HomeMy WebLinkAboutWQ0018352_Residual Annual Report 2018_20190131js�� s�,
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!19:11,' TOWN OF BOILING SPRINGS
January 17, 2019
NCDENR-Division of Water Quality
Aquifer Protection section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2018 Annual Land Application of Residuals
Town of Boiling Springs
Permit# WQ0018352
To Whom It May Concern:
RECEIVEDINCDFO'014"JR
JAN 3 1 2019
Non-D sch-'
Perrni;ung Unit
Please find enclosed the original and (2) copies of all applicable forms and test results for
The Annual Land Application Report for the Town of Boiling Springs. Aerobic digested residuals
continue to be land applied to permitted fields for beneficial reuse as a soil conditioner and
fertilizer supplement.
Please give me a call if you have any questions or if additional information is needed at (704)
434-2357.
Sincerely,
i(XW.;
Lucas Shires
Town Manager
Cc: File
Enclosures
Rl=ri=l\/F[)
JAN 31 2019
DWR SECTION
INFORMATION PROCESSING UNIT
114 East College Ave I P.O. Box 1014 128017 1 (704) 434-2357 1
www.BoilingSpringsNC.net
ANNUAL LAND APPLICATION
OF RESIDUALS
2018 ANNUAL REPORT
TOWN OF BOILING SPRINGS
Permit No. WQ0018352
C.
0- SPR
41
19.1 AA 11
CERTIFICATION FORM
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit*: W00018352 County:
Faci ity Name (as shown on permit):
Land Application Operator:
Cleveland
Year: 2018
Town of Boiling Springs
Mike Gibert Phone: 704-434-2357
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Anolication Summarv:
Total number of application fields in thepermit:
3
Total number of fields utilized for land application during the yearl
2
Total amount of dry tons applied during the year for all application sites:1
10.51
Total number of acres utilizes for land application during the year: 1
26.2
Part B - Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Lucas Shires / Town Manager
Permittee Name and Title (type or print)
41
Signature of Permittee — ate
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)
RESIDUALS SAMPLING FORM
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00018352
Facility Name: Town of Boiling Springs
Laboratory: 1) Pace Analytical Services
2)
Residual Source WQ # or NCO071943 3)
NPDES #: 4)
WWTP Name: Town of Boiling Springs WWTP 5)
Residual Analvsis Data
Parameter
Sample or Composite Date
Total Phosphorus
' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
71,11:� =7 4.a
Signature of Preparer *
Date
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00018352 Laboratory: 1) Pace Analytical Services
Facility Name: Town of Boiling Springs 2) Waypoint Analytical
Residual Source NCO071943 3)
NPDES # or WQ#: 4)
WWTP Name: Town of Boiling Springs WWTP 5)
Residual Analysis Data
Parameter
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
DENR FORM RSSF - B (12/2006)
METALS FIELD LOADING SUMMARY
0
LAND APPLICATION FIELD SUMMARY
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: Town of Boiling Springs
Land Owner: James Pell
Operator: Mike Giber[
Crop 1 Name: pasture
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0018352 Field #: I Acres Utilized: 9.84
Annual Dry Tons Applied: 6.7554 Site*: JPI Acres Permitted:
Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 220 Crop 2 Name:
Crop 2 Max. PAN:
`o
o
A
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
qo
Solids
Volume
Applied per
Acre
(Dry TonslAc)
Residual Sources
(NPDES #, WQ#,
Fen.. Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
D
K'
m 'a
S m
ii c
°
o
a ^
m _,
N
*
.°�
'�
o m
m -
Q
TKN0
mg/kg
z a
6
3
R.
