NC0024911_ARO file DWR collected monitoring wells sample results._20190131

DATE SAMPLED
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
OSD
BARIUM
BERYLLIUM
BICARBONATE
CADMIUM-
1 47, vo-)�7
CALCIUM
--
CARBONATE
CHLORIDE
CHROMIUM, TOTAL
COBALT
COD
COLIFOP-q, FECAL
COLIFORM, TOTAL
COPPER
CYANIDE
DISSOLVED SOLIDS
FLUORIDE
HARDNESS CaCo,,----
HARDNESS, NON -CARBONATE
IRON
LEAD
LITHIUM
Red Ink = Sample taken by
4 0. 010
o.oqg
.4 0- 0 0
cx O'L5
,4
0. C-,>O'f Of o
facility
co
z 0. 0�-o
o'
o. oo�-7
0. ol-i 3
0, 00 c
LINTY

M 97-0
COUNTY 19(,41V C &1-16
DATE SAMPLED
MBAS
MAGNESIUM
MANGANESE
MERCURY
NICKEL
-
NITROGEN , AMMONIA
03
NITROGEN, KJELDAHL
NITRATE & NITRITE
c
0.6
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS, TOTAL
o.073
POTASSIUM
SELENIUM
0.
4 0.06-0
SILVER
D, 00.5-
z 0. oo-o
SODIUM
SPECIFIC CONDUCTANCE
SULFATE
TOC (UNFILTERED)
TON.
T S S
VOC
ZINC
STATIC WATER LEVEL

COUNTY ,9 "IV C�,O --113L-
DATE SAMPLED
4-
4
`r',' 8- 9
ALKALINITY, TO pIi 4.5
ALI:ALINITY, TO pII 8.3
ALUMINUM
ARSENIC
40 0S'O
4 0. -050
` d • Oil 6
4 C%• 0iG>
[ O> OT C?
0, 0-:5-0
BARIUM
Cle
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Cid �%La"�
(,�, /�
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BERYLLIUM
BICARBONATE
CADMIUM,.
O&JI
.e C) • 003 !
4 O. Oe):5Y%
C 0. OaA
C O- c ct i
t 0. o0. %
CALCIUM
CARBONATE
CHLORIDE
—
CHROMIUM. TOTAL
0. 0 4 &
C O. 0496
G 0,00 ( 6
C U. 0 C)
COBALT
COD
_.
COLIFOP-M, FECAL
!"
COLIFORM, TOTAL
G I I
I. _
d• %
% <, %
/- !
�' /l
COPPER
CYANIDE
DISSOLVED SOLIDS��
FLUORIDE
HARDNESS CaCo,
HARDNESS, NON -CARBONATE
_
IRON
LEAD
d
t U•©3.�
C1. 03�,
G A,, ®!Li
� ®. �r3�
� lie c�O�C►
LITHIUM
Red Ink = Sample taken by facility

COUNTY /9 " /i" C G%M & l5"
DATE SAMPLED
rY'i �'
- .2 - 9 ff
F .._ t� ' Gp
_ Y �1 �}
�✓ �? 1 L%`_i�
MBAS
i
MAGNESIUM
-- -
MANGANESE
MERCURY
-
NICI7EL
-
- -
NITROGEN, AMMONIA
0
4 0. 0 30
o, 03
k
� � c� �' ``�
< 0, 030
NITROGEN, I:JELDAHL
NITRATE & NITRITE
lV03
/JO,3
v3
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS, TOTAL
POTASSIUM
SELENIUM
4 0. C)So
4 0, 0.! �
� CI F ®� ®
4 C�. ®Pg
L 0- C7 !� !?
4 fyF C> � �1
SILVER
<®,00l ?
G U, 0.0&7
L 0, 0030
� O'0025-
i 0,cooC�
SODIUM
SPECIFIC CONDUCTANCE
SULFATE
TOC ( UNFILTERED)
J
TO k
Tss
S o o
956)
s �
� 7�
� -� c>
r °f �
VOC
/V 0
A/rr
ZINC
STATIC WATER LEVEL
7° 7
C,
J��M/'f-C-5 Di-s C_-1 CA A ,C-reaRE✓ 4A1"+LysEs

M vv_
Al NO. / '% Q / cj -6
COUNTY ,�UAIC O",a L
DATE SAMPLED
D q
3v,. y Z
L!" 3 6 - �.
v� - �'f` `�
� .30 `" h7..3
C O. O /O
©. /-O
ALIALINITY, TO pH 4.5
ALKALINITY, TO .pH 8.3
ALUMINUM
0 ° 0 s
ARSENIC
c. r Q
G. O. 0O.S1
Oe 00 /'7
Oa 00/ 7
O. O.ri O
BARIUM
0. Cd'f'
fj. /l
0.O
0,(,-6-
0.13
BERYLLIUM
BICARBONATE
CADMICI*i
C.� L�GI
C) ° f /
CJ � !
O. Ou' /t
'4 0- 0031
r 0. 00.2
CALCIUM
CARBONATE
CHLORIDE.`
CHROMIUM. TOTAL
4. 0,23
Z. � ClOS�
� t�. �a�?��
0, �L S
(,a, i�t�y�
G U• l?�5
COBALT
COD
COLIFOPM, FECAL
/A i
COLIFORM, TOTAL
3000
0-0
COPPER
4 0, 00
CYANIDE
DISSOLVED SOLIDS
®Z & 4)
% 0
70
o
FLUORIDE
HARDNESS CaCo,
HARDNESS, NON -CARBONATE
IRON
y
LEAD
t 0 ° 0 / 0
G CJ. SOS
O. 00,2
Or 0,2
C% ® 0.. A
. 4- 0. 0 / O
LITHIUM
Red Ink = Sample taken by facility
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-M 97 1
uoU`NTY 0/14
DATE SAMPLED
jb
-7-- -,
-2 -,
6, -- 3,0 "VY
MBAS
MAGNESIUM
"T
MANGANESE
MERCURY7G13.00
0,2,2
40.000.4A
0 OOA
NICK EL
NITROGEN. AMMONIA
0 cl
Cl
o"I $—
0. 0.7,7
c'.
NITROGEN, KJELDAHL
NITRATE & NITRITE
00,3
JV03
ORGANIC SCAN
pH
PHENOLS
PHOSPHORUS, TOTAL
c. 03
POTASSIUM
SELENIUM
0 6-15
0 •l>os-
0. 0 -Z 1
A I
4 C), C) 50
0. L) 0.S;
SILVER
r?,o
0, o06
SODIUM•
SPECIFIC CONDUCTANCE
SULFATE
TOC (UNFILTERED)
TOX
TSS
3
VOC
ZINC
STATIC WATER LEVEL
'7 -7

A N0.
S'7 j .5 COUNTY 6" A)C e� M i3
DATE SAMPLED
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r7930 L '',Engineering
NDtl-2t—'93 TUE 13:23 iD:PFCE ING
Law ;Engineering
4 Interchangg Blvd,
areenv1114, SC 29607
Attu: ter. Robert MacPhee
Cl lent Reference: Total Col iform MpN
PACE Sample Number•
F-767 T- i P003
TEL NO:252 4618
NOV 29 195 10:12
P02
October of $ 1!001
PACE ProJact Mumborc l90ftS
Vitt Colldctgd:
03 a"' ZZ
93 0131530
93 013154,
Oetr Received:
09/26/95
09/25}95
09/25/93
Went, Sample I4:
Lira meter
09/26/916
!' w-I
99/25/25
09/15108
Units MbL
MM_2R
I"DRGANIC ANALYSIS
"..".._—.-,
......�..«�.......
..
INTIVIDUAL PARAMETERS
Bacteria, Total C011forh col/100ml I
IZ MPM
>23 MPK
<l.l MPR
These data have been rOviewed and are approved for release.
Sherry 1. Ratt1 ri
Supervisor, Biaessay Department
NOV 2 91995"
GROl1NU' LATER 70TC [10N
ASHEVILLE REGIONAL OFFICE
34 PAWOM* Dive

_377938 ' `1 Engineering
NM-21 95 7UI= 13:23 ,ID: PACE I14C.
F-767 T 9 P-004 NOV 29 195 10:13
TEL ND-252 461B 14926 P03
REPORT OF LABORATORY ANALYGM
Mr. Robert MacPhee FOOTNOTES
Page F for page 1
Client Reference: tottl Coli form WPN
L■:s than reported value.
GreaCer than reported value.
MOL Method Deteettah Limit
October OF, 1999
PACE Project Humber; A60925E20
SR P&Nfwd onw A��E
MMIN to no
sec,: sue
f 7a-9eIf

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
10/06/95
.ge 1
--- Project Information ---
Lab Number : 95-2544-03
Project No. : 30290-5-4492-12 Cust. No. :
Project Name : MSD - TRI ANNUAL SAMPLING
Manager: ROBERT MACPHEE
Station ID : MW-2R
Matrix : W
Type : GRAB
Collector : RM
--- Sample Information ---
Sampled Date/Time
: 09/25/95 13:00
Received Date/Time
: 09/26/95 16:03
Received From/By
: RM/CE
Chain of Custody
: 32771
Number of Containers
: 8
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/l
1.0
6.8
10/02/95
JS
Chloride
EPA
325.3
mg/l
1.0
26
10/03/95
JR
Nitrogen, Ammonia
EPA
350.1
mg/1
0.030
ND
09/29/95
DF
Nitrogen, Nitrate
EPA
353.2
mg/l
0.050
0.60
09/28/95
JS
Residue, Filterable (TDS)
EPA
160.1
mg/l
10
570
09/27/95
RH
Residue, Non Filterable (TSS)
EPA
160.2
mg/l
10
300
09/28/95
RH
-- METALS ANALYSIS - METALS PREP RESULTS --
Mercury, Total EPA 7470A mg/l
-- METALS PREP RESULTS --
T. Metals Prep: Aqueous, Hg EPA 7470A
Metals Prep: Acid Extracted (ICP) SM 3030C
Metals Prep: Acid Extracted (Furnace) SM 3030C
0.00015 ND 10/03/95 ER
N/A 10/02/95 ER
EXTRACTED 09/27/95 CW
EXTRACTED 09/27/95 CW
--- SERIES 39000
Arsenic, Extractable
EPA
6010A
mg/l
0.050
ND
09/28/95
ASH
Barium, Extractable
EPA
6010A
mg/l
0.019
0.29
09/28/95
ASH
Cadmium, Extractable
EPA
6010A
mg/l
0.0057
ND
09/28/95
ASH
Chromium, Extractable
EPA
6010A
mg/l
0.0066
0.023
09/28/95
ASH
Lead, Extractable
EPA
7421
mg/l
0.0040
0.0066
09/29/95
SDE
Selenium, Extractable
EPA
6010A
mg/l
0.050
ND
09/28/95
ASH
Silver, Extractable
EPA
6010A
mg/l
0.0050
ND
09/28/95
ASH
--- SERIES 88000
Dichlorodifluoromethane
EPA
502.2
ug/l
3.2
ND
09/29/95
VZ
Chloromethane
EPA
502.2
ug/l
0.90
ND
09/29/95
VZ
Vinyl chloride
EPA
502.2
ug/l
1.9
ND
09/29/95
VZ
Bromomethane
EPA
502.2
ug/1
0.80
ND
09/29/95
VZ
Chloroethane
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
Trichlorofluoromethane
EPA
502.2
ug/1
1.8
ND
09/29/95
VZ
Remarks:
DL = Detection Limit
ND
= Not Detected at the
DL
Unless otherwise noted,
all soil test results
are calculated based
on dry weight.
G
Signed

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
10/06/95
.ge 2
Lab Number 95-2544-03
Project No. 30290-5-4492-12
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
--- SERIES 88000
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
cis-1,3-Dichloropropene
Toluene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Dibromochloromethane
1,2-Dibromoethane
Ethylbenzene
1,1,1,2-Tetrachloroethane
Xylene, Total
Styrene
Isopropylbenzene
Bromoform
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
n-Propylbenzene
Bromobenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
sec-Butylbenzene
p-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
EPA
502.2
ug/1
0.83
ND
09/29/95
VZ
EPA
502.2
ug/l
0.62
ND
09/29/95
VZ
EPA
502.2
ug/l
0.92
ND
09/29/95
VZ
EPA
502.2
ug/l
0.63
ND
09/29/95
VZ_
EPA
502.2
ug/1
0.84
ND
09/29/95
VZ
EPA
502.2
ug/1
0.79
ND
09/29/95
VZ
EPA
502.2
ug/l
0.42
ND
09/29/95
VZ
EPA
502.2
ug/l
0.56
ND
09/29/95
VZ
EPA
502.2
ug/1
0.88
ND
09/29/95
VZ
EPA
502.2
ug/1
1.2
ND
09/29/95
VZ
EPA
502.2
ug/l
0.87
ND
09/29/95
VZ
EPA
502.2
ug/l
0.65
ND
09/29/95
VZ
EPA
502.2
ug/1
0.90
ND
09/29/95
VZ
EPA
502.2
ug/l
0.70
ND
09/29/95
VZ
EPA
502.2
ug/l
0.56
ND
09/29/95
VZ
EPA
502.2
ug/1
0.72
ND
09/29/95
VZ
EPA
502.2
ug/l
0.80
ND
09/29/95
VZ
EPA
502.2
ug/l
0.90
ND
09/29/95
VZ
EPA
502.2
ug/l
0.82
ND
09/29/95
VZ
EPA
502.2
ug/l
0.73
ND
09/29/95
VZ
EPA
502.2
ug/1
2.0
ND
09/29/95
VZ
EPA
502.2
ug/l
0.68
ND
09/29/95
VZ
EPA
502.2
ug/l
0.41
ND
09/29/95
VZ
EPA
502.2
ug/1
0.77
ND
09/29/95
VZ
EPA
502.2
ug/1
0.92
ND
09/29/95
VZ
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
EPA
502.2
ug/l
0.47
ND
09/29/95
VZ
EPA
502.2
ug/l
0.86
ND
09/29/95
VZ
EPA
502.2
ug/l
0.79
ND
09/29/95
VZ
EPA
502.2
ug/l
1.9
ND
09/29/95
VZ
EPA
502.2
ug/1
1.9
ND
09/29/95
VZ
EPA
502.2
ug/l
2.0
ND
09/29/95
VZ
EPA
502.2
ug/l
2.0
ND
09/29/95
VZ
EPA
502.2
ug/l
0.80
ND
09/29/95
VZ
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
EPA
502.2
ug/l
1.1
ND
09/29/95
VZ
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
EPA
502.2
ug/l
0.58
ND
09/29/95
VZ
EPA
502.2
ug/l
1.1
ND
09/29/95
VZ
EPA
502.2
ug/1
1.2
ND
09/29/95
VZ
EPA
502.2
ug/1
1.1
ND
09/29/
VZ
Signed
C

LAW ENVIRONMENTAL NATIONAL
LABORATORIES
TEST DATA
REPORT
10/06/95
.ge 3
Lab Number : 95-2544-03
Project No. : 30290-5-4492-12
Parameter ..............................
Method....
Units
DL........ Results...
Test Date Analy
--- SERIES 88000
1,2,3-Trichlorobenzene
EPA 502.2
ug/l
1.1 ND
09/29/95 VZ_
1,2,4-Trimethylbenzene
EPA 502.2
ug/l
1.5 ND
09/29/95 VZ
Signed

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
10/06/95
.ge 1
--- Project Information ---
Lab Number : 95-2544-04
Project No. : 30290-5-4492-12 Cust. No.
Project Name : MSD - TRI ANNUAL SAMPLING
Manager: ROBERT MACPHEE
--- Sample Information ---
Station ID : TRIP BLANK Sampled Date/Time : 09/12/95
Matrix : W Received Date/Time : 09/26/95 16:03
Type : GRAB Received From/By : RM/CE
Collector : Chain of Custody : 32771
Number of Containers : 2
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
--- SERIES 88000
Dichlorodifluoromethane
EPA
502.2
ug/l
3.2
ND
09/29/95
VZ
Chloromethane
EPA
502.2
ug/1
0.90
ND
09/29/95
VZ
Vinyl chloride
EPA
502.2
ug/l
1.9
ND
09/29/95
VZ
Bromomethane
EPA
502.2
ug/1
0.80
ND
09/29/95
VZ
Chloroethane
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
Trichlorofluoromethane
EPA
502.2
ug/1
1.8
ND
09/29/95
VZ
1,1-Dichloroethene
EPA
502.2
ug/l
0.83
ND
09/29/95
VZ
Methylene chloride
EPA
502.2
ug/l
0.62
ND
09/29/95
VZ
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.92
ND
09/29/95
VZ
1,1-Dichloroethane
EPA
502.2
ug/l
0.63
ND
09/29/95
VZ
cis-1,2-Dichloroethene
EPA
502.2
ug/1
0.84
ND
09/29/95
VZ
Chloroform
EPA
502.2
ug/l
0.79
ND
09/29/95
VZ
Bromochloromethane
EPA
502.2
ug/1
0.42
ND
09/29/95
VZ
1,1,1-Trichloroethane
EPA
502.2
ug/l
0.56
ND
09/29/95
VZ
1,1-Dichloropropene
EPA
502.2
ug/1
0.88
ND
09/29/95
VZ
Carbon tetrachloride
EPA
502.2
ug/1
1.2
ND
09/29/95
VZ
Benzene
EPA
502.2
ug/1
0.87
ND
09/29/95
VZ
1,2-Dichloroethane
EPA
502.2
ug/1
0.65
ND
09/29/95
VZ
Trichloroethene
EPA
502.2
ug/1
0.90
ND
09/29/95
VZ
1,2-Dichloropropane
EPA
502.2
ug/l
0.70
ND
09/29/95
VZ
Bromodichloromethane
EPA
502.2
ug/l
0.56
ND
09/29/95
VZ
Dibromomethane
EPA
502.2
ug/1
0.72
ND
09/29/95
VZ
cis-1,3-Dichloropropene
EPA
502.2
ug/1
0.80
ND
09/29/95
VZ
Toluene
EPA
502.2
ug/l
0.90
ND
09/29/95
VZ
trans-1,3-Dichloropropene
EPA
502.2
ug/l
0.82
ND
09/29/95
VZ
1,1,2-Trichloroethane
EPA
502.2
ug/1
0.73
ND
09/29/95
VZ
Tetrachloroethene
EPA
502.2
ug/l
2.0
ND
09/29/95
VZ
1,3-Dichloropropane
EPA
502.2
ug/1
0.68
ND
09/29/95
VZ
Dibromochloromethane
EPA
502.2
ug/1
0.41
ND
09/29/95
VZ
1,2-Dibromoethane
EPA
502.2
ug/1
0.77
ND
09/29/95
VZ
Ethylbenzene
EPA
502.2
ug/l
0.92
ND
09/29/95
VZ
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry weig
Signed ��

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
10/06/95
.3e 2
Lab Number 95-2544-04
Project No. 30290-5-4492-12
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
--- SERIES 88000
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
Xylene, Total
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ*
Styrene
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
Isopropylbenzene
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ.
Bromoform
EPA
502.2
ug/l
0.47
ND
09/29/95
VZ
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/l
0.86
ND
09/29/95
VZ
1,2,3-Trichloropropane
EPA
502.2
ug/l
0.79
ND
09/29/95
VZ
n-Propylbenzene
EPA
502.2
ug/1
1.9
ND
09/29/95
VZ
Bromobenzene
EPA
502.2
ug/1
1.9
ND
09/29/95
VZ
1,3,5-Trimethylbenzene
EPA
502.2
ug/1
2.0
ND
09/29/95
VZ
2-Chlorotoluene
EPA
502.2
ug/l
2.0
ND
09/29/95
VZ
4-Chlorotoluene
EPA
502.2
ug/l
0.80
ND
09/29/95
VZ
tert-Butylbenzene
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
sec-Butylbenzene
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
p-Isopropyltoluene
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
1,3-Dichlorobenzene
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
1,4-Dichlorobenzene
EPA
502.2
ug/l
1.0
ND
09/29/95
VZ
n-Butylbenzene
EPA
502.2
ug/l
1.1
ND
09/29/95
VZ
1,2-Dichlorobenzene
EPA
502.2
ug/1
1.0
ND
09/29/95
VZ
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/l
0.58
ND
09/29/95
VZ
1,2,4-Trichlorobenzene
EPA
502.2
ug/l
1.1
ND
09/29/95
VZ
Hexachlorobutadiene
EPA
502.2
ug/l
1.2
ND
09/29/95
VZ
Naphthalene
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
1.1
ND
09/29/95
VZ
1,2,4-Trimethylbenzene
EPA
502.2
ug/l
1.5
ND
09/29/95
VZ
Signed �/`y%c��-z

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GROUNDWATER FIELD/LAB FORM
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT- GROUNDWATER SECTION
County L? a E Lab Number
Quad No M 97J s Serial No. 3 O a 7 SAMPLE PRIORITY Date Received 9 ZS ' q-5- Time r0
Lat. 35' 3 8 �'S Long. $1 3S 1-/-3 Rec'd by: G�1� From: Bus, Courier and De ,
ROUTINE EMERGENCY MwI -.2 R Other:
Report To: ARO FRO, MRO, RRO, WaRO, WiRO, ❑CHAIN OF CUSTODY Data Entry By: 5 Ck:�-
WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: /n —
Shipped by: Bus, Courier, and De , Other-- Purpose:
M�NN�CK
Collector(s): R u.y [3�uc /� Date 9 ".2 S - 17S Time �a % � S PM Baseline, Complaint, om lianc LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner MG i c Po z
nH400 Spec. Cond.94 at 250 C Location or site
1p.t0 oC Odor Description of sampling oint
Appearance Sampling Method 8,4 / L E Sample Interval 7, O 7. O
ump, batler eic
Field Analysis By: Remarks S? 4 7i c �+/fl? L E�'� L %, `'f
(pumpS� L / —F .5 M /-� L C.5 VV / ? , -1 rnq /V` �a ! /� f'►'cte- / ,.j
LABORATORY ANALYSES
BOD 310 mg/I
COD High 340 mg/I
COD Low 335 mg/I
Coliform: W Fecal 3 6<I,/ /100ml
Coliform: ME Total 8 d /100ml
TOC 680 m /I
Turbidity 76 NTU
Residue., Suspended 530 41 p mg/I
pH 403 unit
Alkalinity to pH 4.5 410 mg/I
Alkalinity to pH 8.3 415 mg/I
Carbonate 445 mg/I
Bicarbonate 440 m /I
Carbon dioxide 405 mg/I
D $
Chloride 940 a S mg/I
Chromium: Hex 1032 ug/l
Color: True eo Pt -Co
Cyanide 720 MCA
01 S
Diss. Solids 70300 j5 m /1
A - Silver 46566 u I
Flouride 951 maA
Al - Aluminum 46557 u /I
Hardness: Total 900 mcvl
As - Arsenic 46551 u I
Hardness non-carb 902 m I
Ba - Barium 46558. u /I
Phenols 32730 u /I
Ca - Calcium 46552 m /I
S ecific Cond. 95 uMhos/cm2
Cd - Cadmium 46559 u /l
Sulfate 945 m I
Cr - Chromium 46560 u /1
Sulfide 745 m
Cu - Copper 46562 ugA
Fe - Iron 46563 u /1
Hg - Mercury 71900 ua/I
K - Potassium 46555 mg/I
M - Magnesium 46554 ma/I
Mn - Manganese 46565 u I
NH as N 610 moll
Na - Sodium 46556 m /I
Ni - Nickel u /I
NO + NO as N 630 moll
Pb - Lead 46564 u /I
P: Total as P 665 m I
Se - Selenium u /I
Zn - Zinc 46567 _..._ - ---u 1
Comments: j C,4�e r'l E rU .. b
AAPN
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
Semivolatile Organics
Volatile Organics (VOA bottle)
TPH - Gasoline Range
TPH - BTEX Gasoline Ranqe
-193 For Dissolved Analysis - submit filtered sample and write "DIS" in block.

Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Metropolitan Sewerage District Non -Discharge
Address 2225 Riverside Drive NPDES NMn?4911
Asheville, North Carolina County Buncombe IYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Well Location Downgradient of Ash/Sludge Storage lagoon x Lagoon SepticTank/Drain Field
Well Identification Number M87015 M-211) Well Depth 17 Ft. Spray Field Subsurface Low -Pressure
Well Diameter 2.0" Sample (Screened) Interval 7 Ft. To —17 Ft. Piping (LPP)
Depth to Water Level 6.8 ft. below measuring point (before sampling) Land Application of sludge
Measuring point is 0.0 ft. above land surface Other
'allons of water pumped/bailed before sampling 6 gallons Rotary Distributor
yield Analysis: pH 6 Specific Conductance 755 uMhos Temp. 17 °C Odor NA Appearance clear
Date Sample Collected June 27, 1995 Date Lab Sample Analyzed .tune 27 through JW vv 14, 1995
Laboratory Name Law Environmental Inc and Pace Inc Certification No. 287, 37712
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED ___A_YES NO
COD
mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel
s"
'. mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N 2.4
g/I
Pb - Lead 0.0048
mg/I
Coliform: MF Total 1.1 MPN
/100ml
Phosphorus: Total as P
4/1
Zn - Zinc
(Note: Use MPN method for highly turbid samples)
Al - Aluminum
mg/I
Pesticides/Herbicides
'
Dissolved Solids: Total 680
mg/I
Ba - Barium 0.040
mg/I
(Specify Compounds)
pH (when analyzed)
units
Ca - Calcium
mg/I
T=; ug/I
TOC 4.8
mg/I
Cd - Cadmium <0.0057
mg/I
: ug/I
Chloride 30
mg/I
Chromium: Total <0.0066
mg/I
,°-
> ug/l
Arsenic <0.050
mg/I
Cu - Copper
mg/I
Other (Specify Compounds and
"irease and Oils
mg/l
Fe - Iron
mg/I
Concentration units)
a iardness: Total
mg/I
Hg - Mercury <0.00015
mg/I
Total Suspended Solids = <10
mg/i
Phenol
mg/1
K - Potassium
mg/I
Selenium = <0.050 mg/l
Sulfate
mg/I
Mg - Magnesium
mg/I
Silver = <0.0050 mg/l
Specific Conductance
uMhos
Mn - Manganese
mg/I
Total Ammonia <0.053
mg/I
Na - Sodium
mg/I
TKN as N
mg/I
Results attached
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
3 �
of Permittee (or Authorized Agent*) Date
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on hack)
* See back for instructions.
** Submit blue, green, and yellow copies only to address above.
,/93

1 Sampbs PDX tie jislyied as SM-,o pozssibi-SiAiNAIPLES I Hih'-,Ii ARE t-,i�OTA,,-,,.ALYSEDW;-45411�tTF:,E
F11HCl FOIF-I EE FAEFTHEa. USED (SEE U4. ?JST BE EMSCAR08 A;-D zIEW MAIM LE C, n' c-TE17;_
n NRANs AnaysnE Oe fiur pr p2faZiiun I-I'E'R INFI
WARwen samp.ew, for th.3,n field acidifiek r1it8 ic;ai,-,i4€5,--,r iibw ol san-ple,, aindsinc-nuidbe -suNrnilujedto Cie
into WTV; 2ANiurs-
a"rini.rfli" in i&cii,'-,m,,,a,,ry ir�� thiun 72 hours cit collection.
i-inn) MU�s-1, i:�e -n-I pea-u-J, �tA
AN144J,-"Y P-11E K ULVE, -3 WELL AS COLLOMIA THE ;
M
-,H ,,"VATIE"P, I&I Tki-Q�Wgj 11joll ATf k PABIT fIF "J!"IAGIT ASSiD", TH - I ELL
-CaATE D —
CT 14 E 11 K W 1 T 14 IF (3�J R EL 0 R-1 A-�- 0 F! Y 0 1 P 0, E DO ',r
f IFFLE 4 -,LL A RESER fA TN
As 0e; 7,,lc, I '111"'Ik-ir"U'l Codt:', SubtNapieNAL, no jr 4 C
nbef i
Ow Ounw!"; cmr'by c-ii"he''r me,,,n- -d",., appin-oved by -Nnt� En-vin-aim-m-itai
fo,, ExashinaVan of Wei- -ano -,0L--'as--",t--,wa-,.Ed.tior,., and 151.h Editt,37, ISI-33_ PW-,,JNs;hC-c-,i itm-lx'-rojhv
An Arrie,;,,rar--, -0 atez r'---:;souadon and %. ater
sflor i'-hamica! Analysis,,of V, are- Eund Wass, 1975, Environmri, Mal Pr.otac.tfic,----r-, Agency
FPA-60C3i'A- 79-02C), as revisod fvIach 1983;
(,"c') --�'es, ih,.,I,thoJ.s for Evalua�ing, Solid Wastes: "Aie.,tho s-- 3rd Ed.iflon, 1986, 21-11.8, lEnvironme. PLiotct;on P,,-enci
pui.Ace,tion niurnber , W846:
,d) TsislPc refor theArayLcAF%fluaf U1ieWhFedera!RgserVoLNo20940 CFRP-9. . 4 ,(,:ts f,lss is neClean aer at
October 26, 1984;
�-nd reawd dlept-in of vvater in tlhie well prior to pumping -or bailing any water from thewell
At least :1 volurnes of water in the well sh�cjuld b;�.-, parnped or Wed prior to co�fecvng a sarnoe for analysis. If thewe'll is pumpediba-fled d'iy before 3 WII']IH"--
4
cc
voi,amez are removed, samp& can bc c-oliected as scon as Me W! recovers U-, thee r int whare enough water is available t flec! your,,,sarnple,
7, .Dete� rninalJon for plH, Specific Conductance-, Iternperallure, ador and appearance must be made in the field on 'unfiltered -I samples when the sample is
coNactad,
a�'ed kn wcordance, with recornmendations by V-1a manufacturer.
Fold ouit.0pinent be calib.
0 Saa4wes rm,,st be filtered uhroulli a 0.45 rnicron filter irr.-rneediat-ely after colleovor, vvhien adissolved analysis is requiram, d. (See #4, atve)
The s container should be labeled a", the tir- c '01, collactic-'n 'vvth i& fadilivy niat 9- _vvefl ideniffication numbear and date and time coliectef.-J.
h o, ri z e�rj, ag a n'U' j s any cc rpo add oR to r o r Fw bI & click i au V ii-c- riz ed b--, the ic-,c r zn pany . co rporatic n , a r gover n m en tal bod y to sign, off ici, ai dc-u u- --m.,,e r

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
a 07/25/95
age 1
Lab Number : 95-1942-01
Project No. : 2490449211
Project Name : MSD
Manager: ROBERT MACPHEE
Station ID : MW-2R
Matrix : W
Type : GRAB
Collector : JA
--- Project Information ---
Cust. No. .
--- Sample Information ---
Sampled Date/Time
: 06/27/95 12:30
Received Date/Time
: 06/28/95 10:00
Received From/By :
JA/JA
Chain of Custody :
32042
Number of Containers :
5
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
Chloride
Nitrogen, Ammonia
Nitrogen, Nitrate
Residue, Filterable (TDS)
Residue, Non Filterable (TSS)
EPA
415.1
mg/1
1.0
4.8
07/11/95
JAS
EPA
325.3
mg/l
1.0
30
07/08/95
RJO
EPA
350.1
mg/l
0.030
0.053
06/29/95
KAA
EPA
353.2
mg/l
0.050
2.4
07/06/95
DF
EPA
160.1
mg/l
10
680
07/10/95
DF
EPA
160.2
mg/l
10
ND
07/06/95
RH
-- METALS ANALYSIS - METALS PREP RESULTS
Mercury, Total EPA 7470
-- METALS PREP RESULTS --
T. Metals Prep: Aqueous, Hg EPA 7470
Metals Prep: Acid Extracted (ICP) SM 3030C
Metals Prep: Acid Extracted (Furnace) SM 3030C
--- SERIES 39000
Arsenic, Extractable
Barium, Extractable
Cadmium, Extractable
Chromium, Extractable
Lead, Extractable
Selenium, Extractable
Silver, Extractable
mg/l 0.00015 ND 07/10/95 ER
N/A 07/10/95 ER
EXTRACTED 06/29/95 ER
EXTRACTED 06/29/95 ER
EPA
6010
mg/1
0.050
ND
06/30/95
ASH
EPA
6010
mg/1
0.019
0.040
06/30/95
ASH
EPA
6010
mg/1
0.0057
ND
06/30/95
ASH
EPA
6010
mg/l
0.0066
ND
06/30/95
ASH
EPA
7421
mg/l
0.0040
0.0048
06/30/95
SDE
EPA
6010
mg/l
0.050
ND
06/30/95
ASH
EPA
6010
mg/l
0.0050
ND
06/30/95
ASH
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry weight.
Signed

i N c o R P I R A T E o° REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF QUALITY
Law Engineering
4 Interchange Blvd.
Greenville, SC 29607
Attn: Mr. Robert MacPhee
Client Reference: MSD/2490449211
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
Units
MDL
July 06, 1995
PACE Project Number: A5062750`
93 0099335 93 0099343 93 0099351
06/27/95 06/27/95 06/27/95
06/27/95 06/27/95 06/27/95
MW-2R MW-1 MW-3
INDIVIDUAL PARAMETERS
Bacteria, Total Coliform c01/100ml 1 1.1 MPN >23 MPN <1.1 MPN
These data have been reviewed and are approved for release.
Sherry L. Ratzlaff
Supervisor, Bioassay Department
54 Ravenscroft Drive An Equal Opportunity Employer
Asheville, NC 28801
TEL:[phone]
FAX:[phone]

,oace.
REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF QUALITY
Mr. Robert MacPhee FOOTNOTES
Page 2 for page 1
Client Reference: MSD/2490449211
< Less than reported value.
> Greater than reported value.
MDL Method Detection Limit
July 06, 1995
PACE Project Number: A50627501
54 Ravenscroft Drive An Equal Opportunity Employer
Asheville, NC 28801
TEL:[phone]
FAX:[phone]

or Use a ball-point pen and press firmly.
PERMIT NUMBER: (REQUIRED)
Facility Name Metropolitan Sewerage District Non -Discharge
Address 2225 Riverside Drive NPDES NC 0024911
Asheville, North Carolina County Buncombe TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Well Location Downaradlent of Ash/Sludge Storage
lagoon
x Lagoon SepticTank/Drain Field
Well Identification Number M87J5 (MMI-211)
Well Depth 17.0 Ft.
Well Diameter 2.0" Sample (Screened) Interval
7.0 Ft. To 17.0 Ft.
Spray Field Subsurface Low -Pressure
Piping (LPP)
Depth to Water Level 7.04 ft. below measuring point
(before sampling)
Land Application of Sludge
Measuring point is 0.0 ft. above land surface
Other
allons of water pumped/bailed before sampling 6 gallons
Rotary Distributor
r=ield Analysis: pH 6 Specific Conductance
550 uMhos Temp. 13 °C
Odor NA Appearance turbid
Date Sample Collected February 27, 1995 Date Lab
Sample Analyzed January 27 through
March 8, 1995
Laboratory Name Law Environmental, Inc. and Pace, Inc.
Certification No.
287, 37712
SAMPLES 1=®R METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED X
YES NO 61
COD mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel° ° °mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N 3.6
/I
Pb - Lead <0.0040mg/I
Coliform: MF Total <1_1 MPN /100ml
Phosphorus: Total as P
4/1
Zn - Zinc = mg/I
(Note: Use MPN method for highly turbid samples)
Al - Aluminum
mg/I
Pesticides/Herbicides
Dissolved Solids: Total 500 mg/I
Ba - Barium 0-11
mg/I
(Specify Compounds) a
pH (when analyzed) units
Ca - Calcium
mg/I
ug/I
TOC 3.9 mg/I
Cd - Cadmium <o.0057
mg/I
y ug/I
Chloride 7.6 mg/I
Chromium: Total 0.012
mg/I
ug/I
Arsenic <0.050 mg/I
Cu - Copper
mg/I
Other (Specify Compounds and
;cease and Oils mg/I
Fe - Iron
mg/I
Concentration units)
. iardness: Total mg/I
Hg - Mercury <0.00015
mg/I
Total Suspended Solids = 140 mg/1
Phenol mg/I
K - Potassium
mg/I
Selenium = <0.050 mg/1
Sulfate mg/I
Mg - Magnesium
mg/I
Silver = <0.0050 mun
Specific Conductance uMhos
Mn - Manganese
mg/I
Total Ammonia <0.030 mg/I
Na - Sodium
mg/I
TKN as N mg/I
Results attached
I CERTIFY THAT THIS REPORT IS TRUE ANIita RATE LL
Note:
Values should reflect dissolved
.
and
t Yi
colloidal concentrations. (see #3 on back)
�f
d
@
see back for instructions.
e of Permittee (or Authorized Agent*)
Date a
** Submit blue, green, and yellow copies only to address above.
9/93
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N C 0 R P 0 R A T E 0 REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF QUALITY
Law Engineering
4 Interchange Blvd.
Greenville, SC 29607
Attn: Mr. Robert MacPhee
Client Reference: Monitoring Wells
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Bacteria, Total Coliform
March 08, 1995
PACE Project Number: A50227522
93 0066194 93 0066208 93 0066216
02/27/95 02/27/95 02/27/95
02/27/95 02/27/95 02/27/95
MW-1 MW-2R MW-3
Units MD1
col/100m1 1 >23 MPN <1.1 MPN <1.1 MPN
These data have been reviewed and are approved for release.
Sherry L. Ratzlaff
Supervisor, Bioassay Department
54 Ravenscroft Drive An Equal Opportunity Employer
Asheville. NC 28801
TEL [phone]
rAX:704.252-4618

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
03/09/95
ge 1
--- Project Information ---
Lab Number : 95-1121-03
Project No. : 2490449210 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: ROBERT MACPHEE
Station ID MW-2R
Matrix W
Type GRAB
Collector RM
--- Sample Information ---
Sampled Date/Time
: 02/27/95 13:05
Received Date/Time
: 02/28/95 09:33
Received From/By
: RM/LG
Chain of Custody
: 27479
Number of Containers
: 5
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
Chloride
Nitrogen, Ammonia
Nitrogen, Nitrate
Residue, Filterable (TDS)
Residue, Non Filterable (TSS)
EPA
415.1
mg/l
1.0
3.9
03/02/95
GW
EPA
325.3
mg/1
1.0
7.6
03/03/95
DF
EPA
350.1
mg/l
0.030
ND
03/08/95
KAA
EPA
353.2
mg/l
0.050
3.6
03/01/95
DF
EPA
160.1
mg/1
10
500
03/01/95
DF
EPA
160.2
mg/l
10
140
03/01/95
DF
-- METALS ANALYSIS - METALS PREP
RESULTS --
Mercury, Total
EPA
7470
-- METALS PREP RESULTS --
T. Metals Prep: Aqueous, Hg
EPA
7470
Metals Prep: Acid Extracted
SM 3030C
--- SERIES 39000
Arsenic, Extractable
EPA
6010
Barium, Extractable
EPA
6010
Cadmium, Extractable
EPA
6010
Chromium, Extractable
EPA
6010
Lead, Extractable
EPA
7421
Selenium, Extractable
EPA
6010
Silver, Extractable
EPA
6010
mg/l 0.00015 ND 03/03/95 ER
N/A 03/03/95 ER
EXTRACTED 03/01/95 CW
mg/1
0.050
ND
03/05/95
SDE
mg/l
0.019
0.11
03/05/95
SDE
mg/1
0.0057
ND
03/05/95
SDE
mg/1
0.0066
0.012
03/05/95
SDE
mg/l
0.0040
ND
03/05/95
SDE
mg/l
0.050
ND
03/05/95
SDE
mg/l
0.0050
ND
03/05/95
SDE
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated bas d on dry weight.
Signed

I GROUNDWATER FIELD/LAB FORM'
County 13l.4/V cCoh1 a r
Quad No Mr7 j.6' Serial No. / 3 9 D. % SAMPLE PRIORITY
Lat. 3 S 3 F `f s Long. 0 3S' y 3
IE
OUTINE []EMERGENCY
Report To:(O, FRO, MRO, RRO, WaRO, WiRO, F�;16HAIN OF CUSTODY
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by Bus urie Hand Del Other•
North Carolina
Department of Environment, Health, and Natural Resources
,�IVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION
Lab Number 'L
Date Received Time .S
Rec'd by: � rom: Bus, ouri r Hand Del.,
M W-,? k Other:
Data Entry By: Ca'Ck:
Date Reported: ✓� '�y� 9y
MiNN Gh! Purpose:
Collector(s): Date 9 -� `� -rime / % O a PM Baseline, Complaint, �, - LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner M ETkO PP c i 7-�`i N S� C°ir°2: i� Gc_ O is Ye i c -r
� aoo Spec. Cond.94 at 250 C Location or site o ^> ' / eN i to F .1 s` Fl o sP e s.� L A C s. o,
_;1mp.10 oC Odor Description of sampling point WELL- /-/E'A O
Appearance Sampling Method 8A / I E 9 Sample Interval %• D
S7`�) -ri G V✓A7-4,e " neV liT % SPL 7 Sflh1pLt H L..�fW L=NG,
Field Analysis By: Remarks o�5 vV/7
'
( um in tim airtem etc
LABORATORY ANALYSES �` ME-r."I L S. mpi-es HA vE i3�E;v° ,�'c�v/ �iCa /I ND f�JLTi'�'� t7 13,1
BOD 310 m /I Diss. Solids 70300 m /I *D,S A - Silver 46566 !, D u /I Organochlorine Pesticides
COD High 340 mg/I
Flouride 951 m /I
IAl
- Aluminum 46557 u /l
Organophosphorus Pesticides
COD Low 335 mg/I
Hardness: Total 900 m /l
315
As -Arsenic 46551 -/0 u /I
Nitrogen Pesticides
Coliform: MF Fecal 31616 /100m1
Hardness (non-carb) 902 m /1
A/s
Ba - Barium 46558 Fc u /I
Coliform: MF Total 31504 /100ml
Phenols 32730 u /I
Ca - Calcium 46552 m /I
Acid Herbicides
TOC 680 m /I
Specific Cond. 95 uMhos/cm2
0/5
Cd - Cadmium 46559 -4 ?, u /I
Turbidity 76 NTU
Sulfate 945 m /l
0/5
Cr - Chromium 46560 E0 u /I
Semivolatile Organics
Residue., Suspended 530 mg/I
Sulfide 745 m /I
Cu - Copper 46562 u /l
Fe - Iron 46563 u /I
*D/S
Hg - Mercury 71900 t D. ,;;_' ug/I
Volatile Organics (VOA bottle)
pH 403 _ unit
K - Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/I
M - Ma nesium 46554 A5 m /I
TPH - Gasoline Range
Alkalinity to pH 8.3 415 mg/I
Mn - Manganese 46565,.700o u /I
TPH - BTEX Gasoline Range
Carbonate 445 mg/l
0/5
NH as N 610 m /l
Na - Sodium 46556 m /I
Bicarbonate 440 m /I
Ni - Nickel Ye- u /I
Carbon dioxide 405 mg/I
D/.5
NO + NO as N 630 - m /I
x0i 5
Pb - Lead 46564 <'/O u /I
Chloride 940 mg/I
Q/ S
P: Total as P 665 mg/1
015
Se -Selenium 5 , u /I
Chromium: Hex 1032 ug/I
Zn - Zinc 46567 u /l
Color: True 80 Pt -Co
Cyanide 720 mg/I
Comments:
t-or Uissolved Analysis- submit filtered sample and write "DIS" in block.

