Z
0
m
O
O, (DD
Q. N
01 �
n �
O O
O =
CD
7
O
= CL
N N
-. to
CO) O
CD :
f cD
W Q.
O
O �
a v'
C1
O
-irncn-U >c)-i70 oz C-)Oo
T�070 C ::r �o 2:dlF•o p p
Za�0W:3O-vmOC�^ `" 0
w — r* p O (n 0 �. O c 0 0
z3n ��30 (n �Q9....
:� �� pO3-n-n
0- 00 - �
O C ', ��1l
—O (ND a n
D 0—
CD _3
3
I �
Li a
A
O w 0 o a
F-� F w N
o
U1 �1 O O -1
Ul :D
33 zr3 3 3 3 3 3 3 3 003
(a (o o n cQ cc ca cQ cm ca cQ w � 3
��Z--
Z��T.2TIC�C�C�C� W D�ZZ
O
o � 000 CD o -.w w Wr- = °-�
3AiNsr� �� � 3��0
WCD �e ��cw�
D 03 3 3-�w cn
cn3 0cz
—z
w
co
O
ON o •O 1--i
Li J IN �.o
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
C-) 0
O
CO CD
cD CD
W Cn
_70
O O
n
C `<
�- n
O
O
C
7
a
co
W
a
TIN-0Z
CD p 0- _.
CD o = ' '
Q = CD n
o�c>Qm
a =
c O
CD
=3 0-
Q 6.
CD
Cn
333
% C
D 0 CD (D CD N (DD
o
r- W � CD 3 o
CD n
Cm 3 w o 3 w
-n z m Z�T * a w(D 0 o
70 0 r O
0
m n 3 Nc
a 3 n
F W
m � F- a CD No
J (n cr
CO
0 0 �m CD W 6 0 --3O O CS n. O 07 CD
r = CD o O CD
m (DO N CD CD
I (D m
m a - a
® () co cn
0 c m ro
z
r CD CD 0 CD o -
m cr
m w CD m
v 3 0 o
a
D m c m
o DZ w
1I N cn "0 O w
v S.
CD CD N
r �
n
v C)
m �
m
v
I o
n
0
w
-< o ~ O
M cD'\ a
to _
o
w
m
A
C
z
0
m.
v
Z
D
O
CD
I
�
�
o
I
w
70
c�i
CD
°
w
a
w
n
w
0
l<
0
y
O
CD
N
6
0.
0
Z
0
c
m
rw
00
CD
0
.D
CD
m
w
c>
D�
az
CCD
CD CD
CD
O
m
-DI
O
z
m
m_
z
G)
K
O
z
Zi
O
M
m
0
am,
m
m
zzz
a c
M CO m
0
�o
OCD m
N D
Ul c
Ln v

T D
>mw CD
Day$ 3
.-non =
fTl— v
CD
0
�� �o
p10
a
0 w
> C' n
0 �
D N Cr
-I
O
tom
o�
Dv03Up
0
2o0T
o
Cf)
cn
m
0
D
Sr) °
S
n
-1
n
o
w
ocn
c
Cl
u
aA
�
CD
0
CD
�
o
w
o�
o
v
o
CD
0
cn
0
�ocnpr0
(D w CD O
CD
3 3 (n 0
cl)
R-- o'
O
3 o
cn o Ln.
1
st,
fl
D
Z
-1CL3`°�3
co
1 w �
-
--I
m CD
o
�o
<
r �
w
a
�o
awn
z t'
0
� w
w
0
(.1i LQ
u'
O
Z 'O
m r
rn
m O
K m
G
m
z
3 rc
�a
Cm 0
mC: dr�(11�cn opO�opr
°Q O m m w m CD cr
y 3 m m a z
C7'°_
I'll CD o 42 (D �
� (D
a a
1 CD
3 m
f% m
CD -n vs
r c ' o
co -n 3
�w \ 0 w
3
0
CD
c
CD
1
`
N
w
c,
C-
O
p
CD
_v
0
z
Om
n.
m�
z3
0
z-
0.
m 7
ZSZ
i 1 O
0
D 7 S
Z-
Sn
m m d
m?0
zd—
�Q�
0 zm
O�
c
Cd
v�
>0
is
m0
��
(n
m
n
O
z

N
s
Irl
2
A
•
k
0
0
0
O
O
o
•o
F
�
k
k
w
w
m
N
a
o
m
0
6
A
�
T
x
x
x
x
O
Y,
�HC
z
w
ri
O
4
B�
O
z
z
O
a
f]
J
N
H
N
6
o
N
E;
o0
0
o.
N
k
kilill
k
k
z
z
x
x
n
n
n
m
N
a
a
y
Y
ra
A
J
A
N
O
3
N
zz
N
to
N
H
H
H
<
H
z
O
O
xx
m_
x3.
n
a
�ww
y
y
b
?
w
o
rn
i
d 0
p O
p c
to
0 o
° ..
O
Z
C
C
�
r
r
►c �
x
0
O
n
>
C]
d
a
9 0
❑
n
O ry
MCI
A
z
H
a
a
o

0
3
3
CD
-.;
D
C)
l<
0
0
o
o
w
o
D
D
-0
37
-I
-1
C)
n
0
0
W
o
=r
a)
o
S
cn
c
0
o
o
0
0
0
o
0
30
0
m
v?
a
w
v
A
w
�'
ag.m
o
n-
o
-
oCD
o
0
0
D
-i
CL
C'D
o
m
w
•�
m
CD
3
rS
0
m
v
c
O
cc,=
O
X
(D
o.
o
D
w
Z
N_>
�
O
cyl
WO
m
ca
n
cfl
3
(n
3
cfl
33
(o
3
cn
3
(n
C:
3
(fl
Z
3
co
o
C
Icy
a
ti
I
I
Z
Z
cn
co
cn
-0
S
S
T
p
O
S
c
c
o
m
aL
FL
su
o
m
v,
a
m+
w
a
m
ai
m
0
_'
o
m
a
Z
a
z
v
cc)
y
m
o
d
O
fl-
O
0
0-
W
3
mz
w
i
0
rn
C
o
y
o
ID
N
i
3
3
3
3
3
3
3
0
c
3
3
3
j
-
�
-
3
v
N
m
Z
S-
o
o
o
o
07
D
D
D
a�
—
azi
c
(o
o
a>
m
a
—
nr�
N
C
(D
z
n
C-)
n
S
C)
c
n
CD
ID
7c-
Q
N
SD
A�
a
N
j
o
o
m
a
0
�.
ID
N
m
�.
<.
ri
¢
m
3
A
�
c
3
�
°�'
C•
3
a
3
N
C
-�
,
w
3
C
3
m
n
A.
C
3
A
a
COD
c
3
A
O
i
O
�.
A
A
A
COT1
C�TI
O
O
A
A
v1
O
O
N
O
O
-
CJ1
N
O
_.
L"
v
A
�
1,D
QS
c IC
c
c
3
c
3
3
c
C
c
c 1C
3
c
c
c
c
—
—
(fl
w
\
cn
a
z
0
0
y
S
S
o
m
3
a
o
cn
cfl
�a
o
o
o
p�
0
a
O
m
ro
�
p.
p
m
y
o
0
x
o
cfl
m
CD
a
a
y
N
o
�.
0
a
o
m
0
o
0
CD�
CD
m
O
y.
37
a1
D
cr
S
c-
^
0
CD
m
a
a
_n D -i 'a
m -a CD S
^, 0 (n
o
�
=
CD
a 3o
wtl
d� a
o
iU
N (D
® a
> � Q
Z �-:
0
x
cn
O
U)
D
Cf)3
Z
o
_
-
�rn�_
mO
o D
Q p
CD
Q
��-
0
O.
y
C
O
-
a
Q
n
�
aA
W CD
CD
0
o
m
0
�(:t"-
o
0
`
o
w
�
O
o
�
n
77cnpr0
o
(D
CD W (D
3 3 n �
-0
g
n) .
N 3.. 0
CD
a
CD N.
i
Q
�Q371
rn
<
r,
t
CQ Q
(�•� o
r cn
o CD
0 !
�o �
a
V.1
Ul
U)
o
Z fl
n m r
rn
D_ 'Tp
Z ❑ .N
m O
m
�_
C -i
O m
n
r
O
T o
3
CD
llm
-4
nmc�
S
0 g a 0 0 m 0
mm .a
r�s
io
(D W (D
? m
�1
m o LDD
co t<� c�D
a
cn
,n
p�
n.
�
�
m
�
�
v
CD
C
0
m
I
m
r
r
co
v_
e
T
O
Z
O�
-n'o
m �'
C
CD
M M
z 5.
9m
m=
z<_ZII'
o 0 1
D� S
Z -
S
n
m �_ m
m?o
Z CL
C)zC
M
O�
C m
z—
am
:*m
Dc
m
m
� a
m
0
--i
O
z

0
I No 14-IM
0
m
r
Cf)
m
m
a
0
MA
Ec, Zn
o CD"
C
0
0 %D
m
r -
0.
— —
a
p
(D
crs
W
(D
(D
0
0 0
:3 0
<D
(D
0
00)
CD
=0
0
0
0 f-P
79.
0 CL
(D
W
N.
0
(n 0
CD —
(D <
0
(D
CL
0)
CL
n
CL
0
(D
CL
w
W
Cr
%D
0)
0
--q C/)
cn
-U. >
;r,, 0 -D
C:
:r �J, (()
M 000Sv
z
* 0 o d
FH
O 0
CD
0 :3 2.
CD CD 0 E
CD
::r
CD
z 3 0
3
(n
cD
CL
0 0
CL
Cl) z
=3
0
00
0 3 -n -n
0
--i -n
Er 0 CD
N (n 0
CD 0. w 0
0- 0
0
CD
c
E
a
O
A
A
CL
0
0
C
3
00
3=r3333333c03
C) CD
663
(a 0 CO
(a
La La La (a (a
;:;:(a 3 310
A� CCU (a CD c: 0 C)- W W
I I I , 0
0 > (n w ;=i:
CD C,) 3 CO --a �� CD
0
o CD 0 o -- C: =r
a 3 o --3 Z
c: a:� Ln. 0 -6 3 3 c 53 2
00
CD - (n Co N)
W CD --ic 3 c
D (n 3 03 CD
(n 0 (n (n
CD
Z z
0
C)
C) F-
3 333 3 3 3 3 3 E 3 3 3 3
0
0
0
:3
CIO (D
C/)
O
cl)
o
0
3
_0
0
cz
c.
c c c
-0 N -0 Z
CD Cr
CD (n
0 =
0-
— — CD z C-) =3
00 CD U) CL CD w 77
3
-0
0 CD
0-
CD
cn
z
. ' 3 3 3
(0(0(0
cnr-0:
> �C'r F� 0
o CD E 0= W,
cn > (n = a
M. w M —, 0
W =3 —
o 0
m 3 0 0 3
(n -0 'Z CD
n Z ?F Ln. -0 W
�q
0 0 CD
0 - - r - 0
.
(D m 0 -a CD
M Z
q (D ZE
> CL 3 En
CD Cr rt
CL
C/) C) Ln cn (D
w :5
-L-j Ix- 3 0)
m CD -a rt
X CL CD 0 (D
m %�Cl) cr — rQ Fj
0 LQ � (D cn
rt M CD 8 6 CT 0
0 CY CD a
CD 0 CD
o cn CD < :3
(�D M w CD rt
En 3 5T 3
vi
C: W n rt
0
C C 0 = < Ili
z
n Cl) 0 0
CD -0
0
m 07
Ln DO
Ct) cr CD
m D) (D
> CD CD CD
z c U)
a > K W
m =r 3
-4
o CD
> 3
0
"n N TI
F-
Fn -
Q0
CI% 0
0rt.
0
M CD 0 -0 EIJ CL
%,00
0 110
PL) Cr
0
:3
z
0
z >
0
00 CD
0 0 _cn r-
CD 110,
> 0
L
D crm.
C
fn
JCCD
om
ca
O
(n Cf)
r
-:2p C (D
cn
C 0
Ul�
S 'o,
00
,T CD
c
E2
T
W CD
co
CD
a
0
> Z
Q- z
3
(D
ol 11
B � -mu
0
m -a Di
m
C: 0
:X) nzzz
mo-uo7 C
555 C) �
U M co U
0 (n 0 5-3, m
0
::) CD M
m
m
> JI m
m
z
0)
m
2
G)
K
0
0
m
m
0

m
m CD
o
w � Lh
cD
O
A
C
zr
O
N
CD
a
D
m
TI
2
-I
CA
m
m
0
c
m
D
Z
p
n
c
D
-i
m
�v
Fad'°
CD
3
•f.
�,! r�a�9
y.qy
c
cc C.5
LLA
r »
C C
a(D
3
®'
c c
((D 0
� c
D) 0
fl. 3
`G y
tD
0
O
72.
Fn
O
7
O
L)
Q
a
Cl)
N
v
Q
O
fD
z
O
(D
O la)
CD
O C
O N
to
ff �
O O
(fl Q
C
CD
�. C.)
0 Q
N
O
CD
O O
:3 Q
a
!S1
C�
-i -Ifn Cn
;rl O 'p C
Z5C
n CD
Z3 n
00
W 0
CD
O I-�
0
Ln Ui
ACC
CD Al CD Cn
C Q W CD O
�.
OCD O O CD
iv
00
A
O N
O N
O
V7
-I-a p z
O O C7
O=in
0 0 0
O C
O O
CD
cD
C/)z
�o(D
m-n
®
N ( o
a
CD
n
ao o
—�
'+ ?
n
o
F
U'I
CJO.z
C3�
N
ON�c
N
a
A
tv
3
N
I I C:
33=33333333
�(Q 0(aa:)(a a")cQ(acQ ._;a:)
0o13
a121
ZKK;r,mm 0000m>TZZ
W=3 (a
CD c:
o ° O
C/) K: n3 nnooD� CD
Wm�-0C:
3ozZ
-v33C:9.=3a
����.c
O
3
CD 3`�
o 3
3
CD3
A'cnZ
-Z
O
h
A
rt
O
Om
N
�
3333333333
E 3333
cs?�cQCQCQ�cs?��cQcca(a(a(aca
�I
w
rt
r•r
00
CD
CD
Cl)
O CD
c n.
c �
3• n
3
0
c
Q
w
Q
tQ CQ Ct? CQ
-0N-Z
CD C Cr
n =
c) N r Z
o CD n Q CD
-0 _
O
c CD
cr
w n
Q
CD
(t] Ct? (Q
cn r p♦ �_� 1� 0
cr (D W O O fD lD (D
m o
CD Q p
N -� _
rD
0
(nn
3
-- 0 Q O
0 CD C-)
m
0 o
co <w
,1Zm
w•*-0
A- CD n o
3
0 CD
-
o
CD
CD CD m -0
vi CD
:3
a
Q
-0
CD
3
r-
LTI Q
OF
�0 m
c
mOL
CDCD
Nj
O:
Ln-0 (D
CD
Cr
A CD
N f0�D
0
CD
r
m
0
nw
w m
nl
cD
o �
m a
mm
®
Q3•
QN
n (Q
0
C c CD
�
ro
z
:3�w
0�
w
CD
oo
CD o
m
0,
m
w
v
a
3
0
-
CD
0
CD
v
v K
W�
m
=3 Z
� 0
3
� - 4
0
p
Q cDD
cQ
w
D
3
N
n
Z3
h-
T T
m
to
v
Ln
m
wa
CD
cn 3
o
Ln
o
z
�
O
00
mo
Ln
CD
w
((D
O
� �o
a
D o
c
?5. CL
c
0
o
3
0
(1)
cn
c
-.i
C+a
v
v m
c
O
>>
lD
09
N
(p
MY
w
a
-
-n
n
0L Z
CD °'
0
0
c
S
v
m- m
Dm
O
T Z Z Z
m0 U O C:
v�o000
•cn6-)'m
D o
0OCD m
M Ui C
jFJ m
� my
O
Z
co
m
Z
O
Z
m
0

Aquatic Bioassay Testing • Aquatic Toxicity Reduon Evaluations
Ail I Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
BURLINGTON
RESEARCH 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
ANALYTICAL REPORT
CUSTOMER: HUFFMAN FINISHING WORK ORDER #: 51K279-001
REPORT TO: Mr. Lee Huffman RECEIVED: 11/15/95
REPORTED: 12/01/95
SAMPLE DESC: NOV. MONITORING, WELL MONITORING
SAMPLE TYPE: GROUND WATER, GRAB
COLLECTED: 11/14/95 09:20 SITE: MW #2
PARAMETER DATE/TIME/ANALYST RESULT
Ammonia Nitrogen Started 11/16/95 11:40 < 0.5 mg/L
EPA 350.1 Analyzed 11/16/95 by LMB
Chemical Oxygen Demand
Started
11/22/95 11:15
62.4 mg/L
EPA 410.4
Analyzed
11/22/95 by THE
Chloride
Started
11/21/9511:45
2.2 mg/L
EPA 325.2
Analyzed
11/21/95 by LMB
Nitrate
Started
1111519511:19
1.86 mg/L
EPA 353.1,354.1
Analyzed
11/16/95 by LMB
pH
Started
11/16/95 09:50
5.22 SU
EPA 150.2
Analyzed
11/16/95 by RAW
* * Sample received out of hold time
Phosphorus, Ortho- Started 11/15/95 14:00 0.47 mg/L
EPA 365.2 Analyzed 11/15/95 by THE
Soli; Total Dissolved Started 11/20/95 15:55 86 mg/L
E"16(� Analyzed 11/20/95 by ENP
�,..L
Stgfe '° Started 11/22/9510:15 105 mg/L
E1�75t Analyzed 11/22/95 by ENP
A 524.2 VOXs
Started 11/16/9516:00
Analyzed 11/20/95 by BRL
DETECTED ANALYTES (see attachment for all analytes)
NONE
Page 1
BR2

Aquatic Bioassay Testing • Aquatic Toxicity Reduc on Evaluations \
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
BURLINGTON
RESEARCH 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
(5K279-001 continued)
PARAMETER DATE/TI M E/ANALYST RESULT
Total Organic Carbon, Liquid
Started
11/16/95 16:00
< 1.0
mg/L
EPA 4151
Analyzed
11/29/95 by ATE
Total Organic Halides, Liquid
Started
11/16/95 16:00
10.0
ug/L
EPA 9020
Analyzed
11/28/95 by ATE
Arsenic, Total-GF
Started
11/16/95 13:50
< 0.005
mg/L
EPA 206.2
Analyzed
11/27/95 by VPS
Copper, Total by ICPMS
Started
11/16/95 13:50
< 0.002
mg/L
EPA 200.8
Analyzed
11/22/95 by RTW
Sodium, Total-ICP
Started
11/16/95 13:50
2.1
mg/L
EPA 200.7
Analyzed
11/30/95 by RTW
Zinc, Total by ICPMS
Started
11/16/95 13:50
0.006
mg/L
EPA 200.8
Analyzed
11/22/95 by RTW
c
C
+
r'j
LO
`c
€
C.
Page 2
BR2

TARGET ANALYTES
SM 6230D/EPA 524.2 VOA's
ANALYTE
QUANTITATION LIMIT
BENZENE
0.5
ug/L
BROMOBENZENE
0.5
ug/L
BROMOCHLOROMETHANE
0.5
ug/L
BROMODICHLOROMETHANE
0.5
ug/L
BROFORM
0.5
ug/L
BROMOMETHANE
0.5
ug/L
n-BUTYLBENZENE
0.5
ug/L
sec-BUTYLBENZENE
0.5
ug/L
tert-BUTYLBENZENE
0.5
ug/L
CARBON TETRACHLORIDE
0.5
ug/L
CHLOROBENZENE
0.5
ug/L
CHLOROETHANE
0.5
ug/L
CHLOFORM
0.5
ug/L
CHLOROMETHANE
0.5
ug/L
2-CHLOROTOLUENE
0.5
ug/L
4-CHLOROTOLUENE
0.5
ug/L
DIBROMOCHLOROMETHANE
0.5
ug/L
1,2-DIBROMO-3-CHLOROPROPANE
0.5
ug/L
1,2-DIBROMOETHANE
0.5
ug/L
DIBROMOMETHANE
0.5
ug/L
1,2-DICHLOROBENZENE
0.5
ug/L
63-DICHLOROBENZENE
0.5
ug/L
-V,,4-DICHLOROBENZENE
0.5
ug/L
.DJCHLORODIFLUOROMETHANE
0.5
ug/L
T1-DICHLOROETHANE
0.5
ug/L
o 2-DICHLOROETHANE
0.5
ug/L
�.�
.l-DICHLOROETHENE
0.5
ug/L
ails-1,2-DICHLOROETHENE
0.5
ug/L
tmns-1,2-DICHLOROETHENE
0.5
ug/L
W
-DICHLOROPROPANE
0.5
ug/L
"-DICHLOROPROPANE
0.5
ug/L
4Z,2-DICHLOROPROPANE
0.5
ug/L
1,1-DICHLOROPROPENE
0.5
ug/L
cis-1,3-DICHLOROPROPENE
0.5
ug/L
trans-1,3-DI CH LO ROP ROPEN E
0.5
ug/L
ETHYLBENZENE
0.5
ug/L
HEXACHLOROBUTADIENE
0.5
ug/L
ISOPROPYLBENZENE (CUMENE)
0.5
ug/L
para-ISOPROPYLTOLUENE
0.5
ug/L
METHYLENE CHLORIDE
0.5
ug/L
NAPHTHALENE
0.5
ug/L
n-PROPYLBENZENE
0.5
ug/L
STYRENE
0.5
ug/L
1,1,1,2-TETRACHLOROETHANE
0.5
ug/L
Page
BR2

BURLINGTON
RESEARCH
Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations \
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
(5K279-001 continued)
C
X�
m
ANALYTE
QUANTITATION LIMIT
1,1,2,2-TETRACHLOROETHANE
0.5
ug/L
TETRACHLOROETHENE
0.5
ug/L
TOLUENE
0.5
ug/L
1,2,3-TRICHLOROBENZENE
0.5
ug/L
1,2,4-TRICHLOROBENZENE
0.5
ug/L
1,1,1-TRICHLOROETHANE
0.5
ug/L
1,1,2-TRICHLOROETHANE
0.5
ug/L
TRICHLOROETHENE
0.5
ug/L
TRICHLOROFLUOROMETHANE
0.5
ug/L
1,2,3-TRICHLOROPROPANE
0.5
ug/L
1,2,4-TRIMETHYLBENZENE
0.5
ug/L
1,3,5-TRIMETHYLBENZENE
0.5
ug/L
VINYL CHLORIDE
0.5
ug/L
o-XYLENE
0.5
ug/L
m, p-XYLENE
0.5
ug/L
Page 4
BR2

CLIENT:
Burlington Research, Inc.
615 Huffman Mill Road
Burlington, N.C. 27215-5122
Attention: Dr. David Chang
DATE RECEIVED: November 17, 1995
DATE REPORTED:
AMPLE NUMBER
511-2068G
November 21, 1995
SAMPLE DESCRIPTION
Water; 5K279-001 for 6230D.
PARAMETER
511-2068G - 6230D
- Benzene
- Bromobenzene
- Bromochloromethane
- Bromodichloromethane
il"3
_w•
- Bromoform
Bromomethane
- n-Butylbenzene
- sec-Butylbenzene
- tert-Butylbenzene
Sara
Carbon Tetrachloride
- Chlorobenzene
- Chloroethane
Nov
1995 .
RESULTS
MOLL
DATE STARTED
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
1 1 /20/95
*
0.5
ug/I
1 1 /20/95
*
0.5
ug/I
1 1 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
*
0.5
ug/I
11 /20/95
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.

PARAMETER
511-2068G 6230D
- Chloroform
- Chloromethane
- 2-Chlorotoluene
RESULTS
*
*
*
- 4-Chorotoluene
- Dibromochloromethane
- 1,2-Dibromo-3-Chloropropane*
1,2-Dibromoethane (EDB)
- Dibromomethane
- 1,2-Dichlorobenzene
MQL
0.5
ug/I
0.5
ug/I
0.5
ug/I
0.5 ug/I
0.5 ug/I
0.5 ug/I
0.5 ug/I
0.5 ug/I
0.5 ug/I
DATE STARTED
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
- 1,3-Dichlorobenzene
*
0.5
ug/I
11/20/95
ts
- 1,4-Dichlorobenzene
*
0.5
ug/I
11/20/95
W
CID
- Dichlorodifluoromethane
*
0.5
ug/I
11/20/95
W
- 1, 1 -Dichloroethane
*
0.5
ug/I
11/20/95
Orr
- 1,2-Dichloroethane
*
0.5
ug/I
11/20/95
- 1, 1 -Dichloroethene
*
0.5
ug/I
11/20/95
U-)
- cis- 1,2-Dichloroethene
*
0.5
ug/I
11/20/95
ON
- trans- 1,2-Dichloroethene
*
0.5
ug/I
11/20/95
- 1,2-Dichloropropane
*
0.5
ug/I
11/20/95
- 1,3-Dichloropropane
*
0.5
ug/I
11/20/95
- 2,2-Dichloropropane
*
0.5
ug/I
11/20/95
- 1, 1 -Dichloropropene
*
0.5
ug/I
11/20/95
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.

PARAMETER RESULTS OL DATE STARTED
511-2068G
- 6230D
- cis- 1,3-Dichloropropene__
* -
0.5
ug/I
- Trans- 1,3-Dichloropropene
*
0.5
ug/I
- Ethyl Benzene
*
0.5
ug/I
- Hexachlorobutadiene
*
0.5
ug/I
- Isopropylbenzene
*
0.5
ug/I
- p-isopropyltoluene
*
0.5
ug/l
- Methylene Chloride
*
0.5
ug/I
- Naphthalene
*
0.5
ug/I
- n-Propylbenzene
*
0.5
ug/I
- Styrene
*
0.5
ug/I
- 1,1,1,2-Tetrachloroethane
*
0.5
ug/I
- 1,1,2,2-Tetrachloroethane
*
0.5
ug/l
4�
- Tetrachloroethene
*
0.5
ug/I
- Toluene
*
0.5
ug/I
- 1,2,3-Trichlorobenzene
*
0.5
ug/l
-
1,2,4-Trichlorobenzene
*
0.5
ug/I
-
1,1,1-Trichloroethane
*
0.5
ug/I
-
1,1,2-Trichloroethane
*
0.5
ug/I
-
Trichloroethene
*
0.5
ug/I
-
Trichlorofluoromethane
*
0.5
ug/I
-
1,2,3-Trichloropropane
*
0.5
ug/I
-
1,2,4-Trimethylbezene
*
0.5
ug/l
-
1,3,5-Trimethylbenzene
*
0.5
ug/I
-
Vinyl Chloride
*
0.5
ug/I
* Concentrations are below Minimum Quantification
Limit except where noted.
NC Laboratory Certificate No.
275.
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95.
11/20/95
11/20/95
11/20/95
11/20/95
11/20/95

PARAMETER
511-2068G - 6230D
Xylenes (m & P)
- o-Xylene
RESULTS M L DATE STARTED
* 0.5 ug/l 11 /20/95
* 0.5 ug/I 11 /20/95
REPORTED BY: _ _____________
D. R ssinger - General Manager
UJ
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.

J 1.5;Ue HIEL 1NU. - MHKIUIY b14 .566
i.�bir,r T"�<<.•
.s�_ :`a•��.1lA►i4'ci.1'iiQt?.:i '. >;i;?:.�:�•.•. •:
Aqua Tech Environmental Laboratories, Inc.
To: BURLINGTON RESEARCH
615 HUFFMAN MILL ROAD
BURLINGTON NC 27215-5122
Attn: DAVID CHANG
Client # : S0064 Lab # : 10-95-130846
Your Sample ID: 5K279-001 Login Date 11/22/95
Sample Matrix : GW Date Reported: 12/01/95
PO #: 0262 Date Printed 12/01/95
COLLECTION INFORMATION
Date/Time/By: 11/14/95 09:20 CHANG
Location ,
Report Approved 8y: 2%�j4/t,
Ando'.-j—
Deborah K. Johnso
-----------------------------------------------------------------------------------------
Analysis Result Units Analyst EPA Date of Run
Method No. Analysis Number
-----------------------------------------------------------------------------------------
10-95-130846
TOTAL ORGANIC CARBON < 1.0 MG/L BKH 415.2/9060 11/29/93 11000561
(TOC)
Total Organic Halogens 10.0 UG/L TDC 9020/450.1 11/28/95 11000560
(TOX)
1776 MARION-WALDO RD. - P.O. BOX 436 - MARION, OH 43301-0436
PHONE [phone] - FAX [phone]

c
m
m m
o
�
-n
rn -�
(D
w
2
D
(D
2
CD
C/)
O
D
c
m
O
�
(D
Q
Cn
cQ
0
�
C
m
z
C7
D
C�
C7
C
D
CD
*�
ea
sv Y
0
c �
_z
(D
cr o
n
0
O
0
�
to
Q N
n
0
0 O
d
C=
n Q
y
(D
: CD
0
0
o
•�
m CZ
(D
N N
.-. N
3
N 0
0
CL a
4 i
CL
CL
0
N
Q.
N
a
a
0
c
<
pr
m
...
—I Cl)
Cl)
)DC7
z 000
T -oc�Q;
��,�p2�000p
Z m=.mQ�CD0
—E..�vv�v�
-(1) F-Ei.p
goc00
cn3OCDn
2- CD CD
mm� 33
z 3 n
cn
CL
o
ov
CL
C/) z
-n -n
:3
00
vo3
— (D
N Q o 0 CD
�v
_ 0
0.CD
o
10
(D
0
W
¢� to
A
^
W
O W
F- F-
O
y
•C
c
33=3
3 3 3 3 3
3' 3 003
cQ co 0 cQ
c0
c0 co cv cQ c0
;;:(a 3 3 c0
Z��T.2�7C7C7C7C7Q7Ds�ZZ
�(acDc=rQww 7 ter«.,
oK�OK`o30000D--amm
Q �cQ N n v� c s?� �•3 o ZZ
coc3 0
n33 3o¢'ca'n
CD w (n z
z
0
r-
o
O N
N O ON
W
3 3 3 3 3 3 3 3 3 3 E 3 3 3 3
CQ CQ CQ (Q (Q CQ CQ CQ CQ c o C� CQ CQ CQ c.Q
0 O
O
CD
'. cn
o
0 0
O
c `<
�• n
3
O
c
D
Q_
(n
A�
Q_
�-0N-0Z
0CDv0-_.
CD U)
< CL - CD
77
o CD n (i CD
- Z
0 CD
Q_ S
n
CD
(n
3 3 3
COC.0(a (a(a(n
CD
O 0 ca. o= = =
cn c pQr-
r � N
m o 3� O o 3 CD 0
-nZN cn o ' CD
o
Ow m w
3 n CD
o o70 •
m n = = (n CD
NZ
mq CD 3 _E
A Q• CD 0
m cn Cl U m Qj
CN ,
+G O C,W NN\ 0
m N F\ (D �
Q
m °�° cn cr
n (0 N Cn (OD O 0 Cr NO 1-1
m (-, W CD r2 O F"
o �• Sl
rn Q° - -aw D
v �G n cQ � c fD
c ^` o 0
z P- a
O
r Nro- N °DfD o,
Ln
m Cr QJ W Lnn CDCD
_ r
n -0 O CD o
z m c (n mom.
v > � w
m �o
a�
D
n
v
n v rt
m
v `0
Ln
Ix 1
0
c� ) O
m CD o Q.
cn wo
l) o
(D
0
z
O
w -a
D T
o CD
0 Q
w
o•
0
fn
Ix m
p _v Cn
a.6
3 U)
c
-o
�0
ID
(D
w
CIO
0
0
0
m
0
Q -Z
Z
m 3
CD
0
c
(-D
N
H
c�
0
2)
N
ii � m
0m
co
MO-ooc
vv,o? .� 0 M 0
Ov,'m
0
OZCCDD m
m c)c
yo m
m
O� v
ED
m
Z
G)
O
z
O
(n M
CD m
0
A
v
w
T
a

7Jaro�g ��
D> � o p o
:0O
o
a o
G,� z .�
JJ w
N (D
D�
v
N
o
o
(^�
l 1
N>
� W
CO
0
D
{
CD
n 0
oCD
c �,
o
o CO
n
a
QA
y a
a �
?
Z
o
\
o
CD -
E
o
=9:°
g
tail
w
,CD
o
m
g
O
�'
p
W
o
�
C CD
R1 w -o �_ w m
O
o
'O
N `Q
n
m
M
r^M
m
C
z
:13
�CL 3
2c
-n
m
03
3
�
o
z
�
o.
w
A
m.
0
0 0 0 :0 0 r
m w m
o
CD
m
-n
m
r
v
r
m
O
E
0
0
za
o�
�a
m
z�
�ro
00
m=
�z<z
1a0 0
rM
Dh/
� \/
LJ ro
mmd
m?0
z0
Od m
M
O�
cd
z-
am
ro
n o
-I c
m�
mro
(0
m
n
--1
O
z

0
3
v
n
n
b
n
n
n
n
S
<
D
o
5-
>
0
0Tz
w
CD
3
1
V
m
CD
3
0
c
ID
0
o
C
C
j
A
N
CA
m
o
o
o
o x
p
0
-
-
o
v o
L a
0
0
m-
o
P
3
o
cc w
O
c
-n
-n
w
o
fD
a-
�
w
O
w
wa
w
j
`a o `� a`� 3.1`� I`a I`e I V; I 11(?
I C:I� I3 I3 19
I`e
NWTZZ KK
m m o i i
o' w 7• a w w
A 2
C C, 3 w T
n n
o �• w w w c
A O c M.
CD .
En - C' C' 3 a n c A
w� 3 A m m
N
A
0
D
a
-n
�v
ch
a'
co 3
0
O
'o
`
CL
cn cu
C
D v .c
Z , .
o
U�
W
3cn
0
70
rn
Z20
-n
0
-
-n
9�r
v
0 CD
%Z c-i
m
0
00
o m
o
a
w
Zak
O
- .n
�A
Karoo
z'r
lg\CD �
o
w
o
o
w
m
O
w
o
v�
n
_I
m
Cn p O
U)
w �
m col) su
\'
CD
� 3• -0 O
Ci
cn co = 3
0
0 0
•,
CD o cn
O
0 cD
3
rn
��
yam
m
�Z3
IIN
em
m
m
O
O
2
o
m
m
o
n
_z
1
w
w
fD
<,
ma
0
:3o
0O
Om0m
a
ss
o
m
Q.
m
y>
v
ox
G)
:3
CD
?
O
m
N
-
0
CD
._,..
0
2.
N•
a
w
"O
CD
CD
m
O
D
�,
v
w
g
rwn
O.
a
m
to
n
fA
CD
m
m
co
co
w
3
.D
m
5
m
N
c
❑ Z
D
C
m
=
D
M
m
Z❑
O
m
p
m
s'i (7)
O m
< 0
v
v 0
m
m
A) m
mm
Q
cr
�o
z
c
CD
o
N
Cr
CD
qA
C*N
G
-n
N
0
C-
I
W
7c
fD
O
C
CD
w
a
a
v
fD
L
a
_v
N
O
zo
Oa
m�
z3
w
x�
z S.
mm
z<_z
yoo
row
D ? S
z .—
x
n
mdw
C-
m
0
z—_
, CL
Ozw
O~
e
cam
G y
m�
xm
N to
m
n
q
O
z

-C-
CD
L
i
A
Z
0
O F
0 FL
cncn -o zi)Do --i=oz Sin
�cv-9 O
�.w�a�u�cDoC�r. 000
CDi (D o cD (D 0 CD� � � � 3
Z 0 v KK
p T
^yam A o
tY
K
n
A o
w O 01 N Ln p
O U-1
C � �
33=r3333333'3 003
cc cc 0 (a cc cc cc cc cc cc ,_: cc 3 3 cc
� 0 � — - � = � � O � ==
ZKK7m rtOOROw>-OZZ
co ccCDC� SDOtip"•
aff
3 D - CD
c 0^Z
o 3c35cn 0N
W.
3 z
Z
_
0
n W
0
oCD •
333333333333333
cc cc cc cc cc cc cc cc cc cc cc cc cc cc cc
i6 cQ m a
th
D
02
Z i6 v, i
�,. -
.. a
5-
0
CD
2
C
3
Z Z
C
�
CT1
3
Ln
~
N
u
1
I
o
w
e
Fo xv
o
cn m
En
02
�
CD
Q N
c- �
S,
O
CD c
�
(� ;�n
O
W
�
N
O
op
W
N
-n'n
o
0
0
C
'A 2
CD�o
o U'
M
z
0
00
m
o M
S ME
s
�
I
i NF-�.
N O N
n
t N O
RL
d co
t O �
�-7
O b N
C f!1
C
N
N
m
Dm
c �
m' -uo C,:
vob=
cnmoCC)
u' m
w
zCD m
g m
o
°ul
o m
w
Ul
m
I
0
v
v

CAD R C=D N (D V) 2: � S) 0
CD � A O n �
O (D (DCD CD �.
Z o o� �g'-n -n
O
_S
A ^ h
o w o W�c"ul No
Cn O O O � r—I O
O
Ul
1
3 3 F3 3 3 3 3 3 3 S 3 003
cc cc o cc CO cc cc cc cc cc ,: cc 3 cc
Z
a
O
C �
�
v
ZKKXM c ORO wi �mZZ
D) = 8i Ev EF
m
wFKS dD S RC O OWC O Z
!R 3co3 Z
� °.c`z �3 3 3 c �W
v
3 3 oa'�
ZZ
O
A O
N O O N
cpUl
No
3,33333333333333
to cc cc cc cc cc cc cc cc cc cc cc cc cc cc
Z�m
c c c
cc cc co
N
N �4
?
�7 0- (D
o CD 0
D
3
c,
O n
c.
<D
co
O
N {'+
:3
333
cc cc ca
z
N
u
Sv
CD
o 0_
=3
N
N :3
Lt
3
3
�,Ocn�
: c3
m
rt
ch
�
� � 3
a
rt
rt
m
78
.t
110 a
�_
�
m
w
N �
�
W
p
-n -n
00
0
a
o
Ui wi L
a
9 z
A
i
v
O 1
m
m
g9z
000
�m
r
c
m�
pp cr
ZLr
m
z
G)
0
m
v

m
m
0)
co
m
o
CD
3
O
S
O
N
m
Q
CD
CD
-C
z
0
c CD
cr m
a
n
0 O
c o O C
m .�
Q O
n 3
O
a) = 0 O
CL
� y CD
(D cD
g �? CD
.n
7° 0 CL
N :n vi
U) O
O CL
Ca W O
O O
m O O.
N
N a
y 0)
6 O
C/) Cf) -0
�DZJCD C7—I�
oz
nnn
%.=N
�0
_
Fl
000
m
D o
o 6' 0_
=' o c
00
CCDD CCDD
O
--I O_.
w (/q z
Q
00
� o'3°
-n -n
�
�(n
Naa
ON
0
Q®o
w
—�
O
S
—
CD
Pe
s
A
W
O W
61 G•
I ' y
N
O
CTF O
O N
N O�
O
Ln
ro
i i i i I I I I -" - I
3953 3 3-3 3 3 3 c 3 003
Co CQ O Cc (a CQ Cc cc (a (c n CQ (o
� � 0 �
z,KK;;�mm0000W>-czz
O GGO (Q (D c Q fl) iD = ;;:.-=�.'
s O a � � ill
CDKKO Kz 03 OOM--a m m
Q�(Qmm�-0cQo 3o^Z
c(0�v'•c -a33cc��z0
m c 3 O 3 CO
m 3
zz
0
N n
OON O
o O�
333333333333333
(Q (0 cc cQ co co cQ co cc cc cc cc (0 cn (0
"&5 T N"-0 Z
a CD Cr -'
0 = o
,C o N r- Z
O CD n Q CD
O (D
c
cr
Q n.
CD
U)
n
t I'" 14 jfn
'a; a a if ., i P•. .'
c c c tr —
C0 (0 (0 t0 (0 (0
i::� i-z:
>c �c� w cc(c
(D CD (D
'S o N Q& W
N
r- WD(nn - ---
o
va o`er o3
F
mz<p O•-0 w -n
O
CD.
CD
o
m (D _ vi
O
N Z
3
_
'c
n
r
UJ Q
D
3
ri-
Sn
Cn m
2�INm
m
m
N.
D
I 0.
O-p
m
O
(D
Fi
m
"c Q�=�Ny®n
(ODD pN_ CD
03
m
[(D
w
--I
m
o 3 w 3 a
-0 c CD
a a w
r�r
v
cQ C c CD
b
zCD
n
CO
CD
n
O -O
rt
-I
m
to
�
m
Cl)rn
"D
co
v
>
3
N
OCD
Z
v
CD c
> K
m m
w
m
Z3 --T
N (n
3
o
®
CD (cD
cQNJ
0
0
v
2
00
m
v
o
�
x
Q
rn CD
fn
O
0•
"t.0�'
z
fmJ
c
�
z
(D
o
O
z
D
®
00
_, CD
0
o a
a cc
42 `� oo
O -0 -n =
v m
�• Q
c o
o
rt
o
(l)
�¢
O _0 Cn Cn
S -6, t
CD y
(D
lQ C
p'
l
N
o
0
m
CD
q
Q
CD
w
0
Q
Z
90
(n CD
m
O c,
2-Do z
C
aM0000
C/)�•m
0 37
�cQ
O M O CD m
m O fJ
N S
>N m
O� g
z
c
m
z
O
K
O
z
m
D

