NC0029122_Plan of Action_20180129

ZAPATA
TRUST- INTEGRITY• QUALITY
November 8, 2017
North Carolina Department of Environmental Quality
Division of Water Resources
Wilmington Regional Office
Attn: Tom Tharrington
1618 Mail Service Center
Raleigh, North Carolina 27699-1618
Re: North, Center, and South Wharf Lagoon Closure Plan
Military Ocean Terminal, Sunny Point
Southport, North Carolina
Project ID: NCO029122
Final Closure Certification of South Wharf Lagoon Closure Plan
Dear Mr. Tharrington,
ZAPATA Engineering of North Carolina, Inc. (ZAPATA) provides the attached documents as a final
certification for the North, Center, and South Wharf Lagoon Closure Plan, Project ID #: NC00292122,
specific to the South Wharf Lagoon within the Military Ocean Terminal, Sunny Point (MOTSU). Per the
October 9, 2017 email verification of the clay liner and sludge testing sampling testing results, the lagoon
closure activities have been completed in accordance with the Construction of Repairs and Closure of
South Wharf Lagoon Plans Dated 11/21/2016. Please see the major lagoon closure activity milestones and
sampling/testing results below.
MAJOR MILESTONE LIST OF LAGOON CLOSURE EVENTS
• 7/2/16 — Dixon Wastewater began chlorination and discharge of liquid waste through the existing
outfall structure. This phase lasted until late September 2016 with weekly monitoring of flow
rates provided by Dixon Wastewater during this period of discharge.
• 9/28/16 — Liquid waste treatment and discharge was stopped and a temporary breach was created
to allow sheet flow of residual rainwater that had collected in the lagoon per approval from the
NCDWQ local representative and MOTSU DPW.
• 11/7/16 — Sludge removal commenced and continued through 11/11/2016. Removal was stopped
due to excess sludge material being encountered beyond the original estimated cubic yardage of
materials requiring removal/disposal offsite.
• 2/22/17 — Intermediate testing of sludge performed by the Government revealed the residual
sludge could remain, be mixed with clay liner material onsite, and would not require removal and
disposal at an offsite location based upon the intermediate test results.
• 8/1/17 — Site contractor installed new temporary breach to allow surface water to drain from
lagoon that had collected during the period from February 2017 through July 2017.
0 8/28/17 — Samples were taken of residual sludge/liner materials for final clearance testing.

DEQ Project ID #: NCO029122
Closure of Permitted Wastewater Ponds and Lagoons
Attn: Tom Tharrington
Page 2
• 9/28/17 — Test Results for residual sludge/liner materials received and forwarded to Government
for review/approval.
• 10/10/17 — Residual sludge / liner material test results were approved for final closure efforts.
• 10/13/17 -- Site contractor remobilized and began rough/final grading of lagoon bottom &
installation of permanent breach of berm.
• 10/20/17 — Final grading of lagoon bottom was completed and disturbed areas hydroseeded.
Lagoon Closure completed.
LAGOON
SLUDGE & CLAY LINER SAMPLING/TESTING
RESULTS
Test
Sample Date
Report Date
Results
Initial Results for top portion of
Initial
8/24/2016
9/13/2013
sludge in lagoon at start of project.
Sludge Materials were found to be
below thresholds and could be tilled
and mixed with liner material with
not offsite removal or special
Intermediate
2/6/2017
2/22/2017
handling required.
Per Government review comments
received on 10/9/17, the residual
sludge/clay liner material were
Final
8/28/2017
9/25/2017
acceptable to continue the closure.
See the enclosure documents for further result information shown in the test reports.
If you have questions about any part of the response or included information, please call us at 704-358
-8240.
Sincerely,
ZapataEngineering of North Carolina, Inc.
By:
Shane Smith, PE, LEED BD+C
Engineering Operations Manager
Enclosure:
1) Coastal Farms and Residuals, LLC Land Application, Permit No. WQ0034806, Dated 11/8/2013
2) Coastal Farms and Residuals, LLC Land Application, Permit No. WQ0034806 Correction, Dated
8/29/2016
3) Environmental Chemists, Inc. — Initial Sampling Test Reports — 09/13/16
4) Environmental Chemists, Inc. — Intermediate Sampling Test Reports — 02/22/17
5) Environmental Chemists, Inc. — Final Sampling Test Reports — 09/20/17
6) Lagoon Closure Progress Photos

ENCLO SURE 1

'A
HCDENR
North Carolina Department of Environment and Natural
Division of Water Resources
Pat McCrory
Governor
Wesley Wooten., President
Coastal Farms and Residuals, LLC.
8l 55 Malpass Corner Road
Currie, North Carolina 28435
Dear Mr. Wooten:
Water Quality Programs
Thomas A. Reeder
Director
November 8, 2013
Resources
John P. Skvaria, III
Secretary
Subject: Permit No. WQ0034806
Coastal Farms and Residuals,
LLC.
Land Application of Class B
Residuals (Non -Dedicated)
Pender County
In accordance with your permit major modification request received September 17, 2013, we are
forwarding herewith Permit No. WQ0034806 dated November 8, 2013, to Coastal Farms and Residuals,
LLC, for the continued operation of the subject residuals management program.
Modi ications to the subject permit are as follows:
The nomenclature has been changed on the existing land application sites.
See Attachment B for new field names.
Adding 23.4 acres land application area (Field AW-4).
Adding six (6) new residuals sources from Wallace Chicken Processing
Plant (I50 dry tons per year), Richlands WWTP (35 dry tons per year),
Swansboro WW'T1' (35 dry tons per yeas), New Topsail School Complex
(5 dry tons per year), Morehead City WWTP (300 dry tons per year), and
North Topsail WWTF (35 dry tons per year).
'T'his permit shall be effective from the date of issuance until December- 31, 2016, shall void
Permit No. WQ0034806 issued rune 25, 2010, Attachment A certification issued February 24, 2011 and
the Attachtfient B carl:i ica,tion issued September 7, 2012 and shall he subject to the conditions and
limitations as specified therein. Please pay particular attention to the monitoring requireirten'ts listed in
Attachments A. for they may differ from the previous permit issuance. Failure to establish an adequate
system for collecting and maintaining the required operational information shall result in future
compliance problems.
WATER QUALITY PERMITTING SECTION
1636 Mail service Center, Raleigh, North Carolina 27699.1636
Location: 512 N. Salisbury St., Raleigh, North Carolina 27604
Phone: 919M7-64641 FAX: 91M07-6496
Intemet; httg:lloorial-ncdenr.orglweblwq
An Equal Opportunity 1 Affirmative Action Employer