North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
DIVISION OF ENVIRONMENTAL MANAGEMENT- GROUNDWATER SECTION
n
County /-2 W N C ®/-' & e- Lab Number �2 1 & /
Quad No-",? 7 J -' Serial No. 3 8 0,2 7 SAMPLE PRIORITY Date Received 5 - a K - `i y Time
Lat. 3S 3 Y-S-Long. 6-2 3 S Rec'd by: � From: Bus, Court Flan e
ROUTINE EMERGENCY Other:
Report To: ARO FRO, MRO, RRO, WaRO, WiRO, ❑CHAIN OF CUSTODY ,
Data Entry By: ��,�/� Ck:
ED
WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: ld
Shipped by: Bus, Courier, d De Other-
NOV / c � Purpose:
Collector(s): Rurr� ccf ; rl' Date 9 7 Time / / GD Baseline, Complaint, om iance LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES circlsone
Owner L rR0 /0 � ��'I /14 ]SE WG6 Z) - TRI C
pH,,, Spec. Cond.94 at 250 C Location or site 00 v✓r G RA®/C^) . c) F --I s N /'1 sPo sj-
Temp.io oC Odor Description of sampling oint WE C 4- �-/640
Appearance Sampling Method 9� / L CR Sample Interval_
Field Analysis By: Remarks 5 TA 7 / C. W,q 7. r
(pumping time air temp. etc.)
LABORATORY ANALYSES 510z- I' - .5A ^y PC E s w, --/-f Llpn w Cn/G / iv c=. f^j
m "
COD High 340 mg/I
COD Low 335 ar4 N mg/I
Ui5
Diss. Solids 70300 360 m /I
A -Silver 46566 u /I
Flouride 951 m /I
Hardness: Total 900 m /I
Al - Aluminum 46557 u /I
As - Arsenic 46551 u /I
Coliform:-ktP Fecal �ts#6 t „ /100m1
Coliform:;bIF Total 344 a ,/ /100m1
TOC 680.E m /I
Turbidity 76 NTU
Hardness non-carb 902 m /I'
Phenols 32730 u /I
Specific Cond. 95 uMhos/crn2
Sulfate 945 m I
Ba - Barium 46558 u /I
Ca - Calcium 46552 m /I
Cd - Cadmium 46559 u /1
Cr - Chromium 46560 u /I
Residue., Suspended 530 QV,mg/I
Sulfide 745 m /I
Cu - Copper 46562 u /I
Fe - Iron 46563 u /I
Hg - Mercury 71900 ug/I
pH 403 it
� , � un
K -Potassium 46555 mg/IM
Alkalinity to pH 4.5 410 mg/I
- Magnesium 46554 m /I
Alkalinity to pH 8.3 415 mg/I
Carbonate 445 mg/I
Bicarbonate 44o m /I
NH as N 610 m /I
Mn - Man Manganese 46565 u /I
Na -Sodium 46556 rn /I
Ni -Nickel u /I
Carbon dioxide 405 mg/I
NO + NO as N 630 m /I
Pb - Lead 46564 u /I
D i 5
Chloride 940 mg/I
P: Total as P 665 m /I
Se - Selenium u /I
Chromium: Hex 1032 ug/I
Color: True 80 Pt -Co
Zn - Zinc 46567 u /I
Cyanide 720
4
v k,urnmenTs:
7.O /-/, o'
,chlorine Pesticides
phosphorus Pesticides
n Pesticides
Acid Herbicides
Semivolatile
Volatile Organics (VOA bottle)
TPH - Gasoline Rang(
TPH - BTEX Gasoline
6/93 For Dissolved Analysis - submit filtered sample and write "DIS" in block.

Please use ink pen and press firmly. PERMIT NUMBER: (REQUIRED)
Metropolitan Sewerage District Non -Discharge
Facility Name NPDES NC nn7do»
Address Asheville.
Riverside Drive TYPE OF DISPOSAL OPERATION BEING MONrrORED
Asheville, North Carolina County Buncombe (REQUIRED)
X La con Septic Tank/Drain Field
Well Location Downgradient of ash/sludge storage lagoon g
Well Identification Number M87J5 (MW-2R) Well Depth 17.0 Ft. spray Field
Well Diameter 2.0° Sample (Screened) Interval 7.0 Ft To 17.0 Ft.
Land Application of Sludge
Depth to Water Level 7.8 ft. below measuring point (before sampling) other
Measuring point is 0-0 ft. above land surface Rotary Distributor
" 11lons of water pumped/bailed before sampling 4.7 gallons mo era e xy
,ad Analysis: pH 6.0 Specific Conductance 390 uMhos Temp. 20 ° C Odor NA Appearance �r bi d
Date Sample Collected September 28. 1994 Date Lab Sample Analyzed September 29-October 12. 1994
Laboratory Name
Law Environmental, Inc., Pace, Inc. Certification No. 287, 37712
Subsurface Low -Pressure
Piping (LPP)
m /I Ni - Nickel - .► :=fig/I
C®® mg/I Nitrite (NO 2) as N g <0.032 g/I
Coliform: MF Fecal /100ml Nitrate (NO 3) as N 4.o mg/I Pb -Lead
< 1.1 MPN A 00ml Phosphorus: Total as P mg/I Zn - Zinc g/I
Coliform: MF Total I m /I Pesticides/Herbicides
(Note: Use method for highly turbid samples) Al - Aluminum g
360 m /I Ba - Barium 0.16 mg/I (Specify Compounds)-
Dissolved Solids: Total g u /1
pH (when analyzed) units Ca - Calcium mg�� ug/I
4.0 m /1 Cd - Cadmium <0.0031 g
®oride 8.7 mg/I Chromium: Total 0.011 mg/I ug/I
Arsenic < 0.050 mg/I Cu -Copper mg/I Other (Specify Compounds and
mg/I Concentration units)
Grease and Oils mg/I Fe - Iron <0.00015 mg/I Total Suspended Solids .= 240 mg/l
ardness: Total mg/1 Hg - Mercury Selenium = <0.050 mg/l
Phenol mg/I K - Potassium mg/I Silver = <0.0069mg/l
Sulfate mg/I Mg - Magnesium g vocs (502.2) = ND
Specific Conductance uMhos Mn - Manganese mg/I
Total Ammonia 0.055 mg/I Na - Sodium mg/1 Results attached
TKN as N g
I CERTIFY THAT THIS REPORT IS TR , . U` Note: Values should reflect dissolved and
colloidal concentrations. (see #2 on back)
NOV 2
U Ll.,. 4 6-9y see bads for Instructions
•e of Permittee (or Authorized Agent ate '* submit blue, green, and yellow copies only to address above.
9/92

wQ4 N
R�_
EFL SA14PLES
Samples should be analyzed as scar cis possible after collection, M S WHICH E
NOT ANALYSED WITHIN THE HOLDING
TIME SPECIFIED FOR E METHOD USED e EL UST BE DISCARDED AND NEW SAMPLESCOLLECTED.
ZA ANALYSES ARE TO BE MADE F SHE MOBILE CONSTITUENTS (DISSOLVED As WELL AS
COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT AREv f . CHECK WITH YOUR LABORATORY ON PROPER
PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
. At least 3 volumesof grater in the well should be pumped or bailed prier to collecting a sample for analysis. If the well is pumpedlbailed dry
before 3 well volumes are removed, pl can be collected as soon as the well recovers to the paint where enough water is available t
collect your sample.
Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field an unfiltered samples when the
sample is collect
. Field equipment mod be calibrated in accordance with recommendations by the manufacturer,
. Samples must be fiftered through a 0,45 micron filter immediately after collection when a dissolve analysis is required, (See . above)
n The sample container sftUld be labeled at the time of collection with the facility name, well Identification number and date and time 1
lecteda
." thorned agent" is any corporate, officer or public official authorized by the company, corporation, or governmental boc(Y to alga cffi$ d0GUmer its.

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
.:e 10/17/94
.-age 1
--- Project Information ---
Lab Number : 94-9122-03
Project No. : 2490449209 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: ROBERT MACPHEE
Station ID : MW-2R
Matrix : W
Type : GRAB
Collector : RM
--- Sample Information ---
Sampled Date/Time :
09/28/94 13:00
Received Date/Time :
09/29/94 08:46
Received From/By :
RM/LD
Chain of Custody :
30326
Number of Containers :
8
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/l
1.0
4.0
10/12/94
DF
Chloride
EPA
325.3
mg/l
2.0
8.7
10/07/94
DF
Nitrogen, Ammonia
EPA
350.1
mg/l
0.030
0.055
10/04/94
DLM
Nitrogen, Nitrate
EPA
353.2
mg/1
0.050
4.0
10/06/94
DLM
Residue, Filterable (TDS)
EPA
160.1
mg/1
10
360
09/30/94
DF
Residue, Non Filterable (TSS)
EPA
160.2
mg/l
10
240
09/30/94
DF
-- METALS ANALYSIS - METALS PREP RESULTS --
Mercury, Total EPA 7470
-- METALS PREP RESULTS --
Metals Prep: Acid Extracted SM 3030C
mg/l 0.00015 ND 10/03/94 CW
EXTRACTED 09/30/94 CW
--- SERIES 39000
Arsenic, Extractable
EPA
6010
mg/l
0.050
ND
10/03/94
SDE
Barium, Extractable
EPA
6010
mg/1
0.0089
0.16
10/03/94
SDE
Cadmium, Extractable
EPA
6010
mg/l
0.0031
ND
10/03/94
SDE
Chromium, Extractable
EPA
6010
mg/1
0.0052
0.011
10/03/94
SDE
Lead, Extractable
EPA
6010
mg/1
0.032
ND
10/03/94
SDE
Selenium, Extractable
EPA
6010
mg/1
0.050
ND
10/03/94
SDE
Silver, Extractable
EPA
6010
mg/l
0.0069
ND
10/03/94
SDE
--- SERIES 88000
Dichlorodifluoromethane
EPA
502.2
ug/1
3.2
ND
10/11/94
VZ
Chloromethane
EPA
502.2
ug/l
0.90
ND
10/11/94
VZ
Vinyl Chloride
EPA
502.2
ug/l
1.9
ND
10/11/94
VZ
Bromomethane
EPA
502.2
ug/l
0.80
ND
10/11/94
VZ
Chloroethane
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
Trichlorofluoromethane
EPA
502.2
ug/1
1.8
ND
10/11/94
VZ
1,1-Dichloroethene
EPA
502.2
ug/l
0.83
ND
10/11/94
VZ
Methylene Chloride
EPA
502.2
ug/l
0.62
ND
10/11/94
VZ
Remarks:
DL = Detection Limit
ND
= Not Detected at the DL
%:gWBe noted,
all soil test results
are calculated based on
dry weight.
Lli,
Signed
ALI

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
_e 10/17/94
-age 2
Lab Number : 94-9122-03
Project No. : 2490449209
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
--- SERIES 88000
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.92
ND
10/11/94
VZ
1,1-Dichloroethane
EPA
502.2
ug/l
0.63
ND
10/11/94
VZ
cis-1,2-Dichloroethene
EPA
502.2
ug/1
0.84
ND
10/11/94
VZ
Chloroform
EPA
502.2
ug/l
0.79
ND
10/11/94
VZ
Bromochloromethane
EPA
502.2
ug/l
0.42
ND
10/11/94
VZ
1,1,1-Trichloroethane
EPA
502.2
ug/l
0.56
ND
10/11/94
VZ
1,1-Dichloropropene
EPA
502.2
ug/1
0.88
ND
10/11/94
VZ
Carbon Tetrachloride
EPA
502.2
ug/1
1.2
ND
10/11/94
VZ
Benzene
EPA
502.2
ug/l
0.87
ND
10/11/94
VZ
1,2-Dichloroethane
EPA
502.2
ug/l
0.65
ND
10/11/94
VZ
Trichloroethene
EPA
502.2
ug/l
0.90
ND
10/11/94
VZ
1,2-Dichloropropane
EPA
502.2
ug/l
0.70
ND
10/11/94
VZ
Bromodichloromethane
EPA
502.2
ug/1
0.56
ND
10/11/94
VZ
Dibromomethane
EPA
502.2
ug/l
0.72
ND
10/11/94
VZ
cis-1,3-Dichloropropene
EPA
502.2
ug/l
0.80
ND
10/11/94
VZ
Toluene
EPA
502.2
ug/l
0.90
ND
10/11/94
VZ
trans-1,2-Dichloropropene
EPA
502.2
ug/l
0.82
ND
10/11/94
VZ
1,1,2-Trichloroethane
EPA
502.2
ug/1
0.73
ND
10/11/94
VZ
Tetrachloroethane
EPA
502.2
ug/l
2.0
ND
10/11/94
VZ
1,3-Dichloropropane
EPA
502.2
ug/l
0.68
ND
10/11/94
VZ
Dibromochloromethane
EPA
502.2
ug/l
0.41
ND
10/11/94
VZ
1,2-Dibromoethane
EPA
502.2
ug/1
0.77
ND
10/11/94
VZ
Ethylbenzene
EPA
502.2
ug/l
0.92
ND
10/11/94
VZ
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
Xylene, Total
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
Styrene
EPA
502.2
ug/l
1.1
ND
10/11/94
VZ
Isopropylbenzene
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
Bromoform
EPA
502.2
ug/l
0.47
ND
10/11/94
VZ
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/l
0.86
ND
10/11/94
VZ
1,2,3-Trichloropropane
EPA
502.2
ug/l
0.79
ND
10/11/94
VZ
n-Propylbenzene
EPA
502.2
ug/l
1.9
ND
10/11/94
VZ
Bromobenzene
EPA
502.2
ug/1
1.9
ND
10/11/94
VZ
1,3,5-Trimethylbenzene
EPA
502.2
ug/l
2.0
ND
10/11/94
VZ
2-Chlorotoluene
EPA
502.2
ug/1
2.0
ND
10/11/94
VZ
4-Chlorotoluene
EPA
502.2
ug/1
0.80
ND
10/11/94
VZ
tert-Butylbenzene
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
sec-Butylbenzene
EPA
502.2
ug/l
1.1
ND
10/11/94
VZ
p-Isopropyltoluene
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
1,3-Dichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
1,4-Dichlorobenzene
EPA
502.2
ug/1
1.0
ND
10/11/94
VZ
n-Butylbenzene
EPA
502.2
ug/l
1.1
ND
10/11/94
VZ
1,2-Dichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/11/94
VZ
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/l
0.58
ND
10/11/94
VZ
1,2,4-Trichlorobenzene
EPA
502.2
ug/1
1.1
ND
10/11/94
VZ
Hexachlorobutadiene
EPA
502.2
ug/1
1.2
ND
10/11/94
VZ
Naphthalene
EPA
502.2
ug/1
1.1
ND
10/11/94
VZ
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
1.1
ND
10/11/94
VZ
Signed

Facili
well
well
well
ty
Please use ink pen and press firmly. PERMIT NUMBER: (REQUIRED)
Name METROPOLITAN SEWERAGE DISTRICT Non -Discharge
Address 2225 RIVERSIDE DRIVE NPDES NC 0024911
ASHEVILLE. NORTH CAROLINA County BUNCOMBE TYPE OF DISPOSAL OPERATION
D
Location OWNGRADIENT OF ASH/SLUDGE STORAGE LAGOON (REQUIRED) X
Lagoon
Identification Number M87J5(MW-2R) well Depth 17.0 Ft.
Diameter 2.0" Sample (Screened) Interval 7.0 Ft To 17.0 Ft. Spray Field
Depth to water Level 7.38 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 0.0 ft. above land surface
'allons of water pumped/bailed before sampling 7.0 gallons
Rotary Distributor
ield Analysis: pH 6.5 Specific Conductance 390 uMhos Temp. 17 °C Odor NA Appearance SLIGHTLY TURBID
Date Sample Collected JUNE 30, 1994 Date Lab Sample Analyzed JULY 1 - 12, 1994
Laboratory Name LAW ENVIRONMENTAL INC., PACE, INC. Certification No. 287.37712
BEING MONITORED
COD mg/I
Coliform: MF Fecal /1 ooml
Coliform: MF Total < 1.1 MPN /100ml
(Note: Use MPrd method for highly turbid samples)
Dissolved Solids: Total 330
pH (when analyzed)
TOC 6.5
Chloride 9.0
Arsenic < 0.050
Grease and Oils
aardness: Total
Phenol
Sulfate _
Specific Conductance
Total Ammonia 0.038
TKN as N
_ mg/I
units
mg/I
mg/I
_ mg/I
mg/I
_ mg/I
mg/I
_ mg/I
uMhos
mg/I
mg/I
Nitrite (NO 2) as N
mg/I
Nitrate (NO 3) as N 3.6
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium 0.10
mg/I
Ca - Calcium
mg/I
Cd - Cadmium < 0.0057
mg/I
Chromium: Total < 0.0066
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury < 0.00015
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Septic TanWDrain Field
Subsurface Low -Pressure
Piping (LPP)
Other
Ni - Nickel
mg/I
Pb - Lead < 0.032
mg/I
Zn - Zinc
�
jPg/I
Pesticides/Herbicides'
F°
(Specify Compounds)
A
;fig/I
Other (Specify Compounds
and 7
Concentration units)
TOTAL SUSPENDED SOLIDS = 56 mg/l­
SELENIUM
= < 0.050 mg/1
SILVER
= < 0.0050
RESULTS ATTACHED
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see 42 on back)
AA See back for inshuctions.
of Permittee (or Authorized 'A"errt* �. I it ** submit blue, green, and yellow co onl to address above,
t 3;L. r a t y
9/92
_. _._, `, i ad$

COLLECTION AND ANALYS)IS OF GROUNDWATER SAMPLES
Samples should analyzed as soon as, possible after collection. SAMPLES WHICHNOT ANALYSED
SPECIFIEDTIME USED S ELF MUST BE DISCARDED SAMPLES L
ANALYSES2. F THE MOBILE CONSTTrUENTS (DISSOLVED AS WELL AS COLLOIDAL)
GROUNDWATER, NOT THOSE THAT H
SAMPLEPROCEDURES FOR lON AND PRESERVATION.
. Determination for pH, Specific Conductance, temperature, actor and appearance must be made in the field can unfiltered samples when the
sample is collected.
. Field equipment must be calibrated in accordance ith recommendations by the manufacturer.
x Samples mat be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (Seeabove)
9. The sample ntai ar should be labeled at the time of collection with. the facility mama, well identification number and data and time cok
lasted
10."Autl ri ad agent" is any c rp rate aft c, r or publk- official aUtl r riZed by the `company, c rp ation, or governmental boo, to alga off,

LAW ENVIRONMENTAL NATIONAL LABORATORIES
ce 07/18/94 TEST DATA REPORT - RED IVEO "")
`"t. €e a �,
Page 1t .
--- Project Information
Lab Number : 94-8526-03
Project No. : 2490449208 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: ROBERT MACPHEE
Station ID MW-2R
Matrix W
Type GRAB
Collector RM
--- Sample Information ---
Sampled Date/Time : 06/30/94 14:00
Received Date/Time : 07/01/94 09:35
Received From/By : RM/LD
Chain of Custody : 31921
Number of Containers : 5
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/l
1.0
6.5
Chloride
EPA
325.3
mg/l
2.0
9.0
Nitrogen, Ammonia
EPA
350.1
mg/l
0.030
0.038
Nitrogen, Nitrate
EPA
353.2
mg/l
0.050
3.6
Residue, Filterable (TDS)
EPA
160.1
mg/1
10
330
Residue, Non Filterable (TSS)
EPA
160.2
mg/l
10
56
-- METALS ANALYSIS - METALS
PREP RESULTS --
Mercury, Total
EPA
7470
-- METALS PREP RESULTS --
T. Metals Prep: Aqueous, Hg
EPA
7470
Metals Prep: Acid Extracted
SM
3030C
--- SERIES 39000
Arsenic, Extractable
EPA
6010
Barium, Extractable
EPA
6010
Cadmium, Extractable
EPA
6010
Chromium, Extractable
EPA
6010
Lead, Extractable
EPA
6010
Selenium, Extractable
EPA
6010
Silver, Extractable
EPA
6010
mg/l 0.00015 ND
07/05/94 RJO
07/06/94 JR
07/11/94 KAA
07/12/94 DLM
07/07/94 JR
07/07/94 GW
07/12/94 CW
N/A 07/12/94 CW
EXTRACTED 07/01/94 CW
mg/l
0.050
ND
07/08/94
BM
mg/1
0.019
0.10
07/08/94
BM
mg/l
0.0057
ND
07/08/94
BM
mg/1
0.0066
ND
07/08/94
BM
mg/l
0.032
ND
07/08/94
BM
mg/l
0.050
ND
07/08/94
BM
mg/l
0.0050
ND
07/08/94
BM
Remarks:
DL = Detection Limit ND = Not Detected at the DL
a� i{se noted, all soil test results are calculated based on dry weight.
1,0 `7
%0 P,
Signed
rAUG 2 5 1994�W
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LAW ENVIRONMENTAL NATIONAL LABORATORIES
03/18/94 TEST DATA REPORT
,a 1
--- Project Information ---
Lab Number : 94-7651-02
Project No. : 2490449206 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: ROBERT MACPHEE
Station ID
MW-2R
Matrix
W
Type
: GRAB
Collector
JL
--- Sample Information ---
Sampled Date/Time 03/02/94 14:11
Received Date/Time 03/03/94 10:00
Received From/By JA/JA
Chain of Custody 26568
Number of Containers 5
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
Chloride
Nitrogen, Ammonia
Nitrogen, Nitrate
Residue, Filterable (TDS)
Residue, Non Filterable (TSS)
EPA
415.1
mg/1
1.0
1.5
03/07/94
CVD
EPA
325.3
mg/l
0.20
8.9
03/14/94
KAA
EPA
350.1
mg/l
0.030
ND
03/09/94
KAA
EPA
353.2
mg/l
0.050
4.9
03/04/94
KAA
EPA
160.1
mg/l
10
380
03/14/94
TT
EPA
160.2
mg/l
10
850
03/08/94
KAA
-- METALS ANALYSIS - METALS PREP RESULTS --
Mercury, Total EPA 7470
-- METALS PREP RESULTS --
T. Metals Prep: Aqueous, Hg EPA 7470
Metals Prep: Acid Extracted SM 3030C
--- SERIES 39000
Arsenic, Extractable
Barium, Extractable
Cadmium, Extractable
Chromium, Extractable
Lead, Extractable
Selenium, Extractable
Silver, Extractable
mg/l 0.00015 ND 03/14/94 ER
N/A 03/13/94 ER
EXTRACTED 03/04/94 ER
EPA
6010
mg/l
0.050
ND
03/17/94
DF
EPA
6010
mg/1
0.0089
0.14
03/17/94
DF
EPA
6010
mg/l
0.0031
ND
03/17/94
DF
EPA
6010
mg/1
0.0652
ND
03/17/94
DF
EPA
6010
mg/l
0.032
ND
03/17/94
DF
EPA
6010
mg/l
0.050
ND
03/17/94
DF
EPA
6010
mg/l
0.0069
ND
03/17/94
DF
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry weight.
Signed i

