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HomeMy WebLinkAboutWQ0018352_Residual Annual Report 2018_20190131js�� s�, lm .. •, "The Crossroads of Opportunity" !19:11,' TOWN OF BOILING SPRINGS January 17, 2019 NCDENR-Division of Water Quality Aquifer Protection section Land Application Unit 1636 Mail Service Center Raleigh, NC 27699-1636 RE: 2018 Annual Land Application of Residuals Town of Boiling Springs Permit# WQ0018352 To Whom It May Concern: RECEIVEDINCDFO'014"JR JAN 3 1 2019 Non-D sch-' Perrni;ung Unit Please find enclosed the original and (2) copies of all applicable forms and test results for The Annual Land Application Report for the Town of Boiling Springs. Aerobic digested residuals continue to be land applied to permitted fields for beneficial reuse as a soil conditioner and fertilizer supplement. Please give me a call if you have any questions or if additional information is needed at (704) 434-2357. Sincerely, i(XW.; Lucas Shires Town Manager Cc: File Enclosures Rl=ri=l\/F[) JAN 31 2019 DWR SECTION INFORMATION PROCESSING UNIT 114 East College Ave I P.O. Box 1014 128017 1 (704) 434-2357 1 www.BoilingSpringsNC.net ANNUAL LAND APPLICATION OF RESIDUALS 2018 ANNUAL REPORT TOWN OF BOILING SPRINGS Permit No. WQ0018352 C. 0- SPR 41 19.1 AA 11 CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit*: W00018352 County: Faci ity Name (as shown on permit): Land Application Operator: Cleveland Year: 2018 Town of Boiling Springs Mike Gibert Phone: 704-434-2357 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Anolication Summarv: Total number of application fields in thepermit: 3 Total number of fields utilized for land application during the yearl 2 Total amount of dry tons applied during the year for all application sites:1 10.51 Total number of acres utilizes for land application during the year: 1 26.2 Part B - Annual Compliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Lucas Shires / Town Manager Permittee Name and Title (type or print) 41 Signature of Permittee — ate Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RESIDUALS SAMPLING FORM ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00018352 Facility Name: Town of Boiling Springs Laboratory: 1) Pace Analytical Services 2) Residual Source WQ # or NCO071943 3) NPDES #: 4) WWTP Name: Town of Boiling Springs WWTP 5) Residual Analvsis Data Parameter Sample or Composite Date Total Phosphorus ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 71,11:� =7 4.a Signature of Preparer * Date DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00018352 Laboratory: 1) Pace Analytical Services Facility Name: Town of Boiling Springs 2) Waypoint Analytical Residual Source NCO071943 3) NPDES # or WQ#: 4) WWTP Name: Town of Boiling Springs WWTP 5) Residual Analysis Data Parameter "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date DENR FORM RSSF - B (12/2006) METALS FIELD LOADING SUMMARY 0 LAND APPLICATION FIELD SUMMARY ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Town of Boiling Springs Land Owner: James Pell Operator: Mike Giber[ Crop 1 Name: pasture PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0018352 Field #: I Acres Utilized: 9.84 Annual Dry Tons Applied: 6.7554 Site*: JPI Acres Permitted: Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 220 Crop 2 Name: Crop 2 Max. PAN: `o o A Volume applied (enter one) Solids/ Liquid 9 Cu. Yds Gallons qo Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDES #, WQ#, Fen.. Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches D K' m 'a S m ii c ° o a ^ m _, N * .