WQ0013419_Annual Monitoring_20151230

&6i
G L A T F E L T E R
Beyond Paper
December 30, 2015
Landon Davidson
NCDENR - Division of Water Quality
Aquifer Protection Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Dear Mr. Davidson,
Please find enclosed a CD containing the Pace Analytical November 2015 test reports
for the Sludge Landfill. Also included on the CD is the lab data presented in the EDD
format used by the Solid Waste Section.
If you have any questions or need anything clarification on the enclosed data packages
Please contact D. Mike Cody our Contract Consultant for the site at 828-246-1388 or at
[e-mail]
Sincerely,
4�L"& �/W'_
Kathy Wiedeman
Director, Environmental, Health & Safety, SPBU Glatfelter
Phone: [phone]
Mobile: [phone]
Fax: [phone]
katherine.wiedeman(?ilglatfelter.com
Spring Grove Facility 228 South Main Street • Spring Grove, PA 17362 U.S.A. • Phone [phone] • Fax [phone]
www.glatfelter.com

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November 30, 2015
Mr. D.M. Cody
Glatfelter Corp.
228 South Main Street
Spring Grove, PA 17362
RE: Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Dear Mr. Cody:
Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Revised Report. 8270 data has been re -loaded into system after an error was found in initial upload.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 77

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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 77

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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92275067001
SWP-1
EPA 6010
CDF
18
PASI-A
EPA 1631E
HVK
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
NB
63
PASI-C
SM 2320B
MLS
1
PASI-A
SM 2540C
SAM
1
PASI-A
EPA 300.0
MDW
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
MDW
1
PASI-A
92275067002
SWP-2
EPA 6010
CDF
18
PASI-A
EPA 1631E
HVK
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
NB
63
PASI-C
SM 2320B
MLS
1
PASI-A
SM 2540C
SAM
1
PASI-A
EPA 300.0
MDW
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
MDW
1
PASI-A
92275067003
Q06V09
EPA 6010
CDF
18
PASI-A
EPA 1631E
HVK
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
NB
63
PASI-C
SM 2320B
MLS
1
PASI-A
SM 2540C
SAM
1
PASI-A
EPA 300.0
MDW
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
MDW
1
PASI-A
92275067004
Q06V10
EPA 6010
CDF
18
PASI-A
EPA 1631E
HVK
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
NB
63
PASI-C
SM 2320B
MLS
1
PASI-A
SM 2540C
SAM
1
PASI-A
EPA 300.0
MDW
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
MDW
1
PASI-A
92275067005
Q06V11
EPA 6010
CDF
18
PASI-A
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 1631E
HVK
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
NB
63
PASI-C
SM 2320B
MLS
1
PASI-A
SM 2540C
SAM
1
PASI-A
EPA 300.0
MDW
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
MDW
1
PASI-A
92275067006 Field Blank
EPA 1631E
HVK
1
PASI-A
92275067007 Trip Blank
EPA 8260
NB
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 4 of 77

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Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Lab Sample ID Client Sample ID
Method Parameters
92275067001 SWP-1
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
Field Specific Conductance
Oxygen, Dissolved
REDOX
Turbidity
Odor
Appearance
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 1631 E
SM 2320B
SM 2540C
EPA 300.0
SM 4500 -CI -E
SM 5310B
92275067002
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 1631 E
SM 2320B
SM 2540C
EPA 300.0
Barium
Calcium
Cobalt
Magnesium
Potassium
Sodium
Mercury
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
Chloride
Total Organic Carbon
SWP-2
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
Field Specific Conductance
Oxygen, Dissolved
REDOX
Turbidity
Odor
Appearance
Barium
Calcium
Cobalt
Magnesium
Sodium
Zinc
Mercury
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
SUMMARY OF DETECTION
Result
MPS
11/5/15
13:45
7.6
18.4
1034
6.94
188.6
106.9
No odor
Rusty tint,
opaque
182
39600
9.3
48000
12100
20300
0.643
549
420
2.0
30.8
8.1
MPS
11/5/15
12:35
7.5
16.3
280
9.26
184.3
17.65
No odor
Clear, rusty
sediment
89.8
41700
3.3J
5930
11100
5.8J
0.726
140
122
8.6
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Units Report Limit Analyzed
ug/L
5.0
11/17/15 10:28
ug/L
500
11/17/15 10:28
ug/L
5.0
11/17/15 10:28
Std. Units
0.10
11/17/15 10:28
deg C
0.50
11/17/15 10:28
umhos/cm
1.0
11/17/1510:28
mg/L
0.50
11/17/15 10:28
my
5.0
11/17/15 10:28
NTU
1.0
11/17/15 10:28
mg/L
2.0
11/17/15 10:28
mg/L
5.0
11/17/15 10:28
ug/L
5.0
11/11/15 18:14
ug/L
500
11/12/15 23:21
ug/L
5.0
11/11/15 18:14
ug/L
100
11/11/15 18:14
ug/L
5000
11/11/15 18:14
ug/L
5000
11/11/15 18:14
ng/L
0.50
11/11/1515:15 B
mg/L
5.0
11/17/15 18:59
mg/L
250
11/11/1515:48 D6
mg/L
2.0
11/10/15 09:07
mg/L
5.0
11/12/15 19:48
mg/L
1.0
11/08/15 03:06
ug/L
5.0
11/17/15 10:29
ug/L
100
11/17/15 10:29
ug/L
5.0
11/17/15 10:29
Std. Units
0.10
11/17/15 10:29
deg C
0.50
11/17/15 10:29
umhos/cm
1.0
11/17/1510:29
mg/L
0.50
11/17/15 10:29
my
5.0
11/17/15 10:29
NTU
1.0
11/17/15 10:29
mg/L
2.0
11/17/15 10:29
11/17/15 10:29
ug/L
5.0
11/11/15 18:26
ug/L
100
11/11/15 18:26
ug/L
5.0
11/11/15 18:26
ug/L
100
11/11/15 18:26
ug/L
5000
11/11/15 18:26
ug/L
10.0
11/11/15 18:26
ng/L
0.50
11/11/1516:01 B
mg/L
5.0
11/17/15 19:18
mg/L
50.0
11/11/15 15:49
mg/L
2.0
11/10/15 09:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Oimlifiars
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SUMMARY OF DETECTION
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92275067002
SWP-2
SM 4500 -CI -E
Chloride
2.6
mg/L
1.0
11/12/15 19:49
SM 5310B
Total Organic Carbon
0.72J
mg/L
1.0
11/08/15 03:19
92275067003
Q06V09
Collected By
MPS
11/17/15 10:31
Collected Date
11/6/15
11/17/15 10:31
Collected Time
12:30
11/17/15 10:31
Field pH
6.2
Std. Units
0.10
11/17/15 10:31
Field Temperature
19.5
deg C
0.50
11/17/15 10:31
Static Water Level
29.43
feet
11/17/15 10:31
Field Specific Conductance
1377
umhos/cm
1.0
11/17/15 10:31
Oxygen, Dissolved
2.79
mg/L
11/17/15 10:31
REDOX
144.9
mV
11/17/1510:31
Turbidity
9.26
NTU
1.0
11/17/1510:31
Odor
No odor
11/17/15 10:31
Appearance
Clear
11/17/15 10:31
EPA 6010
Antimony
5.4
ug/L
5.0
11/19/15 22:54
EPA 6010
Barium
317
ug/L
5.0
11/19/15 22:54
EPA 6010
Calcium
179000
ug/L
500
11/20/1514:17
EPA 6010
Cobalt
13.3
ug/L
5.0
11/19/15 22:54
EPA 6010
Magnesium
82300
ug/L
100
11/19/15 22:54
EPA 6010
Nickel
18.0
ug/L
5.0
11/19/15 22:54
EPA 6010
Potassium
5200
ug/L
5000
11/19/15 22:54
EPA 6010
Sodium
28600
ug/L
5000
11/19/15 22:54
EPA 6010
Vanadium
8.9
ug/L
5.0
11/19/15 22:54
EPA 6010
Zinc
9.2J
ug/L
10.0
11/19/15 22:54
EPA 1631E
Mercury
0.937
ng/L
0.50
11/11/1516:09 B
SM 2320B
Alkalinity, Total as CaCO3
776
mg/L
5.0
11/17/15 21:25
SM 2540C
Total Dissolved Solids
110
mg/L
25.0
11/10/15 10:22
EPA 300.0
Sulfate
5.1
mg/L
2.0
11/16/1516:10
SM 4500 -CI -E
Chloride
57.3
mg/L
5.0
11/17/15 20:25
SM 5310B
Total Organic Carbon
4.7
mg/L
1.0
11/10/15 21:32
92275067004
Q06V10
Collected By
MPS
11/17/15 10:36
Collected Date
11/6/15
11/17/15 10:36
Collected Time
11:30
11/17/15 10:36
Field pH
6.8
Std. Units
0.10
11/17/15 10:36
Field Temperature
16.7
deg C
0.50
11/17/15 10:36
Static Water Level
24.23
feet
11/17/15 10:36
Field Specific Conductance
24
umhos/cm
1.0
11/17/15 10:36
Oxygen, Dissolved
6.49
mg/L
11/17/15 10:36
REDOX
80.0
mV
11/17/1510:36
Turbidity
19.57
NTU
1.0
11/17/1510:36
Odor
No odor
11/17/15 10:36
Appearance
Clear to
11/17/15 10:36
muddy
EPA 6010
Barium
11.9
ug/L
5.0
11/19/15 23:06
REPORT OF LABORATORY ANALYSIS
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SUMMARY OF DETECTION
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92275067004
QO6V10
EPA 6010
Calcium
1220
ug/L
100
11/19/15 23:06
EPA 6010
Cobalt
2.7J
ug/L
5.0
11/19/15 23:06
EPA 6010
Copper
2.6J
ug/L
5.0
11/19/15 23:06
EPA 6010
Magnesium
832
ug/L
100
11/19/15 23:06
EPA 6010
Nickel
3.OJ
ug/L
5.0
11/19/15 23:06
EPA 6010
Zinc
7AJ
ug/L
10.0
11/19/15 23:06
EPA 1631E
Mercury
52.7
ng/L
0.50
11/11/1516:16
SM 2320B
Alkalinity, Total as CaCO3
6.0
mg/L
5.0
11/18/15 16:59
SM 2540C
Total Dissolved Solids
62.0
mg/L
25.0
11/10/15 10:23
EPA 300.0
Sulfate
2.3
mg/L
2.0
11/16/1516:24
SM 4500 -CI -E
Chloride
3.4
mg/L
1.0
11/19/15 18:26
92275067005
QO6V11
Collected By
MPS
11/17/15 10:38
Collected Date
11/6/15
11/17/15 10:38
Collected Time
11:50
11/17/15 10:38
Field pH
6.2
Std. Units
0.10
11/17/15 10:38
Field Temperature
15.4
deg C
0.50
11/17/15 10:38
Static Water Level
35.43
feet
11/17/15 10:38
Field Specific Conductance
75
umhos/cm
1.0
11/17/15 10:38
Oxygen, Dissolved
3.81
mg/L
11/17/15 10:38
REDOX
103.0
my
11/17/1510:38
Turbidity
9.02
NTU
1.0
11/17/1510:38
Odor
No odor
11/17/15 10:38
Appearance
Clear
11/17/15 10:38
EPA 6010
Barium
6.9
ug/L
5.0
11/19/15 23:09
EPA 6010
Calcium
6540
ug/L
100
11/19/15 23:09
EPA 6010
Magnesium
2870
ug/L
100
11/19/15 23:09
EPA 6010
Sodium
4090J
ug/L
5000
11/20/1517:20
EPA 1631E
Mercury
1.07
ng/L
0.50
11/11/1516:25 B
SM 2320B
Alkalinity, Total as CaCO3
27.3
mg/L
5.0
11/18/15 17:31
SM 2540C
Total Dissolved Solids
72.0
mg/L
25.0
11/10/15 10:23
EPA 300.0
Sulfate
4.8
mg/L
2.0
11/16/1516:37
SM 4500 -CI -E
Chloride
1.7
mg/L
1.0
11/19/15 18:27
92275067007
Trip Blank
EPA 8260
Methylene Chloride
1.0J
ug/L
2.0
11/10/15 16:01
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: SWP-1 Lab ID: 92275067001 Collected: 11/05/15 13:45 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
Field Specific Conductance
Oxygen, Dissolved
REDOX
Turbidity
Odor
Appearance
6010 ICP Groundwater
Antimony
Arsenic
Barium
Cadmium
Calcium
Chromium
Cobalt
Copper
Lead
Magnesium
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
1631E Mercury,Low Level
Mercury
8270 MSSV HVI Semivol Organic
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Date: 11/30/2015 02:17 PM
Analytical Method
MPS
ug/L
10.0
1
11/12/1515:39
11/17/15 10:28
83-32-9
11/5/15
ug/L
10.0
1
11/12/1515:39
11/17/15 10:28
208-96-8
13:45
ug/L
10.0
1
11/12/1515:39
11/17/15 10:28
62-53-3
7.6
Std. Units
0.10
1
11/12/1515:39
11/17/15 10:28
120-12-7
18.4
deg C
0.50
1
11/12/1515:39
11/17/15 10:28
56-55-3
1034
umhos/cm
1.0
1
11/12/1515:39
11/17/1510:28
50-32-8
6.94
mg/L
10.0
1
11/12/1515:39
11/17/1510:28
7782-44-7
188.6
mV
10.0
1
11/12/1515:39
11/17/1510:28
191-24-2
106.9
NTU
1.0
1
11/12/1515:39
11/17/1510:28
207-08-9
No odor
1
11/17/15 10:28
Rusty tint,
1
11/17/15 10:28
opaque
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-36-0
ND
ug/L
10.0
1
11/10/15 20:00
11/11/15 18:14
7440-38-2
182
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-39-3
ND
ug/L
1.0
1
11/10/15 20:00
11/11/15 18:14
7440-43-9
39600
ug/L
500
5
11/10/15 20:00
11/12/15 23:21
7440-70-2
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-47-3
9.3
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-48-4
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-50-8
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7439-92-1
48000
ug/L
100
1
11/10/15 20:00
11/11/15 18:14
7439-95-4
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-02-0
12100
ug/L
5000
1
11/10/15 20:00
11/11/15 18:14
7440-09-7
ND
ug/L
10.0
1
11/10/15 20:00
11/11/15 18:14
7782-49-2
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-22-4
20300
ug/L
5000
1
11/10/15 20:00
11/11/15 18:14
7440-23-5
ND
ug/L
5.4
1
11/10/15 20:00
11/11/15 18:14
7440-28-0
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:14
7440-62-2
ND
uq/L
10.0
1
11/10/15 20:00
11/11/15 18:14
7440-66-6
Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
0.643 ng/L 0.50 1 11/11/1513:00 11/11/1515:15 7439-97-6 B
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
83-32-9
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
208-96-8
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
62-53-3
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
120-12-7
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
56-55-3
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
50-32-8
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
205-99-2
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
191-24-2
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 77

aceAnalytical
-pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-1 Lab ID: 92275067001 Collected: 11/05/15 13:45 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Benzoic Acid
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:02
65-85-0
Benzyl alcohol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 17:02
100-51-6
4-13romophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:02
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
85-68-7
4 -Chloro -3-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:02
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:02
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:02
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:02
108-60-1
2-Chloronaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
91-58-7
2 -Chlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:02
7005-72-3
Chrysene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
132-64-9
1,2 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:02
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
84-66-2
2,4 -Dimethylphenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
84-74-2
4,6-Dinitro-2-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:02
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:02
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
11/12/1515:39
11/13/1517:02
117-81-7
Fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
206-44-0
Fluorene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
193-39-5
Isophorone
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
78-59-1
1 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
90-12-0
2 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:02
Naphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:02
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:02
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:02
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
98-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-1
Lab ID: 92275067001 Collected: 11/05/15
13:45
Received: 11/06/15 07:20 Matrix: Water
Parameters
Results
Units
PQL
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV HVI Semivol Organic
Analytical Method:
EPA 8270 Preparation Method: EPA 3510
2-Nitrophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:02
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
86-30-6
Pentachlorophenol
ND
ug/L
25.0
1
11/12/1515:39
11/13/1517:02
87-86-5
Phenanthrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
85-01-8
Phenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
108-95-2
Pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
120-82-1
2,4,5 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:02
88-06-2
Surrogates
Nitrobenzene -d5 (S)
81
%
21-110
1
11/12/15 15:39
11/13/15 17:02
4165-60-0
2-Fluorobiphenyl (S)
80
%
27-110
1
11/12/15 15:39
11/13/15 17:02
321-60-8
Terphenyl-d14 (S)
77
%
31-107
1
11/12/15 15:39
11/13/15 17:02
1718-51-0
Phenol -d6 (S)
25
%
10-110
1
11/12/15 15:39
11/13/15 17:02
13127-88-3
2-Fluorophenol (S)
32
%
12-110
1
11/12/15 15:39
11/13/15 17:02
367-12-4
2,4,6-Tribromophenol (S)
62
%
27-110
1
11/12/15 15:39
11/13/15 17:02
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/15 21:46
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/15 21:46
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/15 21:46
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/15 21:46
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/15 21:46
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/15 21:46
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/15 21:46
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 21:46
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 21:46
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/15 21:46
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/15 21:46
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/15 21:46
74-87-3 M1
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 21:46
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 21:46
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/15 21:46
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/15 21:46
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 21:46
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/15 21:46
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/15 21:46
75-71-8 M1
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/15 21:46
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/15 21:46
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/15 21:46
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-1 Lab ID: 92275067001 Collected: 11/05/15 13:45 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 21:46
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 21:46
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 21:46
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/15 21:46
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 21:46
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/15 21:46
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 21:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 21:46
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 21:46
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/15 21:46
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/15 21:46
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/15 21:46
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/15 21:46
99-87-6
Methylene Chloride
ND
ug/L
2.0
1
11/10/15 21:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 21:46
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 21:46
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/15 21:46
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/15 21:46
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 21:46
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 21:46
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/15 21:46
127-18-4
Toluene
ND
ug/L
1.0
1
11/10/15 21:46
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 21:46
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 21:46
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 21:46
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/10/15 21:46
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/10/15 21:46
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/10/15 21:46
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/10/15 21:46
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/10/15 21:46
75-01-4
Xylene (Total)
ND
ug/L
2.0
1
11/10/15 21:46
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/10/15 21:46
179601-23-1
o -Xylene
ND
ug/L
1.0
1
11/10/15 21:46
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
11/10/15 21:46
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70-130
1
11/10/15 21:46
17060-07-0
Toluene -d8 (S)
101
%
70-130
1
11/10/15 21:46
2037-26-5
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 549 mg/L 5.0 1 11/17/15 18:59
2540C Total Dissolved Solids Analytical Method: SM 2540C
Total Dissolved Solids 420 mg/L 250 1 11/11/15 15:48 D6
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 77