-
m
3
C)
C
COC)
n
C")
co
C)
D
D-0
�°
sum
p
N
�
�
=
m
CD
o
�.
o
�.
g?
w
w
to
v
c
3(
a
m?
W
O
CDco
O
X
M
W
cr
C)
=
X
A
?
(n
_
=
c
y
A
O
co
A
(DD
w
6
w
Q
N
A
Q
cn
o
Ln
Wo
-1 0 n 0 n W
00 0 0 0 o o
r =_
W O
T -n N
o m �
N 0
`° o c13 c� 143! 113
`e I C 13 I I I`� `�
v-
o
m
0
Z
O
O
2
2
m
3
n.
o
m
w
co0
o
CD
m
0
0
1;
X
O
X)
n
O
En
O
O
:3
CD
O
m
-0
j.
i
N
m
y-
w
to
n
o
0
c
(D
v
CD
.aCDm
Y
(D
0.
g
cD
D
0
a
Co
o
cn
cn
.n
. c
j0 8 r a O� W Z_
w o0 �
D n Din c o
:X] co r A3y _ J
o
D Cn m 3270 �j n 0
Z 0 `° �
p CCD (>
-< o tn p �.
m a a z
aA wo C mO o00
mc:to 2 O ,
6� Op W 4
➢� O w
V m O
o
n �
m � o O D
to n C
w D = N -�
N� �_ 0 o
.� � o
n mocn.
sN� z
a 3 3 O�
O
b W�
� o �. n 0 m
C-)
f� o
3
v 0 3
m
Um
ila
3�®� 0 0 0 m 0 r
N CD W CD
1 m m z
CD CY c
2 (D o m
U, m
TINc n �
T�:, O_
ncDr�
(D -n
j c 1 O
C
LAI O
r C
kc,
CD
0
U)
O
z
O ro
m�
Z�
O
Z —
Cm
m:3
Z< z
D 0 0
D(D ?
D ~
2 C)
m v d
m?0
z
O�
C pj
CO (D
G y
-DI cm
u)
m
n
O
z

0
O
3
U1
0
0
0
m
a
D
w
N
N
N
c
cr
3
m
m
N
w
3
-a
CD
w
C
a
0
O
n
m�
0 O
Co)
C)
0y
CtQN�-
TA
n
0
2
od'
pOW
O
00_WO
aoA3ww
trn7
'
o3
Oo
CL
[N,o
g
o3
o
C CD
CD
--
Cn
`
o
NOQ
N
,�
-n0
O (D
�
o
CA a
(D
w
o
N
�
L3 to
O_
(D
—
� W
cn o
W
0
P am
n
-i
3
cfl
�
L
3 3
E
- ri CCDD���o
D(D-0
M—
Cn
m
p
3
p a .D
�•
o
:0
0
0
> �o
o a
-
D ov
Q
o
m
D
Tof
73
O
m
Sato
3l
o
D
Cn
m
E4 S�
-n
O
Z
D
O (D
O CD
T �'
�y
cn
rn
o
Q
Z Q
aA CD
CD
O
o CD
O
w
o
O
O
w
o
�
O
_
N
Cn
O
C7
* C Or O
W
CD CO
333N�
0 0
►,\
r
(AC O
N
yoPa
3
-"cote
n
cc
e
N;
kA
�3
g
20
Z
r
,
G
-3
f
n
Z
O
O
Ll
O
O
CD
z=
w
3
n
o
w
CZ)
O
CD
<
=
(D
7
7
0
-i
w
O
Xo
f6
CD
N
3'
m
nDO
O
m
N
�
O
m'
w
(A
cf7
a
<
Ch
CD
O
N
CD
C
CD
D
N
a
CD
w
O�
n
N
co
CD
!0
N
m r>
Za r�_��, j
n
^� J
W Q `
r cn
O CD
M c-
to W
Z
w Ul
t!?
0
❑ m ram'
im
D i7
z M_
o� O
c m -�
4 0
on
tJm
„
C
�
U
U Q;
3m o a c
`
(D
rn3
m
CD 0
I
C CD
j
U
CD
CD
�3
Z
y
+
-
oCD
m
L
y
vZ
Q4 I
0 r-
T �j w CT
6 cD 3
CD CT
CD
3 ��I C

0
c
O
N
F
2
CD
Son (A"G)DC���
�.��i
=y�93 PRO
0
:3 Cl- ID
CD
ZanmOm�n(QD
n
� �� mm
a o 4
W c
W=r
s
A A
O W- O[vNCnOa
E
A
O
�� O O.ON
CD
A0�
O
to
C
� J
33=3333333S3 003
Ca Ca O ca Ca Ca ca ca Ca ca !-:� 3 3
ZKK7mO OOROwkszz
� � � o m
KK'o CD , Rc-O owc O � z
c w� p 3 c 3 z0
31�o�.3� �`033 3 ��
�63 6' �z
z
O to
� w
333333333333333
cc cccacacacccacacccacacccaca(a
09 0
CD
0
0
2.
ut 3
4
®ON
5 .3
c c c
3 3 3
co cc ca
ca ca ca
D cn p r
9 z�
0 ..P'5 o
3 m
cn �'
17
O
La a w� N a
cn CD E�
(� o a " r,
cn . I
(D CL cQ cn
r
r
Co
CB
-o
�N -n-n
O
o
Wo
F
ro
m
Q z
a No
4
m
cam^'
m
70
(D
70 'zzzz
z
mop?
C
o
cD
rn
D�
m
co
Ul
I r
CD
g
CD
v
�
g
m
c
m
s
o_
Z`
v
Aa
o
Q,r
f.
!R
o
a
�
iv u2
G
CL

m
m
C
m
C)
C
CD
c
g
CnCn-0�7 n
CD
�.su0-382 asumop� oop
CD CD a
0 n'
w 2.c m
�=3 �o �
CL
n ^
o�vww
. . . .
U7
33=r3339333S3 003
c0 cc 0 cc Cc cn cn cc cfl Cc ;: ca
��cn �������0 ::-. 3 3
0)K cK cQ CDc � � N !v � 3 Z Z
KK0 Ko pa-0 0� c 0 -
coal n�0 3QDo'
c'32Z
3�=.3•2_.�c33c�w�'
%3i3
ZZ
w
o
w
333333333333333
co c0 c0 cQ c0 c0 co cQ cc cQ cfl c0 cn cfl cc
:::m� � � � z-
0
o
�CD � z
gQ
R_
Z
�n
o
a0g0��'
Q n Ci N
cD
3
c
m
o
0
3
N
m
c
cn
c
c c 3 33
cc
cc
ca co %cQ ca
z�N
0 c�" oo�
3 mz
c
3 rt
\ � � yr 3
to CO --T� �I
:moo
" m ��pp Z
o Cn Q
= - Q N " n
d rt
N�$
c cc
o
N N
00
N co
eD to
wo
10
00
Mm
c�
m
m
�m
r
m
m
Z
c
m
iB
2
m
m
^Y'7

-' v x D m 2 o s O C..
in QJ Q D o` o .' a\
A 3 00000>M0DD-o --i000000 � �o o �o a � Z
m 3 o�°,'u,ow��2 �O°oOOO>E3 �� o
m CD ° o° o v m w� w w cr 0 _` � 0 0 0 D� o D �, < o
< 3 a.. 3: 3.cr° °'3'CD ago o
m -i o� ca r 2 m' Z
w° n 3 w .�' �' co 3 3° D ov o ;7J
N �c 3 cD- -ice o.. Ica co r- {_'_ °
V s >7 ,� { vv,
om o°x'o CD ao o rn ��ww� < -n
w 2 a w & 4 v& m m w 0 O m
OX m j A 22 �TUl D ° 2 n
�Oo 004 ° m Cl)cn � O O
�o o �N W� D °� �� rn
N w w t 0 0 � CD � Or Cl)
?_-Al '� 0 O
n� Vt O a O OY'jC 3 O ZI
�' €' °' CD m a 0 o IT1
a 3 _33 3333= z3 :333 o� 4 O
;..
0 7 cQ co co co cQ cQ cQ 3 -1 \ O o � cQ cD -• °
c0) ° — r
C w —
21
m 3 v0
�0;;�2
40 Al Z w Cn�>u2i 3a2i ,Q�7p cNn
C, D o
Dm + (DCl) o
O0° 0zz
El
CD CA
CA iw0
CA
O Ln U7 O N U1 N 0 CD O` D
m y 'chit O ° O H O O ,yy 3 SD 0° C
�' z a°i �o ow w a o, m Z
ofw :C) o cQ� o m M
_ o o 0 0
o� N o w
� 0 o 8 ID El
9! �3j�3 3 3 3 2 3 9 3
to
CD
7 0 _ -p
CD
CD ►vCn"aZz��x2m�?C�C�( w>> �'
3 cD — sv 3 cQ c s¢ W sv F O '
N Co m crD 0o ° W CD o 0 3 n n CO cn D N
-
CD
CL :3 3CD O
n N3coitrn�'o�'•3``Ln a33 3o vOm
0 -' V N O= (O O O '� v At m rt
CD fD 3 ? — O
.p 3 . 3
1 0 o N ro V o v ,� C
n V O N O O V w
U1 a, m a o 0Ct c
_ d".�
:. a m 0
T i cD A CD z c z
CD c c c c 3 c 3 3 cc c c c 3 c c c s c2D � c2D Z a c
o c 3
-i
a a o z'
a=0
o
(n O mm�
a
CD
'W > z 0 O 3 CD k m? o
o �' a o a CD CO
CL
o `s' 0 x Z CD o o o Oz�
a a Q Q c Q 3- cD 70
3p O w ° (D 0 o �; W c
fD cQ cr f�D A. -0 (3. 0 c z D
IF
su CD to a O 0(Dy
CD 0
CD
Dm CDOL N m
0
o ca m -A1
N O O
(D A,
Z
N

r
0
O
3
3
CD
y
0
��
A,
0
�E�)
5F5�=
0
0
a
o
O
o
o
0
0
0
0
w
Cr
m
w
1
0_=
0
0
0
a
3
Q
0
A
o_
5.
5_
o
a
rn
w
o
o
r
2
CD
OOOOON
V.-.
wma
�
-0
-n--nn
W�u'oCDiu,
�.3
oo
i
�
C:)
Q
co
l
W
CO1I
N
W
U7
A,
N
n
j
w
1
Q
v,
o
o
•+'
rn
3
C
3
3
C
3
3
3
3
C
z
3
1
3
3
3
CO
r�l
cp
Cp
.�
co
cfl
co
tQ
O
"
A
\
0
3
3
D
p
o
c,
�Z
-iz
(nCA
0
�.
O
Z
W
A
ID
d
d
C
N
.f
A,
Al
O
A�i
CD
n'
W0
0fD
o
en
o
Z
Z
.4.
O
co
N
cn
too
QQ
rn
rn
C�Jt
o
N
v
o
i
w
my
tNno
co
v
w
v,
Z
v,
Q
c
o0
p
CA)©
o
.
0
o
9,
o
N
�
d
�
3
3
3
3
3
3
�
C
3
3
3
3
3
ro
O
fl
N
Cn
-
Z
Z
K
g
X=
�'I
n
n
C�
n
W>
D
CD
C
0-
a
w
W
Z
o
-p
°
o
o
�.
c
,
m(D
CD
o
w
w
c�0
_
C
o
0
3
:3n
v0
i
C
C
iCL
�_
-i
3
c
3
C
3
i
C
3
-�
i
0
N
3
LAV
f0
r\3
(D
C
O
O
i
C0
cn
cD
3
CO
Co
O
N
O
O
V
_
to
-4O
4
O
N
V
W
V
L
Ln
c
C
C
c
3
c
3
3
c
c
c
c
c
3
c
C
c
-�
�
>
z
0
0
`°
o
CD
o,
m
x
CD
_
m
0
0
o
CDw
C
9.0
o•
=-
3
0
A
CD
00
R.
tD
m
y
A'
CD
-
a
N
o
0
m
CD
N
to
.n.
(D
cn
D
0
°
O
�.
a
N
pCp
E
m
o
--
w
0
0'
y
-n D -i -0 -
o ?
cu
D�v-n
O
0
m �
0 o C
Dye
::3-i
D
Zv
3.
o
D
co
C
o
o
�
Co-<
Z3P
D
co
rn
3 cCf)
O
m
z
D
0-9
0
���
CD
-<
0
33
O
Kn rn
� 3 C
2(
mN
0
O
CD 0
C
G
o
°0
?:
yj
0
i
w
C7
3
c�D 0 m o 0 m
3330=CD0
a, -0 -. . 0
R�
y 3' 0* 0
�-
0 o
O N
v7
.ID
L3
L
"1%
=
0
0
r
�
co
n
,SD
Ari c ' o,.
�o
1�1 X3 T-
r
O CD
to) Z
O
W
w �
lr� W
o\�
C ?�
Z r
m rn
M
❑ m
m 0
m --I
G
m
z
n
CD
r2'o
O
iZt r� y3
c
� �t�ID*'
n, O o�v�°:.CD_ 'cr tea
r- o Z o Er
m
°�° co
a
U7 Z 0
20 �a w (D
tm
6 CD
r
C
CD
O
U4
O
�
, O
� `
O
v_
0
z
Ola
z `
C
A
00
z-
Mm
z<.z
-1 'p 0
n�?
z
s
n
mm0
K?1
m_ 0
za
a�
�zm
pc
Cm
vm
a0
m
cn N
m
-n_.i
0
z

F.
m
N
IQ
a;.
CD
go
c
SD
c�S
G
0
m
13
m
C
m
Z
C.
I'l
�o-a c -o-,G)>0 220 L CD % CD ClW CAD O o
A CD
A' CD CD
Z o a
-n -n
jT
CL
N °' A
O N F- Cii
p N O A
p O OLn
lfl
�c
33=,3333333S3 003
coca O cn (a cQ ca ca (a cQ cQ 3 3 ca
� � A � ` � � = � � N
ZKK;r,m r1C)C�ROF� !TZZ
MCC Ca CD C 3
O , , CD
3 CD
�� � m � ��'
n 3 0-A.c'32 z0
CO O C.0 3. 3 C .N o�
3`z o33 Sow n
3 �ZZ
W O N
CD
0 w 0-j
333333333333333
co cc (a cc co cc (a ca co ca co cc cc to cc
� � � = � � � �
O 0
C
CD �
Z
�C
(n
Z
-�
QQ
0 CD n
m
ol
o 0
a. CD
R✓'
�.2.
c
n<
CD
3
o
N
A
a
'CD
A
O
o
O
00
LQ Ca
c c c 3
Ca Ca to Ca
3 3
Ca
moo` (�
w CpDN 5Qr�
,z N o �i
Cry P`F
CD O 2
3 cn
3 rr
N �LW N• o w
�l w F- 3 rt
(D
ill W co -t N hj
(D � N D
Cn A � �j rF
A N _
R.
DIz
Qz
c�
CD
EAI
F o 3 f m -- �
(? a r�'
a �' 7 N
cQ cn c 'TJ co
c�
$,8
rto
5.
n
o,
w
�
r�
C
D
u'
N
F-
w�
--1
ul
w0
i
0
w
N
cn o
�
mm
o w
�o
z
voo
o
00
LTI
D
-0m
(/)
n
m
�a
m v'
0
.�
Lr
ou
m
33
z
c
K
co
m
�o
g
m
m
v

w
m
m
m
N
�
3—
_
CD
0
,
m
c
0FT
-i
C
C
m
v
C
®
O
CD
*
Z
0
LD
m
a
g
rg
N
s
°CL
.
o
C
7
Z y�
UgO
CD�CD
I
O Off' � Sn -n -n
O 15
SU c pj Q �- O -n
A �! E o
o �wcn� o
c,
0 0 00
0 Lrl
L11
33=r3333333S3 003
coca o cQ cQ cQ cQ cQ (Q co co 3 3 cQ
� � 0 � � � � — � — O _ —
zKK;rNMT OO2Ow�TZZ
�QCQ cQc�c= 8i Ef
' O (�D
> r _
sue^ CD coZZ
3Qc�.c�.2O0
31 =3 c',� �C c 3
R 3 0 3 3 n,
�3 � NZ
z
5
0
Ln 0 00
0 orn
333333333333333
to ccco(aco(oaaccco(a(QCQcococo
o
� CD
CD
Z
/)
2.0
CD
N
o
aa�
o
1
Q0
cQ
c� co cQ
cc
r0M -7
0 OCE z
cu o 70 -• r C L7 ' d .�
to �p
2 = c L p
3
co rt
Ln CD
r. 0i F—
O P o P-
CD
� n
CL
00
c (� (n M.
co _*
C rt c
Y, ch
c
o
co (D
ON -, „
00
10
w n
a �0 m
mm
N zo g
� m -0oc.
Z 000?
o
m
Ul
03
mm
o Li M
ME
v gLn
w J g
L
s z
o �
0
L
W

0
Z)7
0
N
CD
SD
to
0
(D
(h
0
O
fD
0
m
U)
m
m
a
0
M
05
C:
m
z
C:
m
Cf) U) -0 z:
-0 7 a) =O:Z—'O 0
CD 54 2D , — T) ?� � E�
Q. Rl =) Om W CD 0 —0 00
> CD 0 O- PD � �O
3 CD 0_
D M
00 0-
cn z
0
0 CD "0
ri- D
0
=r
(D
CL
00
00 C:) N) LA) Ln LA)
A
U,
C) CD
3 D 9 3 3 3 3 3 D D CD "D D
(a co 0 Qo (a CO (a (0 (a (0 (D 3 3(0
-n
CD
0
cub)
>-a cl)
Z
o o
CD
0 z
o
CD C:
u)-
CD C: 3
(1)
cD 3
O
C)
CSl
C)
O
333333333333333
0 Q 0
Z3 =
0
C CD
D
M
D.
0
CL
0L
C: C: c 3 3"3
0
c) >
a)
=3 0 CD
3
3
z
-a
K
w
CD0
Z
cn
Lrl-3
U)
3
(D
C/)
CD
C/)
C)
(D'
t
=4; CD
C) CD
rt
0 3
M
FaT 3
c:3, CD
rt
cn
(D
0 (a
Eli, a
U)
c
�6 ::,
C-D
a (Do
CD
CD
O
-n
:3 0
_0®
0
Z,
3
-P
C)
N)
0
1 c)
co
Eli
[�. 0
CD
-- a
1,00
M
0
zc
0
=5
55
z
m
9
.9
CD
co
0
0
-CR'
w
(00
lw
>
72. ?5q
0
0
A)
U)
x
-u U)
0
CD
CD
0
0
-u
m
m 70
Z Z Z
U 0 c::3
W M 0
u
o Fn* m
0
CD m
m zn c
C) Fa
C:) m
QD
z Ul
m
2
G)
O
m
0
co
a-

CD
-�a c w U)O= �, ° o p cy C' 0) CD m m
.� CD a ° O o — D° CD Q o
Z 3—_—
—I a cn o o cn a r
ci Q- ° CD
M N y �: m �° ° m m 3 3 0 aQi o cfl ° o
m 3 � Q- 0 3 .. 0
z 3 n a co < < •a (D _•
n o ° o ° o -n -n Z m� O a' m o o
m
m � �' c N a° n CD o vi r o
DO_ o CD
° a < Z C
W ° O rn 3 eJ CD N c
m D C o Pi o o
_ n W CD
C r+
� � N �•
N
® O O W -0 CD< '0 fi
En
pM co tQ O cQ tQ cQ (Q cQ cQ ?. to O O c0 n M CL 0
D O 33 O 7 rt
Mm CJ Q - N
z D z 2 -n o 0 C� C� oo D Z Z c o a
o U) W N v w
D '0 aw 'Qw :3 <cQ CD
� v �<C7 ON O — N c ".
g(=D
r
C c �OcZzQ_ cQ W - 3 a
D �7p c C: c 3 CDl .°
D3°cn M Ocm o
o 00
0
CD
Q
N °.
w c m
° o (D o
m Cn
uz
D -� Q
'D 3 S
N (0 -n -n
5 n
U) U) (D
cr
a
3 3
3 3 3 3 3
3
3
3 3 3
3
cQ
3
o
o
I I
I
�0
m-
Q
�
c '
a
�
cQ cQ
� c� cfl cQ co cQ
�
cQ cQ cfl
cQ
cQ
o
n
o �
Cl)�
d
C
c
'
0
a
a
o'
7
N
O
3
y
v_
CA
cD
fD
O
0
.
m
a
r
0
z
M
z
P
0
'G
r
z
m
M
M
0
--I
In

ari
0
:.
W a 3 �•
rfi
o
n M,
D �, o
m
O 71
°
00000
w
0
>
>
o00co
0 c-
-i
a-o
�,
m
3
w
a
o
o
Q
m'
w
w
w
p
v
n
-'
p
0
o
D m
Zt
v, '
;'
Z
m
o
o,
o
r:
CO
3
3
0
W
�•
'�
O
..
7
w
`G
`�
o
..
(Q
w
s
07
r
.c
cn
Q
v
W
N
(D
J,
°
O_
O
O
O)
W
CA)
n
0
G
N
O
N
O
O
p
O
O
CW71
P
m
O
D
x
o�O
w�
1�
�o
o
()I
N
Ww
F
D
0
,0
m
o m
W
co
O
:
() N
cn
o
fll
a
Z
n1
°o
(D
o
CD
3
c
3
3
c
3
3
'3
3
Z
3
1
1
3
3
3
o ro
v
D
-I
o
o
m
cu�
0
d 0
c3
Z
Z
c:��w
w
o
°+
(N1i
0
Z
w
=;
Mq.
C
a
a
c
p
O
ui
+
w
SD
(D
(D
::t
o
>
CD
>
CD'a
Cn
�
O
Uf
Cl)0
0
00M
N
0
s `'"
cn
0
Z
Z
(fin
'0
O
Co
N
fUl
N (n r
3
w_
N
m
a
W
o
O
o
m w cm °c�
3 3
C
CD'
O
N
(n
O
O
Al
W 0 -
oo ;� .
r
LTI
Z
Ul
(o
..... a
N �'
m
CD aw
O
O
(DEl
O
O 0
O N
.�
fD
O
°oo
ow
m
3
3
3
3
33
c
3
3
3
3
o
CD
L
-
ED
0
ro
.
o''o
o
m
00
W
m
NU)
zz
�
=mCD
�a�
wODD
�
C)7;c
N
r
Z
o
0
3
w
D
0
Q
q
ww
o°
0
a'
N
cD
D
c
0_
a�i
Z.
c
3•
m
y
o
Z o
_o
0
c'
a
0
c'
3
w
CD
�"
c
3
c
3
3
c
a
�3
0
OF,
�"m
,oc
n
N
3
0
(D
(yD
c
3
�
cn
-•
o
3
ca
O
3
o
v
;' �.
°f
w
m;
�
0
V
0
n
CD
V>
V
co
" d.
O
3 '.
O 77 r'
z C
�m
-
tv
w .w
.. r.
(D w w
=r 0 -- a
-�
mCD
21
^`
for
cp m
7c c
a o
=
c
c
c
c
3
c
3
3
c
c.c
c
c
3
c
c
c
�r
w
r3 w
vm,
(Q(fl
Ma
Cal
a
a �
2n
m
G)
0
m 01
0
1
-o
D
co
D
z
0
O
�
(D
m _S
zm=
o
cQ
a
CD
n.
o
0
w
`
w
p
a
7
o
ai
m
z
2
o
m
m
n
m
3
0,•
m
:,
O
°o
o
m
a
o
cD
s
0
:.:.
3
Q
cQ
(D
X
a°
op
#
o w
a p
w
n•
0
(D
c
CDCD
CA
w
0
w
A
a.
CD
-
M
m
m
2
0
0
a
a
�a
co
O
aN
07
o
cQ
CD
m
p
if
Z
y

r
cr D
n
3000sDDOp) Acn
CD :3a " ° °
In (D c (CD Q n j Ali
N (D � A ° O (D 0
0 CD CL � cn
x (D =
CC) N O co
CJ
�00000
�no.o 0�
n;CD0 0 r=
CD co 3 � CO
n -n w w
O-{ CD O
** n
Yt Ln
� W
4
z r:l
>
W
z
0
0
N
c
a
En
—'
9
CD
XCD
CD0
°
3
fdCr
0
3
N
m
N
o
o
C.
°
x
a
0
'0
S
N
n
CD
N
C
(n
CD
y
m
C
CS
�
CD7
C�
NW
CD
c
CL
D
Z°
o
m
U)
m
2.
°
D (D (D = O C (D
�+ m — �o a no�°ao� D:o
D.< 0� D N ° U�°
—� (n (D Z
33
m 32 0
D 0-9 u- r Cn
n n CCD
{ 0 C1Ro 0O M m
r
-na =CD 00 Z r
n 0cx o O o
m ° CD
o w v�
N ,D 0 1
O
0
f�MC0 r-0
O A) y pOp C
�- -,o.m Z
m rn
o O
U, M
ZZ :3n c� ° N
en
��3 00
-3 m � c �
o z
r n� �2`D
� � W
-4
D
in o
1 3 ,
Q
o
v
r
o
v
a�
cD
cc
C=Dra
m
z
cr
Cc
3
o
0-
cD
CD
a
CO
v_
sa
0
zo
o(o
n
m�
z3
m�
00
°.
m�
z<z
0 G
ate?
zr
mm0
m="
m_ o
� CL
z m
o=
cm
v�
w
,c
n�n
� A
N a
m
4
O
z

,,i�MIVOLATILE ORGANICS REPOR,. - DEM
LAB
LAB NUMBER:
2G563
SUPERVISOR �� ' LAB #:
2G563
DATE a
REPORTED BY
CHECKED BY
ENTERED BY
7 k—
REVIEWED BY
CHECKED BY
SAMPLE TYPE:
WATER
DILUTION FACTOR
CONC.
CAS NUMBER
TQL
ANALYTE NAME
UG/L
X 1
108-95-2
10
PHENOL
U
111-44-4
10
BIS(2-CHLOROETHYL) ETHER
U
95-57-8
10
2-CHLOROPHENOL
U
541-73-1
10
1,3-DICHLOROBENZENE
U
106-46-7
10
1,4-DICHLOROBENZENE
U
100-51-6
20
BENZYL ALCOHOL
U
95-50-1
10
1,2-DICHLOROBENZENE
U
95-48-7
10
2-METHYL PHENOL
U
108-60-1
10
BIS(2-CHLOROISOPROPYL) ETHER
U
106-44-5
10
4-METHYL PHENOL
U
621-64-7
10
N-NITROSO-DI-N-PROPYLAMINE
U
67-72-1
10
HEXACHLOROETHANE
U
98-95-3.
10
NITROBENZENE
U
78-59-1
10
ISOPHORONE
U
88-75-5
10
2-NITRO PHENOL
U
105-67-9
10
2,4-DIMETHYL PHENOL
U
65-85-0
50
BENZOIC ACID
U
111-91-1
10
BIS(2-CHLOROETHOXY) METHANE
U
120-83-2
10
2,4-DICHLORO PHENOL
U
120-82-1
10
1,2,4-TRICHLOROBENZENE
U
91-20-3
10
NAPHTHALENE
U
106-47-8
20
4-CHLOROANILINE
U
87-68-3
10
HEXACHLOROBUTADIENE
U
59-50-7
20
4-CHLORO-3-METHYL PHENOL
U
91-57-6
10
2-METHYL NAPHTHALENE
U
77-47-4
10
HEXACHLOROCYCLOPENTADIENE
U
88-06-2
10
2,4,6-TRICHLORO PHENOL
U
95-95-4
10
2,4,5-TRICHLORO PHENOL
U
91-58-7
10
2-CHLORO NAPHTHALENE
U
88-74-4
50
2-NITROANALINE
U
131-11-3
10
DIMETHYL PHTHALATE
U
208-96-8
10
ACENAPHTHYLENE
U
606-20-2
10
2,6-DINITROTOLUENE
U
99-09-2
50
3-NITROANALINE
U
83-32-9
10
ACENAPHTHENE
U
51-28-5
50
2,4-DINITRO PHENOL
U
100-02-7
50
4-NITRO PHENOL
U
132-64-9
10
DIBENZOFURAN
U
121-14-2
10
2,4-DINITROTOLUENE
U
84-66-2
10
DIETHYL PHTHALATE
U
7005-72-3
10
4-CHLOROPHENYL PHENYL ETHER
U
86-73-7
10
FLUORENE
U
100-01-6
50
4-NITROANALINE
U
- 534-52-1
50
4,6-DINITRO-2-METHYL PHENOL
U

�" , i EMIVOLATILE ORGANICS REPO)�:,,•- DEM
LAB
86-30-6
10
N-NITROSODIPHENYLAMINE
U
101-55-3
10
4-BROMOPHENYL PHENYL ETHER
U
118-74-1
10
HEXACHLOROBENZENE
U
87-86-5
50
PENTACHLORO PHENOL
U
$5-01-8
10
PHENANTHRENE
U
120-12-7
10
ANTHRACENE
U
84-74-2
10
DI-N-BUTYL PHTHALATE
U
206-44-0
10
FLUORANTHENE
U
129-00-0
10
PYRENE
U
85-68-7
10
BUTYLBENZYL PHTHALATE
U
91-94-1
20
3,3--DICHLOROBENZIDINE
U
56-55-3
10
BENZO(A)ANTHRACENE
U
218-01-9
10
CHRYSENE
U
117-81-7
10
BIS(2-ETHYLHEXYL) PHTHALATE.
U
117-84-0
10
DI-N-OCTYL PHTHALATE
U
205-99-2
10
BENZO(B)FLUORANTHENE
U
207-08-9
10
BENZO(K)FLUORANTHENE
U
50-32-8
10
BENZO(A)PYRENE
U
193-39-5
10
INDENO(1,2,3-CD)PYRENE
U
53-70-3
10
DIBENZO(A,H)ANTHRACENE
U
191-24-2
10
BENZO(G,H,I)PERYLENE
U .
OTHER SEMIVOLATILE
ORGANICS FOR SAMPLE NUMBER
2G563
NO BASE/NEUTRAL OR
ACID EXTRACTABLE ORGANICS
DETECTED BY
GC/MS.
TQL= TARGET
QUANTITATION LIMIT
T= TENTATIVELY IDENTIFIED ESTIMATED CONCENTRATION
E= ESTIMATED CONCENTRATION
U= COMPOUND
ANALYZED FOR NOT DETECTED
N= COMPOUND
NOT ANALYZED FOR
D= DETECTED
BELOW
QUANTITATION LIMIT
H= HOLDING
TIME EXCEEDED
TQL SUBJECT
TO CHANGE DUE TO INSTRUMENT SENSITIVITY

d;pNOo)WPM L&9NW&TaPV Wa&iTILr.D AN&LVTIPiL DCPADT
- LA. 9 M. ?11563
REPORTED 8Y SUPER' SOR -
CHECKED BY DATE b
REVIEWED BY � ENTERED BY
CHECKED BY
SAMPLE TYPE. WATER ANALYSIS RESULTS
j CAS# VOA Target Compound TQL Cone
ug/L Detected M
( uq/L I
CAS* VOA Target Compound TOL Cono
ugfl. Detected MS
u iL
75-35-4 i 1-Dichloroethene
0.75
U
96-18-4
i 2 3-Trichloro ro ane
0.25
U
75-09-2Methylene Chloride
0,25
U
108-86-1 18ramobenzene
1
U
156-60-5 trans-1 .,2-Dichloroethene
0.75
U
95-49-8
2-Chlorotoluene
0.25
U
75-34-3 1 1-Dichloroethane
590-20-7 2 ,2-Dichlor ro ane 10.25
0.25
U
U
106-43-4
541-73-1
4-Chiarataluena
1 3-Dichlorobenzene
0.25
0.25
U
U
1 156-59-4
cis-1 2-Dichloroethene
0.251
i
U
106-46-7
1 4-Dichlorobenzene
0.25
U
67-66-3 Chloroform
0 5
U
95-50-1
1 2-Dichlorobenzene
0.25
U
I 74-97-516romochloromethane
0.75
U
96-12-8
1 2-Dib-ro-mo--3-Chloro rc ane
1
U
71-5
563-58-6
richloroethane
1 1-Dichloro ro ene
0.251
0 =�
U 1
U
1
120-82-1
87-68-3
1 2 4-Trichlorobenzene
Hexachlorobutadiene
0.25
0.25
U
U
56-23-51
Carbon Tetrachloride 10.75
U
87-61-6
1 .2 3-Trichlorobenzene
0.75
U
107-06-2
i 2-Dichioroethane
0.25
U
1634-04-4
Me# l-tert-but 1 ether
5
U
79-01-+6
Trichloroe#hene
0.25
U
71-43-2
Benzene
i
U
78-87-5i1
2-Dichior ro ane
0.25
U
108-88-3
Toluene
1
U
75-27-4
Bromodichloromethane
0251
U
100-41-4
Ethyl benzene
i
U
74-95-3
Dibromome#hane
1
U
108-38-3
M,P-Xylenes
1
U
0061-01-5
cis-1 3-Dichloro ro ene
0.25
U
95-47-6
o-Xy lene
1
U
0061-02-6
trans-1 3-Dichloro r 'ene
0.25
U
100-42-51
Styrene
1
U
79-00-5
1,1 .2-Trichloroethane
0.25
U
98-82-8
Is opylbenzene
1
U
127-18-4
Tetrachloroethene
025
U
1
103-65-1
n-Propylbenzene,
1
U
142-28-9
1 3-Dichloro ro ane
0.251
U
I
108-67-5
1 3 5-Trimeth lbenzene
1
U
I 124-48-11
Dibromochloromethane
0.75
U
1
98-06-61
tert-Bute lbenzene
1
I U
1
i 06-93-4
1 2-Dibromoethane
i
U
95-r,3-6
1 2 4-Trimeth lbenzene
1
U
108-90-7
1 Chlorobenzene
02:151
U
1
135-98-8
sec -But ]benzene
1
U
630-20-a
1,1 1-Tetrachioroethane
0.25
U
99-87-6
- Iso a ltoluene
i
U
75-25--2
7'9-3�t-5
Bramofarm
1 1 ,1 ,2 ,2-Tetra chloraethane
0.5
0.75
U
U
104-51-8
91-20-3
n-But lbenzene
Na thalene
1
1
^-
U
U
TQL- target quantitation limit Other purgeables (up to 10 highest peaks) Detected
T- tentatively identified compound ug/L
E- estimated value NO VOLATILE ORGANIC COMPOUNDS DETECTED BY GCIELCDIPID.
11- compowui was analyzed for but
not detected
N- not analyzed for this compound
D- detected below quan#itation limit
MS- X=GC1MS analysis performed
TQL subject to change due to instrument sensitivity
COMMENTS:

ar6veiALuA-4-er, A4'vti;4-or4*en -i�l 'Z4,-n A,r, 40L A CL
ODM,, Rec..e:v,,L
pa V-4Z r-A c4e
P"I SA
tjwe-(l d� ;2- 7
IV d e 3 L? C/ UC� �4
7-�2x
oz) 4,20
to
j����/�� ,�/�EICa � r�2r /fist`/�s l�� � ���r„ �2 f Jdv�
Oe
3 j�3
f Ivi,
Owe rZ,
cet,
jW T

m
1
�aG -0(D1'Dn0o�c
(D
®-�-vZPo 9
�? =
�
O
CD
0. OC0D OMA
CisO 0 0
z>0(DOCDkv
g��3
v -�Q- ooa'
n-
Q- ® O OOsi
0~..0
0 'n
Q
O
vi
Ow
s
N F- �r
ON O
CL
N N NNWNN�
N
\
ON V N :-I
O 03 to
F`
3353333333S3
603
(aaa OCQ(c(Q(a(a(aCn
0 ��..�` ��0
,..o-� 3 3cn
e
0
ZKKXMMOOROw>-oZZ
CO CD
fy O CO ' C
' O
CD
KO Ko �3 (70
CD
o Z
�cQ
�-0 3 Q-�2•-3.
5.2 ZO
�ZZ
0
0
r•'
m
'v
r-
r-
N
N
N
N
N
N
333333333333333
�(n(�co(O(OCQ��cQCO�(�(OeO
� � zzt
�0
CDcn
�'m��Z
o 2
0m^
n.NrZ
Cn
06.
O. CD n
A C2 (D
S
ro
0-;0)
3
c
n
o
o CD
� c
C
O
O
(D
n
N
a
o•O
c
CD
Oo
�
N
CT
N
N'� CCc
1333
N (O CO CO
CO CO CO
r.c)yy
gao
0 cQ O
* m
zy�`S
w
o
3n -0
��
No
v
CD o
CD
�j•Z
3
a
�
P.
c3
�
4-
(D
rr�
N
N
�•
N
3
00-0.
rt
F
N
N�
CD
10
c r
fD
R
o'
C
0 33
v
j aCD�
in c) CO Cnv � CDct
:3pp
(�
(p
cD p
~ O
O�
3
(3
H
O -0 O
N
3
(D
0
'n
.. .Tln
Ft
P.
(D O
¢n
Ft
0
ri
Q
CD'
a
W ?
�o
0
mm
�
H
I
r
Z
3
ID
m
p
o
(D
0
O
(DD
yr
o
w m
m
C)
a
o
(D
4
tf
Z
m
zzi
O
-p (n
w
o
(D
f
P)
rt
�
(D
TI
n
Q z
m
95) CD
Gd
x
IV
Q
m
ZZ
0 0 C
mpg.
�m'm
A
nCD m
O C
N m
v-i m

EE S engineering and environmental services
April 16, 1992
Ms. Sherry Phillips
North Carolina DEM
Groundwater Section
P O Box 29535
Raleigh, NC 27626-0535
Dear Ms. Phillips:
AN
io�sa`
SECTiori
tic
Engineering and Environmental Services is submitting the February, 1992
groundwater sampling and testing results on behalf of the Huffinan
Finishing Company for their NPDES Permit No. NC 0025135.
Groundwater samples were collected from monitoring wells upgradient (MW-2)
and downgradient (MW-3) of the wastewater treatment plant on February 21,
1992. North Carolina DEM Form GW-59 and the laboratory reports are
attached.
If you have any questions regarding the enclosed materials please call Keith
Seramur or Ron Bannister at [phone].
Sincerely,
Keith C. Seramur, P.G.
Engineering and Environmental Services
KCS:alb
Enclosures
cc: Mr. Lee T. Huffman
Huffman Finishing Co.
Ms. Kay Dechant
North Carolina DEM
R
A
Post Office 3009 [phone]
Hickory, NC 28603

IMP
CLIENT: _ Engineering a##!1
DATE RECEIVED February a 1992
DATE REPORTS 1-11a ch 1 1 i_2
DATE REPORTED: 7 t+�! �•ii # L_ 1 � _ i
DATE E REISSUED: April. t, 1 3~y
5A 1PLE INUR ER 5AnE l= DESCRIPTInN
+--- -
Winter; iO4 5 a. i 1-92 0 0v 733I COD.
2` 2-:-i302B
W;-j -ter; 9 1075-2-2 j -92-#Li03 for r ice
rt r` \Ti•r
.' 2-�' 02C
7,t_} {•,a �T� Fk r-!i +1 Tf r t +4
it` Q f.er ; `: 1 075-2-2 1 -` 2-'L 03 o N ii.
02•-302D
9 j tY , 5-2; -9:?—tic E3, for Orthophosphate.
202-0302
Water, 91075-2-21-1--42-003 for pH & TDS.
202-i 30 6
Water; 910E 5-2-21-92- 0 4 for CA.
.202-0302H
Water,
9 10 5-2-21-92-003 for SOT
,
202-03021
Water; ater; 91075-2- 1-92-003 for As Cu, Zr! Na-
2Sv;2-r►v02J
` titer; 91075-2-21-9 2-003 for TO .
PARAMETER
a �y
all 13
��® r"
4 F�
RESULTS 11p1w DATE STARTED
320
202-03Q2B - TOC 26.1 0.10 Mg/1 3/6/92
202-0302C - NH3N 0.50 mg/1 2/26 92
Ccncentratiun3 acre below Minimum Quantification Limit except %where noted.
NC Laboratory Certfflcate No_ Z75_

PARAMETER
RESULTS
rip 1M
E a 4 T 1 � SUF AAA V?TJ rEEAD
202-0302D -
Orthophosphate
•
1105
mg/I
2/21/92
202-0302E-
NO3
2/25/92
202-0302F
p H
5.5 8::
0. Q 1
su
2/21/92
TDS
435
1
RT/I
2/2B/92
202-03026
CI
270
0. i
Mg/l
2/27/92
202-0302H s
604
103
1
UT
2/27/92
202-073021
As
0.0 0 73
0.001
Inn
2/21/92
-
cu
0067
U01
Mg/l
2/21/92
-
Zn
U4
0.01
Mg/I
2/21//92
-
Na
91
al
Mg/I
/22.6
2
202-0302i -
T O.c,
0.094
(0.0 i 0
mg/]**
3/1"€/92
** NOTE: Reissued due to typographical error for TOX IIQL value.
z2�
--)
REPORTED BY:
D- R- Wessingyr
- General Manager
Concentrations are below Minimum Quantification Limit except where noted.
HC Laboratory Certificate No- Z75-