\.,._
fl C O R P 0 8 A T t? 0
oace.,
HE ASSURANCE OF OUALrTY
REPORT OF LABORATORY ANALYSIS
Law Engineering
4 Interchange Blvd.
Greenville, SC 29607
Attn: Mr. Robert MacPhee
Client Reference: 2490449206
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter Units MDL
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Bacteria, Total. Coliform col/100ml 1
These data have been reviewed and are approved for release.
Sherry . Ratzlaff
Supervisor, Bioassay Department
March 08, 1904
PACE Project Number: A40302510
93 0189563 93 0189571 93 0189580
03/02/94 03/02/94 03/02/94
03/02/94 03/02/94 03/02/94
MW-1 MW-2R MW-3
<1.1MPN 1.1 MPN <1.1 MPN
54 Ravenscrolt Drive An Equal Opportunity Employer
Asheville, NC 28801
TEL [phone]
FAX: [phone]

,Oace"
/� N l O R P O R A T e o® REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF QUALITY
Mr. Robert MacPhee FOOTNOTES
Page 2 for page 1
Client Reference: 2490449206
< Less than reported value.
MDL Method Detection Limit
54 Ravenscrott Drive
Asheville, NC 28801
TEL: [phone]
FAX: [phone]
March 08, 1994
PACE Project Number: A40302510
An Equal Opportunity Employer

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I N C O R P O R A T E D
goo Cl ce'�""
THE ASSURANCE OF QUALITY
REPORT OF LABORATORY ANALYSIS
Law Engineering
4 Interchange Blvd.
Greenville, SC 29607
Attn: Mr. Robert MacPhee
Client Reference: Metropolitan Sewerage District
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter Units
INORGANIC ANALYSIS
DRINKING WATER COLIFORM BACTERIA
Total Coliform by Colilert MMO-MUG312 1
MDL
These data have been reviewed and are approved for release.
t M. 4.4
Barbara M. Miller
Supervisor, Inorganic Chemistry
54 Ravenscroft Drive
Asheville, NC 28801
TEL: [phone]
FAX: [phone]
Offices Serving: Minneapolis, Minnesota
Tampa, Florida
Iowa City, Iowa
San Francisco, California
Kansas City, Missouri
Los Angeles, California
July 08, 1993
PACE Project Number: A30630514
93 0048684 93 0048692 93 0048765
06/30/93 06/30/93 07/01/93
06/30/93 06/30/93 07/01/93
MW-2R MW-1 MW-3
ABSENT (1) PRESENT PRESENT
(2) (2)
Charlotte, North Carolina An Equal Opportunity Employer
Asheville, North Carolina
New York, New York
Pittsburgh, Pennsylvania
Denver, Colorado

,oace.,
I N C 0 R P 0 R A T E 0REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF 0 U A L 1 T Y
Mr. Robert MacPhee FOOTNOTES July 08, 1993
Page 2 for page 1 PACE Project Number: A30630514
Client Reference: Metropolitan Sewerage District
MDL Method Detection Limit
(1) This sample does meet state bacteriological standards.
(2) This sample does not meet state bacteriological standards.
54 Flavenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina
Asheville, NC 26601 Tampa, Florida Asheville, North Carolina
TEL: [phone] Iowa City, Iowa New York, New York
FAX: [phone] San Francisco, California Pittsburgh, Pennsvlvania
Kansas City, Missouri Denver, Colorado
Los Angeles, California
An Equal Opportunity Employer

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LAW ENGINEERING
Ak geotechnical, environmental & construction materials consultants
FOUR INTERCHANGE BOULEVARD
GREENVILLE, SOUTH CAROLINA 29607
[phone]
LETTER OF TRANSMITTAL
TO: North Carolina Division of Environmental
Management - Groundwater Section
P.O. Box 29535
Raleigh, NC 27626-0535
ATTENTION:
DATE:
RE:
GENTLEMEN:
Ms. Betty Wilcox
November 5, 1992
Metropolitan Sewerage District, Asheville North Carolina
Tri-Annual Sampling Program
WE ARE SENDING YOU X Attached
Draft report
Copy of report
Plans
Proposal Dated
Under separate cover via the following items:
Prints Change order
Letter W.A.S.
Invoice Specifications
Preliminary Data
THESE ARE TRANSMITTED AS CHECKED BELOW:
For approval x For your use Other
As requested For review and comment Number of Copies
Number of conies:
Other
REMARKS: Dear Betty,
Attached are the tri-annual sampling results for the month of September. The Groundwater
Quality Monitoring: Compliance Report Forms are attached along with all of the analytical data.
If you have any questions regarding the analytical results please do not hesitate to call, 1-800-
365-7891.
Sincerely, Robert E. MacPhee
LAW ENGINEERING INC. Project Hydrogeologist

LAW ENVIRONMENTAL. INC.
112 TOWNPARK DRIVE
KENNESAW, GEORGIA 30144-5599
404-421-3400
October 20, 1992
Law Engineering, Inc.
Four Interchange Blvd.
Greenville, SC 29607
Attention: Bob MacPhee
Job Number 2490449203
Subject: Chemical Analysis of Samples Received on 10/01/92.
Dear Mr. MacPhee:
Law Environmental National Laboratories has completed its analysis
of your samples and reports the results on the following pages.
These results relate only to the contents of the samples as
submitted. This report shall not be reproduced except in full
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
LAW ENVIRONMENTAL NATL BS
Clifford H. McBride
QC Coordinator
Attachment: Data Report
Invoice

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
15/92
1
--- Project Information ---
Lab Number : 92-3769-01
Project No. : 2490449203 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: BOB MACPHEE
Station ID : MW-1
Matrix : W
Type : GRAB
Collector : JA
--- Sample Information ---
Sampled Date/Time :
09/29/92 14:30
Received Date/Time :
10/01/92 14:45
Received From/By :
JA/LD
Chain of Custody :
15311
Number of Containers :
10
Parameter .............................. Method.... Units DL........ Results... Test Date Anal}
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/1
1.0
6.6
10/08/92
TH
Chloride
EPA
325.3
mg/1
0.20
2.0
10/02/92
JR
Nitrogen, Ammonia
EPA
350.1
mg/l
0.030
0.13
10/02/92
ORF
Nitrogen, Nitrate
EPA
353.2
mg/1
0.050
0.051
10/02/92
ORF
Residue, Filterable (TDS)
EPA
160.1
mg/l
10
77
10/12/92
ORF
Residue, Non Filterable (TSS)
EPA
160.2
mg/1
10
ND
10/07/92
ORF
-- METALS ANALYSIS - METALS PREP RESULTS --
Barium, Total
EPA
6010
mg/1
0.0089
ND
10/12/92
JST
Mercury, Total
EPA
7470
mg/1
0.00022
ND
10/13/92
HH
Arsenic, Total
EPA
7060
mg/1
0.0017
0.0017
10/08/92
DF
Cadmium, Total
EPA
7131
mg/1
0.0011
ND
10/08/92
DF
Chromium, Total
EPA
7191
mg/l
0.0026
ND
10/09/92
DF
Lead, Total
EPA
7421
mg/l
0.0028
ND
10/08/92
DF
Selenium, Total
EPA
7740
mg/l
0.0021
ND
10/08/92
DF
Silver, Total
EPA
7761
mg/1
0.0014
ND
10/12/92
DF
--- SERIES 35000
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
10/07/92
HH
Total Metals Prep: Aqueous Furnace
EPA
3020
N/A
10/07/92
HH
Total Metals Prep: Aqueous, Hg
EPA
7470
N/A
10/12/92
HH
-- GC ORGANIC ANALYSIS RESULTS --
Chloromethane
EPA
502.2
ug/l
5.0
ND
10/09/92
EA
Vinyl Chloride
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
Bromomethane
EPA
502.2
ug/1
5.0
ND
10/09/92
EA
Chloroethane
EPA
502.2
ug/1
5.0
ND
10/09/92
EA
Trichlorofluoromethane
EPA
502.2
ug/1
0.9
ND
10/09/92
EA
1,1-Dichloroethene
EPA
502.2
ug/l
0.9
ND
10/09/92
EA
Methylene Chloride
EPA
502.2
ug/l
5.0
ND
10/09/92
EA
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.6
ND
10/09/92
EA
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry we' t.
Signed �

LAW ENVIRONMENTAL NATIONAL LABORATORIES
\ TEST DATA REPORT
15/92
2
Lab Number : 92-3769-01
Project No. : 2490449203
Parameter .............................. Method.... Units DL........ Results... Test Date Anall
-- GC ORGANIC ANALYSIS RESULTS --
1,1-Dichloroethane
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
cis-1,2-Dichloroethene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Chloroform
EPA
502.2
ug/1
2.0
ND
10/09/92
EA
Bromochloromethane
EPA
502.2
ug/1
0.3
ND
10/09/92
EA
1,1,1-Trichloroethane
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
1,1-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Carbon Tetrachloride
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Benzene
EPA
502.2
ug/1
0.2
ND
10/09/92
EA
1,2-Dichloroethane
EPA
502.2
ug/1
0.9
ND
10/09/92
EA
Trichloroethene
EPA
502.2
ug/l
0.6
ND
10/09/92
EA
1,2-Dichloropropane
EPA
502.2
ug/l
0.3
ND
10/09/92
EA
Bromodichloromethane
EPA
502.2
ug/l
0.9
ND
10/09/92
EA
Dibromomethane
EPA
502.2
ug/1
0.6
ND
10/09/92
EA
cis-1,3-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Toluene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
trans-1,2-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
1,1,2-Trichloroethane
EPA
502.2
ug/l
0.9
ND
10/09/92
EA
Tetrachloroethane
EPA
502.2
ug/1
2.0
ND
10/09/92
EA
1,3-Dichloropropane
EPA
502.2
ug/1
2.0
ND
10/09/92
EA
Dibromochloromethane
EPA
502.2
ug/l
0.9
ND
10/09/92
EA
1,2-Dibromoethane
EPA
502.2
ug/l
2.0
ND
10/09/92
EA
Ettylbenzene
EPA
502.2
ug/1
0.5
ND
10/09/92
EA
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/1
2.0
ND
10/09/92
EA
Xylene, Total
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
Styrene
EPA
502.2
ug/1
0.5
ND
10/09/92
EA
Isopropylbenzene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Bromoform
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/1
2.0
ND
10/09/92
EA
1,2,3-Trichloropropane
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
n-Propylbenzene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
Bromobenzene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
1,3,5-Trimethylbenzene
EPA
502.2
ug/1
0.5
ND
10/09/92
EA
2-Chlorotoluene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
4-Chlorotoluene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
tert-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
sec-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
p-Isopropyltoluene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
1,3-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/09/92
EA
1,4-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/09/92
EA
n-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
1,2-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/09/92
EA
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/1
3.0
ND
10/09/92
EA
1,2,4-Trichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
Hexachlorobutadiene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Naphthalene
EPA
502.2
ug/l
1.0
ND
10/09/92
EA
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
1.0
ND
10/09/92
EA
Signed
�1 ��

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
/15/92
1
--- Project Information ---
Lab Number : 92-3769-02
Project No. : 2490449203 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: BOB MACPHEE
Station ID : MW-2R
Matrix : W
Type : GRAB
Collector : JA
--- Sample Information ---
Sampled Date/Time : 09/30/92 12:00
Received Date/Time : 10/01/92 14:45
Received From/By : JA/LD
Chain of Custody : 15311
Number of Containers : 10
Parameter .............................. Method.... Units DL........ Results... Test Date Anal.
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/l
1.0
9.8
10/08/92
TH
Chloride
EPA
325.3
mg/l
0.20
3.0
10/02/92
JR
Nitrogen, Ammonia
EPA
350.1
mg/1
0.030
0.29
10/02/92
ORF
Nitrogen, Nitrate
EPA
353.2
mg/l
0.050
2.0
10/02/92
ORF
Residue, Filterable (TDS)
EPA
160.1
mg/1
10
260
10/12/92
ORF
Residue, Non Filterable (TSS)
EPA
160.2
mg/l
10
440
10/07/92
ORF
-- METALS ANALYSIS - METALS PREP RESULTS --
Barium, Total
EPA
6010
mg/1
0.0089
0.086
10/12/92
JST
Mercury, Total
EPA
7470
mg/1
0.00022
ND
10/13/92
HH
Arsenic, Total
EPA
7060
mg/l
0.0017
ND
10/08/92
DF
Cadmium, Total
EPA
7131
mg/1
0.0011
ND
10/08/92
DF
Chromium, Total
EPA
7191
mg/1
0.0026
ND
10/09/92
DF
Lead, Total
EPA
7421
mg/1
0.0028
ND
10/08/92
DF
Selenium, Total
EPA
7740
mg/l
0.0021
ND
10/08/92
DF
Silver, Total
EPA
7761
mg/l
0.0014
ND
10/12/92
DF
--- SERIES 35000
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
10/07/92
HH
Total Metals Prep: Aqueous Furnace
EPA
3020
N/A
10/07/92
HH
Total Metals Prep: Aqueous, Hg
EPA
7470
N/A
10/12/92
HH
-- GC ORGANIC ANALYSIS RESULTS --
Chloromethane
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
Vinyl Chloride
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromomethane
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
Chloroethane
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
Trichlorofluoromethane
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
1,1-Dichloroethene
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Methylene Chloride
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.6
ND
10/10/92
EA
Remarks:
DL = Detection Limit ND - Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on d weight.
Signed

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT f
, 15/92
2
Lab Number : 92-3769-02
Project No. : 2490449203
Parameter .............................. Method.... Units DL........ Results... Test Date Ana1S
-- GC ORGANIC ANALYSIS RESULTS --
1,1-Dichloroethane
cis-1,2-Dichloroethane
Chloroform
Bromochloromethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
cis-1,3-Dichloropropene
Toluene
trans-1,2-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
1,3-Dichloropropane
Dibromochloromethane
1,2-Dibromoethane
Ethylbenzene
1,1,1,2-Tetrachloroethane
Xylene, Total
Styrene
Isopropylbenzene
Bromoform
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
n-Propylbenzene
Bromobenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
sec-Butylbenzene
p-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
EPA
502.2
ug/l
0.3
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
0.2
ND
10/10/92
EA
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
EPA
502.2
ug/l
0.6
ND
10/10/92
EA
EPA
502.2
ug/l
0.3
ND
10/10/92
EA
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
EPA
502.2
ug/1
0.6
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
0.5
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
EPA
502.2
ug/l
3.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Signed

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
.L5/92 -
l
--- Project Information ---
Lab Number : 92-3769-03
Project No. : 2490449203 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: BOB MACPHEE
Station ID : MW-3
Matrix : W
Type : GRAB
Collector : JA
--- Sample Information ---
Sampled Date/Time
: 09/30/92 14:30
Received Date/Time
: 10/01/92 14:45
Received From/By
: JA/LD
Chain of Custody
: 15311
Number of Containers
: 10
Parameter .............................. Method.... Units DL........ Results... Test Date Anal
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
Chloride
Nitrogen, Ammonia
Nitrogen, Nitrate
Residue, Filterable (TDS)
Residue, Non Filterable (TSS)
EPA
415.1
mg/l
1.0
2.5
10/08/92
TH
EPA
325.3
mg/1
0.20
3.0
10/02/92
JR
EPA
350.1
mg/1
0.030
ND
10/02/92
ORF
EPA
353.2
mg/1
0.050
0.15
10/02/92
ORF
EPA
160.1
mg/1
10
52
10/12/92
ORF
EPA
160.2
mg/1
10
2900
10/07/92
ORF
-- METALS ANALYSIS
- METALS PREP RESULTS --
Barium, Total
EPA
6010
Mercury, Total
EPA
7470
Arsenic, Total
EPA
7060
Cadmium, Total
EPA
7131
Chromium, Total
EPA
7191
Lead, Total
EPA
7421
Selenium, Total
EPA
7740
Silver, Total
EPA
7761
--- SERIES 35000
Total Metals Prep: Aqueous ICP
Total Metals Prep: Aqueous Furnace
Total Metals Prep: Aqueous, Hg
-- GC ORGANIC ANALYSIS RESULTS --
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
trans-1,2-Dichloroethene
Remarks:
mg/l
0.0089
0.017
10/12/92
JST
mg/1
0.00022
ND
10/13/92
HH
mg/1
0.0017
ND
10/08/92
DF
mg/l
0.0011
ND
10/08/92
DF
mg/1
0.0026
ND
10/09/92
DF
mg/1
0.0028
ND
10/08/92
DF
mg/1
0.0021
ND
10/08/92
DF
mg/l
0.0014
ND
10/12/92
DF
EPA
3010
N/A
10/07/92
HH
EPA
3020
N/A
10/07/92
HH
EPA
7470
N/A
10/12/92
HH
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
EPA
502.2
ug/1
0.6
ND
10/10/92
EA
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry weigh
Signed L. I `�( z

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
/15/92
2
Lab Number : 92-3769-03
Project No. : 2490449203
Parameter .............................. Method.... Units DL........ Results... Test. Date Analv
-- GC ORGANIC ANALYSIS RESULTS --
1,1-Dichloroethane
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
cis-1,2-Dichloroethene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Chloroform
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
Bromochloromethane
EPA
502.2
ug/l
0.3
ND
10/10/92
EA
1,1,1-Trichloroethane
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
1,1-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Carbon Tetrachloride
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Benzene
EPA
502.2
ug/1
0.2
ND
10/10/92
EA
1,2-Dichloroethane
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Trichloroethene
EPA
502.2
ug/l
0.6
ND
10/10/92
EA
1,2-Dichloropropane
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
Bromodichloromethane
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Dibromomethane
EPA
502.2
ug/l
0.6
ND
10/10/92
EA
cis-1,3-Dichloropropene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Toluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
trans-1,2-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,1,2-Trichloroethene
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Tetrachloroethene
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
1,3-Dichloropropane
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
Dibromochloromethane
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
1,2-Dibromoethane
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
Ethylbenzene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
Xylene, Total
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Styrene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
Isopropylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromoform
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
1,2,3-Trichloropropane
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
n-Propylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromobenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,3,5-Trimethylbenzene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
2-Chlorotoluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
4-Chlorotoluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
tert-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
sec-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
p-Isopropyltoluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,3-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
1,4-Dichlorobenzene
EPA
502.2
ug/l
0.3
ND
10/10/92
EA
n-Butylbenzene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
1,2-Dichlorobenzene
EPA
502.2
ug/l
0.3
ND
10/10/92
EA
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/l
3.0
ND
10/10/92
EA
1,2,4-Trichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Hexachlorobutadiene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Naphthalene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Signed'r��e .01

LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST DATA REPORT
/15/92
1
-- Project Information ---
Lab Number : 92-3769-04
Project No. : 2490449203 Cust. No.
Project Name : METROPOLITAN SEWERAGE DISTRICT
Manager: BOB MACPHEE
--- Sample Information ---
Station ID : BAILER RINSE Sampled Date/Time : 09/29/92 14:45
Matrix : W Received Date/Time : 10/01/92 14:45
Type : GRAB Received From/By : JA/LD
Collector : JA Chain of Custody : 15311
Number of Containers : 4
Parameter .............................. Method.... Units DL........ Results... Test Date Anal!
-- METALS ANALYSIS - METALS PREP RESULTS
--
Barium, Total
EPA
6010
mg/1
0.0089
ND
10/12/92
JST
Chromium, Total
EPA
7191
mg/l
0.0026
ND
10/09/92
DF
Lead, Total
EPA
7421
mg/1
0.0028
ND
10/08/92
DF
--- SERIES 35000
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
10/07/92
HH
Total Metals Prep: Aqueous Furnace
EPA
3020
N/A
10/07/92
HH
-- GC ORGANIC ANALYSIS RESULTS --
Chloromethane
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
Vinyl Chloride
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromomethane
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
Chloroethane
EPA
502.2
ug/l
5.0
ND
10/10/92
EA
Trichlorofluoromethane
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
1,1-Dichloroethene
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Methylene Chloride
EPA
502.2
ug/1
5.0
ND
10/10/92
EA
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.6
ND
10/10/92
EA
1,1-Dichloroethane
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
cis-1,2-Dichloroethene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Chloroform
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
Bromochloromethane
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
1,1,1-Trichloroethane
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,1-Dichloropropene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Carbon Tetrachloride
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Benzene
EPA
502.2
ug/1
0.2
ND
10/10/92
EA
1,2-Dichloroethane
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
Trichloroethene
EPA
502.2
ug/l
0.6
ND
10/10/92
EA
1,2-Dichloropropane
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
Bromodichloromethane
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
Dibromomethane
EPA
502.2
ug/1
0.6
ND
10/10/92
EA
cis-1,3-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Remarks:
DL = Detection Limit ND = Not Detected at the DL
Unless otherwise noted, all soil test results are calculated based on dry w ght.
Signed Z / `"t'