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: SWP-1
Lab ID: 92275067001 Collected: 11/05/15 13:45
Received: 11/06/15 07:20 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2.0 mg/L 2.0
1
11/10/1509:07
14808-79-8
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
30.8 mg/L 5.0
5
11/12/1519:48
16887-00-6
5310B TOC
Analytical Method: SM 53108
Total Organic Carbon
8.1 mg/L 1.0
1
11/08/15 03:06
7440-44-0
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 77

aceAnalytical
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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SWP-2 Lab ID: 92275067002 Collected: 11/05/15 12:35 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
Field Specific Conductance
Oxygen, Dissolved
REDOX
Turbidity
Odor
Appearance
6010 ICP Groundwater
Antimony
Arsenic
Barium
Cadmium
Calcium
Chromium
Cobalt
Copper
Lead
Magnesium
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
1631E Mercury,Low Level
Mercury
8270 MSSV HVI Semivol Organic
Analytical Method
MPS
ND
ug/L
1
1
11/17/15 10:29
11/13/1517:27
11/5/15
Acenaphthylene
ND
1
10.0
11/17/15 10:29
11/12/1515:39
12:35
208-96-8
Aniline
1
ug/L
11/17/15 10:29
1
7.5
Std. Units
0.10
1
ND
11/17/15 10:29
10.0
16.3
deg C
0.50
1
Benzo(a)anthracene
11/17/15 10:29
ug/L
280
umhos/cm
1.0
1
56-55-3
11/17/1510:29
ND
9.26
mg/L
1
1
11/13/1517:27
11/17/1510:29
7782-44-7
184.3
mV
10.0
1
11/12/1515:39
11/17/1510:29
205-99-2
17.65
NTU
1.0
1
1
11/17/1510:29
11/13/1517:27
No odor
Benzo(k)fluoranthene
ND
1
10.0
11/17/15 10:29
11/12/1515:39
Clear,
207-08-9
1
ANALYSIS
11/17/15 10:29
rusty
This report shall not
be reproduced, except
in full,
sediment
without
the written consent
of Pace Analytical Services,
Inc..
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-36-0
ND
ug/L
10.0
1
11/10/15 20:00
11/11/15 18:26
7440-38-2
89.8
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-39-3
ND
ug/L
1.0
1
11/10/15 20:00
11/11/15 18:26
7440-43-9
41700
ug/L
100
1
11/10/15 20:00
11/11/15 18:26
7440-70-2
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-47-3
3.3J
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-48-4
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-50-8
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7439-92-1
5930
ug/L
100
1
11/10/15 20:00
11/11/15 18:26
7439-95-4
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-02-0
ND
ug/L
5000
1
11/10/15 20:00
11/11/15 18:26
7440-09-7
ND
ug/L
10.0
1
11/10/15 20:00
11/11/15 18:26
7782-49-2
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-22-4
11100
ug/L
5000
1
11/10/15 20:00
11/11/15 18:26
7440-23-5
ND
ug/L
5.4
1
11/10/15 20:00
11/11/15 18:26
7440-28-0
ND
ug/L
5.0
1
11/10/15 20:00
11/11/15 18:26
7440-62-2
5.81
ug/L
10.0
1
11/10/15 20:00
11/11/15 18:26
7440-66-6
Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
0.726 ng/L 0.50 1 11/11/1513:00 11/11/1516:01 7439-97-6 B
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
208-96-8
Aniline
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
62-53-3
Anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
207-08-9
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 11/30/2015 02:17 PM
without
the written consent
of Pace Analytical Services,
Inc..
Page 13 of 77

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-2 Lab ID: 92275067002 Collected: 11/05/15 12:35 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Benzoic Acid
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:27
65-85-0
Benzyl alcohol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 17:27
100-51-6
4-13romophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:27
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
85-68-7
4 -Chloro -3-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:27
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:27
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:27
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:27
108-60-1
2-Chloronaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
91-58-7
2 -Chlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:27
7005-72-3
Chrysene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
132-64-9
1,2 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:27
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
84-66-2
2,4 -Dimethylphenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
84-74-2
4,6-Dinitro-2-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:27
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:27
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
11/12/1515:39
11/13/1517:27
117-81-7
Fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
206-44-0
Fluorene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
193-39-5
Isophorone
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
78-59-1
1 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
90-12-0
2 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 17:27
Naphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:27
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:27
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1517:27
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
98-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 77

aceAnalytical
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Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-2
Parameters
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92275067002 Collected: 11/05/15 12:35 Received: 11/06/15 07:20 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Nitrophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1517:27
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
86-30-6
Pentachlorophenol
ND
ug/L
25.0
1
11/12/1515:39
11/13/1517:27
87-86-5
Phenanthrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
85-01-8
Phenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
108-95-2
Pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
120-82-1
2,4,5 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1517:27
88-06-2
Surrogates
Nitrobenzene -d5 (S)
78
%
21-110
1
11/12/15 15:39
11/13/15 17:27
4165-60-0
2-Fluorobiphenyl (S)
79
%
27-110
1
11/12/15 15:39
11/13/15 17:27
321-60-8
Terphenyl-d14 (S)
84
%
31-107
1
11/12/15 15:39
11/13/15 17:27
1718-51-0
Phenol -d6 (S)
28
%
10-110
1
11/12/15 15:39
11/13/15 17:27
13127-88-3
2-Fluorophenol (S)
36
%
12-110
1
11/12/15 15:39
11/13/15 17:27
367-12-4
2,4,6-Tribromophenol (S)
50
%
27-110
1
11/12/15 15:39
11/13/15 17:27
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/15 20:02
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/15 20:02
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/15 20:02
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/15 20:02
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/15 20:02
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/15 20:02
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/15 20:02
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 20:02
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 20:02
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/15 20:02
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/15 20:02
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/15 20:02
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 20:02
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 20:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/15 20:02
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/15 20:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 20:02
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/15 20:02
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/15 20:02
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/15 20:02
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/15 20:02
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/15 20:02
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: SWP-2 Lab ID: 92275067002 Collected: 11/05/15 12:35 Received: 11/06/15 07:20 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 20:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 20:02
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 20:02
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/15 20:02
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 20:02
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/15 20:02
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 20:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 20:02
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 20:02
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/15 20:02
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/15 20:02
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/15 20:02
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/15 20:02
99-87-6
Methylene Chloride
ND
ug/L
2.0
1
11/10/15 20:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 20:02
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 20:02
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/15 20:02
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/15 20:02
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 20:02
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 20:02
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/15 20:02
127-18-4
Toluene
ND
ug/L
1.0
1
11/10/15 20:02
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 20:02
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 20:02
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 20:02
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/10/15 20:02
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/10/15 20:02
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/10/15 20:02
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/10/15 20:02
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/10/15 20:02
75-01-4
Xylene (Total)
ND
ug/L
2.0
1
11/10/15 20:02
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/10/15 20:02
179601-23-1
o -Xylene
ND
ug/L
1.0
1
11/10/15 20:02
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
11/10/15 20:02
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70-130
1
11/10/15 20:02
17060-07-0
Toluene -d8 (S)
101
%
70-130
1
11/10/15 20:02
2037-26-5
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 140 mg/L 5.0 1 11/17/15 19:18
2540C Total Dissolved Solids Analytical Method: SM 2540C
Total Dissolved Solids 122 mg/L 50.0 1 11/11/15 15:49
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 77

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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: SWP-2
Lab ID: 92275067002 Collected: 11/05/15 12:35
Received: 11/06/15 07:20 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
8.6 mg/L 2.0
1
11/10/1509:20
14808-79-8
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
2.6 mg/L 1.0
1
11/12/1519:49
16887-00-6
5310B TOC
Analytical Method: SM 53108
Total Organic Carbon
0.72J mg/L 1.0
1
11/08/15 03:19
7440-44-0
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V09 Lab ID: 92275067003 Collected: 11/06/15 12:30 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method
Collected By
MPS
ug/L
5.0
1
11/17/15 10:31
Collected Date
11/6/15
Arsenic
ND
1
11/17/15 10:31
Collected Time
12:30
11/19/15 22:54
7440-38-2
1
11/17/15 10:31
Field pH
6.2
Std. Units
0.10
1
11/17/15 10:31
Field Temperature
19.5
deg C
0.50
1
11/17/15 10:31
Static Water Level
29.43
feet
179000
1
11/17/15 10:31
Field Specific Conductance
1377
umhos/cm
1.0
1
11/17/15 10:31
Oxygen, Dissolved
2.79
mg/L
11/12/15 19:30
1
11/17/15 10:31 7782-44-7
REDOX
144.9
mV
5.0
1
11/17/1510:31
Turbidity
9.26
NTU
1.0
1
11/17/1510:31
Odor
No odor
11/19/15 22:54
7440-50-8
1
11/17/15 10:31
Appearance
Clear
1
11/12/15 19:30
1
11/17/15 10:31
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
5.4
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-36-0
Arsenic
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 22:54
7440-38-2
Barium
317
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-39-3
Cadmium
ND
ug/L
1.0
1
11/12/15 19:30
11/19/15 22:54
7440-43-9
Calcium
179000
ug/L
500
5
11/12/1519:30
11/20/1514:17
7440-70-2
Chromium
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-47-3
Cobalt
13.3
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-48-4
Copper
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-50-8
Lead
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7439-92-1
Magnesium
82300
ug/L
100
1
11/12/15 19:30
11/19/15 22:54
7439-95-4
Nickel
18.0
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-02-0
Potassium
5200
ug/L
5000
1
11/12/15 19:30
11/19/15 22:54
7440-09-7
Selenium
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 22:54
7782-49-2
Silver
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-22-4
Sodium
28600
ug/L
5000
1
11/12/15 19:30
11/19/15 22:54
7440-23-5
Thallium
ND
ug/L
5.4
1
11/12/15 19:30
11/19/15 22:54
7440-28-0
Vanadium
8.9
ug/L
5.0
1
11/12/15 19:30
11/19/15 22:54
7440-62-2
Zinc
9.2J
ug/L
10.0
1
11/12/15 19:30
11/19/15 22:54
7440-66-6
1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
Mercury 0.937 ng/L 0.50 1 11/11/1513:00 11/11/1516:09 7439-97-6 B
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
208-96-8
Aniline
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
62-53-3
Anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
207-08-9
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 77

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V09
Lab ID: 92275067003
Collected: 11/06/15
12:30
Received: 11/06/15 16:05 Matrix: Water
Parameters
Results
Units
PQL
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV HVI Semivol Organic
Analytical Method:
EPA 8270
Preparation Method: EPA 3510
Benzoic Acid
ND
ug/L
50.0
1
11/12/1515:39
11/13/1518:18
65-85-0
M1
Benzyl alcohol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 18:18
100-51-6
4-13romophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 18:18
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
85-68-7
M1
4 -Chloro -3-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1518:18
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1518:18
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 18:18
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 18:18
108-60-1
2-Chloronaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
91-58-7
2 -Chlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 18:18
7005-72-3
Chrysene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
132-64-9
1,2 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
11/12/1515:39
11/13/1518:18
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
84-66-2
2,4 -Dimethylphenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
84-74-2
4,6-Dinitro-2-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1518:18
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1518:18
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
121-14-2
M1
2,6-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
606-20-2
M1
Di-n-octylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
117-84-0
M1
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
11/12/1515:39
11/13/1518:18
117-81-7
M1
Fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
206-44-0
Fluorene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
118-74-1
M1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
193-39-5
Isophorone
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
78-59-1
1 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
90-12-0
2 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 18:18
Naphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1518:18
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1518:18
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1518:18
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
98-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 77

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Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V09
Parameters
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92275067003 Collected: 11/06/15 12:30 Received: 11/06/15 16:05 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Nitrophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1518:18
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
86-30-6
Pentachlorophenol
ND
ug/L
25.0
1
11/12/1515:39
11/13/1518:18
87-86-5
Phenanthrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
85-01-8
Phenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
108-95-2
Pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
120-82-1
2,4,5 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1518:18
88-06-2
Surrogates
Nitrobenzene -d5 (S)
89
%
21-110
1
11/12/15 15:39
11/13/15 18:18
4165-60-0
2-Fluorobiphenyl (S)
89
%
27-110
1
11/12/15 15:39
11/13/15 18:18
321-60-8
Terphenyl-d14 (S)
78
%
31-107
1
11/12/15 15:39
11/13/15 18:18
1718-51-0
Phenol -d6 (S)
31
%
10-110
1
11/12/15 15:39
11/13/15 18:18
13127-88-3
2-Fluorophenol (S)
41
%
12-110
1
11/12/15 15:39
11/13/15 18:18
367-12-4
2,4,6-Tribromophenol (S)
82
%
27-110
1
11/12/15 15:39
11/13/15 18:18
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/15 22:03
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/15 22:03
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/15 22:03
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/15 22:03
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/15 22:03
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/15 22:03
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/15 22:03
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 22:03
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 22:03
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/15 22:03
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/15 22:03
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/15 22:03
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:03
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/15 22:03
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/15 22:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 22:03
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/15 22:03
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/15 22:03
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/15 22:03
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/15 22:03
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:03
75-35-4
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V09 Lab ID: 92275067003 Collected: 11/06/15 12:30 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:03
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:03
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:03
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:03
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:03
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 22:03
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/15 22:03
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/15 22:03
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/15 22:03
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/15 22:03
99-87-6
Methylene Chloride
ND
ug/L
2.0
1
11/10/15 22:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 22:03
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 22:03
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/15 22:03
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/15 22:03
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:03
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:03
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/15 22:03
127-18-4
Toluene
ND
ug/L
1.0
1
11/10/15 22:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:03
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:03
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:03
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/10/15 22:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/10/15 22:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/10/15 22:03
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/10/15 22:03
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/10/15 22:03
75-01-4
Xylene (Total)
ND
ug/L
2.0
1
11/10/15 22:03
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/10/15 22:03
179601-23-1
o -Xylene
ND
ug/L
1.0
1
11/10/15 22:03
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
11/10/15 22:03
460-00-4
1,2-Dichloroethane-d4 (S)
111
%
70-130
1
11/10/15 22:03
17060-07-0
Toluene -d8 (S)
101
%
70-130
1
11/10/15 22:03
2037-26-5
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 776 mg/L 5.0 1 11/17/15 21:25
2540C Total Dissolved Solids Analytical Method: SM 2540C
Total Dissolved Solids 110 mg/L 25.0 1 11/10/15 10:22
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 77

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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: Q06V09
Lab ID: 92275067003 Collected: 11/06/15 12:30
Received: 11/06/15 16:05 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
5.1 mg/L 2.0
1
11/16/1516:10
14808-79-8
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
57.3 mg/L 5.0
5
11/17/1520:25
16887-00-6
5310B TOC
Analytical Method: SM 53108
Total Organic Carbon
4.7 mg/L 1.0
1
11/10/1521:32
7440-44-0
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 77

aceAnalytical
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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: Q06V10 Lab ID: 92275067004 Collected: 11/06/15 11:30 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
Static Water Level
Field Specific Conductance
Oxygen, Dissolved
REDOX
Turbidity
Odor
Appearance
6010 ICP Groundwater
Antimony
Arsenic
Barium
Cadmium
Calcium
Chromium
Cobalt
Copper
Lead
Magnesium
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
1631E Mercury,Low Level
Mercury
8270 MSSV HVI Semivol Organic
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Date: 11/30/2015 02:17 PM
Analytical Method
MPS
ug/L
10.0
1
11/12/1515:39
11/17/15 10:36
83-32-9
11/6/15
ug/L
10.0
1
11/12/1515:39
11/17/15 10:36
208-96-8
11:30
ug/L
10.0
1
11/12/1515:39
11/17/15 10:36
62-53-3
6.8
Std. Units
0.10
1
11/12/1515:39
11/17/15 10:36
120-12-7
16.7
deg C
0.50
1
11/12/1515:39
11/17/15 10:36
56-55-3
24.23
feet
10.0
1
11/12/1515:39
11/17/1510:36
50-32-8
24
umhos/cm
1.0
1
11/12/1515:39
11/17/1510:36
205-99-2
6.49
mg/L
10.0
1
11/12/1515:39
11/17/1510:36
7782-44-7
80.0
mV
1
11/17/1510:36
19.57
NTU
1.0
1
11/17/1510:36
No odor
1
11/17/15 10:36
Clear to
1
11/17/15 10:36
muddy
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-36-0
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:06
7440-38-2
11.9
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-39-3
ND
ug/L
1.0
1
11/12/15 19:30
11/19/15 23:06
7440-43-9
1220
ug/L
100
1
11/12/15 19:30
11/19/15 23:06
7440-70-2
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-47-3
2.7J
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-48-4
2.6J
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-50-8
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7439-92-1
832
ug/L
100
1
11/12/15 19:30
11/19/15 23:06
7439-95-4
3.OJ
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-02-0
ND
ug/L
5000
1
11/12/15 19:30
11/19/15 23:06
7440-09-7
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:06
7782-49-2
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-22-4
ND
ug/L
5000
1
11/12/1519:30
11/20/1517:17
7440-23-5
ND
ug/L
5.4
1
11/12/15 19:30
11/19/15 23:06
7440-28-0
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:06
7440-62-2
7AJ
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:06
7440-66-6
Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
52.7 ng/L 0.50 1 11/11/1513:00 11/11/1516:16 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
83-32-9
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
208-96-8
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
62-53-3
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
120-12-7
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
56-55-3
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
50-32-8
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
205-99-2
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
191-24-2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 23 of 77