mg/kg
Nitrate
and
Nitrite
mglkg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1-10-18
16000
1.2
0.081
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
5.214
NA
pasture
2-23-18
15000
1.2
0.076
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
4.888
NA
pasture
2-27-18
15000
1.2
0.076
NCO071943
dry
1 0
S
0.5
0.3
57900
859
1 14500
4.888
NA
pasture
3-27-18
6000
1.2
0.031
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
1.955
NA
pasture
4-4-18
21000
1.2
0.107
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
6.844
NA
pasture
9-13-18
16000
1.2
0.081
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
5.214
NA
pasture
10-3-18
12000
1.2
0.061
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
3.911
NA
pasture
10-4-18
24000
1.2
0.122
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
7.821
NA
pasture
10-5-18
10000
1.2
0.051
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
3.259
NA
pasture
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
135000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
43.995
0.000
Lime Applied
Annuallbs/acre
0.108
0.011
0.320
0.000
0.054
0.002
0.054
0.054
0.108
1.061
18.110
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.581
0.074
3.129
0.277
0.378
0.009
0.379
0.384
0.759
9.469
Current Cumulative Ibs/ac
0.689
0.085
3.449
0.277
0.432
0.011
0.433
0.438
0.867
10.530
Permitted C. P. L. R.****
36
34
1338
n/a
267
15
n/a
74
89
2498
Permit PAN Limit lstl2nd Crop
220
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
q *Application Method: S - Surface, IN - Injection, INC - Incorporation
1 f / **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual): 6.75
Permit #: NCO071943 Cation Exchange Capacity (non 503 only):
Operator: Mike Gibert Owner: James Petty Predominant Soil Series: 3acolet-Bethlehem
Acres Used: 9.84 Acres Permitted: Site #: 1 Field #: JPl
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
9/26/18
2-J
9/26/18
3
9/26/18
41
9/26/18
51
9/26/18
61
9/26/18
7
9/26/18
8111
9/26/18
9
9/26/18
10
11
12
% Solids
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
Arsenic
78.4
78.4
78.4
78.4
78.4
78.4
78.4
78.4
78.4
Cadmium
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
7.8
Copper
1 233
233
233
233
233
233
233
233
233
Chromium
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
1.7
rdenum
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
39.2
78.4
78.4
78.4
78.4
78.4
78.4
78.4
78.4
78.4
773
773
773
773
773
773
773
773
773
Total
Phos-
horus
13200
13200
13200
13200
13200
13200
13200
13200
13200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
y
Event
0.08
0.08
0.08
0.03
0.11
0.08
0.06
0.12
0.05
"
Arsenic
0.013
0.012
0.012
0.005
0.017
0.013
0.010
0.019
0.008
0.000
0.000
0.000
0.108
Cadmium
0.001
0.001
0.001
0.000
0.002
0.001
0.001
0.002
0.001
0.000
0.000
0.000
0.011
Copper
0.038
0.035
0.035
0.014
0.050
0.038
0.028
0.057
0.024
0.000
0.000
0.000
0.320
Chromiud
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.006
0.006
0.006
0.002
0.008
0.006
0.005
0.010
0.004
0.000
0.000
0.000
0.054
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.006
0.006
0.006
0.002
0.008
0.006
0.005
0.010
0.004
0.000
0.000
0.000
0.054
denum
Nickel
0.006
0.006
0.006
0.002
0.008
0.006
0.005
0.010
0.004
0.000
0.000
0.000
0.054
Selenium
0.013
0.012
0.012
0.005
0.017
0.013
0.010
0.019
0.008
0.000
0.000
0.000
0.108
Zinc
0.125
0.117
0.117
0.048
0.165
0.125
0.094
0.189
0.079
0.000
0.000
0.000
1.061
Total
Phos-
2.138
2.006
2.006
0.818
2.825
2.138
1.610
3.221
1.346
0.000
0.000
0.000
18.110
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
I -I 7-I �
Date
DENR FORM MFLSF (1212006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: Town of Boiling Springs
Land Owner: James Petty
Operator: Mike Gibert
Crop I Name: pasture
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit*: WQ0018352 Field #: 2 Acres Utilized: 16.36
Annual Dry Tons Applied: 3.7530 Site*: JP2 Acres Permitted:
Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503):
Crop 1 Max. PAN:
220 Crop 2 Name:
Crop 2 Max. PAN:
c s
c
m O
C]
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
PP Pam'
Applied
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(�'
Wet,
Moist)
PrBc1P•
past 24
Hrs.
inches
>
m
� �
0
m
m _.