WELL NO.: K72g3 HUFFMAN FINISHING COMPANY
COUNTY: CALDWELL
DATE SAMPLED
ALKALINITY,TO pH 4.5
ALKALINITY,TO pH 8.3
ALUMINUM
ARSENIC
0, 010
e 0. 0,2 0
0, 0loq
c o 0,2
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
CHROMIUM,TOTAL
COBALT
COD
c ao. c�
c a0,0
Dt>(
o
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
c 0. 05'0
c 0.0.2 _5
0.0
c 0, 0:z 0
CYANIDE
DISSOLVED SOLIDS
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
L p.
L 0. 5�
NITROGEN, KJELDAHL
NITRATE & NITRITE
°
"� •
p,
Nao• as�
ORGANIC SCAN
ORTHOPHOSPHATE
PHENOLS
PHOSPHORUS, TOTAL
POTASSIUM
SELENIUM
SILVER
SODIUM
!
/,2, 3
/0
RR
SPECIF. CONDUCTANCE
511
J�0
179
SULFATE
q, .6
9.1717
9i
9,71
TOC (UNFILTERED)
0. 50
0 • ✓
U
0-s-if
TOX
TSS
VOC
4-7-7--4c-i4eO
ZINC
0. o,2o
0. U 3,;Z
o. o-f%
40,020
STATIC WATER LEVEL
'
1
'
Red Ink=Sample taken by facility

WELL NO.: K72g3 HUFFMAN FINISHING COMPANY
DATE SAMPLED
(-/ -01
- a-0
11--/ -a
ALKALINITY,TO pH 4:5
ALKALINITY,TO pH 8.3
ALUMINUM
ARSENIC
0.01ou40,0,o40,00g
0,oio
0. oil
)k
0.0,25
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
�j
`i• g
9. O
6.0
12.5'
30
�
CHROMIUM,TOTAL
COBALT
COD
, .` o. o
- .20. 0
,c 2®-o
-:5 -
<.xo. o
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
0 0 0
O. 0
d, 00-6,
0, 610 y'
.: D. ®;Z6
o. o 0,2 9
e 0. 0,2!
CYANIDE
DISSOLVED SOLIDS
60
17.2, 0
l a7
39.0
9 6
60.0
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
M BAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
0, os o
< C9. 5
t o .
4 0 t
c 0..
o, 0,7- u
< 0. S'
NITROGEN, KJELDAHL
NITRATE &NITRITE
/, U
ORGANIC SCAN
ORTHOPHOSPHATE
p H
.
.red
�o•0,2-
PHENOLS
PHOSPHORUS, TOTAL
0 '80
POTASSIUM
SELENIUM
SILVER
SODIUM
zo
! 0
0.44
/ < //
/ 3' 4
SPECIF. CONDUCTANCE
15 . 5
73
SULFATE
5~C/
�,,. /7
.c 5, t�
< S .O
�.s
u
//.
TOC (UNFILTERED)
s"
0 . 6 7
/. *2.
�_ O® D
Q, �0
S �(
-0-so
TOX
TSS
VOC
c S
v.s
ZINC
0,034
oj
0. 007
0, 0'Y-
0.00
STATIC WATER LEVEL
9, 9 "
/ U
q
f9
1
T r
8
Red Ink=Sample taken by facility
* LA8 ERP-oe- :RF-Pop-r--.ra )/v6-rEAd oF' �RStNiC

DATE SAMPLED
ALKALINITY, TO pl 14.5
ALKALINITY,TO PH 8.3
ALUMINUM
ARSENIC
c®.ovS'
c 0.010
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
CHROMIUM, TOTAL
COBALT
COD
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
0. UO F
0, vv s'
CYANIDE
DISSOLVED SOLIDS
'
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM

DATE SAMPLEll
MI3AS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
0,
9a,
NITROGEN, KJELDAI-1L
NITRATE & NrTRITE
N�3
1vv�
ORGANIC SCAN
1)11
6.
Il IENOLS
Pl-IOSPHORUS, TOTAL
I'OTASSIUM
SELENIUM
SILVER
SODIUM
960
1l 7
SPECIF. CONDUCTANCE
SULFATE
G.6,1-
�.
TOC (UNFILTERED)
TOX
Tss
VOC
1D.5ug i
ZINC
<0. 0/0
• /J l
STATIC WATER LEVEL
Reel Ink = Sample taken by facility

WELL NO.
MN
COUNTY: C4 L z) VIL:: L L
DATE SAMPLED
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
e 0. 0 1
< 0. 006-
0. 00 6�-
L 0. 0 1
e 0, oot;'
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
•
'TI-6
lo.
/0-0
CHROMIUM, TOTAL
COBALT
COD
.3
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
00
00
0. 00 7
0.
•o 1.5-
CYANIDE
DISSOLVED SOLIDS
C'
6.-
S:2
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
jxvu juliK = aampie YaKen by iaciiity

COUNTY: C A L 0 v6 1. L_--
DATE SAMPLED
3-10-00i-/y-
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
0 . / 6
0.03
< 0.
L 0. ®L
< 0.5
NITROGEN, KJELDAHL
NITRATE &NITRITE
®. (�
®. "�
SO
�3:
�. D. C� 1
0.76
ORGANIC SCAN
PHENOLS
PHOSPHORUS, TOTAL
0, ;,2, /
0 , /, 2
POTASSIUM
SELENIUM
SILVER
SODIUM
SPECIF. CONDUCTANCE
SULFATE
6. All
7
7- O !
TOC (UNFILTERED)
�,
/ , &
/ ,
TOX
.40 • o / o
TSS
V OCT7acN
E
En
NE.ET
ZINC
®. Q
0. UO 6
4- 0,
0. 0,2 7
l?• o
0. 0,15
op- -rao PNpsP/ A%
C 0, d ®L0P
1p
4 0 .s,
t 0, 0
STATIC WATER LEVEL
17,6s
g, C
9,
g ,
O 6s
Red Ink = Mmple taken by facility

M v�
AI
WELL NO. K U a 3 COUNTY: C A
DATE SAMPLED
r/- /�-
.3- r1 8
G H ..
74- 19
i/- y- y j
I- icy- ` 7
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
0, v®S
< 0, 005
0 , 0 J
t 0. 00�
4 0.005
z 0. 4 o
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
1, 7
3 . !
3
e
Y. 5.1
lk ki"
CHROMIUM, TOTAL
COBALT
COD�..t
o.. o
al. ®
� D. O
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
0. 0 04
0, 00 6'
00,A
® . 00-4
0. oo 9
O. 0-0 7
CYANIDE
DISSOLVED SOLIDS
/ o
/ O A 0
I A 7
10,0
73".
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
nea inx = 6ample taken by facility

COUNTY: CA L O W t,
DATE SAMPLED
it-
Il - gs
6 - i - i
- ff - `v a/v-
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
.
�F r?
Oe 0,5
0.
o
NITROGEN, KJELDAHL
NITRATE & NITRITE
NV
N�
N/�3
6
/7e0)3'a
N0 I
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS. TOTAL
o O5'
POTASSIUM
SELENIUM
SILVER
SODIUMr
SPECIF. CONDUCTANCE
FATE
PTOC
(UNFILTERED)
/ , 6
J, g
!J� 1
o
TOX
o.19
TSS
VOC
L3oL-
�
ZINC '
0. 017
0-0/0
0. O5-6'
0- 00&
o, it
0 e -T f-t o f 1-10-s f1f A-r6
C> a (?
0` U 7
o' o g`
` o./ o '4
o' O
STATIC WATER LEVEL
Red Ink = Camnln taL-a., h., Fo r•;i;
(.� ,r
tom,
I
®
�� j r
, 0 '

WELL NO. rI C
COUNTY: GA L -0 lot![_ t - L
DATE SAMPLED
C p- / 7- ` 6
7-
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
e 0. 010
.40. 00.6
0, 0/0
0.007
< 0.0/0
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
//r.z
.3/•
91,�
CHROMIUM, TOTAL
COBALT
COD
G 0
Y ?, .a.
0. o
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
0, 00,,23
0,00
0. 0/,?
0. 0"7
p.®®cG
0.003
CYANIDE
DISSOLVED SOLIDS
% (0 0
14,0
7, 0
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

WELL NO.
COUNTY: G 1 [- 0 VV C= L L
DATE SAMPLED
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AMMONIA
c 0, 0)
-4 0- 3r
4 0 , �'
� �r �
< 0. 01
. � , �-
NITROGEN, KJELDAHL
NITRATE &NITRITE
i•®
N°3
c�•&A
N�3
Q,/1
M03
0.6,
0,9&
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS, TOTAL
0. 0.2
d. o;
POTASSIUM
SELENIUM
SILVER
SODIUM
37
%
7A
Z2
.3 A
30,
SPECIF. CONDUCTANCE
SULFATE
TOC (UNFILTERED)
1 /, ®�
TOX
TSS
VOC
< o, oac's`
ZINC
.40.010
0.t7J4
0.
0,o1
®.D
®. o®.y
R7-ND 19905P#14
d
0.31
0, /
0. 1
STATIC WATER LEVEL,
l.0lift - oa,npie Laxen Dy iacuiry

CAL®We-_LL--
DATE SAMPLED
.,3-,73�-`J.5ALIALINITY,
TO i�H 4.FF
ALKALINITY, TO pH 8.3
ALL?�1INUM
ARSENIC
C�. !�!✓']
(�.
t 0. ®/
®• c� /i"
t7 a �?/'
BARIUM
BERYLLIUM
BICARBONATE
—
CAD`iIUM
-
CALCIUM
--
-
CARBONATE
_
CHLORIDE
2
- ✓
% �o
/ ,3. I
`�
_ % 7 e
CHROMIUM, TOTAL
---
COBALT
14,
COD
COLIFORM, FECAL
_--
—
COL TFOR_M, TOTAL:
- --
---
Q 0/0
u1l
�.
CYANTDE
—
DISSOLVED SOL:I.P.S
%
-
Al-
g
FLUORIDE
-- —
--_..
-
--
—�
--
HARDNESS Ct?Co
—
-----
I ---
HARDNESS. NON -CARBONATE
------
-..-__--
IRON
LEAD
LITHIL?i
_---
----
—
Red Ink = Sample taken by facility
,f 0% i O" I M M} i f4 m iY'f U/-- F-A,3

DATE SAMPLED
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
NITROGEN, AW10NIA
a, 6,
C)
4 �• `.�
� �' ��
NITROGEN, Y:JELDAHL
_
NITRATE & NITRITE
IV03
0
/V03
(),30
0 • 30
/V03
0 _/ ®
A10-5
o , 33
/VO3
% • �
ORGANIC SCAN
PHENIOLS
PHOSPHORUS, TOTAL
POTASSIUM
SELENIUM
SILVER
SODIUM
` . 5�
-q
- 0
SPECIFIC CONDUCTANCE
_
_
SULFATE
TOC (UNFILTERED)
%_
S
L
r° 7
`
TOv,
(� . u //
_
c� • C) t) 7 7
TSS
ZINC
0.03
y 1 A
STATIC WATER LEVEL

NO.
DATE SAMPLED
Go ' �' /� 3
%' % - 9-3
/ j -3_ i -3
---��—
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
0 r 6
fi a
4 0 ° tS i C%
< O• �
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
CHROMIUM, TOTAL
COBALT
COD
a O
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
V . G'/�,
O- O '
C < C;>.,g
, '
®. 00
C! • O
CYANIDE
DISSOLVED SOLIDS
FLUORIDE
HARDNESS CaCa,
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

! ,? 3
\COUNTY C
DATE SAMPLED
G �_ � 3
�- , � `1
/1- 3 - i3
MBAS
C
I
MAGNESIUM
MANGANESE
MERCURY
NICI:EL
NITROGEN, AMMONIA
., (
d • S
.� U ,
p <
,
NITROGEN, KJELDAHL
NITRATE & NITRITE
G�• i
U •�
P.
F
ORGANIC SCAN
PH
r
PHENOLS
PHOSPHORUS, TOTAL
�'
o
POTASSIUM
SELENIUM
SILVER
SODIUM
, c / %
%, 0
J
SPECIFIC CONDUCTANCE
SULFATE
C
,t 3, 3
taE,
TOC ( UNFILTERED).
TO,.
C�
TSS
VOC
ZINC
. G%- -
0 , US"6
o' C�'��i
• 4'
STATIC WATER I.E17EL,

DATE SAMPLED
12".2 l - `i,7,
.67-
1.E q.
v/- / 7- `3:2
,./ 13, ,
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALIIMINLI`i
ARSENIC
0 003
Q . O / ®
c U. l.�Us'
0- 007
�. !�, t7C?5
O, 0
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
-% ®
CHROMIUM, TOTAL
COBALT
COD
O
7,2,
COLIFORM,'FECAL
COLIFORM, TOTAL
COPPER
0. 0; /
0. 003
V., 0,)t,
[ 0. a 0
0, os-
CYANIDE
DISSOLVED SOLIDS
x74
FLUORIDE
HARDNESS CaCo
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by facility

DATE SAMPLED
2 _ a
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICI:EL
NITROGEN, AMMONIA
•� 0 • �®
i7• C9 0%
C �• %
1 /r i�
.t / . O
�. Q r S
NITROGEN, KJELDAHL
NITRATE & NITRITE
A/03
o . 6,24
A303
0.30
MO3
J ®i
--i
f
ORGANIC SCAN
pHg�-��
PHENOLS
{
PHOSPHORUS, TOTAL
0.01
0• 67
POTASSIUM
SELENIUM
SILVER
SODIUM
43
3
„3 l•
©. ��
16, y
SPECIFIC CONDUCTANCE
SULFATE
103
(>
• 0
J.
"% O
r ,
TOC ( UNFILTERED)
°y
f•
TOX
0.OR
TSS
voC
N D
ZINC
0,
o- a /
O. 06-
0,
OR 7"H ® P 1-/o SP1414- TE
12
0
13/VA ORCAA)l cs
ND
STATIC WATER LEVEL
%� . �'
D ��
�' fJ J

DATE SAMPLED
v O G
u�/t
Lu-6I'C
0a3
©.g
ETHyL 13CArz EME
0.6
To -r4l- X L-eme s
c .
1tf -r14j 4eAO'4F LNGo.�it�L
3. G

-i -i co Cn -T) Q -i'D ❑ z C) C7 C)
ZW CDC 0 0 0-O=Cn.m 00 Q
n W C M
O p C_ _'. O C O O❑
(n n cD — CD n C c('D C: m 33 m
z3o = =ate.... m
�.:3 Q = o m � -n Icn
m� U) `z°'
N Cl)a 0 oCD
CD m
n 0-
CD
to
=r -%
.¢ O
3
CD
�-o 00 .O rn
Cb OOl• m (Vw
J • Ul O v O
O O dA N
m
N V CD CD
m
A
-5-3 3 3 3 3 3 cS 3 003
CO CO O (o (o (O (n CO (O —•(O (p IDN ������� 3 3 a
c
��T.=�C7C�C)C�a7DQ�ZZ �
�(n (OCDC=ra(vCo-4.� �3
�o C)3.p0coDD� cp cD
tv O W 0 C O C W m WM C C- ?
3aD0o -00— 3•pozZ
N COD C o '' C 3 C � O
c w
CD 3 U_� CD O cn C/)
�u z Z
pcn
"D
Z
O
YI w
o, C) -,
b I cn a
3 3 3 3 3.3 3 3 3 3 3 3 3 3 3
cn cn (n (Q (n c0 aD (a (a (a (a (o (a (n cn n
cD
a
<�in O cn0DN-�ZI
CD M
Da � ZCo U)
nC� CD CD
� (n "z —
CL a o p
,)3 D
.. Q n o
3 3 3 (n a a
CD CD N � Cn N
x• _
CLaa DCL
v� � � r d C� p n n
n n u :3 C)
z m �` � (n
rno�.� w
jti __. co (Q cn c0

,cARCii & ANAI,yTICA�
L_AbORATOR1 f , INC.
Analytical/Process Consultations
1
temtca Analysts for Selected raratneters and Water Sample Identified as Huffinan Finishing
Water Tech Labs Inc Proiect c ll t 'I In N
o ec e ovember 2003)
Volatile Organics
Quantitation
MW02
MW03
EPA Method 6210 D
Limit
Parameter
I,l-Dichloroethane
0.5
BQL
BQL
2,2-Dichloropropane
0.5
BQL
BQL
Chloroform
0.5
BQL
BQL
1,1,1-Trichloroethane
0.5
BQL
BQL
1, 1 -Dichloropropene
0.5
BQL
BQL
Carbon Tetrachloride
0.5
BQL
BQL
Benzene
0.5
BQL
BQL
1,2-Dichloroethane
0.5
BQL
BQL
Trichloroethene
M
BQL
BQL
1,2-Dichloropropane
0.5
BQL
BQL
Dibromomethane
0.5
BQL
BQL
Toluene
0.5
0.9
0.8
1,1,2-Trichloroethane
0.5
BQL
BQL
1,3-Dichloropropane
0.5
BQL
BQL
Tetrachloroethene
0.5
BQL
BQL
1, 1, 1,2-Tetrachloroethane
0.5
BQL
BQL
I.1,2,2-Tetrachloroethane
0.5
BQL
BQL
1,2,3-Trichloropropane
0.5
BQL
BQL
Hexachlorobutadiene
0.5
BQL
BQL
Bromobenzene
0.5
BQL
BQL
Ethylbenzene
0.5
0.9
0.6
Styrene
0.5
BQL
BQL
Bromoform
0.5
BQL
BQL
p-isopropyltoluene
0.5
BQL
BQL
N-Butylbenzene
0.5
BQL
BQL
Naphthalene
0.5
BOL
BQL
1.3,5-Tri methyl benzene
0.5
BQL
BQL
1,2,4-Trimethylbenzene
0.5
BQL
BQL
1,2,4-Trichlorobenzene
0.5
BQL
BQL
1,2,3-Trichlorobenzene
0.5
BQL
BQL
Chlorobenzene
0.5
BQL
BQL
2-Chlorotoluene
0.5
BQL
BQL
4-Chlorotoluene
Q.5
BQL
BQL
Tert-Butylbenzene
0.5
BQL
BQL
Sec -Butyl benzene
0.5
BQL
BQL
1,4-Dichlorobenzene
0.5
BQL
BQL
1,2-Dichlorobenzene
0.5
BQL
BQL
Total \ylenes
0.5
0.8
0.6
I-Propylbenzene
0.5
BQL
BQL
N-Propylbenzene
0.5
BQL
BQL
1,3-Dichlorobenzene
0.5
BQL
BQL
Dibromochloromethane
0.5
BQL
BQL
Dichloroditluoromethane
0.5
BQL
BQL
Chloromethane
0.5
BQL
BQL
Vinyl Chloride
0.5
BQL
BQL
Bromomethane
0.5
BQL
BQL
Chloroethane
0.5
BQL
BQL
Trichlorofluoromethane
0.5
BQL
BQL
1,1-Dichloroethene
0.5
BQL
BQL
Methylene Chloride
0.5
3.8
3.0
Trans-1,2-Dichloroethene
0.5
BQL
BQL
Cis-1,2-Dichloroethene
0.5
BQL
BQL
Bromodichloromethane
0.5
BQL
BQL
Bromochloromethane
0.5
BQL
BQL
Cis-1,3-Dichloropropene
0.5
BQL
BQL
Trans-1,3-Dichloropropene
0.5
BOL-
BQL,
Methyl-Tert-Butyl ether (MTBE)
0.5
BQL
BQL
Isopropyl ether (IPE).
0.5
BQL
BQL
Dilution Factor
I
I
Sample Number
490827
490828
Sample Date .
11/10/03
11/10/03
Sample Time (hrs)
0750
0830
Sample Analyzed
11/18/03
11/18/03
Time Analyzed
2332
2056
B L =
Q Below Quanntation Llmrts,
ppb = parts per billion

x
x
x
nnn
�n>>
a
zG
`'nn000
m
A
O
K
D
x
x
a
H
M
°'
a
N
0.
a.
�
�
c
C
N
O
C
x
x
x
x
IV
z
z
o
o
N
o
M
N
x
d
R.
0
c.
CL
°
;(nf1
0.
d..
+
m
m
C
CL
N
n
y
m.
y
a'
O
H
ZZM
n
V
W
n
0
W
N
�^
y
a
o
N
o
O
o
00
Ln
A
Ln
co
r
r
r
r
r
r
r
r
r
r
r
r
y
r
r
r
r
r
\
x
I
x
x
x
z?"x�
d
nna�
c
d
N
va
o
a
°
Q.
Y.
G
rp
oCoC
M
7
G
p°p
G
C
G
&
rn
C
ol
�
N
oo
,'p.
0,V
a,
'
VNi
N
ol
N
00
N
O
N
V
V
O
V
N
<
p
V
~
O
C
C
G
C
C
G-
G
C
G
G
G
G
G
G
C
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
A o
r
m
a o"
ac
.�
0..
08
O
v
K
y
a
a
>
�zO
IN n
►C
x
x
x'.
P.
°
o�
d
d
o
„
M
R
Qn
z
z>
ra
N
0
Q
0 0
❑
`O
<
W
n
p
z
o
y
C
a
m � c
A H
z
< G
-00 A.
0. :°.
l7 r+
No
o .,
a00
w
G
�w�

W
'IC'?
^
0
o (^
70
c p o
i N
On
h
2
W
c
0
l a
D
rn
N
v
O
0
p
c
o W D
0
� v
a o !?
!0 O
N
0 h
c p
Z
o
o O
s
N O
N
O = N
�°
co P z
v
o
m
t,
a
v
O
m
—
o
s
Q i
v
� O
n �
0
w
V
O
C
R
�
y
O
d
a
^.rn
0
0
3 0
O
^
O a
0
Z
5
co
O-
x
<C
V
C
p
to
O
C
{
to
f0
Q
�
�
V
v
v p;o a r
^
c
p
m A
G�

NC DENR/DWQ Chemistry Laboratory
Sample Anomaly Report (SAR),;.,.
Report to: ARO
Lab Number:
3G1189
Sample ID:
3
Station Location:
Huffman Finish
County:
Caldwell Region:
Sample Type:
Water
Priority:
Routine Collector:
Date collected:
8/19/03
Date received:
8/21/03 Date analyzed:
Affected Parameter(s):
Oaic ��
Z yam,
Analytical Area (check one):
❑ WCH ❑X METALS
❑ NUT ❑ MICRO
The following anomalies occurred (check all that apply):
Samples
Improper container used
VOA vials with headspace
Sulfide samples with headspace
Samples not received, but listed on fieldsheet
Samples received, but not listed on fieldsheet
Mislabeled as to tests, preservatives, etc.
Holding time expired
Prior to receipt in lab
After receipt in lab
Insufficient quantity for analysis
Sample exhibits gross non -homogeneity
Sample not chemically preserved properly
pH out of range (record pH):
Improper chemical
Residual chlorine present in sample
Color interference
Heavy emulsion formed during extraction
Sample bottle broken in lab - no reportable results
Other (specify):
❑ VOA
❑ PEST
Metals Form RWB 0:
r. Minnick
V 0 / 03
GS
❑ SVOA
uality Control
Instrument failure - no reportable results
Analyst error - no reportable results
Surrogates
None added
Recovery outside acceptance limits
like recovery
None added
Recovery outside acceptance limits
Failed to meet criteria for precision
Internal standards
Blank contamination
QC data reported outside of controls (i.e. QCS, LCS)
Incorrect procedure used
SOP intentionally modified with QA and Branch Head approval
Invalid instrument calibration
Elevated detection limits due to
Insufficient sample volume
Comments: Zinc concentration for LRB is 29 µg/L for associated sample. Value of LRB is NOT subtracted from sample value.
Corrective Action:
Samples were rejected by DWQ Lab. Authorized by: Date:
Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
Sample(s) on hold until:
x I Sample reported with qualification. Data qualification code used: V
-Jj Other (explain):
Notification Required (check one)?
Person Contacted:
Lead Chemist Review (initial):
❑ BIOCHEM
❑ METALS
anch Head Review (initial
gA/QC Review (init' 1):
QATormsVAomtory\SAR
Yes ❑ NoIIIIII
Form Completed by:
El PE,1
❑ VO E U V E
L.1 47 .
Date:
Date:
❑ SVOA
Logged into database by (initial)_
06112/03RWB
GROU":OVVATLER SECTION
ASI EVILi_F REGIONIAL OFFICE

w
O
mm
0
F
co
c>
w
0
0 O
O
O
O
o
o
a°
0
3
3
F
C
3
O.
N.pp..
�
o
o
ti
--n
W
A
.
(m
pJ.
-1
-n
O
=
co
=
N
a
o�
�
P
�
P
w
N
LM
W
(31
N
Ul
W
W
O
cn
o
w
Cn
o
9
n
C
c
�U3
3
3
a
3
k
3
l\
3
l:)
3
l�
c
3
l0�
Z
3
(�
�3
uz)
3
3
uz
-
_
y
C
_
o
3
x
Z
-i
Z
O
O
(n
cn
'0
S
S
"n
a
�
pp
CL
O
Z
Z
C'tl
'D
0
w
N
(yn
a
O.
Q�
G
3
J
j
Ul
y
rn
Z
O
3
c
O
W
U1
o
n
°
0
O
O
00
O
s
O
N
hi
n
m
3
3
3
3
3
3
3
c
3
3
3
3
_
—
—
-
3
(0
P O u
O m A
y
`�
O
a <
O T
n
OD
U1
f0
n
0
�
P
I
I
-
I
-
lill.
-
N
U)
IT
Z
Z
3
?
7c
2
(°
-n(l
N
C
n
,
n
P_
n
P
w
P
D
y
a
-
a
(O
3
3(
l0
Z
P
3-
o
�s
,
H
fl
o
o
Y
In
o
o
o
o,
c
307
o.
°
to
c
c
c
cLn
3
n
3
rn
v
rn
v
rn
J.
�
u
Urn
p
(n
(n
C71
4.
cn
Ln
Q
w
rn
N
°`
(m
u
(�ii
N
cn
cn
.�..
rn cn
rn
G,
LM
c
(o
c
(o
c
(o
c
(o
3
c
m10
3
3
le
c
c
c
c
c
(o
3
c
c
c
c
S
S
o
2
3
o
1O
P
o
m
o_
o
y
_+
s
x
�
to
-
�i
A
y
o
O
y
y
n
0.
�
N
W
0.
O
N
d
p l0
o Cl
c O
Z
p
w S
o
OD o
0 �.
v
C
m
-
O
v
o
O
S
N
v
n v
O
{ P
a�
w
Ulo
rn
N
P
V
N
a
a
w
�
—
rn
o�
m
P
0
O
00
N
a
w
W
W
.n
O
o�pq
W
W
70
N o S 0 N 6
70 m 0 c
a
v9
N 3
Z
m
m 0 Z
7O 3 p
C X
ar n
F•1 �a D
Z O
G
e a
0
z
0
v �
a A
-I y
A
N
2
Z

--i .. i cf) C/) C) -2
7r, 0 -0 C:
Z (D --Z
=- 0
(D — 0 :E Zn 0 0 0
CD 5 =. =
>
m
> =
M Cl) (D 0 0— Co .. --o
C/) :3 0 C: 00
—0 -'% '-I
>
?.
cl)
30
CD o—' CL
CD
< 0
(D CD 33
m
30
0-r. .. ..
--i
0 0
"' R: Ez
Co C/) z
:3 -n -n
m
0
W o
Icn
cn
= —
�< CL
N 0 0
a
0
mCD
3
0
CD
—
0
rr
CD
cx
W
0)
00
A
w
3
A
to
L,,'�j
CD
CD
C:)
CD
:D
Lrl
. 0
CD 0
3 D 3
3 3 3 :3 o 5 3
(a co 0 (0 (c (C) cc (o (a =(o
coemu,
-n > 0 z z
cgo
O (a i CC
(D c: :r Cl W SD 7L - = =
C,D
0
0 =r 0
0 C) CO --O-o 6 (D
a
(D
0 M 2) M zr = —
-0 3 o 0'2Z
-0
W CD i�
C/)
3 53' 00�
CD — C: C C/) C, ro
3
0
3
cn
(D
(D 0cn
—
p Z z
ca
cn
z
0
A
C)
ca
Ln
Ln
co
CL
m
3 3 3 3
3 3 3 3 3 3 3 3 3 3 3
0
(o (o
(a cc cc cc (a (p (0 (p p (a (a
CD
CL
< 0 CD m -(:n- C)
0 0 o
>
> Z
o
=r
CD CL
C,
B P
CD
CD E333woo.K
a
0 o o >
a CIL CL r-
:It It 4t 0 C)
=r
z
cfD
0
me
j-
O>N-UZ I�
—r =3 cr
cD 3
CD M Cl)
CD
E2. Z
s
o
0
0 z
C:
=1 0
CL
LI)
03
=3
C-
100
of IV 41110
=3
(0 oa
0
3 3 3 3

"I _"�
o�?oC�-,M. om ==O
aCn n CD 0C00
QD (SD CAD m 3 3 m
r.
-oZF.
ol� a co�z mm
cn °- o pro Cl)
a —0
Qo o W v
`u m W
.� o
` 3
CD
A M UI C, ••
O• slur N G
p O • . ro O (A
Lri fn O�
O O m O
CD
n
O
935-333333CS, 03'
(n O (n (O (0 (o (n (Q =(a 3 3 (n 10
(A =_��� =fn a
co
7
D0-0ZZ CD
0 CD
CL
W W W CD O O -' W W m C C- CD
� a3:3—c'3��zz0 >
o (n•3� W CDo 0 3 3 3 3 w Ov COm
C
(n -_�{ W W
CD W FDocn(n
sv z Z
W
z
O
o m
o
0 o a
Ln
o (n (n m
a
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 2.
co cn �n (m (a (n (n (n (a to (n cn cn cn (n o-
CD
a
<
0 C)3 ,
� D �CDoNozm
a�CD 5-0 n (D W O W CD N
o _, z —
I —
CL �' L� o
•,)3 n 3
o
:3 Z
CD o n = O
3 3 3 0 aa
0.O 0.O O D = :3��:-gym C7
n n u "0
z [I,:
(] 1
I �
(] v
N
m
t7ti
o
CD
a
O
O'C
an (o
N y
Jj
�
Cn
C
C;J
T
O
O
z
m
r
r
O
m
D
m
m
O
z
r

(D
y
M CI'
� � �.•
-
CD CD u, _ c O O
.,
p can � O �� O c O O
cn
-
- (D n' CL
=r Z
CD CD m
m
a
OL)
-n -n
a
p
o
kn
co
cn
NacocCD
Hal=
:3a
CD a W n
—I o �
C)CD1
r-w S
.�
o
1
�
3
a
a
o
N
m
�
y
—i
A
O
01
3
C31
A
N g
A•
•
O v
O CD
•Q
u,
p
.
m
C
A
p
p
N
0
O f f
3
c-3 3 3 3 33 5 3 o03 o
/3
CO C(O O (O (c (O (O (O CD --(O CO (D
3 a
C
Dp,-oZZ CD
CD c O C1 n) sv - - O- �. r. C'9
n3 c)c�wD-0-0 6 CD
CD = 0 C aCo a C =? I�
=(a (n-0
wc 033�'c�-�c-0
Oto
�o�333n�i
cn
c
CZ
Z mi
—
(n(n
c Z
cn
O
A
p
ca
a
Ln
a
33333333339333.3�
(n cn (n (n (a cn (n (n (O (n (Q (n (Q (O cn a
cD
a
OCD
O o ,n
D
D Z
CD
n m (n
� O
CD a
a3 n
CD
E n
3 3 3 w a K
(D cD co I !m Cn
�PC ��=
a a o �D
It :tl-
u
u to u
N 6�
_ Z
iV-5 Z3
d 'DOfrs(
O v
N-0Z I9C
=3 cr
N Z -�
CD m
w
z
O
m
��C3333
it G)
CD N
(D O r Co
a O
cc")•p CD-'!D
N
O
'-, CD CD
° CD CD
7
CD = C
CD
<
m
3
CD �
�C
�Ln0�00
4�-,
cl a
-�
o
���
-0
D
a Q.
_
O CT CD
c
0
0 T
CD *
(D
W
z�3
CD
o
..
0:03�
0-W
a)
3
CL O
CA fA
Cco
CD(D
c
m
1
0
(D
W
O
N
D
�
5
m
,
�
�1
W
0
a
m ° a
Cv
CD CDCD
d.
co C
CO CD
w
co
H
CD w W
ocD
m co
o co
3
��'_ o
(D
z mO CD
Z
o o a o
m m
CD
O Q O
�� °
�W" 0 F.
a
p (D --+
cD
CD
p 0
O
(D
n p
N O
o n.
CD o
� a
3
0-o
M DD
O�
AN
C L
V-CCC3:-:))>
N N
* 0
(D O
-
r w
o 0 - S
aCD
O y,
cn
CD r
z
3
`D x
M 4
ro
N
co
W
p
a
o m o
O CD ? .
0
CD :3
CD
n
o �
CD
a CO (D
a �
3
6mi CD W
Z CL
m
(D CD CD
N O.
CD
c�
O
M
tt
(D
w
O
J
O
3 cu
zz-u
o 0 m
m
mO b
0
T
N
S
OO
Ia
XL
m
CD G1
O
=
n
a
-
Q
LTI
o
Cn
D
a
3
3
CD
ZZ
m
x
a
m
m
CO
=
o'
Z
CD
O
o
=
O
cn
m
Z
D
c
a
o
-I
Q
4
m
CD
CD
w
_.m
CD
V
�( J
`
0
n.
DQ�7�
r . .o -
M C:
�Oo"z
Z A.O
C% ^ m
ro
N
m .. m m
D
z a
m r
-Cl
m
En
v n:
::r z .
0 0
n
o
m r
yz
c> m.
i� C
N Z
N

- t�t<<ul�u•
s�
RESEAr" i & ANALyT1 CAL e'•h' 'Y•
LAbORATOMES INC.
NO 13ilfl1 7.
i Anal bcaUProcess'Consultations ,
�r P�'•�lRECSOQ'. SoSN
<<ilN t l l,000
Volatile Orl anic Analysis from Selected Sampling Locations Identified as Huffman Monitoring 'Wells #2 & #3
(A Water Tech Labs, Inc. Project, 06 November 2002)
Volatile Organics Ouantitation Volatile Orp: nics (CONTINUED) Quantitation
EPA Method G 1 OD Limit Weli 92 Welf 93 EPA Method 6210D Limit Well v2 Welt rt5
Parameter Pt P81 PPB P( PB) Parameter IP_ PEi Pj_P81 rip5I
1,1 Dichlorceth .rie .. , 0.5 .. , . BQL SOL Chlorobenze,ie .. , ......... 0 5 .... SOL ... SOL
2,2-Dichloropro ,ane . . , 0.5 .... SQL . BQL 2-Chlorotoluana .......... . 0.5 .... BQL . SQL
Chloroform .. ..... . 0.5 ; . BQL ... SOL 4-Chlorotolt;ona .... 0.5 , SOL . BQL
1,1,1-Trichloroer,hans ........ 0.5- 9OL .. , BQL Tert•Sutyibe,¢one . , . 0.5 SOL BOL
1,1-Dichloroprol.ene ......... C.5 BOL SOL Sec•Butyibertzene , ..........,0.5 . , SQL .. SOL
Carbon Tetra(;h' )ride ........ 0.5 . , .. BQL .. , BQL 1,4-Dichlorot�enzene .. , . .. 0.5 . , .. SOL BQL
t3anzene .. ... ... , . 0.5 , COL ... SQL 1,2-Dichlorot•enzene. ... , ..0.5 . , , , BQL .. -BQL
1,2-Dichloroeth: ne ...... , ... 0.5 .... SOL SOL P-Xylone . . 0.5 .. , . SOL ... BQL
Trichlorcethane .. , .. 0,5 .. SOL ]SQL 0-Xylene . , ..... , , . 0.5 SOL . SOL
1,2-Dichioropro, nne ......... 0.6 :.., 8QL ... SQL I-Propylbenzc:ne , . , .. .. , . 0.5 .... SOL ... BQL
Dibromomethani ........... 0.5 SQL ... SOL N-Propyber.:r me ........... 0.5 .. , SOL ... SQL
Toluene „ . , . • • .. • , .. 0.5 • . SOL SOL 1,3-Dichtorotenzene ......... 0.5 . SOL ... BQL
1,1,2-Trichloroe hane ...... 0.5 , .. , SOL . SOL DibromochlorDmethane . 0.5 SOL , . , SOL
1.3.0icllloroprol ine , .. , .. , . 0.5 . , .. SOL , OOC Dichlerodifluoromethana ... 0.5 .. . SOL ... BQ-
Tetrachloroether e ... , .... 0.5 . . BQL , SOL Chloromethara ............ 0.5 .. , . SOL . . SOL
1,1 ,1,2-Tatrao 1: roethane .... 0.5 .... BQL .. , SOL Vinyl Chloride; .. I .. , . 0.5 , ... SOL .: • 5QL
1^,1.2,2-Tetraehl aeetharie , .. , 0.5 .... SOL BQL 8rom.ome;hane ... 0.5 .... BQL 8QL
1,2,3rTrichloropi opane . 0.6 . , , SOL BQL Chloreethane .............. 0.5 , SOL , SOL
Hexach;crobutad one ........ 0,5 , .. BQL SOL Trichiorofiuonrmethane ... , ... 0.5 . SOL SOL
Bromobenzena .. , ... , ... 0.5 .. BQL ... BQL 1,1'Dlchloroe.hene , , ..... , , . 0.6 . , . BQL , .. SQL
Ethylbenzene .... I , . , 0,5 .... SOL • .. BQL Methylene Ch oride ......... 0.5 .... SOL ... SOL
Styrene . . ....... , 0,5 SOL . , . 8QL Trans-1,2-Dic.11oroethens ..... 0,5 .... SQL .. , SOL
Brcmoform C,5 , .. SOL ... SOL Ci4-1,2•Dichh;;roothene 0.5 .... SOL SOL
p-tsopropyltolueri. .. ... , .. 0.5 .... BQL BQL Sromod6chlorcenothane ....... C.S-. , SQL ... BCL
N-Sutylbenzene , .. , 0.5 .. BQL SOL dromochloron•ethane ........ 0.5 , ... SOL . BQL
Naphthalene .. .. 0.5 , SOL :. C BQL" cis- 1,3•Dichlu-opropcne O.E BQL ... BQL
M-Xy.ene , .. ; . 0.5 . SOL . , . SOL Trans-1,30-.1iloropropens . ,. C.5. , , SOL BQL
1,3,5.7rlmethylb nzene .. 0.5 .... SOL „ . SOL; Methy6Tart-S, tyl ether (V78E) . 5 0 _ , .. SOL ... BQL
1,2,4 Tnrnetnvlb nzenc .. , . C.5 .... SOL SOL isopropyl ethc 0PEI . .. . 5 0 .. SQL BQL
1,2,4-Trichlo•obelzere 0.5 .... 8QL . SQL
1,2,3-Trichlorobt 11e11e :.... , , C.5 .... EaL BC Dilution Faetod . 1 .......
Di;utYon Factor ..... . 1 1
Sample Nimbor 4e3628 453629 Sample Numb, r 455628 463629
Sample Date 1111061102 11106l02 Sample Date 11105/02 11/05r0Z
Sample Time 08C0 OS40 Sample Time 0800 C640
Date Analyzed 11114i02 L1114IO2 Oate Analyzed 11ill 410211:441C2
Time A,ia:yzed 1236 1259 Time Analyzed 1236_ 1259
PO. .cx 473 106 Snot Street • Kernersvilla, tyarch Carokra 27234 • :'t3E 3co c5 " =ax 36.39'c-O a2s
BQL = Below Q antitztion Limi;s PPS - Pars Per Bilker,
i
GROI i D _=CT10N
ASHEVULE `',= OFFICE

\**2

ƒ
\
g
ƒ
8
a
cr
&/
q
7
¥.
/
/
0
/
e
°
?o
°
] D
(
5
c
ƒ
w
¥
&
_
q
to
�
.
g
�
\ ƒ_
o
.
.. \
00
w
\ z
g
m Q&
g
B
_
;a
%
_
/
z
^
=
o q
o
/
G
/ }
/.
ƒ
0 \
\
:
.
t.
\
/
3
/
$
_
,-
.
C'
>
m{
\ �n
m
®
m
\
2 j
$ I°
2
ƒ;
\;
�
m
Iz
\
�
�
-
-
i
ƒ
f
.
)
= R
\
z
%
},
m
_
-n
n
OD.
7
1
y
»
.
§
°°�[
1
/ \
z
/
m
m
p
k
m
M
H
m
r
0
�
�
�
O�
�
�»
j\
z ?
q &
m.
/
» §
■
2 ©� �
� i 2
z E
S ƒ z
k E
§ §