°� '� o m m - Q TKN0 mg/kg z a 6 3 R. mg/kg Nitrate and Nitrite mglkg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1-10-18 16000 1.2 0.081 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 5.214 NA pasture 2-23-18 15000 1.2 0.076 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 4.888 NA pasture 2-27-18 15000 1.2 0.076 NCO071943 dry 1 0 S 0.5 0.3 57900 859 1 14500 4.888 NA pasture 3-27-18 6000 1.2 0.031 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 1.955 NA pasture 4-4-18 21000 1.2 0.107 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 6.844 NA pasture 9-13-18 16000 1.2 0.081 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 5.214 NA pasture 10-3-18 12000 1.2 0.061 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 3.911 NA pasture 10-4-18 24000 1.2 0.122 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 7.821 NA pasture 10-5-18 10000 1.2 0.051 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 3.259 NA pasture 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 135000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 43.995 0.000 Lime Applied Annuallbs/acre 0.108 0.011 0.320 0.000 0.054 0.002 0.054 0.054 0.108 1.061 18.110 Date lbs/ac Prior Years Cumulative lbs/ac 0.581 0.074 3.129 0.277 0.378 0.009 0.379 0.384 0.759 9.469 Current Cumulative Ibs/ac 0.689 0.085 3.449 0.277 0.432 0.011 0.433 0.438 0.867 10.530 Permitted C. P. L. R.**** 36 34 1338 n/a 267 15 n/a 74 89 2498 Permit PAN Limit lstl2nd Crop 220 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." q *Application Method: S - Surface, IN - Injection, INC - Incorporation 1 f / **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual): 6.75 Permit #: NCO071943 Cation Exchange Capacity (non 503 only): Operator: Mike Gibert Owner: James Petty Predominant Soil Series: 3acolet-Bethlehem Acres Used: 9.84 Acres Permitted: Site #: 1 Field #: JPl Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 9/26/18 2-J 9/26/18 3 9/26/18 41 9/26/18 51 9/26/18 61 9/26/18 7 9/26/18 8111 9/26/18 9 9/26/18 10 11 12 % Solids 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 Arsenic 78.4 78.4 78.4 78.4 78.4 78.4 78.4 78.4 78.4 Cadmium 7.8 7.8 7.8 7.8 7.8 7.8 7.8 7.8 7.8 Copper 1 233 233 233 233 233 233 233 233 233 Chromium 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 rdenum 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 39.2 78.4 78.4 78.4 78.4 78.4 78.4 78.4 78.4 78.4 773 773 773 773 773 773 773 773 773 Total Phos- horus 13200 13200 13200 13200 13200 13200 13200 13200 13200 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App. y Event 0.08 0.08 0.08 0.03 0.11 0.08 0.06 0.12 0.05 " Arsenic 0.013 0.012 0.012 0.005 0.017 0.013 0.010 0.019 0.008 0.000 0.000 0.000 0.108 Cadmium 0.001 0.001 0.001 0.000 0.002 0.001 0.001 0.002 0.001 0.000 0.000 0.000 0.011 Copper 0.038 0.035 0.035 0.014 0.050 0.038 0.028 0.057 0.024 0.000 0.000 0.000 0.320 Chromiud 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.006 0.006 0.006 0.002 0.008 0.006 0.005 0.010 0.004 0.000 0.000 0.000 0.054 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.006 0.006 0.006 0.002 0.008 0.006 0.005 0.010 0.004 0.000 0.000 0.000 0.054 denum Nickel 0.006 0.006 0.006 0.002 0.008 0.006 0.005 0.010 0.004 0.000 0.000 0.000 0.054 Selenium 0.013 0.012 0.012 0.005 0.017 0.013 0.010 0.019 0.008 0.000 0.000 0.000 0.108 Zinc 0.125 0.117 0.117 0.048 0.165 0.125 0.094 0.189 0.079 0.000 0.000 0.000 1.061 Total Phos- 2.138 2.006 2.006 0.818 2.825 2.138 1.610 3.221 1.346 0.000 0.000 0.000 18.110 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier I -I 7-I � Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Town of Boiling Springs Land Owner: James Petty Operator: Mike Gibert Crop I Name: pasture PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit*: WQ0018352 Field #: 2 Acres Utilized: 16.36 Annual Dry Tons Applied: 3.7530 Site*: JP2 Acres Permitted: Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 220 Crop 2 Name: Crop 2 Max. PAN: c s c m O C] Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume PP