`* d
fe
o
5'
m R
m^
�•
r _
8
TKN
mgtkg
? S
o 3
c
-'m•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
8
Application
Crop 1
Crop 2
Crop 1
Crop 2
3-27-18
6000
1.2
0.018
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
1.176
NA
pasture
3-28-18
15000
1.2
0.046
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
2.940
NA
pasture
3-29-18
9000
1.2
0.028
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
1.764
NA
pasture
6-6-18
9000
1.2
0.028
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
1.764
NA
pasture
6-15-18
6000
1.2
0.018
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
1.176
NA
pasture
8-8-18
30000
1.2
0.092
NCO071943
dry
0
S
0.5
0.3
57900
859
14500
5.880
NA
pasture
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
75000
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
14.701
0.000
Lime A lied
Annual lbs/acre
0.036
0.004
0.107
0.000
0.018
0.001
1 0.018
0.018
0.036
0.356
6.072
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.533
0.069
0.849
0.277
0.355
0.008
0.356
0.361
0.711
8.889
Current Cumulative Ibs/ac
0.569
0.073
0.956
0.277
0.373
0.009
0.374
0.379
0.747
9.245
Permitted C. P. L. R.****
36
34
1338
n/a
267
15
n/a
374
89
2498
Permit PAN Limit lst/2nd Crop
F 220
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
(� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual): 3.76
Permit #: NCO071943 Cation Exchange Capacity (non 503 only):
Operator: Mike Gibert Owner: James Petty Predominant Soil Series:'acolet-Bethleherr
Acres Used: 16.36 Acres Permitted: Site #: 2 Field #: JP2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
posite
Date
1
9/26/18
r9/26/18
9/26/18
9/26/18
9/26/18
6
9/26/18
78
9
10
11
12Com-
% Solids
1.2
1.2
1.2
1.2
1.2
1.2
Arsenic
78.4
78.4
78.4
78.4
78.4
78.4
Cadmiuml
7.8
7.8
7.8
1 7.8
7.8
1 7.8
Copper
1 233
233
233
233
233
233
Chromium
Lead
39.2
39.2
39.2
39.2
39.2
39.2
Mercury
1.7
1.7
1.7
1.7
1.7
1.7
Molyb-
denum
39.2
39.2
39.2
39.2
39.2
39.2
Nickel
39.2
39.2
39.2
39.2
39.2
39.2
Selenium
78.4
78.4
78.4
78.4
78.4
78.4
Zinc
773
773
773
773
773
773
Total
Phos-
horus
13200
13200
13200
13200
13200
13200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1 1
0.02
2
0.05
3
0.03
4
0.03
5
0.02
6 j
0.09
7
81
91
101
12
_
r
Arsenic
0.003
0.007
0.004
0.004
0.003
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Cadmium
0.000
0.001
0.000
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.008
0.021
0.013
0.013
0.008
1 0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.107
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.001
0.004
0.002
0.002
0.001
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.001
0.004
0.002
0.002
0.001
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Nickel
0.001
0.004
0.002
0.002
0.001
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Selenium
0.003
0.007
0.004
0.004
0.003
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Zinc
0.028
0.071
0.043
0.043
0.028
0.142
0.000
0.000
0.000
0.000
0.000
0.000
0.356
Total
Phos-
horus
0.475
1.214
0.739
0.739
0.475
2.429
0.000
0.000
0.000
0.000
0.000
0.000
6.072
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1-1-I-tq
Date
DENR FORM MFLSF (12/2006)
RESIDUALS ANALYSIS LAB SHEETS
ce,4na�ytica�• ANALYTICAL REPORT
N•aorrei o)Vi/eaarg smnovxno', October 09, 2018
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1029978
Samples Received: 09/28/2018
Project Number: 92400957