-10 -i -0 012 C) C) C-)
,D<<�O=�° 000
CD 0 � O c o o
FA
yam CD CD m
c CL
w CAz K� m
2_ aom-n-n
V) N (' c O CD Cn
a — n w
a —� o
m
o
c �
P �D
n n �
m m N
LTI m
CD
v 0
l Y °
O53 (C) (o o o
CO cO c10
3 a
C
C�C�C�C�mDQ'vZZ �
C: maw w �� - cD
o ' =rocv a
73 7C)mC�•D CD CD
a c aF 3 o-O"Z
CD.. 3 c 3 �� ti O �
Q-t
,33 3-�vw N
m —
cn��z
Z
CU
Z
O
n
n w
p o CL
a
cn cn cn cn cn co ca cn cn � o.
c�
a
cn0>P"
053::3c-
�CDoc c
NrZ-t^^
co
n Z l' }� \✓
`C .••r
O O (D
o Z
C: O
a
N
w
(� a
!! 0 0 O
n
m
11-4
t h o
0
c3333
d m C�
cma
'' CD
M 0
" �
° °
o a
w o
o.-
N'N
p w
1
CD
c
� it
L
U, c
,
.M
�a
o
O
Q (cD O
C
a n.
w
o O
M
C
3
M CD
o °
a w
w
3
a�
c
=L
CD
w i
co
0
n
0
CD -0O
N
DCD
uj
c='
w
w
0 0
CD
i
❑ ❑
n Li
�Cn
O c
Nc
cD CD
rt N
-
N
d
(�D C
y
COco
C°0
co
N•
c
H
CD D)
Co
o CD
000 m N
m
o 3
0 -0
o
m
Z CD
0
p
c
CD
3 a
a
y
(D
w
N
ry�
n
O
=r
O
a
c
0
a
C:)
J
.•
CD
M
o
o
a_
O
y
y
N
N
O
cD
� o a
W CD =3
.A N CS.
w
3
.D
CD
w
CD
azoo
rJ
ow
CD
CDCOCO
Q. n
o 0-
l< l
Da
Cl)
aZi m
a3
:o
mmCl)
Vl
CD
Q
Z
cD
wCD
3
CD
�.
V1
01
o �_ o
o CD 3
c
0
CD '
CD
O
CD
Cn
w
3
cD
a
3 '
3
i•.
T
o m
x
m
o
o
m
0
0
m
o
9
p
w�
71
a
—
Q
c
0
O
0
m
73
D
a
(D
3
a
ZZ
CO
X
w
m
w
Z
n -Di
_
�_
O
o
=
°'
o
Z
cn
c
p
{
D
OL
0
m
m
w
CD
CD
rz
Z
.
n
A
m
�A
m
O_...-:.
Z
0:. ,
Z
D 'Q 0 <
m�zo
�a0=
= x`:�: a;
ztr-n.
nLnm
N 4:zt.n
m cn m
w 40
o O c
4 Z r—A-
m -,
m�
? z
o o:
o C-)
O
m r
w z
w M
� c
PS.: ,:

cn C/) 0,2 C) C) C)
0 -0 c =r 0 a: o o to >
m 0 Ei! M>
:3 M. o do
>=
0 CD =r <
3 CD CD CID
a
3 0 =
0 0 0 Cl) z
0 = it v
CA --i)
0 (n CA 0 CCD
-n
N 0
0) CD
0
ma --j -0
(D CD
0 1
3
m Ul w a A CO
OD H ti 03
c>
n c)
C)
0
i7-
9: o c)
3 D = D 3 9 93 9 99 0cD
(0 0 (a (10 (C) (a (C) (0 ;:;:(a
:3
CD C =r CD. M W ;L =r
0 > C) Ln
003 0 0 CO -0 6 CID
3 0 5ZZ
C: C: j Oo
0
cn cC
I In
zz
cn
o
0
CD C:) ra
m
.n
3 3 3 3 3 3 3 3 3 3 3 D 9 3 0
0 181,
Al1 zi ii
co 0 > z Ix
0 —=r 3 0'-'
CD 3 z H--n 0
CD c)
c)
CD CD
z
0
3
0C z
0
A A
• C) CD CD
CD
:3
010
cl
Lqc:393B

-� --� cn cn -D a - a
Z 0 -0 �.� m �' c OSu� a°° p
cD o` cn
ND � mc:3. ocooC7
nCL =zs
Zo o a� cD �I
c �0 �o��
0 c - -I -n
n+ a O
N ca
CD
CD =r
om w
.� o
c �
n a Gi
O u
V7 O l0 • • N� N
• O A-1�1i, OCCD
O Un 0 N Ln • m
O A
C O
3 3 =3 3 3 3 3 3� 3 003 1
ca ca o ca ca ca ca ca ca ._.. ca (0 co
C
7
(Dc cn6M.3ooZZ x
�. 3 C3c-0cn��-c
3 —3 3 c "a) �
_ CD O Cl)
e a) zZ
C
m
Z
C. O
n
O n p m
p a
O N
o v,
a
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 0
ca ca �a ca ca ca ca ca ca ca ca ca ca ca ca g
CD
a
<M- O
oCD
O n +�
>
D ,, Z
C)
o w
)3
CD
CD
3 3 3 cn a K
cacao
::r =r
rn
td f mmilak f ,C
:8/ i-a?�
d I 0
o�
oil
cno>N-uz I�
a = 3 :3 a.-'
GHG•rooNrzCD �
B� �nwA-C
M CD
A, z
`G .-a
o O o
3 ca
6
o z
c O
a
N
w
a .:
O
al n .
• A O O
CD .
Cn N
c 3 3 3 3
n
n
0
n
0
D
n
z
D
_z

RESEARI H Ot ANALyTiCAL
LABORATORIES, INC.
Analytical/Process Consultations
Mtn
Volatile Organic. Analysis from Selected Sampling Locations Identified as
Huffman Monitoring Wells #2 & #3 (A Water Tech Labs, Inc. Project, 07 November 2000)
Volatile Organics
Quant
EPA Method 6210D
Limit
MW
#2
MW #3
Parameter
(PPB)
(PPB)
PPB
I,l-Dichloroethane .....
0.5
.....
BQL
...
BQL
2,2-Dichloropropane ....
0.5
..... BQL
...
BQL
Chloroform ..........
0.5
..... BQL
...
BQL
1, 1, 1 -Trichloroethane ...
0.5
.....
BQL
...
BQL
I,1-Dichloropropene ....
0.5
.....
BQL
...
BQL
Carbon Tetrachloride ...
0.5
.....
BQL
... BQL
Benzene ............
0.5
.....
BQL
...
BQL
1,2-Dichloroethan( .....
0.5
.....
BQL
...
BQL
Trichloroethene .......
0.5
.....
BQL
...
BQL
1,2-Dichloropropane ....
0.5
.....
BQL
...
BQL
Dibromomethane .. , ...
0.5
. , , , ,
BQL
, , .
BQL
Toluene ............
0.5
.....
BQL
...
BQL
1,1,2-Trichloroethane ...
0.5
.....
BQL
...
BQL
1,3-Dichloropropane ....
0.5
.....
BQL
...
BQL
Tetrachloroethene ......
0.5
.....
BQL
...
BQL
1,1,1,2-Tetrachloroethane .
0.5
.....
BQL
...
BQL
1,1,2,2-Tetrachloroethane .
0.5
.....
BQL
...
BQL
1,2,3-Trichloropropane . ,
0.5
.....
BQL
...
BQL
Hexachlorobutadiene ....
0.5
.....
BQL
...
BQL
Bromobenzene ........
0.5
.....
BQL
...
BQL
Ethylbenzene .........
0:5
.....
BQL
...
BQL
Styrene .............
0.5
.....
BQL
...
BQL
Bromoform ..........
0.5
......
BQL
...
BQL
p-Isopropyl toluene .....
0.5
.....
BQL
...
BQL
N-Butylbenzene .......
0.5
.....
BQL
...
BQL
Naphthalene ..........
0.5
.....
BQL
...
BQL
NI-Xylene ...........
0.5
.....
BQL
...
BQL
1,3,5-Trim ethyl benzene ..
0.5
.....
BQL
...
BQL
1,2,4-Trimethylbenzene ..
0.5
.....
BQL
...
BQL
1,2,4-Trichlorobenzene ..
0.5
.....
BQL
...
BQL
1,2,3-Trichlorobenzene ..
0.5
.....
BQL
...
BQL
Volatile Organics (CONTINUED)
Quant
EPA Method 6210D
Limit
MW
#2
MW #3
Parameter
(PPB)
PPB
PPB
Chlorobenzene ...............
0.5 ....
BQL
....
BQL
2-Chlorotoluene ..............
0.5 ....
BQL
....
BQL
4-Chlorotoluene ..............
0.5
BQL
....
BQL
Tert-Butylbenzene ............
0.5 ....
BQL
....
BQL
Sec-Butylbcnzene ........... . .
0.5 ....
BQL
....
BQL
1,4-Dichlorobenzene ...........
0.5 ....
BQL
....
BQL
1,2-Dichlorobenzene ...........
0.5 ....
BQL
....
BQL
P-Xylene ...................
0.5 ....
BQL
....
BQL
O-Xylene ..................
0.5 ....
BQL
....
BQL
I-Propylbenzene ..............
0.5 ....
BQL
....
BQL
N-Propylbenzene .............
0.5 ....
BQL
....
BQL
1,3-Dichlorobenzene ...........
0.5
BQL
BQL
Dibromo0doromethane .........
0.5 ....
BQL
....
BQL
Dichlorod:fluoromethane ........
0.5
BQL
....
BQL
Chloromethane ............
0.5 ....
BQL
....
BQL
Vinyl Chloride ..............
0.5 ....
BQL
...
BQL
Bromonicthane ...............
0.5 ....
BQL
....
BQL
Chloroethane ................
0.5 ....
BQL
....
BQL
TrichIorofluoromethane .........
0.5
BQL
....
BQL
l,l-Dichforoethene ............
0.5 ....
BQL
....
BQL
Methylene Chloride ...........
0.5 ....
BQL
.. , .
BQL
Trans-1,2-Dichloroethene ........
0.5
BQL
....
BQL
Cis-1,2-h . hloroethene .........
0.5
BQL
....
BQL
Bromoclic'lloromethane .........
0.5 .. , .
BQL
....
BQL
Bromoch'- mmethane ..........
0.5
BQL
....
BQL
Cis-1,3-D . hloropropene ........
0.5 ....
BQL
....
BQL
Trans-1,7-Dichloropropene .......
0.5 ....
BQL
....
BQL
Methyl-Te,t-Butyl ether (MTBE) ..
5.0 .
BQL
.. , .
BQL
Isopropyl crher (IPE) ..........
5.0
BQL
....
BQL
Dilution I:::ctor ................ . ...... 1 1
Dilution Factor . ...............
. l .....
, I
Sample Number
436185
436186
Sample Ni
Samplc 1
Sample Date
11/07/01
11/07/01
Sample I .:
Sample Time
0940
I025
Date
Date Analyzed
I1/20/01
11/20/01
Time An:
Time Analyzed
1419
1451
BQL
PPB
rr
e:v
1
O'otind��aler Section
Rshevi sa tfice
436185 436186
11 /07/01 l 1 /07/01
0940 1025
11 /20/01 11 /20/01
1419 1451
ow Quant'ation Limits
Parts Per Billion
Fn:.\WATERS\62IOM OTECH.621
P0. Box 473 • 106 Short Street Kernersville, North Carolina 27284 • 336-996-2641 • Fax [phone]

V/
)--10 'D
Z60 =z0
ll/
O lJ
o o O
0 iU = N
�30000"�
CD 0 C7 �� co o
"-n
zo
=ems
a
a C/ 2
22.c'
p
�°2 'r1n
0 CD
Co
:3
CA
CD -
Q.
O
Fo
coCD
•i
O
c
a
3
a
a
CD
�
O
3
�
N N
o
Jl
M
-41
m
. CD
O -0
C
33323333�3
003.a
0
O
cn cp o cn Cc (n
cn
cc cc (Q
c
KK;�2-noc)C)C-)mDO-OZZ
CD
ccn CD
0.W2)—a.0—r CD
K�° Ko C-)3
o c• o _,
tn
CSC m -0 ID0sysvCD
o—cvwa�c
�cp cn n �a
=r
C 0- -, O?o--Z
m e
0 3
3 — m
oN cn
CD3
—
L ZZ
a�
I
z
0
0
o
A
C>
A
Da
m
:3
c�
a
3 3 3 3 3 3
3 3 3 3 3 3 3 3 3
<mz p
O-0 M=r3ccr
O>N-oZ
noo
(D3 1
�=,>
:0NrZ-c
w y 0
-p �
0 CD
0
n
CL
� o
•� 3
cCD
3 CD
••
••
nn
M ^y/
•• S
O
z
\/
CD
3 3 3 CD a `'
c
a
O
S S
S =
D
O
a
Z °'
LAJ
0
0
cn
c3333
_cntouaun

n
o
n
x
s
x
w>
Y
o
H
n
n
(5
n
0
o
o
p
p
O
O
toC
S
w
�
'
�i7
o
ii
•o
v
a
•p
"�rl
4+
a
�
cn
c
g
n
c
0O
3@
ao
as
oc
9
o
3-3
ao
ao
c
2.
a
as
w
z
5
as
o
o
w
3
To
Z�
r'
—
r•'
i
�
r
r
r
�
ram•'
r-
C
^•
�
r'
=
r'
L
x
x
x
x
x
y
O
u
C
z
z
w
0
N
o
a
0o
w
0)
,O
O
7a
70
�O
ao
@'a
Qo
as
OG
ao
00
00
�
IQ
Do
3
00
3
7o
3
A
ram-
r^
n
i
r
r
t=
r
r
�
o
�
�•"
r
i-
r
r
n
a
N
x
x
x
x
6?
z
?c
x„
n
n
n
m
y>>
N
Z
?'
7
w
a?
h
n
y
>
rn
=
a
R
C
w
7
3
C
.
a
y
O
C
p`
A
`•
�
�
n`
�
A
0a
r
O
N
U
O
U
D\
b
N
U
v
i.l
e
c
c
c
�❑�
3
e
c
e
e
c�
c
c
c
r
r
r
r
r
r
r
r
r
r
r
r
i
r
r
r
r
r
H
H
0
H
>
?
0
0
a
�
0
c
v
o
w
H
w
2
O
Q
b
ao
o
.n.
n
m
A O
®
mrHr0
OZ
r)�
zH
O..
Q
7
ryl
�
pp_
r
r
e
C�
z� C7o C
ao 0
ry
v
o
0
n
z
zly
r m
❑ 4
C
Ay
n � m
��zz
dpt7o
N
�1

c_
tx0
x
Cl
n
n
C',
ClcNa
n
n
n
n
0-{
sry
0J
^wO
O
a
0
aooCl
v
n
v
O32o�
C
O
=
W
N
d
C
S
u
rc
3
-aJ
�-..
O�=
Q
X
m
a
o
o
-
r
P
T
T
W
.wA
O
X
to
U�1
(71
O
o
S
co
S
m
J
o_
o
o
m
o
w
cn
iw
in
to
CL
H
-
-
W
W
O
O
Ln
a,U1
P
e
C
\
tc
t o
a
to
?
t c
Z
3
t`
\\
3
to
3
3
\
\
\
\
\
\
\
b
\
C
0..
o
r p C%
W
d
v
O a c
p =
�
n
Z
-I
4
o
O
m
m
N
_
"
a
o
m
(Aj
3'
O
N
o
m
W.
A
41
H
m
>
T
C
o
to
o
T
s
:I o..
° a
�°
r
W
W
c�
c
=q o ao >
w
Gm
a
w
p
A m O
v
w
ca
A
O (%
w
C O
w
Ai
_ O Ol z
N \ S N
p�
11��yI
Xi
b
N
a
n�
a.
X
X
X
0
N
X
v.NO
c
c
-0
s
o
p
G
z
IOit.
IOii
a
N
y
N
O
�
�i
H
N
O
o
O
Z
'
V
'o
n•
n
wu
Cm
u
'
Wo
Ol`
Z
(X
o
o
«�
o
cn
w
c°it
p
to
w
O
n
v'
o
N
3
3
3
3
o
3
3
c
c
3
9
B
3
A
3
°
c
3
O
o
m
v
N
O
®to
to
�
n'
O. T
3 '.V
O
c
N N co
w
m
m
T
m 0 X
�l
X
X
X
X
Z
3-
3.
o
D
D
D
N
A
Z
O
N
Ip
o•
tD
o
T
o
0
0>
!A
1p
A
tNo
(o
J.
00
p
f0
o
c
o
o
to
Pn
c
m
^
oCL
A
v
(a
o
'o
3
3.
c'
3
3<
P
c
3
P
cm
3
J
(0to
COe
3
C
3
e
.p
o,
A
A
e
?
P
a
P
N
3
a
w
U,
a
Ln
P
C',
to
P
0
N
0,
N
�
tr
a,P
P
cm
f.11
C10
V
c
e
\
e
to
\
c
to
\
e
to
\
3
t0
\
c
tc
\
3
\
3
\
c
to
\
c
(c
\
c
to
\
c
to
\
c
to
3
\
c
to
\
c
to
c
to
\
c
to
=
2
0
2
3
W
c
Z
to
UO
a
to
=
m
to
m
0
0
X
°:
o-'
to
?
v
o
J
l0
N
A
f0
N
0
to
to
N
to
N
?
y
n
O
ti
y
n
to
N
0
w
�
I
f
I-H
d
ttl
NI
N
3
nC'
o
'o
y
r
W
0
�
3
�
G
to
to
73,
O
H
S
O
O .
e
a
3 T
11
d-
O R
J 7
T
D
m
..F
N.
® v
�o-
N
O
M
S
CHC p
O
M
°
O 3
a
Z q
N
y
o
`JG Ov p 0 N. O G
-A
p
m -f c
N O ry O_ l0 Z
m
v K n 70
3
M, Z
`G m•
p
a CL
A
e C%
a a
c o
t � G
41 Z
ty
m
p
m
m
O
cn
o
Z
y
U1
y
O
l0
S
P
J
.
o_
0
to

NC DENR/DWQ Chemistry Laboratory
Sample Anomaly Report (SAR)�
Lab Number:G'`l 1 Sample Type ��t`
Priority:
e Sampfled: _ I o �� I Date of Analysis: /a c log
Affected Parameters:"
Analytical Area (check one): /
❑ WCH
V METALS ❑
VOA ❑ SVOA
❑ NUT ❑ MICRO 13
PEST
The following anomalies occurred (check all that apply);
Samples ❑
Quality Control
❑ Improper container used
❑ Data flag may be needed.
❑ VOA vials with headspace
❑ No trip blank included w/ S10A samples
❑ Sulfide samples with headspace
❑ Instrument failure — no reportable results
O Samples not received, but listed on fieldsheet
❑ Analyst error — no reportable results
❑ Samples received, but not listed on fieldsheet
Cl Surrogates
❑. ° P islabeled as to tests, preservatives, etc.
❑ None added
❑ Holding time expired
❑ Recovery outside acceptance limits
13 Prior to receipt in lab
❑ Spike recovery
❑ After receipt in lab
❑ None added
❑ insufficient quantity for analysis
❑ Recovery outside acceptance limits
❑ Sample exhibits gross non -homogeneity
❑ Internal standards
❑ Sample not chemically preserved properly
Blank contamination
❑' pH out of range (record pH):
❑ QC data reported outside of controls
Q Improper chemical
❑ Incorrect procedure used
❑ Residual chlorine present in sample
❑ SOP intentionally modified with QA and Branch Head
® Color interference
approval
❑ 'Heavy emulsion formed during extraction
❑ Invalid instrument calibration
❑ Elevated detection limits due to:
❑ Sample matrix — does not have high analyte content
❑ Insufficient sample volume
❑ Other (specify):
Comments ,�
✓ .
��r�t: 2�,1�,�fa wl� �},.�;�;o•.lin�ucl f �JI �?� �;1��
.,Lf,G rs�� 7� ,�--,lL--
Corrective Action:
❑ Samples were rejected by DWQ Lab. Authorized by
Date:. ! /
❑ Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be `secured...
❑ Sample(s) on hold until:
W"' Sample reported with qualification. Bata qualification code used:.,-V
® - Other (explain):
Notification Required (circle one)?
Person Contacted:
Date: ! /
Form completed by: rJr j' Cr
Date: / -7 /
TT -it Leader Review (initial): Lf
NUT VOA
SVOA
WCH PEST
M C
Branch Head Review (rnrti -
QA/QC Review
QA\Forms\ aboratory\SAR
3/29/01dbs

m
A
a
sr
—1 o (D
N H
CD � Y
a
o
o
'v Z M
a D
m P)
� a
d�
N
o'0
—I —i Cl) Cn G � —
1 C) - -0 z C) CS C)
ZcvC SQ=gym ooQ
CDCD
n Co
W Dim o cn
CD 0 (7 •-� cn
_c M. O c 00
z30
�0CD
CD CD ��
wad....
m
3n
00
=
a
wCnz
'mm
aci' CL
a� � m T T
'_"
0cn
".
N N 0 O0 CD
a —0CD
m
0
Q p
cD
?
_m
w
.�
0
c
R
C
G
Cl)
n
dl
•
O
W
3
•fl
O
O
-�i
O
O
n
33033333303
o03
(a n 0 cc cc cc
ca cn cn —• cc 3 3 aDcD
c
��T.2'nC�C�C�C�QIDQ'�ZZ
�
ccn �cncDcc-c,w07--L
�
003-w0In
-for
wwW—
cnncnnCa30'0.c'�.00zZx
w m c'�
cD
�03
��•� 3 C'o (n
.<
w
3
cn
—
00CDcwn
w ZZ
ifl
a�
I
G=T
Z
0
CD
m
�
U LI-
1 9
O
•
O
O
O
0
�.
l.7'1
Ln
33333333333
a
cn cn cn � cn cp cn cn cc] � cn ca ca ca �
a
c�
a
O.B
cnODNZ
0
x
CD�o
n0 0 O
0 3 cT
3
-t
D?�3���-cmn
F.
•~• y C7
CD
m w
Q.
Z
CD
0 V:
a
0
Q
•J 3 n
0
3CD
CD
o c
Z
co m
m �* cn
N
0 0
0 D=p
w
a
C)II
u � j iy '
It 11 �� 0
-1 n
A
O
Z Q.
�j
Ln
0 ,1
y
0
333
o
y = cQ to «\

--i --1 C/) cl) -0 G) -00,2000
70,0 C: =r -1
Z 6 CD CD CD
CD 0
0 0 0
CA = =
>
M
— Q. n 0)
> 20 = =.
.. — � 0
0 a 00
" —1
>
W CD F)' CL
E3 0 CD
=r Z to
CD CD 33
m
Zan
3
CL
'z
--4
M
00
0-
:3 p -n -n
Boa
CL
0
ca
0
cn
rj) 0 06,
N .. CL —0
CD
2)
0
0
0,
(A
0
A
M
0)
Ul M
FA
0
ow
LJ
OD
to
10
CD
-1
c
0
0
33 B 33333
S3 003
MM o cc Cc M (0 (a a:) =n M
Z:l 3 3
CD
K K;r, -7 M C) C-) C)
C) co > 0 -0 z z
a:) (D a =r CL
W CD �. =r
, I
0
0— K Q 3 C-)
I I =r C)
>
C-) --00 "00 CD
CL
w 0 w CD 0 -- w
-0 C a---.3
w C =r =r —
o2z
X
I
:3 M
Ln. 0
rn
-5 3 3
CD
.
c 5 ch 2oO
C: -0 cn C, "
-<
Ca
C,*
CA
Z z
cl)
I
z
0
r
C=
C=
c)
A
CD
0
03
�D
C)
CL
co
C.
3333333333333330
cm MCC an nn nan(onnn
p(pcp
2t
CL
< -5i 0
1-3
Cn 0 >
aZ
0 CD -0 :0
0"D m
0
><
0 S: 3 1
r
0 o 0
>
Oj 3 Z
0 r-
M
> z
2. CD
Cl)
0
CD
0 Z
CD
0
CD
aCL
0
3 P
3 CD
0
z
CD 0
C:
D
CL
0
—
B 3 3
Ix
c/) cL
W
0 0
CL o-
>
=
A
C)
0 CL
�C)
A
C)
A
0
03
—0
III �I III
al 0
=
0
I
Ul
.
C)
CA z a)
0 V
C)
CD
R.
C)
0
3
3 3 3
NO
2. M
2

ESEARCh & ANAl TICAI
RECEIVED/DEN R- CW ; a:cn'.
LABORATORIES, INC. 0170 GftOUNDIYATER SEITIOb Nc#37701 x•
i
i 00 DEC 20 AM 1i:�F9.°/Ro¢:���``,.
?*� A Analytical/Process Consultations
Volatile Organic Analysis from Selected Sampling Locations Identified as Huffman Monitoring Wells ##2 & #f3
(A Water Tech Labs, Inca Project, 9 November 2000)
Volatile Organics Quantitation Volatile Organics (CONTINUED) Quantitation
EPA Method 6210D Limit Well #2 Well #3 EPA Method 62100 Limit Well #2 Well #3
Parameter(PPB) LPPBZ PPB Parameter PPB PPB (PPB)
1,1-Dichloroethane .. . , 0.5 BQL .. BQL Chlorobenzene ............. 0.5 BQL . BQL
2,2-Dichloropropane ......... 0.5 BQL ... BQL 2-Chlorotoluene ...... . ... 0.5 .... SOL ... BQL
Chloroform .............. 0.6 .... BQL ... BQL 4-Chlorotoluene ............ 0.5 ... BQL ... BQL
1, 1, 1 -Trichloroethane ........ 0.5 .... BQL ... BQL Tert-Butylbenzene .... . , 0.5 .... BQL ... BQL
1,1-Dichloropropene ......... 0.5 . BQL ... SOL Sec-Butylbenzene ........... 0.5 .... BQL BQL
Carbon Tetrachloride . 0.5 .... BQL ... BQL 1,4-Dichlorobenzene ......... 0.5 .... BQL ... BQL
Benzene ................. 0.5 .... BQL ... SOL 1,2-Dichlorobenzene ......... 0.5 .... BQL BQL
1,2-Dichloroethane ........... 0.5 .... BQL ... BQL P-Xylene ................. 0.5 ... SOL ... BQL
Trichloroethene ............ 0.5 .. BQL ... SOL O-Xylene ................. 0.5 .... BQL ... BQL
1,2-Dichloropropane ..... 0.5 .... BQL ... BQL I-Propylbenzene ............0.5 .... BQL ... BQL
Dibromomethane ........... 0.5 .... BQL BQL N-Propylbenzene ........... 0.5 .... BQL ... BQL
Toluene ................. 0.5 .... BQL ... BQL 1,3-Dichlorobenzene ......... 0.5 ._... BQL ... BQL
1,1,2-Trichloroethane ........ 0.5 .... SOL ... BQL Dibromochloromethane ....... 0.5 .... BQL ... BQL
1,3-Dichloropropane .......... 0.5 .... BQL ... BQL Dichlorodifluoromethane ...... 0.5 .... BQL ... BQL
Tetra chi oroethene .... , ..... 0.5 .... SOL ... BQL Chloromethane ............ 0.5 .... BQL . BQL
1,1.1,2-Tetrachloroethane . , . 0.5 ..... BQL ... SOL Vinyl Chloride ...... 0.5 .... BQL BQL
1,1,2,2-Tetrachloroethane .... 0.5 .... BQL ... BQL Bromomethane ............. 0.5 . BQL ... BQL
1,2,3-Trichloropropane ....... 0.5 .... BQL ... BQL Chloroethane .............. 0.5 .... BQL ... BQL
Hexachlorobutadieno ........ 0.5 . BQL ... BQL Trichloiofluoremethar,e ....... 0.5 ... BQL BQL
Bromobenzene ............. 0.5 .... BQL ... BQL 1,1-Dichloroethene .......... 0.5 BQL ... BQL
Ethylbenzene .............. 0.5 .... BQL ... BQL Methylene Chloride ......... 0.5 .... BQL ... BQL
Styrene .................. 0.5 .... BQL ... BQL Trans-1,2-Dichloroethene ..... 0.5 BQL ... BQL
Bromoform ............... 0.5 ... BQL ... BQL Cis-1,2-Dichloroethene ....... 0.5 .... SOL ... BQL
p-Isopropyltoluene .......... 0.5 .... SOL ... BQL Bromodichloromethane 0.5 .... BQL ...BQL
N-Butylbenzene ............ 0.5 .... BQL ... BQL Bromochloromethane ........ 0.5 .... BQL ... BQL
Naphthalene .............. 0.5 . , .. BQL BQL Cis- 1,3-Dichloropropene ...... 0.5 .... BQL ... BQL
M-Xylene ................ 0.5 .... BQL ... BQL Trans-1,3-Dichloropropene .... 0.5 .... BQL BQL
1,3,5-Trimethylbenzene ...... 0.5 BQL ... BQL Methyl-Tert-Butyl ether (MTBE) . 5.0 .... BQL ... BQL
1,2,4-Trimethylbenzene ...... 0.5 .... BQL ... BQL Isopropyl ether (IPE) ......... 5.0 .... BQL ... BQL
1,2,4-Trichlorobenzene ....... 0.5 . BQL ... BQL
1,2,3-Trichlorobenzene ....... 0.5 .... BQL ... BQL Dilution Factor ........
Dilution Factor .................... 1 ..... 1
Sample Number 406902 406903 Sample Number 406902 406903
Sample Date 11/09/00 11/09/00 Sample Date 11/09/00 11/09/00
Sample Time 0815 0900 Sample Time 0815 0900
Date Analyzed 11/15/00 11/15/00 Date Analyzed 11/15/00 11/15/00
Tirne Analyzed 1 119 1201 Time Analyzed 1119 1201
BQL = Below Quantitation Limits PPB = Parts Per Billion
P0. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 Fax 33o-996-0326 Fn "2='Ea.-

CD
OD
-i -1(A Cn -v O
j -1 0 z C) 0 C)
;r, O 'O c= -1 �,,;, j 0= f!i ° 0 0 0
ZWn ��:3 C)a0p�
cl)D mZ5-cL
3 m
::-<'a -4
cucn333
m
Z3 0
a
�z ��
m�.a
O
w
o ��
m
t v
o a E�
a o o
-
3
.a
n
CD
E
-m
0
c
3
c
m
Ul
n
OCl7
a
Nm
...
NN
N
CY
Ul
A
l0
m
LTI CD
CD
A
=3 3 3 3 3 3 c;3 003
(c (m 0 (O (a (n (O (o (a -(o 3 3 (o ID
CL
c
�0.0WDO�ZZ C
CD
0
nn� �� cD
=(o F �-o
(ncLn.� 533c
c a� ='.3 o o
c(n-00.�
ZZ �c
= con c
�
--1c'3 c S..cw m
3�cn
0C3
o3
-
ty
co3
o�NZ
- Z
03
cn
I
"D
Z
O
0
O
^
m
�
o
O
a
(n
O
J
M
(n
o
o,
333333333333333�
m
cn (n (o (o (o (c (o (a (Q (a (o (o co (m (D n.
cD
a
<:0
cn0DN-0Z
x
I
Don
-o
a�3
�
no
o
o 0
a o
H. 0 NrZ m
D
Z
G -c c="N
'0¢i n
�
co
w 3
co
Z
o
-
0
C
L
(0
I
..a
3 p
3 cD
-<
= n
c
Z
p
3 3 con °n
n.
w
.�
ro m m
� (n
w
0 0 0
D
n.
o
C. a ate-- r-
v�C7
n
D:
�N
JI 11 II
Ul
Z
cn
O Q
A�
O
I
0
c3333

Oo ° °
0
S
m �-
6.
3
to
a
>
n
O
n
m
p
m
3•
�
�
C
0
� O
Q
m
s'
C
A
l
Y
co
o
0
o
g
k
2
g
o
0
0
0
0
ry
°
g
ro
�'
m
°
°
-1
c'
m
2•
�
2
w
00
A
O
A
y�
p•
O
o
A
?+
O
3
��
w
3
3
(eQ.-
3
3
3
1p-
2.
3
3
z
c"n
3
0
0
3
3
3
f-
cam-
C
3
3q.-
r
y
'd O n
�O n
a
td
0ao0
O
mm H
O
Z
O 0
G
� ..
-
'17
"C
3
2
z
O
a
C
a�
�
r
o
14
W
n
O
A m O o O �
3 v d
�.
0
w
x
x
x
x
o
'[y�i,;
w
O
o
�'
k
k
k
k
�
H
Y.
w
d
o
d
<
3
3
c
c
c
c
c
c
°
3
3
t'
P�p
f
[f
o
p
o
o
2
2
w
2
3
a
p
w
as
G�
m'
m
H
y
n
0

T >
cr -n o S C N
� r igy-� •T, rr as ��ss
')o 000 v n D D 0 37 -I C7 n n v ID c O Q O W�` Z
0 '� m ci w �c = m O 0 0 0 0 O C� D C,- o "1 °
y o 0 0 o Q o w o' ° a rn 0 0 v 0 y`N Z n
i �• n o o c w c -- r 2 y y � 1,
y c c m CL c w �c � 0 3 3* w Q r c 0
CD o °' co 0 o cn rn w W c �L7 -< r 3 cn T O
aCD Ate__ �T�� moZo �� 1 r D
c c w car, a °—' w 0 CD Z c' CD O U
N A A a n 7e n cn
t11
CD w ° o
r i CD
a,o o A�
Cl) o ��o �,.n
n a r
CA aA p r
3 0 c 3 3 3 3 3 3 c 3 Z 3 0 0 3 3 m O w 0
C 10 cn cp co C 3 Q 0 D
- — ==— O t�aV1
O b * O W
v, v, N �„ � Ga tat 'n
ZO z O c c w w o ro OO O W m
0 0) a ai = a a c p o
7 • 0
07 In rL
Z w O A? n w to cn o n
O Z cn cn o
� v_ -4 a 3 ❑❑ n
v w m o.0 0 0 -4 i`�CA0r-O CD pcn
rn m o w w CD cD 0 .. 0 'D
u' Z coil cD o n psi �+ _ 11
rn Q oo i1i a N ❑ -4
w X, C
o N w 0. 0 m m
L! CD 0 to 1 Gi
a yam $Z �' ❑pn
° 3 ..1 3 c m��
3 3 3 3 3 3 c 3 3 3 �. y 0
_�3 n ma Q. ��: m
-- - _ - - - ao �3�0 3
0
a R� 3
Ncn-0ZzK �zm 0 00 w N DD titi ��w Q 0i 7.i i i e
NCnrZCn o K-0000 >>— � io Z
IA
c CD 0CD W�° 0 0 0 0 0 o c• 0 0 N Z; c< I�
c N m c c rn m 3 3 c 3 �. a T �� 41 O v
3 y c A v w A a A �cn m� y Z y_n�
CD 3 rn. rn" rn cn cn cn rn ``g f`, O Z yJ O
rn rnal o N cn ro CP o v n�.��� fir- QCD
Q.
�C
cn A O 7 Nch 0 0 0 N 0 r D rt1
�3 3 U - :3
CD m n) CD CD m z
A= :o m CD a c �o c 0
c c c c 3 c 3 3 c c c c c 3 c c c c 3 0 0 �c m
0
CMD
cn co co = CD r 3 S
Q
2
2
S
3
m
a
o
co
co
ID
CD
o
m
m
N
O
A
g
o
s
X
0
co
�:
g
CD
�
o
L�
w
O
CD
3
y
N
07.
3
Co
01
CDa
CD
°
C
CD
C
_y
<
O
Ca
CD
CD
[n
Cn
(D
0
D
CD
M
0a
o
ci
CD
U)
CD
=
a
CD
o
Z
�
�CDQ
'i
T
m a)
1
A)
C
m s 0
n
T
Za0
v d
`\
cn
D
pi
<�
O
c
-I
m 01
(7
CD
m 0A
c
-
50
I
-
Z w

n
0
3
m
_
y
--i
<
-i
Cn
-D
D
z
0
0
0
'0
m
n
a
cfl
ca
co
p
o
m
to
CD
>
0
0
d
0
w
cr
-0
o
N
m
m
n
a
O
CD
O
0
d
(O
cn
O
CD
co
_
7CD
Q.
-D
�.
<
0
y
En
70
D
co
m
T
a
7
0
C)a
rn
N
_0 m1
m o �
cn
cn
-O( DD
n CD -0g
�- m _0:0o
o
o a
O
.«
w
D
0
03
r-
m
_0
�On=-CD
m�
.0
0 CD
i. CD,
Q.
o
2o
o(D o
Q?
ono
m
CCD-
o (D
0
1
o
6�
m
0
w
DO
0
m
m
V0
�
o
a
3
w o r 0 m
0
CD
0 9 m
O
El
a =
0
y m
0
1a Q. 3
c
P
S
n
y
Co
'a
U)
o
Q
A CD5
m�
ko
� w
�Jn
O r
1 (�ccn
S-i O m 0 r
CD m w m 0 co
Ci CAD cr (�D =
m�CD o
Q� Qm
a
- C�
a O
m 9" 0
O
C o
a 3
n o
O
C7 m
-A o
/ CD
= W
e
0
CD
❑D
m �o
m
CD m
ov
C CD
(n N
0
z3
03
�o
am
-43
m 5. Z
O C
Dom
D � �
r�
(Dm n
• m
M- 0
C�-
Za3
vZd
DC
m
N y
m 0
Z W

-i -i CIJ U) 'n ) , J
-- -o Z In o o
;jr o
Z F CD= (D (D CD 0
O
_�
Q= N ,F O 0 0
�� O O O
=«� N
30•���c�CCL DD
C
mms "�
Zan
_
:3CL .
rn
O�
n.
go Cl)
�. CL.
0
: 0 m -n -n
NU)o -.
o
no0
CD
—m
2,
CD
a
a
a)
v
n
0
�
00a
N
O
�:
(D.
cD
K
33s3.33333c3
�i �►
003
CD
(Q 9 0 (Q (o to cc to
(n = CD 3 3 aEL
.+
a
c
3
KK?;M r1n000m>O-OZZ
O
+ + •� + + + o + + + + c'O m -
a
�Ko �'o o �•0 M
0 E-0 0•CD,�
w c'c
3•c co
0�
3 ccr,
�0
-t
c
0
0�3 30 .�W'
�
CD
Iw
_
Z
-- Z
�
I
z
O
O
O
,7
OLnt].
N
Ln
Ln
cD
33333333333333��
n an n cQ p cc (o (o cQ c(D (n (a
a
co
o.
O(CD-�
0 > �z
I�
10 CD
C)CD
� = D
3
-1 O Nr-Z
m
n
CD
A Z
CD
CD
CL
.v P
p (c
CD
o
.. .. 0
(R Ll
C
y
0
(D (D (p
N
0 o o
D •D
a
II It II
n
O
Z �
O cr
�.
m
Ln
N
O
�
I
c3333
o
v
CA

-I -i C/) C/) 'O ) �� j -i'o 0,2 0 0 0
;r,o-0a=•-�;�0m-aooQ
Z c v m 0 ^ cn m= =.; p
• D..;� cn�= *oa00
cn 0 oCl) C CD CD m 3
Zen m =ate....
O0 a ccnz��
o =�0 cn N� c 0CCD
a--1
(�
3
n Q0o
0 s
CD om w
.� o
3
rn n -j cn M c •• CD
O W a N d
�l C71 C o O —
• In 0 m O O O
in m 1
j CD
33�333333c3 003
cc cm 0 cn cfl cn cc ca n = cn 3 3 cfl a
(o CD c =r a o W 7 ;:L =r : c�
�•W W "0-0 n
w w M CD
p �C
- = co 0 C� 0 'p C a n C 3 o O Z Z DC
cc=3TC . �33c3�ac0�-e
CD CD -s _
n cn. 3� 0 3 3 a ��-- o N
3_ C .. 0 CO CA
cD3 cDR�ZZ
CD
0 o P LU
0
0
> Z
_ o
C) n m
p . C
Z � O • � Cl
c p o m
CL
_Z 3333333333 a
o Cfl CII c0 CQ CO CO cC� CQ Cfl ff] (II C1
— — CD
M
N „
O
+ <� N 0 EnQDN -0
a
D q CD m °� DM Z � 3.� w � N
N 0 CD iU CD
z -
=r _N
CD a o cc I
•J 3 Ci � CD
n c p
• a 3 3 w CD a CL
0 0 0 X D= a
aaa^, �
4tft n o n O
II it 11
O
Ul O
., Z d T 01
0 a=
O D O
c3333
_. a:) co cn cn
N O —
N
O
1 -,