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V10 Lab ID: 92275067004 Collected: 11/06/15 11:30 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Benzo(k)fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
207-08-9
Benzoic Acid
ND
ug/L
50.0
1
11/12/1515:39
11/13/1519:09
65-85-0
Benzyl alcohol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 19:09
100-51-6
4-13romophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 19:09
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
85-68-7
4 -Chloro -3-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1519:09
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1519:09
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 19:09
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 19:09
108-60-1
2-Chloronaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
91-58-7
2 -Chlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 19:09
7005-72-3
Chrysene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
132-64-9
1,2 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
11/12/1515:39
11/13/1519:09
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
84-66-2
2,4 -Dimethylphenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
84-74-2
4,6-Dinitro-2-m ethyl phenol
ND
ug/L
20.0
1
11/12/1515:39
11/13/1519:09
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1519:09
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
11/12/1515:39
11/13/1519:09
117-81-7
Fluoranthene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
206-44-0
Fluorene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
193-39-5
Isophorone
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
78-59-1
1 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
90-12-0
2 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 19:09
Naphthalene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1519:09
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
11/12/1515:39
11/13/1519:09
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
11/12/1515:39
11/13/1519:09
100-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 77

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Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V10
Parameters
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92275067004 Collected: 11/06/15 11:30 Received: 11/06/15 16:05 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Nitrobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
98-95-3
2-Nitrophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/12/1515:39
11/13/1519:09
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
86-30-6
Pentachlorophenol
ND
ug/L
25.0
1
11/12/1515:39
11/13/1519:09
87-86-5
Phenanthrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
85-01-8
Phenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
108-95-2
Pyrene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
120-82-1
2,4,5 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
10.0
1
11/12/1515:39
11/13/1519:09
88-06-2
Surrogates
Nitrobenzene -d5 (S)
75
%
21-110
1
11/12/15 15:39
11/13/15 19:09
4165-60-0
2-Fluorobiphenyl (S)
79
%
27-110
1
11/12/15 15:39
11/13/15 19:09
321-60-8
Terphenyl-d14 (S)
87
%
31-107
1
11/12/15 15:39
11/13/15 19:09
1718-51-0
Phenol -d6 (S)
29
%
10-110
1
11/12/15 15:39
11/13/15 19:09
13127-88-3
2-Fluorophenol (S)
38
%
12-110
1
11/12/15 15:39
11/13/15 19:09
367-12-4
2,4,6-Tribromophenol (S)
52
%
27-110
1
11/12/15 15:39
11/13/15 19:09
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/15 22:38
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/15 22:38
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/15 22:38
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/15 22:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/15 22:38
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/15 22:38
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/15 22:38
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 22:38
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 22:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/15 22:38
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/15 22:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/15 22:38
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:38
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/15 22:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/15 22:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 22:38
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/15 22:38
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/15 22:38
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/15 22:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/1522:38
107-06-2
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V10 Lab ID: 92275067004 Collected: 11/06/15 11:30 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:38
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:38
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:38
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:38
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:38
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:38
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 22:38
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/15 22:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/15 22:38
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/15 22:38
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/15 22:38
99-87-6
Methylene Chloride
ND
ug/L
2.0
1
11/10/15 22:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 22:38
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 22:38
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/15 22:38
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/15 22:38
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:38
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/15 22:38
127-18-4
Toluene
ND
ug/L
1.0
1
11/10/15 22:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:38
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:38
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:38
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/10/15 22:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/10/15 22:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/10/15 22:38
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/10/15 22:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/10/15 22:38
75-01-4
Xylene (Total)
ND
ug/L
2.0
1
11/10/15 22:38
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/10/15 22:38
179601-23-1
o -Xylene
ND
ug/L
1.0
1
11/10/15 22:38
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
11/10/15 22:38
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70-130
1
11/10/15 22:38
17060-07-0
Toluene -d8 (S)
102
%
70-130
1
11/10/15 22:38
2037-26-5
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 6.0 mg/L 5.0 1 11/18/15 16:59
2540C Total Dissolved Solids Analytical Method: SM 2540C
Total Dissolved Solids 62.0 mg/L 25.0 1 11/10/15 10:23
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 26 of 77

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: Q06V10
Lab ID: 92275067004 Collected: 11/06/15 11:30
Received: 11/06/15 16:05 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2.3 mg/L 2.0
1
11/16/1516:24
14808-79-8
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
3.4 mg/L 1.0
1
11/19/1518:26
16887-00-6
5310B TOC
Analytical Method: SM 53108
Total Organic Carbon
ND mg/L 1.0
1
11/10/1521:42
7440-44-0
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V11 Lab ID: 92275067005 Collected: 11/06/15 11:50 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method
Collected By
MPS
ug/L
5.0
1
11/17/15 10:38
Collected Date
11/6/15
Arsenic
ND
1
11/17/15 10:38
Collected Time
11:50
11/19/15 23:09
7440-38-2
1
11/17/15 10:38
Field pH
6.2
Std. Units
0.10
1
11/17/15 10:38
Field Temperature
15.4
deg C
0.50
1
11/17/15 10:38
Static Water Level
35.43
feet
6540
1
11/17/15 10:38
Field Specific Conductance
75
umhos/cm
1.0
1
11/17/15 10:38
Oxygen, Dissolved
3.81
mg/L
11/12/15 19:30
1
11/17/15 10:38 7782-44-7
REDOX
103.0
mV
5.0
1
11/17/1510:38
Turbidity
9.02
NTU
1.0
1
11/17/1510:38
Odor
No odor
11/19/15 23:09
7440-50-8
1
11/17/15 10:38
Appearance
Clear
1
11/12/15 19:30
1
11/17/15 10:38
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-36-0
Arsenic
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:09
7440-38-2
Barium
6.9
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-39-3
Cadmium
ND
ug/L
1.0
1
11/12/15 19:30
11/19/15 23:09
7440-43-9
Calcium
6540
ug/L
100
1
11/12/15 19:30
11/19/15 23:09
7440-70-2
Chromium
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-47-3
Cobalt
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-48-4
Copper
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-50-8
Lead
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7439-92-1
Magnesium
2870
ug/L
100
1
11/12/15 19:30
11/19/15 23:09
7439-95-4
Nickel
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-02-0
Potassium
ND
ug/L
5000
1
11/12/15 19:30
11/19/15 23:09
7440-09-7
Selenium
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:09
7782-49-2
Silver
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-22-4
Sodium
4090J
ug/L
5000
1
11/12/1519:30
11/20/1517:20
7440-23-5
Thallium
ND
ug/L
5.4
1
11/12/15 19:30
11/19/15 23:09
7440-28-0
Vanadium
ND
ug/L
5.0
1
11/12/15 19:30
11/19/15 23:09
7440-62-2
Zinc
ND
ug/L
10.0
1
11/12/15 19:30
11/19/15 23:09
7440-66-6
1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
Mercury 1.07 ng/L 0.50 1 11/11/1513:00 11/11/1516:25 7439-97-6 B
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
208-96-8
Aniline
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
62-53-3
Anthracene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
207-08-9
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V11 Lab ID: 92275067005 Collected: 11/06/15 11:50 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Benzoic Acid
ND
ug/L
50.0
1
11/12/1515:39
11/13/1520:00
65-85-0
Benzyl alcohol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
100-51-6
4-13romophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
85-68-7
4 -Chloro -3-m ethyl phenol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
111-44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
108-60-1
2-Chloronaphthalene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
91-58-7
2 -Chlorophenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
7005-72-3
Chrysene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
132-64-9
1,2 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
84-66-2
2,4 -Dimethylphenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
84-74-2
4,6-Dinitro-2-m ethyl phenol
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/12/15 15:39
11/13/15 20:00
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
11/12/15 15:39
11/13/15 20:00
117-81-7
Fluoranthene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
206-44-0
Fluorene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
193-39-5
Isophorone
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
78-59-1
1 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
90-12-0
2 -Methylnaphthalene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
Naphthalene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
11/12/15 15:39
11/13/15 20:00
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
11/12/15 15:39
11/13/15 20:00
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
11/12/15 15:39
11/13/15 20:00
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
98-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 29 of 77

aceAnalytical
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Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V11
Parameters
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92275067005 Collected: 11/06/15 11:50 Received: 11/06/15 16:05 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
8270 MSSV HVI Semivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Nitrophenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/12/15 15:39
11/13/15 20:00
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
86-30-6
Pentachlorophenol
ND
ug/L
25.0
1
11/12/15 15:39
11/13/15 20:00
87-86-5
Phenanthrene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
85-01-8
Phenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
108-95-2
Pyrene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
120-82-1
2,4,5 -Trichlorophenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
10.0
1
11/12/15 15:39
11/13/15 20:00
88-06-2
Surrogates
Nitrobenzene -d5 (S)
85
%
21-110
1
11/12/15 15:39
11/13/15 20:00
4165-60-0
2-Fluorobiphenyl (S)
84
%
27-110
1
11/12/15 15:39
11/13/15 20:00
321-60-8
Terphenyl-d14 (S)
99
%
31-107
1
11/12/15 15:39
11/13/15 20:00
1718-51-0
Phenol -d6 (S)
27
%
10-110
1
11/12/15 15:39
11/13/15 20:00
13127-88-3
2-Fluorophenol (S)
36
%
12-110
1
11/12/15 15:39
11/13/15 20:00
367-12-4
2,4,6-Tribromophenol (S)
56
%
27-110
1
11/12/15 15:39
11/13/15 20:00
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/15 22:55
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/15 22:55
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/15 22:55
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/15 22:55
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/15 22:55
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/15 22:55
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/15 22:55
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 22:55
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 22:55
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/15 22:55
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/15 22:55
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/15 22:55
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:55
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/15 22:55
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/15 22:55
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/15 22:55
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 22:55
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/15 22:55
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/15 22:55
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/15 22:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/15 22:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:55
75-35-4
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 30 of 77

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Q06V11 Lab ID: 92275067005 Collected: 11/06/15 11:50 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:55
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/15 22:55
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:55
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:55
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/15 22:55
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:55
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:55
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/15 22:55
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 22:55
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/15 22:55
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/15 22:55
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/15 22:55
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/15 22:55
99-87-6
Methylene Chloride
ND
ug/L
2.0
1
11/10/15 22:55
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 22:55
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 22:55
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/15 22:55
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/15 22:55
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:55
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/15 22:55
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/15 22:55
127-18-4
Toluene
ND
ug/L
1.0
1
11/10/15 22:55
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/10/15 22:55
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:55
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
1
11/10/15 22:55
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/10/15 22:55
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/10/15 22:55
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
11/10/15 22:55
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
11/10/15 22:55
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
11/10/15 22:55
75-01-4
Xylene (Total)
ND
ug/L
2.0
1
11/10/15 22:55
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
11/10/15 22:55
179601-23-1
o -Xylene
ND
ug/L
1.0
1
11/10/15 22:55
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
11/10/15 22:55
460-00-4
1,2-Dichloroethane-d4 (S)
111
%
70-130
1
11/10/15 22:55
17060-07-0
Toluene -d8 (S)
102
%
70-130
1
11/10/15 22:55
2037-26-5
2320B Alkalinity Analytical Method: SM 2320B
Alkalinity, Total as CaCO3 27.3 mg/L 5.0 1 11/18/15 17:31
2540C Total Dissolved Solids Analytical Method: SM 2540C
Total Dissolved Solids 72.0 mg/L 25.0 1 11/10/15 10:23
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: Q06V11
Lab ID: 92275067005 Collected: 11/06/15 11:50
Received: 11/06/15 16:05 Matrix: Water
Parameters
Results Units PQL
DF
Prepared Analyzed
CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
4.8 mg/L 2.0
1
11/16/1516:37
14808-79-8
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
1.7 mg/L 1.0
1
11/19/1518:27
16887-00-6
5310B TOC
Analytical Method: SM 53108
Total Organic Carbon
ND mg/L 1.0
1
11/10/1521:53
7440-44-0
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Field Blank Lab ID: 92275067006 Collected: 11/06/15 12:40 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
1631E Mercury,Low Level Analytical Method: EPA 1631 E Preparation Method: EPA 1631 E
Mercury ND ng/L 0.50 1 11/11/1513:00 11/11/1516:32 7439-97-6
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 33 of 77

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Sample: Trip Blank Lab ID: 92275067007 Collected: 11/06/15 00:00 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND
ug/L
25.0
1
11/10/1516:01
67-64-1
Benzene
ND
ug/L
1.0
1
11/10/1516:01
71-43-2
Bromobenzene
ND
ug/L
1.0
1
11/10/1516:01
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
11/10/1516:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/10/1516:01
75-27-4
Bromoform
ND
ug/L
1.0
1
11/10/1516:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/10/1516:01
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/10/15 16:01
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
11/10/15 16:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/10/1516:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/10/1516:01
75-00-3
Chloroform
ND
ug/L
1.0
1
11/10/1516:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/10/1516:01
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
11/10/1516:01
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/10/1516:01
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
11/10/1516:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/10/1516:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/10/15 16:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
11/10/1516:01
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/1516:01
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/1516:01
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
1
11/10/1516:01
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/10/1516:01
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/10/1516:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/10/1516:01
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/10/1516:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/1516:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/10/1516:01
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/10/1516:01
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
11/10/1516:01
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
11/10/1516:01
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
11/10/1516:01
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/1516:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/10/1516:01
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/10/15 16:01
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
11/10/1516:01
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
11/10/1516:01
87-68-3
2-Hexanone
ND
ug/L
5.0
1
11/10/1516:01
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
11/10/1516:01
99-87-6
Methylene Chloride
1.0J
ug/L
2.0
1
11/10/15 16:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/10/15 16:01
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/10/15 16:01
1634-04-4
Naphthalene
ND
ug/L
1.0
1
11/10/1516:01
91-20-3
Styrene
ND
ug/L
1.0
1
11/10/1516:01
100-42-5
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/1516:01
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/10/1516:01
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/10/1516:01
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 34 of 77

aceAnalytical
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ANALYTICAL RESULTS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Sample: Trip Blank Lab ID: 92275067007 Collected: 11/06/15 00:00 Received: 11/06/15 16:05 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1,1,2 -Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o -Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene -d8 (S)
Date: 11/30/2015 02:17 PM
Analytical Method: EPA 8260
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
104 %
107 %
102 %
1.0
1
11/10/15 16:01
108-88-3
1.0
1
11/10/15 16:01
87-61-6
1.0
1
11/10/15 16:01
120-82-1
1.0
1
11/10/15 16:01
71-55-6
1.0
1
11/10/15 16:01
79-00-5
1.0
1
11/10/15 16:01
79-01-6
1.0
1
11/10/15 16:01
75-69-4
1.0
1
11/10/15 16:01
96-18-4
2.0
1
11/10/15 16:01
108-05-4
1.0
1
11/10/15 16:01
75-01-4
2.0
1
11/10/15 16:01
1330-20-7
2.0
1
11/10/15 16:01
179601-23-1
1.0
1
11/10/15 16:01
95-47-6
70-130
1
11/10/15 16:01
460-00-4
70-130
1
11/10/15 16:01
17060-07-0
70-130
1
11/10/15 16:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 35 of 77