Description: Digester Sludge
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
fltv4u"'�vs/-�i
Pam Langford
Project Manager
„
Resuhs relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
-:� reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pac onal
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304
WNW..o,�.,
zaceAnalytical e
waw.pacelabs. con,
ANALYTICAL RESULTS
Project: Digester Sludge
Pace Project No.: 92400957
Pace Ana"cal Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: Digester Sludge Lab ID: 92400957001 Collected: 09126/1806:55 Received: 09/2611808:55 Matdx:Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Aluminum
13800 mglkg
784
1 09/27/18 10:58
09128/18 05:48
7429-90-5
Arsenic
NO mglkg
78.4
1 09/27/18 10:58
09128118 05:48
7440-38-2
Cadmium
NO mglkg
7.8
1 09/27/18 10:58
09128/18 05:48
7440-43-9
Copper
233 mg/kg
39.2
1 09/27/18 10:58
09/28/18 05:48
7440-50-8
Lead
NO mg/kg
39.2
1 09/27/18 10:58
09/28/18 05:48
7439-92-1
Molybdenum
ND mg/kg
39.2
1 09127/1810:58
09/28/18 05:48
7439-98-7
Nickel
ND mg/kg
39.2
1 09/27/18 10:58
0928118 05:48
7440-02-0
Potassium
ND mg/kg
39200
1 09127/1810:58
09/2811806:48
7440-09-7
Selenium
ND mg/kg
78.4
1 09/27/18 10:58
09/28/18 05:48
7782-49-2
Zinc
773 mglkg
78.4
1 09/27/18 10:58
09/28/18 05:48
7440-66-6
7471 Mercury
Analytical Method: EPA 7471E Preparation Method: EPA 7471E
Mercury
1.7 mg/kg
0.44
1 09/29/1815:49
10101/1811:51
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
1.2 %
0.000010
1
09/27/18 16:08
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.8 %
0.10
1
0927/18 16:00
9046 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
9.9 Std. Units
0.10
1
0927/18 16:29
Q
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Plant Available Nitrogen
32000 mg/kg
0.12
1
10/04/1813:38
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
859 mg/kg
815
1 10/0111822:48
10/02/1814:10
7664-41-7 J(R1)
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation Method: EPA 361.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
57900 mg/kg
2670
1 09/30/18 10:38
09/30/18 19:22
7727-37-9
363.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
14500 mg/kg
841
5 09/28/18 07:55
09/28/18 09:36
Nitrogen, Nitrate
14100 mg/kg
841
5 09128/1807:55
0928/1809:36
14797-55-8
Nitrogen, Nitrite
409 mg/kg
84.1
1 0928/1807:55
0928/1809:26
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA365.1 Rev 2.01993
Preparation
Method: EPA365.1 Rev 2.01993
Phosphorus
13200 mg/kg
847
5 0912811815:00
0929/1816:19
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/10/2018 08:56 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 27
e DIGCSTER SLUDGE SAMPLE RESULTS — 01 ONE LAB. NATIONWIDE.
Collected date/time: 09/26/18 06:55 L1029978
Metals (ICP) by Method 6010D
Result
Qualifier MDL
RDL
DiluBon Analysis
Analyte
mg/kg
mg/kg
mg/kg
mm10.0
date/time
Calcium
533
0463
�1 10/05/201810:57
Magnesium
180
0111
10.0
.1 10/05/201810:57
Sodium
49.1
0,985
10.0
.1 10/05/201810:57
Batch LP
WG1175645 TC
WG1175645
WG1175645 a 5s
QCn
aQC
7G1
�AI
BSc
ACCOUNT: PROJECT: SDG:
Pace Analytical- Huntersville. NC 92400957 L1029978
..Page 22 of 27
DATE7TIME: PAGE:
1010911817:01 5 of 10
CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical w
Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields
LASUSEONLY.AffixWorkordeq[ oginLabelHere orustPace.WorkorderNumberor
MTJL Logdn Number Here .