LAW ENVIRONMENTAL NATIONAL LABORATORIES
\ TEST DATA REPORT
15/92
2
Lab Number s 92-3769-04
Project No. n 2490449203
Parameter .............................. Method.... Units DL........ Results... Test Date Analy
-- GC ORGANIC ANALYSIS RESULTS --
Toluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
trans-1,2-Dichloropropene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,1,2-Trichloroethane
EPA
502.2
ug/1
0.9
ND
10/10/92
EA
Tetrachloroethene
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
1,3-Dichloropropane
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
Dibromochloromethane
EPA
502.2
ug/l
0.9
ND
10/10/92
EA
1,2-Dibromoethane
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
Ethylbenzene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/l
2.0
ND
10/10/92
EA
Xylene, Total
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Styrene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
Isopropylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromoform
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/1
2.0
ND
10/10/92
EA
1,2,3-Trichloropropane
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
n-Propylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Bromobenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,3,5-Trimethylbenzene
EPA
502.2
ug/1
0.5
ND
10/10/92
EA
2-Chlorotoluene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
4-Chlorotoluene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
tert-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
sec-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
p-Isopropyltoluene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
1,3-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
1,4-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
n-Butylbenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,2-Dichlorobenzene
EPA
502.2
ug/1
0.3
ND
10/10/92
EA
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/1
3.0
ND
10/10/92
EA
1,2,4-Trichlorobenzene
EPA
502.2
ug/l
1.0
ND
10/10/92
EA
Hexachlorobutadiene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Naphthalene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
1.0
ND
10/10/92
EA
Signed Z a

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ENGINEERS,
LABORATORY SERVICES
& SEWER DESIGN RoGms &-C 'uCO' 1 T
ES MONITORING
�STRIAL WASTES ENGINEERS. ice' WATER ANALYSIS
.:ANTS & PERMITS P.O. Box 5655. Greenville. SC 29606 MONITORING WELL ANALYSIS
HAZARDOUS WASTES Phone [phone] • FAX[phone] TREATABILITY STUDIES
SUBDIVISIONS TCLP ANALYSIS
RECREATIONAL FACILITIES SAMPLING & PICK-UP
LABORATORY SERVICES:
CLIENT: LAW ENGINEERING
ATTENTION: BOB MCPHEE �--.
4 INTERCHANGE BLVD . 'pP�
GREENVILLE, SC 29607�'.,
DATE RECEIVED: 09/30/1992
DATE REPORTED: 10/06/1992
S.C. LABORATORY IDENTIFICATION NUMBER 23105
SAMPLE NUMBER
22465
22466
22467
PARAMETER
TOTAL COLIFORM
(COLONIES/100 mL)
NON-COLIFORM GROWTH
(COLONIES/100 mL)
SAMPLE DESCRIPTION
MSD (JOB # 2490449203)
MW-2R GRAB ON 09/30/92 AT 12:00
MW-1 GRAB ON 09/30/92 AT 14:50
MW-3 GRAB ON 09/30/92 AT 14:30
RESULT
22465 22466
0* 5
12 78
22467
0*
TNTC
*RESULT MAY BE INACCURATE DUE TO THE HIGH SEDIMENT CONTENT OF THE SAMPLE
TNTC = TOO NUMEROUS TO COUNT
REPORTED BY:
ORIGMA1,ME f

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i'
COMMONWEALTH LABORATORIES OF S.C.,
INCORPORATED
P. O. BOX 16387
209 WEST ANTRIM DRIVE
GREENVILLE, SOUTH CAROLINA 29606-6387
CERTIFICATE OF ANALYSIS
October 8, 1992
Law Engineering
F
AREA CODE 803
TELEPHONE: [phone]
FAX: [phone]
Four Interchange Blvd. ;ram
Greenville, SC 29607 s`
Attn: Bob McPhee
One sample was received on September 30, 1992 for the following
analysis:
Sample
ID No.
Parameter 92-50-5633 Date Analyst Time
Total Coliform, MPN 4 * 1011/92 AS 0800
Sample markings
Location: MW-2R (MSD)
Date: 9/30/92
Time: 1200
Collected by: J. Allison
Type sample: Grab
Methodology is 16th and 17th Edition Standard Methods and/or EPA.
Holding times comply with 40 CFR Part 136.
*Sample was extremely turbid. <2 colonies for Fecal.
Program Area: Drinking Water
South Carolina Lab Identification No. 23101
North Carolina Certification No. 24
Outside Laboratory Certification No. 10120
Respectfull,Y submitted,
Cheryl F. Somrngrs
Laboratory Manager

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1J. 2G736
'PORTED BY
MCKED BY
3VIEW1D BY
AMPLE TYPE: WATER
n
BHNR/DBM LABORATORY
VOLATILE ANALYTICAL REPORT
SUPERVISOr
DATE
ENTERED BY
CHECKED BY
ANALYSIS RESULTS
CASE VOA TARGET COMPOUND TQL DETECTED
uo/l uQ/1
75-35-4
1,1-Dichloroethene
0.75
0.25
75-09-2
156-60-5
Methylene Chloride
trans-1,2-Dichloroethene
00.75
75-34-3
1,1-Dichloroethane
0 25
590-20-7
156-59-4
2,2-Dichloropropane
cis-1,2-Dichloroethene
0.25
67-66-3
Chloroform
0 75
74-97-5
Bromochloromethane
0 25
71-55.6
1,1,1-Trichloroethane
0 25
563-58.6
1,1-Dichloropropene
0 75
56-23-5
Carbon Tetrachloride
0 25
107-06-2
1,2-Dichloroethane
0 25
79-01-6
Trichloroethene
0 25
78-87-5
1,2-Dichloropropane
0.25
75-27-4
Bromodichloromethane
1
14.95-3
Dibromomethane
0.25
71V061-01-5
cis-1,3-Dichloropropene
10061-02-6
trans-1,3-Dichloropropene
0.25
25
79-00-5
1,1,2-Trichloroethane
0 25
127-18-4
Tetrachloroethene
0.25
142-28-9
1,3-Dichloropropane
015
124-48.1
Dibromochloromethane
,1
106-93-4
1,2-Dibromoethane
0 25
108-90-7
630-20-6
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.25
75-25-2 Bromoform
79-34-5 1,1,2,2-Tetrachloroethane
0.75
116
TQL- Target Quantation Limit- Subject to
change due to instrument sensitivity
T. Tentatively Identified, not confirmed
B- Estimated Value
U- Samples analyzed for this compound but
not detected
N- Sample not analyzed for this compound
D- Detected below quantitation limit
M- GC/MS Analysis performed
-'nMNBNTS:
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
CAS$ VOA TARGET COMPOUND TQL DETECTEDaa u9/1
96-18=4 1,2,3-Trichloropropane
108-86-1 Bromobenzene.
95-49.8 2-Chlorotoluene
106-43-4 4-Chlorotoluene
541-73-1 1,3-Dichlorobenzene
106-46-7 1,4-Dichlorobenzene
95-50-1 1,2-Dichlorobenzene
96-12.8 1,2-Dibromo-3-Chloropropane
120.82-1 1,2,4-Trichlorobenzene
87-68-3 Hexachlorobutadiene
87-61-6 1,2,3-Trichlorobenzene
1634.04-4 Methyl-tert-butyl ether
71-43-2 Benzene
108-88-3 Toluene
100-41-4 Ethyl benzene
108-38-3 m,p-lYlenes
95-47.6 o-xylene
100-42-5 Styrene
98-82-8 Isopropylbenzene
103-65-1 n-Propylbenzene
108-61-8 1,3,5-Trimethylbenzene
98-06-6 tert-Butylbenzene
95-63.6 1,2,4-Trimethylbenzene
135-98-8 sec-Butylbenzene
99-87-6 p-isopropyltoluene
104-51-8 n-Butylbenzene
91-20-3 Naphthalene
Other purgeables detected
(up to 10 highest peaks)
0.25
1
0.25
0.25
0.25
0.25
0.25
1
0.25
0.25
0.75
1
1
I
1
1
1
1
1
1
El
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Detected
ug/l

SLMIVOLATILE ORGANICS REPORT--,- DEM LAB
LAB NUMBER:2G736 SUPERVISOR-&L LAB #:2G736
DATE �---
REPORTED BY
CHECKED BY ENTERED BY Sit -
REVIEWED BY CHECKED BY,T�S _
SAMPLE TYPE: WATER DILUTION FACTOR
CAS NUMBER
TOL
ANALYTE NAME
X 1
108-95-2
10
PHENOL
111-44-4
10
BIS(2-CHLOROETHYL) ETHER
95-57-8
10
2-CHLOROPHENOL
541-73-1
10
1,3-DICHLOROBENZENE
106-46-7
10
1,4-DICHLOROBENZENE
100-51-6
20
BENZYL ALCOHOL
95-50-1
10
1,2-DICHLOROBENZENE
95-48-7
10
2-METHYL PHENOL
108-60-1
10
BIS(2-CHLOROISOPROPYL) ETHER
106-44-5
10
4-METHYL PHENOL
621-64-7
10
N-NITROSO-DI-N-PROPYLAMINE
67-72-1
10
HEXACHLOROETHANE
98-95-3
10
NITROBENZENE
78-59-1
10
ISOPHORONE
88-75-5
10
2-NITRO PHENOL
105-67-9
10
2,4-DIMETHYL PHENOL
65-85-0
50
BENZOIC ACID
111-91-1
10
BIS(2-CHLOROETHOXY) METHANE
120-83-2
10
2.4-DICHLORO PHENOL
120-82-1
10
1.2,4-TRICHLOROBENZENE
91-20-3
10
NAPHTHALENE
106-47-8
20
4-CHLOROANILINE
87-68-3
10
HEXACHLOROBUTADIENE
59-50-7
20
4-CHLORO-3-METHYL PHENOL
91-57-6
10
2-METHYL NAPHTHALENE
77-47-4
10
HEXACHLOROCYCLOPENTADIENE
88-06-2
10
2,4,6-TRICHLORO PHENOL
95-95-4
10
2,.4.5-TRICHLORO PHENOL
91-58-7
10
2-CHLORO NAPHTHALENE
88-74-4
50
2-NITROANALINE
131-11-3
10
DIMETHYL PHTHALATE
208-96-8
10
ACENAPHTHYLENE
606-20-2
10
2,6-DINITROTOLUENE
99-09-2
50
3-NITROANALINE
83-32-9
10
ACENAPHTHENE
51-28-5
50
2.4-DINITRO PHENOL
100-02-7
50
4-NITRO PHENOL
132-64-9
10
DIBENZOFURAN
121-14-2
10
2,4-DINITROTOLUENE
84-66-2
10
DIETHYL PHTHALATE
7005-72-3
10
4-CHLOROPHENYL PHENYL ETHER
86-73-7
10
FLUORENE
100-01-6
50
4-NITROANALINE
534-52-1
50
4,6-DINITRO-2-METHYL PHENOL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
CONC.
UG/L

LV_L� t1:Y�3Li L+Ulii'vii21�i3i JlY L1!`111
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U= COMPOUND ANALYZED FOR. NOT DETECTED
N= COMPOUND NOT ANALYZED FOR
D= DETECTED BELOW QUANTITATION LIMIT
H= HOLDING 'DIME EXCEEDED
TQL SUBJECT TO CHANGE DUE TO INSTRUMENT SENSITIVITY

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COMMONWEALTH LABORATORIES OF. S.C.,
INCORPORATED o✓
P. O. BOX 16387
209 WEST ANTRIM DRIVE
GREENVILLE, SOUTH CAROLINA 29606-6387 AREA CODE 803
y TELEPHONE:[phone]
AFAX-.803-235-8340
CERTIFICATE OF ANALYSIS
Page
Law Engineering/
Air Products
Sample
. No.
Parameter IID D No.
Date Analyst Time
Total Coliform, MF/lOOmis O ***
6/30/92 CK 1650
A �{
Sample Markings
Location: MW-2R
Date: 6/30/92
Time: 1430
Collected by: Dudney Fox
Type sample: Grab
***Heavy non-coliform growth.
South Carolina Lab Identification No. 23101
North Carolina Certification No. 24
Outside Laboratory Certification No. 10120

� )LAW ENVIRONMENTAL NATIONAL LA( TORIES
TEST DATA REPORT
j7/17/92
1
--- Project Information ---
Lab Number : 92-3021-03
Project No. : 2490444501 Cust. No.
Project Name : MSD
Manager: BOB MACPHEE
--- Sample Information ---
Station ID : MW-2R Sampled Date/Time : 06/30/92 14:30
Matrix : W Received Date/Time : 07/01/92 11:45
Type : GRAB Received From/By : JA/LD
Collector : JA Chain of Custody : 13537
Number of Containers : 8
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units PQL....... Results... Test Date Anal
-- INORGANIC CHEMISTRY RESULTS --
Carbon, Total Organic (TOC)
EPA
415.1
mg/1
Chloride
EPA
325.3
mg/l
Nitrogen, Ammonia
EPA
350.1
mg/1
Nitrogen, Nitrate
EPA
353.2
mg/1
Residue, Filterable (TDS)
EPA
160.1
mg/1
Residue, Non Filterable (TSS)
EPA
160.2
mg/1
-- METALS ANALYSIS
- METALS PREP RESULTS --
Barium, Total
EPA
6010
Mercury, Total
EPA
7470
Arsenic, Total
EPA
7060
Cadmium, Total
EPA
7131
Chromium, Total
EPA
7191
Lead, Total
EPA
7421
Selenium, Total
EPA
7740
Silver, Total
EPA
7761
--- SERIES 35000
Total Metals Prep: Aqueous ICP
Total Metals Prep: Aqueous Furnace
Total Metals Prep: Aqueous, Hg
-- GC ORGANIC ANALYSIS RESULTS --
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1.0
7.0
07/07/92
TH
0.20
8.6
07/07/92
BC
0.030
0.27
07/01/92
BC
0.050
6.5
07/06/92
ORF
10
260
07/16/92
TH
10
6300
07/15/92
TH
mg/l
0.10
0.11
07/08/92
JST
mg/1
0.0005
ND
07/08/92
HH
mg/1
0.005
ND
07/07/92
KE
mg/l
0.002
ND
07/08/92
LB
mg/l
0.005
ND
07/08/92
LB
mg/l
0.005
ND
07/09/92
LB
mg/1
0.005
ND
07/07/92
KE
mg/1
0.01
ND
07/08/92
LB
EPA
3010
N/A
07/06/92
CW
EPA
3020
N/A
07/06/92
CW
EPA
7470
N/A
07/07/92
HH
EPA
502.2
ug/1
0.5
ND
07/08/92
AMS
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
/ i� /
Signed iya.� ef

//17/92
2
Lab Number : 92-3021-03
Project No. : 2490444501
SLAW ENVIRONMENTAL NATIONAL LABJTORIES
TEST DATA REPORT
--- Test Data ---
Parameter .............................. Method.... Units PQL....... Results... Test Date Analy
-- GC ORGANIC ANALYSIS RESULTS --
1,1-Dichloroethene
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
Methylene Chloride
EPA
502.2
ug/1
2.5
ND
07/08/92
AMS
trans-1,2-Dichloroethene
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
1,1-Dichloroethane
EPA
502.2
ug/l
0.1
ND
07/08/92
AMS
cis-1,2-Dichloroethene
EPA
502.2
ug/l
0.3
ND
07/08/92
AMS
Chloroform
EPA
502.2
ug/1
0.2
0.97
07/08/92
AMS
Bromochloromethane
EPA
502.2
ug/1
0.3
ND
07/08/92
AMS
1,1,1-Trichloroethane
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
1,1-Dichloropropene
EPA
502.2
ug/l
0.2
ND
07/08/92
AMS
Carbon Tetrachloride
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
Benzene
EPA
502.2
ug/l
0.13
ND
07/08/92
AMS
1,2-Dichloroethane
EPA
502.2
ug/l
0.2
ND
07/08/92
AMS
Trichloroethene
EPA
502.2
ug/1
0.2`�'
ND
07/08/92
AMS
1,2-Dichloropropane
EPA
502.2
ug/l
0.2
ND
07/08/92
AMS
Bromodichloromethane
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
Dibromomethane
EPA
502.2
ug/l
0.2
ND
07/08/92
AMS
cis-1,3-Dichloropropene
EPA
502.2
ug/1
0.3
ND
07/08/92
AMS
Toluene
EPA
502.2
ug/1
0.13
ND
07/08/92
AMS
trans-1,2-Dichloropropene
EPA
502.2
ug/l
0.3
ND
07/08/92
AMS
1,1,2-Trichloroethane
EPA
502.2
ug/l
0.2
ND
07/08/92
AMS
Tetrachloroethene
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
1,3-Dichloropropane
EPA
502.2
ug/l
0.1
ND
07/08/92
AMS
Dibromochloromethane
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
1,2-Dibromoethane
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
Ethylbenzene
EPA
502.2
ug/l
0.14
ND
07/08/92
AMS
1,1,1,2-Tetrachloroethane
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
Xylene, Total
EPA
502.2
ug/1
0.44
ND
07/08/92
AMS
Styrene
EPA
502.2
ug/l
0.17
ND
07/08/92
AMS
Isopropylbenzene
EPA
502.2
ug/1
0.13
ND
07/08/92
AMS
Bromoform
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
1,1,2,2-Tetrachloroethane
EPA
502.2
ug/1
0.4
ND
07/08/92
AMS
1,2,3-Trichloropropane
EPA
502.2
ug/1
0.2
ND
07/08/92
AMS
n-Propylbenzene
EPA
502.2
ug/1
0.14
ND
07/08/92
AMS
Bromobenzene
EPA
502.2
ug/1
0.13
ND
07/08/92
AMS
1,3,5-Trimethylbenzene
EPA
502.2
ug/1
0.25
ND
07/08/92
AMS
2-Chlorotoluene
EPA
502.2
ug/1
0.1
ND
07/08/92
AMS
4-Chlorotoluene
EPA
502.2
ug/l
0.1
ND
07/08/92
AMS
tert-Butylbenzene
EPA
502.2
ug/1
0.16
ND
07/08/92
AMS
sec-Butylbenzene
EPA
502.2
ug/1
0.17
ND
07/08/92
AMS
p-Isopropyltoluene
EPA
502.2
ug/l
0.14
ND
07/08/92
AMS
1,3-Dichlorobenzene
EPA
502.2
ug/1
0.15
ND
07/08/92
AMS
1,4-Dichlorobenzene
EPA
502.2
ug/1
0.49
ND
07/08/92
AMS
n-Butylbenzene
EPA
502.2
ug/l
0.38
ND
07/08/92
AMS
1,2-Dichlorobenzene
EPA
502.2
ug/1
0.13
ND
07/08/92
AMS
Signed [_ -- / 9.-

LAW ENVIRONMENTAL NATIONAL LAP^^ATORIES
� TEST DATA REPORT l
/17/92
3
Lab Number : 92-3021-03
Project No. : 2490444501
- Test Data ---
Parameter .............................. Method.... Units PQL....... Results... Test Date Analy
-- GC ORGANIC ANALYSIS RESULTS --
1,2-Dibromo-3-Chloropropane
EPA
502.2
ug/l
1.0
ND
07/08/92
AMS
1,2,4-Trichlorobenzene
EPA
502.2
ug/l
0.14
ND
07/08/92
AMS
Hexachlorobutadiene
EPA
502.2
ug/l
0.64
ND
07/08/92
AMS
Naphthalene
EPA
502.2
ug/1
0.72
ND
07/08/92
AMS
1,2,3-Trichlorobenzene
EPA
502.2
ug/1
0.32
ND
07/08/92
AMS
Signed

s Department of Environrr' '\ Health, and Natural Resources
&ion of Environmental Manage _ant - Groundwater Section
P.O. Box 29535 - Raleigh, N.C. 27626-0535
Phone [phone]
WELL CONSTRUCTION RECORD
FOR OFFICE USE ONLY � �-
QUAD. NO. M d�' "I j «5.. SERIAL NO. �,/
Lat. 3 5- .3 5' 1/ ~Long. � '. i Pc
Minor Basin
Basin Code
DRILLING CONTRACTOR: Metro Drill Inc. Header Ent. GW-1 Ent
STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER: NC 1282 PERAfAIIT41UERi - -1�2
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Asheville County:
(Road, Community, or Subdivision and Lot No.)
f i
DEPTH
2.
OWNER Metropolitan Sewerage District
From To
ADDRESS 2225 Riverside Drive, P. 0. Box 8969
0 - 2
(Street or Route No.)
Asheville, North Carolina 28814
City or Town State Zip Code
2 4
3.
DATE DRILLED June 24, 1992LJSE OF WELL Monitoring
4.
TOTAL DEPTH 17.0
5.
CUTTINGS COLLECTED YES []X IN OF--]
6.
DOES WELL REPLACE EXISTING WELL? YES OX NOF ]
4 - 8.5
7.
STATIC WATER LEVEL Below Top of Casing: 8.5 FT.
(Use "+" if Above Top of Casing)
8.
TOP OF CASING IS 2.5 FT. Above Land Surface"
8 - 17.5
• Casing Terminated at/or below land surface is illegal unless a variance is issued
In
accordance with 15A NCAC 2C .0118
9.
YIELD (gpm): N/A METHOD OF TEST N/A
10.
WATER ZONES (depth): 7 - 10 feet
41
i
"li j
DRILLING
Formation Description
Gray to brown v, micaceous
Silty fine sand with rubble
Fill - Trash
Dark gray to black very
micaceous silty fine sand
aithr gravel and trash
Gray very micaceous silt
with weathered rock
fragments — Residuum
Orange to brown very micaceous
fine to medium sandy silt
11. CHLORINATION: Type NSA Amount N/ If additional space is needed use back of form
12. CASING:
Depth
From 0 To -
From To -
From To -
13. GROUT:
Wall Thickness
Diameter or Weight/Ft. Material
7 Ft.
— Ft. s�
— Ft.
Depth
From 0 To 3.5
From To
14. SCREEN:
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
° Iss?
Depth Diameter Slot Size Material
From 7 To 17 Ft 2.0 in. .01 in. PVC GR�� � +I
From To Ft. in. in.
From To Ft. in. in.
15. SAND/GRAVEL PACK:
Depth Size Material
From 4.5 To 17 Ft.
From To Ft.
16. REMARKS: To monitor ash/sludge disposal lagoon
Material Method
Ft. Grout Tremmie
Ft.
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
SIGNATURE OF CONTRACTOR OR AGENT DATE
GW-1 REV. 5/91 Submit original to Division of Environmental Management and copy to well owner.