Pam' Applied Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (�' Wet, Moist) PrBc1P• past 24 Hrs. inches > m � � 0 m m _. `* d fe o 5' m R m^ �• r _ 8 TKN mgtkg ? S o 3 c -'m• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual 8 Application Crop 1 Crop 2 Crop 1 Crop 2 3-27-18 6000 1.2 0.018 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 1.176 NA pasture 3-28-18 15000 1.2 0.046 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 2.940 NA pasture 3-29-18 9000 1.2 0.028 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 1.764 NA pasture 6-6-18 9000 1.2 0.028 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 1.764 NA pasture 6-15-18 6000 1.2 0.018 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 1.176 NA pasture 8-8-18 30000 1.2 0.092 NCO071943 dry 0 S 0.5 0.3 57900 859 14500 5.880 NA pasture 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 75000 As Cd Cu Cr Pb H Mo Ni Se Zn P 14.701 0.000 Lime A lied Annual lbs/acre 0.036 0.004 0.107 0.000 0.018 0.001 1 0.018 0.018 0.036 0.356 6.072 Date lbs/ac Prior Years Cumulative lbs/ac 0.533 0.069 0.849 0.277 0.355 0.008 0.356 0.361 0.711 8.889 Current Cumulative Ibs/ac 0.569 0.073 0.956 0.277 0.373 0.009 0.374 0.379 0.747 9.245 Permitted C. P. L. R.**** 36 34 1338 n/a 267 15 n/a 374 89 2498 Permit PAN Limit lst/2nd Crop F 220 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation (� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual): 3.76 Permit #: NCO071943 Cation Exchange Capacity (non 503 only): Operator: Mike Gibert Owner: James Petty Predominant Soil Series:'acolet-Bethleherr Acres Used: 16.36 Acres Permitted: Site #: 2 Field #: JP2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or posite Date 1 9/26/18 r9/26/18 9/26/18 9/26/18 9/26/18 6 9/26/18 78 9 10 11 12Com- % Solids 1.2 1.2 1.2 1.2 1.2 1.2 Arsenic 78.4 78.4 78.4 78.4 78.4 78.4 Cadmiuml 7.8 7.8 7.8 1 7.8 7.8 1 7.8 Copper 1 233 233 233 233 233 233 Chromium Lead 39.2 39.2 39.2 39.2 39.2 39.2 Mercury 1.7 1.7 1.7 1.7 1.7 1.7 Molyb- denum 39.2 39.2 39.2 39.2 39.2 39.2 Nickel 39.2 39.2 39.2 39.2 39.2 39.2 Selenium 78.4 78.4 78.4 78.4 78.4 78.4 Zinc 773 773 773 773 773 773 Total Phos- horus 13200 13200 13200 13200 13200 13200 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 1 0.02 2 0.05 3 0.03 4 0.03 5 0.02 6 j 0.09 7 81 91 101 12 _ r Arsenic 0.003 0.007 0.004 0.004 0.003 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Cadmium 0.000 0.001 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.008 0.021 0.013 0.013 0.008 1 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.107 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.001 0.004 0.002 0.002 0.001 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.001 0.004 0.002 0.002 0.001 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Nickel 0.001 0.004 0.002 0.002 0.001 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Selenium 0.003 0.007 0.004 0.004 0.003 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Zinc 0.028 0.071 0.043 0.043 0.028 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.356 Total Phos- horus 0.475 1.214 0.739 0.739 0.475 2.429 0.000 0.000 0.000 0.000 0.000 0.000 6.072 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1-1-I-tq Date DENR FORM MFLSF (12/2006) RESIDUALS ANALYSIS LAB SHEETS ce,4na�ytica�• ANALYTICAL REPORT N•aorrei o)Vi/eaarg smnovxno', October 09, 2018 Pace Analytical - Huntersville, NC Sample Delivery Group: L1029978 Samples Received: 09/28/2018 Project Number: 92400957 Description: Digester Sludge Report To: Angela Baioni 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Entire Report Reviewed By: fltv4u"'�vs/-�i Pam Langford Project Manager „ Resuhs relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be -:� reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pac onal is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304 