ALL SHADED AREAS are for LAB'USfi=ONLY
Company: Town of Boiling Springs
Billing Information: same
Address: PO Box 1014 Boiling Springs NC 28017
Container Preservative Type "
Lab Project Manager:
Report To: Mike Gibert
Email To: mike.gibert@bo]lingspringsnc.net
'. Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7)sodium bisulfate, (a) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other
Copy To: Todd HUmphries
.Rockford
Site Collection Info/Address: WWTP 2556
Road
Analyses
tab Profile/Line:
Customer Project Name/Number:
State: County/City: Time Zone Collected:
NC / Cleveland [ ]PT [ ]MT I ]CT [ x ]ET
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tab Checklist: Sample. Receipt ,,
Cust6dy SaaiS Pre rtnt/tatacti. IA
Custody Signatures .ilresent NACL
Colleatoi .SignaCure Present. _. ti"NA
Bottles 'Intact NA'
Correct Aottic N NA
Sucient,volume N,NA -
Samples iteceived an 'Ice Y N A
VOA = Headspace Acceptable •.Y N�
USDA Regulated Soils N�;::�•
Samplr s in 'holding •Time Ll NA
Residtial' Chlorine present �Y NA
Cl Strips:
'Sample pH Acceptable Y'N N
pit 'atrips
Sulfide Present x 'N t1A
Lead Acetate._Strips:
LAB USE ONLY-
Lab 'Sample 4 I Comments'
1 0 v t t
Phone: 704-434-2357
Email:
Site/Facility ID'#: N00071943
Compliance Monitoring?
I ] Yes ( ] No
Collected By (print):
Purchase Order # :
Quote#:
DW PWS ID #:
DWLocationCode:
Collected By (signature):
Turnaround Date Required:
Immediately Packed on Ice:
[ ] Yes [ - ] No
Sample Disposal:
Dispose
(] appropriate ( ] Return[
( ] Archive:
( ]Hold:
Rush:
] Same Day ( j Next Day
2 Da 3 Da 4 Da 5 Da
( ] y ( ] y [ ] Y [ ] Y
(ExpediieCharges Apply)
Field Filtered (if applicable):
[ ]Yes [ ) No
Analysis;
Y
` Matrix Codes (Insert in Matrix box below):' Drinking Water (OW), Ground Water(GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tlssue.(TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
Matrix `
Camp /
Grab
C011e[ted (Or
Composite Start)
End
Res
Res
CI
# Of
Ctns
Date
Time
Date
Time
Digester Sludge
WW
Grab
9/26/18
ao
Digester Sludge
WW
Grab
9/26/18
S^''
T
X
X
Digester Sludge
WW
Grab
9/26/is
}Iw
1
X
Digester Sludge
WW
Grab
9/26/18
X
X
X
X
Digester Sludge
WW
Grab
9/26/18
2
X
Customer Remarks / Special Conditions Possible Hazards:
All results must be in MG/KG except for
SAR
Type of.Ice Used Wet Blue - Dry: ' None
.:.. ,:.. ..
SHORT HOLDS PRESENT (<72' hours).:
" Y -
N/A
BpSampin Te p ` tu��nfo. NA
Te Blank R era .
18 tell
Therm D{
E n
Cooler 1 .Temp Upon Receipt C
cooler 1 Therm Carr. Factorl. cc
Cooler 1 Corrected Temp: i' cc
Comments:
j
Packing.Matertal Used: ttr'
.tC,: •
�
lab Tracking#
Radchem sampie(sj screened (<500 cpm): Y N NA
Samples recelved'via
FEDEX UPS'; r .Client Courier PaceCourler
_ . .:
R uis ed mpan : (Signature)
Date ime:
g u si o f
ec ' e om y: ignature)
Dat /Time:
/Y �.
MTJLIAB USEONLY ',
Table,q:.
R m hed y/Comp ny: (Signature)
m inr
D to e:
f � Y Ll
Received by/Company: (Signature)
% ` � `T, 1 (J �'C•L
Date/Time:
p
j' f G3 I It �,i
Acctnum:
Template:
Prelogin.