ALIZED ASSAYS ``� C.
2460 F»,ter Creighton Dr.
P.O. Box 40566
Nashville, TN 37204-0566
Phone [phone]
:-;URLINGTON RESEARCH, INC 2100
WAYNE ALTHOUSE
-1302 BEL_MONT' ST
3URLING TON, NC 27219
Pro ject:
:"r•o ject Name: BURLINGTON RE'SEARCHr INC
Samp 1 er•: S. C.
^M^L_1jrT I C ^L- R IMP OR T
Report yuaa
Raaigte Result Units Littit Littit
Lab Number: 99-A169379
Sample ID: 9K100-002
Sample Type: Water
Site ID:
Date
Collected:
il/,3/99
Time
Collected:
9:20
Date
Received:
il/ 9/99
Time
Received:
9:00
Oil
Factor Fate Titre Aftalgst Rethod Batch
.ATiLf R€RTMICS bg GC*
Senzene
Ho
ug11
0.1
0.1
1
111131'99
0:21
R.Hinelick
dR6230D
5426
Bronoibetzzeae
no
ugli
0.1
0.1
1
11/13l99
0:29
R.H€tielick
SR6230D
5426
a-6utg1be-azeae
RD
ugll
6.3
0.1
1
11/13197
0:29
R.Hitielick
SR6230D
5426
sec-Butglbeazeae
RRD
u511
0.1
0.1
1
11113/99
0:29
R.Hittelick
SR6230D
5426
tert-&it'glbeazene
ND
ug/i
0.1
0.1
1
11113/99
0:29
R.Hiae1€ck
SH6230D
5426
Chiorobenzeae
RRD
ug/l
0.1
0.1
1
11113/99
0:29
ffAnelick
SR6230D
5426
2-Chlorotoluene
ND
u111
0.1
0.1
1
11/13199
0:29
flAtielick
06230D
5426
4-Chlor*tolueee
HD
ug/l
0.1
0.1
1
11113199
0:29
R.HLtielLek
SR6230D
5426
1,2-Diobiorobenzene
KD
ug/1
0.1
0.1
1
11113/99
0:29
i1Anelick
SR62300
5426
1,3-Dicblorobenzene
RRD
ug/l
0.1
9.1
1
11113/99
0:29
RR.Hinellok
M6230D
5426
1,4-Di.hlorobenzene
HD
ugfl
0.1
0.1
1
11/13/99
0:29
flAtielick
SRi6230D
5426
Ethglbeazeae
HD
u511
0.1
0.1
1
11113179
0:29
3fAtielick
SR{UM
5426
Isopropglbeazene
RRD
u9/1
0.1
0.1
1
11113199
0:29
n-Hinelick
06230D
5426
4-Isopropg1toluene
RRD
ug/l
0.1
0.1
1
11113199
0:29
n.Hittelick
SN6230D
5426
RRaphthalerfe
RRD
ug/I
0.1
0.1
1
11/13199
0:29
M. Hinelick
SH6230D
5426
a-Propglbenzene
No
ug/l
0.1
0.1
1
11i13/99
0:29
R.Hinelick
S1162300
5426
Styrene
HD
u911
0.1
0.1
1
11113199
0:29
ft.Hitiel€ck
SR62300
5426
Toluene
0.3
u9/1
0.1
0.1
1
11113/99
0:29
".Hinelick
M6230D
5426
1,2,3-Triehlorobeazene
No
u9/1
0.1
0.1
1
11/13/99
0:29
M.Hlnelick
06230D
5426
1,2,4-Trichloroberizene
RRD
09/1
0.1
0.1
1
11113/99
0:29
H.Hlnellck
M623DD
5426
1,2,4-Trinethglbeazene
No
ug/1
0.3
0.1
1
11/13/99
0:29
ft.Hittelick
MUM
5426
1,3,5-Trinetbg1berzene
RRD
ug/l
0.1
0.1
1
11113/99
0:29
N.Hinelick
StR6230D
5426
nj-xglenes
}RD
ug/l
0.2
0.1
1
11/13/99
0:29
H.Hinelick
SH6230D
5426
o-xglebe
?RD
ttg/l
0.1
0.1
1
11/13/79
0:29
Ri. Hinelick
SM6239D
5426
Hexacblorobutadiene
RRD
ug11
0.1
0.1
1
11113199
0:29
R.Hitieiick
SR62300
5426
Oronocbloronethaae
No
u911
0.1
0.1
1
11/13199
0:29
R.Hinelick
SH6230D
5426
Bronodichloronethaite
RRD
ug/l
0.1
0.1
1
11/13199
0:29
N.Hinellck
SM6230D
5426
Bronoforn
no
ug/l
0.1
0.1
1
11113/99
0:29
ft.Hitielick
3R62300
5426
Brononethane
HD
0911
0.1
0.1
1
11113/99
0:29
R.Hittelick
SH6230D
5426
Carbon tetrachloride
HD
ug/i
0.1
0.1
1
11113l99
0:29
flAnelick
SH62300
5426
Chioroethane
HD
ugil
0.1
6.1
1
11/13199
0:29
It Hinel€ck
SR62300
5426
Chlorofrsrn
RRD
ug/l
0.1
0.1
1
11/13/99
0:29
N.RHinelick
SN62300
5426
Chloronethane
RRD
u9/1
0.1
0.1
1
11113199
0:29
RI.Hinellck
Sn6230D
5426
DlbroHochloronethare
no
ug/i
0.1
0.1
1
11/13/99
0:27
11.RHinelick
"6230D
5426
1,2-Dibrowethaae
HD
u911
0.1
0.1
1
11113197
0:29
R.Hinelick
SH6230D
5426
Dibrononethine
RRD
ug11
0.1
0.1
1
1111,3199
0:29
flAtielick
S1162300
5426
COPY 1

SPECIALIZED ASSAY'C
2960 foster Creighton Dr.
P.0. W)x 40566
Nashville, TN 37204-0566 A t'+tl A Y T I4-- A tt._ R3-= tP O R-r
Phone [phone]
Laboratory Number: 99-A169379
Sample ID: 9K100-002
Page 2
Report Doan DI1
Aaalyre result units Limit Limit factor
Date Tine Analyst "ethod catch
1,2,3 'richloropropane
YD
ug/3
0.1
0.1
1
11113/77
0:27
ff.Hinelick
M62300
5426
v"lnyi Chiorlde
lets
sign
0.1
0.1
1
M'13/99
0:27
tf.Hineliek
Sti6230ii
5426
Dichlorodiiluoronethine
RD
u911
0.1
0.1
1
11/13/99
9:29
It. Hinelick
SUM
5426
1,1-0i.hloroethane
HO
ug/l
0.1
0.1
1
11113199
0:29
M.HinelLek
S1162300
5426
1,2-Dschloroethane
HD
u9/1
0.1
0.1
1
11/13/79
0:29
n.Himelick
M6230D
5426
1,1-Dirhloroethene
HD
u9/1
0.1
0.1
1
11/13/99
0:29
It Hinelick
SM2300
5426
cis-1,2-OLchloroethene
Il0
uy/1
0.1
0.1
1
11/13/99
0:29
ff.Hinelick
MGM
5426
trans-1,2-Dichloroethebe
RD
ug/l
0.1
0.1
1
11113/99
0:29
n.Hinelick
M6230D
5426
1,2-D€chlorapropane
HD
ug/1
0.1
0.1
1
11/13/99
0:29
M.HimelIck
MUM
5426
1,3-Dichloropropabe
MD
ug/l
0.1
0.1
1
11/13/99
0:29
N.Hinelick
SH6230D
5426
2,2-01chloropropane
#D
u9/1
0.1
0.1
1
11/13/99
0:27
n.Hinelick
SM230D
5426
1,1-Di.hlorupropene
HO
v9/1
0.1
0.1
1
11113199
0:29
R.Hinelick
Si MOD
5426
cis-1,3-Dichloroproyene
#D
u5/1
0.1
0.1
1
11/13/79
0:29
n.Hinelick
MUM
5426
trans 3,3-Dichloropropeae
NO
UP/1
0.1
0.1
1
11113/97
0:27
n. Mmeliok
M6230D
5426
fethglene chloride
Htk
v5/1
0.5
0.1
1
11113/97
0:21
if.HInelick
SN62M
5426
1,1,1,2-Tetrachloroethane
no
U411
0.1
0.1
1
11113199
0:27
if. Hinelick
Stt62300
5426
1,1,2,2-Tetrachloroethane
HD
u911
0.1
0.1
1
11113/99
0:27
f.Hinelick
SitUM
SC46
Tetrichloroethelle
HD
ug/l
0.1
0.1
1
11113199
0:29
n.Hinelick
SR6230D
5426
1,1,1-Trichloroethane
HP
ug/1
0.1
0.1
1
11113/99
0:29
tf.Hfnelick
3"62300
5426
1,1,2-Trichloroethane
HD
u911
0.1
0.1
1
11113199
0:27
A.Hlnelick
S1162300
5426
Trickloroethene
RD
u9/1
0.1
0.1
1
11/13/77
0:21
n.Hinelick
S"6230D
5426
Iricklorofluoronethane
#D
ug/1
0.1
0.1
1
U/13/99
0:27
N.Hinelick
SM230D
5426
1,2-01#rono-3-chloropropane
8D
u9/1
0.3
0.1
1
11113/77
0:27
11.Hinelick
SUM
5426
?liflSf:iuAEMS CHOISTRY
Total organic Carbon
1.6
ng/2
1.0
1.0
1
11/15199
21:30
A Hardison
415.1
6373
Total Urgaoic Halogens
HD
n911
0.010
0.010
1
ll/20/99
1I:27
A Hardison
90200
3360
V = ?rot detected at the report limit.
Surrogate
'/, Recovery
Target Range
5011502 Surrogate #2
501PM Surrogate #3
95.63. - 122.
68. 57. - 117.
COPY

SPECIALIZED ASSAY`4�1C. �F ,
2960 FE,?ster Creighton Dr.
E O. Bo;x 40566
Nashville, TN 37204-0566 +4P4 L—YT S C rAL_ R 3E—=P OR T
Phone [phone]
Laboratory Number: 99—A169379
Sample ID: 7KIOD-002
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permissions of the laboratory.
Report Approved By:Report Date: 11122l99
Theodore J. Duello, Ph.D., Lab Director
Michael H. Dunn, M. ^a. , Technical Director
Johnny A. Mitchell., Dir. Technical Services
Eric Smith, Assistant Technical Director
Gail A Lage, Technical Services
Laboratory Certification Number: 387

70-0
Z6 C
ND0m
Z3 n
00
� 0
w
n
CD
W
s
0 :c
5wooC?,..u,m
—CDCD
CD CD
0 QT
n,
w Uy z
O
=m
cn
CL c
N
En
CD • a
O o
_ m
z
�c
C
n
33533333333
ca cQ o cQ cQ to co cn co —•ca
0o p�
oo0>
33
n -
om C
CA
O
3
CD
m
N N
O CCD
O m
� � O
003
a
c
KK7=MC)OOOM>OMZz i
OCo a:) O C Q.w w
M a
0 K:0; C nnMD•0p-0 CD CD
=n cn c"D =•0 O a0 �•3 ?O^Z x
2 0 3�'03'EncZO
w CD C C -0 Cn N -C
N C 3� 0 3 3 3, �w w N
CD w CD cn
w Zz
w
z
0
n o -
O o m
� c
o �o M
O o
co c�
a
33333333333333SM
c0 � cn cn cn cn cn co cn cn ca cn � cQ cQ a
a
Om
C
n0 n
D
Mz
cn
CD a"
a3 n
CD
CD 0
333cchEL
CD CD fD � (n
0 0 o n
at at cu r
n n
Z�
O cr
I a
C5
O 3 0— �x
CD "
o Nrz -<
c i3� i3 Cl)
m w CD
Q. Z
0 0
an
CD i
OCL
z
o
C v
N
m
a
n o
CD
o t cif
O
orb LJ
c3333
2. c0 cn cn

0
m
z
cn
y
I
I
I
I
x
Il
I
I
n
o
-'
°n'
>>
x
o
A
a
p�
o
o01
p
--
p
A
N
0
N
1
In
H
W
a
n
Ln
?
F
9
9
9
9?
c
3
3
9
9
3
9
c
Oq
g
x
x
x
x
m+
y
d
c
c
F
Ow
10
o
c
oZz�
c�
�
H
H
a
N
T
Cn
nWH
O
N
H
VI
o
a-
0
N
0
0
o
n
\
x
x
x
x
c
Z
z
a>
Chit
W
N
V1
O
N
hi
_
V1
N
V
O
V
O
.p
t0
p
\
\
\
\
\
\
\
\
\
\
\
\
\
\
O
>
5
^
A
-
m
r
c
7ao�
iOo
,y
O p
v .•
O
a
azo
0
r
v�
p
o
e
n
0
m
n
000
n
o
a
-�
a
z
O
3,
r
F
C
�
C
a
r
�it
�
�
O
a
0
o
�
s
A
rr.
Y
a
� ry ry n f�i
m a
00
ljp �
e e
O I
Chi
r�
•
rm
7
F

II
I
I
I
I
I
I
�
o �nDni
mw
-_
OOo
m
c
Oo
o
Q o
o
Q
m
cr m
y
a
N.
c
0==
o
v
v
D
to
a
CD
s
(D
a 0
O
fn
W
O
�J
te=
a
X
a. •O
'Q
C
�i
�•1
W
>cn
•�
a
O
w
Z.
(D
O
(D
D
N
a
s
C
C.)
C.)D
Vt
O
(JI
O
a
�
CD
(m�
///J��
m
C
Vn
c
C '
cC
(o
R cn
c
to
cn
3
Z
a
o
cn
3
3
i
rl�
O
c
c
w
p
o
o
=
d
a
o
a
c
a
CL
c
(o
cn
A
Q
Z
o
fii
a
CIO
a
y
(n
(A
m
O
CD
y
Q.
Q
=
0
'�'E
�
N
C
`D
en
Z
w
cc
0
3
W
0
Fro
rn
a
N
d
(/1
N
�
N
NCn'II
z
m
�I��=-
naa0i
DD
a
c
nmi
y
—
O
mD
A
t
10
c
o
m
O
a
A
G
i
(a
O
a
v
mc
3
CA
r-
rn
3
c
ce
c
c
3
3'
c
3
c
c
a
Q
Cy!
3
a
m
C
a
V
W
3
3
�
Cn
Co
(D
3
m
CO
O
a
a
a
(DTI
8' Q1
Uci
�
Qai
Qi
•2' 8� Q
Q�j
C,
T
OG
N
C,(n
N
�
�
a
CT1
c
CO
V
�3
U
nm
10
m
`Y U
in
c
kin
c
c
0
3
c
3
3
c
c
c
c
3
c c
c
c
R.
Z
T
"O
O
"0
cD
0 D
nmao
Z
o-
O
2=su
23
m
0�0�
(D
pa
w
o
w
a
o
x
cD
CD
°
y
CD
CA
=•
mm
d(D
Q
F
CD
°
=
!•
3
A'
(D
c
-0
In
C
o
O
y
N
W
cD
Q
a
o
(D
W
CL
CD
.
V
A
0
aCD
T o
m_
c
D:a.
CD r-1
O
j
c o
O a
D
In (D
Z `-
o
D cz
y
o
0o
I-
a
uo
6`
m 3Z
p
O
C/)
t?�_
0
n n
i].
K
-4
a
CL
a'
o a
m
�
0
0
m
o
v
6�
o
0
CD
y�
n
o
-44
0
n
�
m
DCAvr°
D 0 (D
33��,
❑
K_°
(n
�(D OCD
oCL
m _0
w
0
CD
.t1 c (D
CL
'C
(D (D
If
e �
a r
as
0
3
a
CD
3
(D
Z
23
ElQ In
O
aDi
(D
a0i
M - (D
n
(D
m
v z
c
CD
o
I
(�D a-
0
co
1CD
S
Q
v
_vp
C �
(A m
Z3
O�
110
D3
ms z
=3 o
D3
D � �
r_
•mot � A
� Um m
O,
� � O
m-
3
aCL
Zm
ac
-4 ,
m
m y
ma
n
Z w

co
n
�G
()
O
O
O
T
O
D
D'a
M
m
-•(
C
-4
O
0
p
0
O=
0
o
w
w
O
p
.T
S
0)
o
w
w;,F
w
x_
v
T.
n-
'
aa?
®
D
CL
(D
a0a0
W
ca0o
3
o
O
im
c.
m
a
O
w
m
o
o
o)
a
CD
(n
C
T1
'Pl
CA
Ul
A
x
o
A
O
00
A
CDn
D?
D
Z
N
CA)in
a
-
CA)
D
N
a
o
;
CT
O
Ul
C.
A
-
a)
3
(c
0
c_
c
cn
3
(n
3
3
=
3
(n
3
(o
3=
(o
=
3
co
z
C
3
z
0
0
3
(°
3
(n
3
H
z
z
Q
c
c
w
m
m
m
o
o
m
CD
y+
w
((DD
m
n
F
o
to
CD
D
CL
(D
CD
O
—
(n
z
O
Q)
Z
Q
v
A
CA
(D
A
al
C7
p
W
r
W
0
M
(n-
O
CD
d
o
0
O
w
w
z
_O
(D
�
°
Q
w
rn
Ca`
rz
o
csa
C
`
O
3
3
3
3
3
3
3
Z
c
B
3,
-
n
3
N
=
33
u
N_
Z
z
K
K
7
z
m
c
n
N
m
D
m
o
w
1
,
,
-
1
,
a
1
1
1
cn
r
(n
o
-
0
n
n
n
�n
D
c
�
C
7
y.
C
C1
3.
C
C
-a
c
A
CA
3
T,
3
cn
CA
A
c
c
3�
i9'
A
3
A
A
Ln
y CD
m
C
A
O
�'
(O
CJ
lA
O1
A
d.
CD
(n
(B
(iCP
Cfl
rn
A
W
Cis
cr3
5
O
M
q
O
N
CA
CP
Ul
N
O6
....
i
cn
(D
CJI
CD
O
tD
,may
e
i
c
c
c
3
c
3
3
c
c
c
c
c
3to
c
c
c
>
>
>
m
-1'1<
'0
�q"9i(n
_0zO6
C�
'
1
-1
O
!0
(D
0
;
(� W
(D
®w
O
m
_
Doi
O
�
=
a
�
0
7
'
�
®
D
(i.D
07
(D
n
C
m
R
C
O
n
y
N
n
m
D
m
-
n�i
0
o;
(mil p
to
m
CL
CD
w
-n b � n CQ
�
JJ
� v CD
m 3 g,�,
c
o?
Tl (o •°
cn
m
(Da
0
j
p.
O
~.
p�1j o
W
O
1
D cr
o
N (AD
Z
W
C:
c
°
cl)
0
-n
C0 (D
AA
a
o
a
-�
CL
U(CD)
aA
o(DO
o
pow
6'NCD
°
a
L
O
m
E
CD
O
o
Cn m ® ®
° (D3
3 n w
-o
(D
w
3
(o O O
C)
O N ro
a
0
a
0
w�
O
p
R
C
D
M
(WD m
C7
CL(D
n
(D
m
a
"I
co(7 (3D
O
C
w
w
7
CL
0v
ro
a
o-
z
c
3
cs
ro
VI

I—icoCJ»Qfin�7—�� Oz C�C7C7
ZvCD (DCD, 'O=�m0OQ
in :3 m —cn
CD --C m -, -•
ZeO O n CD CD CD
Cl.a� Cn z
O 3 i7 -n �cn
U —
n Cl) N Q o O (D Cl)
CD
CD iU m t�A
?_ O
3
m
a ^�
ro ^N
n 3 N)
A W M o OCD
m �
O m
- A p_
3 3 s3 3 3 3 3 3� 3 003 .��.
to cn 0 cc cn Co cc cn cn = cO 3 3 R.cn CD
c
��T2TiC�C�C�C�O�DQZ7ZZ
Ica (0 CD m
K K° EZ-, 0 3 C� C� 07 D 0 -0 m CD
O O • w A) w O a� ^ �C
Ica c�'n -a - Q-0 -•3 0 0^z
cn - �.� 0 3 3 �-C cn ZO
w CD C -� 3 C-6 cnCO, N -G
COD c 3 O = ..GN
cD 3 W cn
CD O cn
M. zZ
Z
O
O m
o a
c� � o c�
o.
333333333332
cn cn cn cn cn cn cn cn cn cn cQ a
CD
a
0a cn p 3 N 0— Ix
;,D oNrZm
DCD Z o M•� N
n� n CD
°, Z
0vN
CDCL
s^ no
53n ��
-G n ° - ZO
CD 0
sow D= �a
a 0- 0 ,,,
at * � m C-) o
o 0
00ID
Z . =3 o 0
0 v' cn o
I co uI
p

boa c 3n'1a Do
Zsu � cD 0-0=C m
0)=.;--pcnc=. �cc
cn 3 n —ca c�'CD CDm m
z3n � Qa�
00 CL _CI)z
c• O w m
� c —
"" N CO °a
ao
ca ?
•c
e
c
n a
N a)
• O �
00 O w
� v
C
33�333333�3
cn (Cl o to cQ to to to cc = cQ
-cn ;===�=w =
00n
00
33
n-n
i -n N
O 0 w
tw 3
O
3
c�
m
N N
Ln
• O
O �
e
.` O
A
oa3
3 =1 CO ca
c.
KK7C='nOOOOm>O'Ozz
KK0 Ko 03 0C�m C �
wcnc� �..3-0 00
= "cn,3�c 0 3 3 "=-"�
CD �oyN
a� z z
v
C
z
0
O m
CO
a
DO c�
a
33333333333333a�
cQ ca cQ cQ cQ cQ cQ cQ cQ cQ cQ cQ cc cQ cQ a
a
< M- 0
O� R
D Z
0
�w N
c9�^
Q� C)
3 3 3 CA 0. K
m ce m � cn
_Dr-
CLCLCL
_. p) n
3
Z0
0 •r
I V
O
v
O3W�Z�
�
o NrZ •�
CD
F � w CD CDW
0 Z
0 o I
m
c c Z
0
o.
to
w
a.
o C O
a
CD Ln
' `1•, \J c33,33

Mw4r, 0,
I N c o R P o R A T E D
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
23601 8K165-002
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
11/04/1998 10:15
Rep.
Date
Analyte Method
Result
Limit
Units Flags
Analyzed
6230D (GC/MS CONFIRMED AQ) 6230D
Benzene
<0.50
0.50
ug/L
11/12/1998
Bromobenzene
<0.50
0.50
ug/L
11/12/1998
Bromochloromethane
<0.50
0.50
ug/L
11/12/1998
Bromodichloromethane
<0.50
0.50
ug/L
11/12/1998
Bromoform
<0.50
0.50
ug/L
11/12/1998
Bromomethane
<0.50
0.50
ug/L
11/12/1998
n-Butylbenzene
<0.50
0.50
ug/L
11/12/1998
sec-Butylbenzene
<0.50
0.50
ug/L
11/12/1998
tert-Butylbenzene
<0.50
0.50
ug/L
11/12/1998
Carbon tetrachloride
<0.50
0.50
ug/L
11/12/1998
Chlorobenzene
<0.50
0.50
ug/L
11/12/1998
Chlorodibromomethane
<0.50
0.50
ug/L
11/12/1998
Chloroethane
<0.50
0.50
ug/L
11/12/1998
Chloroform
<0.50
0.50
ug/L
11/12/1998
Chloromethane
<0.50
0.50
ug/L
11/12/1998
2-Chlorotoluene:
<0.50
0.50
ug/L
11/12/1996
4-Chlorotoluene
<0.50
0.50
ug/L
11/12/1998
2-Chloroethyl vinyl ether
<0.50
0.50
ug/L
11/12/1998
1,2-Dibromo-3-c:hloropropane
<0.50
0.50
ug/L
11/12/1998
1,2-Dibromoethane
<0.50
0.50
ug/L
11/12/1998
Dibromomethane
<0.50
0.50
ug/L
11/12/1998
1,2-Dichloroberzene
<0.50
0.50
ug/L
11/12/1998
1,3-Dichlorobenzene
<0.50
0.50
ug/L
11/12/1998
1,4-Dichlorobenzene
<0.50
0.50
ug/L
11/12/1998
Dichlorodifluoromethane
<0.50
0.50
ug/L
11/12/1998
trans-1,4-Dichloro-2-butene
<0.50
0.50
ug/L
11/12/1998
Page 29 of 31
1491 TwILIGHT TRAIL / FRANKFORT, KY 40601 / 502-223-0251 / FAX: [phone]

M
I N C O R P O R A T E f)
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
23601 8K165-002
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
11,/04/1998 10:15
Rep.
Date
Analyte Method
Result
Limit
Units Flags
Analyzed
1,1-Dichloroethane
<0.50
0.50
ug/L
11/12/1998
1,2-Dichloroethane
<0.50
0.50
ug/L
11/12/1998
1,1-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
cis-1,2-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
trans-1,2-Dichloroethene
<0.50
0.50
ug/L
11/12/1998
1,2-Dichloropropane
<0.50
0.50
ug/L
11/12/1998
1,3-Dichloropropane
<O.50
0.50
ug/L
11/12/1998
2,2-Dichloropropane
<0.50
0.50
ug/L
11/12/1998
1,1-Dichloropropene
<0.50
0.50
ug/L
11/12/1998
cis-1,3-Dichloropropene
<0.50
0.50
ug/L
11/12/1998
trans-1,3-Dichloropropene
<0.50
0.50
ug/L
11/12/1998
Ethylbenzene
<0.50
0.50
ug/L
11/12/1998
Hexachlorobutadiene
<0.50
0.50
ug/L
11/12/1998
Isopropylbenzene
<0.50
0.50
ug/L
11/12/1998
Isopropryl ether (IPE)
<0.50
0.50
ug/L
11/12/1998
p-Isopropyltoluene
<0.50
0.50
ug/L
11/12/1998
Methylene chloride
<0.50
0.50
ug/L
11/12/1998
Methyl-tert-butyl ether (MTBE)
<0.50
0.50
ug/L
11/12/1998
Naphthalene
<0.50
0.50
ug/L
11/12/1998
n-Propylbenzene
<0.50
0.50
ug/L
11/12/1998
Styrene
<0.50
0.50
ug/L
11/12/1998
1,1,1,2-Tetrachloroethane
<0.50
0.50
ug/L
11/12/1998
1,1,2,2-Tetrachloroethane
<0.50
0.50
ug/L
11/12/1998
Tetrachloroethene
<0.50
0.50
ug/L
11/12/1998
Toluene
<0.50
0.50
ug/L
11/12/1998
1,2,3-Trichlorobenzene
<0.50
0.50
ug/L
11/12/1998
1,2,4-Trichlorobenzene
<0.50
0.50
ug/L
11/12/1998
Page 30 of 31
1491 TWILIGHT TRAIL / FRANKFORT, KY 40601 / 502-223-0251 / FAX: [phone]

I N C O R P O R A T E D
ANALYTICAL REPORT
Michael Teixeira
BURLINGTON RESEARCH
1302 Belmont Street
Burlington, NC 27215
Test. America Job Number: 98.02843
Client Project ID: SUB 1482
SAMPLE NO. SAMPLE DESCRIPTION
2360j- 8K165-002
11/13/1998
Matrix Type: WATER
DATE -TIME SAMPLED
11/04/1998 10:15
Rep.
Date
Analyte Method
Result
Limit
Units Flags
Analyzed
1,1,1-Trichloroethane
<0.50
0.50
ug/L
11/12/1998
1,1,2-Trichloroethane
<0.50
0.50
ug/L
11/12/1998
Trichloroethene
<0.50
0.50
ug/L
11/12/1998
Trichlorofluoromethane
<0.50
0.50
ug/L
11/12/1998
1,2,3-Trichloropropane
<0.50
0.50
ug/L
11/12/1998
1,2,4-Trimethylbenzene
<0.50
0.50
ug/L
11/12/1998
1,3,5-Trimethylbenzene
<0.50
0.50
ug/L
11/12/1998
Vinyl acetate
<0.50
0.50
ug/L
11/12/1998
Vinyl chloride
<0.50
0.50
ug/L
11/12/1998
m+p-Xylenes
<0.50
0.50
ug/L
11/12/1998
o-Xylene
<0.50
0.50
ug/L
11/12/1998
SURR: Toluene-d8
72.0
%
11/12/1996
SURR: 1,2-Dichloroethane-d4
74.0
%
11/12/1998
SURR: 4-Bromofluorobenzene
85.0
%
11/12/1998
Page 31 of 31
1491 TWILIGHT TRAIL / FRANKFORT, KY 40601 / 502-223-0251 / FAX: [phone]

.30
m m
< O
CO
`U
(D
m N
sL
c m
QO
3
a0
c -*
(D 0
3 O
aCl)
CD =
O O
O
0 N
0
m•
CA
0
0
O
CD
a
a
CA
N
01
a
O
CD
C)
m
Z1
T�
—I
1.
U.)
:1)
m
71
�i
U)
�7
C-
m
D
z
0
D
C)
C:
D
m
Z_
O
m
O a�
c: v
0
O O
G
0 c'
O �
C1 CD
O �*
= c'
cn O
CND 0
CD 6
f# CD
CA)
O-
0 O
� c
U CL
a)
0
X0-0 C zT�'- 'DS0=�° O O 0O
CD �, CD (D CA m = �,
Z� o :3 2) =3 M. 0 c 00 P
c 0 CD CD CD n Q G
z nco � CD CD
3 0 t� O U)z
00 � Qo3 -nT1
2. 0_ 00 W (D —i -n
n u, N Q' o3 O CD
zCD a
H. C L —
h 0 —OCD
-
K
0
CD
A a
O n N U7
O rn VVv C
Un
In y C
3 3 =3 3 3 3 3 3 3 Z)3 003
c0 cQ O cQ c0 cc cQ cQ cc c0 7:;c0 3 3 c0
ZKKAMMnC)C)OM>Mzz
� CQ i CQ (D)
C� Q i C
I I O > cn
.-.
Cn��� �o n_3 C 0m`0 m cD
2OCQc�O76cQ"0=•3ozz
ccQ Q T.� 3 3 3"3 0 c p0
3WCDC: �" ccnC'O
me.3`G 033 3—{"c,
mcn
3 z
—z
sy
CD
-o
O
0 0
o O•
O W O O
In
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
00
O
CD
CD
w Cf
o m
= O
o n
O
3
-a
O
C
Cz
o
w
0-
�, -0N-0Z
0 CDO0-
CD
a O CD C7
CC) cD n QCD CD
-0 2
O
C CD
cn n.
CND
9
1,4
"j0C: c c
3 3 3
D CD ,_
0 (D a
m m CD CD CD
cn>=3
r
CL
r w o
m� 3 w O
o CD 0
CD *-a
c0 � CD 7 o.
-1ZC
O w yi w
w CD
o CD w o
m 3 o
-
o
__0
u� CD
Nz
�
CD
m
3
�°
D
a
Vnm
3
N
C-
W
W
Cn m
m
n
m
a
Ca
CD
O
�� 0
6 m m
w
r
t-t
00 CD
O O CD
r
o
(D
m CD
n
o 3
w 3 g
mCL
C L W
v
rD
Cn
3
c) Cc: m
c
c
Z
(D _
�
n
CD
m�
07
N
N�
m
w
`4
CD
v
o
D
w c
CD -0
z
>
i1
w 0
CO
3. �
-0 O
N
v
a�
D
O�
0
V
v
\o
I"
�
00
m
v
�
'o0
00 C)
oo
�
m
CA
CD
Q
N �
o Do
� 00
�
z
OD
O
O
00 _0
Ul CD
w
m
° _ ° T
w a c
n
D
o -o
-o C
r
CD
y a
6 w
o
h
o
0
U)
giro
Cn iv O
fD W
W fD 0
rr X
� V
HI-'O
W
N
rt z
Cj i
N
t00
O
N C] F
w
:30
ct �
n
1-�
tD
I-'
r-'
cD
d
0
a
v
m
CA
N
�o m
Q m
co =�
m nzzz
mo-uo c
v 0MC)
0 U) m
Cl) Zw
O C) m
0
DO Q
m� c
�� m
v
oUl
co
m
z
G)
K
O
Z
vC
CD
CD to
0
C7
�
-0m
m
-0C
0
0
0
f
w
�
7
y
C
N
a
CD

x
O
O
0
A
N
O.
W
W
o
�a
a
3
3
x
x
x
Ix
.y
.5
z
y
z
o
o
y
o
z
O
N
3
O
COIL
3
O
fN71
3
3
O
(OJI
3
3
3
3
3
3
A
�
3
c
c
3
33c
3
� 30
0
N
x
I
I
x
I
x
x
m
Y
w
m
0
d
5.
n
O.
N
o
O
A
A
i.
J
�
J
CA
CT
V
v
A
A
0
o
a
n
o
o
r
o
0
8
m
x
�
O
b
S
O
S
00
N
Ij
N
O
�
o
a
a°o
co
A
v
O
yy
y7� a
n
z �
o
a
r
►e
101
x
0
O
R
�o w v
ei M.
g
H ^. 0
w S o
..
0
0 q.
G.
C
W Cx)
O
�
0
m
3•
y
-yt
m W
�
C
C
Cw
O
O
m
.�.
v
O
m
A
m
o
W
m
O
H
i9
z
g
�
A
Y
k

n
0
3
CD
Q7
'o
0
l<
0
0
O
0
C13
0
D
D
--I
c
o_
0
0
0
07
0
o?
w
o
w
,r,r=
(D
O
-000
O
p
O
Er
W
a-w
w
A
�'
r
n_
o
_.
v
v
D
d
".
3a=
0
aQaCD
m
p
3
3
Q
o
C
C
X
Op
(Dw
p
w=
p
(D
a
p
cn
w
c
A
(D
O
CD
D
A
cn
w
is
=a
z
CA
N
A
A
m
a
W
D
cn
p
W
cn
A
O
O
m
Cl)
3
C)
c
3
3
3
3
3
3
r
3
Z
3
j�
0
0
3
3
3
co
C_
=
co
co
co
co
co
7-..
cc
C
3
3
`a
`n
b
v►
%A
�
Pz
=
O
cncn�nv==�v
o
w
a
m
o
sw
a
a
c
+
w
C.
cD
A
cD
A.
=
N
w
(=D
a
CD
(w/J
O
Z
Ow
N
O
d
w.
01
O_
W
O
0
V
'
rn
c
(D
m
p
w
w
al
Z
cn
m
o
0
CA)
�p
m
O
tD
`1
N
a
r
c
3
3
3
3
3
3
o
�
c
3W3!
\
3
DF
7
w
Q
m
c
n
a
w
D
D
T•
su
-
.=
m
w
5
CD
CD
n
m
o
w
o
o
a
w
3<
rn
CD
3
w
m
Cl)m
c
c�
CD
3
3
c
c
ath
4
3
Off
CD
=
y
fA
C
`G
(pJ
3
c
3
A
OAf
�
3
%t
A
cn
(D
3
A
O
cn
t0
c
�
(pn
--�
CO
cn
O
c
Qi
CJ1
(n
Q
0
N
(n
CD
CCn
<O
N
r
1�w
1
cn
cn
Ji-
n3
�m
tEID
c
c
c
3
c
3
3
c
c
c
c
c
3
c
c
c
c
0
0
S=
w
=
3
ca
a
o
�
,
O
y
=
oD
Li
(D
v_
CD
(D
O
O
rriX
o
1
w
(D
Q.
0.
cD
y
o
d2.
y
y
O.
fD
In
CD
CD
<
ID
1
to
(D
D
co
N
cD
o
(�l
�
(D
C
m
7
o
_w
CD
(a
0.
(Q
(D
..
...
CL
CD
N
D —fin n cn
T
n3
m
Cn
m�
•o
j �o
m
o
Oo0
o
CL
-
n'm
m
'
o
m320Q�
}�►�
71
c
cn
(AZ
-
0
00
��
°
�
_
t _
a
==
CL=
aw
m
0
o
0
v
w
0a
0
CD
0
n
t1k
0
n
=v)pr-0 m
m w m 0 * ,
3 3 0 w =
a
w - m
❑
(n(= �• _
°o
0
="
mop
c,
3
�°
3
0] "0
0
w
o
0.
$�
cw°—. o
Q-
Z�
SD
�r
C-)
0
co
w
T3
V_
m
_
CD
w
U
1
1
-a
CD
m
A
°-
m
a
l<
0
CD
❑ ❑ b'
0 ca
5 m
m
❑RI N
mM
3 0 r
CD CD (3D
0 0
ww
w —
0
w
w
CD2)��c
m
m
L
=
Z
(D
=
,a
m
c
0
bcL
(D
m
(CD
X,
w
_
a
gv
C A
N n)
Z
fD
00
Dw
m<Z
moo
D3
D3 =
k cZo A
m m
�? o
0 m -_
Z o.
vZm
Dc
1
m
M
(A (Amo
Z N

r
rn
tom:
0)cr
b
O
3
l<
o=�
w
5F�
m
�
0
0
0
0
0
37
W
S
0
3
o
o
a
Q
Q
w
w
A
y
o-
0-
-
v
v
v
D
(p
N
m
�
co
O
w
m
0
0
(A
O)
K
i
W
°
Oo
O
S
X
CD
A
A
io
O
c
-n
-n
W
°
m
m
A
0
S
2
'o
-1
In
o
Ao
�
00a
is
(n
m
a
o
w
°
w
D
Z
ca
N
A
A
m
O_
w
D
Ut
O
O
N
A
A
Cl)
e
/m/om�
C(o
C
3
(o
(o
3
(o
;o
z
z
O
cn
cn
o
m
m
m„p
o
w+
y
c.
m
m
o
z.
V
A
(D
A
°
n
N
w
N
N
N
N
(D
O
O
a
Cl)°
O
CD
V
N
O
N
N
N
n.
O?
o
VO
O>
(n
z
(D
coCA
w
m
W
o
Q
o
O
(O
0
N
C
0
0
3
3
3
3
3
3
3
�
c
3
3
3=
3
r�
N
co
-0
z
z
K
K
7:
S„
n
n
n
n
w
D
n
D
7
m
Q
Al
7
(D
(D
C-
O.
0)
0)N
�
JO
m
1
o
I
I
I
o
I
,
�
1
1
1
cA1
o
o
N
n
0
3<
°
C
c)
m
CD
ANC3
?rn3
3
C
(nn
V
CA
m
3
im
m
(n
rn
b.
AA3
O
(n
O
N
cn
N
O
Nn
(
i
cn
O
O
V
d
r
d
a
c
c
c
3
c
3
3
c
c
c
3
c
c
c
in
c
(a
cn
o
'0
m
n
z
O
V
xxw
x3
COao'O(°
c_,
=
<
v;
_(o
>
dCD
A
0
'
O
?'
(T
X.
:r
=r
'o
N
n
m
O1
(D
O
Al
w
(D
O
O
d
7
.-.
0
f0
W
N
(D
A.
D
N
a
0
n
(A
N
CD
0 3 o
Fn 0
'(D
DR�J
p m
o
O
I
00
2.
00
w
Cl.
D IT
-.-j
o
m
Z
y
u�
D
W
3 N
o
5
o
m
3Z0
°
-
cn
�
o
o-0
CD
o,
C
P-
n 0
CD
:
OL
n
CL
o
m
O
1
_p
@
O
C
E
m
o
0
oCA
o
O
0
3
M U)
0 m
(D Al N 0
3 o °'
m
❑
�•
N (0
O
O
0
�=
u l CDD : O W
or N (D
1
0�
0
o
a
O
3
-o
(u
5
N
0
c o
OL j
W O K
o U)
r
o r
w�
vw
v o 0
m
o
N su N
7) m
O
°
(D
Z
v —
o
l<
( c
m cr
m
a `�
N
a
i
-n
o
3coW
n
7C'
N
-I
m
O
1
.'J
v_o
< m
cn d
O-
z
Oa
"n 0
7
m < z
xo 0
p3�
Dm
r�
�3 A
D� 01
� S �
70 ? o
Za3
vzly
a
1
m
cn N
m0
n
� A
z N

fJ
JUL , 1998
Groundwater Section
Asheville Regional Office„
�P c aa Qjftm aoz 170
'�crite C�t%/, 28630
July 02, 1998
Ann C,. Rumbough
NCDENR
Division of Water Quality
59 Woodfin Place
Asheville, N.C. 28801-2414
Subject: Monitoring Well COD results
March 1998
Dear Ms. Rumbough:
COD results for the March 1998 sampling event were mistakenly not reported on form
GW-59. Enclosed is a revised report form for monitoring wells #02 and # 03 which include
the COD results.
If you have any questions please contact me at [phone].
Sincerely,
M,
JAo L� —:—
M. Shuford Wise
Huffman Finishing Company

m CD
O
CO
CD
3
(D
(D
O
D
O
CND
Q-
D
CD
0
w
CD
CD (n
C m
0--(D
3
�
cr
m 0 o
v.
aw
%<. "
CD c
— n
O 0
O
0 lA
O
cD
N
O
3
u
a
a
m
CA
v
Q
O
SD
C7
fTl
:T7
:D
cI�
z7
0
•-I
0)
c-
m
D
Z
D
C
:D
rn
0
N
O
O
�. cn
0 :r
O. O
O. C
0 C
CD
CD
CD `•
..« C)
O '*
:3 t2
(n
cn
can 0
CD
(D <(D
� Q
CA)
O w
a Q-
a)
0
-I -I cn Cn ' ;) D C) -i -o z n C'•) C7
0 T . -IN, K 0
�0-0C :-= FJ)-o 000
D
a
''mmmmm
Z iv c) w Z Q- w CD O C7^ (n fD _.: _.:
o
N D-F o m cn �'� �"� y
(D
o W
�. o
m
0
z3 m (D
m-a'
o
m
w
03 O� Q �z ��
M
o m
m
O. Q 0 0 � O m � �
�
3 00 �
�_
w e -_ Q -I T1
0 CD
m
CD= a
Cn m
P_Z
a
w (D w
�
m 3
-
c
QO o -
D
CQ O.,m
3
rr
(D --� ?
n • a
to CD
m
t-.: m
a
rr
c
�7
.;c fl-
m
D
m
-r +-. cn cr
h c
rl c
n
'� -. m m w
ci t"
O
r0
w=im
o.o
m
�l r,
C. Go vi
m
r
m
OP5CO0 cn
n w
m
=
m
;D r
._:.
n
D
0 3
3
Q.
=a
m
C
c� a�.aw
�r
-.
C:
.n c
c� cfl
m Cl)
cn C
r
3 �D 3 3 3 3 3 3 003
Z
��
-
co(c 0 cQ cQ (Q cQ cQ (Q (Q ;:;:(aiQ
m
m
m.
o
m
Tm
�c
7\-n C) C) 0 C) co > m z z
m
:.c
w -
3
a m
(D
-
: o
"'C:
w Zcn cn (D w w
0
o
0
<
' 0 ' cn w r«
CD
D
m e
n p
O O
0 CD
0
=
w
S
O O w w
Q. w (D 0-0 O Q— s O^Z
r1
w o
3
-1
zcQ: T. � 3 3 9•c z - ZO
m
-0
_
W (n Z `< CD 0 � N�
O
v
N5.
Q m
3
cc
O C' w w
OON
D
m3 of
—
n
�.
v
„ „
cn
m
o
m
cn
m n.
c
333E333E3333333
Z ,•a
m
cn (n (Q n cn cc cn cn cQ n cQ cQ cn (Q ca
o
O
a
a
no -UN-0Z
w� w
o (D c 07-`
O (D
0
cn
r-
D c) NrZ
m
a)w
a o
o
o
nn-0�0
n
D
-0
,
O Q (D
O
T
o
m
nCD =
< p CD
0.
a.
a
3
4L o Q
® i CD
' (n
-
a
mn
cn
6ot. I a ' w
''..
O
-u c
m
go
(D°•
Q
-0
o c
o
51
�0
w
7�
c0 c0 cQ co co cc
ID
w
0
-� O
C
(n m
• Cr
ro �
a
t�
((DD
W
N
m
O
0-0o Z
C
0 �
�m0�
OC/) c-n- m
C/) S
D ._
O -m m
m c
D ,
my
O --
03
m
z
O
Z
O
m
0 -