WNW..o,�., zaceAnalytical e waw.pacelabs. con, ANALYTICAL RESULTS Project: Digester Sludge Pace Project No.: 92400957 Pace Ana"cal Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Digester Sludge Lab ID: 92400957001 Collected: 09126/1806:55 Received: 09/2611808:55 Matdx:Solid Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E Aluminum 13800 mglkg 784 1 09/27/18 10:58 09128/18 05:48 7429-90-5 Arsenic NO mglkg 78.4 1 09/27/18 10:58 09128118 05:48 7440-38-2 Cadmium NO mglkg 7.8 1 09/27/18 10:58 09128/18 05:48 7440-43-9 Copper 233 mg/kg 39.2 1 09/27/18 10:58 09/28/18 05:48 7440-50-8 Lead NO mg/kg 39.2 1 09/27/18 10:58 09/28/18 05:48 7439-92-1 Molybdenum ND mg/kg 39.2 1 09127/1810:58 09/28/18 05:48 7439-98-7 Nickel ND mg/kg 39.2 1 09/27/18 10:58 0928118 05:48 7440-02-0 Potassium ND mg/kg 39200 1 09127/1810:58 09/2811806:48 7440-09-7 Selenium ND mg/kg 78.4 1 09/27/18 10:58 09/28/18 05:48 7782-49-2 Zinc 773 mglkg 78.4 1 09/27/18 10:58 09/28/18 05:48 7440-66-6 7471 Mercury Analytical Method: EPA 7471E Preparation Method: EPA 7471E Mercury 1.7 mg/kg 0.44 1 09/29/1815:49 10101/1811:51 7439-97-6 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 1.2 % 0.000010 1 09/27/18 16:08 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.8 % 0.10 1 0927/18 16:00 9046 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 9.9 Std. Units 0.10 1 0927/18 16:29 Q Plant Available Nitrogen Analytical Method: SM 271OB-2011 Plant Available Nitrogen 32000 mg/kg 0.12 1 10/04/1813:38 N2 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia 859 mg/kg 815 1 10/0111822:48 10/02/1814:10 7664-41-7 J(R1) 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 361.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 57900 mg/kg 2670 1 09/30/18 10:38 09/30/18 19:22 7727-37-9 363.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 14500 mg/kg 841 5 09/28/18 07:55 09/28/18 09:36 Nitrogen, Nitrate 14100 mg/kg 841 5 09128/1807:55 0928/1809:36 14797-55-8 Nitrogen, Nitrite 409 mg/kg 84.1 1 0928/1807:55 0928/1809:26 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA365.1 Rev 2.01993 Preparation Method: EPA365.1 Rev 2.01993 Phosphorus 13200 mg/kg 847 5 0912811815:00 0929/1816:19 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 10/10/2018 08:56 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 27 e DIGCSTER SLUDGE SAMPLE RESULTS — 01 ONE LAB. NATIONWIDE. Collected date/time: 09/26/18 06:55 L1029978 Metals (ICP) by Method 6010D Result Qualifier MDL RDL DiluBon Analysis Analyte mg/kg mg/kg mg/kg mm10.0 date/time Calcium 533 0463 �1 10/05/201810:57 Magnesium 180 0111 10.0 .1 10/05/201810:57 Sodium 49.1 0,985 10.0 .1 10/05/201810:57 Batch LP WG1175645 TC WG1175645 WG1175645 a 5s QCn aQC 7G1 �AI BSc ACCOUNT: PROJECT: SDG: Pace Analytical- Huntersville. NC 92400957 L1029978 ..Page 22 of 27 DATE7TIME: PAGE: 1010911817:01 5 of 10 CHAIN -OF -CUSTODY Analytical Request Document aceAnalytical w Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields LASUSEONLY.AffixWorkordeq[ oginLabelHere orustPace.WorkorderNumberor MTJL Logdn Number Here . ALL SHADED AREAS are for LAB'USfi=ONLY Company: Town of Boiling Springs Billing Information: same Address: PO Box 1014 Boiling Springs NC 28017 Container Preservative Type " Lab Project Manager: Report To: Mike Gibert Email To: mike.gibert@bo]lingspringsnc.net '. Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, (6) methanol, (7)sodium bisulfate, (a) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other Copy To: Todd HUmphries .Rockford Site Collection Info/Address: WWTP 2556 Road Analyses tab Profile/Line: Customer Project Name/Number: State: County/City: Time Zone Collected: NC / Cleveland [ ]PT [ ]MT I ]CT [ x ]ET '' Q) CX O V �_' E U `' Cj C N" Q E C )_CIS ¢ _ O U Z — i'' 3 U _ rn c t31 «t J V tV. 3 . O „ E: ,=.,, C Ct E O 'a O •rn cB O D_ E v U O c- +-• '�,,. , . c` -. _ a C7 fA p )— C () o a- Z ,� �^•• .O � � V t6 U „� .0. , it CO O N C O n -Op : p U) to O N O d- C N p L Z O E a tab Checklist: Sample. Receipt ,, Cust6dy SaaiS Pre rtnt/tatacti. IA Custody Signatures .ilresent NACL Colleatoi .SignaCure Present. _. ti"NA Bottles 'Intact NA' Correct Aottic N NA Sucient,volume N,NA - Samples iteceived an 'Ice Y N A VOA = Headspace Acceptable •.Y N� USDA Regulated Soils N�;::�• Samplr s in 'holding •Time Ll NA Residtial' Chlorine present �Y NA Cl Strips: 'Sample pH Acceptable Y'N N pit 'atrips Sulfide Present x 'N t1A Lead Acetate._Strips: LAB USE ONLY- Lab 'Sample 4 I Comments' 1 0 v t t Phone: 704-434-2357 Email: Site/Facility ID'#: N00071943 Compliance Monitoring? I ] Yes ( ] No Collected By (print): Purchase Order # : Quote#: DW PWS ID #: DWLocationCode: Collected By (signature): Turnaround Date Required: Immediately Packed on Ice: [ ] Yes [ - ] No Sample Disposal: Dispose (] appropriate ( ] Return[ ( ] Archive: ( ]Hold: Rush: ] Same Day ( j Next Day 2 Da 3 Da 4 Da 5 Da ( ] y ( ] y [ ] Y [ ] Y (ExpediieCharges Apply) Field Filtered (if applicable): [ ]Yes [ ) No Analysis; Y ` Matrix Codes (Insert in Matrix box below):' Drinking Water (OW), Ground Water(GW), Wastewater (WW), Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tlssue.(TS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix ` Camp / Grab C011e[ted (Or Composite Start) End Res Res CI # Of Ctns Date Time Date Time Digester Sludge WW Grab 9/26/18 ao Digester Sludge WW Grab 9/26/18 S^'' T X X Digester Sludge WW Grab 9/26/is }Iw 1 X Digester Sludge WW Grab 9/26/18 X X X X Digester Sludge WW Grab 9/26/18 2 X Customer Remarks / Special Conditions Possible Hazards: All results must be in MG/KG except for SAR Type of.Ice Used Wet Blue - Dry: ' None .:.. ,:.. .. SHORT HOLDS PRESENT (<72' hours).: " Y - N/A BpSampin Te p ` tu��nfo. NA Te Blank R era . 18 tell Therm D{ E n Cooler 1 .Temp Upon Receipt C cooler 1 Therm Carr. Factorl. cc Cooler 1 Corrected Temp: i' cc Comments: j Packing.Matertal Used: ttr' .tC,: • � lab Tracking# Radchem sampie(sj screened (<500 cpm): Y N NA Samples recelved'via FEDEX UPS'; r .Client Courier PaceCourler _ . .: R uis ed mpan : (Signature) Date ime: g u si o f ec ' e om y: ignature) Dat /Time: /Y �. MTJLIAB USEONLY ', Table,q:. R m hed y/Comp ny: (Signature) m inr D to e: f � Y Ll Received by/Company: (Signature) % ` � `T, 1 (J �'C•L Date/Time: p j' f G3 I It �,i Acctnum: Template: Prelogin. PM: PS: Trip Blank Received Y A HCL M60H TSP Other 41inquished by/Company: (Signature) O _ N Date/Time: Received by/Company: (Signature) Date/Time: Non Conformance(s): YES J NO Page: of: Analytical Results STATESVILLE ANALYTICAL Pace Analytical 9800 Kincey Suite 100 Huntersville, NC 28078 Receive Date: 09/26/2018 Reported: 09/27/2018 For: Digester Sludge Town of Boiling Springs Comments: Geometric Mean 16,268 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 180926-22-01 Fecal Coliforms 1 17557 MPN/g SM92210E-20o 09/26/2018 WC 180926-22-01 Percent Solids 1 1.31 % SM2540B4011 09/26/2018 WC 180926-22-02 Fecal Coliforms 2 62992 MPN/g SM92210E-2006 09/26/2018 WC 180926-22-02 Percent Solids 2 1.27 % SM2W8-2011 09/26/2018 WC 180926-22-03 Fecal Coliforms 3 17164 MPN/g SM92210E-2006 09/26/2018 WC 180926-22-03 Percent Solids 3 1.34 % SM2WB-2011 09/26/2018 WC 180926-22-04 Fecal Coliforms 4 5674 MPN/g SM92210E-2006 09/26/2018 WC 180926-22-04 Percent Solids 4 1.41 % SM2WB-2011 09/26/2018 WC 180926-22-05 Fecal Coliforms 5 17829 MPN/g SM92210E-2006 09/26/2018 WC 180926-22-05 Percent Solids 5 1.29 % SM2540B-2011 09/26/2018 WC 180926-22-06 Fecal Coliforms 6 9353 MPN/g SM92210E-200B 09/26/2018 WC 180926-22-06 Percent Solids 6 1.39 % SM2WB-2011 09/26/2018 WC 180926-22-07 Fecal Coliforms 7 16788 MPN/g SM92210E-2006 09/26/2018 WC 180926-22-07 