PM:
PS:
Trip Blank Received Y A
HCL M60H TSP Other
41inquished by/Company: (Signature)
O _
N
Date/Time:
Received by/Company: (Signature)
Date/Time:
Non Conformance(s):
YES J NO
Page:
of:
Analytical Results STATESVILLE
ANALYTICAL
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date:
09/26/2018
Reported:
09/27/2018
For:
Digester Sludge Town of
Boiling Springs
Comments:
Geometric Mean 16,268 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
180926-22-01
Fecal Coliforms
1
17557
MPN/g
SM92210E-20o
09/26/2018
WC
180926-22-01
Percent Solids
1
1.31
%
SM2540B4011
09/26/2018
WC
180926-22-02
Fecal Coliforms
2
62992
MPN/g
SM92210E-2006
09/26/2018
WC
180926-22-02
Percent Solids
2
1.27
%
SM2W8-2011
09/26/2018
WC
180926-22-03
Fecal Coliforms
3
17164
MPN/g
SM92210E-2006
09/26/2018
WC
180926-22-03
Percent Solids
3
1.34
%
SM2WB-2011
09/26/2018
WC
180926-22-04
Fecal Coliforms
4
5674
MPN/g
SM92210E-2006
09/26/2018
WC
180926-22-04
Percent Solids
4
1.41
%
SM2WB-2011
09/26/2018
WC
180926-22-05
Fecal Coliforms
5
17829
MPN/g
SM92210E-2006
09/26/2018
WC
180926-22-05
Percent Solids
5
1.29
%
SM2540B-2011
09/26/2018
WC
180926-22-06
Fecal Coliforms
6
9353
MPN/g
SM92210E-200B
09/26/2018
WC
180926-22-06
Percent Solids
6
1.39
%
SM2WB-2011
09/26/2018
WC
180926-22-07
Fecal Coliforms
7
16788
MPN/g
SM92210E-2006
09/26/2018
WC
180926-22-07
Percent Solids
7
1.37
ova
SM2WB-2011
09/26/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of Aage 5 of 8
CHAIN -OF -CUSTODY Analytical Request Document
LAS USE ONLY -Affix Wwkofd&/login Label Here or Lkt Paca Workorder Number or
ceAnalytical e
MTJL tog4n Number Here
Chalnrof-Custody, is a LEGAL DOCUMENT - Complete all rekvent fields
ALL SHADED AREAS are for LAB USE ONLY
Company: Town of Boiling Springs
Billing Information: same
Address: PO Box 1014 Boiling Springs NC 28017
Container Preservative Type"
tab Project Manager:
ReportTo: Mike Gibert
Email To: mike.gibert@boilingspringsnc.net
u 1
" Praerva#ve Types: (1) runic acid, (2) svlf..r arid. (31 hydrochloric acid. (a) sodium hydroxaa (5) zinc acetrte
(6) methanol, (7) sodium bisulfate, (a) sodium thiosuHate, (9) hexane, (A) ascorbic acid. IBI ammonium sulfate,
Copy To: Todd Humphries
Site Collection Info/Address: VVWTP 2556
Rockford Road
tC) ammonium hydroxide,(0) TSP, ILI Unpresered,(01 Other _
Customer Project Name/Number:
State: County/City: Time Zone Collected
Analyses
lab Pm le/U-
Lab Sample Reoeipt Cheeklipt:
Custody Seals Present/Intact thy'
custody signature. &R�
NC / Cleveland I IPT [ IMT I )CT [ x JET
Phone: 704-434-2357
Site/FacilitylD #: NC0071943
Compliance Monitoring?