A?-
DEPAFTMMP—F NATURAL RESOURCES AND COMUN7- DEVELOPMENT
,41SIOjq OF MIROMWYrAL HANAGEi--ij
WELL AND PUMP INSPECTION REPORT
Date /0
Area
Well location /'l ,7 1/"4'- V 4- Lot No*)
(Town, Subdivision and County
71��`, Ael --'l Road/Street
Owner
Address Quad No
A 7
4-:- Al Serial No.
Lat. Long.
WELL CONSTRUCTION
Drilling Contractor. ILA VV Name Address Reg. #
Permit
Location
Distance from
Pollution source
Other location standards
Total Depth
Casin
Depth
Diameter
Weight/thickness
Height
Drive shoe
Exception approved by owner
Grout:
Type
Thickness
Depth
Meets min. Standards
Measure Yes No
6 ""6 L5
'7— id,
Screens
Development
1. D. Plate
Abandonment (temporary/pe n e nt
Water level 7. d
Well test
Chlorination
Cuttings
Reports
Water samp e (appearance)
Remarks

WELL HEAD COMPLETION
Pun,; i:s to Iit: r
Na E, Add re.ss
Meets Min. Standards
Measure Yes No
Enclosure
Enclosure floor
Casing height
Access port
Valved flow `
Water tight pipe entry
Well entry
Vent
Nose bib
Tee {jet)
Suc t ion line
Chlorination
Temporary Aband.
Date Well Constructed (re ,j %2—
Date Puma Installed
Signature
Witness
Name Address Tyke
Name Address Type
WEAVE
PS N q
WFAVErTPLI-E V11OF'OUTAN 1
P5 NU. 2 AS«WA14n
1 �AlMEN'j
P AN1
Mw-3 cn
p
It f6.
:4v Is 5�Irr�, i'.J+RPIEc p y'te:=-•. ' %15 ^, /✓'`'"� \�
Q. M <AGoe� A"I_
Ij
C
�)At

i
WELL NO.: M87j5
MSD
COUNTY: BUNCOMBE
DATE SAMPLED
ALKALINITY,TO pH 4.5
ALKALINITY,TO pH 8.3
ALUMINUM
ARSENIC
O. oo.53
BARIUM
p,3
BERYLLIUM
BICARBONATE
CADMIUM
CALCIUM
CARBONATE
CHLORIDE
i3
CHROMIUM,TOTAL
p OQ , -
COBALT
COD
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
CYANIDE
DISSOLVED SOLIDS
3 (�
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
-
LEAD
0.010
LITHIUM
M BAS
MAGNESIUM
MANGANESE
MERCURY
�, 000
NICKEL
NITROGEN, AMMONIA
NITROGEN, KJELDAHL
NITRATE & NITRITE
ORGANIC SCAN
ORTHOPHOSPHATE
pH
6. 06
PHENOLS
PHOSPHORUS, TOTAL
POTASSIUM
SELENIUM
p rjpy
SILVER
SODIUM
SPECIF. CONDUCTANCE
SULFATE
TOC (UNFILTERED)
TOX
� p_
——f-
�—
TSS
--
--
VOC
ZINC
--
-
-
STATIC WATER LEVEL
Red Ink=Sample taken by facility
`7— ciirv', c, A1v OveRsfrNT 'Vac s r vER—C- No-r
7//S�o3 ,SA MPL i we it e_ ► .

- mw'�7pz
WELL NO.: M87j5 MSO COUNTY: BUNCOMBE
DATE SAMPLED
03
ALUMINUM
BERYLLIUM
--
BICARBONATE
CALCIUM
CARBONATE
COBALT
COD
COLIFORM, FECAL
COLIFORM, TOTAL
COPPER
CYANIDE
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LITHIUM
MBAS
MAGNESIUM
MANGANESE
NICKEL
NITROGEN, KJELDAHL
NITRATE & NITRITE
fio-4
ORGANIC SCAN
ORTHOPHOSPHATE
pH
6,97
PHENOLS
PHOSPHORUS, TOTAL
o
POTASSIU
SODIUM
SULFATE
TOX
TSS
ZINC
,STATIC WATER LEVEL
Red |nk=Smnmphotaken byfacility

g¢� x
WELL NO. _-Mg 7 � 4j� COUNTY; 9"NC Ci C—
DATE SAMPLED
��..��- 9i
.. g- !�
00
%- j0- oo
10,
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
0. j
0. 0.'
z 0. 0 1
BARIUM
0,090
0. 0 88.E
0 , 0 66
0. 0 "i7&
c,?
o q o
BERYLLIUM
BICARBONATE
CADMIUM
0. 00A
c 0. 0 S
0, 0o-36'
0.00-2
� �����:�
, 0011
CALCIUM
CARBONATE
CHLORIDE
S
3%. ,�
f 0
f
J3
CHROMIUM, TOTAL
0. U
0. o I o
> o . oo rE
COBALT
!COD
COLIFORM, FECAL
<
jo
COLIFORM, TOTAL
3
/ , /
j
i
> �2 3
COPPER
CYANIDE
DISSOLVED SOLIDS
600
(a ��'
-"go' 0
sg0
�' o
& vO
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
0 s 0 1
-Z 0, 00t0
t a- 003
� 0, 01
co
LITHIUM
Red Ink = Sample taken by facility

WELL NO. / 4 9 / J S-
COUNTY: q cz1y c o m o g
DATE SAMPLED
f - Y 9 ✓
-'4- i 1
Y- 00
7- /d - 00
'%- e '
4 • ®1
MBAS
MAGNESIUM
MANGANESE
MERCURY
c C 0oog
c e?. a ��e
�.� a e
c7aU 3j
<z=.Cj',e;46,
NICKEL
NITROGEN, AMMONIA
/
0 . `76
0,
0,71
NITROGEN, KJELDAHL
NITRATE & NITRITE
�0
67
a0 . o
ORGANIC SCAN
pH
tom,
PHENOLS
PHOSPHORUS, TOTAL
D . o
POTASSIUM
SELENIUM
00
0- ico
v010
4 b. 0 0-5
SILVER
< b. On
° C i� o
0 • oo.a
c 0. Go- r
4 C .
SODIUM
SPECIE. CONDUCTANCE
SULFATE
TOC (UNFILTERED)
TOX
TSS
ZINC
STATIC WATER LEVEL
��
! J
7
Red Ink = Sample taken by facility

tvi
WELL NO. ` COUNTY: /°�i �� 9`� ✓a
DATE SAMPLED
% / y
S.. / - y;r
- r®1- 98
Ll
ALKALINITY, TO pH 4.5
ALKALINITY, TO pH 8.3
ALUMINUM
ARSENIC
X. 0. 0 "� e; 0
4 o � �'s �
z. i o
< o. ®.;1 .ti v
0. 0'4.s o
BARIUM
0, 0600
0 � 120
0 , 0,6
o. i & 6
o, 10.3
BERYLLIUM
BICARBONATE
CADMIUM
00J-40
a oo-;
a d. 00 0-
0. ooSFoc.
CALCIUM
CARBONATE
CHLORIDE
CHROMIUM, TOTAL
4 0 o f CIO
0/0,0
0 g 004
0. 0i00
COBALT
COD
COLIFORM, FECAL
. f
COLIFORM, TOTAL
®,
- ®9 vi
d
COPPER
CYANIDE
DISSOLVED SOLIDS
1-0
,
300
/
.2 S ;'
FLUORIDE
HARDNESS CaCo3
HARDNESS, NON CARB
IRON
LEAD
C>, v ir3
v. D'oid'�
zfa.�c5"ti@
LITHIUM
Red Ink = Sample taken by facility

WELL NO. M F 7 � -�- COUNTY:
c of i e f
DATE SAMPLED
7-11- 97
S-_ie_ g %
MBAS
MAGNESIUM
MANGANESE
MERCURY
` 0, 000do
NICKEL
NITROGEN, AMMONIA
NITROGEN, KJELDAHL
NITRATE & NITRITE
Arm ,$
N� 9 1
`
� �
v
ORGANIC SCAN
pH
To
�:�
�.�vS
6.7
(vG
6,.-70
PHENOLS
PHOSPHORUS, TOTAL
®°
POTASSIUM
SELENIUM
, y' c>
e. o. ioo
0. 00-5
.� fir, )00
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SILVER
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0,01.50
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15111
SODIUM
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73
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TOX
TSS
VOC
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ZINC
STATIC WATER LEVEL
07
6, 7
S.,31
("
Red Ink = Sample taken by facility

y s
WELL NO.
UA1'E SANPLrD
.3
A-LVAL1NITY, 'TO T,H 4.5
AI.I.ALINITY, TO TRH 8.3
A I TIM 114111
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BATE SAMPLER
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ORGANIC SCAN
pH
6.3
PHENOLS
PHOSPHORUS, TOTAL
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WELL NO.: M87j5
DATE SAMPLED r o
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MSD
COUNTY: BUNCOMBE

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I'D

ace Anal ytical l°
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9249176
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 923251102
Project Sample Number: 9249176.002
Date Collected: 08/15/03 12:10
Client Sample ID: MW 2R
Matrix: Water
Date Received: 08/15/03 14:05
Parameters
Results
Units Report Limit Analyzed By
CAS No. Qual RegLmt
Field Services
Monitoring Well Data
Method:
Static Water Level
4.65
08/15/03 MPS
Well Volume Purged
6.25
08/15/03 MPS
GC Volatiles
GC VOCS in Water
Method: SM
6230D
ND
ug/l
0.50
08/16/03
01:07 STC
71-43-2
Benzene
Bromobenzene
ND
ug/l
0.50
08/16/03
01:07
STC
108-86-1
Bromochloromethane
NO
ug/1
0.50
08/16/03
01:07
STC
74-97-5
Bromodichloromethane
ND
ug/1
0.50
08/16/03
01:07
STC
75-27-4
Bromoform
ND
ug/l
0,50
08/16/03
01:07
STC
75-25-2
Bromomethane
ND
ug/l
0.50
08/16/03
01:07
STC
74-83-9
n-Butylbenzene
ND
ug/l
1.0
08/16/03
01:07
STC
104-51.8
sec-Butylbenzene
ND
ug/l
0.50
08/16/03
01:07
STC
135-98-8
tert-Butylbenzene
ND
ug/l
0.50
08/16/03
01:07
STC
98.06-6
Carbon tetrachloride
ND
ug/l
0.50
08/16/03
01:07
STC
56-23-5
Chlorobenzene
NO
ug/1
0.50
08/16/03
01:07
STC
108-90-7
Chloroethane
NO
ug/l
0.50
08/16/03
01:07
STC
75-00-3
Chloroform
ND
ug/l
0.50
08/16/03
01:07
STC
67-66-3
Chloromethane
ND
ug/l
2.0
08/16/03
01:07
STC
74-87-3
2-Chlorotoluene
ND
ug/l
0.50
08/16/03
01:07
STC
95-49-8
4-Chlorotoluene
ND
ug/1
0.50
08/16/03
01:07
STC
106.43-4
1,2-Dibromo-3-chloropropane
ND
ug/l
2.0
08/16/03
01:07
STC
96-12-8
Dibromochloromethane
ND
ug/l
0.50
08/16/03
01:07
STC
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/l
0.50
08/16/03
01:07
STC
106-93.4
Dibromomethane
ND
ug/l
0.50
08/16/03
01:07
STC
74-95-3
1,2-Dichlorobenzene
ND
ug/1
1.0
08/16/03
01:07
STC
95.50-1
1,3-Dichlorobenzene
ND
ug/l
1.0
08/16/03
01:07
STC
541-73-1
1,4-Dichlorobenzene
NO
ug/1
1.0
08/16/03
01:07
STC
106-46-7
Dichlorodifluoromethane
NO
ug/l
0.50
08/16/03
01:07
STC
75-71-8
1,1-Dichloroethane
NO
ug/l
0.50
08/16/03
01:07
STC
75-34-3
1,2-Dichloroethane
NO
ug/l
0.50
08/16/03
01:07
STC
107-06-2
1,1-Dichloroethene
ND
ug/l
0.50
08/16/03
01:07
STC
75.35-4
cis-1,2-Dichloroethene
ND
ug/1
0.50
08/16/03
01:07
STC
156-59-2
trans-1,2-Dichloroethene
NO
ug/l
0.50
08/16/03
01:07
STC
156.60-5
1,2-Dichloropropane
NO
ug/l
0.50
08/16/03
01:07
STC
78-87-5
1,3-Dichloropropane
ND
ug/l
0.50
08/16/03
01:07
STC
142-28-9
2,2-Dichloropropane
ND
ug/l
0.50
08/16/03
01:07
STC
594-20-7
Date: 08/25/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,a accoga
e° 4y
nelac
E C E � U
S E P _1 S 2 '33
GROUNDWATER SECTION
ASHEVILLE REGIONAL OFFICE
Page: 3 of 18
Charlotte Certification IDS
NC Wastewater 12
INC Drinking Water 37706
Sc 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 923251102
Client Sample ID: MW-2R
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9249176
Client Project ID: GROUNDWATER WELLS
Project Sample Number: 9249176-002 Date Collected: 08/15/03 12:10
Matrix: Water Date Received: 08/15/03 14:05
Results
Units
Report Limit
Analyzed By
CAS No. Qual RegLmt
Parameters
NO
ug/.l
0.50
08/16/03 01:07 STC
563-58.6
1,1-Dichloropropene
NO
ug/l
0.50
08/16/03 01:07 STC
10061.01-5
cis-1,3-Dichloropropene
NO
ug/l
0.50
08/16/03 01:07 STC
10061-02-6
trans-1,3-Dichloropropene
NO
ug/l
0.50
08/16/03 01:07 STC
108-20.3
Diisopropyl ether
ND
ug/l
0.50
08/16/03 01:07 STC
100-41-4
Ethylbenzene
ND
ug/l
2.0
08/16/03 01:07 STC
87-68-3
Hexachloro-1,3-butadiene
NO
ug/l
0.50
08/16/03 01:07 STC
98-82-8
Isopropylbenzene (Cumene)
ND
ug/l
1.0
08/16/03 01:07 STC
99-87-6
p-Isopropyltoluene
NO
ug/l
2.0
08/16/03 01:07 STC
75-09-2
Methylene chloride
Methyl-tert-butyl ether
NO
ug/l
0.50
08/16/03 01:07 STC
1634-04-4
Naphthalene
NO
ug/1
2.0
08/16/03 01:07 STC
91-20-3
n-Propylbenzene
NO
ug/l
0.50
08/16/03 01:07 STC
103-65-1
NO
ug/l
0.50
08/16/03 01:07 STC
100-42-5
Styrene
1,1,1,2-Tetrachloroethane
NO
ug/l
0.50
08/16/03 01:07 STC
630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/l
0.50
08/16/03 01:07 STC
79-34-5
Tetrachloroethene
NO
ug/l
0.50
08/16/03 01:07 STC
127-18-4
NO
ug/l
0.50
08/16/03 01:07 STC
108-88-3
Toluene
1,2,3-Trichlorobenzene
NO
ug/1
2.0
08/16/03 01:07 STC
87.61-6
1,2,4-Trichlorobenzene
ND
ug/1
2.0
08/16/03 01:07 STC
120-82-1
1,1,1-Trichloroethane
ND
ug/l
0.50
08/16/03 01:07 STC
71-55-6
1,1,2-Trichloroethane
NO
ug/1
0.50
08/16/03 01:07 STC
79-00.5
Trichloroethene
NO
ug/l
0.50
08/16/03 01:07 STC
79-01-6
Trichlorofluoromethane
NO
ug/l
0.50
08/16/03 01:07 STC
75-69.4
1,2,3-Trichloropropane
NO
ug/l
0.50
08/16/03 01:07 STC
96-18-4
1,2,4-Trimethylbenzene
NO
ug/l
0.50
08/16/03 01:07 STC
95-63.6
1,3,5-Trimethylbenzene
NO
ug/l
0.50
08/16/03 01:07 STC
108-67-8
Vinyl chloride
NO
ug/l
0.50
08/16/03 01:07 STC
75-01-4
m&p-Xylene
NO
ug/l
0.50
08/16/03 01:07 STC
NO
ug/1
0.50
08/16/03 01:07 STC
95-47-6
o-Xylene
1-Chloro-3-fluorobenzene (S)
98
%
08/16/03 01:07 STC
625-98-9
Date: 08/25/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCOgO,,
ti� c
nelac
GROUNDWATER SECTION
ASHEVILLE REGIONAL OFFICE
Page: 4 of 18
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

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Q

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923146070
Client Sample ID: MW-2R
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9247328
Client Project ID: GROUNDWATER WELLS
Project Sample Number: 9247328-002 Date Collected: 07/15/03 10:25
Matrix: Water Date Received: 07/15/03 10:50
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Field Services
Monitoring Well Data
Method:
Field pH
6.06
07/15/03
MPS
Field Specific Conductance
355
07/15/03
MPS
Field Temperature
18.8
07/15/03
MPS
Static Water Level
4.64
07/15/03
MPS
Microbiology
Total Coliform MPN Water
Method: SM 9223
Coliform, Total
2.2
07/15/03
ACL
Metals
3030C Metals, ICP, Trace
Prep/Method:
SM 3030C /
EPA 200.7
Arsenic, 3030C
0.0053
mg/l
0.0050
07/18/03
DJR
7440-38-2
Barium, 3030C
0.34
mg/l
0.0050
07/18/03
DJR
7440-39-3
Cadmium, 3030C
0.0016
mg/l
0.0010
07/18/03
DJR
7440-43-9
Chromium, 3030C
0.047
mg/1
0.0020
07/18/03
DJR
7440-47-3
Selenium, 3030C
NO
mg/l
0.0050
07/18/03
DJR
7782-49-2
Silver, 3030C
NO
mg/l
0.0020
07/18/03
DJR
7440-22.4
Date Digested
07/16/03
07/16/03
Lead, AAS Furnace, 3030C
Prep/Method:
SM 3030C /
EPA 239.2
Lead, 3030C
0.010
mg/l
0.0050
07/21/03
EWS
7439-92-1 1
Date Digested
07/16/03
07/16/03
Mercury, CVAAS, in Water
Method: EPA
245.1
Mercury
NO
mg/l
0.00020
07/23/03
LBG
7439-97-6
Wet Chemistry
Total Dissolved Solids
Method: EPA
160.1
Total Dissolved Solids
390
mg/1
20.
07/21/03
ACL
Chloride (Mercuric Nitrate)
Method: EPA
325.2
Chloride
13.
mg/l
1.0
07/18/03
DAW1
16887-00.6
Ammonia
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Date: 07/30/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Method: EPA 350.1
0.44 mg/l
Method: EPA 353.2
0.10 07/24/03 DAW1 7727-37-9
MD r �-- -Eon
p <0 3 3 of 23
I
a
EIS
REPORT OF LABORATORY ANALYST$
This report shall not be reproduced, except in full, Charlotte Certification IN
without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
N ACCO, NC Drinking Water 37706
`onel%- Sc 99006
a,C = FL NELAP E87627

Pace Analytical Services, Inc.
ace Anal ical � 2225 Riverside Drive
�/% Asheville, NC 28804
acelabs.com Phone:[phone]
www.pacelabs.com Fax:[phone]
Lab Project Number: 9247328
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 923146070 Project Sample Number: 9247328-002 Date Collected: 07/15/03 10:25
Client Sample ID: MW-2R Matrix: Water Date Received: 07/15/03 10:50
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Nitrate as N 8.7 mg/l 0.050 07/16/03 ALA
Total Organic Carbon Method: EPA 9060
Total Organic Carbon ND mg/l 0.50 07/22/03 EWS 7440-44-0
Date: 07/30/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
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GROLINDWATiER l;TiON
ASHEVILLE RFC::: ""%rs_`,)F1:GE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCo,
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Page: 4 of 23
Charlotte Certification IDs
NC Wastewater
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37706
SC
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Pace Analytical Services, Inc.
' 2225 Riverside Drive
laceAna Asheville, NC 28804
yficaf
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9331019
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 931280713
Project Sample
Number: 9331019-002
Date Collected: 07/23/02 10:45
Client Sample ID: MW-2R
Matrix: Water
Date Received: 07/23/02 11:37
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Field Services
Monitoring Well Data
Method:
Field pH
6.58
Std. Units
07/23/02
MPS
Field Temperature
20.3
deg C
07/23/02
MPS
Static Water Level
5.00
feet
07/23/02
MPS
Total Coliform MPN Water
Method: SM 9223
Coliform, Total
<1.1
1
07/23/02
ACL
Metals
Metals. ICP, trace -level
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.0050
08/07/02
19:38
TRW
7440.38-2
Barium
0.21
mg/l
0.0050
08/07/02
19:38
TRW
7440-39.3
Cadmium
0.0036
mg/l
0.0010
08/07/02
19:38
TRW
7440-43-9
Chromium
0.020
mg/l
0.0050
08/07/02
19:38
TRW
7440-47.3
Selenium
NO
mg/l
0.020
08/07/02
19:38
TRW
7782-49-2
Silver
NO
mg/l
0.0020
08/07/02
19:38
TRW
7440-22-4
Date Digested
08/06/02
Lead, AAS Furnace
Prep/Method:
EPA 3020
/ EPA 7421
Lead
0.0049
mg/l
0.0030
08/19/02
TRW
7439-92.1
Date Digested
08/05/02
Mercury in Water
Method: EPA
7470
Mercury
NO
mg/l
O.00020
08/06/02
TRW
7439-97-6
Wet Chemistry
Total Dissolved Solids
Method: EPA
160.1
Total Dissolved Solids
230
mg/l
10.
07/25/02
ALA
Chloride(Mercuric Nitrate)
Method: EPA
325.3
Chloride
16.
mg/l
1.0
07/26/02
MPS
16887.00-6
Ammonia
Method: EPA
350.1
Nitrogen, Ammonia
NO
mg/l
0.100
07/31/02
EWS
7727-37-9
Nitrogen, Nitrate plus Nitrite
Method: EPA
353.3
Nitrogen, Nitrate
2.8
mg/l
0.10
07/24/02
EWS
Date: 08/22/02
rj
Page: 3.
i�
0.
Laboratory Certification IDs �.__
LA ORATORY ANALYSIS
Laboratory Certificatiom IDs
NC Wastewater 40
NC Drinking Water 37712
C �� r
`' .'fhys r6FtCsall be reproduced, except in full,
TN Drinking water 029e0
SC Environmental 99030
_ .
without the written consent of Pace Analytical Services, Inc.
N ALSO,'
'L!1I�1{tO14 �l\^
JL'JI�V\ z