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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: MERP/8639 Analysis Method: EPA 1631 E
QC Batch Method: EPA 1631E Analysis Description: 1631E Mercury,Low Level
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005, 92275067006
METHOD BLANK: 1603696 Matrix: Water
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005, 92275067006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ng/L ND 0.50 11/11/1513:16
METHOD BLANK: 1603697 Matrix: Water
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005, 92275067006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ng/L ND 0.50 11/11/1515:08
METHOD BLANK: 1603698 Matrix: Water
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005, 92275067006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ng/L 0.396J 0.50 11/11/1517:33
LABORATORY CONTROL SAMPLE: 1603699
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ng/L 5 5.11 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1603700 1603701
MS MSD
92275065001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ng/L 0.425J 25 25 25.7 26.1 101 103 71-125 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1603702 1603703
MS MSD
92275067001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ng/L 0.643 25 25 24.3 24.4 95 95 71-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 36 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: MPRP/19999 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater
Associated Lab Samples: 92275067001, 92275067002
METHOD BLANK: 1603342
Associated Lab Samples: 92275067001, 92275067002
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Cadmium
ug/L
Calcium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Lead
ug/L
Magnesium
ug/L
Nickel
ug/L
Potassium
ug/L
Selenium
ug/L
Silver
ug/L
Sodium
ug/L
Thallium
ug/L
Vanadium
ug/L
Zinc
ug/L
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
5.0
11/11/1517:47
ND
10.0
11/11/1517:47
ND
5.0
11/11/1517:47
ND
1.0
11/11/1517:47
ND
100
11/11/1517:47
ND
5.0
11/11/1517:47
ND
5.0
11/11/1517:47
ND
5.0
11/11/1517:47
ND
5.0
11/11/1517:47
ND
100
11/11/1517:47
ND
5.0
11/11/1517:47
ND
5000
11/11/1517:47
ND
10.0
11/11/1517:47
ND
5.0
11/11/1517:47
ND
5000
11/11/1517:47
ND
5.4
11/11/1517:47
ND
5.0
11/11/1517:47
ND
10.0
11/11/1517:47
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1603343
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
510
102
80-120
Arsenic
ug/L
500
494
99
80-120
Barium
ug/L
500
500
100
80-120
Cadmium
ug/L
500
489
98
80-120
Calcium
ug/L
5000
4910
98
80-120
Chromium
ug/L
500
475
95
80-120
Cobalt
ug/L
500
495
99
80-120
Copper
ug/L
500
500
100
80-120
Lead
ug/L
500
493
99
80-120
Magnesium
ug/L
5000
4520
90
80-120
Nickel
ug/L
500
486
97
80-120
Potassium
ug/L
5000
4650J
93
80-120
Selenium
ug/L
500
495
99
80-120
Silver
ug/L
250
231
93
80-120
Sodium
ug/L
5000
4680J
94
80-120
Thallium
ug/L
500
410
82
80-120
Vanadium
ug/L
500
476
95
80-120
Zinc
ug/L
500
494
99
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 37 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
1603344
1603345
MS
MSD
92273910001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
539
510
108
102
75-125
6
Arsenic
ug/L
ND
500
500
526
500
105
100
75-125
5
Barium
ug/L
47.7
500
500
578
548
106
100
75-125
5
Cadmium
ug/L
ND
500
500
516
485
103
97
75-125
6
Calcium
ug/L
13000
5000
5000
18300
18100
106
101
75-125
1
Chromium
ug/L
ND
500
500
502
471
100
94
75-125
6
Cobalt
ug/L
38.4
500
500
557
526
104
98
75-125
6
Copper
ug/L
ND
500
500
525
495
105
99
75-125
6
Lead
ug/L
ND
500
500
515
484
103
97
75-125
6
Magnesium
ug/L
6970
5000
5000
11800
11500
97
90
75-125
3
Nickel
ug/L
3.OJ
500
500
512
481
102
96
75-125
6
Potassium
ug/L
4090J
5000
5000
9150
8800
101
94
75-125
4
Selenium
ug/L
ND
500
500
524
494
104
98
75-125
6
Silver
ug/L
ND
250
250
245
228
98
91
75-125
7
Sodium
ug/L
6710
5000
5000
11800
11400
101
93
75-125
4
Thallium
ug/L
ND
500
500
432
407
86
81
75-125
6
Vanadium
ug/L
ND
500
500
508
476
101
95
75-125
6
Zinc
ug/L
ND
500
500
523
491
104
98
75-125
6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 38 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: MPRP/20016 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater
Associated Lab Samples: 92275067003, 92275067004, 92275067005
METHOD BLANK: 1605419 Matrix:
Associated Lab Samples: 92275067003, 92275067004, 92275067005
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Antimony
ug/L
ND
5.0
11/19/1521:46
Arsenic
ug/L
ND
10.0
11/19/1521:46
Barium
ug/L
ND
5.0
11/19/1521:46
Cadmium
ug/L
ND
1.0
11/19/1521:46
Calcium
ug/L
ND
100
11/19/1521:46
Chromium
ug/L
ND
5.0
11/19/1521:46
Cobalt
ug/L
ND
5.0
11/19/1521:46
Copper
ug/L
ND
5.0
11/19/1521:46
Lead
ug/L
ND
5.0
11/19/1521:46
Magnesium
ug/L
ND
100
11/19/1521:46
Nickel
ug/L
ND
5.0
11/19/1521:46
Potassium
ug/L
ND
5000
11/19/1521:46
Selenium
ug/L
ND
10.0
11/19/1521:46
Silver
ug/L
ND
5.0
11/19/1521:46
Sodium
ug/L
ND
5000
11/19/1521:46
Thallium
ug/L
ND
5.4
11/19/1521:46
Vanadium
ug/L
ND
5.0
11/19/1521:46
Zinc
ug/L
ND
10.0
11/19/1521:46
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1605420
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
473
95
80-120
Arsenic
ug/L
500
456
91
80-120
Barium
ug/L
500
474
95
80-120
Cadmium
ug/L
500
470
94
80-120
Calcium
ug/L
5000
4800
96
80-120
Chromium
ug/L
500
471
94
80-120
Cobalt
ug/L
500
468
94
80-120
Copper
ug/L
500
473
95
80-120
Lead
ug/L
500
463
93
80-120
Magnesium
ug/L
5000
4510
90
80-120
Nickel
ug/L
500
470
94
80-120
Potassium
ug/L
5000
4680J
94
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
221
88
80-120
Sodium
ug/L
5000
4680J
94
80-120
Thallium
ug/L
500
465
93
80-120
Vanadium
ug/L
500
468
94
80-120
Zinc
ug/L
500
463
93
80-120
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 39 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
1605421
1605422
MS
MSD
92275060005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
459
455
92
91
75-125
1
Arsenic
ug/L
ND
500
500
441
438
88
88
75-125
1
Barium
ug/L
4.OJ
500
500
468
461
93
91
75-125
2
Cadmium
ug/L
ND
500
500
456
452
91
90
75-125
1
Calcium
ug/L
663
5000
5000
5220
5140
91
89
75-125
2
Chromium
ug/L
26.4
500
500
462
454
87
85
75-125
2
Cobalt
ug/L
ND
500
500
456
451
91
90
75-125
1
Copper
ug/L
ND
500
500
462
457
92
91
75-125
1
Lead
ug/L
ND
500
500
449
446
90
89
75-125
1
Magnesium
ug/L
364
5000
5000
4900
4820
91
89
75-125
2
Nickel
ug/L
14.4
500
500
458
453
89
88
75-125
1
Potassium
ug/L
ND
5000
5000
4790J
4720J
89
88
75-125
Selenium
ug/L
ND
500
500
444
440
89
88
75-125
1
Silver
ug/L
ND
250
250
216
214
86
86
75-125
1
Sodium
ug/L
ND
5000
5000
5340
5270
91
90
75-125
1
Thallium
ug/L
ND
500
500
455
455
90
90
75-125
0
Vanadium
ug/L
ND
500
500
456
453
91
91
75-125
1
Zinc
ug/L
10.9
500
500
458
453
89
88
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 40 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: MSV/34220 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92275067002, 92275067007
METHOD BLANK: 1602736
Associated Lab Samples: 92275067002, 92275067007
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2 -Tetrachloroethane
ug/L
ND
1.0
11/10/1515:09
1,1,1 -Trichloroethane
ug/L
ND
1.0
11/10/1515:09
1,1,2,2 -Tetrachloroethane
ug/L
ND
1.0
11/10/1515:09
1,1,2 -Trichloroethane
ug/L
ND
1.0
11/10/1515:09
1,1-Dichloroethane
ug/L
ND
1.0
11/10/1515:09
1,1-Dichloroethene
ug/L
ND
1.0
11/10/1515:09
1,1-Dichloropropene
ug/L
ND
1.0
11/10/1515:09
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/10/1515:09
1,2,3-Trichloropropane
ug/L
ND
1.0
11/10/1515:09
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/10/1515:09
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
11/10/1515:09
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/10/15 15:09
1,2 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:09
1,2-Dichloroethane
ug/L
ND
1.0
11/10/1515:09
1,2-Dichloropropane
ug/L
ND
1.0
11/10/1515:09
1,3 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:09
1,3-Dichloropropane
ug/L
ND
1.0
11/10/1515:09
1,4 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:09
2,2-Dichloropropane
ug/L
ND
1.0
11/10/1515:09
2-Butanone (MEK)
ug/L
ND
5.0
11/10/15 15:09
2-Chlorotoluene
ug/L
ND
1.0
11/10/1515:09
2-Hexanone
ug/L
ND
5.0
11/10/1515:09
4-Chlorotoluene
ug/L
ND
1.0
11/10/1515:09
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/10/15 15:09
Acetone
ug/L
ND
25.0
11/10/1515:09
Benzene
ug/L
ND
1.0
11/10/1515:09
Bromobenzene
ug/L
ND
1.0
11/10/1515:09
Bromochloromethane
ug/L
ND
1.0
11/10/1515:09
Bromodichloromethane
ug/L
ND
1.0
11/10/1515:09
Bromoform
ug/L
ND
1.0
11/10/1515:09
Bromomethane
ug/L
ND
2.0
11/10/1515:09
Carbon tetrachloride
ug/L
ND
1.0
11/10/15 15:09
Chlorobenzene
ug/L
ND
1.0
11/10/1515:09
Chloroethane
ug/L
ND
1.0
11/10/1515:09
Chloroform
ug/L
ND
1.0
11/10/1515:09
Chloromethane
ug/L
ND
1.0
11/10/1515:09
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/10/1515:09
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/10/1515:09
Dibromochloromethane
ug/L
ND
1.0
11/10/1515:09
Dibromomethane
ug/L
ND
1.0
11/10/1515:09
Dichlorodifluoromethane
ug/L
ND
1.0
11/10/1515:09
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 41 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
METHOD BLANK: 1602736
Associated Lab Samples: 92275067002, 92275067007
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
11/10/15 15:09
Ethylbenzene
ug/L
ND
1.0
11/10/1515:09
Hexachloro-1,3-butadiene
ug/L
ND
1.0
11/10/1515:09
m&p-Xylene
ug/L
ND
2.0
11/10/1515:09
Methyl-tert-butyl ether
ug/L
ND
1.0
11/10/15 15:09
Methylene Chloride
ug/L
ND
2.0
11/10/15 15:09
Naphthalene
ug/L
ND
1.0
11/10/1515:09
o -Xylene
ug/L
ND
1.0
11/10/1515:09
p-Isopropyltoluene
ug/L
ND
1.0
11/10/1515:09
Styrene
ug/L
ND
1.0
11/10/1515:09
Tetrachloroethene
ug/L
ND
1.0
11/10/1515:09
Toluene
ug/L
ND
1.0
11/10/1515:09
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/10/1515:09
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/10/1515:09
Trichloroethene
ug/L
ND
1.0
11/10/1515:09
Trichlorofluoromethane
ug/L
ND
1.0
11/10/1515:09
Vinyl acetate
ug/L
ND
2.0
11/10/15 15:09
Vinyl chloride
ug/L
ND
1.0
11/10/15 15:09
Xylene (Total)
ug/L
ND
2.0
11/10/15 15:09
1,2-Dichloroethane-d4 (S)
%
103
70-130
11/10/15 15:09
4-Bromofluorobenzene (S)
%
101
70-130
11/10/15 15:09
Toluene -d8 (S)
%
101
70-130
11/10/15 15:09
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1602737
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2 -Tetrachloroethane
ug/L
50
49.7
99
70-130
1,1,1 -Trichloroethane
ug/L
50
52.4
105
70-130
1,1,2,2 -Tetrachloroethane
ug/L
50
47.1
94
70-130
1,1,2 -Trichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethane
ug/L
50
49.2
98
70-130
1,1-Dichloroethene
ug/L
50
51.7
103
70-132
1,1-Dichloropropene
ug/L
50
52.1
104
70-130
1,2,3-Trichlorobenzene
ug/L
50
52.9
106
70-135
1,2,3-Trichloropropane
ug/L
50
48.3
97
70-130
1,2,4-Trichlorobenzene
ug/L
50
53.5
107
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
44.8
90
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.3
105
70-130
1,2 -Dichlorobenzene
ug/L
50
47.7
95
70-130
1,2-Dichloroethane
ug/L
50
45.8
92
70-130
1,2-Dichloropropane
ug/L
50
48.4
97
70-130
1,3 -Dichlorobenzene
ug/L
50
49.6
99
70-130
1,3-Dichloropropane
ug/L
50
48.5
97
70-130
1,4 -Dichlorobenzene
ug/L
50
47.6
95
70-130
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 42 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
LABORATORY CONTROL SAMPLE:
Parameter
1602737
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
55.4
111
58-145
2-Butanone (MEK)
ug/L
100
100
100
70-145
2-Chlorotoluene
ug/L
50
46.2
92
70-130
2-Hexanone
ug/L
100
104
104
70-144
4-Chlorotoluene
ug/L
50
49.9
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-140
Acetone
ug/L
100
96.1
96
50-175
Benzene
ug/L
50
49.2
98
70-130
Bromobenzene
ug/L
50
47.9
96
70-130
Bromochloromethane
ug/L
50
52.4
105
70-130
Bromodichloromethane
ug/L
50
52.0
104
70-130
Bromoform
ug/L
50
38.8
78
70-130
Bromomethane
ug/L
50
51.9
104
54-130
Carbon tetrachloride
ug/L
50
53.2
106
70-132
Chlorobenzene
ug/L
50
47.1
94
70-130
Chloroethane
ug/L
50
43.5
87
64-134
Chloroform
ug/L
50
48.2
96
70-130
Chloromethane
ug/L
50
52.5
105
64-130
cis-1,2-Dichloroethene
ug/L
50
49.7
99
70-131
cis-1,3-Dichloropropene
ug/L
50
53.3
107
70-130
Dibromochloromethane
ug/L
50
43.9
88
70-130
Dibromomethane
ug/L
50
49.2
98
70-131
Dichlorodifluoromethane
ug/L
50
57.9
116
56-130
Diisopropyl ether
ug/L
50
52.8
106
70-130
Ethylbenzene
ug/L
50
48.0
96
70-130
Hexachloro-1,3-butadiene
ug/L
50
60.3
121
70-130
m&p-Xylene
ug/L
100
97.5
97
70-130
Methyl-tert-butyl ether
ug/L
50
52.7
105
70-130
Methylene Chloride
ug/L
50
45.8
92
63-130
Naphthalene
ug/L
50
55.8
112
70-138
o -Xylene
ug/L
50
50.6
101
70-130
p-Isopropyltoluene
ug/L
50
53.5
107
70-130
Styrene
ug/L
50
51.4
103
70-130
Tetrachloroethene
ug/L
50
47.6
95
70-130
Toluene
ug/L
50
48.5
97
70-130
trans-1,2-Dichloroethene
ug/L
50
50.6
101
70-130
trans- 1,3-Dichloropropene
ug/L
50
47.4
95
70-132
Trichloroethene
ug/L
50
47.5
95
70-130
Trichlorofluoromethane
ug/L
50
52.0
104
62-133
Vinyl acetate
ug/L
100
103
103
66-157
Vinyl chloride
ug/L
50
55.1
110
50-150
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene -d8 (S)
%
100
70-130
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 43 of 77