Email:
[x I Yes I ]No
Present y
Collector signature Present A
Bother, Intact A
Collected. y (print):
Purchase Order # :
DW PWs ID #:
Quote#
DW Location Code:
Correct Settles NA:
Sufficient Voluae RNA
Samples Received on Ice N
Collected By (signature):
Turnaround Date Required:
Immediately Packed on Ice:
( jYes [ ]No
t
.�
3
C
VOA - Headapace Acceptable Y Ii NA
Usm Ragulated Boils % A
Sample. in molding Tim. Y NA
Sample Disposal:
[ J Dispose as appropdate I ]Return
push:
I I Same Day [ I Next Day
Field Filtered lit applicable):
( I Yes f I Na
I ) Archive:
)Hold;
[ ] 2 Da y I ] 3 Day ( 14 Day [ ] S Day
�
O
U
Residual Chlarina Present NA
Cl Strips:
(Expedite ounges Apply)
Analysis:
N
10
ig
U
m
Sample PH Acceptable Y N tO
PH Strips:
sulfide Present x R NA
'Matrix Codes ([risen In Matrix box below): Drinking Water (OW), Ground Water(GW), wastewater [WW),
Product (P), Soil/Solid (SL], Oil (OL), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), Vapor IV), Other (Or)
C
mm
O
O
O
Lead Acetate Strips:
LAB USE ONLY;
Comp)
Collected (Of
Composite End
Res
# of
Customer Sample ID
Matrix •
Grab
Com
Composite Start
p )
Cl
Ctns
i
C�
Lob satmple ; /Comments:
Date
Time
Date
Time
a-
cT
C1 2 0 /"1/ / n 1
1 �/�
Digester Sludge
WW
Grab
9/26118
2
X
X
001
Digester Sludge
WW
Grab
9/26/18
r7
2
X
X
Digester Sludge
WW
Grab
9/26/18
'.(
2
X
X
Digester Sludge
WW
Grab
9/26118
cn
2
X
X
Digester Sludge
WW
Grab
9/26/18
U 71
2
X
X
Digester Sludge
WW
Grab
9/26/18
Li
2
X
X
Digester Sludge
WW
Grab
9/26/18
2
X
X
Customer Remarks /Special Conditions /Possible Hazards:
Type of Ice Used: We SIM Dry None
SHORT HOLDS PRESENT (<72 hours) : Y & N/A
LAB Sample Temperature Info:
Temp Blanc nee iva (itJ
Therm IOI: '
Packing Material Used: �/,�] I _ ,.,-�
LCJ
lab Tracking #:
jJ�;IG �
Cooler 1 Temp Upon Receipt:
Radchem samples) screened (<SDO cpm): Y N NA
Samples received via:
(�1/l 3s Z
Cooler t Therm Corr. 'actO
Cooler r Corrected
FEDEX UPS Client Louder Pace Co r
Temp: �:.
Comments.
(Signatur
Date/Time:
eiv �a�y�: gn ure)
�Da,t�T e:
MTJL LAB USE ONLY
Fell (ignature)
Da e/Ti e:
Rece d by/C mpan Signature)
Date/Time:
Acamum:
Trip Blank Received: Y A
M
L,J (
�G('1a..,
4 �'(lV
Template:
HCL MCOH TSP ri
Prelogln:
PM:
(Signature)
Date/Time:
ReceN y7Company: (Signature)
te�me:
Non Confomance(s):
Page
PB:
YES / NO
of:
| ---'--------------~--------------------------------------
LAND APPLICATION OF RESIDUAL SOLIDS
Tanker truck and spreader used (19ft. X 600ft. Approx.) 11,780 gal/acre
or 3.8 loads/acre
DATE
Ph
% solids
Location
Field
Condition
Condition
Gallons
Initials
Rain
6-76
6q
111,q
Aq,
va
claw I
A -VI
-:00
20181
I
PATHOGEN & VECTOR ATTRACTION
REDUCTION FORMS
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boiling Springs WQ Permit Number: W00018352
WWTP Name: Town of Boiling Springs WWTP NPDES Number: NCO071943
Monitoring Period: From 1/1/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ 1
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
I Thetmophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 p
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
F Air Drying❑
Composting ❑
Aerobic Digestion E
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimurr
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
5674
16268
62992
MPN/g
0
7/year
Grab
SM9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
I Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑Alt.
It.4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Gibert / Public Works Director
Preparer Name and Title (type or print)
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)
' r 1
Annual Pathogen and Vector Reduction Summary
Town of Boiling Springs permit # WQ0018352
2018
Fecal Coliform - Class B
There were seven (7) test results provided by Pace Analytical Services in Huntersville.
The calculated Geo Mean for the Fecal Coliform samples was 16268 MPN/g.
Vector Attraction Reduction
Option 4 - Sour test results are reported in the attached data showing seven (7)
test results at 1.18 mg Oxygen/g/hr or less for Specific Oxygen Uptake Rate.
End temperature for each test result was under 30 Degrees Celsius and the percent
solids were under 2% for each result.