Pace Analytical Services, Inc.
2225 Riverside Drive
laceAnalyficafw Asheville, NC 28804
Phone: [phone]
www.pacelabs.com Fax., 828.252.4618
Lab Project Number: 9331019
Client Project ID: GROUNDWATER WELLS
L,ab Sample No: 931280713 Project Sample Number: 9331019.002 Date Collected: 07/23/02 10:45
Client Sample ID: MW-211 Matrix: Water Date Received: 07/23/02 11:37
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Total Organic Carbon Method: SM 5310C
Total Organic Carbon 2.7 mg/l 0.50 07/24/02 ALA 7440-44-0
- ng
C� c E0 -�J---�
Date: 08/22/02 g 3
Jti,
Laboratory Certification IN `'-'-"-&IJI�' '�-A60RATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
N ACCOF\
Page: 4,
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

/ / �
�. � �J
� j

1-'A)CeAnaVica1"
!�i'LS't1t. jk"!C.2?ia"i}S:C4frf
s
Lab Sample No: 931280713
Client Sample ID: KW-2R
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Nuntersville, NC 28078
Phone., 704.875.9092
faK.- 704.875.9091
Lab Project Number: 9234851
Client Project ID: MSD 9331019
Project Sample Number: 9234851-002 Date Collected: 07/23/02 10:45
Matrix: Water Date Received: 07/23/02 11:37
Parameters
Results
Units
Report Limit
DF
Analyzed
By
CAS No. Qual RectLmt
GC Volatiles
CC VOCe in Water
Method: SM
6230D
Benzene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
71-43-2
Bromobenzene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
108-86-1
Bromochloromethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
74-97-5
Bromodichloromethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
75-27-4
Bromoform
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
75-25-2
Bromomethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
74-83-9
n-Butylbenzene
ND
ug/1
1.0
1.0
07/27/02
10:55
STC
104-51-8
sec-Butylbenzene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
135-98-8
tert-Butylbenzene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
98-06-6
Carbon tetrachloride
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
56-23-5
Chlorobenzene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
108-90-7
Chloroethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
75-00-3
Chloroform
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
67-66-3
Chloromethane
ND
ug/1
2.0
1.0
07/27/02
10:55
STC
74-87-3
2-Chlorotoluene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
95-49-8
4-Chlorotoluene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/1
2.0
1.0
07/27/02
10:55
STC
96-12-8
Dibromochloromethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
106-93-4
Dibromomethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
74-95-3
1,2-Dichlorobenzene
ND
ug/1
1.0
1.0
07/27/02
10:55
STC
95-50-1
1,3-Dichlorobenzene
ND
ug/1
1.0
1.0
07/27/02
10:55
STC
541-73-1
1,4-Dichlorobenzene
ND
ug/1
1.0
1.0
07/27/02
10:55
STC
106-46-7
Dichlorodifluoromethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
75-71-8
1,1-Dichloroethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
75-34-3
1,2-Dichloroethane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
107-06-2
1,1-Dichloroethene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
75-35-4
cis-1,2-Dichloroethene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
156-59-2
trans-1,2-Dichloroethene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
156-60-5
1,2-Dichloropropane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
78-87-5
1,3-Dichloropropane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
142-28-9
2,2-Dichloropropane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
594-20-7
1,1-Dichloropropene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
563-58-6
cis-1,3-Dichloropropene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
10061-01-5
trans-1,3-Dichloropropene
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
10061-02-6
Diisopropyl ether
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
108-20-3
Ethylbenzene
ND
ug/1
0.50
1.0.0
07�10:
-41-4
Date: 07/30/02 Page: 3
q ,
L
ahoratory Certification los REPORT Of LABORATORY ANALYSIS I ahoratory Certification IDs
KY
NC Wastewater 12 Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99D06 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Nuntersville, NC 28078
Phone:[phone]
ly�Svr.lk7[>�£ar7S.ro+>f Fax- 704.875.9091
Lab Project Number: 9234851
Client Project ID: MSD 9331019
Lab Sample No: 931280713
Project Sample
Number: 9234851-002
Date Collected: 07/23/02 10:45
Client Sample ID: MW-2R
Matrix: Water
Date Received: 07/23/02 11:37
Parameters
Results
Unite
report Limit
DF
Analyzed
By
CAS No. Oual ReaLmt
Bexachloro-1,3-butadiene
ND
ug/l
2.0
1.0
07/27/02
10:55
STC
87-68-3
Isopropylbenzene (Cumene)
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
98-82-8
p-Isopropyltoluene
ND
ug/l
1.0
1.0
07/27/02
10:55
STC
99-87-6
Methylene chloride
ND
ug/1
2.0
1.0
07/27/02
10:55
STC
75-09-2
Methyl-tert-butyl ether
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
1634-04-4
Naphthalene
ND
ug/l
2.0
1.0
07/27/02
10:55
STC
91-20-3
n-Propylbenzene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
103-65-1
Styrene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
79-34-5
Tetrachloroethene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
127-18-4
Toluene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
108-88-3
1,2,3-Trichlorobenzene
ND
ug/l
2.0
1.0
07/27/02
10:55
STC
87-61-6
1,2,4-Trichlorobenzene
ND
ug/l
2.0
1.0
07/27/02
10:55
STC
120-82-1
1,1,1-Trichloroethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
71-55-6
1,1,2-Trichloroethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
79-00-5
Trichloroethene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
79-01-6
Trichlorofluoromethane
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
75-69-4
1,2,3-Trichloropropane
ND
ug/1
0.50
1.0
07/27/02
10:55
STC
96-18-4
1,2,4-Trimethylbenzene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
95-63-6
1,3,5-Trimethylbenzene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
108-67-8
Vinyl chloride
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
75-01-4
m&p-Xylene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
o-Xylene
ND
ug/l
0.50
1.0
07/27/02
10:55
STC
95-47-6
1-Chloro-3-fluorobenzene (S)
127
%
1.0
07/27/02
10:55
STC
625-98-9
Date: 07/30/02
nbnratoly Certification lDs REPORT OF LABORATORY ANALYSIS I ahoratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. Fl- NEIAP E87627
Page: 4

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Pace Analytical Services, Inc.
54 Ravenscroft Drive
ace Analytical Asheville, NC 28801
Phone: [phone]
www.paceiahs.com Fax: [phone]
Lab Project Number: 9326321
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 931098529 Project Sample Number: 9326321.002 Date Collected: 01/14/02 14:15
Client Sample ID: MW-2R Matrix: Water Date Received: 01/14/02 14:55
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Field Services
Monitoring Well Data
Method:
Field pH
6.8
Std. Units
01/14/02
MPS
Field Temperature
14.0
deg C
01/14/02
MPS
Static Water Level
5.79
feet
01/14/02
MPS
Metals
Metals, ICP, trace -level
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
ND
mg/l
0.010
01/23/02
14:15
TRW
7440.38-2
Barium
0.12
mg/l
0.0050
01/23/02
14:15
TRW
7440-39.3
Cadmium
0.0019
mg/l
0.0010
01/23/02
14:15
TRW
7440-43-9
Chromium
ND
mg/l
0.0050
01/23/02
14:15
TRW
7440-47-3
Selenium
ND
mg/l
0.020
01/23/02
14:15
TRW
7782-49-2
Silver
ND
mg/l
0.0020
01/23/02
14:15
TRW
7440-22-4
Date Digested
01/21/02
Lead, AAS Furnace
Prep/Method:
EPA 3020 /
EPA 7421
Lead
NO
mg/l
0.0050
01/17/02
TRW
7439.92.1
Date Digested
01/16/02
Mercury in Water
Prep/Method:
EPA 7470 /
EPA 7470
Mercury
NO
mg/l
0.00020
01/22/02
TRW
7439-97-6
Wet Chemistry
Total Dissolved Solids
Prep/Method:
EPA 160.1
/ EPA 160.1
Total Dissolved Solids
600
mg/l
10.
01/18/02
AAB
Chloride(Mercuric Nitrate) Prep/Method: EPA 325.3 / EPA 325.3
Chloride
29.
mg/l
2.0
01/16/02
MPS 16887-00-6
Ammonia
Prep/Method:
EPA 350.1
/ EPA 350.1
Nitrogen, Ammonia
0.400
mg/l
0.100
01/21/02
JDA 7727.37-9
Nitrogen, Nitrate plus Nitrite
Prep/Method:
EPA 353.2
/ EPA 353.3
Nitrogen, Nitrate
1.2
mg/1
0.10
01/16/02
JDA
Total Organic Carbon
Prep/Method:
SM 5310C
/ SM 5310C
Total Organic Carbon
11.
mg/l
2.0
01/21/02
AAB 7440.44-0
Date: 01/28/02
Page: 3
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030
,N ACCpgO
MIX; ;
s

le Analytical m
www.pacelabs.com
Lab Project Number: 9326321
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 931098529 Project Sample Number: 9326321-002 Date Collected: 01/14/02 14:15
Client Sample ID: MW-2R Matrix: Water Date Received: 01/14/02 14:55
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Total Coliform MPN Water Prep/Method: Standard Methods / SM 9223
Coliform, Total 1.1 1 01/14/02 JGJ
Date: 01/28/02
Laborato�Certification IN
NC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
` 54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
O `N ACCpgO
� 4 MC z
Page: 4
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

I
COUNTY: BUNCOnIBE
QUAD NO:
REPORT TO ARO Regional OfFic
COLLECTOR(S) : A RUMBOUGH
DATE: _ --
TIME: �—
PURPOSE:
j
DIVISION OF WATER QUALITY 7_,
r 1G1153
Chemistry Laboratory Report / Ground water Quality ed 7/26/200f
ed : 9:45 AM
SAMPLE PRIORITI yX]ROUTINE EMERGENCY
X� CHAIN OF CUSTODY eleased B
e MW-ZR Date reported: 9/21/2001
W� SAMPLE TYPE
Owner: METROPOLITAN SENVER EE DISTRICT
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
1G1153.x1s

..�.. L.no Full
NORTH CAROLINA
Department
Buncombe
r� M87j5
of Environment and
DIVISION OF Natural Resources
WATER
Serial No.
�- __ 138027
..r. 35 38 45 Long,
Sample Type
Water X
QUALITY _ GROUN DWATER SECTION
Sam le priori
82 35 43
Soil
Routine X Lab Number
Report To: ARO
(ARO' CO, Other)
Other
Emergency Date Received _
Shipped by: Courier
(Bus, Courier, Handpel.,
Chain of Custody
Rec'd by:
MW-2R Other
TMinnick/ARumbough
Date: 7/24/01
Other) q � � From: BusCollector(s):
$ �"� d" �OurieQhd
Data y y.
I r Entry b
Time: 1100
Ck:
FIELD ANALYSES
purpose: (Baseline, Complaint Com liance Date Reported:
UST, pesticide
� �'aoo 6.48
Spec. Cond.94
(crrcieone)
Study, Federal Trust, Other):
femplo 20.3 oC
524
Odor None
at 25oC
Owner
Metropolitan Sewerage District
Location or site
Appearance Water dingy
Down g radient of ash disposal lagoon
Description of
Field Analysis by:
sampling point Well Head
Sampling Method
Bailer
LABORATORY ANALYSIS
StSample Interval: 7.0 ft.
Remarks Level - 17.0
Water L_
5
-Static
6.03 ft. ft.
MSD i/_7R

NORTH CAROLINA
GROUNDWATER FIELD&AB FORAM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
County Buncombe Sample Type 5ample Priority Lab Number
Quad No. M87j5 5erial No. 138027 Water N
Routine X -- — C)�1%
bete Received -� � � Time /
Lat. 35 38. 45 Long. 82 35 43 Soil Emergency Rec'd by: � From: Bus, Courier,`!and Del.
Other MW_2R Other
Report To: ARO (ARO, CO, Other) Chain of Custody F Data Entry by: Ck: ti
Shipped by: Hand Delivered (Bus, Courier, Hand Del., Other)
Collector(s): TMinnick/ARumbough Date: 7/24/01 Date Reported:
Time: 1100
�'�--
Purpose: (Baseline, Complaint, Cam liance LUST, Pesticide Study, Federal Trust, Other):
FlF' ^.ANALYSES (circle om)
Owner Metropolitan Sewerage District
pl "- , 6,48 Spec. Cond.94 524 at 250C Location or site Downgradient of ash disposal lagoon
Templo 20.3 oC Odor None Description of sampling point Well Head
Appearance Water dingy Sampling Method Bailer Sample Interval 7.0 ft. - 17.0 ft.
Field Analysis by: Remarks Static Water Level = 6.03 ft. Split samples with Pace, Inc.
LABORATORY ANALYSIS
BOD5310mg/I
COD High 340 mg/l
COD Low 335 mg/I
X
Coliform:JWFecal33646• /100ml
X
Coliform: OrTotal94004 /100ml
TOC 680 mg/l
Turbidity 76 NTU
Residue., Suspended 530 mg/1
pH 403 units
lkalinity to pH 4.5 410 mg/I
Alkalinity to pH 8.3 415 mg/I
Carbonate 445 mg
Bicarbonate 440 mg/I
Carbon dioxide 405 mg/I
Chloride 940 mg/I
Chromium: He 1032 ug/I
Color: True 80 CU
Cyanide 720 mg/I
�B �
MSD MW-2R

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: M�-t"bPo� tta" Sewe�age�-C?;str�cl"
Permit Name (if different):
Facili Address: 9 225 IZ', v
A yilte (Street) NC ZRSV� County $�r\covv�be
(Ci ) (Syve (zip)
Contact Person: �'� t^�^ K V ►'� ' i Telephone # �$ 2 -7 3
Well Location/ Site Named of (\Sl,l-40W6. of Wells to be Sampled: o(,Lr
from�t
Well Identification Number (from Permit): %3- Pv1 For Groundwater Treatment Systems
Well Depth: 17 ft. Well Diameter: Z in. Check One: ❑ Influent (98)
Screened Interval: —ft. to _-_ ft. ❑ Effluent (99)
Depth to Water Level: ©� ft. below measuring point.
Measuring Point (M.P.) is: On 0 ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/ba' ed before sampling: (e: G Date sample collected: 2 f7
Field analysis: pH—t— , Specific Co�n/d��Vuc�tance -2 uMhos
Temp. °C,Odor. C_ Appearance CIeL'^
fj M1 I[9n=j DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH NC 27699-1636 Phone: [phone]
PERMIT #: N C00, 14 11 EXPIRATION DATE:
�.;
Non -Discharge UIC c's
NPDES X
TYPE OF PERMITTED OPERATION BEING MONITORED tv
x_ Lagoon Remediation: Infiltration Gallery ,
Spray Field Remediation: _
Rotary Distributor Land Application of Sludge ,
C�
Other.
NOTE: Values should reflect dissolved and -
colloidal concentrations.
Date sample analy 7 ' 4
Laboratory Name:
Certification No.
PARAMETERS (Samples for metals were collected unfiltered X YES
NO and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/`
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
/� g
Coliform: MF Total z ! • ) P1v
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total ZZOC'
mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
• C'`1 mg/I
TOC
mg/I
Ca - Calcium
mg/I
Chloride 7 mg/I
Cd - Cadmium
• 0 mg/I
Arsenic < 4 dIVmg/I
Chromium: Total
• 0 c'9 mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
< - 0 O G.2 mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
'W-59 JUUJ AUG 2 12001
r. 03/2000
%C YES NO)
Ni -Nickel � � C,y mg/I .' Pb - Lead
Zn - Zinc mg/I
Ammonia Nitrogen 772 mg/I
Other LSp cify Compounds and Concentration Units)
SS
i V ` O 0 v� I
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. gttach lab report.)
Report Attached? Yes �, (1) No � 0)
VOC method # = �_�3 Off
method # =
method # =
- Please pnnt or type
�-/c3iCI

lce Analyticafm
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9322101
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 93933265 Project Sample Number: 9322101.002 Date Collected: 07/24/01 11:00
Client Sample ID: MW-2R Matrix: Water Date Received: 07/24/01 13:33
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Field Services
Monitoring Well Data
Method:
Field pH
6.48
Std. Units
07/23/01
MPS
Field Specific Conductance
524
umhos/cm
07/23/01
MPS
Field Temperature
20.3
deg C
07/23/01
MPS
Static Water Level
6.03
feet
07/23/01
MPS
Well Volume Purged
6.00 GA
No units
07/23/01
MPS
Metals
Metals, ICP, trace -level
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
NO
mg/l
0.010 07/25/01 22:29 TRW
7440-38-2
Barium
0.078
mg/l
0.0050 07/25/01 22:29 TRW
7440-39.3
Cadmium
NO
mg/l
0.0010 07/25/01 22:29 TRW
7440.43-9
Chromium
0.0051
mg/l
0.0050 07/25/01 22:29 TRW
7440-47-3
Selenium
NO
mg/l
0.020 07/25/01 22:29 TRW
7782-49-2
Silver
NO
mg/l
0.0020 07/25/01 22:29 TRW
7440-22-4
Date Digested
07/25/01
Lead, AAS Furnace
Prep/Method:
EPA 3020 /
EPA 7421
Lead
0.0070
mg/l
0.0050 08/02/01 TRW
7439 92 1
Date Digested
07/30/01
Mercury in Water
Prep/Method:
EPA 7470 /
EPA 7470
Mercury
NO
mg/l
0.00020 08/01/01 TRW
7439-97-6
Wet Chemistry
Total Dissolved Solids
Prep/Method:
EPA 160.1
/ EPA 160.1
Total Dissolved Solids
400
mg/l
10. 07/30/01 AAB
Chloride(Mercuric Nitrate)
Prep/Method:
EPA 325.3
/ EPA 325.3
Chloride
27.
mg/l
1.0 08/08/01 TRW
16887-00-6
Ammonia
Prep/Method:
EPA 350.1
/ EPA 350.1
Nitrogen, Ammonia
1.20
mg/l
0.100 07/31/01 JDA
7727-37-9
Date: 08/10/01
Laboratory Certification IDs
REPORT OF
LABORATORY ANALYSIS
NC Wastewater 40
This report
shall not be reproduced, except in full,
NC Drinking Water 37712
without the written consent of Pace Analytical Services, Inc.
N AC COA
0
Page: 3
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

Pace
e Analytical
www.pacelabs.com
Asheville, NC 2b,,
Phone: [phone]�,
Fax: [phone]
Lab Project
Number: 9322101
Client Project
ID: GROUNDWATER WELLS
93933265
Project Sample
p
Number: 9322101-002
Date Collected: 07/24/01 11:00
ab Sample No:
Matrix: Water
Date Received: 07/24/01 13:33
lient Sample ID: MW-2R
Results
Units
Report Limit Analyzed
CAS No. Ftnote Reg Limit
arameters
Nitrogen, Nitrate plus Nitrite
Prep/Method:
EPA 353.3
/ EPA 353.3
Nitrogen, Nitrate
1.4
mg/l
0.10 07/25/01
JDA
Total Organic Carbon
Prep/Method:
SM 5310C /
SM 5310C
07/31/01
AAB
7440 44 0
Total Organic Carbon
3.0
mg/l
2.0
Total Coliform MPN Water
Prep/Method:
Standard Methods / SM 9223
Coliform, Total
<1.1
1 07/24/01
KAS
Date: 08/10/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
M ACCpq
C-
Page: 4
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

ace Analytical
www.pacelabs.com
Lab Sample No: 93933265
Client Sample ID: MW-2R
Parameters
GC VolatiLes
GC VOCs in Water
Dichlorodifluorcmethane
Chloraoethane
vinyl chloride
Brananethane
Chloroethane
Trichlorofluoranethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
cis-1,2-Dichloroethene
BranochLoranethane
Chloroform
2,2-Dichloropropane
1,2-Dichloroethane
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon tetrachloride
Dibrananethane
1,2-Dichloropropane
Trichloroethene
Bromodichloranethane
cis-1,3-Dichloropropene
trans-1,3-Dichlorcprcpene
1,1,2-Trichloroethane
1,3-Dichloropropane
Dibrarochloranethane
1,2-Dibromoethane (mB)
Tetrachloroethene
1,1,1,2-Tetrachloroethane
Chlorobenzene
Branoform
1,1,2,2-TetrachLoroethane
1,2,3-Trichloropropane
Bromobenzene
Date: OB/02/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project NuTber: 9224756
Client Project ID: MSD/9322101
Project Sample Nurber: 9224756-002 Date Collected: 07/24/01 11:00
Matrix: Water Date Received: 07/24/01 13:33
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Reg Limit
Prep/Method: SM 6230D
/ SM 6230D
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
75-71-8
0.94
L19/L
0.50
1.0
07/28/01 10:25
KST
74-87-3
ND
ug/L
0.50
1.0
(7/2B/01 10:25
KST
75-01-4
ND
ug/1
0.50
1.0
07/2B/01 10:25
KST
74-83-9
ND
Ug/L
0.50
1.0
07/28/01 10:25
KST
75-00-3
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
75-69-4
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
75-35-4
ND
ug/L
0.50
1.0
07/28/01 10.25
KST
75-09-2
ND
LW
0.50
1.0
07/28/01 10:25
KST
156-60-5
ND
Ug/L
0.50
1.0
07/28/01 10:25
KST
75-34-3
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
156-59-2
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
74-97-5
ND
i.g/L
0.50
1.0
07/28/01 10:25
KST
67-66-3
ND
Ug/L
0.50
1.0
07/28/01 10:25
KST
594-20-7
ND
Ug/L
0.50
1.0
07/28/01 10:25
KST
107-06-2
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
71-55-6
ND
ug/L
0.50
1.0
07/2B/01 10:25
KST
563-58-6
ND
ug/t
0.50
1.0
07/28/01 10:25
KST
56-23-5
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
74-95-3
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
78-87-5
ND
ug/L
0.50
1.0
07/2B/01 10:25
KST
79-01-6
ND
ug/t
0.50
1.0
07/28/01 10:25
KST
75-27-4
ND
Vg/L
0.50
1.0
07/28/01 10:25
KST
10061-01-5
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
10061-02-6
ND
LG/L
0.50
1.0
07/28/01 10:25
KST
79-00-5
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
142-28-9
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
124-48-1
ND
ug/l
0.50
1.0
07/23/01 10:25
KST
106-93-4
ND
LWL
0.50
1.0
07/28/01 10:25
KST
127-18-4
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
630-20-6
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
108-90-7
ND
WL
0.50
1.0
07/28/01 10:25
KST
75-25-2
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
79-34-5
ND
ug/L
0.50
1.0
07/2B/01 10:25
KST
96-18-4
ND
ug/l
0.50
1.0
07/28/01 10:25
KST
108-86-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N At�agO
Page: 3
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