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
MATRIX SPIKE SAMPLE:
1602738
92275254021
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2 -Tetrachloroethane
ug/L
ND
20
19.5
97
70-130
1,1,1 -Trichloroethane
ug/L
ND
20
22.6
113
70-130
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
19.2
96
70-130
1,1,2 -Trichloroethane
ug/L
ND
20
18.9
95
70-130
1,1-Dichloroethane
ug/L
ND
20
21.8
109
70-130
1,1-Dichloroethene
ug/L
ND
20
23.6
118
70-166
1,1-Dichloropropene
ug/L
ND
20
22.4
112
70-130
1,2,3-Trichlorobenzene
ug/L
ND
20
19.5
98
70-130
1,2,3-Trichloropropane
ug/L
ND
20
19.5
98
70-130
1,2,4-Trichlorobenzene
ug/L
ND
20
19.2
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.6
93
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.8
104
70-130
1,2 -Dichlorobenzene
ug/L
ND
20
19.1
96
70-130
1,2-Dichloroethane
ug/L
ND
20
19.4
97
70-130
1,2-Dichloropropane
ug/L
ND
20
20.4
102
70-130
1,3 -Dichlorobenzene
ug/L
ND
20
20.2
101
70-130
1,3-Dichloropropane
ug/L
ND
20
20.3
102
70-130
1,4 -Dichlorobenzene
ug/L
ND
20
19.6
98
70-130
2,2-Dichloropropane
ug/L
ND
20
20.6
103
70-130
2-Butanone (MEK)
ug/L
ND
40
40.7
102
70-130
2-Chlorotoluene
ug/L
ND
20
21.1
105
70-130
2-Hexanone
ug/L
ND
40
41.8
105
70-130
4-Chlorotoluene
ug/L
ND
20
21.1
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
41.5
104
70-130
Acetone
ug/L
ND
40
36.9
85
70-130
Benzene
ug/L
ND
20
21.2
106
70-148
Bromobenzene
ug/L
ND
20
20.7
103
70-130
Bromochloromethane
ug/L
ND
20
22.0
110
70-130
Bromodichloromethane
ug/L
ND
20
20.3
101
70-130
Bromoform
ug/L
ND
20
17.0
85
70-130
Bromomethane
ug/L
ND
20
21.3
107
70-130
Carbon tetrachloride
ug/L
ND
20
21.5
107
70-130
Chlorobenzene
ug/L
ND
20
20.0
100
70-146
Chloroethane
ug/L
ND
20
22.4
112
70-130
Chloroform
ug/L
ND
20
21.2
106
70-130
Chloromethane
ug/L
ND
20
27.3
137
70-130 M1
cis-1,2-Dichloroethene
ug/L
ND
20
21.3
107
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
19.1
95
70-130
Dibromochloromethane
ug/L
ND
20
17.9
90
70-130
Dibromomethane
ug/L
ND
20
20.1
101
70-130
Dichlorodifluoromethane
ug/L
ND
20
26.5
132
70-130 M1
Diisopropyl ether
ug/L
ND
20
22.2
111
70-130
Ethylbenzene
ug/L
ND
20
20.8
104
70-130
Hexachloro-1,3-butadiene
ug/L
ND
20
24.1
121
70-130
m&p-Xylene
ug/L
ND
40
41.1
103
70-130
Methyl-tert-butyl ether
ug/L
ND
20
21.6
108
70-130
Methylene Chloride
ug/L
ND
20
17.9
90
70-130
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 44 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1602738
Units
92275254021
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Naphthalene
ug/L
ND
20
20.7
104
70-130
o -Xylene
ug/L
ND
20
20.6
103
70-130
p-Isopropyltoluene
ug/L
ND
20
21.1
105
70-130
Styrene
ug/L
ND
20
20.8
104
70-130
Tetrachloroethene
ug/L
ND
20
20.5
103
70-130
Toluene
ug/L
ND
20
20.9
105
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
21.9
109
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
19.1
95
70-130
Trichloroethene
ug/L
ND
20
20.1
100
69-151
Trichlorofluoromethane
ug/L
ND
20
24.1
120
70-130
Vinyl acetate
ug/L
ND
40
37.2
93
70-130
Vinyl chloride
ug/L
ND
20
25.3
126
70-130
1,2-Dichloroethane-d4 (S)
%
ug/L
ND
ND
101
70-130
4-Bromofluorobenzene (S)
%
Acetone
ug/L
ND
103
70-130
Toluene -d8 (S)
%
ND
100
70-130
SAMPLE DUPLICATE: 1602739
Parameter
Units
92275254022
Result
Dup
Result
1,1,1,2 -Tetrachloroethane
ug/L
ND
ND
1,1,1 -Trichloroethane
ug/L
ND
ND
1,1,2,2 -Tetrachloroethane
ug/L
ND
ND
1,1,2 -Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,1-Dichloropropene
ug/L
ND
ND
1,2,3-Trichlorobenzene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
1,2,4-Trichlorobenzene
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2 -Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,3 -Dichlorobenzene
ug/L
ND
ND
1,3-Dichloropropane
ug/L
ND
ND
1,4 -Dichlorobenzene
ug/L
ND
ND
2,2-Dichloropropane
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Chlorotoluene
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Chlorotoluene
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Benzene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 45 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
SAMPLE DUPLICATE: 1602739
Parameter
Units
92275254022
Result
Bromobenzene
ug/L
ND
Bromochloromethane
ug/L
ND
Bromodichloromethane
ug/L
ND
Bromoform
ug/L
ND
Bromomethane
ug/L
ND
Carbon tetrachloride
ug/L
ND
Chlorobenzene
ug/L
ND
Chloroethane
ug/L
ND
Chloroform
ug/L
ND
Chloromethane
ug/L
ND
cis-1,2-Dichloroethene
ug/L
ND
cis-1,3-Dichloropropene
ug/L
ND
Dibromochloromethane
ug/L
ND
Dibromomethane
ug/L
ND
Dichlorodifluoromethane
ug/L
ND
Diisopropyl ether
ug/L
ND
Ethylbenzene
ug/L
ND
Hexachloro-1,3-butadiene
ug/L
ND
m&p-Xylene
ug/L
ND
Methyl-tert-butyl ether
ug/L
ND
Methylene Chloride
ug/L
ND
Naphthalene
ug/L
ND
o -Xylene
ug/L
ND
p-Isopropyltoluene
ug/L
ND
Styrene
ug/L
ND
Tetrachloroethene
ug/L
ND
Toluene
ug/L
ND
trans-1,2-Dichloroethene
ug/L
ND
trans- 1,3-Dichloropropene
ug/L
ND
Trichloroethene
ug/L
ND
Trichlorofluoromethane
ug/L
ND
Vinyl acetate
ug/L
ND
Vinyl chloride
ug/L
ND
Xylene (Total)
ug/L
ND
1,2-Dichloroethane-d4 (S)
%
108
4-Bromofluorobenzene (S)
%
104
Toluene -d8 (S)
%
102
Dup
Result RPD
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
109
103
103
I
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 46 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: MSV/34221 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92275067001, 92275067003, 92275067004, 92275067005
METHOD BLANK: 1602781 Matrix: Water
Associated Lab Samples: 92275067001, 92275067003, 92275067004, 92275067005
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2 -Tetrachloroethane
ug/L
ND
1.0
11/10/1515:26
1,1,1 -Trichloroethane
ug/L
ND
1.0
11/10/1515:26
1,1,2,2 -Tetrachloroethane
ug/L
ND
1.0
11/10/1515:26
1,1,2 -Trichloroethane
ug/L
ND
1.0
11/10/1515:26
1,1-Dichloroethane
ug/L
ND
1.0
11/10/1515:26
1,1-Dichloroethene
ug/L
ND
1.0
11/10/1515:26
1,1-Dichloropropene
ug/L
ND
1.0
11/10/1515:26
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/10/1515:26
1,2,3-Trichloropropane
ug/L
ND
1.0
11/10/1515:26
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/10/1515:26
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
11/10/1515:26
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/10/15 15:26
1,2 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:26
1,2-Dichloroethane
ug/L
ND
1.0
11/10/1515:26
1,2-Dichloropropane
ug/L
ND
1.0
11/10/1515:26
1,3 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:26
1,3-Dichloropropane
ug/L
ND
1.0
11/10/1515:26
1,4 -Dichlorobenzene
ug/L
ND
1.0
11/10/1515:26
2,2-Dichloropropane
ug/L
ND
1.0
11/10/1515:26
2-Butanone (MEK)
ug/L
ND
5.0
11/10/15 15:26
2-Chlorotoluene
ug/L
ND
1.0
11/10/1515:26
2-Hexanone
ug/L
ND
5.0
11/10/1515:26
4-Chlorotoluene
ug/L
ND
1.0
11/10/1515:26
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/10/15 15:26
Acetone
ug/L
ND
25.0
11/10/1515:26
Benzene
ug/L
ND
1.0
11/10/1515:26
Bromobenzene
ug/L
ND
1.0
11/10/1515:26
Bromochloromethane
ug/L
ND
1.0
11/10/1515:26
Bromodichloromethane
ug/L
ND
1.0
11/10/1515:26
Bromoform
ug/L
ND
1.0
11/10/1515:26
Bromomethane
ug/L
ND
2.0
11/10/1515:26
Carbon tetrachloride
ug/L
ND
1.0
11/10/15 15:26
Chlorobenzene
ug/L
ND
1.0
11/10/1515:26
Chloroethane
ug/L
ND
1.0
11/10/1515:26
Chloroform
ug/L
ND
1.0
11/10/1515:26
Chloromethane
ug/L
ND
1.0
11/10/1515:26
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/10/1515:26
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/10/1515:26
Dibromochloromethane
ug/L
ND
1.0
11/10/1515:26
Dibromomethane
ug/L
ND
1.0
11/10/1515:26
Dichlorodifluoromethane
ug/L
ND
1.0
11/10/1515:26
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 47 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
METHOD BLANK: 1602781 Matrix: Water
Associated Lab Samples: 92275067001, 92275067003, 92275067004, 92275067005
Blank Reporting
Parameter Units Result Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
11/10/15 15:26
Ethylbenzene
ug/L
ND
1.0
11/10/1515:26
Hexachloro-1,3-butadiene
ug/L
ND
1.0
11/10/1515:26
m&p-Xylene
ug/L
ND
2.0
11/10/1515:26
Methyl-tert-butyl ether
ug/L
ND
1.0
11/10/15 15:26
Methylene Chloride
ug/L
ND
2.0
11/10/15 15:26
Naphthalene
ug/L
ND
1.0
11/10/1515:26
o -Xylene
ug/L
ND
1.0
11/10/1515:26
p-Isopropyltoluene
ug/L
ND
1.0
11/10/1515:26
Styrene
ug/L
ND
1.0
11/10/1515:26
Tetrachloroethene
ug/L
ND
1.0
11/10/1515:26
Toluene
ug/L
ND
1.0
11/10/1515:26
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/10/1515:26
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/10/1515:26
Trichloroethene
ug/L
ND
1.0
11/10/1515:26
Trichlorofluoromethane
ug/L
ND
1.0
11/10/1515:26
Vinyl acetate
ug/L
ND
2.0
11/10/15 15:26
Vinyl chloride
ug/L
ND
1.0
11/10/15 15:26
Xylene (Total)
ug/L
ND
2.0
11/10/15 15:26
1,2-Dichloroethane-d4 (S)
%
105
70-130
11/10/15 15:26
4-Bromofluorobenzene (S)
%
102
70-130
11/10/15 15:26
Toluene -d8 (S)
%
101
70-130
11/10/15 15:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1602782
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2 -Tetrachloroethane
ug/L
50
48.4
97
70-130
1,1,1 -Trichloroethane
ug/L
50
51.2
102
70-130
1,1,2,2 -Tetrachloroethane
ug/L
50
45.3
91
70-130
1,1,2 -Trichloroethane
ug/L
50
45.4
91
70-130
1,1-Dichloroethane
ug/L
50
48.4
97
70-130
1,1-Dichloroethene
ug/L
50
50.9
102
70-132
1,1-Dichloropropene
ug/L
50
51.0
102
70-130
1,2,3-Trichlorobenzene
ug/L
50
53.5
107
70-135
1,2,3-Trichloropropane
ug/L
50
46.7
93
70-130
1,2,4-Trichlorobenzene
ug/L
50
53.6
107
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
44.8
90
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.4
101
70-130
1,2 -Dichlorobenzene
ug/L
50
47.6
95
70-130
1,2-Dichloroethane
ug/L
50
44.5
89
70-130
1,2-Dichloropropane
ug/L
50
47.9
96
70-130
1,3 -Dichlorobenzene
ug/L
50
49.1
98
70-130
1,3-Dichloropropane
ug/L
50
47.5
95
70-130
1,4 -Dichlorobenzene
ug/L
50
47.1
94
70-130
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 48 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
LABORATORY CONTROL SAMPLE:
Parameter
1602782
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
54.0
108
58-145
2-Butanone (MEK)
ug/L
100
99.1
99
70-145
2-Chlorotoluene
ug/L
50
45.8
92
70-130
2-Hexanone
ug/L
100
102
102
70-144
4-Chlorotoluene
ug/L
50
49.2
98
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
104
104
70-140
Acetone
ug/L
100
94.7
95
50-175
Benzene
ug/L
50
48.6
97
70-130
Bromobenzene
ug/L
50
47.5
95
70-130
Bromochloromethane
ug/L
50
51.2
102
70-130
Bromodichloromethane
ug/L
50
50.9
102
70-130
Bromoform
ug/L
50
38.1
76
70-130
Bromomethane
ug/L
50
54.4
109
54-130
Carbon tetrachloride
ug/L
50
52.3
105
70-132
Chlorobenzene
ug/L
50
45.7
91
70-130
Chloroethane
ug/L
50
45.0
90
64-134
Chloroform
ug/L
50
48.0
96
70-130
Chloromethane
ug/L
50
53.0
106
64-130
cis-1,2-Dichloroethene
ug/L
50
48.9
98
70-131
cis-1,3-Dichloropropene
ug/L
50
52.8
106
70-130
Dibromochloromethane
ug/L
50
42.7
85
70-130
Dibromomethane
ug/L
50
48.5
97
70-131
Dichlorodifluoromethane
ug/L
50
56.1
112
56-130
Diisopropyl ether
ug/L
50
52.2
104
70-130
Ethylbenzene
ug/L
50
47.5
95
70-130
Hexachloro-1,3-butadiene
ug/L
50
62.1
124
70-130
m&p-Xylene
ug/L
100
95.4
95
70-130
Methyl-tert-butyl ether
ug/L
50
51.8
104
70-130
Methylene Chloride
ug/L
50
44.5
89
63-130
Naphthalene
ug/L
50
57.2
114
70-138
o -Xylene
ug/L
50
49.5
99
70-130
p-Isopropyltoluene
ug/L
50
54.2
108
70-130
Styrene
ug/L
50
50.1
100
70-130
Tetrachloroethene
ug/L
50
46.4
93
70-130
Toluene
ug/L
50
48.0
96
70-130
trans-1,2-Dichloroethene
ug/L
50
50.2
100
70-130
trans- 1,3-Dichloropropene
ug/L
50
47.0
94
70-132
Trichloroethene
ug/L
50
47.3
95
70-130
Trichlorofluoromethane
ug/L
50
51.1
102
62-133
Vinyl acetate
ug/L
100
101
101
66-157
Vinyl chloride
ug/L
50
55.8
112
50-150
Xylene (Total)
ug/L
150
145
97
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene -d8 (S)
%
100
70-130
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 49 of 77

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
MATRIX SPIKE SAMPLE:
1602783
92275067001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2 -Tetrachloroethane
ug/L
ND
20
19.7
99
70-130
1,1,1 -Trichloroethane
ug/L
ND
20
23.5
118
70-130
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
19.5
97
70-130
1,1,2 -Trichloroethane
ug/L
ND
20
19.4
97
70-130
1,1-Dichloroethane
ug/L
ND
20
22.8
114
70-130
1,1-Dichloroethene
ug/L
ND
20
24.1
120
70-166
1,1-Dichloropropene
ug/L
ND
20
23.5
118
70-130
1,2,3-Trichlorobenzene
ug/L
ND
20
20.8
104
70-130
1,2,3-Trichloropropane
ug/L
ND
20
20.1
100
70-130
1,2,4-Trichlorobenzene
ug/L
ND
20
20.3
101
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
19.5
97
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.5
108
70-130
1,2 -Dichlorobenzene
ug/L
ND
20
20.2
101
70-130
1,2-Dichloroethane
ug/L
ND
20
20.0
100
70-130
1,2-Dichloropropane
ug/L
ND
20
21.3
107
70-130
1,3 -Dichlorobenzene
ug/L
ND
20
21.3
106
70-130
1,3-Dichloropropane
ug/L
ND
20
21.2
106
70-130
1,4 -Dichlorobenzene
ug/L
ND
20
20.3
101
70-130
2,2-Dichloropropane
ug/L
ND
20
21.4
107
70-130
2-Butanone (MEK)
ug/L
ND
40
42.5
106
70-130
2-Chlorotoluene
ug/L
ND
20
22.7
114
70-130
2-Hexanone
ug/L
ND
40
43.3
108
70-130
4-Chlorotoluene
ug/L
ND
20
22.0
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
43.7
109
70-130
Acetone
ug/L
ND
40
44.9
102
70-130
Benzene
ug/L
ND
20
21.8
109
70-148
Bromobenzene
ug/L
ND
20
21.1
106
70-130
Bromochloromethane
ug/L
ND
20
23.2
116
70-130
Bromodichloromethane
ug/L
ND
20
20.9
104
70-130
Bromoform
ug/L
ND
20
17.7
89
70-130
Bromomethane
ug/L
ND
20
25.1
126
70-130
Carbon tetrachloride
ug/L
ND
20
22.7
114
70-130
Chlorobenzene
ug/L
ND
20
20.4
102
70-146
Chloroethane
ug/L
ND
20
21.7
109
70-130
Chloroform
ug/L
ND
20
22.0
110
70-130
Chloromethane
ug/L
ND
20
27.7
139
70-130 M1
cis-1,2-Dichloroethene
ug/L
ND
20
22.1
111
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
20.2
101
70-130
Dibromochloromethane
ug/L
ND
20
18.6
93
70-130
Dibromomethane
ug/L
ND
20
20.7
104
70-130
Dichlorodifluoromethane
ug/L
ND
20
27.0
135
70-130 M1
Diisopropyl ether
ug/L
ND
20
23.0
115
70-130
Ethylbenzene
ug/L
ND
20
21.1
106
70-130
Hexachloro-1,3-butadiene
ug/L
ND
20
24.9
125
70-130
m&p-Xylene
ug/L
ND
40
42.3
106
70-130
Methyl-tert-butyl ether
ug/L
ND
20
22.7
114
70-130
Methylene Chloride
ug/L
ND
20
21.6
106
70-130
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 50 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1602783
Units
92275067001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Naphthalene
ug/L
ND
20
22.3
111
70-130
o -Xylene
ug/L
ND
20
21.1
106
70-130
p-Isopropyltoluene
ug/L
ND
20
22.6
113
70-130
Styrene
ug/L
ND
20
21.5
107
70-130
Tetrachloroethene
ug/L
ND
20
20.4
102
70-130
Toluene
ug/L
ND
20
21.6
108
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
23.2
116
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
19.5
98
70-130
Trichloroethene
ug/L
ND
20
21.0
105
69-151
Trichlorofluoromethane
ug/L
ND
20
24.1
120
70-130
Vinyl acetate
ug/L
ND
40
39.9
100
70-130
Vinyl chloride
ug/L
ND
20
26.0
130
70-130
1,2-Dichloroethane-d4 (S)
%
ug/L
ND
ND
104
70-130
4-Bromofluorobenzene (S)
%
Acetone
ug/L
ND
100
70-130
Toluene -d8 (S)
%
ND
100
70-130
SAMPLE DUPLICATE: 1602784
Parameter
Units
92275067003
Result
Dup
Result
1,1,1,2 -Tetrachloroethane
ug/L
ND
ND
1,1,1 -Trichloroethane
ug/L
ND
ND
1,1,2,2 -Tetrachloroethane
ug/L
ND
ND
1,1,2 -Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,1-Dichloropropene
ug/L
ND
ND
1,2,3-Trichlorobenzene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
1,2,4-Trichlorobenzene
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2 -Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,3 -Dichlorobenzene
ug/L
ND
ND
1,3-Dichloropropane
ug/L
ND
ND
1,4 -Dichlorobenzene
ug/L
ND
ND
2,2-Dichloropropane
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Chlorotoluene
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Chlorotoluene
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Benzene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 51 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
SAMPLE DUPLICATE: 1602784
Parameter
Units
92275067003
Result
Bromobenzene
ug/L
ND
Bromochloromethane
ug/L
ND
Bromodichloromethane
ug/L
ND
Bromoform
ug/L
ND
Bromomethane
ug/L
ND
Carbon tetrachloride
ug/L
ND
Chlorobenzene
ug/L
ND
Chloroethane
ug/L
ND
Chloroform
ug/L
ND
Chloromethane
ug/L
ND
cis-1,2-Dichloroethene
ug/L
ND
cis-1,3-Dichloropropene
ug/L
ND
Dibromochloromethane
ug/L
ND
Dibromomethane
ug/L
ND
Dichlorodifluoromethane
ug/L
ND
Diisopropyl ether
ug/L
ND
Ethylbenzene
ug/L
ND
Hexachloro-1,3-butadiene
ug/L
ND
m&p-Xylene
ug/L
ND
Methyl-tert-butyl ether
ug/L
ND
Methylene Chloride
ug/L
ND
Naphthalene
ug/L
ND
o -Xylene
ug/L
ND
p-Isopropyltoluene
ug/L
ND
Styrene
ug/L
ND
Tetrachloroethene
ug/L
ND
Toluene
ug/L
ND
trans-1,2-Dichloroethene
ug/L
ND
trans- 1,3-Dichloropropene
ug/L
ND
Trichloroethene
ug/L
ND
Trichlorofluoromethane
ug/L
ND
Vinyl acetate
ug/L
ND
Vinyl chloride
ug/L
ND
Xylene (Total)
ug/L
ND
1,2-Dichloroethane-d4 (S)
%
111
4-Bromofluorobenzene (S)
%
103
Toluene -d8 (S)
%
101
Dup
Result RPD
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
110
102
101
I
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 52 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: OEXT/39029 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV HVI
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005
METHOD BLANK: 1605123 Matrix: Water
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
11/13/1514:56
1,2 -Dichlorobenzene
ug/L
ND
10.0
11/13/1514:56
1,3 -Dichlorobenzene
ug/L
ND
10.0
11/13/1514:56
1,4 -Dichlorobenzene
ug/L
ND
10.0
11/13/1514:56
1 -Methylnaphthalene
ug/L
ND
10.0
11/13/1514:56
2,4,5 -Trichlorophenol
ug/L
ND
10.0
11/13/1514:56
2,4,6 -Trichlorophenol
ug/L
ND
10.0
11/13/1514:56
2,4-Dichlorophenol
ug/L
ND
10.0
11/13/1514:56
2,4 -Dimethylphenol
ug/L
ND
10.0
11/13/1514:56
2,4-Dinitrophenol
ug/L
ND
50.0
11/13/1514:56
2,4-Dinitrotoluene
ug/L
ND
10.0
11/13/1514:56
2,6-Dinitrotoluene
ug/L
ND
10.0
11/13/1514:56
2-Chloronaphthalene
ug/L
ND
10.0
11/13/1514:56
2 -Chlorophenol
ug/L
ND
10.0
11/13/1514:56
2 -Methylnaphthalene
ug/L
ND
10.0
11/13/1514:56
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
11/13/1514:56
2-Nitroaniline
ug/L
ND
50.0
11/13/1514:56
2-Nitrophenol
ug/L
ND
10.0
11/13/1514:56
3&4 -Methyl phenol (m&p Cresol)
ug/L
ND
10.0
11/13/15 14:56
3,3'-Dichlorobenzidine
ug/L
ND
20.0
11/13/1514:56
3-Nitroaniline
ug/L
ND
50.0
11/13/1514:56
4,6-Dinitro-2-m ethyl phenol
ug/L
ND
20.0
11/13/1514:56
4-Bromophenylphenyl ether
ug/L
ND
10.0
11/13/15 14:56
4 -Chloro -3-m ethyl phenol
ug/L
ND
20.0
11/13/1514:56
4-Chloroaniline
ug/L
ND
20.0
11/13/1514:56
4-Chlorophenylphenyl ether
ug/L
ND
10.0
11/13/15 14:56
4-Nitroaniline
ug/L
ND
20.0
11/13/1514:56
4-Nitrophenol
ug/L
ND
50.0
11/13/1514:56
Acenaphthene
ug/L
ND
10.0
11/13/1514:56
Acenaphthylene
ug/L
ND
10.0
11/13/1514:56
Aniline
ug/L
ND
10.0
11/13/1514:56
Anthracene
ug/L
ND
10.0
11/13/1514:56
Benzo(a)anthracene
ug/L
ND
10.0
11/13/1514:56
Benzo(a)pyrene
ug/L
ND
10.0
11/13/1514:56
Benzo(b)fluoranthene
ug/L
ND
10.0
11/13/1514:56
Benzo(g,h,i)perylene
ug/L
ND
10.0
11/13/1514:56
Benzo(k)fluoranthene
ug/L
ND
10.0
11/13/1514:56
Benzoic Acid
ug/L
ND
50.0
11/13/1514:56
Benzyl alcohol
ug/L
ND
20.0
11/13/15 14:56
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
11/13/1514:56
bis(2-Chloroethyl) ether
ug/L
ND
10.0
11/13/15 14:56
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 53 of 77