. , . j
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Town of Boiling S rim
s,NC
W00018352
26-Se
24.2
26-Se
Terry Price
9/26/18 0615
Todd Humphries
300
1.31
24.2
22.4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.2
1.0
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
4.54 mg Oxygen/hr
1.15 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 1.00 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
102 3 4 5 6 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number
Date,
Digester Temperature.
Sampling Date/Time.
Sampled By.
Analysis Date/Time.
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6f;.1.7
6XFa
Town of Boiling S rin
s,NC
WQ0018352
26-Se
23.9
26-Se
Terry Price
9/26/18 0630
Todd Humphries
300
1.27
23.9
22.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.5
1.0
milliliters
'/o Dry Solids
iegrees Celsius
iegrees Celsius
5.22 mg Oxygen/hr
1.37 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 1.18 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1(D3 4 5 6 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time-
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
of BoilingS rim
s,NC
WQ0018352
26-Se
ETer
24.8
26-Se
Price
9/26/18 0645
Todd Humphries
300
1.34
24.8
23.8
0.1
6.3
1.0
milliliters
%u Dry Solids
Jegrees Celsius
Jegrees Celsius
4.24 mg Oxygen/hr
1.06 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.87 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 24 5 6 7
Circe Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling S
rin s,NC
WO0018352
26-Se
25.5
26-Se
Ter Price
9/26/18 0700
Todd Humphries
300
1.41
25.5
24
0.1
6.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4.93 mg Oxygen/hr
1.17 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.97 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 0 5 6 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
A
Slope:
Intercept:
Correlation Coefficient:
Town of Boilina S rin
s.NC
WO0018352
26-Se
25.5
26-Se
Terry Price
9/26/18 0715
Todd Humphries
300
1.29
275'
23.6
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.4
1.0
'nilliliters
%u Dry Solids
iegrees Celsius
iegrees Celsius
4.46 mg Oxygen/hr
1.15 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.80 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 n 6 7
Circle Tes
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
611M
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boilina S
rim s.NC
WO0018352
26-Se
24.8
26-Se
Terry Price
9/26/18 0730
Todd Humphries
300
1.39
24.8
23.4
0.1
6.4
1.0
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
3.27 mg Oxygen/hr
0.79 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 6Q 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
MYA
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boilinq S
rim s,NC
W00018352
26-Se
25.5
26-Se
Terry Price
9/26/18 0745
Todd Humphries
300
1.37
25.5
23.7
0.1
6.6
1.0
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
4.16 mg Oxygen/hr
1.01 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.79 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 6 0
Circle Test #
._ y
SOIL ANALYSIS REPORT
Page 1 of 1
Report No: 18-061-0733
Account No: 05734 Waypoint.,
ANALYTICAL
Advisor: PACE ANALYTICAL SVCS INC (for Angela Salem) Client: Work Order # 92375055
ANGELA BAIONI PO# AMB17058
9800 KINCEY AVENUE
SUITE 100
HUNTERSVILLE NC 28078
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Farm:
Date Received: 03/02/2018
Date of Report: 03/05/2018
Lab No Field ID
Sample ID
Soil Class
HM%
WN pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
16626
Petty Field JP1
MIN
2.6
6.2
1.0
110
90
10
50
128
128
160
7.9
87
52
28
1.5
0A
16627
Petty Field JP2
M-0
3.7
6.9
0.2
210
228
8
150
450
563
295
13.1
99
61
28
0.9
0.1
16628
Petty Field JP3
M-0
3.6
6.3
1.4
268
187
10
206
523
653
280
13.6
89
55
27
0.7
0.1
Comment:
v
d
m
u,
Test i4�sult units = CEC and Na in meq/100cm3; NO3-N in mg/dm3; WN in g/cm3
North(l.arollna Division of Water Quality Certification #257, Analysis and fertility recommendations shorn on this report are pedonned in accordancewithin NCDA guidelines, Analysis prepared by. Waypoint Analytical Virginia, Inc.
.`
CHAIN -OF -CUSTODY / Analytical Request Document o ,
PdCeIV ldlICdl The Cnaln-ol-Cusloi is a LEGAL DOCUMENT. All relevant fields must be completedcc aurately,
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