If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the
North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and
binding.
If you need additional information concerning this matter, please contact Alice M. Wessner at
[phone] or [e-mail].
Sincerely,
Thomas A. Rceder
cc: Brunswick County Health Department
Carteret County Health Department
Duplin County Health Department
Onslow County Health Department
Pender County Health Department
Wilmington Regional Office, Water Quality Regional Operations Section
Martin Mabe, S&ME, Inc., 3718 Old Battleground Road, Greensboro, North Carolina 27410
Beth Buffington, Public Water Supply Section — Protection and Enforcement Branch
Permit File WQ0034806
Notebook File WQ0034806
2

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
RALEIGH
LAND APPLICATION OF CLASS B RESIDUAL SOLIDS PERMIT (NON -DEDICATED)
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Coastal Farms and Residuals, LLC®
Pender County
FOR TI-IE
continued operation of a residuals management: program for Coastal Farms and Residuals, LLC. and
consisting of the land application of Class B resid3.€als generated by the approved facilities listed in
Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters,
pursuant to the application received September 17, 2013, and in conformity with other supporting data
subsequently filed and approved by the Department of Environment and Natural Resources and
considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of
Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the
federal regulations.
This permit shall be effective from the date of issuance until December 31, 2016, shall void Permit No.
WQ0034806 issued June 25, 2010, Attachment A certification issued February 24, 2011 and the
Attachment B certification issued September 7, 2012 and shall be subject to the following specified
conditions and limitations:
I. SCHEDULES
No later than six months prior to the expiration of this pertnit, the Permittee shall request renewal of
this permit on official Division forrns. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein. and if warranted, will renew the permit for such period of
time and Linder such conditions and lituitai:orrs as ii may deem appropriaie. Please note Rule; 15A
NCAC 027' .0105(d) requires an updated site Wrap to be submitted with the permit renewal
application.
2. The permittee shail be in full compliance with the regional office notification requirements
established in Condition III.3. within 90 days of the effective date of this pertnit.
3.. The permittee shall be in full compliance with the signage requirements established in Condition
I11.13, within 180 days of the effective date of this permit.
WQ0034806 Version 1.3 Shell Version 131016 Page I of 12

H. PERFORMANCE STANDARDS
1. The subject residuals management program shall be effectively maintained and operated at all times
so there is no discharge to; surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance
conditions due to improper operation and maintenance, the Permittee shall immediately cease land
applying residuals to the site, contact the Wilmington regional office supervisor, and take any
immediate corrective actions.
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or
surface water resulting from the operation of this residuals management program.
3. Only residuals generated by the facilities listed in Attachment A are approved for land application in
accordance with this permit.
4. Only the sites listed in Attachment B are approved for residuals land application.
5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not
exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant
Loading Rates (CPLRs):
F- Parameter
Ceiling Concentration
(rnilligrarns per kilogram)
CPLR
(pounds per acre)
� �- _____
I Arsenic
75
_
36
Cadmium
85
_ 34
Copper
4,300
1,338
Lead
840
267
Mercury
57
15
Molybdenum
Nickel
Selenium
Zinc
75
420
100
7,500
_ n/a
374
89
2,498
The Permittee shall deterinine compliance with the CPLRs using one of the following methods:
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. For land where residuals application have not occurred or for which the required data is
incomplete, by determining background concentrations through reprIsentativc soil sampling.
Residuais that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC
02T . i 106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A.
7. Biological residuals (i.e. residuals generated during the treatanerit of domestic or animal processing
wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A)
that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T
.1107(a). Exceptions to this requirement shall be specified in Attachment A.
8. Setbacks for treatment and storage facilities shall be as follows:
Setback Description Setback
feet
Habitable residence or place of public assembly under separate ownership or not 100

to be maintained as part of the project site
Property lines
50
.Private or public water supply
100
Surface waters (streams - intermittent and perennial, perennial waterbodies, and
wetlands)
50
_
Wells with exception to monitoring wells
100
9. Setbacks for land application sites shall be as follows:
Setback by application type
(feet)
Setback Description
Vehicular Irrigation I
Injection /
Surface Surface
Incorporation
Application Application
)"Habitable residence or place of public assembly
under separate ownership or not to be maintained as
400
400
200
art of the project site
Habitable residence or places of public assembly
owned by the Permittee, the owner of the land, or the
0
200
0
lessee/operator of the land to be maintained as part
of the project site
Property lines
50
150
1 50
Public right of way
50
50
50
Private or public water supply
100
100
100
Surface waters (streams — intermittent and perennial,
i00
] 00
50
perennial waterbodies, and wetlands)
Surface water diversions (ephemeral streams,
25
100
25
waterways, ditches
Groundwater lowering ditches (where the bottom of
25
100
25
the ditch intersects the SHWT)
Subsurface groundwater lowering system
0
100
0
Wells with exception to monitoring wells
100
100
100
Bedrock outcrops
25
25
25
Top of slope of embankments or cuts of two feet or
15
1.5
15
more in vertical height
1
WQoo34806 Version 1.3 Shell Version 13 1 016 Page 3 of 12

Setback by
Setback
Setback by
Setback Description
application
Descript
application
type
ion
type
(feet)
(feet)
Building foundations or basements
0
15
0
Water lines
0
10
0
Swimming pools
100
100
100
Nitrification fields
0
20
0
* Unless otherwise noted in Attachment A. "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
10. Land application areas shall be clearly marked on each site prior to and during any residuals
application event.
11. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in
exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected
nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the
following methods:
a- Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. Noah Carolina Historical Data for specific crop and soil types as provided by North Carolina
State University Department of Soil Science (http:.//nutrients.soil.nesu.edu/yields/index.Dhi)).
A copy shall be kept on file and reprinted every five years in accordance with Condition IV,11.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Cousumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(http://www.neagr.gov/SWC/tech/documents/9th�Guidance Doc 100109.1)df).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (atri:81" p-Tc.so. ego v.usda. ov/NFlQ/ practice-standards/5taraclard.s/590.ur.ir. .
d. If the RYE and appropriate nutrient application rates cannot be determined, the Pcrmitfce shall
contact the Division to determine necessary action.
12. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25% in accordance with the USDA-NRCS 590 Nutrient Management Standards.
13. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer
and rye grass in the winter with both crops to receive residuals), then the second crop can receive an
application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may
be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted
for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied.
4

14. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee
shall maintain written records of these recommendations and details of their implementation.
15. The compliance boundary for residual land application sites shall be specified in accordance with
15A NCAC 02L .0107(b). These sites were individually permitted on or after December 30, 1983;
therefore, the compliance boundary is established at either 250 feet from the residual land application
area, or 50 feet within the property boundary, whichever is closest to the residual land application
area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to
remediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in
accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved
relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B.
I6. In accordance with 15A NCAC 02L .0108, the review boundary shall be established midway between
the compliance boundary an(] the residual land application area. Any exceedance of groundwater
standards at the review boundary shall require action in accordance with 15A NCAC 02L .0106.
III. OPERATION AND MAINTENANCE REQUIREMENTS
The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards.
2. The Wilmington Regional Office, telephone number [phone], and the appropriate local
government official (i.e., county manager, city manager, or health director) shall be notified at least
48 hours prior to the initial residuals land application to any new land application site. Notification to
the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday,
excluding State Holidays.
3, The Wilmington Regional Office shall be notified via email or telephone, (91.0) 796-7215, at least 24
hours prior to conducting any land application activity. Such notification shall indicate, at a
minimum, the anticipated application times, Held IDs, and location of land application activities. If it
becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be
notified prior to commencing the application to those fields.
4. The Penmittee shall maintain an approved Operation and Maintenance flan (O&M Plan) pursuant to
ISA NCAC 02T .1110. Modifications to the O&AA Plan shall be approved by the Division prior to
utilization of the new plan. The O&M Plan, of the minimum, shall include:
a) Operational finnctions;
b) Maintenance schedules;
c) Safety measures;
d) Spill response plan;
e) Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
WQ0034806 Version 1.3 Shell Version 131016 Page 5 of 12

iii. Detailed description of inspection procedures including record Keeping and actions to be
taken by the inspector in the event that noncompliance is observed pursuant to the
noncompliance notification requirements under the monitoring and reporting section of the
permit;
f) SampIing and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for
any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that
Iand apply multiple times per year but have an annual sampling frequency, may need to
sample during winter months when pathogen reduction is most likely to be negatively
affected by cold temperatures).
Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in
responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with
15A NCAC 08G .0201. The ORC or their back-up shall visit the facilities in accordance with 15A
NCAC 08G. 0204, or as specified in the most recently approved O&M plan, and shall comply with all
other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources's Technical Assistance &
Certification Unit at [phone].
6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of' O&M Plan shall
be maintained at the land application sites during land application activities.
When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles.
8. Residuals shall not be stored at any land application site, unless written approval has been requested
and received from the Division.
9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals froth the land application sites onto adjacent
properties or intro surface waters.
10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on
land application sites onto which residuals are applied in accordance with the crop management plan
outlined by the local Cooperative Extension Office, the Department of Agriculture and Consu€ner
Services, the Natural Resource Conservation Service, or an agronomist and as approved by the
Division.
11. Bulk residuals shall not be. land applied under the following conditions:
If the residuals are likely to adversely affect a threatened or endangered species listed under
section 4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
If the land fails to assimilate the bulk residuals or the application causes the contravention of
surface water or groundwater standards;
If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the I00-year flood elevation, unless the bulk residuals are injected or incorporated within
a 24-hour period following a residuals land application event;
i

f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the soil pI-I is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the
pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved
variations to the acceptable soil pH (6.0) will be noted in this permit;
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in
a USDA no -till program shall be exempted from meeting this vegetative cover requirement;
j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
1. Application exceeds agronornic rates.
12. The following public access restrictions apply to residual land application sites:
a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted
for 365 days after a residuals land application event;
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event.
13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g.,
1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and
contact information, including the Permittee or applicator's telephone number. Signs shall be posted
in a clearly visible and conspicuoLas manner at the entr-ance to each land application site during a land
application event, and for as long as the public access restrictions required under 111.12 apply.
14. The following harvesting and grazing restrictions apply to residual land application sites after each
land application event:
Harvesting and Grazing Description
Restricted
Duration
Animals shall not be allowed to graze during land application activities and
restricted period. Sites that are to be used for grazing shall have fencing to
30 days
prevent access after each land application event.
k-
Food crops, feed crops and fiber crops shall not be harvested for:
30 days
Turf grown on land where residuals have been applied shall not be harvested for:
12 months
I
Food crops with harvested parts that touch the residual/soil mixture and are
totally above the land surface (e.g.. tobacco, inclons, cucumbers, squasia, etc.)
14 months
shall not be harvested for:
When the residuals remain oil the land surface for four months or longer prior to
incorporation into the soil, food crops with harvested parts below the land
20 months
surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be
harvested for:
When the residuals remain oat the land surface for less than four months prior to
incorporation into the soil, food crops with harvested parts below the land
38 months
surface shall not be harvested for:
WQ0034806 Version 13 Shell Version 131016 Page 7 of 12

15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for
those operations where a NMP is required by the US Department of Agriculture - National Resources
Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable
nutrient loading rates based on the provided information and use appropriate reductions -
For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CLAMP) shall also be considered a Nutrient
Management Plan.
16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (L,OAA)
between the Permittee and landowners or lessees/operators of the land application site is in full force
and effect. These agreements shall be considered expired concurrent with the permit expiration date,
and shall be renewed during the permit renewal process.
IV. MONITORING AND REPORTING RE URUMENTS
1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed.
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). The analyses [corrosivity, ignitabiiity, reactivity, and toxicity
characteristic leaching procedure (TCLP)) shall be performed at the frequency specified in
Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any
exceptions frorn the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
senic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
um (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
zene (0.5)
r
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
mium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
orac-hloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
� Chlorobenzene (100.0}
Heptachlor (and its hydroxide)
Toxaphene (0,5)
-
(0.008)
Chloroform (6.0)
_-...................
Hexachloro-1,3-butadiene (0.5) II
._
_._............................ - 1
Trichloroethylene (0.5)
... _._.. _.....__.._....._.....
Chromium (5.0) J
flex achlorocthanc (3.0) �
2,4,5-Trichlorophenol (400.0)
r r-Cresol (200-0)---
(5.0)^ I
2,-^,,6-Trichlorophenol (2.0)
o-Cresol (200.0)
-Lead
T^^
Lindane (0.4)
2,4,5-TP (Silvex)
p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2)
Cresol (200.0) MethoxychIor (10.0) _
2,4--D (10.0) Methyl ethyl ketone (200.0)