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
METHOD BLANK: 1605123 Matrix: Water
Associated Lab Samples: 92275067001, 92275067002, 92275067003, 92275067004, 92275067005
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroisopropyl) ether
ug/L
ND
10.0
11/13/15 14:56
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
11/13/1514:56
Butylbenzylphthalate
ug/L
ND
10.0
11/13/1514:56
Chrysene
ug/L
ND
10.0
11/13/1514:56
Di-n-butylphthalate
ug/L
ND
10.0
11/13/1514:56
Di-n-octylphthalate
ug/L
ND
10.0
11/13/1514:56
Dibenz(a,h)anthracene
ug/L
ND
10.0
11/13/1514:56
Dibenzofuran
ug/L
ND
10.0
11/13/1514:56
Diethylphthalate
ug/L
ND
10.0
11/13/1514:56
Dimethylphthalate
ug/L
ND
10.0
11/13/1514:56
Fluoranthene
ug/L
ND
10.0
11/13/1514:56
Fluorene
ug/L
ND
10.0
11/13/1514:56
Hexachloro-1,3-butadiene
ug/L
ND
10.0
11/13/1514:56
Hexachlorobenzene
ug/L
ND
10.0
11/13/1514:56
Hexachlorocyclopentadiene
ug/L
ND
10.0
11/13/1514:56
Hexachloroethane
ug/L
ND
10.0
11/13/1514:56
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
11/13/1514:56
Isophorone
ug/L
ND
10.0
11/13/1514:56
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
11/13/1514:56
N-Nitrosodimethylamine
ug/L
ND
10.0
11/13/1514:56
N-Nitrosodiphenylamine
ug/L
ND
10.0
11/13/1514:56
Naphthalene
ug/L
ND
10.0
11/13/1514:56
Nitrobenzene
ug/L
ND
10.0
11/13/1514:56
Pentachlorophenol
ug/L
ND
25.0
11/13/1514:56
Phenanthrene
ug/L
ND
10.0
11/13/1514:56
Phenol
ug/L
ND
10.0
11/13/1514:56
Pyrene
ug/L
ND
10.0
11/13/1514:56
2,4,6-Tribromophenol (S)
%
39
27-110
11/13/15 14:56
2-Fluorobiphenyl (S)
%
69
27-110
11/13/15 14:56
2-Fluorophenol (S)
%
34
12-110
11/13/15 14:56
Nitrobenzene -d5 (S)
%
73
21-110
11/13/15 14:56
Phenol -d6 (S)
%
29
10-110
11/13/15 14:56
Terphenyl-d14 (S)
%
82
31-107
11/13/15 14:56
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
LABORATORY CONTROL SAMPLE:
1605124
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
35.8
72
31-120
1,2 -Dichlorobenzene
ug/L
50
33.8
68
38-120
1,3 -Dichlorobenzene
ug/L
50
30.7
61
30-122
1,4 -Dichlorobenzene
ug/L
50
33.2
66
37-120
1 -Methylnaphthalene
ug/L
50
41.0
82
34-113
2,4,5 -Trichlorophenol
ug/L
50
34.3
69
43-113
2,4,6 -Trichlorophenol
ug/L
50
34.7
69
42-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 54 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
LABORATORY CONTROL SAMPLE:
Parameter
1605124
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4-DichIoro phenol
ug/L
50
34.5
69
30-120
2,4 -Dimethylphenol
ug/L
50
37.1
74
29-111
2,4-Dinitrophenol
ug/L
250
80.7
32
19-132
2,4-Dinitrotoluene
ug/L
50
35.3
71
58-128
2,6-Dinitrotoluene
ug/L
50
36.5
73
54-129
2-Chloronaphthalene
ug/L
50
33.7
67
43-117
2 -Chlorophenol
ug/L
50
29.8
60
37-120
2 -Methylnaphthalene
ug/L
50
39.2
78
33-120
2-Methylphenol(o-Cresol)
ug/L
50
25.7
51
31-120
2-Nitroaniline
ug/L
100
53.9
54
48-121
2-Nitrophenol
ug/L
50
30.3
61
25-116
3&4 -Methyl phenol (m&p Cresol)
ug/L
50
23.6
47
23-120
3,3'-Dichlorobenzidine
ug/L
100
80.8
81
10-154
3-Nitroaniline
ug/L
100
57.7
58
43-115
4,6-Dinitro-2-m ethyl phenol
ug/L
100
55.2
55
44-124
4-Bromophenylphenyl ether
ug/L
50
39.8
80
34-113
4 -Chloro -3-m ethyl phenol
ug/L
100
79.9
80
31-110
4-Chloroaniline
ug/L
100
70.1
70
20-120
4-Chlorophenylphenyl ether
ug/L
50
34.0
68
34-116
4-Nitroaniline
ug/L
100
47.0
47
46-128
4-Nitrophenol
ug/L
250
50.4
20
11-120
Acenaphthene
ug/L
50
39.3
79
48-114
Acenaphthylene
ug/L
50
38.7
77
48-112
Aniline
ug/L
50
14.5
29
26-120
Anthracene
ug/L
50
44.5
89
57-118
Benzo(a)anthracene
ug/L
50
49.2
98
56-121
Benzo(a)pyrene
ug/L
50
47.7
95
55-127
Benzo(b)fluoranthene
ug/L
50
45.3
91
53-128
Benzo(g,h,i)perylene
ug/L
50
54.0
108
54-125
Benzo(k)fluoranthene
ug/L
50
54.1
108
51-123
Benzoic Acid
ug/L
250
74.4
30
10-120
Benzyl alcohol
ug/L
100
58.6
59
27-120
bis(2-Chloroethoxy)methane
ug/L
50
36.7
73
32-120
bis(2-Chloroethyl) ether
ug/L
50
31.3
63
33-111
bis(2-Chloroisopropyl) ether
ug/L
50
20.9
42
15-120
bis(2-Ethylhexyl)phthalate
ug/L
50
51.5
103
50-145
Butylbenzylphthalate
ug/L
50
54.0
108
54-138
Chrysene
ug/L
50
50.8
102
58-127
Di-n-butylphthalate
ug/L
50
49.4
99
56-125
Di-n-octylphthalate
ug/L
50
51.2
102
50-134
Dibenz(a,h)anthracene
ug/L
50
53.7
107
53-129
Dibenzofuran
ug/L
50
35.7
71
45-120
Diethylphthalate
ug/L
50
41.8
84
53-120
Dimethylphthalate
ug/L
50
42.1
84
55-116
Fluoranthene
ug/L
50
44.8
90
57-125
Fluorene
ug/L
50
40.1
80
53-118
Hexachloro-1,3-butadiene
ug/L
50
34.7
69
23-120
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 55 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
LABORATORY CONTROL SAMPLE:
1605124
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachlorobenzene
ug/L
50
53.1
106
49-116
Hexachlorocyclopentadiene
ug/L
50
30.1
60
26-158
Hexachloroethane
ug/L
50
31.2
62
30-114
Indeno(1,2,3-cd)pyrene
ug/L
50
55.6
111
55-128
Isophorone
ug/L
50
44.6
89
31-118
N-Nitroso-di-n-propylamine
ug/L
50
34.7
69
32-119
N-Nitrosodimethylamine
ug/L
50
22.8
46
13-120
N-Nitrosodiphenylamine
ug/L
50
40.4
81
43-120
Naphthalene
ug/L
50
36.1
72
32-120
Nitrobenzene
ug/L
50
36.3
73
33-110
Pentachlorophenol
ug/L
100
70.7
71
10-137
Phenanthrene
ug/L
50
44.3
89
57-117
Phenol
ug/L
50
12.7
25
10-120
Pyrene
ug/L
50
53.5
107
55-122
2,4,6-Tribromophenol (S)
%
95
27-110
2-Fluorobiphenyl (S)
%
69
27-110
2-Fluorophenol(S)
%
37
12-110
Nitrobenzene-d5(S)
%
77
21-110
Phenol -d6 (S)
%
25
10-110
Terphenyl-d14 (S)
%
99
31-107
MATRIX SPIKE SAMPLE:
1605125
92275067003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
50
45.0
90
10-110
1,2 -Dichlorobenzene
ug/L
ND
50
41.3
83
10-110
1,3 -Dichlorobenzene
ug/L
ND
50
37.8
76
10-110
1,4 -Dichlorobenzene
ug/L
ND
50
41.5
83
10-110
1 -Methylnaphthalene
ug/L
ND
50
51.8
104
14-110
2,4,5 -Trichlorophenol
ug/L
ND
50
46.3
93
19-105
2,4,6 -Trichlorophenol
ug/L
ND
50
46.3
93
13-108
2,4-Dichlorophenol
ug/L
ND
50
44.3
89
29-111
2,4 -Dimethylphenol
ug/L
ND
50
44.5
89
21-103
2,4-Dinitrophenol
ug/L
ND
250
135
54
10-109
2,4-Dinitrotoluene
ug/L
ND
50
40.2
80
27-104 M1
2,6-Dinitrotoluene
ug/L
ND
50
44.5
89
28-101 M1
2-Chloronaphthalene
ug/L
ND
50
42.2
84
14-102
2 -Chlorophenol
ug/L
ND
50
37.3
75
16-110
2 -Methylnaphthalene
ug/L
ND
50
49.2
98
13-110
2-Methylphenol(o-Cresol)
ug/L
ND
50
32.3
65
19-110
2-Nitroaniline
ug/L
ND
100
67.7
68
26-103
2-Nitrophenol
ug/L
ND
50
40.5
81
20-110
3&4 -Methyl phenol (m&p Cresol)
ug/L
ND
50
31.0
62
20-110
3,3'-Dichlorobenzidine
ug/L
ND
100
33.7
34
25-112
3-Nitroaniline
ug/L
ND
100
51.0
51
29-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 56 of 77