C7
CD
1l
O
OD
(D
D
CD
=
CD
o
D
m
�
c
OCD
•�
Q
D
c
CD
m
D'.
n
m
c.
w
CD
_o
CA cn
Cr CD
3 c
C7
e
CD O
a U;
CD O
n
O
3
O N
S
CD
(n
O
O
a)
a
a
CD
N
CA
Cv
rr
O
C
fD
z
0
N
O
O CCD
C O
�. co
C) a
O O
= v
0 C1
CD
0 . CD
o
O
, -*
O Cz
Cl) N
CA
N O
CD
U Q
CA)
O O
7 O
cr O.
2)
0
x
—
IHCAfJ»a DC) oC)C)
To70 c =rw — =-©=gin � 0 0
ZW0aiZQaoim0C) Jp
ty —: — O � cn _O o c O O
m om—cCDn�oCD CCDDcCDD3 33
Z Q cn
3 O o_ w (n z
•Q oO �os 71TI
Q p O CD
N a " C)
W M
0 —0-
O
CD w a
— m
s
e
c
c
n a
A O cyi
3
o• O
In W O LO • N w
u, o--
c
3 3 3 3 3 3 3 3 3 D 3 003
� (D o co (a co co (Q co co ;:;:c0 3 3 (c
sv�co cocDczraww
W�o �� m,
CDQ3 C)CCn��� K
Qe�o-ae-53ozz
3WmcC � 3035c0nC,ONO
�E3� 033
� 30`ncn
z
cD 3 — Z
v
-o
O
z
H
O
Q o
F" Q • N
Q O N
r✓v
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
co co co co cQ cQ co co co co co co co cQ (Q
-0N-UZ
CD h ,
g CD 0
omOQm
3
O
C CD
n.
CD
to rr
a
c
r°
CD
O G
p
m
D
r
Cn
m
M
m
O
O
r
r
m
O
-a
m
v
e
z
n
r
i
m
m
m
v
a
z
v
m
r
v
a
n
v
m
m
v
xl
p -n 0
W CD f.,,: (D CD CD CD CD
cD ao W= = =
F Cp y = — 17 a 0
3 W o 3 Z)W CD
C
yew*-0a�iro��
CD
Fn A) O.
O ^ O
O C Nz `c
3 m c cn
Q CT CD 6 rt
a
OOw N��3�w
W CD �--L H
a m rD
w
0•
D�
Q- z
aw
(D- 3
�D 0l
c-r I Cd
(D O
rt�cn c -" �
sv�co cocDczraww
W�o �� m,
CDQ3 C)CCn��� K
Qe�o-ae-53ozz
3WmcC � 3035c0nC,ONO
�E3� 033
� 30`ncn
z
cD 3 — Z
v
-o
O
z
H
O
Q o
F" Q • N
Q O N
r✓v
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
co co co co cQ cQ co co co co co co co cQ (Q
-0N-UZ
CD h ,
g CD 0
omOQm
3
O
C CD
n.
CD
to rr
a
c
r°
CD
O G
p
m
D
r
Cn
m
M
m
O
O
r
r
m
O
-a
m
v
e
z
n
r
i
m
m
m
v
a
z
v
m
r
v
a
n
v
m
m
v
xl
p -n 0
W CD f.,,: (D CD CD CD CD
cD ao W= = =
F Cp y = — 17 a 0
3 W o 3 Z)W CD
C
yew*-0a�iro��
CD
Fn A) O.
O ^ O
O C Nz `c
3 m c cn
Q CT CD 6 rt
a
OOw N��3�w
W CD �--L H
a m rD
w
0•
D�
Q- z
aw
(D- 3
�D 0l
c-r I Cd
(D O
rt�cn c -" �
on
w
CD
NCD a
w
r�
o CT
�O =^ CD O O CD
Il
fn
CD
o3 w 38
rt
Q�.aw
.
y ccn
CD
C�
n� m <
rt
BCD
0
r m
m o
cy,
O
CDm
3
3
o
0
CDc
CD-�
> K
0
3
-4
O
CD CD
Q
a3
0
1-"w
w
�
0
0
I
O
3
CD
0
0
CD
-
-o U)
°•
o-
� c
r w
vCD
v r-
0
ni
(D
N
C
CD
G
t-h
m
B
w
H. O'
~ cn
m �
� O
rr« e
a'
O
w 3
G
CD
N
cn.
m m
M m
Am
O =�
�nzzz
mo-Do C
®UO0OOD
O� M
�..
r O�
Oo A
Mc:In
N
w m
un 0
z
co
m
Z
O
Z
m
m
o C7
w
m
T
Q.

w �
m m 1
C O
Oo
rn m
A
m
m
_T
in
x
m
Cn
C
m
D
z
D
n
C)
C
m
CD
(D
31 ..
d
., n
�W_
O
.CD o
G.r-
Q. N
7
cn
A
(D c
C
-0
0
a
n
0
CD CD
(fl
0 a�i
O
:
0 CD
CD
N
A "�
7 CL
O
:n f/h
CA
A
O
(D
(D CD
a
w
N
a C.
w
0
0)
n
<fD
--Cl)cn-0
j>0-1-0
®z 0 Q
Q
°CD
CD roIn�-02�,a
CD O
000
)
w-Q
mO
�
OcOO
�
o�
N m 6 CDCD�D
33
30
�a
®00
w�z��.
3 O 3 -n -n
�•
Qo O CD
w +
N cn o
c)
CD ��
QDo
n
CD
w a
— (a
s
c
i2
A
OLO
A I
h' C7� F" M)
O
O2,
In
O
In r
c
3 3 ZY3
3 3 3 3 3
3 Q 3 003
(Q (m O (Q
(Q
(Q (Q (Q (Q (Q
,�(a (Q
Z���2,°1C�C�C�C�OoD�ZZ
(D o- w W
o D cn w�
Cf) � o C� 3 Q C) 00 (DCD
2.
z
WCDc'� CD--- Q�nW0)
c'3 0 3 3 3 0_� n
w
CCD 3
cn
w o x
O O
O O
O O 00
0
(a (a (Q cc cc (0 (0 (a (Q (a (Q (c (Q CQ (Q
-UN-UZ
-0 CD n (T
n =
O (D C)
o (D n aN
-0 _
n
c (D
CT
Q Q
CD
GQ ccc 333
coo-
p-t �:p�2`<'
D
C. a m' -'CD w m m
CD
�n
(D a® W�
M
0 3 w Q 3=
w
nZmO
*7t4 Z5,0
O
w Na 2. w C� ww
C)
7
(D -
w
m 2 FD' CDNo
sZ
Aa K
m
0 (p
m w
C
(D CD
:9� rt
m
r+ �-O
o�
p
0�C/)
n o a m m
�n o
KJ cn
M
0
w ?
(D n w CD a
cO 3 5 3 3
w
rr
M
O CD
W a -• a Ca Z
,
(D C)
C: W® K c � m
rt
C:n
p w -m-
(v
"
F
m m m
�tJ 00
m
w Q.
C7
w
m
o m
r+ 0
®
w
3CD
o
<
D
Q (D
co c m -n O
C�
v
> cn s
?'
we ao
a
m
w
DQ
(D (Q N
n
r-
v
0-)
m
o
v
o
Ix
�
�m
O
m
w
0
D�
Q- z
mw
m
X JN' O
C,
m�
pm
o�O
cO
0
�°
M
-'Z
z
V
(p
O -0
55 0
O
`)
Z
y
O0
I
I
I
O
w
r:z
Or
o
=
a
C
w
n
w
(o
o D N
D
0
Q �-
_
Q
Z�
o
o
_
m
Z
o
G)
o
I
�
C s
CD
M
6
(�D = N
a
m
(Q c
o
p
P w
w
�C
0
w.
Vl
v,
CD
a
m
m
o z
C C
0 00
0 00
w
CD
c_
m
v

HYDROLOGIC SAMPLE NUM13ER:
HYDROLOGIC LAB ID #
SAMPLEIDENTIFICATION:
DATE SAMPLED:
DATE EXTRA=
DATE/TIME ANPL=
9722343
399
7K501-001
11/19/97
N/A
11/26/97
NETHCED 6230 D (GC-NJS
CCNFIMVED)
ANALYSIS
CAS NO.
SDL
RESULT
ug/1)
( ug/1)
Dichlorodifluoromethane
75-71-8
0.5
BDL
Chloromethane
74-87-3
0.5
BDL
Vinyl chloride
75-01-4
0.5
BDL
Bromomethane
74-83-9
0.5
BDL
Chloroethane
75-00-3
0.5
BDL
Trichlorofluoromethane
75-69-4
0.5
BDL
1,1-Dichloroethene
75-35-4
0.5
BDL
Methylene chloride
75-09-2
0.5
BDL
trans -1,2-Dichloraathene
156-60-5
0.5
BDL
1,1-Dichloroethane
75-34-3
0.5
BDL
2,2-Dichloropropane
590-20-7
0.5
BDL
cis-1,2-Dichloroethane
0.5
BDL
Chloroform
67-66-3
0.5
BDL
Bromochloromethane
74-97-5
0.5
BDL
1,1,1-Trichloroethane
71-55-6
0.5
BDL
1,1-Dichlorcpropene
563-58-6
0.5
BDL
Carbon tetrachloride
56-23-5
0.5
BDL
Benzene
71-43-2
0.5
BDL
1,2-Dichloroethane
107-06-2
0.5
BDL
Trichloroethene
79-01-6
0.5
BDL
1,2-Dichloropropane
78-87-5
0.5
BDL
Bromodichloromethane
75-27-4
0.5
BDL
Dibromomethane
74-95-3
0.5
BDL
Toluene
108-88-3
0.5
BDL
1,1,2-Trichloroethane
79-00-5
0.5
BDL
I
s
JAN 6
Gr©ts�dc
1491 TWILIGHT TRAIL FRANKFORT,
KY40601
502-223-0251 FAX: [phone] / TOLL FREE 800-728-2251

HYDROLOGIC PROJECT NUMBER: K9722343
HYDROLOGIC SAMPLE NUMBER: 9722343
SAMPLE IDENTIFICATION: 7K501-001
DATE SAMPLED: 11/19/97
I�I�Iy.l�1� . 1 � t; �F. •; I �'1 lal� �
ANALYSIS
CAS NO.
SDL
RESULT
( ug/1)
( ug/1)
Tetrachloroethene
127-18-4
0.5
BDL
1,3-Dichloropropane
142-28-9
0.5
BDL
Dibromochl-oromethane
124-48-1
0.5
BDL
1,2-Dibromoethane
106-93-4
0.5
BDL
Chlorobenzene
108-90-7
0.5
BDL
Ethylbenzene
100-41-4
0.5
BDL
1,1,1,2-Tetrachloroethane
630-20-6
0.5
BDL
m-Xylene
108-38-3
0.5
BDL
p-Xylene
106-42-3
0.5
BDL
o-Xylene
95-47-6
0.5
BDL
Styrene
100-42-5
0.5
BDL
Iscprcpylbenzene
98-82-8
0.5
BDL
Bromoform
75-25-2
0.5
BDL
1,1,2,2-Tetrachloroethane
79-34-5
0.5
BDL
1,2,3-Trichloropropane
96-18-4
0.5
BDL
n-Propylbenzene
103-65-1
0.5
BDL
Bromobenzene
108-86-1
0.5
BDL
1,3,5-Trimethylbenzene
108-67-8
0.5
BDL
2-C,llorotoluene
95-45-8
0.5
B u
4-Chl-orotoluene
106-43-4
0.5
BDL
tert-Butylbenzene
98-06-6
0.5
BDL
1,2,4-Trimethylbenzene
95-63-6
0.5
BDL
sec-Butylbenzene
135-98-8
0.5
BDL
p-Isoprcpyltoluene
99-87-6
0.5
BDL
L oz
JAN f a
1491 TWILIGHT TRAIL FRANKFORT, KY 40601
502-223-0251 FAX: [phone] / TOLL FREE 800-728-2251

■SM' • ■ ♦ ■ �i
HYDROLOGIC PROJECT NUMBER: K9722343
HYDROLOGIC SAMPLE NUMBER: 9722343
SAMPLE IDENTIFICATION: 7K501-001
DATE SAMPLED: 11/19/97
METHOD
6230 D (GC -MS
C"CWrnUME=)
ANALYSIS
CAS NO.
SDL
RESULT
( u9/1)
( u9/1)
1,3-Dichlorobenzene
541-73-1
0.5
BDL
1,4-Dichlorobenzene
106-46-7
0.5
BDL
n-Butylbenzene
104-51-8
0.5
BDL
1,2-Dichlorobenzene
95-50-1
0.5
BDL
1,2-Dibromo-3-chloropropane
96-12-8
0.5
BDL
1,2,4-Trichlorobenzene
120-82-1
0.5
BDL
Hexachlorobutadiene
87-68-3
0.5
BDL
Naphthalene
91-20-3
0.5
BDL
1,2,3-Trichlorobenzene
87-61-6
0.5
BDL
Surrogate Recovery:
BFB
BDL = Below Sample Detection Limit
SDL = Sample Detection Limit
86%
i d 2
JAN 1 1998
t �.
1491 TWILIGHT TRAIL FRANKFORT, KY 40601
502-223-0251 FAX: [phone] / TOLL FREE 800-728-2251

m
co
O
-1(Afl1-u" )>C)---0 ®z C)C)n
� -O (_ m a)`_ r - � 0 :E Fn' O O 0
CD
:3 CD CD a w cD Z. � O c O O
3 0 (D O CD CD
n � CD (D@ 3 3
3
o� -IQ �03 �n-n
O, C1 00 cn
U NQ- :rO CD
0 C7
x O (D
w O O 3 —
(D Sll
c
c
A w a N
O O F- C. coo y O
3
(J1 C)EliO cp O
U
C
�
3 3333333�00
33
(O O (O (C (O CQ (o (.0 (0 r,c0 3 3 (c
� w -- -- -- -- -- a-- (n
ZKg: ;;�2- c c) C)
WD�ZZ
A) (Q (Q � h 1 0 -t
U) h O��C)3C�0 -0
BCD
��� O �
Q- w wCD o -0 C: 0— . 0,2 Z
cn
C CQ O cn. C CAD 3 �' ® )
Z3 CO
CD 3 �' Ezz
Z
O
0 0 '_'
o•
0 0 �
C) r' w
w �
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
cQ CO CQ (Q CO (a co (O (o (a (Q (O (o (a
IN
C)
(D CD
w 0
O (D
7
C ,C.
O
3
0
c
(z
cn
N
(z
0=t
� -0N-0Z
L, CD O 0-
CD h i
0- C) NrZ
mm� X
0 Cn (2 CD
"o =
0
c CD
7 (S
s n.
CaD
cn
r
Q,
nol v'
l`s
13338
c c c
3 3 3
CQ (O (Q
(L] (O (Q
Pr- po*2*
® Q w (D . ,(D CD (D (D (D
C/ C-:.. OCD
O
m O 3 w o 3 w
-'' o
0 30 CD
CD = - o
o
r
mfD CD = C N N z
�c
D Q CAD 6
CA CJJ Ln � W ¢
Fi '
cO ([
m C N L CD w r
m cl) cr
O O 0 0 6 CD m
r (D o O (D
mW CD CD
0(D o 3 3° e
CD
m (D Q �_ Q r
® C O N C (D h
A'� C < (�(
Z
,n COD 0 r
r
m
m w 0 -
p 3 0 0
_0 CD
Z m c CD -n a
v ? ¢'
m
v d 3 (fl
0
o
m �
m
® 0
n
I '
x
mm a
o
" o
I o
Z (D
0
O 7
�70
I I I
D)
(D o :
w C,-
-0
m
Sh]iJ 6 �
� o
o �
o_
m I
0 v Cl)
s -2,
CD M�
rw
vCD
v
v
CD
c
CD
w
D `<
o- Z
C1 w
CD(D 3
CD m
D
J 0
n C
Z CA
N
0)
n v
wI
O
7
(D
CD
(n
cn
70 m
m-0 7)
pm
e0 �
70�ZZZ
mo-oo c
mp(n
OU)� m
O o ((DD m
r m ON G
0 m CT7
o w m
O Ul
z
co
m
Z
I 0
O
z
c O
CD m
m
o (7
w
O
w.
m
R

wr
f
m
0
Z
p
p
_
=
m
3
m
o
c
c
I
..
n�
m
N
p
_�
=r
S
'^P�'}
x
O
U3
gyp'.
n
CD
0
0
m
F
_
o
O
N
mCD
N
n,
a
0
m
o
L�
-,
m
!"i
m
D
cr
N
a
0
N
m
m
m
N
a-0 3 „j>o
a
-a-'
CD-0
w�
�o
v
a
0
-0
w c
a
z�
A�
cr
x o
U��I
u) (D
in- D v y
ED r �3 y
m3Zo r) 6\�
�
�'Z
m
0
°
onm
� A:,
a
r (
o
c
O
c'
Q
w
n
N
aA
0 0
j0
�o
1
CD
��
oo
wU
o
O
v
Er m
1
0
�W
N
cn
0
v
cn
�"
m
3
*
CO
>
(n
j
o
D
m
fil
0m
3
—
w -0
C
m
13�
�o
5 N
m m
O
m
i�
G�
w
r3 S
w• �
0 W
EC r
vo0�o
o�
O
y cD N
m Q (D Z
Q. CD
Q.
-03
� � _
CL
j"
mcn
3
m
v
CD
-
n v
3 v
1
A�
1
Q J
W
lr
o CD
�
C
l
c
N'
w
��
a 4
0
<
0
zo
Ovm,
m�
z3
< ,D
��
z0
m =
Z5.Z
> 0 0
8 ; S
Z -
n
2
mdd
1
Jzm0
rL _
Z al
d
O�
cm
vm
-Dt c
m�
m 0
m
c�
m
n
O
Z

ro
st-
N
'
`c
X
O
o
e
0
0
0
N
d
t/r
o
A
W
a\
n
cn
C
fC
fA
!�
fp
W
W
O
O
�.
_i OD C m
m
m
O
C
Cy
mn--ii
to Z
O
°
m
z{
O
00
..
y
O
.G
3
z
a
a
z
p
r
o
>
J
r
CA
G'
n
a
w
o'
O
X
x
X
x
O
ZO
X
S
o
o
N
c
c
c
s
m
o
0
O
O
N
0
0
O
N
O
N
03
OI
O
n
3
(r�-
3
Q!�-
3
(P-
3
rF
3
1
3
o�
3
3
3
3
3
c
T
y
r
3
r
3
r
3
v
c-
3
�
r
r
r
r
r-
r
r
r
r
r
r
r
3
N
x
x
x
x
N
rt
r
Z
0
7-
n
�•
y
IN
=
3
c
�
to
o•
y
m
�
�
•°o
0
0.
2.
c�
n=
❑
A
p
N
OI
O
c
c
c
c
3
c
3
g
c
c
c
c
c
g
c
c
c
O
O
11
o
=
°
s
_
n
c
c
A
m
i
c.
9
❑❑❑
O
T >
3
x
a
G
..
z
z
a
>m
p
m
3
z �
T
�
3•
m
a
r
O
v
p
a
m
o
p
Q
m
°
=_
W
o.
Z
A
�
:i
vn A�'Or-
m m - X m Z
°
urn
o
J O. vm y w
= o

0
0
3
m
N
00000g!0>>-o
__40000m
o.000
w 0
am
0
0
5F5
O
o
o
3
0
Q-
0>>
w
CL
a
rn°
°
r
S
C
a.CDD
o
o
..
..
* U3
N CD
-- .OP
O
A
O
O
Cn
m
K
W
O
m
S
X
CD
a
v
v
N
n
'T
Ln
o
O fD
A
VI
S
S
'D
0
0
co
X
A
O
O
CO
.p
bi
7
A�
N
W
G7
C1
co
i
W
Vn
o!o
NWM Z y K T' � S m c o Q m vDi D D
N CA Z Cn o n n n D � n C
r
CDa w M w 0 o C �
` N
�+ 1 a m c- N. c rn 3 c- . <
e 3
m e w rn 3 3 rn Ln� tn
in
a rn
CD Z.O O N (n� N .► Ln V
? in
O O
> FD -0 CD S ! CD
Q cD Q$ � O
13 = wo 0 a
A>y Q o
> 0 �c
N D,. N
0 7J
pGo
<
rn o0
3Za
'D 0 C- CD
D CD. m n.
< \\� C O
p a CLTI s
n - a� o p
0 CD*—
O
�soo
o �
FD 0
o �1
n �
3
�(n0r'O t°
S3 3
o -'. CD p
Ri N o o
o 0w
�►1 m o y
r y o CO
�a co-
3 n CD
04
_
(' .. 0
0
�
-A 5t, Z
o
r
�3
r1 Z
rl.� 0
C n ti
m � a
Zm. o n,cl)
3 m J CD
C
CD
D
Z O
O
2
2
o
v
3
a
-CD m to
co
G
<D
O
CD O
O
O
S
0
X
O
n
O N
w
O
v
p
m
N
O
tD C
Q
0.
N
N
CD
N
(DD
`D
D
co
w
a
CD
7
-�
a
N
_
m
CD
m
y
CL
L
CD
�
�
C
CD
O
0 O
0
CD
W 1
CD
s
Z
c
CD
(T
�c2
3
m
CT
o,
CD
/ll
m
CD
0
C
C
S
0
_
CL
v_
N
O
zo
0
„�
m�
zA
Z �.
9m
m�
z<z
noo
ro
ate?
z.:-
s
0
m
m0
-
z� Z
a3
�Zd
OC
�n
vs
Do
m�
s�
N
m
0
4
O
z

m
m
< O
00 -+
C.0 _
CD
CD
0
c
O
N
CD
Q
U) CD
Cr Co
3 a
C
m 0
CD O
— 0
O
3
0 N
0
.a
CD
W
0
3
�G
0
a�
a
CL
CD
N
N
G)
O'
0
G
--I
_Z
Cn
m
m
u
m
.--I
r
® a)
o CD
CO)
U)
n :r
O O
m C
CD a
(D
C)
,.«
N
Cn
... CA
O
CD
CD CD
*� a
w
0 =�
rr a
n
v
U) C/) i > C) —i -0C7 z C) C) C)
;rN(D c gyp;
z CD (D' 0- p= �,' o 000
n Q W m O 0^ Cn fD Ei: _.:
O �: " p Q Cn _•. * O c do
-
Cn > (D 0 CD CD (� a ZT < -
z3c) c� CD moQ333
pC)
OQ Q_ W C/) i
:Do 3 1l -n
Q (_1 N m
n cn `e Q a o CCDD
z -a N (/? a
CD . C-) o o
W CD s
f0
S
Q
a
N
�10 rn (n to co rn
cn O oo.S Cb
O M W U1
c
33�33333333 003
co cct o co (Q cQ cQ cQ cQ cQ - (Q 3 3 (o
Z K K;;�= M C O O O W> T Z Z
ZQ i (Q CD c S Q.. W Ill zr +
o i O w
0WW CD0 o --o o we zT o
Q(�(n-o-5�Q_-c3®zz
W CD c 3. c Q Q
CD `� 033 �,
CD 3 sv
11 zz
0
N O O O
N
C) A N
J
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
(c (Q (Q tQ (Q (c (Q (Q (Q (Q (Q (Q CC (Q (Q
n
O —
Z5 = N -U Z
-0 CD Q 0-CD -
o �- ,
�0-m�n
o CD n Q N
"O =
0
c CD
iS
0
CD
W L6
(Q (Q (Q
O
O
N
�P
3 3 3
nI
m
'T1 '
Os.
m
D
!r
Cl)
m
m
m
0
O
r
m
n
q
m
v
C
z
-ri
m
m
m
v
D
z
v
Fri
r
v
D
n
v_
"n
m
v
o -nr'
S CD
,moo*:*
{D 0
D CDQ.. o
0 0
,a � p = =
Cn
-.
�
'3 w o
o m
`Q *
7
-0 CD
u
D O
-� r
O
NZ
n=
C:<
3
o
c
CD
i
CD v,
.
I
�
/� CS
Cn m
W
J.
s
w
CD
\�'
3
_0
C0
2
CD U
)
Cl) cy,__
O
d
O
(D
O" 0
O
0 1
(DD O
i
o 3
3 a
jQ-0.Q(D
=3
10— CD
(D 0
�
P
^"
N
N
p
CD
—
3
o
o
oo
CD c
(D --n-0
v
w
sv C
o
N —{
CD 0
(Q
1=
A
W
N
W
O
n
x �
()
Cml) <;D U' o
O
� (p
z
0
z a
O Cp 0
U'CD
w
w
m
O
CD
n
Fj
0
m
CD
r
O
0
w
0
an
m
rt
O ((DD
rt
F
�(
()
rt
ro00
W
C)
rt.
O
C
w
V
N
N
-a' c m
0- -o
�o c
pv
ON 3
v � 0
0
� m-
0 D
m
w m
c o-
CD
W
0
Q
CL z
(D 3
co
(D
b
.
0
C
N
CD
v
6 m
CD
rrt 3
(D
a
(D (D
� 0
�o < m
m -D m
pm
co73 =�
movoc
v FDo � R
�OmoC
OU)55'm
s..
D n(
Opm m
mi c
Ui
�w
v
O U'i co
m_
Z
O
K
O
z
O
m
m
0

m
Cl
w
C
CD
O
0
D
c
0
N
CD
0-
(C)
CD
CD
N
Im
O
Cr CD0
cu
3cr
—
.* o
O C
�XCh
Q
fcD O
co
>
n
>
d
(D n
-
at
i 0
(D
0
a cu
72
o
(D
y
0
_a
N
.�
co N O_
O
(D
a
CCa 0.
N
7 7
Q
N
cr
w
O
?+
cD
D 0—I -00z
QQCi
Z CD CD C��0Z: _
m=.mQ
000
CD0C)^cn
5 O C:
D =" CD
060
(n CD CD Q
0
z3�'
(D
CD
CDmI33
Q
pC�
O
Q
w (/� z
-n -n
OC2
00
:0m
w
(n
N Q =
O CD
a
1 0
0}—/
ao o
CD
Q00
°D
C)
�-
ow�M
•
•
F-c.
A to
N
cn
00
o
•
00
m
O3
ON1400
3 3 53 3 3 3 3 3 S
003
3 3
(0(0 0(0(0nnn(0(0 ;:;:(Q
3 3(O
ZKK? =MM )C)OOM>MZZ
c0 i (0 CD c =r Q w w =r ;:;: r=,:
C/)KKE �� C)3 C)C�WD- CD
Qw CD 00 O C• w a% C 3^^
c(Q�n -0 Qn—•3O Z
c(D 0 T.c 3 3 �'c 3 c Z0
3=�c�-�c33c0w0-
m3 w ocncn
O O
0 0�
[? o w
N F-
00
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
(s? (0 cQ cQ c0 cQ (c (0 cQ (0 (0 cQ (0 (0 c0
00
XO CD (D
N 0 o
cD Q.
Z!N-0Z
o CD :3 0-
CD o =
o N_r-Z
0- Mo CAD n Q CAD
-a
0
c CD
Q
0CD
-
1,k ,
f�>r#
333
CD r-
o m m m
o
m aw
O -5�
'OE3
fnDM c Qr-
CD
w=3 0 (D n
-1zm
Ow
T. (j'O
�•C � w
C)
CD
3
CD 7 -
(D (n (D
=
N
m
3
m
c
w
DoQ
_0
(D
Q
3
rt
(n w
w
3
rrt
70
N Q
(D
vj
CD
wo
OQ
070 CD
(OD O 07 CCDD n
N
_.
�. CDC CD o CD
0
m
C) w CDCD
m
Q�.awE
rrh
z
i�
�' p 0 00
z w < rn
z CD o
=' CD (D CD -0 r+
r
r o
w
Q
M
Cn Lnn CD
w O (D =
G
3 o o
(D
z
9m
G
C,
= W
zr
m
O 0 —
v(D
N
Q3 (�
n
F---p
u, cn
m
O
� cn
0
��
Ix
O
m (D\
',0Q
o, o
w
o
OZ
o
N
z
D
O
O0
Cn (D
w
0
m
O
n.
a0
C
o �
0
0)
0_
(n
m
0
5
a w
0
0
-n
CL
-u Cl)
-0 c
7 N
f0 C
r- p)
00
v
0
v
CD
co
c
m
C)
0
c
m
0m
Cp
mp-0o c
0-0:? K
V UmoC
OCl) �'m
D 0 M
0 QCD m
m C C
C
:j m
o
z
co
m
z
O
O
z
CD
M
0
w
m
a
N
(D
0)
v
0
m

{ FEBI3199
Client : Burlington Research, Inc.
1302 Belmont Street
Burlington, NC 27215-6935
Attention: Mr. Wade Edwards
Date Received:
11/15/96
Report Date:
18-Nov-96
Sample Date:
13-Nov-96
SDG #:
SDG-001614
Lab Sample ID:
LSID-009782
Client Sample ID:
6K260-001
Parameter
Result MQL
Unit
Method
Analysis
Time
Analysis
Date
Analyst
Benzene
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Bromobenzene
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Bromochloromethane
* 0.5
ug/I
EPA-623013/5
1:15 -
11/16/96
DRW -
Bromodichloromethane
* 0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
Bromoform
* 0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
Bromomethane
* 0.5
ug/I
EPA-623013/5
1:15
11/16/96
DRW
Butylbenzene, n-
* 0.5
ug/I
EPA-623013/5
1:15
11/16/96
DRW
Butylbenzene, sec-
* 0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
Butylbenzene, tert-
* 0.5
ug/I
EPA-623013/5
1:15
11/16/96
DRW
Carbon Tetrachloride
* 0.5
ug/I
EPA-623013/5
1:15
11/16/96
DRW
Chlorobenzene
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Chloroethane
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Chloroform
* 0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
Chloromethane
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Chlorotoluene, 2-
* 0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
Chlorotoluene, 4-
* 0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Dibromo-3-Chloropropane, 1,2-
0
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Reported By:
S. Matheson
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
pnap 1 S nf ';0

Client :
Burlington Research, Inc.
1302 Belmont Street
Burlington, NC 27215-6935
Attention:
lei. Wade Edwards
Date Received:
11115/96
Report Date:
1Nov-96 -
Sample Date:
13-Nov-96
SDG #:
-001614
Lab Sample ID:
ILSID-009782
Client Sample ID:
6K260-001
Analysis
Analysis
Parameter
Result
MQL
Unit Method
Time
Date
Dibromochlorometham'
*
0.5
ug/l EPA-6230D/5
1:15
11/16/96
Dibromoethane, 1,2- (EDB)
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dibromomethane
*
0.5
ug/1- EPA-6230D/5
1:15
11/16/96
Dichlorobenzene, 1,2-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichlorobenzene, 1,3-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichlorobenzene, 1,4-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichlorodifluorom
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloroethane, 1,1-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloroethane, 1,2
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloroethene, 1,1-
*
0.5
ug/l EPA-6230D/5
1:15
11/16/96
Dichloroethene, cis-LZ-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloroethene, trans-1,2-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloropropane, 1,2-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloropropane, 1,3-
*
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloropropane,2,2-
*
0.5
ug/I EPA-6230D/5
1:15
11/16/96
Dichloropropene, 1,1-
0.5
ug/1 EPA-6230D/5
1:15
11/16/96
Dichloropropene, cis-1,3-
ug/1 EPA-6230D/5
1:15
11/16/96
FWported By:
'
- o. �•
S. Matheson
*' Concentrations are
a ow Minimum Quantification Litdiit except where noted.
NC Laboratory Certificate No. 275
Pa of. 1 F of 10
Analyst
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW

-
0
Client
0
Client
116figton Research, Inc.
1302 Belmont Street
Budiigton, NC 27215-6935
Attention:
W Wade Edwards
Date Received:
, , .96
Report Date:
-96
Sample Date:
3 -96
SDG #:
1614
Lab Sample ID:
9782
Client Sample M
t -001
Analysis
Analysis
Parameter
Result
MQL
unit
Method
Time
Date
Analyst
Dichloropropene, trams Ij-
*
0.5
ug/I
EPA-6230D/5
1:15
11/16/96
DRW _
Ethyl Benzene
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Heaachlorobutadie
- *
0.5
ug/l
EPA-6230D/5
1:15_
11/16/96
DRW
Isopropyltoluene, p
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Isopropypbenzene
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Methylene Chloride
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Naphthalene
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Propylbenzene, n-
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Styrene
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Tetrachloroethane, i,li_-
*
0.5
ug/I
EPA-6230D/5
1:15
11/16/96
DRW
Tetrachloroethane, LL22=
*
0.5
ug/I
EPA-6230D/5
1:15
11/16/96
DRW
Tetrachloroethene
*
0.5
ug/I
EPA-6230D/5
1:15
11/16/96
DRW
Toluene
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Trichlorobenzene, 1,2, -
*
0.5
ug/l
EPA-6230D/5
1:15
11/16/96
DRW
Trichlorobenzene, 1,24-
*
0.5
ug/l
EPA-623013/5
1:15
11/16/96
DRW
'Trichloroethane, 1,1,1-
*
0.5
ug/l
EPA-6230D/5
1:15
11116/96
DRW
Trichloroethane, 1,1,2
ug/I
j PA-6230p/5
1:15
11/16/96
DRW
lqpmkd By:
�evin S. Matheson
centrations are -below Mini am
Quantification Limit except where noted.
NC Laboratory Certificate No. 275
PAOP 17
of 10

Client :
Bgton Research, Inc.
1302 Belmont Street
Bw iVon, NC 27215-6935
Attention:
Mr- Wade Edwards
Date Received:
IM/96
Report Date:
I8-Nov-96
-
Sample Date:
I3-Nov 96
SDG #:
1614
Lab Sample ID:
ISED-009782
Client Sample ID:
. 01
Parameter
Result
MQL Unit Method
Analysis
Time
Analysis
Date
Analyst
Trichloroethene
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Trichlorofluorometham
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Trichloropropane, 1,2,3-
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Trimethylbenzene, 1,?,-
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Trimethylbenzene, 1,3,a"-
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Vinyl Chloride
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Xylene, o
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Xylenes, in & p-
* 0.5 ug/1 EPA-6230D/5
1:15
11/16/96
DRW
Rtpwkd y:
WY S. Matheson
*'Concentrations are Blow Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Pa o(. 1 R of 10

C m
CD
3A
sT 0
CD
a u;
(D c
0
0
0 fn
'O
cD
0
0
O
w
Q
Q
CD
cn
N
Sv
0
(D
z
0
m
0 0l1
O
e �
C) 3
O O
� c
m Q'
O "*
3 O'
N
cD O
CD
*k a
CA)
O w
� O
tv
n
—I Cf)
C/)
D C7
�-o 0 2 C) C) C)
;rNo-0
Z m-
c
CDaa)CDoC7-1U)R
in �-
d=in o 000
_.E�;0
Cn >
CD
CD CD
n 0-
� � cn o o
Zan
C7
COw
m
�Q933
O�
0
s?
0 o
:3o 3 TI -n
W —
0
—
cD
Q�
O
CA
N cn o CAD
CD o.
zz
O
x0
w
co
n
O
F-+
O F-,
Ui
N
F-
O
. v Q O
O"oNfl-
O
O N
v'
w
3
3
m
3 3 =-3
3 3 3
3 3
3 0 3 003
cv cv o cv
(o
(o CO cQ
M (c
,� cQ 33(c
ZKKXMMOC)OC W>MZZ
Ko o 3 O O Mc �CD CD
����0-oca-c-3ozZ
3wCDc� m �-c3c(aO°
me.3`< �033 3 �--�
m 3 0 ( z
—z
w
O
N
� O O
O N
i
3 3 3 3 3 3 33 3 3 3 3 3 3 3
\ \ \ \ \ \ \ \ \ \ \ \ \ \ \
n
D o
a
a o
� n
C)
B
70
0
C:
Q
O
su
Q
-0N-UZ
0 CD Z) 0-
m CD ,
o Nrz
o CD n QCD CD
-0 _
CO CD
p iT
Cl
N
c c c 3 3 3
(Q (C] CQ (Q (Q (Q
CID r0
Du�
r N O
m o ° o o
-nzm a w 0 o
m ° o. r m °
(D 2 CD N
m ° 3 Z
D a 0 3 Z
N Q- w 4�- Cn CD cn
0 w \~ 3 rt
m �' m
Q
M ' ~ -0 0 n
Orrmo 07m
�3
m " w m CD N
--II N -0 CD Q rat
m m - Q 0-0
v (D = O m �J
c < rt
z r n n b CD m CD 0
mCs =3� rt
m U) m
0 "
3 _
0 0
CD
CD c m -n-0
v D(n
— � ai a 0 F
v (D CD r (a
n
o -n-n
m F✓
m
v O
I �
Ix O
w
O
m cD, Q
cp 0
0
°
0
z
0
O 70
70
0 CD
CD I
w
0 o -o uri
m a w o
D O
c O
o m
rt
o
O
CL
cn
rt-
-0 cn co
-a c m
0 coo N
K vn
�C
0
0
T
N
m
c a
CD
0
0
C:
(D
N
N
m
90
0
O �
o D
m
J � c
�M CD
a'
d
rt 0 'a
(D o
CDCD
zl
NI
Cb
m
w
0
fmJ m
m
c0
�n
m0v
v�0
"gym
O�
D
r
O
m
D
0
Z
v
m_
z
O
z
O
m
m
0
cu
N
m
z
C:
K
W
m
�o
m
A
c
m
v
4

lJ
0
3
3
CD
ro �D -I 0 ,� n cn
A._ O
4�
c
�
CD
r 0
p
Qc
Z,w;
0
a
c
1•U•Z�
O Wo
w 0
p(,5
O Cl
Dc.
o
U�o
m m
N
D
o
w
N
mQ?�
o0
0
O ` cD
w
Q
(p
n
�
0
o m
0
C
O
Z a
w
r
0,6
oCL
oCDo
or
0
0
9,
\
1
50
V
\
0
w
co
0
W
0
3
(A
�Cl) or-0
c� w m c0i
cD
*
09
c:S
D
�8'o.m
p
❑Z
-0
X c0
n
m
m
K = 0
LA CD 0 T.
y
D
Z
'O
�7
�Q w `°
a
Om0
O
3
O
,�
i
m
�
2
Z
m
o
z
t
<
<
�a
1-3
f-L
+r,
o
000
J
�omro
0
CD
�z
�
c
0
N W
m.
m
Q
G
�
i
i
3
W
oc
n
CD
0
c
CD
0w
Q
O
0
zo
om
m�
m a,
z�
z-
m=
z<_z
'i � 0 o
D(D =r
Z X'
2
n
m m
m_ o
;i CL
/1 "z d
Y0 a
c
c
v �o
q c
m"
n
m
N(a
m
O
z
v
o
m
o
?
0
0v
_
=
0)
CL
o
w
..
o
o
0
W
G)
m
O
CD
m
N
x
O
�
(0
N
n
O
O
=
O
m
'.
LV
N
(D
:0
Q-
N
W
N
n
O
'm
O
�
7p
CD
(
a
g
of
co
a
`°
m

X
n
n�
a)0
a
a�
o
o
o
o
o
O°
°
O
a
n
o
❑
tO+
2
0
o
N
A
o
C
a
O
0
6
A
w
Ol
n
Cn
c ~°ao
P o
aCoC
d
z
�. O0�
y
c
r
o
�
n
x
z
7
0
H
w
z
z
O
H
p
v
b
O
N
O
N
X
k
k
k
J
O
J
o
y
w
c
ti c
c
c
3
ti t
3
g
c
c
ti c
c
y c�
3
I ca
cc
c
cco
w
o
a
L
O � N
O
�
>
O
V
m
C
i
i
o
7
e
O
m
m
z
4
tOn
o.
a
�
A
a
z
H
rn
d
-
z d r
^
z
0