3. An analysis shall be conducted on residuals from each source generating facility at the frequency
specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the followinparameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium.
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
� pH �
Zinc
Lead
Phosphorus
Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the time indicated in the sampling
and monitoring sections of the approved O&M plan. The required data shall be specific to the
stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen
reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction
requirement in 15A NCAC 02`l' .1107 (a) shall be met. Any exceptions from the requirements in this
condition shall be specified in Attachment A.
An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B on which a residuals land application event will
occur in the respective calendar year, This analysis shall be in accordance with the "Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture &
Consumer Services' website (http://www.neagr.gov/agronoini/pubs.htm). The Permittee shall
maintain these results and a description of the sampling methodologies used to determine soil fertility
for a period of no less than five years, and shall be grade available to the Division upon request. At a
minimum, the Standard Soil Fertility Analysis shall include the following parameters:
Acidity
_ Exchangeable Sodium Percentage.
_
Phosphorus
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Copper
Percent Hurnic Matter
pH
'Zinc
6. Laboratory parameter analyses shall be perfortned on the residuals as they are land applied and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505.
WQ0034806 'Version 1.3 Shell 'Version 131016 Page 9 of 12

7. The Permittee shall maintain records tracking all residual land application events. At a minimum,
these records shall include the following:
a. Source of residuals,
b. Date of land application;
c. Location of land application (i.e., site, field, or zone number as listed in Attachment B);
d. Approximate areas applied to (acres);
e. Method of land application;
f. Weather conditions (e.g., sunny, cloudy, raining, etc.);
g. Predominant Soil Mapping Unit (e.g., CbB2);
h. Soil conditions (e.g., dry, wet, frozen, etc.);
i. Type of crop or crops to be grown on field;
j. Nitrogen Application Rate based on RYBs (if using data obtained from the North Carolina State
University Department of Soil Science Website, the printout page shall be kept on file and
reprinted every five years);
k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet
ton per acre;
1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or
wet tons per acre;
in. Volume of soil amendments (e,g., lime, gypsum, etc.) applied in gallons per acre, dry ton per
:r{:rc, or wet tons por acre; and
n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other
sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy
metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury,
molybdenum; nickel, selenium, and zinc:), annual pounds per acre of PAN, and annual pounds per
acre of phosphorus applied to each field.
S. Three copies of an annual report shall be submitted on or before March I". The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting
Dorms, Instructions for reporting and annual report forms are available at
http:.///i)ortal,ne,denr.org/web/wq/aps/lau/reporting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
9. Nf ovcompliance Notification
The Permittee shall report by telephone to the Wilmington Regional Office, telephone number (910)
796-7215, as soon as possible, but in no case more than 24 hours or on the next working day
following the occurrence or first knowledge of the occurrence of any of the followi.rtg:
a. Any occurrence with the land application prograrn resulting in the land application of significant
amounts of wastes that are abnormal in quantity or characteristic.
b. Any failure of the land application program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
10

d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring itnznediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
be taken to ensure that the problem does not recur.
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan.
2. Prior to each bull: residuals land application event, the Permittee or his designee shall inspect the
residuals storage, transport and application facilities to prevent malfunctions, facility deterioration
and operator errors resulting in discharges, which may cause the release of wastes to the
environment, a threat to human health or a public nuisance. The Permittee shall maintain an
inspection log that includes, at a minimum, the date and time of inspection, observations made, and
any maintenance, repairs; or corrective actions taken. The Permittee shall maintain this inspection log
for a period of five years from the date of inspection, and this log shall be made available to the
Division upon request.
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or
copy any records required to be maintained under the terms and conditions of this permit; and may
collect groundwater, surface water or leachate samples.
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to
an enforcement action by the Division in accordance with North Carolina General Statutes 143--
215.6A to 143-215.6C.
This permit shall become voidable if the residuals land application events are not carried out in
accordance v:ith th-- conditions of this permit.
This pert -pit is effective only with respect: to the nature and volume of residuals desGi-flocd in the
permit application and other supporting documentation.
The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules
in 15A NCAC 02B -0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4
and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under
15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of
Chapter 143 of the General Statutes.
W00034806 Version 1.3 Shell Version 131016 Page 1 i of 12

In the event the residuals program changes ownership or the Permittee changes their name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner.
6. This permit is subject to revocation or unilateral modification upon 60 days notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110.
Unless the Division Director grants a variance, expansion of the permitted residuals program
contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC
02T .0120(b).
The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to
pay the annual fee accordingly shall be cause for the Division to revolve this permit pursuant to 15A
NCAC 02T .0105(e)(3).
Permit issued this the 8th day of November- 2013
NORTH CAROLINA ENVJRONMENTAL MANAGEMENT COMMISSION
. A. Reeder, Director-.�—�--------�
iviszan of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0034806
12