aceAnalytical
-pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
MATRIX SPIKE SAMPLE:
1605125
92275067003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
4,6-Dinitro-2-m ethyl phenol
ug/L
ND
100
93.7
94
10-117
4-Bromophenylphenyl ether
ug/L
ND
50
49.3
99
20-105
4 -Chloro -3 -methyl phenol
ug/L
ND
100
102
102
22-110
4-Chloroaniline
ug/L
ND
100
55.7
56
20-100
4-Chlorophenylphenyl ether
ug/L
ND
50
40.8
82
19-102
4-Nitroaniline
ug/L
ND
100
49.9
50
29-110
4-Nitrophenol
ug/L
ND
250
80.7
32
10-110
Acenaphthene
ug/L
ND
50
47.8
96
17-100
Acenaphthylene
ug/L
ND
50
46.0
92
21-100
Aniline
ug/L
ND
50
12.4
25
10-110
Anthracene
ug/L
ND
50
51.4
103
24-109
Benzo(a)anthracene
ug/L
ND
50
52.2
104
22-117
Benzo(a)pyrene
ug/L
ND
50
50.5
101
23-104
Benzo(b)fluoranthene
ug/L
ND
50
47.8
96
23-103
Benzo(g,h,i)perylene
ug/L
ND
50
54.9
110
18-111
Benzo(k)fluoranthene
ug/L
ND
50
55.0
110
22-113
Benzoic Acid
ug/L
ND
250
35.6J
14
10-110 M1
Benzyl alcohol
ug/L
ND
100
71.5
71
19-101
bis(2-Chloroethoxy)methane
ug/L
ND
50
43.7
87
22-110
bis(2-Chloroethyl) ether
ug/L
ND
50
38.1
76
16-110
bis(2-Chloroisopropyl) ether
ug/L
ND
50
30.4
61
14-110
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
57.0
114
23-102 M1
Butylbenzylphthalate
ug/L
ND
50
59.0
118
25-110 M1
Chrysene
ug/L
ND
50
55.2
110
23-115
Di-n-butylphthalate
ug/L
ND
50
54.3
109
26-110
Di-n-octylphthalate
ug/L
ND
50
61.1
122
22-110 M1
Dibenz(a,h)anthracene
ug/L
ND
50
55.7
111
21-112
Dibenzofuran
ug/L
ND
50
43.8
88
19-102
Diethylphthalate
ug/L
ND
50
48.4
97
29-110
Dimethylphthalate
ug/L
ND
50
48.6
97
27-110
Fluoranthene
ug/L
ND
50
47.3
95
23-112
Fluorene
ug/L
ND
50
48.0
96
22-104
Hexachloro-1,3-butadiene
ug/L
ND
50
42.9
86
10-110
Hexachlorobenzene
ug/L
ND
50
63.5
127
21-116 M1
Hexachlorocyclopentadiene
ug/L
ND
50
40.5
81
10-110
Hexachloroethane
ug/L
ND
50
39.2
78
10-110
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
56.4
113
20-113
Isophorone
ug/L
ND
50
55.6
111
50-150
N-Nitroso-di-n-propylamine
ug/L
ND
50
41.9
84
21-105
N-Nitrosodimethylamine
ug/L
ND
50
30.4
61
10-110
N-Nitrosodiphenylamine
ug/L
ND
50
46.4
93
23-107
Naphthalene
ug/L
ND
50
44.9
90
10-110
Nitrobenzene
ug/L
ND
50
42.5
85
20-110
Pentachlorophenol
ug/L
ND
100
99.9
100
10-118
Phenanthrene
ug/L
ND
50
50.5
101
24-106
Phenol
ug/L
ND
50
18.3
37
12-110
Pyrene
ug/L
ND
50
56.4
113
24-114
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 57 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene -d5 (S)
Phenol -d6 (S)
Terphenyl-d14 (S)
1605125
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Units
92275067003 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits Qualifiers
%
121
27-110 SO
%
91
27-110
%
52
12-110
%
93
21-110
%
38
10-110
%
81
31-107
SAMPLE DUPLICATE: 1605126
Parameter
Units
92275067004
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/L
ND
ND
1,2 -Dichlorobenzene
ug/L
ND
ND
1,3 -Dichlorobenzene
ug/L
ND
ND
1,4 -Dichlorobenzene
ug/L
ND
ND
1 -Methylnaphthalene
ug/L
ND
ND
2,4,5 -Trichlorophenol
ug/L
ND
ND
2,4,6 -Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4 -Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
30.9
2,6-Dinitrotoluene
ug/L
ND
40.5
2-Chloronaphthalene
ug/L
ND
ND
2 -Chlorophenol
ug/L
ND
ND
2 -Methylnaphthalene
ug/L
ND
ND
2-Methylphenol(o-Cresol)
ug/L
ND
ND
2-Nitroaniline
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3&4 -Methyl phenol (m&p Cresol)
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
3-Nitroaniline
ug/L
ND
ND
4,6-Dinitro-2-m ethyl phenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4 -Chloro -3-m ethyl phenol
ug/L
ND
ND
4-Chloroaniline
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitroaniline
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Aniline
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
Benzo(b)fluoranthene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 58 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
SAMPLE DUPLICATE: 1605126
Parameter
Units
92275067004
Result
Dup
Result
RPD
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)fluoranthene
ug/L
ND
ND
Benzoic Acid
ug/L
ND
ND
Benzyl alcohol
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Chloroisopropyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butylbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Dibenzofuran
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
7.2J
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
52
54
5
2-Fluorobiphenyl (S)
%
79
70
12
2-Fluorophenol(S)
%
38
41
10
Nitrobenzene -d5 (S)
%
75
73
3
Phenol -d6 (S)
%
29
34
15
Terphenyl-d14 (S)
%
87
94
8
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 59 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WET/41435
Analysis Method: SM 2320B
QC Batch Method: SM 2320B
Analysis Description: 2320B Alkalinity
Associated Lab Samples: 92275067001, 92275067002,
92275067003
METHOD BLANK: 1608074
Matrix: Water
Associated Lab Samples: 92275067001, 92275067002,
92275067003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L
ND 5.0
11/17/15 15:01
LABORATORY CONTROL SAMPLE: 1608075
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L
50 49.2
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608076 1608077
MS MSD
92275800002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 3.7J
50 50 53.9
54.2 100 101 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608078 1608079
MS MSD
92275065001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 198 50 50 245 240 94 84 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 60 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WET/41436
Analysis Method: SM 2320B
QC Batch Method: SM 2320B
Analysis Description: 2320B Alkalinity
Associated Lab Samples: 92275067004, 92275067005
METHOD BLANK: 1608082
Matrix: Water
Associated Lab Samples: 92275067004, 92275067005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L
ND 5.0
11/18/15 16:37
LABORATORY CONTROL SAMPLE: 1608083
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L
50 49.7
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608084 1608085
MS MSD
92275067004
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 6.0
50 50 56.2
56.0 100 100 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608086 1608087
MS MSD
92275794004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 102 50 50 147 146 90 88 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 61 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WET/41308
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92275067003, 92275067004, 92275067005
METHOD BLANK: 1602461
Matrix:
Water
Associated Lab Samples: 92275067003, 92275067004, 92275067005
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND
25.0 11/10/15 10:13
LABORATORY CONTROL SAMPLE:
1602462
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250
236 94 90-110
SAMPLE DUPLICATE: 1602463
92275182007
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Dissolved Solids
mg/L
26100
23600 10 D6
SAMPLE DUPLICATE: 1602464
92275060013
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Dissolved Solids
mg/L
96.0
88.0 9 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 62 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WET/41340
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92275067001, 92275067002
METHOD BLANK: 1603935
Matrix: Water
Associated Lab Samples: 92275067001, 92275067002
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 11/11/15 15:47
LABORATORY CONTROL SAMPLE:
1603936
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 248 99 90-110
SAMPLE DUPLICATE: 1603937
92275067001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
420 520 21 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc.. Page 63 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25302
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92275067001, 92275067002
METHOD BLANK: 1601612
Matrix: Water
Associated Lab Samples: 92275067001, 92275067002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfate mg/L
ND 2.0
11/09/1520:57
LABORATORY CONTROL SAMPLE: 1601613
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Sulfate mg/L
20 18.5
93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1601614
1601615
MS MSD
92275059001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 2.OJ
20 20 19.7
19.9 89 90 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 64 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25410
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92275067003, 92275067004,
92275067005
METHOD BLANK: 1607342
Matrix: Water
Associated Lab Samples: 92275067003, 92275067004,
92275067005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfate mg/L
ND 2.0
11/16/1513:26
LABORATORY CONTROL SAMPLE: 1607343
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Sulfate mg/L
20 18.4
92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1607344 1607345
MS MSD
92275060014
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 13.1
20 20 34.1
33.8 105 104 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1607346 1607348
MS MSD
92275059004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 20 20 20.0 21.8 100 109 90-110 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 65 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25372
Analysis Method: SM 4500 -CI -E
QC Batch Method: SM 4500 -CI -E
Analysis Description: 4500 Chloride
Associated Lab Samples: 92275067001, 92275067002
METHOD BLANK: 1605106
Matrix: Water
Associated Lab Samples: 92275067001, 92275067002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
11/12/1519:24
LABORATORY CONTROL SAMPLE: 1605107
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride mg/L
20 20.7
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1605108 1605109
MS MSD
92275267021
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Chloride mg/L 5.4
20 20 5.6
5.8 1 2 90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1605110 1605111
MS MSD
92275282001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 21.7 40 40 43.3 43.0 54 53 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 66 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25437
Analysis Method: SM 4500 -CI -E
QC Batch Method: SM 4500 -CI -E
Analysis Description: 4500 Chloride
Associated Lab Samples: 92275067003
METHOD BLANK: 1608631
Matrix: Water
Associated Lab Samples: 92275067003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
11/17/1520:08
LABORATORY CONTROL SAMPLE: 1608632
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride mg/L
20 19.5
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608633 1608634
MS MSD
92274926001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Chloride mg/L 9.4
20 20 29.7
29.5 101 101 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1608635 1608636
MS MSD
92275639002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 56.1 1000 1000 1070 1070 101 101 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 67 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25475
Analysis Method: SM 4500 -CI -E
QC Batch Method: SM 4500 -CI -E
Analysis Description: 4500 Chloride
Associated Lab Samples: 92275067004, 92275067005
METHOD BLANK: 1611058
Matrix: Water
Associated Lab Samples: 92275067004, 92275067005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
11/19/1518:19
LABORATORY CONTROL SAMPLE: 1611059
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride mg/L
20 20.1
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1611060
1611061
MS MSD
92275115001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Chloride mg/L 15.4
20 20 34.5
34.5 95 95 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1611062 1611063
MS MSD
92275115002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 14.2 20 20 33.2 33.1 95 95 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 68 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25299
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310B TOC
Associated Lab Samples: 92275067001, 92275067002
METHOD BLANK: 1601596
Matrix: Water
Associated Lab Samples: 92275067001, 92275067002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
11/07/15 20:34
LABORATORY CONTROL SAMPLE: 1601597
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.4
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1601598 1601599
MS MSD
92274821001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 3.3
25 25 28.4
28.4 101 100 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1601600 1601601
MS MSD
92274853001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 359 25 25 413 412 216 213 90-110 0 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 69 of 77

aceAnalytical
—pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
QC Batch: WETA/25328
Analysis Method: SM 53108
QC Batch Method: SM 5310B
Analysis Description: 5310B TOC
Associated Lab Samples: 92275067003, 92275067004,
92275067005
METHOD BLANK: 1602520
Matrix: Water
Associated Lab Samples: 92275067003, 92275067004,
92275067005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
11/10/15 16:52
LABORATORY CONTROL SAMPLE: 1602521
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.7
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602522 1602523
MS MSD
92275185001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND
25 25 25.1
25.2 98 98 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602524 1602525
MS MSD
92275185002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 25.1 25.2 98 99 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/30/2015 02:17 PM without the written consent of Pace Analytical Services, Inc..
Page 70 of 77

aceAnalytical
—pacelabs.com
QUALIFIERS
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
INC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project:
Pace Project No.:
Sludge Landfill November 2015
92275067
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92275067001
SWP-1
FLD/
92275067002
SWP-2
FLD/
92275067003
Q06V09
FLD/
92275067004
Q06V10
FLD/
92275067005
Q06V11
FLD/
92275067001
SWP-1
EPA 3010
MPRP/19999
EPA6010
ICP/18033
92275067002
SWP-2
EPA 3010
MPRP/19999
EPA6010
ICP/18033
92275067003
Q06V09
EPA 3010
MPRP/20016
EPA6010
ICP/18049
92275067004
Q06V10
EPA 3010
MPRP/20016
EPA6010
ICP/18049
92275067005
Q06V11
EPA 3010
MPRP/20016
EPA6010
ICP/18049
92275067001
SWP-1
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067002
SWP-2
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067003
Q06V09
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067004
Q06V10
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067005
Q06V11
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067006
Field Blank
EPA 1631 E
MERP/8639
EPA 1631 E
MERC/8298
92275067001
SWP-1
EPA 3510
OEXT/39029
EPA 8270
MSSV/11519
92275067002
SWP-2
EPA 3510
OEXT/39029
EPA 8270
MSSV/11519
92275067003
Q06V09
EPA 3510
OEXT/39029
EPA 8270
MSSV/11519
92275067004
Q06V10
EPA 3510
OEXT/39029
EPA 8270
MSSV/11519
92275067005
Q06V11
EPA 3510
OEXT/39029
EPA 8270
MSSV/11519
92275067001
SWP-1
EPA 8260
MSV/34221
92275067002
SWP-2
EPA 8260
MSV/34220
92275067003
Q06V09
EPA 8260
MSV/34221
92275067004
Q06V10
EPA 8260
MSV/34221
92275067005
Q06V11
EPA 8260
MSV/34221
92275067007
Trip Blank
EPA 8260
MSV/34220
92275067001
SWP-1
SM 23208
WET/41435
92275067002
SWP-2
SM 23208
WET/41435
92275067003
Q06V09
SM 23208
WET/41435
92275067004
Q06V10
SM 23208
WET/41436
92275067005
Q06V11
SM 23208
WET/41436
92275067001
SWP-1
SM 2540C
WET/41340
92275067002
SWP-2
SM 2540C
WET/41340
92275067003
Q06V09
SM 2540C
WET/41308
92275067004
Q06V10
SM 2540C
WET/41308
92275067005
Q06V11
SM 2540C
WET/41308
92275067001
SWP-1
EPA 300.0
WETA/25302
92275067002
SWP-2
EPA 300.0
WETA/25302
92275067003
Q06V09
EPA 300.0
WETA/25410
92275067004
Q06V10
EPA 300.0
WETA/25410
92275067005
Q06V11
EPA 300.0
WETA/25410
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Sludge Landfill November 2015
Pace Project No.: 92275067
Lab ID
Sample ID
QC
Batch Method
QC Batch
92275067001
SWP-1
SM
4500 -CI -E
WETA/25372
92275067002
SWP-2
SM
4500 -CI -E
WETA/25372
92275067003
Q06V09
SM
4500 -CI -E
WETA/25437
92275067004
QO6V10
SM
4500 -CI -E
WETA/25475
92275067005
Q06V11
SM
4500 -CI -E
WETA/25475
92275067001
SWP-1
SM
53108
WETA/25299
92275067002
SWP-2
SM
53108
WETA/25299
92275067003
Q06V09
SM
53108
WETA/25328
92275067004
QO6V10
SM
53108
WETA/25328
92275067005
Q06V11
SM
53108
WETA/25328
Date: 11/30/2015 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Analytical Method
Analytical
Batch
Page 73 of 77

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'age 74 of 77

Client Name:�r
Courier (Circle): Fed Ex UPS USPS Client Commercial
Custody Seal on Cooler/Box Present: ❑ yes IV"� no Seals intact:
Packing Material: Ej Bubble Wrap 'Rubble Bags 1:1 None M Other
Thermometer Used: IR Gun#3 -130265963 Type of Ice: I%Wet ) Blue
IR Gun #4 SN;140290365 Other `. t. = iii
Tamn CnrmMinn C
* Page 2 of 2 is for Internal Use Only
(Pa'ce Other
n yes F] no
None Samples on Ice, cooling process has begun
Corrected Cooler Tem , (,i C
p"
Temp should be above freezing to 6°C
Document Name: Sample Condition Upon Document Revised: May 15, 2015
aceAnalytical '
Receipt (SCUR) Pae 1 of 2*
Document No.: Issuing Authorities:
❑NIA
1.
F-ASV-CS-003-rev.14 Pace Asheville Q ua I ity Office
Client Name:�r
Courier (Circle): Fed Ex UPS USPS Client Commercial
Custody Seal on Cooler/Box Present: ❑ yes IV"� no Seals intact:
Packing Material: Ej Bubble Wrap 'Rubble Bags 1:1 None M Other
Thermometer Used: IR Gun#3 -130265963 Type of Ice: I%Wet ) Blue
IR Gun #4 SN;140290365 Other `. t. = iii
Tamn CnrmMinn C
* Page 2 of 2 is for Internal Use Only
(Pa'ce Other
n yes F] no
None Samples on Ice, cooling process has begun
Corrected Cooler Tem , (,i C
p"
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No NIA
Comments:
Date and initials of person x mining
contents:
Chain of Custody Present:
OYes ONO
❑NIA
1.
Chain of Custody Filled Out:
11 Oyea
ONO
❑NIA
2.
Chain of Custody Relinquished:
IYes
❑No
❑NIA
3.
Sampler Name & Signature on COC:
OYes
❑No
El NIA
4.
Samples Arrived within Hold Time:
VY.
❑No
❑NIA
5.
Short Hold Time Analysis (<72hr);
Dyes
No
❑WA
6.
Rush Turn Around Time Requested:
Dyes
ONO
©WA
7.
Sufficient Volume:
Z Yes
❑No
❑WA
8.
Correct Containers Used:
-Pace Containers Used:
,dyes
pines
❑No
❑No
❑NIA
❑NIA
9.
Containers intact:
4yes
ONO
❑NIA
10.
Filtered volume received for Dissolved tests
Dyes
El No
12'NIA
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
fires
( i
❑No
❑NIA
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: (VOA, colirorm, TOC, &G, wl-DRO (water)
rt Yes
Yes
Yes
❑No
❑No
0 N
L1 NIA
L3 NIA
13.
Samples checked for dechlorination:
pYes
❑No
❑N/A
14.
Headspace in VOA Vials ( >6mm):
Ores
PNo
❑N!A
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
Dyes OW /11 NIA
©Yes ONO PN/A
/
16.
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: I IDato: I if t' ra T�
a
Note: Whenever there is discrepancy affecting North! Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y 1 N
WO#92275067
1111111111111111111111
Page 75 of 77

;3 s a 'n a. w A w N ITEM #
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Page 76 of 77

Client Name. �` r�. °� .�TC'
0
* Page 2 of 2 is for Internal Use Only
Courier (Circle): Fed Ex UPS LISPS Client Commercial Pace) Other
Custody Seal on Coolor/Box Present: ❑ yes [� no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ Mone ❑ Other
Thermometer Used: IR Gun#3 -9 302653 Type of Ice:C. Wet ' Blue None / Samples on ice, cooling process has begun
IR Gun #4 SNA40290365 Other:
Temp Correction Factor: {Add I Subtract f; . L: C
Corrected Cooler Tem p,:__ . � . C
Document Name: Sample Condition Upon
Document Revised: May 15, 2015
aceAnalytical
Receipt "UR)
Pa e 1 of 2*
Document No.:
Issuing Authorities:
- 'vw.pace/a6s.com
r
'
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Name. �` r�. °� .�TC'
0
* Page 2 of 2 is for Internal Use Only
Courier (Circle): Fed Ex UPS LISPS Client Commercial Pace) Other
Custody Seal on Coolor/Box Present: ❑ yes [� no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ Mone ❑ Other
Thermometer Used: IR Gun#3 -9 302653 Type of Ice:C. Wet ' Blue None / Samples on ice, cooling process has begun
IR Gun #4 SNA40290365 Other:
Temp Correction Factor: {Add I Subtract f; . L: C
Corrected Cooler Tem p,:__ . � . C
Biological Tissue is Frozen: Yes No NIA Date and initlalspf perso examining
Biolo
Temp should be above freezing to 6°C
contents: %''�`�' C.
Comments:
Chain of Custody Present:
YJYes
❑No
❑NIA 1.
Chain of Custody Filled Out:
bYes
❑No
❑N/A 2,
Chain of Custody Relinquished:Yes
❑No
0 t41 3.
Sampler Name & Signature on COC:
LYes
❑No
C7 NIA 4.
Samples Arrived within Hold Time:
OYes
❑No
❑N/A 5.
Short Hold Time Analysis (<72hr):
Dyes
AHo
❑NIA 6.
Rush Turn Around Time Requested:
❑Yes
oNo
❑NIA 7.
Sufficient Volume:
PYes
©No
❑N/A S.
Correct Containers Used:
❑Ws
ONo
0NIA 9.
-Pace Containers Used:
Yes
0 N
❑NIA
Containers Intact:
lrJYes
©No
El N/A 10.
Filtered volume received for Dissolved tests
❑Yes
❑No
NIA 11.
Sample Labels match COC:
0 N
❑N/A 12.
/pees
-Includes date/time/ID/Anal sis Matrix: U )
All containers needing preservation have been checked.
/ .yes
❑No
❑N/A 13.
All containers needing preservation are found to be in
r,�Yes
IJ No
El N/A
compliance with EPA recommendation.
T
exceptions: 1 OA? coliform, TOC, & I_DRO (water)
' Yes
❑No
Samples checked for dechlorination:
yes
❑No
❑N/A 14,
Headspace in VOA Vials (>6mrn):
Dyes
9Ho
❑NIA 15.
Trip Blank Present:
dyes
❑No
El NIA 16.
Trip Blank Custody Seals Present
Oyes
❑No
❑N/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review: Date: /! I
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
WO#:92275067
92275067
Page 77 of 77