Percent Solids 7 1.37 ova SM2WB-2011 09/26/2018 WC Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of Aage 5 of 8 CHAIN -OF -CUSTODY Analytical Request Document LAS USE ONLY -Affix Wwkofd&/login Label Here or Lkt Paca Workorder Number or ceAnalytical e MTJL tog4n Number Here Chalnrof-Custody, is a LEGAL DOCUMENT - Complete all rekvent fields ALL SHADED AREAS are for LAB USE ONLY Company: Town of Boiling Springs Billing Information: same Address: PO Box 1014 Boiling Springs NC 28017 Container Preservative Type" tab Project Manager: ReportTo: Mike Gibert Email To: mike.gibert@boilingspringsnc.net u 1 " Praerva#ve Types: (1) runic acid, (2) svlf..r arid. (31 hydrochloric acid. (a) sodium hydroxaa (5) zinc acetrte (6) methanol, (7) sodium bisulfate, (a) sodium thiosuHate, (9) hexane, (A) ascorbic acid. IBI ammonium sulfate, Copy To: Todd Humphries Site Collection Info/Address: VVWTP 2556 Rockford Road tC) ammonium hydroxide,(0) TSP, ILI Unpresered,(01 Other _ Customer Project Name/Number: State: County/City: Time Zone Collected Analyses lab Pm le/U- Lab Sample Reoeipt Cheeklipt: Custody Seals Present/Intact thy' custody signature. &R� NC / Cleveland I IPT [ IMT I )CT [ x JET Phone: 704-434-2357 Site/FacilitylD #: NC0071943 Compliance Monitoring? Email: [x I Yes I ]No Present y Collector signature Present A Bother, Intact A Collected. y (print): Purchase Order # : DW PWs ID #: Quote# DW Location Code: Correct Settles NA: Sufficient Voluae RNA Samples Received on Ice N Collected By (signature): Turnaround Date Required: Immediately Packed on Ice: ( jYes [ ]No t .� 3 C VOA - Headapace Acceptable Y Ii NA Usm Ragulated Boils % A Sample. in molding Tim. Y NA Sample Disposal: [ J Dispose as appropdate I ]Return push: I I Same Day [ I Next Day Field Filtered lit applicable): ( I Yes f I Na I ) Archive: )Hold; [ ] 2 Da y I ] 3 Day ( 14 Day [ ] S Day � O U Residual Chlarina Present NA Cl Strips: (Expedite ounges Apply) Analysis: N 10 ig U m Sample PH Acceptable Y N tO PH Strips: sulfide Present x R NA 'Matrix Codes ([risen In Matrix box below): Drinking Water (OW), Ground Water(GW), wastewater [WW), Product (P), Soil/Solid (SL], Oil (OL), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), Vapor IV), Other (Or) C mm O O O Lead Acetate Strips: LAB USE ONLY; Comp) Collected (Of Composite End Res # of Customer Sample ID Matrix • Grab Com Composite Start p ) Cl Ctns i C� Lob satmple ; /Comments: Date Time Date Time a- cT C1 2 0 /"1/ / n 1 1 �/� Digester Sludge WW Grab 9/26118 2 X X 001 Digester Sludge WW Grab 9/26/18 r7 2 X X Digester Sludge WW Grab 9/26/18 '.( 2 X X Digester Sludge WW Grab 9/26118 cn 2 X X Digester Sludge WW Grab 9/26/18 U 71 2 X X Digester Sludge WW Grab 9/26/18 Li 2 X X Digester Sludge WW Grab 9/26/18 2 X X Customer Remarks /Special Conditions /Possible Hazards: Type of Ice Used: We SIM Dry None SHORT HOLDS PRESENT (<72 hours) : Y & N/A LAB Sample Temperature Info: Temp Blanc nee iva (itJ Therm IOI: ' Packing Material Used: �/,�] I _ ,.,-� LCJ lab Tracking #: jJ�;IG � Cooler 1 Temp Upon Receipt: Radchem samples) screened (<SDO cpm): Y N NA Samples received via: (�1/l 3s Z Cooler t Therm Corr. 'actO Cooler r Corrected FEDEX UPS Client Louder Pace Co r Temp: �:. Comments. (Signatur Date/Time: eiv �a�y�: gn ure) �Da,t�T e: MTJL LAB USE ONLY Fell (ignature) Da e/Ti e: Rece d by/C mpan Signature) Date/Time: Acamum: Trip Blank Received: Y A M L,J ( �G('1a.., 4 �'(lV Template: HCL MCOH TSP ri Prelogln: PM: (Signature) Date/Time: ReceN y7Company: (Signature) te�me: Non Confomance(s): Page PB: YES / NO of: | ---'--------------~-------------------------------------- LAND APPLICATION OF RESIDUAL SOLIDS Tanker truck and spreader used (19ft. X 600ft. Approx.) 