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NC®ENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Mr. Wesley Wooten — President
Coastal Farms and Residuals, LLC
8155 Malpass Corner Road
Currie, NC 28435
Dear Mr. Mr. Wooten:
Donald R. Van der Vaart
Secretary
April 24, 2015
Subject: Attachment A Certification
Permit No. WQ0034806
Coastal Farms and Residuals Land Application Program
Pender County
In accordance with your permit modification request received April 6, 2015, we are forwarding
herewith modified Attachment A, certified July 30, 2014, to Coastal harms and Residuals, LLC for the
subject residuals program.
This certification is being issued to modify Attachment A by addition of up to 120 dry tons per
year (DT/yr) from Avondale WWTP (20 DT/yr) in Ponder County and Oak Island WWTP (100 DT/yr) in
Brunswick County.
This modified Attachment A shall be effective from the date of certification until December 31,
2016 (i.e. expiration date of the current permit); shall void Attachment A of Permit No. WQ0034806 that
was previously certified on July 30, 2014, and shall be subject to the conditions and limitations as
specified therein and well as those specified in the above -referenced permit. Please replace the
Attachment A of Permit No. WQ0034806 issued on June 25, 2010 with this modified Attachment A.
Please note that only the maps for any new residuals -generating sources and/or land application
sites are attached to this letter, It is the Permittee's responsibility to ensure that a complete permit is
created by inserting these documents into the previously issued permit.
If any parts, requirements, and/or limitations contained in this certification or modified
Attachment A are unacceptable, you have the right to request an adjudicatory hearing upon written
request within 30 days following receipt of the certification. This request shall be in the form of a written
petition, conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of
Administrative Hearings at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such
demands are made, this permit shall be final and binding,
If you need any additional information concerning this matter, please contact Troy Doby at (919)
807-6336 or [e-mail].
Non -Discharge Permitting Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Phone: [phone]Internet htl01portal,nodenr.orghvebhvg
An Equal Opportunity 1 Alfirmaiive Action Employer- Made In parlwith recycled paper

Mr. Wesley Wooten
Apri124, 2015
Page 2 of 2
Sincerely,
S. ]a Zimmerman, Director
Division of Water Resources
cc: Pender County Health Department [[e-mail]] (Electronic Copy)
Brunswick County Health Department [[e-mail]] (Electronic Copy)
Onslow County Health Department [waiter—[e-mail]] (Electronic Copy)
Duplin County Health Department f [e-mail]](Electronic Copy)
New Hanover County Health Department[[e-mail]](Electronic Copy)
Carteret County Health Department[[e-mail]](Electronic Copy)
Wilmington Regional Office, Watcr Quality Regional Operations Section (Electronic Copy)
Martin Mabe — S&ME [[e-mail]] (Electronic Copy)
Rob Wilcox— S&ME [[e-mail]) (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Centrals Files
Digital Pen -nit Archive (EIectronic Copy)

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ENCLO SURE 2

Water Resources
ENVIRONMENTAL QUALITY
PAT MCCRORY
Governor
DONALD R. VAN DER VAART
Secretary
S. JAY ZIMMERMAN
Director
August 29, 2016
WESLEY WOOTEN—PRESIDENT
COASTAL FARMS AND RESIDUALS, LLC
8155 MALPASS CORNER ROAD
CuRR1E, NORTH CAROLINA 28435
I01M- 55 111 • •
Subject: Permit No. WQ0034806
Correction
Coastal Farms and Residuals
Land Application Program
Residuals Management System
Pender County
In accordance with a written request received August 4, 2016, from you, we are forwarding
herewith corrected Attachment A of Permit No. WQ0034806 issued April 24, 2015.
The correction to the subject permit is as follows:
1. 100 tons per year of residuals from MOTSU was omitted from Attachment A and has been
corrected.
Please replace Attachment A of Permit No. WQ0034806 issued April 24, 2015, with the
enclosed corrected Attachment A.
If you need additional information concerning this permit correction, please contact Troy Doby at
[phone] or troy.dobygncdenr.gov.
Sincerely,
S. Jay Zimmerman, P.G., Director
Division of Water Resources
Enclosure
cc: Pender County Health Department [cmoser@pendercountync,gov] (Electronic Copy)
Brunswick County Health Department [[e-mail]] (Electronic Copy)
Onslow County Health Department[[e-mail]] (Electronic Copy)
Duplin County Health [e-mail]](Electronic Copy)
New Hanover County Health Department[[e-mail]](Electronic Copy)
Carteret County Health Department[[e-mail]](Eleetronic Copy)
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail service Center I Raleigh, North Carolina 27699-1617
919 807 6464

Mr. Wesley Wooten
August 29, 2016
Page 2 of 2
Wilmington Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Martin Mabe — S&ME [[e-mail]] (Electronic Copy)
Rob Wilcox — S&ME [[e-mail]] (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

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ENCLO SURE 3

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 13, 2016
Customer PO #:
Customer ID: 14020008
Report #: 2016-12028
Project ID: MOTSU - Lagoon
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-29202 Site: Residuals 8/24/2016 9:30 AM Solid/Sludge Envirochem
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
9140 mg/kg
08/31/2016
Arsenic
EPA 2007
<7.24 mg/kg
08/30/2016
Cadmium
EPA 200.7
<7.24 mg/kg
08/30/2016
Calcium
EPA 200.7
2240 mg/kg
08/31/2016
Chromium
EPA 200.7
12.5mg/kg
08/30/2016
Copper
EPA 200.7
12.0 mglkg
08/30/2016
Lead
EPA200.7
9.36 mg/kg
08/30/2016
Magnesium
EPA 200.7
1040 mg/kg
08/31/2016
Molybdenum
EPA 200.7
<7.24 mg/kg
08/30/2016
Nickel
EPA 200.7
<7.24 mg/kg
08/30/2016
Potassium
EPA 200.7
658 mg/kg
08/31/2016
Selenium
EPA 200.7
<7.24 mg/kg
08/30/2016
Sodium
EPA 200.7
534 mg/kg
08/31/2016
Zinc
EPA 200.7
178 mg/kg
08/30/2016
Nitrate}Nitrite-Nitrogen
EPA353.2
<0.07 mg/kg
09/02/2016
Total Solids (%)
SM 2540 B
27.4 %
08/25/2016
pH
SM 4500 H B
7.23 units
08/30/2016
Ammonia Nitrogen
SM4500NH3 c
402mg/kg
08/29/2016
Total Kjeldahl Nitrogen (TKN)
SM 4500 org B
9550 mg/kg
08/30/2016
Total Phosphorus
SM 4500 P F
1.66 mg/kg
09/02/2016
Mercury
SW8467471B
0.0590 mg/kg
09/06/2016
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2016-12028 Page 1 of 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: a(c.r: s ��+►� �.' �..`�l
PROJECT NAME: /-f� Tay
REPORT NO: l(- r
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIi=AX:
COPY TO:
email:
Sampled Bv: V .0k ✓l ro SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
+
Sample Identification
Collection
q r
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PRESERVATION
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ate
Time
Temp
=
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Relinquished By:
Date/Time
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1.
2.
Temperature when Received: Accepted: jetted: Resample Requested:
Delivered By: 11!!�" ,��--� Received By: Date: g�a' Time:
Comments: 01 U TURNAROUND:

Environmental Chemists, Inc.
envirochem
ANALYTICAL R CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info@elivironmentalc;hemists.com
Date of Report:
Customer PO #:
Customer ID:
Nov 16, 2016
14020008
Attention: Wesley Wooten Report #: 2016-15966
Project ID: MOTSU-South Lagoon
Lab ID Sample ID: Collect Dateliime Matrix Sampled by
16-38509 Site:1
11/7/2016 10:00 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2-540 G
24.7 % 11108/2Q16
Fecal Density SM 02210 E MPN 24 hr 503 162 MPNIg 11 /0812016
Lab ID Sample ID: Collect Date/Timq Matrix Sampled by
16-38510 Site, 2
11/7/2016 10:02 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2640 G
30.5 % 11/08/2016
Fecal Density SM 9221C E MPN 24 hr 503 361 MPN/g 11/08/2016
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-38511 Site:3
11/7/2016 10:04 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
28.1 % 11/08/2016
Fecal Density SM 9221C E MPN 24 hr 503 250 MPN/g 11/08/2016
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-38512 Site.,4
Test Method
Total Solids (%) SM 2540 G
11/7/2016 10:06 AM Solid/Sludge Client
Results
35.9 %
Date Analyzed
11/08/2016
Fecal Density SM 9221C E MPN 24 hr 503 112 MPN/g 11/08/2016
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
16-38513 Site, 5
11/7/2016 10:08 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
325 % 11/08/2016
Fecal Density SM 9221C E MP4 24 hr 503 124 MPNIg 11/08/2016
Report #:: 2016-15966 Page 1 of 2

Environmental Chemists, Inc.
Cvirochem
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention: Wesley Wooten
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 16, 2016
Customer PO #:
Customer ID: 14020008
Report #: 2016-15966
Project ID: MOTSU-South Lagoon
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-38514 Site:6
11 /7/2016 10:10 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
28.8 % 11 /08/2016
Faecal Density SM 9221C E MPN 24 hr 503 278 MPN/g 11/08/2016
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-38515 Site:7
11/7/2016 10:12 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
26.3 % 11 /08/2016
Fecal Density SM 9221C E MPN 24 hr 503 <76 MPN/g 11/08/2016
Comment: Results reported on a dry weight basis.
Reviewed by:
Report #:: 2016-15966 Page 2 of 2

6602
Windml Way
NC
ENVIRONMENTAL CHEMISTS, INC OFFI E:910I392- 223'IFAX99'103922-44245
Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: &J.l S
PROJECT NAME: /V 3TSLI -
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: 61Je�,%vy
PHONEIFAX:
COPY TO:
email:
Samnled Bv: c- A 2--"f SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
C
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E
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PRESERVATION
ANALYSIS REQUESTED
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0
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p
w
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Relinquished By:
DatelTime
Re ived By:
Date/Time
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Temperature when
Delivered Ely:
Comments:
Accepted: R jected: Resample Keq st
Received By. _Date: �G Time:
TII A OUND:

ENCLO SURE 4

Environmental Chemists, Inc.
6602 Windmffl Way, V,'Hmingt�)n, NC 284o-5 , 910.392,0223 Lab o 910,392 -4424 Fax
710 zwsertown Road, Manteo, NIC 27954 0 2,52.473.5702 Lab//Fax
255-A Wilmin&on Highway, Jacksonville, NC 28540 e 910.3347.5843 Lab 'Fax
ANALYTICAL & CONS ULTiNG CHEMISTS nil6, -env:ronmentalchemists.com
(I/
Military Ocean Terminal Public Works Date of Report: Feb 22, 2017
6280 Sunny Point Road Customer PO #:
Southport NC 28461-5000 Customer ID: 08100090
Attention: David Von Kolnitz Report #: 2017-01685
.. .. .............
Lab ID Sample ID: MOTSU Collect Date/Time Matrix Sampled by
17-03961 Site: 1
Test Method
Total Solids (%) SM 2540 G
2/6/2017 12:40 PM Solid/Sludge
Results
48.2%
Envirochern
Date Analyzed
02/08/2017
Fecal Density SM 9221 C E MPN 24 hr 503 5 MPN/g 02/07/2017
Lab ID Sample ID: MOTSU Collect Date/Time Matrix Sampled by
17-03962 Site: 2
2/6/2017 12:45 PM Solid/Sludge Envirochern
Test Method Results Date Analyzed
Total Solids N
SM 2540 G
53.0% 02/08/2017
Fecal Density
SM 9221 C E MPN 24 hr 503
4 MPN/g 02/07/2017
Lab ID Sample ID: MOTSU
Collect Date/Time
Matrix Sampled by
17-03963 Site: 3
2/6/2017 12:50 PM
Solid/Sludge Envirochern
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
53.8% 02/08/2017
Fecal Density
SM 9221 C E MPN 24 hr 503
4 MPN/g 02/07/2017
Lab ID Sample ID: MOTSU
Collect Date/Time
Matrix Sampled by
17-03964 Site: 4
2/6/2017 12:55 PM
Solid/Sludge Envirochern
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
66.0% 02/08/2017
Fecal Density
SM 9221 C E MPN 24 hr 503
<4MPN/g 02/07/2017
Lab ID Sample ID: MOTSU
Collect Date/Time
Matrix Sampled by
17-03965 Site: 5
2/6/2017 1:00 PM
Solid/Sludge Envirochern
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 G
66.5% 02/08/2017
Fecal Density
SM 9221 C E MPN 24 hr 503
7 MPN/g 02/07/2017
Report #:: 2017-01685 Page 1 of 3