OOOO
D
D
S
o
s
o
aa)
-nF'
o
7
O
O
O
&%�
t3'
SU
v
A
c
cD
a�
N
co
3
A
O
CD
CD
O
O
p
m
O
S
p
X
CL
A
a
X
N
B.
S
S
la
O
co
(Jl
O
00
2-
Op
Op
a :
d-
0'
'
tD
a�
ZF
3
3
0
j
Cn
m
W
S O
C
-n
-nLn
?
a
-I
T1
O
CD
O.
CD
CC L
a'
w
a
ci
cn
-
D
z
0
0
-w
=
-p
S
o
m
m
3
a
o
cn
cfl
�.
CD
O
CD
?
O
O
4
v
S
S
XO
(D•
Q
CD
N
O
su
a
CD
v
CD
i..,..:
o
=
N
N
CD
CD
O
N
m
.N-.
f
N
a
°
°
-
_
C)
(n
CD
m
m
Tl o
m o m
0
D S
CCDD
a+ c
a
O
W Z
O
>0 a,
o
UO
- i cn. tD
z
..
Si
O
-n
9J
D
Cl)
GS c
-n
O
D
° CD
c
_
o
= °.
n
n
-n
a
iu
Q
c
c
='
M
Z
r
O
<D
=
C
0
�<
0
a
w
U)�cno�0
D
CD suCD 0
C
CD
c>m
m
:3o
D
'�o m
O70
nm
:13
3�
�?Oo
-�
srnIS�
a
w
3
CD
1 v.
iT-
0
0
0
o
CD
Z
�
m
_
`�
c
O
_
m
Q'
CO
b2
-
O
3
-I
CD
0
M)
0
z
O'o
m°
m�
z�
<CD
Oo
�m
m=
z�z
D O o
D� s
Z=`
n
O y d
m_
m?o
Z t _
CL
Z al
m 47
O�
Cm
z -
v �o
Do
m�
m rD
m
n
O
z

c
70
m m
o
to � 3
M -
c
3
CCDD
CD
0
t*
W
CCD 0
C Na„
m
0 N
O
.0
(D
N
O
m
0
a
a
CD
N
N
N
Q
0
5D
m
2
D•-I
(n
m
"D
C
m
z
0
D
C�
C�
C
rn
a CA
0) CO)
n =r
O O
C
A CL
CD -e
CD
� m
� O
.-r
N a
vi
N O
cD
cD CD
Q
ca
O
� O
cr a
0�
C)
-
xx-nnnC�C7D-0zz
zg: W
v
UCD
0
wow �cQCDC�aw� ���
Z
-
m e
m-
vD
U��o Ko n3 nnm �� CD m
w .-.
0
�
w 0
w
3
C CCl fn
CD
Q
Qo
o
W �> N O
I Lam'✓
a
--- - - _n 1V T
- O
O n
w
Q
m
w a
0 3
�, Q
D
Q
0 0
Q `c
3
o
0
in o
Q
g
° o
33 Q
O CD
cn
7
d
N
w
a
0
o
C C C 3'3 3
CQ CQ CQ � "•.. �
cn
c
a
O
m
w
0
D `<
Q- z
m 3
c
IF
y
- v
m-
JO m
c0
70-'zzz'
mo-vo c
ccn0' K
mo0
O(1)U m
Dphi
r
-0 CD
D
� c
D
m
O v
z
c
m
z
O
I
I
O
-u cn
C)
0
a 6
:
m
cQ c
�i
o
-V w
vm
o
v
O
0
0
v
�
M
N
c
fl-
m

c
CD
o_
CD
3
0
D
C
0
N
CD
Q_
a(D
a(D
3 w
� x-
c 0
� o
(D CO
3 C
61
C. =s
`< y
O
0
n
O
S
U)
O
7
O
Q
a
U)
y
C1
6
O
fD
m
m
-D-I
-i
2
U)
m
m
a
--I
LM
Z
0
N
O_
O C
C. N 0) cn
0 =r
O O
O C
0 Q.
O "
CD
0 CD
n
O
O Q
(n y.
N
O
2s CL
O
=a
c
0)
0
77
—I�C/)Cf)-0 �J)>0 z 000
Zsvo 0 =:;;m n �O=in'O 0 0 O
hm �.m Q m 0 n
uy DEH C):3 cmn _2.3: 0 �
Z3c� ��D CD0m CDQ
C7
O� �� 03 -n -n
a 00 �—o
��' a�0
Z� Quo w
�" 0'
wm aL c
� N
Jl
a
%.0a
CD F-00
�� v
N
33=-3333333n3 003
to cQ O (a c0 c0 C: cQ cn (Q ;=;: cQ 3 3 cQ
w � Z � � � 0
ZKK;r,mmOOOOm>mZZ
�OCQ (QmOOC)_WW 0-;:;:�
WKK! Ko 03 000O -0 m m
am (a 0 3 �z3 0 0-0 --•3.o ZZ
3WCD m 3c3c:co
�' w
cDE 033 3cn
m 3 I a' co
—Z
co
o 00
N I�
O N
0
w
3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
cQ (Q cQ cQ cO c0 cQ cQ c0 c0 c0 cQ cQ (a'(a
o O
�-0N-0Z
0
m
m 0 CT
0
o N r- z
,� CD 0
0
O CD (i 0- m
O n
-O
m
O
0
3
Q 0
0
Q
CD
�
O
Q
Q
ccc
333-
CQ
cQ
cQ
CQ cQ-(Q
i-:
�
:_-: � i-= �:-% ,
y513 of W m CCCC
o m Q_ -0m m m
0
r +' D Q o
m © 3o o
CD 5i_.
m 3 00 m o
CD = F < N Z
c
n a 0 3
r- Q � m
CD
too- P. �3 �
m w m e \1 -0
m
m~o�m;� 0n
w
O nO C' Cr (3
m o m n
m o �, CD
CD m
x1 O Q
a CD
C
zCD fv (Q
N �o
m � rt
v w q fD
D
CD CD
0 D � CD w E
-7 � z 3
N
r m m o
v Q�
a
0 o
v
-n N �•�+
v
s� o
0
x
mm WO
<n N OQ
rn
0
0
O
00 CD
N ° •° to
O_ O
D` °
v _T
N• � N
Cr
� o.
o �
c
rt
Q N
p C N
v -°
a (n
c O
m
m O
o 0
* v
N TI
N N
c °-
W
71
w
D�
Q- z
Qw
CD 3
CD
n
r-
m
rt
m
Z
rt
W
00
0
O
C
AOi
m
N
H
lD
ao < m
Dm DO
90
o o-U0 c
UM
U) �i' m
Dn0
O ®m m
0 N
m �, c
i-' >U m
0
z
c
m
z
O
z
O
m
m
0

m
m m
w m
_
D
(D `
�
O
C
Z]
m
0
m
N
o_
Cn
CQ
o
C
D I
Z
m
CD
cr
AO
(D n
d 0 0 c
O rL
to CD -
p CD
o =
o
0 O "*
� O Q
N
(DD O
O
o Q
m W
C.
n O 0
0 O c.
Ch
fA cr
0'a1
0
CA CA -0 > 0 C z
�0-0
Z ow CLwoon^0
EH, ovcn=.- 0
v Dn�—mCD�Q <�
Z3C� (w CD �c.�
oc �a wC/)
00
+ N U? a
c Quo
N ­0
s
K
W O Lrl N Q
• C A a
O P m
O F_ ON m3
w M
C
(a (a Oca(QcococQco(a ;:;:(a— —_ O � � � � -�= -== 1-z 0 lz:z
0 O
00
331
0 CCD
0
0013
ZKKZ='riC7C7oom>'UZZ
v� TcQ CD c =aW W :D7
Q� 0m o a �� Sm CD
-o c a—� 3 0 Z
3 W D c CAD - c c a)i OO
c w
��3� �_��
m3 I 0cnZ
—Z
Ln
0
0
o w
0
O
0
o �
3 3 3 3 3 3 3 3 3 3= 3 3 3 3
co(acococnC.0(QCQcoc.0cocococo(a
---------------
�I
rt
0 0
CD
Cp
=3 fS
c
�• n
o
3
O
c
D
a
N
w
J
1 C C C
LO CQ CQ CQ
N
M N b Z
�m=3 CY_.
CD (n
Q -CDz
o (D n Q CD
"O =
O
7 CD
Q_
OL
CD
rn
3 3 3
D
o
S@
r�
M
n
� m
m
b
r
cn
mH
0
O0
n �
M En
v
n �T
q
m
m
m
v
a
z
v
m
m
r
v
n
0
v
m
v
x
m
N
z
0
0
CD
0
Z
O
m a o N _ __ -
� D N or
W :3O w O O
3wo�3
�L-o�
0� °�- o
r
CD _ : N < N z Al
CD 3 = c Ul
cl-
�CT cn `i'w
s- w 3 rf
CD
a
-0 cr
CD CO F S
-0 CD 0 W Cr O
CDo o CD ow
0 w C g C
o B 3 a
:3 0-W rf
C7 En
C c CD
co
mCCD
�°o rt
r
w
cr -*
D. m
CD
3CD o p
�_ CD CD
(D c cn -n -0
> K w • 5
w N -�
Qo
CD A
cn
l0 0
Ln
w0
0o
cn
D
CD
m° °
w a 0
z D o
T
N N
0 a
o
0
c
a
-0 c
s �•
CD �
0
Q,Z
OL z
3
NCD
0
N
-a
m
cn
cn
�o < m
0 m
a
„zzz'
mvo-00 c
�. �M0c
OU)�"m
D =r ..
w
0 CD m C
a D
m c
X
D m
v
0
z il
0
m
z
O
0
z
N 0
`° m
a p
m
m
7•
TI
a

Aquatic Bioassay Testing • Aquatic Toxicity Reduct on Evaluations
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
Lai I I
BURLINGTON
RESEARCH 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
ANALYTICAL REPORT
CUSTOMER: HUFFMAN FINISHING WORK ORDER #: 51K279-002
REPORT TO: Mr. Lee Huffman RECEIVED: 11/15/95
REPORTED: 12/01/95
SAMPLE DESC: NOV. MONITORING, WELL MONITORING
SAMPLE TYPE: GROUND WATER, GRAB
COLLECTED: 11/14/95 10:00 SITE: MW #3
PARAMETER DATE/TIME/ANALYST RESULT
Ammonia Nitrogen
Started
11/16/9511:40
< 0.5
mg/L
EPA 350.1
Analyzed
11/16/95 by LMB
Chemical Oxygen Demand
Started
11/22/9511:15
102
mg/L
EPA 410.4
Analyzed
11/22/95 by THE
Chloride
Started
11/21/95 09:00
14.6
mg/L
EPA 325.2
Analyzed
11/21/95 by LMB
Nitrate
Started
11/15/9511:19
0.35
mg/L
EPA 353.1,354.1
Analyzed
11/16/95 by LMB
* pH
Started
11/16/95 09:55
5.56
SU
EPA 150.2
Analyzed
11/16/95 by RAW
* * Sample received out of hold time
Phosphorus, Ortho-
Started
11/15/95 14:00
0.47
mg/1-
EPA 365.2
Analyzed
11/15/95 by THE
Solids, Total Dissolved
Started
11/20/9515:55
244
mg/L
EE5k 1L0.1
Analyzed
11/20/95 by ENP
�t
te=
Started
11/22/9510:15
< 30.0
mg/L
_ 3 7:5---4
Analyzed
11/22/95 by ENP
5 623WEPA 524.2 VONs
Started
11/16/9516:00
6/5g.2
Analyzed
11/20/95 by BRL
` 5
Lo
DETECTED ANALYTES (see attachment for all analytes)
ON
NONE >>
Total Organic Carbon, Liquid
Started
11/16/95 16:00
1.7
mg/L
EPA 4151
Analyzed
11/29/95 by ATE
Page 5
BR2

I �
Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations
L
�ill
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
BURLINGTON
RESEARCH 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
(5K279-002 continued)
PARAMETER DATE/TIME/ANALYST RESULT
Total Organic Halides, Liquid Started 11/16/95 16:00 7.7 ug/L
EPA 9020 Analyzed 11/28/95 by ATE
Arsenic, Total-GF Started 11/16/95 13:50 0.013 mg/L
EPA 206.2 Analyzed 11/27/95 by VPS
Copper, Total by ICPMS Started 11/16/95 13:50 0.010 mg/L
EPA 200.8 Analyzed 11/22/95 by RTW
Sodium, Total-ICP Started 11/16/95 13:50 27 mg/L
EPA 200.7 Analyzed 11/30/95 by RTW
Zinc, Total by ICPMS Started 11/16/95 13:50 0.008 mg/L
EPA 200.8 Analyzed 11/22/95 by RTW
Page 6
BR2

BURLINGTON
RESEARCH
Aquatic Bioassay Testing • Aquatic Toxicity Reou`c"tion Evaluations
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
(5K279-002 continued)
TARGET ANALYTES
SM 6230D/EPA 524.2 VOA's
ANALYTE
QUANTITATION LIMIT
BENZENE
0.5
ug/L
BROMOBENZENE
0.5
ug/L
BROMOCHLOROMETHANE
0.5
ug/L
BROMODICHLOROMETHANE
0.5
ug/L
BROFORM
0.5
ug/L
BROMOMETHANE
0.5
ug/L
n-BUTYLBENZENE
0.5
ug/L
sec-BUTYLBENZENE
0.5
ug/L
tert-BUTYLBENZENE
0.5
ug/L
CARBON TETRACHLORIDE
0.5
ug/L
CHLOROBENZENE
0.5
ug/L
CHLOROETHANE
0.5
ug/L
CHLOFORM
0.5
ug/L
CHLOROMETHANE
0.5
ug/L
2-CHLOROTOLUENE
0.5
ug/L
4-CHLOROTOLUENE
0.5
ug/L
DIBROMOCHLOROMETHANE
0.5
ug/L
1,2-DIBROMO-3-CHLOROPROPANE
0.5
ug/L
1,2-DIBROMOETHANE
0.5
ug/L
DIBROMOMETHANE
0.5
ug/L
1,2-DICHLOROBENZENE
0.5
ug/L
1,3-DICHLOROBENZENE
0.5
ug/L
1,4-DICHLOROBENZENE
0.5
ug/L
DICHLORODIFLUOROMETHANE
0.5
ug/L
1,1-DICHLOROETHANE
0.5
ug/L
W
'
--' 1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
0.5
ug/L
0.5
u
cis-1,2-DICHLOROETHENE
0.5
ug/L
w i
brans-grans-DICHLOROETHENE
0.5
ug/L
�="
1,2-DICHLOROPROPANE
0.5
ug/L
we
a1,3-DICHLOROPROPANE
0.5
ug/L
c'�12-DICHLOROPROPANE
0.5
ug/L
B,1-DICHLOROPROPENE
0.5
ug/L
r
Deis-1,3-DICHLOROPROPENE
0.5
ug/L
Tans-1,3-DICHLOROPROPENE
0.5
ug/L
ETHYLBENZENE
0.5
ug/L
HEXACHLOROBUTADIENE
0.5
ug/L
ISOPROPYLBENZENE (CUMENE)
0.5
ug/L
para-ISOPROPYLTOLUENE
0.5
ug/L
METHYLENE CHLORIDE
0.5
ug/L
NAPHTHALENE
0.5
ug/L
n-PROPYLBENZENE
0.5
ug/L
STYRENE
0.5
ug/L
1,1,1,2-TETRACHLOROETHANE
0.5
ug/L
Page
B R2

---� Aquatic Bioassay Testing • Aquatic Toxicity Redut�lon Evaluations
Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
BURLINGTON
RESEARCH 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone]
(SK279-002 continued)
ANALYTE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
TOLUENE
1,2,3-TRICHLOROBENZENE
1,2,4-TRICHLOROBENZENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
T RI CH LO RO FLU O RO M ETHAN E
1,2,3-TRICHLOROPROPANE
1,2,4-TRIMETHYLBENZENE
1,3,5-TRIMETHYLBENZENE
VINYL CHLORIDE
o-XYLENE
m, p-XYLENE
Page 8
QUANTITATION LIMIT
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
0.5 ug/L
BR2

4 .R©V
CLIENT: Burlington Research, Inc.
615 Huffman Mill Road
Burlington, N.C. 27215-5122
Attention: Dr. David Chang _
DATE RECEIVED: . November 17, 1995
DATE REPORTED: November 21, 1995
SAMPLE NUMBER SAMPLE DESCRIPTION
511-2068H
Water, 5K279-002 for 6230D.
PARAMETER
RESULTS
MOL
DATE STARTED
511-2068H
- 6230D
- Benzene
*
0.5
ug/I
11 /20/95
- Bromobenzene
*
0.5
ug/I
11 /20/95
- Bromochloromethane
*
0.5
ug/I
11 /20/95
- Bromodichloromethane
*
0.5
ug/I
11 /20/95
- Bromoform
*
0.5
ug/I
11 /20/95
- Bromomethane
*
0.5
ug/I
11 /20/95
- n-Butylbenzene
*
0.5
ug/I
11 /20/95
- sec-Butylbenzene
0.5
ug/1
11 /20/95
u
tert-Butylbenzene
*
0.5
ugll
11 /20/95
c:l Cn
�, -
Carbon Tetrachloride
*
0.5
ug/I
11 /20/95
-
Chlorobenzene
*
0.5
ug/I
11 /20/95
-
Chloroethane
*
0.5
ug/I
11 /20/95
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.

PARAMETER
511-2068H - 6230D
- Chloroform
- Chloromethane
- 2-Chlorotoluene
RESULTS DATE STARTED
* 0.5 ug/I 11 /20/95
* 0.5 ug/I 11 /20/95
* 0.5 ug/I 11 /20/95
- 4-Chorotoluene
- Dibromochloromethane
- 1,2-Dibromo-3-Chloropropane*
0.5
ug/I
11 /20/95
0.5
ug/I
11 /20/95
0.5
ug/I
11 /20/95
- 1,2-Dibromoethane (EDB)
*
0.5
ug/I
11 /20/95
- Dibromomethane
*
0.5
ug/I
11 /20/95
- 1,2-Dichlorobenzene
*
0.5
ug/I
11 /20/95
- 1,3-Dichlorobenzene
*
0.5
ug/I
11 /20/95
- 1,4-Dichlorobenzene
*
0.5
ug/l
1 1 /20/95
- Dichlorodifluoromethane
*
0.5
ug/I
11 /20/95
on
�
-
- 1, 1 -Dichloroethane
*
0.5
ug/I
11 /20/95
-M
=
- 1 2-Dichloroethane
*
0.5
ug/I
11 /20/95
-`
- 1, 1 -Dichloroethene
*
0.5
ug/I
11 /20/95
cr
- cis- 1,2-Dichloroethene
*
0.5
ug/I
11 /20/95
- trans-1,2-Dichloroethene
0.5
ug/I
11/20/95
--
- 1,2-Dichloropropane
*
0.5
ug/I
1 1 /20/95
- 1,3-Dichloropropane
*
'0.5
ug/I
11 /20/95
- 2,2-Dichloropropane
*
0.5
ug/I
11 /20/95
- 1, 1 -Dichloropropene
*
0.5
ug/I
1 1 /20/95
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.

PARAMETER
RESULTS
MOL
DATE STARTED
511-2068H
- 6230D
- Cis- 1,3-Dichloropropene
*
0.5
ug/I
11/20/95
- Trans-1,3-Dichloropropene
*
0.5
ug/I
11/20/95
- Ethyl Benzene
0.5
ug/I
11/20/95
- Hexachlorobutadiene
*
0.5
ug/I
11/20/95
- Isopropylbenzene
*
0.5
ug/I
11/20/95
- p-Isopropyltoluene
*
0.5
ug/I
11/20/95
- Methylene Chloride
*
0.5
ug/I
11/20/95
- Naphthalene
*
0.5
ug/I
11/20/95
- n-Propylbenzene
*
0.5
ug/I
11/20/95
- Styrene
*
0.5
ug/I
11/20/95
- 1,1,1,2-Tetrachloroethane
*
0.5
ug/I
11/20/95
- 1,1,2,2-Tetrachloroethane
*
0.5
ug/l
11/20/95
-
Tetrachloroethene
*
0.5
ug/I
11/20/95
-
Toluene
*
0.5
ug/I
11/20/95
�5
:_ -
1,2',3-Trichlorobenzene
*
0.5
ug/I
11/20/95
>
-
1,2,4-Trichlorobenzene
*
0.5
ug/I
11/20/95
Cn -
1,1,1-Trichloroethane
*
0.5
ug/I
11/20/95
c -
1,1,2-Trichloroethane
*
0.5
ug/I
11/20/95
w
-
Trichloroethene
*
0.5
ug/I
11/20/95
rD
-
Trichlorofluoromethane
*
0.5
ug/I
11/20/95
-
1,2,3-Trichloropropane
*
0.5
ug/I
11/20/95
-
1,2,4-Trimethylbezene
*
0.5
ug/I
11/20/95
-
1,3, 5-Trimethylbenzene
*
0.5
ug/I
11/20/95
-
Vinyl Chloride
*
0.5
ug/I
11/20/95
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No 275.

PARAMETER
511-2068H - 6230D
- Xylenes (m & p)
- o-Xylene
REPORTED BY:
RESULTS Mom( L
* 0.5 ug/I
* 0.5 ug/I
__________
D. R.,,*ssinger -General Manager
DATE STARTED
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275.
11/20/95
11/20/95

:35 13:07 ATEL INC. MARION 614 363 601L
J
Aqua Tech Environmental Laboratories, Inc.
To: BURLINGTON RESEARCH
615 HUFFMAN MILL ROAD -
BURLINGTON NC 27215-5122
Attn: DAVID CRANG
Client # S0064 Lab # 10-95-130847
Your Sample ID: 5K279-002 Login Date : 11/22/95
Sample Matrix::. GW Date Reported: 12/01/95
PO #: 0262 Date Printed 12/01/93
COLLECTION INFORMATION
Date/Time/By: 11/14/95 10:00 CHANG
Location
Report Approved By:
Deborah K. Johnson
----------------------------------------------------------------------------
Analysis Result Units Analyst EPA Date of Run
Method No. Analysis Number
-----------------------------------------------------------------
10-95-130847
TOTAL ORGANIC CARBON 1.7 MG/L BKH 415.2/9060 11/29/95 11000561
(TOC)
Total Organic Halogens 7.7 UG/L TDC 9020/450.1 11/28/95 11000560
(TOX)
1776 MARION-WALDO RD. • P.O. BOX 436 • MARION, OH 43301-0436
PHONE [phone] • FAX [phone]

:C
0
LU
fY
G
0
,
,
VA
/
� 4a
x
rn �
44 m N
s r'
a o
0 L:
Q 0)0 m 'a
a E O
W
c z 0
� C L
Z o i
w a a
-
LUL.
O
Z
Q
a,
aca
».
O
U
(n
Oit
.r{
En
E'
�4
44
3
44
44
N IL
Z
LLI
= _v
.!
.�
U
LL
Z =
0OU
_¢n`�
Zcc
C1 b
JW
a: cf)
E cc w
' �=
W b E s •
m ro in sic
Z
a
Q
to
co
J z
cc
d
O
Ix
�
3 u nlda3d W31
"V
A.00031NI
3ldWVS
1
9
t",
4,J z
N
z
�N
w
04
V
Z w
44
CD
U
M
i%U
U
N
ox�
U
o
U
LL ¢Z
OZWZ
Z V a N
O
F
co
aac
>C
X
W
a
W
�
ra
a
a
N
CL
2
o
O
Z
a
X
=
W tL W
6l
\
Z
F-�0
��z
W
0
W0
� O
Z W
J
r� O
W W LU
m
Lr)
c~~
co
N
_-m
o
N
�
�
LU
J
a
J
hi p I
P
i
z
o
as
a�
M
0
m
w
0
a
a
m
c
`o
c
0
E
O
iE
m
0
6
T
0
>
j
•a
co
m
m
m
:3
'v�
a
N
d
>
L
>
U
U
0
z
}
m
co
c
O
y
J
E
z
t v i
a
a
O
v =
r
uw
U)
n Z
a
`o
E w_
N
•o
m
u�i i
v
c
0
a
C
cl
O.
Lcc
J
=
y o
Q
o

m
m
rn
w
(,7
m
C _
CD
O
tAft
C
t�
m
CD
c�
I
Z
0
c CD
a C
cr; 0 0
c
0
. Q N ca
D m cn
CD
0
a 0=
o
c0i a
`< P (D -,
fD (D
O p1 (D
0
72iL
cu N (nN
o N 0
a<
O .# CL
CL � 911
(D 0 Q.
Nty
O (?
N �
—I 16 Cl)
000
CCD
2-2-0
.��54
:mom_-�
g0 00
0 CD
C
n
CD
Z C7
U?
CD
CD v
0.n
z
-n -n
00
0 3
W
NCLa®n
A)
CD Sv
Quo
;
0
i CD
to
A
T
�<
A
i
cn
O I--
W
N F -
O� R
N
3
ID
33.3333333c3
003
(D (a oa:�(acQ(a(ac.QcQ
;=i:cQ 3 3
ZKK;r,=m 0000m>TZZ
.0I I I 0 e (n m .:
cl) w o n 3. 0 0 0 cD cD
2(Q m � �- c q- 3 o ZZ
3Wma'� CCDcc�ccco
i��
mCD
�3� 033
CD —Zou)z
m
n
r
o O ^o
O
00
rn
333333333333t33
(Q(C)(acc(Q(acn(a(a(aca(a(a(a(a
�-0N-Z
CD C Cr —
CD (n e
Q_�CDCD
Z
00CD n QCCDD
-CO
=
0CD
c —
= 07
Q �
CD
f>4
Y•;
q
Y i'V
[A"
334
m m
DICI),ccDD
ID
�o c0 Q-0
�D�
In
c
CD
o
o
OZ En.W
CD N
70 CD 0CD
r-
o`<°
o
rnom=3C
N�
N
Q
_
CD
3
rr
(n
:" Q
W
Irl. U
o0
00 a'.
"
3
rh
m
m
a
m
m
°o
n
oy
Cn �
�
r
Ul�'CD
Cr
0)
rn
Q,
0 cn
0sCD
CD m
rr
m
Q-Q•w�
®
r i-
0 'Q
C
Z
n
0 j
o CCDD 0
N
0
CD
N 0
rF
m
A
Q Z
CD 3
Cn CD
11
m CT
mw cr CD m o
G m 3 o O
a
• 7
CD
io
CD
v
D
m
o
�-a
-
cn
o
0
Q CD
a
n
3
o-0
v
�
-n
-n
,i
..
m
a
Ul
0
10
C)
00
-<
O
O
oO
W
fn
a
o
=
ID
Ul
w
0
o
z
0
Z
D
O
CD
�'
w
0
cD
v
o
s
C
v
p'
O
7
� CD
4
C]
N
m
A
c
mpg
M
U)
D
0
moo
Ln
zUl
c
m_
z
O
Z
--i
O
r 4
O :p Cn
Cn 70
v
tea- m
�i C7
N N
CCD
n`
r
S
r
�
�
7
_
En
En
CD
w :m•
c
a.
(a
m
z
K
co
m
m
A
c
m
v

= '0
CD
CCD
O
p
o
O
Q
o
D
o
m
3i
o
-
cn
, 2
o
° CAD
�—
n
0
� n
c
o
a
uzi
r a
-
M
0,6
Q j' 0 (
m
-o
o�
°p
o
-�
CD
o
o
n �
,00 o
In
o.
Z
o
' o N
c
T
N CD CD
Co • V
cc
CD
SD
°
c
Wu
r 0 3
�3
CD
�C �
Zm�
w CD o o �mnC z
rn3" CD CD
0 �0
CD CD C7
m CR
v °-
3 y `�P
7
�
4
w
t�
c
_
CD
_
h.
J
�
lr�
W
c
3
k�ico
v
a
CD
m
In
m
r
v
r
m
9
N
0
z00
,,
m�
z�
00 °.
m 7
z<z
noo
n�
z ='
C)(�
M_
m-
? Mo
z0=
CL
�, m
O�
c
cm
Q �
n o
m
�m
Nw
m
n
O
z

CDo
Z
_
2)
3
°
o
co co
w
<
_
0
w m
--I
0
?i
-
a
D o
r
x
co
CD
m
o o
CD
a
CD
v
W
0)
o
�.
CD
�.
O=
W
c
fA N.
to
(D
O
W
70
D
g
f(D Q.
Q
o• co
co-
co
a
CD
CD
r— -n e -4
Dmv cc =
a3ac� 3
o s
— mo
c4
r O
0)
0 > wo
c�
O
o
a
�1Z .'�
D �
D CY
q
o
D
'03
A
D
M
3Zo
Q
M
,
0
D
° m
t j5
B
�
-<
11 �-
w
O
cn
rn
on
co ai
r
Aa
�
CD
O
co O
w
��
O
0
w
o
0
m
0cn
�W
Gi
ro
0(`�
m w m o�
O
3 3 cA c)��n
0) -a1 9
•V
S
o
Z
r
M
acpg.
a
p
0
3
3
'�
m
°3(D
w c
c
=•I
Rr
m'
0
m
�n
r o n
Z 3
my�0
ao
m
�3
a
y �
3 a
w o.
m
v � m
CD -�
c
CD
m
� Q
1
000
M
or-
m0ggwa
) m
m
M M n
Q
c
-o
R
`<
3
o
m
a
`�°
FL
G„
1
0
3
n
N
n
c3�a
O
c
m
w
a
0
m
M
-n
rm
v
r
O
O
N
0
zv
m�
z00
Z
m=
zS z
aoa o
r-
bM ?
>
n
MR)
� 1
m- o
,i CL
�z°
O�
c
�m
vm
CD
vo
m�
N to
m
n
O
z

D0-I� pz nC�C�
CD CD S�=fn ° 0 O 0
~ 0 _� ' '2 O C o O
n t om cDc�33
�a z
cn = O CAD
((D a - 0
Da-�o 0
� s
`G
c
a'
c:
N
O1
3
CDF- Ulw"
�1 o N N v
o p1 .
�1 NJ
�1 l0 O
�l �1
333333O3 663
CO cQ CQ cQ cv cQ .W: CQ
a a -
T>-azz
W CQ CD c Q W S '_«� ,..a
W o W B ' (n�_
' W CCDD O O -- w Ali w C � (D
n c
cn "o Q ) -_.3 p Zz
� 3 3 "--
z z
0 0
ON
o w
cn o
3 3 3 3 3 3 3 3 3 3 3
cQcvcocococococa(acn(acv
C-) 0
O
� =
D CD
Cn
O cA
c �
�• n
� O
3
0
c
_
Q
O
W
c
QL
-0N-0Z
a CD O o- -•
CD U) W
o Nr-Z
0 CD 0 Q CAD'
o CD
c
= 6
Q -
cn 0.
Q
CD
L�
}
t
d ad
c C C
O
O
J
3 3 3
a'
D cr o m m
m
m o m a o W-o-==
CD
cmn� o � � cQ < 3
0
mZm (n -0
0 W W O m W
z3
CD Co ro
-ml
m
3
m
z
a
Q
CD
-c
cy-
m
�
w
aw m
o
m
m
m
N
wcoCT
CD
Q
-O
CD
(D
(D
O
0
—
CD CO
o Cr
oFi
w
Lnn 0 CD m
N
m
0 W C CD
(D
(Dc
0 Z3 CD
o �
rt
®
n
-
(D
0
CDo
m
�
� -
my
0
c =
c )
0
aCD
o
z
v
CD C
>�
CD „ O
w�
a
-n
W
3
-0
o
vCD
a CD
� F-
N
3
�
N
n
70
v
o
�N
w
�
N
TI TI'
m
N
'.,
v
O
Ln
Ix
ri-
O
O
-<
4�, O
Cn �•
o o
N
o
u'
c'
z
m
O
v
O
�
CD
I
I
I
I
W
w
°
°
m
a
cc
"a
T
o
0
v
U5•
v
m
�•
a
v
c
ET
o
0
IXi I I
O cn Co
v c m
cm c
--i
00
o v
f d
TI
( 2.
C °-
(D
0- �`
N0
c m
rox
oH,
ON
�1
m
-D x
m
•
z z z
U0c
M CO
OCR m
W
Ocoo m
M
c
D
v
O
z
co
_m
z
O
O
z
D
O

m
Z7
c
-i
m
m
o
W
_
CD
-i
(D
•D
'V2_^
J
O
y
m
c
�
O
�
m
Cn
QL
ca
CD
n
C
m
# » G
c ,(D
0
0,(D
a•
t�
g• � O A)
r c
R Q. (D
tot
(D y
0 0 0
C.
(D
o
n
72. =Pr
d
y :n
7 (n 0
<D
o
d Q.
a
y Q
v
n
_0 c �w -, - =r0 ®o 0 0 0
Z "mv, O cn' oop
(1) > = CD ® (D OCD 5'� � o C 00
z3 0 n c) CD Q� 33
0 �a C/)z
_ 00 o3 m-n
.Q
N N� o O CD�0
CD
rt: �o o
no '0
S
—
mO _
(D
N C
O N W l0 000 Q 6ti
U I N O Ol :A I-
—'L-�L
33 3333333cm3 003
cQ cQ O (Q (Q (Q (Q (Q - (Q (Q3 3 cQ
ZKK;r\mmooC7ow >TZZ
C/) K K® O 3 00A) 0 C o O cDD
O Sv iU (D
�0Q-O33QQOCz0
3 W (D c:-s (D C, 3 c (n ON)
(u3 ((n'Z
Z
o�
N O O O
u� N 00
333333333333333
O
D (D
M
ai C/)
o' CD
c �
�• n
v, o
� 3
0
c
Q-
W
o_
C c c c
N
-N-0Z
O Q Cr
n (1)
,c NrZ
om0QCD
3
0 =
c CD
c
a 0•
E
cQ cQ
v��Q.
SFo_
0 0 0 0
N� ___
r o
w M Cn
o o a�
(i��,�'<-oca
<3w
0 w
q�
2.6 1 22CD
)O
_
cn CD N
m
0
z
c
D
a
u, a
Grp
(n
�-,y
I�
ova a
W
w ,^ 07
j- Cn
-§
rCW
1)
un
w
0
0
�cCDi o
a m
,-
m
�
n�,<
oW
CD
0
-0
3
(D
m
v
m
:3w
0-
_
a w
ro
o�'c
CD
i -
FJ
c
�3'
�
"z�
F
m
cr
u'
m
�
�
�
m
®
-o
w
cD
o
=
z
CD
CD 0
>
W
0
-v
o
v
(D (D
(Q
F
A
n
3
v
I--
„ „
m
�.
0
Ix
rt
O
~ 0
m (D
fR
N o
o
�
m
z
0
z
o
®
Ln
Ln
CD
w
(D
n
D- o
N
o
v m '
N•
— Q
o
w
m
O
°
E
Ix°
LZ
- t`31
0
Q
Z
m 3
c CD
0
0
c
l<
N
00
m
W
O
s
.0
70 m
i m
_c
"'0--00 c
vcno:? jz
�Om0w
COui-m
0
> s
w
(Dm
m O
C
--j m
O v
z
0
m
z
O
O
z_
-I
O
m
0

�cl) cl) DC»-v ca
CD O (n
a) —=«- p (n =,�. * 0 C O O
C? CD cD {y a =
Z Q
30
00 (nz
00 �Om'n-
0 � Cn N (no O CD
Qa n
-1 0 Sv
0
c
A a
CS O N F-+ l0 to Ln
COTS Cr O A (b
c �
33�3333333�3 003
(0cQ ocQcQ�cncQ�cQ n 3 3
� � W � � � � � � � In v Q
ZKKZmmOOOOm>-Uzz
m (a i(a CD c Zr Q W S r•►
0 i e O
® A� CCDD ® O w Z) � C =r (D (^D
fAI�c I—.I3 O^Zc -0
C:(a6 3 3O03ucDcc cam. E•�3c
Clo331
E-M
II II
zz
0
w
3 3 3 3 3 3 3 3 3 3 3 3 3-3 3
e�cQCQc�c�c�cQCQc�c�c��c�c�cs?
0 O
O
zr
CO CD
CD
o A
�• C7
'so
3
70
O
c
c
O_
w
Q
01
�n -0N-0Z
CD =3 Cr -
n .�-f
o NrZ
o n Q CD
3 2
o CD
c -,
O c-
QCD
�.
f.2
Cn
O
P O
c 333
Cl)
N (D (D CD
o --0
o CD a w
CW, _
W Dc(n --Qo
:3 (n
CD
p N
rn 3 ¢7 O *
-.
CD
nzc �' -a w .-. O
Ow O.m CD w
Ovi
3 O CD
CDA
pj
rn
cn
NZ
m
rt
b�CL
N
c
�
v'CD
N�
F-�
CY
N C
02,
rt
N
C�
C
W
O
�-)•
Ln
003
Fj
Q
CD
m 0 N� m � N O N
CD O W Cy A w Al
A Cr CD
m 't
r' A=e CD O o CD
m cn A W CD
O N o 3u a rt
mt Q•aW �c
v 0 Cl) c C5
c c
Z w cQ N rt
r0- CD o
m 0 O-
C ® Ali CDIE"i
-" 0
D 3 O N
Z CD O CD 70
v D 0 �
-n : 3
m l N �, o
v CD cD T)
D Q3
n _0
v o
r
m w
v �
o
�O
O
v
m CD N OL
O
C!? Ij O
w 0o
I �a
w
I
0m
z
Z D
OD 0
Ul
®CD0° •°o
2 o
p -0c o
OCDO :p Cl) cn
Er -2• D
Cc 0
00
CD
p(c CX
CD
C
7
ONwO
cNN
0O(D
Q�ObC
-�n0W
CD OCD F
C(DDONmn
r) 0
�vcm
m
�
D
y m
�v0c
no
K
Co � m
0
S
z� M
O D <D D
moo c
A -I F� m
Ow v
z U'
CO
_m
Z
O
O
Z
O
m
m
v