11,780 gal/acre or 3.8 loads/acre DATE Ph % solids Location Field Condition Condition Gallons Initials Rain 6-76 6q 111,q Aq, va claw I A -VI -:00 20181 I PATHOGEN & VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Town of Boiling Springs WQ Permit Number: W00018352 WWTP Name: Town of Boiling Springs WWTP NPDES Number: NCO071943 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ 1 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ I Thetmophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 p Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ F Air Drying❑ Composting ❑ Aerobic Digestion E Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech - ni ue Minimurr Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 5674 16268 62992 MPN/g 0 7/year Grab SM9221 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ I Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. It.4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ JAIt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Gibert / Public Works Director Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ' r 1 Annual Pathogen and Vector Reduction Summary Town of Boiling Springs permit # WQ0018352 2018 Fecal Coliform - Class B There were seven (7) test results provided by Pace Analytical Services in Huntersville. The calculated Geo Mean for the Fecal Coliform samples was 16268 MPN/g. Vector Attraction Reduction Option 4 - Sour test results are reported in the attached data showing seven (7) test results at 1.18 mg Oxygen/g/hr or less for Specific Oxygen Uptake Rate. End temperature for each test result was under 30 Degrees Celsius and the percent solids were under 2% for each result. . , . j Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level Town of Boiling S rim s,NC W00018352 26-Se 24.2 26-Se Terry Price 9/26/18 0615 Todd Humphries 300 1.31 24.2 22.4 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 6.2 1.0 milliliters Yo Dry Solids iegrees Celsius iegrees Celsius 4.54 mg Oxygen/hr 1.15 mg Oxygen/g/hr 23 degrees Celsius 0.863837599 Temperature Corrected Specific Oxygen Uptake Rate: 1.00 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 102 3 4 5 6 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number Date, Digester Temperature. Sampling Date/Time. Sampled By. Analysis Date/Time. Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level 6f;.1.7 6XFa Town of Boiling S rin s,NC WQ0018352 26-Se 23.9 26-Se Terry Price 9/26/18 0630 Todd Humphries 300 1.27 23.9 22.9 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 6.5 1.0 milliliters '/o Dry Solids iegrees Celsius iegrees Celsius 5.22 mg Oxygen/hr 1.37 mg Oxygen/g/hr 23 degrees Celsius 0.863837599 Temperature Corrected Specific Oxygen Uptake Rate: 1.18 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1(D3 4 5 6 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time- Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: of BoilingS rim s,NC WQ0018352 26-Se ETer 24.8 26-Se Price 9/26/18 0645 Todd Humphries 300 1.34 24.8 23.8 0.1 6.3 1.0 milliliters %u Dry Solids Jegrees Celsius Jegrees Celsius 4.24 mg Oxygen/hr 1.06 mg Oxygen/g/hr 24 degrees Celsius 0.822702475 Temperature Corrected Specific Oxygen Uptake Rate: 0.87 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 24 5 6 7 Circe Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boiling S rin s,NC WO0018352 26-Se 25.5 26-Se Ter Price 9/26/18 0700 Todd Humphries 300 1.41 25.5 24 0.1 6.6 1.0 milliliters % Dry Solids degrees Celsius degrees Celsius 4.93 mg Oxygen/hr 1.17 mg Oxygen/g/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 0.97 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 0 5 6 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level A Slope: Intercept: Correlation Coefficient: Town of Boilina S rin s.NC WO0018352 26-Se 25.5 26-Se Terry Price 9/26/18 0715 Todd Humphries 300 1.29 275' 23.6 Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 