Sludge Landfill
Q06V09 Monitoring Well - Located on west side of Sludge Landfill dam
1L
Standard
Date Sample Collected
07/06/10
11/08/10
07/19/11
11/15/11
07/10/12
11/06/12 07/02/13
11/19/13
07/10/14
11/12/14
07/30/15
11/06/15
Field Data
6.35
6.43
6.3
6.3
6.6
6.2 6.4
6.4
6.0
6.4
6.2
6.2
Field pH
6.5 to 8.5
Field Temperature (deg C)
NE
17.62
16.55
17.15
15.56
19.7
13.72 17.23
15.95
16.80
17.0
19.2
19.5
Static Water Level (feet)
NE
29.76
30.92
30.06
31.58
30.75
31.22 29.38
30.61
29.78
30.46
30.25
29.43
Field Specific Conductance (umhos/cm)
NE
1436
1436
1470
1427
1406
1497 1476
1487
1445
1466
1444
1377
Turbidity (NTU)
Substance (Detects Only)
Antimony
NE
1
9.88
ND
2.95
ND
30
ND
3.67
ND
14.8
ND
9.00 3.41
ND ND
2.42
ND
3.11
ND
3.14
4.1 J
1.60
5.6
9.26
5.4
Arsenic
10
6.5
ND
ND
ND
ND
ND 6.3 J
ND
ND
ND
ND
ND
Barium
700
331
290
306
272
304
288 309
316
296
297
301
317
Calcium
NE
189000
167000
161000
207000
149000
185000 183000
200000
183000
181000
160000
179000
Chromium
10
ND
ND
ND
ND
ND
ND ND
ND
5.2
ND
ND
ND
Cobalt
1
15.7
14.5
19.2
14.6
15.0
11.9 25.2
17.2
13.3
14.0
13.3
13.3
Magnesium
NE
85100
77500
81300
78800
79800
82500 84800
83300
79300
83900
84000
82300
Mercury
1
0.000623
0.000629
0.000561
0.00228
0.000799
0.000763 ND
0.000551
ND
ND
0.001190
0.000937
Nickel
100
12.3
10.4
18.2
16.8
18.2
16.1 18.1
15.9
19.2
19.3
17.9
18.0
Potassium
NE
7340
6520
7310
7980
7310
6810 7040
7460
6500
5000 J
4730 J
5200
Selenium
20
ND
ND
ND
ND
ND
ND ND
ND
18.5
ND
ND
ND
Sodium
NE
29200
28400
30400
34200
31600
33500 34500
36300
34800
28000
27500
28600
Vanadium
NE
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
5.5
8.9
Zinc (mg/L)
1
ND
ND
ND
ND
ND
ND ND
ND
0.0108
ND
0.0093 J
0.0092 J
Acetone (mg/L)
6
ND
ND
0.0054 J
ND
0.0023 J
ND ND
ND
ND
ND
ND
ND
Benzene
1
ND
ND
0.26 J
ND
ND
0.27 J 0.27 J
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 (mg/L)
NE
872
385
879
829
788
779 873
815
811
790
767
776
Total Dissolved Solids (mg/L)
500
888
834
836
878
857
858 892
892
871
874
851
110
Sulfate (mg/L)
250
6.1
ND
5.7
5.9
6.7
6.7 6.0
5.0
5.4
5.1
5.3
5.1
Chloride (mg/L)
250
52.6
51.4
53.8
59.7
57.5
56.9 46.4
56.5
54.4
54.9
53.8
57.3
Total Organic Carbon (mg/L)
NE
26.4
29.9
25.5
23.5
21.1
29.2 30.5
33.8
13.6
7.8
6.7
4.7
0
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
1 of 5

Sludge Landfill
Q06V10 Monitoring Well - Located on former Temporary Sludge Landfill dam
Field Data
MOSEEMIL-
Field pH
Field Temperature (dea C)
Static Water Level (feet)
Field Specific Conductance (umhos/cm
Turbidity (NTU)
Substance (Detects Only
Arsenic
Barium
Calcium
Cobalt
Nickel
Zinc (mg/L)
Acetone (mg/L)
Alkalinitv. Total as CaCO3
Total Dissolved Solids
Sulfate (mg/L)
Chloride (mg/L)
Total Oraanic Carbon
2L
Date Sample Collected
Standard 07/06/10
11/08/10
01/19/11
11/15/11
07/10/12
11/06/12 07/02/13 11/19/13
07/10/14
11/12/14
07/30/15
11/06/15
6.5 to 8.5
6.20
5.58
5.7
5.3
5.9
5.3 5.4 4.7
5.9
5.8
6.6
6.8
NE
14.15
15.13
17.68
15.38
17.2
13.57 14.82 14.74
14.20
15.7
15.7
16.7
NE
27.68
27.54
27.69
28.15
28.03
27.78 26.98 27.94
27.25
27.63
28.11
24.23
NE
33
41
60
41
39
30 22 30
17
30.0
39.0
24.0
NE
710
93.5
ND
81.3
6.0
14
ND
3.33
ND
30
ND
5.58 0.70 1.47
ND ND ND
4.05
7.2 J
2.03
ND
4.54
ND
19.57
ND
700
7.4
24.4
8.0
8.8
7.9
7.8
5.6 6.0
8.1
5.1
5.9
11.9
NE
2820
2690
3200
3080
2860
2730
1400 2210
1250
2350
2670
1220
1
ND
7.6
ND
ND
ND
ND
ND ND
ND
ND
ND
2.7 J
1000
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
2.6 J
NE
842
1110
978
1020
914
944
808 760
788
799
893
832
1
0.000694
0.0057
0.00302
0.00557
0.0157
0.0243
0.0149 0.00475
0.00312
0.00338
0.01860
0.05270
100
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
ND
1
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
ND
0.0074 J
6
ND
ND
0.0043 J
ND
ND
ND
ND ND
ND
ND
ND
ND
NE
23.3
22.3
11.5
12.8
646
9.9
6.4 8.8
6.8
9.4
9.6
6.0
500
38.8
ND
39.0
88.0
ND
ND
32.0 29.0
ND
28.0
35.0
62.0
250
ND
ND
ND
ND
2.8
2.3
2.0 2.3
2.2
2.5
2.5
2.3
250
ND
ND
ND
ND
1.2
1.7
1.2 1.7
0.90 J
1.0
2.0
3.4
NE
1.4
24.0
2.0
2.7
1.8
2.7
1.4 1.8
3.2
ND
ND
ND
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
2of5

Sludge Landfill
Q06V11 Monitoring Well - Located west of former Temporary Sludge Landfill detention basin
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
3of5
2L Date Sample
Collected
Standard 07/06/10
11/09/10
07/19/11
11/15/11
07/10/12
11/06/12
07/02/13 11/19/13
07/10/14
11/12/14
08/30/15 11/06/15
Field Data
Field pH
6.5 to 8.5
6.29
6.23
5.6
5.4
6.2
5.2
5.4 5.2
5.9
5.9
6.0 6.2
Field Temperature (deg C)
NE
15.26
14.09
17.47
14.1
17.3
12.23
17.22 15.16
14.94
14.3
18.0 15.4
Static Water Level (feet)
NE
39.54
40.06
39.03
41.30
40.83
40.31
38.60 40.67
39.03
40.06
40.69 35.43
Field Specific Conductance (umhos/cm)
NE
85
86
88
81
92
82
76 78
79
97.0
96.1 75.0
Turbidity (NTU)
Substance (Detects Only
Barium
7mm7NE
NE 13.1
70011.1
8.08
10.4
18
9.9
6.16
9.6
3.92
7.1
3.25
9.7
2.58 1.12
6.4 6.8
4.72
5.5
3.34
6.0
9.77 9.02
7.5 6.9
Calcium
5950
5300
5940
6010
5840
6000
5710 5890
5720
6660
5830 6540
Magnesium
NE
2720
2480
2620
2710
2650
2880
2520 2810
2580
2880
2660 2870
Mercury
1
ND
ND
0.000568
ND
0.000499 J
0.00274
0.000682 0.000910
0.000916
0.00105
0.00172 0.00107
Sodium
NE
ND
ND
ND
6000
5080
5010
ND ND
ND
4260 J
5130 4090 J
Zinc (mg/L)
1
ND
ND
ND
ND
ND
0.0209
ND ND
ND
ND
0.0073 J ND
Acetone (mg/L)
6
ND
ND
0.0065 J
ND
ND
ND
ND ND
ND
ND
ND ND
Alkalinity, Total as CaCO3 (mg/L)
NE
23.3
28.3
29.3
28.8
9.8
28.1
25.8 28.0
27.1
29.2
26.5 27.3
Total Dissolved Solids (mg/L)
500
69.0
50.0
51.0
115
ND
45.0
58.0 64.0
48.0
77.0
59.0 72.0
Sulfate (mg/L)
250
5.1
6.2
ND
ND
5.2
4.6
5.4 5.7
5.4
5.8
5.1 4.8
Chloride (mg/L)
250
ND
ND
ND
ND
2.3
2.3
2.1 2.0
2.0
1.5
2.2 1.7
Total Organic Carbon (mg/L)
NE
2.8
40.3
2.7
26.2
25.7
5.4
4.4 27.5
3.9
1.1
20.5 ND
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
3of5

Sludge Landfill
SWP1 Stormwater/Leachate Pipe - Located at toe of Sludge Landfill dam
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
4 of 5
2L
Standard
Date Sample
Collected
07/06/10
11/08/10
07/19/11
11/14/11
07/10/12
11/06/12
07/01/13
11/18/13
07/10/14
11/11/14
07/30/15
11/05/15
Field Data
Field pH
6.5 to 8.5
7.42
7.42
7.4
8.0
7.6
7.8
7.6
7.7
6.8
7.4
7.4
7.6
Field Temperature (deg C)
NE
21.12
16.28
20.67
14.62
20.9
11.35
21.09
17.76
21.2
16.6
20.3
18.4
Static Water Level (feet)
NE
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Field Specific Conductance (umhos/cm)
NE
1161
1289
1236
1326
1252
1463
1156
1134
491
1229
1230
1034
Turbidity (NTU)
NE
105
90
100
57.8
74.3
61.4
47.8
39.4
13.2
28.1
40
106.9
u s ance (Detects On y
Arsenic
10
8.8
8.6
ND
ND
ND
ND
ND
ND
6.0 J
ND
ND
ND
Barium
700
230
215
198
217
229
212
213
222
129
187
211
182
Boron
700
90.2
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NA
Calcium
NE
96000
99000
91000
122000
97700
114000
87100
97400
38400
94800
91900
39600
Chromium
10
ND
7.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Cobalt
1
35.4
30.2
27.5
18.9
22.2
8.2
21.4
37.8
5.7
17.9
18.6
9.3
Iron
300
15000
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ND
Magnesium
NE
68100
76700
71400
85000
72600
90900
62300
59800
18500
64800
66600
48000
Manganese
50
4610
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Mercury
1
ND
ND
ND
ND
0.000418 J
0.000795
ND
0.000597
0.00875
0.000531
0.000567
0.000643
Nickel
100
ND
ND
ND
5.4
ND
ND
ND
ND
ND
ND
ND
ND
Potassium
NE
12700
17200
16200
22800
16800
22000
10700
13900
18200
12200
12700
12100
Silcon
NE
8320
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Sodium
NE
43100
41800
41900
50000
44300
44800
39900
42200
9730
33800
38700
20300
Strontium
NE
570
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ND
Zinc (mg/L)
1
ND
ND
ND
ND
ND
ND
ND
0.0106
ND
ND
ND
ND
Vanadium
NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.3 J
ND
Acetone (mg/L)
6
NR
NR
0.0080 J
ND
0.0034 J
ND
ND
ND
ND
ND
ND
ND
Naphthalene
6
NR
NR
ND
ND
ND
ND
0.67 J
ND
ND
ND
ND
ND
Alkalinity, Total as CaCO3 (mg/L)
NE
688
760
651
748
27.3
752
654
589
210
628
591
549
Total Dissolved Solids (mg/L)
500
633
671
633
635
639
741
617
558
256
607
595
420
Total Suspended Solids (mg/L)
NE
35.3
29.8
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
BOD, 5 Day (mg/L)
NE
4.5
8.1
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Chemical Oxygen Demand (mg/L)
NE
53
58
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
Sulfate (mg/L)
250
ND
ND
ND
ND
2.4
ND
ND
ND
3.2
1.8 J
2.6
2.0
Chloride (mg/L)
250
NR
NR
46
52.8
50.4
48.9
45.0
37.9
13.4
39.2
41.9
30.8
Total Organic Carbon (mg/L)
NE
NR
NR
24.7
27.4
22.6
28.3
23.2
33.0
18.9
51.0
13.5
8.1
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
4 of 5

Sludge Landfill
SWP2 Stormwater/Groundwater Pipe - Located at toe of former Temporary Sludge Landfill dam
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
5 of 5
2L Date Sample
Collected
Standard 07/06/10
11/08/10 07/19/11
11/14/11
07/10/12
11/06/12
07/01/13 11/18/13
07/10/14
11/11/14
07/30/15 11/05/15
Field Data
Field pH
6.5 to 8.5
7.23
7.44
7.4
7.6
7.4
7.0
7.1 7.0
7.5
6.9
7.2 7.5
Field Temperature (deg C)
NE
19.02
13.20
19.85
12.95
20.2
11.88
18.08 14.56
17.90
12.9
18.1 16.3
Static Water Level (feet)
NE
NA
NA
NA
NA
NA
NA
NA NA
NA
NA
NA NA
Field Specific Conductance (umhos/cm)
NE
490
486
482
429
408
429
422 394
383
349
299 280
Turbidity (NTU)
Substance (Detects Only
Arsenic
7777700
NE
10ND
56.7
58
6.3
14
ND
35.7
ND
32.7
5.0
27.2
ND
15.3 12.5
6.5 J ND
20.6
5.1 J
6.51
ND
10.08 17.65
ND ND
Barium
162
148
164
127
142
157
150 159
121
107
102 89.8
Calcium
NE
55700
55300
58000
46900
44000
45000
45300 45900
38600
34300
30200 41700
Cobalt
1
12.4
13.1
9.9
ND
ND
ND
5.3 20.3
ND
4.2 J
4.1 J 3.3 J
Magnesium
NE
15500
14700
13900
13500
12700
13900
12000 10900
8940
9200
8320 5930
Mercury
1
ND
ND
ND
ND
0.000405 J
ND
0.000565 0.000534
ND
ND
0.000482 J 0.000726
Sodium
NE
26300
27000
25400
28700
24400
26700
19900 19600
16600
16500
16000 11100
Vanadium
NE
ND
ND
ND
ND
ND
ND
5.9 ND
ND
ND
2.8 J ND
Zinc (mg/L)
1
ND
ND
ND
ND
ND
ND
ND ND
ND
0.0055 J
ND 0.0058 J
Acetone (mg/L)
6
NR
NR
0.0052 J
ND
ND
ND
ND ND
ND
ND
ND ND
Methylene Chloride
5
NR
NR
1.7 J
ND
ND
ND
ND ND
ND
ND
ND ND
Hexachloro-1,3-butadiene
0.44
ND
ND
ND
ND
ND
ND
ND ND
ND
ND
0.92 J ND
Alkalinity, Total as CaCO3 (mg/L)
NE
285
260
232
234
205
215
228 193
178
169
138 140
Total Dissolved Solids (mg/L)
500
321
270
260
216
ND
231
236 193
191
185
148 122
Total Suspended Solids (mg/L)
NE
NR
18.8
NR
NR
NR
NR
NR NR
NR
NR
NR NR
BOD, 5 Day (mg/L)
NE
NR
2.1
NR
NR
NR
NR
NR NR
NR
NR
NR NR
Chemical Oxygen Demand (mg/L)
NE
NR
99.0
NR
NR
NR
NR
NR NR
NR
NR
NR NR
Sulfate (mg/L)
250
ND
8.3
8.8
5.0
5.2
5.8
8.4 7.5
6.8
5.0
4.1 8.6
Chloride (mg/L)
250
7.7
NR
5.8
7.0
5.7
5.4
4.5 4.1
3.7
4.0
4.1 2.6
Total Organic Carbon (mg/L)
NE
5.9
NR
5.7
5.6
4.6
40.2
36.8 5.7
4.5
17.9
0.69 J 0.72 J
All concentrations are in micrograms per liter (ug/L) unless otherwise noted.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NA - Not Applicable
ND - Not Detected
NE - Not Established
NR - Not Reported
5 of 5