Ca
w
-n
CD
0
<-
a
N
_
3
m
(o
a
3
g
w
C
a
0
cy,:
0
a Cn
o w � � = (D = O ° ° O O O w -. 0
m o 0 o g 0 g w w A 0 Q n- - 0 0 0 DB c� Dv Q� O t
� E w a w m o 0 (n D
to m 3 Ao X co A o o cn rn w te(a,� o -A7 W =!a3
A 'D C T T W A '-G '' S R O 0-n \
O x O A = S U -i -n N O z n m
CD D c
i O W VI 2 Z F -r'I O
toCD
;; a D n ohm i- cn
o rn 0 W
m n.
A
z
aO
o= 3 3 (' q- 3 0 0 3 3 3 O
c _ _
�m p
O
5 '° w
z z (n- cn cn _0 S S -n 0 :' �b `CD O v
O S c � w w
w a m a n.
N n' N
w - Z V co (D (A O C)
(a O z �4-„ N o N N F? N a
CF)_o a o� w o cn 0 o p m
M w o0 0 3 n
w Q o 0� " cD O El Z
CD y �" 3 �' n m r-
N �' �= o D m
i n 0 O❑
? N a m m O
3 3 3 3 3 = 3 3 3 3 �® 1
- -
TI, fD.
i (D 0 z
� -U Z Z Zo -G
N cn Z S n n n C� n W D D D A 3
m CT 0) 7 (D C a (C w w
N —
m m o a� N N 0 0 n w C) w D C
O O O �" w w At C
CL
rn �" m 3 w m c" c a) 3- _ 20- c a n 3 1'
0 c C 3
3 ILA 3
N c A w 3 3 A O1
l� vu', m 3 . cg 8" A " L ua',
O (.nO N W Vt m (n 3 m C A
ul
EllA� aR=�
m
0
0 0 O 7J t7 r
n -u Q
r„ co m c� m
q � a z
m M Q c
c c c c 3 c 3 3 c c c c c 3 c c c c �1 3 C 0 W 3 Cr
CD
CD
�
(D N °, � w
_ n o '
CDCD
-u
-u
o
(D
0
?
O
O
S
2
3
a
o
w
m
co
(D
p
S
N
>
ri
-I
w
O
w
v?
X
o
(fl
CD
o
s
0
O
m
w
O
CD
0
cQ
=r
w
(fl
�'
oCD
mw
(D
=
m
p
N
CD
CD
(D
w
0
a
CD
Po
'
O
0
m
C)
CD
m
0
�C
1`b
a
0
0
m
v
L
D
m
11
rn
r
v
ca
O
9
O
Z
O�
-n'o
m�
Z3
C �
O
Z -
Cm
m:3
Z<-.Z
10 O
D (D S
z�
a=C)
Ow
mm�
1
m? o
Z w _-
a�
Ozw
: ?:
O=
c
0 70
Do
A =
m-
:33 n
w
� a
m
n
O
z

w
O
3
a
CD
IQ
►C7
nI�
ICOI
J
bIb!'O_!�-(7IC)!G�
I�
oi�
QI�i�IAI
Via-
�0�01�
C') o_;CIC'Q
l�
y
°
I�
Lc
'
r-
-4
Nj
co!mac
a
?
°
v
o ? ?
I iw
I'O
cn
O
m
x
G
coA
AIA
I�
SI;I
c
-�►T
O.
o
co
m
0 m
a
N
Ln
w in
l
I
a
m
ET 0
12)
A A
Ln 0
[L
Ln
W i W
\
I
\
\
(c CQ I
i0
Z
-
I 1 i �C7
^•
\
IlL`
C
.�
\
-0 �O
''
Iz
c
c
lcn iru
IS
'S
id
lo_
Iy
L=
m
�o
ai
IZCil
�
m
m
o
��
cn
�
�I
�in
�'
°iU��
m
o
a .o
a
°l�
o
cn
Z
O
°
�o
I
c
©
a
N
W
w
o�
�ka�a
C',ia
�3
c
zz
0
mb>!b
�.
Z
,
"•�
,.
Q..
w
,
LU
r
(n
,
,
m
m
o
a
n
o
n
C7
b
b
0
()
a.
=
SU
O.
7'
co
�
c•
47 I
�
Ll7
LOQ
07
y
m
A
�
°
'—'
Oo
SJ
0...
C7
Q.
C^].
c.
N
m
_C
3•
M.
C
N
m
c
a
(�77
ro
-.
c
3
fJ•
G
-<<
A
v+
A,ro
c•
w
A
A
A
m
a
3
o
cn
Ln
rn
m
D.
z
A
N
10
o
N
A
Ln
w
L"can
m
u'
r
'm
cn
coy
.
w
con
�.
a
{n
G7
LT7
N
V
c
c
C
C
3
3
C
C
C
C
ac
cc
IC
07
G)
m
o
m
(D
o
0
4
to
o
X
to
F
52
co
O
o
m
o
°
N
0
�.
m
O
m
N
y
cz
en
o.
aSi
c
0
m
0
a
m
N
I'
m
m
m
In
:
a In�CD
D
�¢3
O
I
oo
f
3(CO
o
CLD
m
�.
b
0
^ f
M cc
I73N
D
cn
m 1�2c
T
OS
C
C7
Z T
O
O c� T,
r
cn
m
0
a
CL
-
S
w
CD
�_
O
v `
O
O
NO
1
c
CL
a
y
cn
�W
Tji'Lr
m
W
rC,
CD
�
m
--i
bm
C
y
0
3
V
c
Zi
in
O
Z
O v
-n 'm
m2
Z 3
< m
zO
9m
and
< Z
>o 0
Z �
mm�
m_ a
� m e
,i CL
Gi � m
o
C m_
y
-f c
m�
N w
m
f7
O
2

m
0
N
0
C
0
c�
CD
a
m
2
m
C
Dm
Z
a
C
Cn(n�l�DC7-�� p� 298
C'- 2. 550
z CD ID
o
�=3 mm
rt
Lr
A F- 0F to N
F0
Ul Cco
ON
33�333333'3c3 003
ca ca o ca ca cc ca cc ca ca , .r cc5. cc
wmcaZ(QMc=Rwty>=ZZ
'� �C RE- 09c o -Z
3 a p. 3 Z
3` ff ��cc3c f�0
�
33
c 3 3 — z
Z
w
N O
epp • 61
0o w
333333333333333
cacccaca(a(aca(QcacQ�acacacaca
0
o
�Z
31
o~
o0=°amz
3
c
_
CD
3
N 0
v
C
SL
o
C)
0
w
c
c
c 333:'
cn D
55,
CD
3 m
r� w rt
o Ln
J N "0 rt
r' �o u O iD
110G7 �.� wy
rt A
cn m rt
A'
En (D � 3 3 �-
D a
c
. ri-
m
DC
o -n -n
o
n
i
0
C.)
Iai
i-? o
w o
0
z
0
co
Ln
m O
v
s. �: s
O s
¢Ill
m m 7D
n �o C
vgo:? cn
Omoca
m
m
m m
g
� m
g
m U'
G
m
0

m
10
U)
m
9
U)
C
m
v
C
_�
j
co cn -o 1'G) > n
�CD ��a SD CD 0
gZ@N�
ci CR P
Z � (D
Q
o �-
CL 0 Q
W
CD^ o
tS7 O OF
�"0 p ",
o=o v
CD C R
15
`� R
�Oj cmD
K
s
a
W .Ln Ili
.P N N� �
C
3353333333c3
coca o ca cc cc ca cc cc cc cc
e5-m 0 5- 5m 5a5-m -�= 5. ZI V
003
3310
:c n O C? O. W w> p�CD
p
�o F-•nn Co—z
3
CD
Z
co
31 =3cNcoN�
z
w o
FLJ7 O N
F ` Ln �
333333333333333
cc ca ca cc cc cc cc cc cc ca ca (a co U3 ca
S►z
o ,
w X m "
5.1 0 (D
7
0 c
&3
3
333
co co ca
,)fg*M*C
a� m at66 c� cu m
U0
Dlo
R o
, Iz a �
z N-5.
-* o
CD
C Z N
3 rt
(D
F~-� Ln r
Ln 3
No- U oh
�c � �� W
O W� o a
E; (D O 7
(Do W
N Q a (D r
(D
[D r
l
(JU
CD
C ;�n
$ - o
o�
--n
W O
I0
I
(� N $
N
a �o m
W 0 O mm C
N m -o c
o �9m
A nag m
n
� ..
co I I r �
0 M g
m �a m o
�c CJi m
FJ v fi = g W
ID LTI
W
C
3353333333c3
coca o ca cc cc ca cc cc cc cc
e5-m 0 5- 5m 5a5-m -�= 5. ZI V
003
3310
:c n O C? O. W w> p�CD
p
�o F-•nn Co—z
3
CD
Z
co
31 =3cNcoN�
z
w o
FLJ7 O N
F ` Ln �
333333333333333
cc ca ca cc cc cc cc cc cc ca ca (a co U3 ca
S►z
o ,
w X m "
5.1 0 (D
7
0 c
&3
3
333
co co ca
,)fg*M*C
a� m at66 c� cu m
U0
Dlo
R o
, Iz a �
z N-5.
-* o
CD
C Z N
3 rt
(D
F~-� Ln r
Ln 3
No- U oh
�c � �� W
O W� o a
E; (D O 7
(Do W
N Q a (D r
(D
[D r
l
(JU
CD
C ;�n
$ - o
o�
--n
W O
I0
I
(� N $
N
a �o m
W 0 O mm C
N m -o c
o �9m
A nag m
n
� ..
co I I r �
0 M g
m �a m o
�c CJi m
FJ v fi = g W
ID LTI
W
(� N $
N
a �o m
W 0 O mm C
N m -o c
o �9m
A nag m
n
� ..
co I I r �
0 M g
m �a m o
�c CJi m
FJ v fi = g W
ID LTI
W

m
0
N
c
0
M.
CD
(D
g
D
0
m
m
c
m
v
C
r-
~, m L u�Di m o o
0o� �D�� Q
Z n
c
CD
a -� n 'n
Q o Q —
W c -0-1
3
a
A A
® hdoa� N
O
m
33�3333333S3 003
ca cc o cc ca ca cc cc ca ca r« co 3 3 cc
--0 �����-��cn = _
5c c� c ccN F>pp3
mmo Rc WOi MUc o^Z
Es c c.c'3 pO
�c�D.3� 03333 0
3'z
Z
N
� o
333333333333333
ca co Z-aca ca ca ca ca Zza(Q ca cc co ca ca ca co
®9 &5mZ
NrZ
�CDcn
CDi
CD
o o
3 \
Q
cD
CD
3
N n
a
CD
O
LM
O
cQ cu m
Zu �� Div R �
o o �.�
N
a C
cn
C N c cT
Cn
c� o
��°�a *�
�
En "
DL
cn
o� rt
® c Iz
o
�-
o
00 I-J TI 'n
O
N
10 O
wn
O
n 00
a
No
0
w
m
c
m
:3
r,1i
z
m
g o
0
m
-o
00
Ln
m n
O
s
u
S.
o
`z
0 : I
b ,
s
f
�
4
e
m
z
c
6
m
3g
I
g
m
G

nD
°
3
00000DMODD'o
-�-1,0000C
3
<
o
=r
=rsv
-
N
n'w
5FX_
Ooo
OOO
3
a
0
0
0
CL
,(D
0
3.
�+
Q
o
w
w
O
a
0:
0
W
o
-.
0
o
rLn
v
v
in
C
(D
3
Q
n
o
3
3
Al
`G
G
W
G
CO
O
��
?
CO
N
(CD
��
X
O
N
(D
(D
o
o
~
O
"n-n
W
W
O
�om
o
P
u,
__
mmW
cr,
o
x
P
1
o
O
o�
o
m
A
o
Oo
Ln
N
wCn
o2
corQ
CO
i
O'
v
OP
3
c
3
3
3
3
3
3
Z
3
=
j
3
3
3
(0
C7
�'
co
---
(o
(a
����y.
(Q
co
(0
-i
c�oo���
O
O
0
0
3
3
e"
-V
Z
�
z
Cn.
CD
Cn
"a
-n
v
-iOzw
7
N
na
a
p
N
O
+
N
N
d
(D
_
(D
n:
A
°
U)
(3D
U)
N -
Uf :
Q
(D
(n
o
O
Z
Z
O
W
y�
o
Q
Cl)���
�j
���
0
~O
","
rna
Lnno
°
o
3
Wo
voi
z
rn
w
(fl
o
O
W
o
(D
N
4
d
3
3
3
3
3
3
N
o
3
3
3
3
�\
�`
N
►�cn-0zz
Xzm0000QJDD
Co
(D
C�
d
0
A)
—
N(nrZ���°
�o
03
0
00M
0
CD
c)
7
_a
C=to
3
3
CD
W
A
-.
3
3
C
3
3(D
-�
0
0
0
3
0
�
J
O
W
(fl
?
0
0
V
N
V
00
N
4
v
O
o
W
Cn
P
c
C
C
C
3.
c
3
3
C
C
C
c
E
3
C
C
C
a
n
T7
-o
Dvo
D
z0O
jV
C
A
a
Al
A
0.
o:.0
-+
c�
,
v
CE
w
x
(n
z
�
CD
:3
0
C
a
0
Q
(D
A�..
(D
c
Q
3
�.
0
A
3
a
.
3
g
0
.-.
crm
�,
A•
CL
m
�,
o
N
���
W
m
CD
Ul
O'
n
0
Cl.
z
m
<
D
�_
o
a
a
o
n•
o
CD
j
o
m
0
�t D
-0 2
D�
m
0
m
.
O
m
3
Fn ,_�
c
o
0
CD
o�06
w Q
Z �
� o
o
�,
G
�
ch ;�
Z
�
.��1
'0 ,
o
W
,
o
m0
`{
n
m
CD
n 0
�
(D 7J
o
m
5' O
(Q
a
m
Z
m
(D
r
_
-°
CD
0
W
w
O
n..
0
Ln
0.
n
U)
33(on 2iCD
�
c
cc)CD
y �
3
o'
m
m
zz °
c� o N
�.
10
3
m
0
o
m
T°
m.
3
C
CD
n'
w
CD
o
'
�
L
5
0
O
Cr
0
C
3 m
� 3
Z If
z '3
V.
' ^,�.•
o
3
yq+
o"O h
M 7
0
O 7o
v
ari
m
CD
=r C.)
m
CD
cr
m 7
z'S. z
o:
`Z
o
�'.
F.
r
c
v
<
y,
U)
CDU) Q
Q CD
00
--
D
O
mw
cn
=
z75D
3
CD�
z o,
-n
y 0.
(C—D
o
zp1
3
3
M�
m.
s,
c
000
1
T
a
(V,,,
o
tD
y c
rn
CD
R
N
z

D
0
0-
CD
R
a
O
v
c
Mill
<,,1111
D
H
0
0
0
0
0>
w
0>
>M
�
-I
C)
0
0
0
M
l<
wo-0
o=
mo
w
N
CD
0
w;.Z*
_
!;
cr
0-•_00
a
0
O
Or,
O
D
oo
ao>
a
w
a
o
o3
r
=
(Di�
a
=w
�
a
N
N--
X
O
m
-nnw=
WWCD
05:5
�
vvo
T
Ul
A
o
0
0?
CD
CDO
z
w
conN
W
O>
wsu
D
(n
o
02
rn
m
3
3
3
c
3
3
3
3
c
z
3
1
3
3
3
-o
co
(a(c
--
,co(acmes
---in
__
�_ooZam
3
3
V
O
C
s
:sS
�
U1
�
�z
--IZ
0)Cn(n-0
0
o
Z
W
-Ci.
C
A
zr
w
O
w
d
p
C
y'
!A
o
CD
Ap
(D
A:
O+
(A
N
m
CO
N
0
Zz
�000W
�y
0
-
(A
U7
O
N
m
N)
0)
v=(�N
0
0
-4
3i
Q
N
z
U1
O
(D
0
3
P1
W
oo
h
cn
cn
oo
y
C)
o
o
r
3
3
3
3
33
c
3
3
3
3
-
-
3
N
NWMZZKKX=M0000m>>
R
'
N(nr?0KK
Ko
03
o
00w
D
(
u
n
O
N
x
Q
w
w
sv
cD
O
O
c
Q
w
3
CD
gl
l
a
m
O�
y
�
0
3
3
'c'
c'
�
3
N3
voio<am
3
�'3
a
-�
3
3
0
W
-icnio
coo
V
v
\Con
V
O
W
V
�
L,
v,
14
c
c
c
c
3
c
3
3
c
c
c
c
c
3
c
c
c
C
0
1
c
o
Z0
O`
-.
i'
N
'
EO
0
ay
w
a
w
w
0
CD
mw
x
Z
=
O
CD
0
-v
0
a-
�
CD
_�
:3
0
TER
3
O
su
°
a
obi
N
0".Q
cy
m
y.
A•
�
(OD
=r
m
x
a
$
l
N
y
(DCD
co
m
D
f
CD
D
0
n
_
i
O
1CL
(�
tOn
0
w
CD
N
(D
�
0
-n D m-I 2 0 cn* m D c
j o m 0 W
Z
SD Dy o
� co �?W0CD Z
�J
O -n
3zU%(wD
m
to taz O O w p
0-8C�
0 AX0 O � -3. tj
w
2 0 0
o -A' CD
w o
L'A,`
O
0
FMCn0r0 CD p\p
0 w N O C 'S
7
phi 8, O. (D Q Z i
(n cn m M
_ __ o M
O (D 0
�� ®� 3
- 0 3 -� m
S c
0
\ O y Z
��] a
CO
Xv `
3
Z y
y� m
m s+1
"tf 3 �wOO CD
�p w m m CD a m z
io 3CD3 crCD 3
0
C: n W ID o0
1 0
CD
�3 .4 s in
a
3
v_
N
O
z 0
oA
m,0
m�
z3
C
M rt
Oo
z<z
F-O C
=�
a�
Z-
x
n
m m m
m _ o_
-Zi w _
OZm
O�
cm
cvx
C y
C
rn R
Na
m
q
O
z

cc ;�
m �
<
m
o
N �
m
CD
O
�
m
D
o
�
D
CD
--i
m
0
c
r�
C-X
CD
Z
o
Lo
g
57
3
7 �
O
a;
14
O
w�
lD
ado cnc -oa > 0O=� ��Q
L 5;CD CL SD (D O n^ Cj O O O
CD 0 CD ID 3
zo a
mT
2. �-cn
:3 �o
S
^ ^
o rn o h� (n 00 Ul
L 0 •
w 03
L
33K3393333c3 003
co (a O co co cQ cfl cfl cfl ca 2 ca 3 3 ca
Z KK Xc= T c ORS Fk3zz
3 D-P-
�aCD� E�cmcozz
�3 n.0c•.2 Q0
n .3 2 2 W.
7b 3 Z
Z
T
o oF�
co Ul
333333333333333
cc cc (O to CQ cO tO ca ca co da ca co ca cc
D
m
O
&f 0
0
CD
Nr
O CD
(D
3
CD
cl
En 0'
Q
C
c
0
Q
c c c 333
w cl,y0n S. r
oc
zuj*-g c
mQ�IRvi D N�
cn 3 3
CD a
w c�i
O cn F F* h
c
w ak
0 cn 8-
o 3 3—
CD CL -P 5
cfl cn c I
Ln
c c
-0 o
w:"' -n-n
N o
0
w0
z
NI
00
ON
w
0
a
m
H
J
o T
4`°.
yy

cn
m
0
c
N
cD
D o
CD
g
D
2
ao
9U)
c �1 O� Dz
_
0
�.W�a.sum;oC��' ooD
M.
corma —;oa (D 33
Z 0 _
0 -n T
DTI
W O cD
Z,�
�r
o
n to o � � cn co o
w
o• oa,•
0 0 0 0 "0
33,3333333C=3 003
Coco o co ca ca ca ca ca co r« ca 3 3 ca
ZKK7=m c ORO F��zz
'0 3 D7?r CD
o
cc'— C o^Z
3,
I U 3 0-03 00
3c3=c3:
31 R3� '033 3 IUD)
�3 � cnZ
Z
A
[v o
0 o w
v, F o
0
F�
3 333333 333 33333
ca ca ca ca cc ca ca ca (a ca cc ca ca ca cc
il=
CD
z
0CDn�'
nm
3
CD
cro
�Q
CD
C
0
0
0
Ul
c c c 333
D U) p r
265. R
_ S
CDcog _ � N � Z �
3 c
cn�
'0 h)
m
n u) (D
j-:Pl-�� rt
(D Q 5 P
0-, 7
c)O
-
j
0
�a
M
F
0
ri
m 4' 2
00
0
z
0
D
a
Co
y
z
v
0
0
Er
IN
mm
c �
voo° �
2nmpcu
n�m
r � �
m m
m
c
v
m
z
Io:
M

O
C
O
CD
-ra
a
CD
Z
0
m
c �N '��:0 0 0
npi�0�mon�- 0 00
fn 3 (� CD e (D c� �p (D 0_
ZO 0 �� c z �n�n
�o
AJn �U 0C
0
—01
O a
n � N
W oa
O ON p O �1
3 3 =F3 3 3 3 3 3 3 S 00
3 3
(.0 (a 0(a(0(0(0(0(0(O :eCO 3310
�(o CD C =T'
e -a e O
e e e e e e O e e e D�
CD ® cCD
'w w = O—Z
c'� --3E3c51co
a
3 3 3
CD 3
— zz
r o 0
0
00
Ul o
333333333333333
0
m cD
0
0
Z3
C
7
v o
�i
Q
(_Cc
®0 N T Z
(D
e e e
FN
Q CD Z
0 � O Q N
3
o (D
C '—s
(T
Q
((DD
amm
O
C
) % w
333
r0ma�(��mmm
=
D N
c. �nr
o
'
o�
A? o
� o ro
O 3
z (D N
N�
(A_
A�
w
o
m�o�vi�
m
0
3
(n
Cn
3 � ¢
CTi
U i
CC1
�1
Q
(D
O (I
N0 m
o o C
A
rh
c,
CD
O
0'3
-.
j m_.
(
0,
Q
C
r
cn
n
cQ
ro
g
r
Cn
NJ
T
0
N
(�
(�—D ccn
w
�
_0 o
C
3
Co
p
I--e
e✓
co
N
O
1 0
co
c�
A O
(D
a
Q.
�o
0
o
�
z
O
0
I
�
CD
I I
I
sv
m
OIo
H a
0 C
O
m
WO
D
Q z
(D
P ro
OR-
0
C'
C)
a
m
r
H
"0
m
Dm
c =+
m -u OZ
C
�0p?
o�
V
� m
w mm m
one
o ON v
O
co ()I
z
G)
O
Z
=1
0
m
a

67
arov-rl uJa�..�er Vlon;ior:�,� l�a�a
/-a..veld
!�¢c� ��� FaG. (, W PQ,-Q MG7Pr RC6u/7S(�fL corhMen'
q� 2
F. ('vl, 31/v�
eel,
79 7. Ys-..
.23
AoLkle %�x r c��c.� do, Aq
% �o nr : / %/vow►-�
00
--- -- - 9 A? a-0!r
--�U'000v I�r�
j- Ve 0U P,5-136" l �,
SEP 2 31992 Li I

0
0�
0
C
C CD
-nz
m U)
:T
0=
�,
0—
O(
w
m
'0
(D
CD (D
O
n
v
0
CL
W CD
O
n
' ,
cnCD
o
0
—
!v
n W
w
Cl)
m
m
CD
CD
3
3
o
w
D
w
M
M o
Q
o
D
m
3
W,
o
a
m
W
0
w
—I
-n
C)
�? '
�'
� m
-
W �
rn
w
CD
m
7o
z
c
Cl)
N°
o
cD
3
o
m
—
m
m
°
0
�'
^D
m—
CD
_0
C/, r-
CD
o
D
_
co
3
0
O
o
0
a
3
`°
C7
G�
b
x
m
D
°
a
=
n
= 3
ry
e
a
`°
1-1(D
rt
O
or
0
D
n
Ili
cn
Ul
rn
F
w
CD
�]
c
m
-
•
m
CDm
--
CD
NJ
w
a
�
`t
_
0
O
CD
Ln
co
o'
cn
In
:U
N
-v
CD
m
o
m
-0
(A)
N
En 3
3
c
3
3
3
3 3
3
3
c
3
o
o
3
-
m
v
m
-
p
c0
c0
O0
to
cn
tQ
t0 cfl
cQ
co
�,
c0
o
o
c0
0
0
aor
0
O
G)
m
rn
0
3
°
c o
CD
00
Z z
7C
2
st
(� C�
C�
C�
W
D
m
z
z
o
a
3'
o
m
a
r-
I
c°
co
cn
c
a
v
v—
O
O
l
o
o
m 3
`
nO
0
n 3
n
i
o
W
'
D
N
a
W
w
N
°'
D
CD
cn
CD
. C�
tlQ
ci O
C a
m
!y
`o
E
CD
O
O C
''oo 3
w
a
0
O
m
c
c
3
O
to
z
c)
Z
CD
<
w
p
d
CW
D 3
cQ
CD
COa_
C
(D
3,
c
_p
°
'a
C
,C
by
m
a'
�`
0
3
3
3
sv
w
m
m
m
_-
w
�rn
co
3
w
o
0
a
m
�
CD
m
c
�
m
v
co
3
cn
—
o
m
v_
o
m
o
C
N
D
_
ni
`D
3
3
!-�
N
cQ
Cl)
CO
A
Q
v
�
C D
c0
n
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3°
(
I
I
I
pm
m
e
a
co
cQ
co
co
(a
cQ
co co
cfl
(ao
o
n
cQ
c0
w
°
o
_
O
C�
o
w
0
C
O
..
w
N
(�N
O
o
o
moo
?
C
�
(D
�.
O
m
Z
a
�.
o¢
6usm
p
W
¢
e
n
(v_
(D
p
rt
x 3
0
z
0
6
0
m
O
z�
m
m
1
r
O
y
rt-s
a—.,
N
r
—•
g
y
NIli
O
(D
CDCl)
a
a;
r
o
,c
mCZ22D_
o
Q
..
a
cu
m
C
c
O�
Q
W
cWn
c
va
rt
�
,l0
>
m
V
x
°
D
o
<
z
CR
ma
'0
CD
CD
I
rn
.�
p
n
�
a c
m
z
A
.
CD
CD
o
Ilim
O
Cl
p,
O
�--
,
O
O
r- 0
CD
D
a
a
3
3
3
co
cQ
c�
co
t
o
o
c0
c
a
p.
..
0
m
n
Q
O'
7
v_
m
CA
m
m
0
0
m
a
--i
m
A
n
r
0
m
0
r
z
0
m
m
m
m
—I
0
c
v
0
w 00
`D o m
co °?per
Q.
w0000
K
Q,V Nt ID
N 01 V (1) R
1 t 00 w
VV~'C
O
7
N
V
(D
ryy
r�yy
yy
La
LO
LQ
IJ

r T!-0 CD 2 0 s�Cn, m .wr. cfJ 0`
` cr ° W o 3 0 77 0 0
' Dw�0 �� (D O � „Z�
° nn0nnDW(�DDo-1—IC�C)80Fn
07 wo ° -i o t.
m 3 w o 0 0 0- cD' w w w LT n o 0 o Dcn m N
ro 3 0 3. o 3. o a °° r'= -1 �, D p0 0
(D -� .E m o o w w 30
w r C r`O
cfl N ro� o o m o o � w w o u0 p
1 p. co � o Z O 0 m� r i71
0 0o Wto w D n� = m o°
co Cn N A w G' -< n ' O O cQ = '71
coo -- om_ 3 =
Ln o` o
0p .P o.; fll Oa O
a < c0'
n c 3 3 3 3 3 3 c Z 3� 1 3 3 3 N o P. CD 'W
j (3 �' cQ r cQ co <n cQ 3 �\0000m o 0 -- m C 3 3
cam° Oin
-- '}
a
n a
(n U) (n '� S S -n
CD °CD
n eZ no 7 7
+ m Oy(n
a oO ai N cm CD
El
Oo(D
o 0 NyoN 1oZZ p,
°
cn LnLnvCD 1 3 . csan^
ow r-N•
m
CL co
,vN�wfl�
0wO0D �V(D w(D obrn
Z -ow ?. CmN3 w oCQ
CD a °
AD ocD
o m
033 33•m 33 mpO
y N
� D
CD Nn0ZZ�m a' w m c 0aw w
Ncnr?to
(D Q O (DO'w �
7
iI'�.�1w7 p<Z
a c � a. c c O
CD e no c 3 w Zn Noc3 vrnom -4
_0NV o V JV co Zr
F' m:Om
m ..
w � m CD (D a CD Z z<Z
3
n 3r m v 33 c �'p o
c c c c 3 c 3 3 c c c c c 3 c; c cE (D ,� (D 3 r
S ^�
(D\ (Q " r O - (D :'tea (D
CI) as0
G) m
w m o
N aw a oo O y T -2
°a p m m� 2 cp o o: o Omm
.G 3 - O -:A Q (D 0:. tmC Z
(O m CD Q (D Ci CD H
O C CD.
CD `� c3 w v m 7o R
m _ cn 52.
N
D m m n
o N z
,. y

-n
S 0
6o
0 N
O
�CD
n.
D
C N
o.
SD y
CD tN
C
C 3
cu =
O
0
0
CD
CC
CD a
of
n�
cq
CD
C7
s
CD
7
n
°0
CD
CD
7
m
M
CD
(A
G)
0
a
c�
7
a
a. IO
n
O
00000D
WpDD'v
f11
O
S
S
Al
A
A7
CD
7
0
0
0
Cr
CD 0
a
W
su
A
7
CD
3.
CD
7
o
�
w
N
N
3
A
ci
=
a
m
CO
0
—i
O
O
O
m
CD
1�
n
M
=
x
A
O C)
OD
A
N
A
A
A
O
c- Q o o 0 n
p p
a coo o =
r
0 3 3 b ca
'n T w w
—{ T7 Cn O
O CD
su
W
C.n
C)
A �
z 3 3 3
C O O =�
I I-
I
N
1� s
I
m
w
c
ca
0 w
° CD
0
a-
Z
O
� Co
-
O
a)
D
DC)CD
0
O
0)C
Q
-0
S
S
S
3
p
� m
O.:
�,
o
� m
m
U
=r
0
yo
n
CD
N
C
N
CD
N
m
D
2. _�
@ CD
(D
co
CD
A
a
O
O
CL
CD
y
t
CD
7
fR
n•
10
D �o -0 CD_
-0
o
r 4
Ir.
mCl)
c'
w o
a
o
-� M.
L
D�
Dv
O
o
I N. m
:a
Z D..
r- lc
:3
o (�
sib
(�
(n
Cl)K-'
�2
o
p p
Z
D
0 0
4 m
r yi
tit
<
O
° �.
m
a $ CD
Q p
oQ o
N O A _
O0
\
Sit
p
tW,,
n
n
rr,^ Mcnpo p
p\D
:3 -0'
0
m
r
rn
n
o
zz 7 -
(D O (A
m
ya9o�
�O
_
'0
Fo.
y
z
z
0
CD
�L�1X�I
-TAM,
G7
w
3
v
5
CD
w
v
o
p
r
CD °
v
cor
m
CD
a
to
Z
CD
�
O
a
a-0
I
�
co..
v_
Ch
s
zc
OA
m'a
z
m�
z—
m=
Z 5. z
m
0 O
r- = -
30 S
Z
A
mom
M70
m- 0
z0-
0.
�zm
O�
C m
v �o
D0
m
N �
m
O
z

-"c11NQ�aEIw LiQAQiTAQY WaLiTiL.EQ iMiLYTIPiL DEPORT
LAD" NO. n,564
REPORTED BY �4*SUPERVISOR
CHECKED BY DATE 6- NIL --
REVIEWED BY ENTERED BY
CHECKED BY
r
SAMPLE TYPE WATER ANALYSIS RESULTS
CAS* VOA Target Compound TQL Conc
i ug/L Detected Ms
J �L
CAS* VOA Target Compound TQL Conc
ug/l Detected MS
��1 /L
75-35-
i i-Dichioroethene
0.75
U
96-18-4
1 3-Trichloro ro ane
0.25
U
75-09-2
Met lene Chloride
0.25
U
108-86-11
Bromobenzene
1
U
156-60-51
trans- l,2-Dichloroethene
10.751
1 U
1
1 95-49-8
2-Chlorotoluene
0.25
U
75-34-3
1 1-Dichloroethane
10-251
U
106-43-4
4-Chlorototuene
0.25
U
590-20-7
2 2-Dichlora ro ane
10.25
U
541-73-1
1 3-Dichlorobenzene
0.25
U
156-59-4
cis- 12-Dichloroethene
10.251
U
J 106-46-7
1,4-Dichlorobenzene
0.25
U
67-66-31
Chloroform
0.25
U
95-50-1
1 2-Dichlorobenzene
0.25
U
i 74-97-5.Bromochloromethane
10.75
U
1 96-12-8
1.2-Dibromo-3-Chloro ro ane
1
U
71-55-611
1 -.1 -Trichloroethane
0-M
U
1 120-82-1
1 ,2.4-Trichiorobenzene
0.25
1U
%3-58-6
1 1-Diohloro ro a
025
U
87-68-3
Hexachlorobutadiene
0.25
U
56-23-51
Carbon Tetrachloride
10.75
I U
87-61-6
1 ,2 3-Trichlorobenzene
0.75
U
107-06.2
1 2-Dichluroethane
10.25
1J
1634-04-4
Methy Hert-buty 1 ether
5
U \
79-01-51
Triehloraethene
10,25
U
71-43-2
Benzene
1
U
-
78-87-511
2-Dichloro o ane
0.25
1 U
108-88-3
Toluene
i
U
5-27-4
Bromodichloromethane
0.25
1
U
100-41-4
Ethyl benzene
1
U
I 74-95-3
Dibromomethane
1
U
108-38-3
m X lenes
1
U
OO6 i -D1-5
cis-1 3-Dichlaro ra ene
0.25
U
95-47-6
o-Xylene
1
U
0061-02-6
trans-1 .3-DichloroprWne
0225
U
100-42-5
St rene
1
U
79-00-5
1 1 2-Trichloroethane
0.25
U
98-82-8
Isopropy lbenzene
1
U
127-1 S-4
Tetrachluroethene
0.25
U
103-65-1
n-Propylbenzene
1
U
1 42-28-9
1 3-Diohloro ro ane
0.25
U
108-67-8
1 3 5-Trimeth lbenzene
1
U
124-48-1
Dibromochloromethane
0.75
U
98-06-6
tert-Bu lbenzene
1
U
106-93-4
1 2-Dibromoethane
1
U
95-63-6
1 2 4-Trimeth lbenzene
1
U
1 108-90-71
Chlorobenzene
0.251
(
U !
135-98-8
seo-But lbenzene
1
U
630-20-6
11 1 2-Tetrachioroethane
0.25
U
99-87-6
-Iso ro Holuene
1
U
75-25-2
Bromoform
0.5
U
104-51-8
n-Bu lbenzene
1
U
79-34-5
1 1 2 2-Tetrachloroethane
0.75
U
91-20-3
Naphthalene
1
U
TQL- target guantitation limit
T- tentatively identified compound
€- estimated value
U- compound was analyzed for but
not detected
N- not analyzed for this compound
D- detected below quantitation limit
MS- X=GCfMS analysis performed
TQL subject to change due to instrument sensitivity
COMMENTS:
Cono
Other purgeables (up to 10 highest peaks) Detected
ug/L
NO VOLATILE ORGANIC COMPOUNDS DETECTED BY GCIELCD/PID.

j8MIVOLATILE ORGANICS REPOR-. DEM LAB
LAB NUMBER: 2G564 SUPERVISOR LAB #: 2G564
DATE 2
REPORTED BY -6rn
CHECKED BY- t4D ENTERED BY
REVIEWED CHECKED BY
SAMPLE TYPE: WATER DILUTION FACTOR
CAS NUMBER
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2-
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
606-20-2
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
121-14-2
84-66-2
7005-72-3
86-73-7
_100-01-6
534-52-1
CONC.
TQL ANALYTE NAME UG/L
X 1
10
PHENOL
U
10
BIS(2-CHLOROETHYL) ETHER
U
10
2-CHLOROPHENOL
U
10
1,3-DICHLOROBENZENE
U
10
1,4-DICHLOROBENZENE
U
20
BENZYL ALCOHOL
U
10
1,2-DICHLOROBENZENE
U
10
2-METHYL PHENOL
U
10
BIS(2-CHLOROISOPROPYL) ETHER
U
10
4-METHYL PHENOL
U
10
N-NITROSO-DI-N-PROPYLAMINE
U
10
HEXACHLOROETHANE
U
10
NITROBENZENE
U
10
ISOPHORONE
U
10
2-NITRO PHENOL
U
10
2`,4-DIMETHYL PHENOL
U
50
BENZOIC ACID
U
10
BIS(2-CHLOROETHOXY) METHANE
U
10
2,4-DICHLORO PHENOL
U
10
1,2,4-TRICHLOROBENZENE
U
10
NAPHTHALENE
U
20
4-CHLOROANILINE
U
10
HEXACHLOROBUTADIENE
U
20
4-CHLORO-3-METHYL PHENOL
U'
10
2-METHYL NAPHTHALENE
U
10
HEXACHLOROCYCLOPENTADIENE
U
10
2,4,6-TRICHLORO PHENOL
U
10.2,4,5-TRICHLORO
PHENOL
U
10
2-CHLORO NAPHTHALENE
U
50
2-NITROANALINE
U
10
DIMETHYL PHTHALATE
U
10
ACENAPHTHYLENE
U
10
2,6-DINITROTOLUENE
U
50
3-NITROANALINE
U
10
ACENAPHTHENE
U
50
2,4-DINITRO PHENOL
U
50
4-NITRO PHENOL
U
10
DIBENZOFURAN
U
10
2,4-DINITROTOLUENE
U
10
DIETHYL PHTHALATE
U
10
4-CHLOROPHENYL PHENYL ETHER
U
10
FLUORENE
U
50
4-NITROANALINE
U
50
4,6-DINITRO-2-METHYL PHENOL
U

'--iMIVOLATILE ORGANICS REPOh- '- DEM
LAB
86-30-6
10
N-NITROSODIPHENYLAMINE
U
101-55-3
10
4-BROMOPHENYL PHENYL ETHER
U
118-74-1
10
HEXACHLOROBENZENE
U
87-86-5
50
PENTACHLORO PHENOL
U
85-01-8
10
PHENANTHRENE
U
120-12-7
10
ANTHRACENE
U
84-74-2
10
DI-N-BUTYL PHTHALATE
U r
206-44-0
10
FLUORANTHENE
U
129-00-0
10
PYRENE
U
85-68-7
10
BUTYLBENZYL PHTHALATE
U
91-94-1
20
3,3'-DICHLOROBENZIDINE
U
56-55-3
10'BENZO(A)ANTHRACENE
U
218-01-9
10
CHRYSENE
U
117-81-7
10
BIS(2-ETHYLHEXYL) PHTHALATE
U
117-84-0
10
DI-N-OCTYL PHTHALATE
U
205-99-2
10
BENZO(B)FLUORANTHENE
U
207-08-9
10
BENZO(K)FLUORANTHENE
U
50-32-8
10
BENZO(A)PYRENE
U
193-39-5
10
INDENO(1,2,3-CD)PYRENE
U
53-70-3
10
DIBENZO(A,H)ANTHRACENE
U
191-24-2
10
BENZO(G,H,I)PERYLENE
U
OTHER SEMIVOLATILE
ORGANICS FOR SAMPLE NUMBER
2G564
NO BASE/NEUTRAL OR
ACID EXTRACTABLE ORGANICS
DETECTED BY
GC/MS.
TQL= TARGET
QUANTITATION LIMIT
T= TENTATIVELY IDENTIFIED
ESTIMATED CONCENTRATION
E= ESTIMATED CONCENTRATION
U= COMPOUND
ANALYZED
FOR NOT DETECTED
N= COMPOUND
NOT ANALYZED FOR
D= DETECTED
BELOW
QUANTITATION LIMIT
H= HOLDING TIME EXCEEDED
TQL SUBJECT
TO CHANGE DUE TO INSTRUMENT SENSITIVITY

m
1
0
m
m
O
13
U5
-i
C
m
Z
n
C
m
--iO.O ��S�Z
�O
C �Sv
CDO^
O�O
Q
00
0
Z �'�,
�
CD 0_
�
W
�
O Q O N
N� 0 'fi llCL
N
O
O O
� N
v? O CD
y
(D
�
cc
co co 00L,
s
N N N
W N N3
W
N N N
N Ny
N
NC N N
NN
33�3333333=3
003
cc cc o cc cc cc cQ cQ cc cc
��0 ��=-- \�O
� cc 3 3 cc
�
0 �
�0
��^►cDc����
CD
3 C�C�'��--
cO 2
CD
c
3 30
�D33
ZZ
�
O
�
F-
W
O
O
N
N
N
rn
N
N
N
333333333339333
cc cc cc cc cc cc cc
cc cc cc cccncccc(a
0 CD
(D O Cr
O
O ch
.NrZ
0
p CD n Q N
3 \
✓
CD
o CD
cr
0
OL
CD
O
O
O Q.
--
-'.
�
�
N
N
� N
� �
CQ Cf? CQ CQ CQ CQ
r�cTD cD�m m m O
cn
ID
CI-
� �o���9
z
3
n [hD 5 - NO
CD
O �_ -' Vi rD (F
ti
�d
�
3
�
�1
O
Fttd
N in
pq
FH.�.
td
�
3
w
(Dx
_
N
CD
1.
w
Wo
=off
O
Ft
t l
u, CD
00 3 a 3
Z
n
Oq
in
a s
D)
O
p � � cn
c M.
d
cQ
CD 0N�
O'QFt
..
NT
O
00
C3
N
ct
v o
v~i
-•►
SL
N
(D
N
n
rL
F•h
N•
�p
Ft
O
K_
c�
m O
CD
a.
W
no;
m
n
m
m
0
w
��,
z
o;
p�
'�
O'
(D
m_0w
Owy
nip
D
m
N
l
I
I
r
a
�. 4
m
.
Co
VNVi
w
ca
n
C
n
z
$'
m
v
Z
n
0
5 D
m
o
z
VI
0
S
T �
'Q.a
•-
,.
W
a
0
CJ
rt
I-J CD
�'
a

n DEPARTMENT OF NATURAL RESO ] CES AND COMMUNITY DE'
,61ON OF ENVIRONMENTAL MANAGEMEN' ,ROUNDWATER SECTION
P.O. BOX 27687 - RALEIGH,N.C. 27611, PHONE [phone] f?
WELL CONSTRUCTION RECOR
Baker's Piedmont Well &FPum
PMENT FOR OFFICE USE O.
Y72 2 3
�Ant� i y ! Quad. No. � �� Serial N�
i°IF1(l 11 19� Lat: ,3.' 4 Long.y/ .13 3
MinorBasin
, PUd& Code
leader Ent
GW-1 Ent._
DRILLING CONTRACTOR 339
DRILLER REGISTRATION NUMBER STATE WELL CONSTRUCTION 339 PERMIT NUMBER: 13-00110-WM-0060
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Granite Falls county: Caldwell
(Road, Community, or Subdivision and Lot No.)
2. OWNER Huffman Finishing
ADDRESS P 0 Box 170
(Street or Route No.)
Granite Falls NC 28637
City or Town State Zip Code
I. DATE DRILLED 2-20-92 USE OF WELL Monitor _
i. TOTAL DEPTH 15' CUTTINGS COLLECTED ❑ Yes ® No
>. DOES WELL REPLACE EXISTING WELL? ❑ Yes ® No
i. STATIC WATER LEVEL: 10 FT. ❑ above TOP OF CASING,
1z1 below
TOP OF CASING IS 1 1 2 FT. ABOVE LAND SURFACE.
'. YIELD (gpm): NA METHOD OF TEST
I. WATER ZONES (depth):
CHLORINATION: Type Amount
D. CASING:
Wall Thickness
Depth Diameter or Weight/Ft. Material
From 0 To 5 Ft. 2" #4.0 pvc
From To Ft.
From To Ft.
I. GROUT
Depth
Material
Method
From
0
To
3
Ft.
cement
pour
3
5
Bentonite
pour
From
To
Ft.
?. SCREEN:
Depth
Diameter Slot Size
Material
From
5
To
15
Ft.
2" in. .010
in pvc
From
To
Ft.
in.
in.
From
To
Ft.
in.
in.
1. GRAVEL PACK:
Depth
From To
nPII I INC" i rlr,
Formation Description
n, F
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State Roads
or other map reference points)
Hwy 321 North
to Granite Falls
Huffman
Finishing
X well
Depth Size Material T
From 5 To 15 Ft. ASTM sand Hwy 321 Southto Hickory & i-4.O
from To Ft.
,REMARKS:For Compliance with permit NO. 0025135
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
SIGNATURE OF CONTRACTOR OR AGENT DATE
W-1 Revised 11/84 Submit original to Division of Environmental Management and copy to well owner.

s CALDWELL COUNTY
HUFFMAN FINISHING
GRANITE
FALLS UNNAMED TRIBUTARY
TO CATAWBA RIVER
RHODIIISS ---�� HICKORY 8�
LONGVIEW
BURKE COUNTY
- U. S. 64. 70 , 321
CATAW BA COUNTY
IT PLANT
MW3

DEPART OF NATURAL RESOURCES AND COMM' Y DEVELOPMENT
DIVISION OF ENVIRONKMAL MAMA
WELL AND PUMP INSPECTION REPORT �! �8 _ 17 Z
Date
Well location
f'T6 �=�1 LLS r A/C Area GRA°Vi-rE j-'ALL
C�R,4 1,)_
(Town, Come., Subdivision and Lot No.) County CAt-z7vV6LL.
Owner-1ItF,1C_MAA1 FIIV!SN1NG C0Mf0/}A'jy
Road/Street -!?rF a' 'S '
Address /" • 0 • .3 D x U Quad No. 3
-r FALLS NG F6 3 D 33
GR/1 Serial No. 1.35
35 44 ��'23 37
Lat. Long.
WELL CONSTRUCTION
237
Drilling Contractor
Address
Reg. #
Name
Meets Min. Standards
Measure
Yes No
Remarks
wA1
Permit
-----
Location
Distance from
_
�
Pollution source
— ----
Other location standards
Total Depth
Casing
Depth
Diameter
Weight/thickness
Sc N 0
(
`/
Height
IV.14
Drive shoe
Exception approved by owner
Grout:
Type
,
Thickness
Depth
0-3
✓
f_ �
-{�
Screens
AIIA
Development
-==
I: D. Plate
AIM
A ,6 V/A RN1 nl G LA l3CL .
Abandonment (temporary/permanent)
Water level
Well test.
—=1144
Chlorination--=F---
CuttinQs
Reports
(a earance)
Water camn e pp