6.4 1.0 'nilliliters %u Dry Solids iegrees Celsius iegrees Celsius 4.46 mg Oxygen/hr 1.15 mg Oxygen/g/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 0.80 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 n 6 7 Circle Tes Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level 611M Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boilina S rim s.NC WO0018352 26-Se 24.8 26-Se Terry Price 9/26/18 0730 Todd Humphries 300 1.39 24.8 23.4 0.1 6.4 1.0 milliliters Yo Dry Solids iegrees Celsius iegrees Celsius 3.27 mg Oxygen/hr 0.79 mg Oxygen/g/hr 24 degrees Celsius 0.822702475 Temperature Corrected Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 5 6Q 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level MYA Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boilinq S rim s,NC W00018352 26-Se 25.5 26-Se Terry Price 9/26/18 0745 Todd Humphries 300 1.37 25.5 23.7 0.1 6.6 1.0 milliliters Yo Dry Solids iegrees Celsius iegrees Celsius 4.16 mg Oxygen/hr 1.01 mg Oxygen/g/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 0.79 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 5 6 0 Circle Test # ._ y SOIL ANALYSIS REPORT Page 1 of 1 Report No: 18-061-0733 Account No: 05734 Waypoint., ANALYTICAL Advisor: PACE ANALYTICAL SVCS INC (for Angela Salem) Client: Work Order # 92375055 ANGELA BAIONI PO# AMB17058 9800 KINCEY AVENUE SUITE 100 HUNTERSVILLE NC 28078 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Farm: Date Received: 03/02/2018 Date of Report: 03/05/2018 Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K-1 S-1 Mn-I Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N 16626 Petty Field JP1 MIN 2.6 6.2 1.0 110 90 10 50 128 128 160 7.9 87 52 28 1.5 0A 16627 Petty Field JP2 M-0 3.7 6.9 0.2 210 228 8 150 450 563 295 13.1 99 61 28 0.9 0.1 16628 Petty Field JP3 M-0 3.6 6.3 1.4 268 187 10 206 523 653 280 13.6 89 55 27 0.7 0.1 Comment: v d m u, Test i4�sult units = CEC and Na in meq/100cm3; NO3-N in mg/dm3; WN in g/cm3 North(l.arollna Division of Water Quality Certification #257, Analysis and fertility recommendations shorn on this report are pedonned in accordancewithin NCDA guidelines, Analysis prepared by. Waypoint Analytical Virginia, Inc. .` CHAIN -OF -CUSTODY / Analytical Request Document o , PdCeIV ldlICdl The Cnaln-ol-Cusloi is a LEGAL DOCUMENT. All relevant fields must be completedcc aurately, wrx.paceiaez cvm rT m Section A Section B Section C` of ReRuired Client Inlormatien: Required Project Informalion: Invoice Informal": O V n O� i I S Felten To: Attention: //� Q 22.�.�.. {� t 1 1 L lJ Address: Po Cic ! O 1 -t Copy To CompmlY Namo REGULATORY AGENCY AdMass: NPDES F GROUNDWATER DRINKING 11'ATrF (- UST - RCRA ( OTHER EmNi To: �7 No Purchase Order .: po rn Ouse, Referorc. O J 6z;t Prole r`C Y t I • j- u.,Po wom=i Site Location Vim! 441 Requested Due Dab?AT: Foci Number. wapmxnrn STATE: Requested Analysis Filtered (Y/N) Suction D Maniw COMB IZ 0- V "'u"eecMNinromccon MATRIX CODE B COLLECTED Preservatives r Christer, Water DIN um zz W.I., WT Waste eWater rrfi ij ~ L r c SofVSolw SL Y SI.T VNESS" r .OM Z # US SAMPLE ID ape 3 y£ Yam (A-Z. 0.91:) Air AR 0 w S. US a 1�— y Sample IDS MUST BE UNIQUE Tusue TS op IL 2 F p _ . l U u Olhar OT X wTIATE... I� O U m m O cd 14 2` u �%Vic * j $d O cNZ m rot i!j p g U IT Q rr V is MTE TIME m u D _ = = Z Z i O y V vi D: Pace Project No./ Lab I.D. 1 � rig lot % CS IOOP ✓✓ , . � •I 2 e� 'e(d -2, )J- ; 19>30 1 ✓ , / lei P3 -IFs 1 00 1Vil ✓ y ✓ a s 8 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS •dzPAc,, •287`4 % J ORIGINAL SAMPLER NAME AND SIGNATURE u 5i c $ V 2 w Zl PRINT Nama of SAMPLER I'F uu 3NL SIGNATUREoI SAMPLER: DATE SIgrlad lY '11 lC e b +......... .......�••..aw-m..w.,.= mon Pa+nwn emeaw rowwweecnel9es of rsn cer moronraary.noKos�paie.�uln meon. F-ALL-O-020rsv.07,1e-May-2W7