Analytical
www.pacelabs.com
Lab Project Nurber: 9224756
Client Project ID: MSD/9322101
Pace Analytica►
9800&cejiAvenue, 6,
Huntersville, NC 2U
Phone: [phone]
Fax: [phone]
Lab Sample No: 93933265 Project Sample Nunber: 9224756-002 Date Collected: 07/24/01 11:00
Client Sample ID• MW-2R Matrix: Water Date Received: 07/24/0113:33
Results
Units
Report Limit Dilution Analyzed
CAS No. Ftnote Reg Limit
Parameters
2-Chlorotoluene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
106-43-4
1,3-Dichlorobenzene
ND
ug/L
1.0
1.0
07/28/01 10:25
Ksr
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1.0
07/28/01 10:25
KST
106-46-7
1,2-Dichlorobenzene
ND
ug/L
1.0
1.0
07/28/01 10:25
KST
95-50-1
1,2-Dibrarn-3-chloropropane
ND
ug/L
2.0
1.0
07/28/01 10:25
KST
96-12-8
1,2,4-Trichtorobenzene
No
tg/L
2.0
1.0
07/28/01 10:25
KST
120-82-1
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.0
07/28/01 10:25
KST
87-68-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1.0
07/28/01 10:25
KST
87-61-6
Methyl-tert-butyl ether
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
1634-04-4
Diisopropyl ether
ND
ug/1
0.50
1.0
07/28/01 10:25
KST
108-20-3
ND
tg/L
0.50
1.0
07/28/01 10:25
KST
71-43-2
Benzene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
108-88-3
Toluene
Ethylbenzere
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
100-41-4
m643-Xylene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
ND
ug/1
0.50
1.0
07/28/01 10:25
KST
100-42-5
Styrene
o-Xylene
No
ug/1
0.50
1.0
07/28/01 10:25
KST
95-47-6
Isopropylbenzene (Cunene)
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
98-82-8
n-Propylbenzene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
103-65-1
1,3,5-TrimethyLbenzene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
108-67-8
tert-Butylbenzene
ND
ag/l
0.50
1.0
07/28/01 10:25
KST
98-06-6
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
95-63-6
sec-ButyLbenzene
ND
ug/L
0.50
1.0
07/28/01 10:25
KST
135-98-8
p-Isopropyltoluerre
ND
ug/1
1.0
1.0
07/28/01 10:25
KST
99-87-6
n-Butylbenzene
ND
ug/L
1.0
1.0
07/28/01 10:25
KST
104-51-8
Naphthalene
ND
ug/l
2.0
1.0
07/2B/01 10:25
KST
91-20-3
1-Chloro-3-fluorobenzene (S)
107
%
1.0
07/28/01 10:25
KST
625-98-9
Date: 08/02/01
Laboratoy Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCORD
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

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ace Analytical'
www.pacelabs.com
Lab Sample No: 93778397
Client Sample ID: MW-2R/M87J5
Parameters Results
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9317970
Client Project ID: GROUNDWATER WELLS
Project Sample Number: 9317970-002 Date Collected: 01/25/01 12:00
Matrix: Water Date Received: 01/25/01 14:25
Units PRL Analyzed Analyst CAS# Ftnote Limit
Field Services
Monitoring Well Data
Method:
Field pH
6.5
Std. Units
01/25/01
MPS
Field Specific Conductance
710
umhos/cm
01/25/01
MPS
Field Temperature
9.7
deg C
01/25/01
MPS
Total Well Depth (ro W attr
5.57
feet
0
01/25/01
MPS
Odor
None
No units
0
01/25/01
MPS
Field Appearance
Clear
No units
0
01/25/01
MPS
Well Volume Purged
3.00
GA No units
0
01/25/01
MPS
Metals
Metals, ICP, trace -level
Method: EPA 6010
Prep Method:
EPA 3010
Arsenic
ND
mg/l
0.010
02/01/01
13:44 TRW
7440-38-2
Barium
0.090
mg/l
0.0050
02/01/01
13:44 TRW
7440-39-3
Cadmium
0.0011 mg/l
0.0010
02/01/01
13:44 TRW
7440-43-9
Chromium
NO
mg/l
0.0050
02/01/01
13:44 TRW
7440-47.3
Selenium
ND
mg/l
0.020
02/01/01
13:44 TRW
7782-49-2
Silver
NO
mg/l
0.0020
02/01/01
13:44 TRW
7440-22.4
Date Digested
01/.30/01
Lead, AAS Furnace
Method: EPA 7421
Prep Method:
EPA 3020
Lead
NO
mg/l
0.0050
02/05/01
JDA
7439-92-1
Date Digested
01/30/01
Mercury in Water
Method: EPA 7470
Prep Method:
EPA 7470
Mercury
ND
mg/l
0.00020
01/31/01
TRW
7439-97-6
Wet Chemistry
Total Dissolved Solids
Method: EPA 160.1
Prep Method:
EPA 160.1
Total Dissolved Solids
690
mg/l
10.
02/01/01
JMS
Chloride(Mercuric Nitrate)
Method: EPA 325.3
Prep Method:
EPA 325.3
Chloride
33.
mg/l
1.0
01/29/01
MPS
16887-00-6
Page: 3
Date: 02/09/01
Laboratory Certification IDs
REPORT OF
LABORATORY
ANALYSIS
Laboratory Certification IDs
NC Wastewater 40
This report shall not be reproduced; except in full,
TN Drinking Water 02980
SC Environmental 99030
NC Drinking Water 37712
without the written
consent of Pace Analytical Services, Inc.

aceAnalytical'
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone. [phone]
Fax: [phone]
Lab Project Number: 9317970
Client Project ID: GROUNDWATER WELLS
Lab Sample No: 93778397
Project Sample Number: 9317970-002
Date Collected: 01/25/U1 12:UU
Client Sample ID: MW-2R/M87J5
Matrix: Water
Date Received: 01/25/01 14:25
Parameters
Results Units PRL
Analyzed
Analyst CAS# Ftnote Limit
Ammonia
Method: EPA 350.1
Prep
Method: EPA 350.1
Nitrogen, Ammonia
1.10 mg/l 0.100
01/31/01
JDA 7727-37-9
Nitrogen, Nitrate plus Nitrite
Method: EPA 353.3
Prep
Method: EPA 353.3
Nitrogen, Nitrate
8.0 mg/l 0.10
02/05/01
JDA
Total Organic Carbon
Method: SM 5310C
Prep
Method: SM 5310C
Total Organic Carbon
9.0 mg/l 2.0
02/06/01
AAB 7440-44-0
Total Coliform MPN Water
Method: SM 9223
Prep
Method: Standard Methods
Coliform, Total
>23.0 1
01/25/01
KAS
Date: 02/09/01 Page: 4
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

SUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or Type
Facility Name:- Metr000l i tan Sewerage District
Permit Name (if different):
Facility Address: 2225 Riverside Drive
Asheville NC 28814 County Buncombe
Contact Person: Bohn Kiviniemi rts.r t Telephone #: [phone]
Well Location/ Site Name: Downgradient of Ash Lagoon NO. of Wells to be Sampled. four
MOM
Well Identification Number (from Permit): M87J5 (MW-2R) For Groundwater Treatment Systems
Well Depth: 17.o H. Weil Diameter: 2 ln. Check One:
Screened.Interval: 7.0 ft. to 17.0 ft. IO Influent (98) CIE:. Values should reflect dissolved and
-Depth to Water Level: (P.-TS ft. below measuring point. p Effluent (99) colloidal concentrations. T tt r
Measuring Point is 0.0 ft. above land surface. 1
Gallons of water pumped/balled before sampling: 2.0 1 Date sample collected: T oQ Date sample analyzed:-111.149
Field analysis: pH ca-Sd , Specific Conductance_ 1210 uMhos Laboratory Name: Severn IM Lahnlr nci2s
Temp. 21.1 °C, Odor t4ony Appearance Clux Certification No. 314
PERMIT #: NCoo249ii EXPIRATION DATE: 9/30/2000
Non -Discharge UIC
NPDES xxx
TYPE OF PERMITTED OPERATION BEING MONITORED
. _X_._ Lagoon Rerhediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
PARAMETERS (Samples for metals were collected unfiltered X YES NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
Mg/I
Coli.form: MF Fecal
/100MI
Nitrate (NO3) as N
4.o mg/I
Coliform: MF Total
/100MI
Phosphorus: Total as P
mgA
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Dissolved Solids: Total B%o
mg/I
Al - Aluminum
mg/I
pH (when analyzed) (D.s
units
Ba - Barium a.o4
mg/I
TOG _2.7
mgA
Ca = Calcium
mg/I
31
mg/I
Cd - Cadmium <o.doF,
mg/I
,__Chloride
arsenic < o.0o s .
mg/I
Chromium: Total 0.
ao S mg/I
Grease and Oils
mg/I
Cu - Copper
mgA
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/l
Hg'-Mercury <o.00n2o.
mgA
Specific Conductance
uMhos
K - Potassium
mgA
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
-k YES NO)
N1- Nickel
mg/i
Pb - Lead
mg/I
Zn - Zinc
mg/I
Ammonia Nitrogen 0,74
1719/1
Other. (Specify Compounds and Concentration Units)
SQl2.nium SQ.a 1 ma /t
silVQ_r <0.00s mu/1
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes__)�.(1) No (0)
VOC : method # = A2t a
method # _
: method # _

SUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or Type
Facility Name: Metr000l i tan Sewerage District
Permit Name (if different):
Facility Address: 2225 Riverside Drive
Asheville () NC 28814 County Buncombe
Contact Person: John Kiviniemi r ierei Telephone #: [phone]
Well Location/ Site Name: Downgradient of Ash Lagoon No. of Wells to be Sampled: f o .rm
Well Identification Number (from Permit): M87J5 (MW-211) For Groundwater Treatment Systems
Well Depth: ' 17.o It. Well Diameter: 2 in. Check One:
%reened.Interval: 7.0 ft. to 17.0 ft. Q Influent (98)
� ,.;epth to Water Level: 1:e.1A ft. below measuring point.
Measuring Point is 0.0 ft. above land surface. O Effluent (99)
Gallons of water pumped/balled before sampling: 2.0
Field analysis: pH Co-54 , Specific Conductance 1230 uMhos
Temp. '41.11 °C, Odor t taae Appearance Clear
PERMIT #: 11CO024911 EXPIRATION DATE: 9/30/2000
Non -Discharge UIC
NPDES xxx
TYPE OF PERMITTED OPERATION BEING MONITORED
X Lagoon Rerhediation: Infiltration Gallery
spray Field Remedlation:
Rotary Distributor Land Application of Sludge
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected: ? (1O Date sample analyzed: t I On
LaboratoryName: lace ArlaISAIi .al 1,.abom+060-5
Certification No. A- 7712
PARAMETERS (Samples for metals were collected unfiltered YES NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
-mg/i
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total < ► J
/100ml
Phosphorus: Total as P
mg/I
(Note: use MPM method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
mg/I
Al - Aluminum
mg/i
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
mg/I
Ca = Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
senic
mg/I
Chromium: Total
mg/I
crease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
YES NO)
NI - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other. (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No _.X _ (0)
VOC : method # im
method # -
: method # =

CcunHted'To Your Success
LOG NO: CO-07159
Received: 11
JUL 00
Reported: 18
JUL 00
Mr. Paul Johnstone
Law Engineering & Environmental
Services, Inc.Client
PO. No.: 30290-5-4492-21-901
4 Interchange Blvd.
Greenville, SC 29607
Requisition: 30290/60110
Project: MSD-ASH
LAGOON
Sampled By:
Client
Code: 124600718
REPORT
OF RESULTS
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID
SAMPLES
TIME SAMPLED
07159-1 MW-1
-
-----------------------
07-10-00/11:30
07159-2 MW-2R
07-10-00/12:10
07159-3 MW-3
07-10-00/11:00
07159-4 MW-4
07-10-00/12:40
PARAMETER
07159-1
07159-2
07159-3 07159-4
Volatile Organic Compounds (8260)
-
--------
---------- ----------
Benzene, ug/l
<5.0
<5.0
<5.0
<5.0
Bromobenzene, ug/l
<5.0
<5.0
<5.0
<5.0
Bromochloromethane, ug/1
<5.0
<5.0
<5.0
<5.0
Bromodichloromethane, ug/l
<5.0
<5.0
<5.0
<5.0
Bromoform, ug/l
<5.0
<5.0
<5.0
<5.0
Bromomethane (Methyl bromide), ug/l
<5.0
<5.0
<5.0
<5.0
Carbon tetrachloride, ug/1
<5.0
<5.0
<5.0
<5.0
Chlorobenzene, ug/l
<5.0
<5.0
<5.0
<5.0
Chloroethane, ug/1
<5.0
<5.0
<5.0
<5:0
Chloroform, ug/1
<5.0
<5.0
<5.0
<5.0
Chloromethane, ug/1
<5.0
<5.0
<5.0
<5.0
2-Chlorotoluene, ug/l
<5.0
<5.0
<5.0
<5.0
4-Chlorotoluene, ug/l
<5.0
<5.0
<5.0
<5.0
Dibromochloromethane, ug/1
<5.0
<5.0
<5.0
<5.0
Dibromomethane (Methylene bromide), ug/1
<5.0
<5.0
<5.0
<5.0
1,2-Dibrom6ethane (EDB), ug/l
<5.0
<5.0
<5.0
<5.0
1,2-Dichlorobenzene, ug/l
<5.0
<5.0
<5.0
<5.0
1,3-Dichlorobenzene; ug/l
<5.0
<5.0
<5.0
<5.0
1,4-Dichlorobenzene, ug/l
<5.0
<5.0
<5.0
<5.0
Dichlorodifluoromethane, ug/l
<5.0
<5.0
<5.0
<5.0
1,1-Dichloroethane, ug/l
<5.0
<5.0
<5.0
<5.0
1,2-Dichloroethane, ug/l
<5.0
<5.0
<5.0
<5.0
3355 McLemors Drive, Pensacola, FL 32514 a part of
Tel: [phone] i Fax: [phone] Severn Trent Services Inc.

Commited To Your Success
LOG NO CO-07155
Received: 11 JUL 00
Re'orteds 18 JUL 00
Mr. Paul Johnstone P
Law Engineering & Environmental Services, Inc.Client PO. No.: 30290-5-4492-21-901
4 Interchange Blvd.
Greenville, SC 29607 Requisition: 30290/60110
Project: MSD-ASH
LAGOON
Sampled By:
Client
Code: 124600718
REPORT OF
RESULTS
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION ., LIQUID SAMPLES
TIME SAMPLED
07159-1 MW-1
-----------
-----------------------
07-10-00/11:30
07159-2 MW-2R
07-10-00/12:10
07159-3 MW-3
07-10-00/11:00
07159-4 MW-4
07-10-00/12:40
PARAMETER
07159-1
---------
07159-2
-----------------------
07159-3 07155-4
------------
1,1-Dichloroethene, ug/l
----------
<5.0
<5.0
--------------------
<5.0
<5.0
cis-1,2-Dichloroethene, ug/1
<5.0
<5.0
<5.0
<5.0
trans-1}2-Dichloroethene, ug/1
<5.0
<5.0
<5.0
<5.0
l,2-Dichloropropane, ug/1
<5.0
<5.0
<5.0
<5.0
1,3-bichloropropane, ug/l
<5.0
<5.0
<5.0
<5.0
2,2 Dichloropropane, ug/l
<5.0
<5.0
<5.0
<5.0
cis-1,3-Dichloropropene, ug/1
<5.0
<5.0
<5.0
<5.0
trans-l3-Dichloropropene, ug/1
<5.0
<5.0
<5.0
<5.0
Ethylbenzene, ug/l
<5.0
<5.0
<5.0
<5.0
Hexachlorobutadiene, ug/l
<5.0
<5.0
<5.0
<5.0
Isopropylbenzene (Cumene), ug/l
<5.0
<5.0
<5.0
<5.0
p-Ieopropyltoluene, ug/1
<5.0
<5.0
<5.0
<5.0
Methylene chloride (Dichloromethane), ug/1
<5.0
<5.0
<5.0
<5.0
Methyl t:-butyl ether (MTBE), ug/l
<5.0
<5.0
<5.0
<5.0
Naphthalene, ug/1
<5.0
<5.0
<5.0
<5.0
n-Butylbenzene, ug/1
<5.0
<5.0
<5.0
<5.0
n-Propylbenzene , ug/l
<5.0
<5.0
<5.0
<5.0
sec-Butylbenzene, ug/1
<5.0
<5.0
<5.0
<5.0
Styrene, ug/1
<5.0
<5.0
<5.0
<5.0
t-Butylbenzene, ug/1
<5.0
<5.0
<5.0
<5.0
1,1,1,2-Tetrachloroethane, ug/l
<5.0
<5.0
<5.0
<5.0
1,1,2,2-Tetrachloroethane, ug/l
<5.0
<5.0
<5.0
<5.0
Tetrachloroethene, ug/1
<5.0
<5.0
<5.0
<5.0
3355 McLemoie Drive, Pensacola, FL 32514 a part of
Tel: (860) 470 ow + Fax: [phone] Severn Trent Services Inc.

Commited To Your Success
LOG NO: CO-07159
Received: 11 JUL 00
Mr. Paul .Johnstone Reported: 18 JUL 00
Law Engineering & Environmental Services, Inc.Client PO. No.: 30290-5-4492-21-901
4 Interchange Blvd.
Greenville, SC
29607
Requisition: 30290/60110
Projects MSD-ASH
LAGOON
Sampled By:
Client
Code: 124600718
REPORT OF RESULTS
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION ,LIQUID
SAMPLES
TIME SAMPLED
07159-1 MW-1
---------------------------
-----------------------
07-10-00/11:30
07159-2 MW-2R
07-10-00/12:10
07159-3 MW-3
07-10-00/11:00
07159-4 MW-4
07=10-00/12:40
PARAMETER
------------------
07159-1
07159-2
-----------------------
07159-3 07159-4
Toluene, ug/l
1,1,1-Trichloroethane,
ug/l
<5.0
<5.0
<5.0
<5.0
1,1,2-Trichloroethane,
ug/l
<5.0
<5.0
<5.0
<5.0
1,2,3-Trichlorobenzene,
ug/l
<5.0
<5.0
<5.0
<5.0
1,2,4-Trichlorobenzene,
ug/1
<5.0
<5.0
<5.0
<5.0
Trichloroethene, ug/1
<5.0
<5.0
<5.0
<5.0
Trichlorofluoromethane,
ug/l
<5.0
<5.0
<5.0
<5.0
1,2,3-Trichloropropane,
ug/l
<5.0
<5.0
<5.0
<5.0
1,2,4-Trimethylbenzene,
ug/l
<5.0
<5.0
<5.0
<5.0
1,3,5-Trimethylbenzene,
ug/l
<5.0
<5.0
<5.0
<5.0
Vinyl chloride, ug/1
<5.0
<5.0
<5.0
<5.0
o-Xylene, ug/1
<5.0
<5.0
<5.0
<5.0
m&p-Xylene, ug/l
<10
<10
<10
<10
Surrogate - Dibromofluoromethane
118 %
114 %
109 9
118
Surrogate - Toluene-d8
107 %
103 %
99 %
104 %
Surrogate - 4-Bromofluorobenzene
105 %
102 %
100 %
104 %
Dilution Factor
1
1
1
1
Analysis Date
07.12.00
07.12.00
07.12.00 07.12.00
Batch ID
LEW159
LEW159
LEW159 LEW159
Prep Method
5030
5030
5030
5030
Analyst
WD
WD
WD
WD
3355 McLem&o Drive, Pensacola, FL 32514 a part of
T61: (850) 474A001 • Fax: [phone] Severn Trent Services Inc.

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