y
f , Environmental Chemists, Inc.
6602 Windmill -v YVij ingto , NC 28405 � 910,392.10223 Lab * 91.0. 92,4424 Fax
710 Bo,,�rse tc��. r� Road, lame ;, NC 2 95252. r j. i 2 Lab jFax
2.,-t its i etc; lil;,acst�ncilla,C su 910.347.5843 Lab/Faxzl
4
ANALYTICAL C iS l $it CHEMISTS
<i:i13;�t;en�,iranm�ertalcbe-iiists.com
Military Ocean Terminal Public Works Date of Report: Feb 22, 2017
6280 Sunny Point Road Customer PO #:
Southport NC 28461-5000 Customer ID: 08100090
Attention: David Von Kolnitz Report #: 2017-01685
Project ID.:
Lab ID Sample ID: MOTSU Collect Date/Time Matrix Sampled by
17-03966 Site: 6 2/6/2017 1:05 PM Solid/Sludge Envirochem
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
21.9 % 02/08/2017
Fecal Density SM 9221C E MPN 24 hr 503 10 MPN/g 02/07/2017
Lab ID Sample ID: MOTSU Collect Date/Time Matrix Sampled by
17-03967 Site: 7 2/6/2017 1:10 PM Solid/Sludge Envirochem
Test
Total Solids (%)
Fecal Density
Method
SM 2540 G
SM 9221 C E MPN 24 hr 503
Results Date Analyzed
30.5 %
7 MPN/g
02/08/2017
02/07/2017
Report #:: 2017-01685 Page 2 of 3

x
�e
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmi'V iAla i kin-ington, Ni. 28405 a 910392,0223 Lab , 910,392.4424 Fax
'10 Bowsertovv n Road, Nianteo, NC 27954 * 252A7?.57021
j1rtax
2 55-A Wlrni lat m Flighway, Jacksonville, NC 28-)40 e 910.31,5843 Lib/Fax
iii.lo tt" c=ivir,)nine xit�tlyhemists.com
Military Ocean Terminal Public Works
Date of Report: Feb 22, 2017
6280 Sunny Point Road
Customer PO #:
Southport NC 28461-5000
Customer ID: 08100090
Attention: David Von Kolnitz
Report #: 2017-01685
Lab ID Sample ID: MOTSU
Collect Date/Time Matrix Sampled by
17-03968 Site: composite
2/6/2017
1:10 PM Solid/Sludge Envirochem
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
13300 mg/kg
02/20/2017
Arsenic
EPA 2001
5.10 mg/kg
02/16/2017
Cadmium
EPA 200.7
3.21 mg/kg
02/16/2017
Calcium
EPA 200.7
744 mg/kg
02/15/2017
Chromium
EPA 200.7
19.2 mg/kg
02/16/2017
Copper
EPA 200.7
6.85 mg/kg
02/16/2017
Lead
EPA 200.7
7.35 mg/kg
02/16/2017
Magnesium
EPA 2007
1100 mg/kg
02/15/2017
Molybdenum
EPA 200.7
<3.21 mg/kg
02/16/2017
Nickel
EPA 200.7
<3.21 mg/kg
02/16/2017
Potassium
EPA 200.7
657 mg/kg
02/15/2017
Selenium
EPA 200.7
<3.21 mg/kg
02/16/2017
Sodium
EPA 200.7
531 mg/kg
02/15/2017
Zinc
EPA 200.7
19.8 mg/kg
02/16/2017
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/kg
02/22/2017
Total Solids (%)
SM 2540 B
61.6 %
02/08/2017
Ammonia Nitrogen
SM 4500 NH3 C
76.10 mg/kg
02/14/2017
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
1390 mg/kg
02/14/2017
Total Phosphorus
SM 4500 P F
188 mg/kg
02/10/2017
pH
SW 846 Method 9045D
6.33 units
02/21/2017
Mercury
SW846 7471E
<0.036 mg/kg
02/10/2017
Comment: Sludge residuals reported
on a dry weight basis.
Reviewed by:
Report #:: 2017-01685 Page 3 of 3

9
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ENCLO SURE 5

TRANSMITTAL OF SHOP DRAWINGS, EQUIPMENT DATA, MATERIAL SAMPLES, OR
MANUFACTURER'S CERTIFICATES OF COMPLIANCE
For use of this form, see ER415-1-10; the proponent agency is CECW-CE
DATE
09/25/2017
TRANSMITTAL NO.
31 00 00-1
SECTION I - REQUEST FOR APPROVAL OF THE FOLLOWING ITEMS (This section will be initiated by the contractor)
TO: Coastal Resident Office
69 Darlington Avenue
Wilmington, NC 28403
FROM: Trend Construction, Inc.
1826 N. Alafaya Trail #100
Orlando, FL 32826
CONTRACT NO.
W912PM 15-D 0005 0008
CHECK ONE
❑X THIS IS A NEW TRANSMITTAL
❑ THIS IS A RESUBMfTTAL OF
TRANSMITTAL
SPECIFICATION SEC. NO. (Cover only one section with each transmittal)
31 00 00 EARTHWORK
PROJECT TITLE AND LOCATION 01-Main Register
SouthWharfLagoon ClosureMOTSU
THIS TRANSMITTAL IS FOR: (Check one)
❑ F10 ❑X GA ❑ DA ❑CR ❑ DA/CR ❑ DA/GA
ITEM
NO.
(See
Note 3)
a.
DESCRIPTION OF SUBMITTAL ITEM
(Type size, model number/etc.)
b.
SUBMITTAL
TYPE CODE
(See Note 8)
C.
NO.
OF
COPIES
d.
CONTRACT REFERENCE
DOCUMENT
CONTRACTOR
REVIEW
CODE
g.
VARIATION
Enter "Y" if
requesting
a variation
(See Note 6)
h.
USACE
ACTION
CODE
(Note 9)
I.
SPEC.
PARA NO.
e.
DRAWING
SHEET NO.
f.
1
Clay Liner Test Samples
SD-06
5
A
REMARKS
Attached are the test results for the clay liner material as requested by MOTSU. Please review and confirm that Trend can begin
scarifying and final grading of the lagoon bottom material accordingly.
I certify that the above submitted items have been reviewed
in detail and are correct and in the strict conformance with the
contract drawings and specifications except as otherwise
stated.
_3)
NAME AND SIGNATURE OF CONTRACTOR
SECTION
II - APPROVAL ACTION
ENCLOSURES RETURNED (List by item No.)
NAME, TILE AND SIGNATURE OF APPROVING AUTHORITY
DATE
ENG FORM 4025-R, MAR2012 REPLACES EDITION OF MAR 95, WHICH IS OBSOLETE. Page 1 Of 1

ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 � 910.3910223 Lab a 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 s 910,347.5843 Lab/Fax
inCor, environmentalch mists.con-i
Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
17-30876 Site: 1
8/28/2017
10:30 AM Solid/Sludge Eric McHorney
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.02 mg/L
09/08/2017
Endrin
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor
SW 846 Method 8081 B/3510
<0.0005 mg/L
09/08/2017
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Methoxychlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Toxaphene
SW 846 Method 8081B/3510
<0.05 mg/L
09/08/2017
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
09/06/2017
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
pH
SW 846 Method 9045D
4.46 units
09/07/2017
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
09/12/2017
2,4-D
SW846 Method 8151A
<0.003 mg/L
09/12/2017
1,1-Dichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Benzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Report #:: 2017-12878
Page 1 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Methyl ethyl ketone
SW846 Method 8260/5030
<0.05 mg/L
09/12/2017
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
RCI
Ignitability
EPA 1030
<0.8 mm/sec
09/06/2017
Cyanide
EPA 335.4
<0.1217 mg/kg
09/07/2017
Sulfide
SM 4500 S D
<0.2434 mg/kg
09/11/2017
Sludge Residuals
Aluminum
EPA 200.7
19900mg/kg
09/12/2017
Arsenic
EPA 200.7
4.31 mg/kg
09/05/2017
Cadmium
EPA 200.7
<1.40 mg/kg
09/05/2017
Calcium
EPA 200.7
343mg/kg
09/11/2017
Chromium
EPA 200.7
23.3 mg/kg
09/05/2017
Copper
EPA 200.7
3.63 mg/kg
09/05/2017
Lead
EPA 200.7
5.63 mg/kg
09/05/2017
Magnesium
EPA200.7
1150mg/kg
09/11/2017
Molybdenum
EPA 200.7
<1.40 mg/kg
09/05/2017
Nickel
EPA 200.7
3.28mg/kg
09/05/2017
Potassium
EPA 200.7
771 mg/kg
09/11/2017
Selenium
EPA 200.7
<1.40mg/kg
09/05/2017
Sodium
EPA 200.7
290 mg/kg
09/11/2017
Zinc
EPA 200.7
14.1 mg/kg
09/05/2017
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
712 mg/kg
09/05/2017
Nitrate+Nitrite-Nitrogen
EPA353.2
<0.29mg/kg
09/15/2017
Reporting limit a evated due to matrix
interference.
Total Solids (%)
SM 2540 B
69.4 %
08/28/2017
Report #:: 2017-12878
Page 2 of 15

Civil Works Contracting Date of Report: Sep 20, 2017
1404 Chadwick Drive Customer PO #:
Sneads Ferry NC 28460 Customer ID: 16090025
Attention: Report #: 2017-12878
Project ID:
Ammonia Nitrogen SM 4500 NH3 C 17.85 mg/kg 09/15/2017
Total Phosphorus SM 4500 P F 129 mg/kg 09/05/2017
Mercury SW846 7471E 0.0610 mg/kg 08/29/2017
TCLP Metals
Arsenic
EPA200.7
<1.0mg/L
09/11/2017
Barium
EPA200.7
<1.0mg/L
09/11/2017
Cadmium
EPA200.7
<1.0mg/L
09/11/2017
Chromium
EPA200.7
<1.0mg/L
09/11/2017
Lead
EPA200.7
<1.0mg/L
09/11/2017
Selenium
EPA200.7
<1.0mg/L
09/11/2017
Silver
EPA 200.7
<1.0 mg/L
09/11/2017
Mercury
EPA 245.1
<0.0020 mg/L
09/08/2017
Report #:: 2017-12878 Page 3 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Lab lD Sample ID:
Collect Date/Time Matrix Sampled by
17-30877 Site: 2
8/28/2017
10:35 AM Solid/Sludge Eric McHorney
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.02 mg/L
09/08/2017
Endrin
SW 846 Method 8081 B/3510
<0.0005 mg/L
09/08/2017
Heptachlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Methoxychlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Toxaphene
SW 846 Method 8081 B/3510
<0.05 mg/L
09/08/2017
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
09/06/2017
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
09/12/2017
2 4-D
SW846 Method 8151A
<0.003 mg/L
09/12/2017
1,1-Dichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Benzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Report #:: 2017-12878
Page 4 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Methyl ethyl ketone
SW846 Method 8260/5030
<0.05 mg/L
09/12/2017
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
RCI
Ignitability
EPA 1030
<0.8 mm/sec
09/06/2017
Cyanide
EPA 335.4
<0.1211 mg/kg
09/07/2017
Sulfide
SM 4500 S D
<0.2422 mg/kg
09/11/2017
pH
SW 846 Method 9045D
4.32 units
09/07/2017
Sludge Residuals
Aluminum
EPA 200.7
18800 mg/kg
09/12/2017
Arsenic
EPA 2001
3.78 mg/kg
09/05/2017
Cadmium
EPA 200.7
<1.53 mg/kg
09/05/2017
Calcium
EPA 200.7
278mg/kg
09/11/2017
Chromium
EPA 2007
20.9 mg/kg
09/05/2017
Copper
EPA 200.7
3.00 mg/kg
09/05/2017
Lead
EPA 200.7
5.31 mg/kg
09/05/2017
Magnesium
EPA 200.7
940 mg/kg
09/11/2017
Molybdenum
EPA 200.7
<1.53 mg/kg
09/05/2017
Nickel
EPA 200.7
3.36 mg/kg
09/05/2017
Potassium
EPA 200.7
659mg/kg
09/11/2017
Selenium
EPA 200.7
<1.53 mg/kg
09/05/2017
Sodium
EPA2001
242mg/kg
09/11/2017
Zinc
EPA 200.7
13.2 mg/kg
09/05/2017
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
292 mg/kg
09/05/2017
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.67 mg/kg
09/15/2017
Total Solids (%)
SM 2540 B
64.0 %
08/28/2017
Ammonia Nitrogen
SM 4500 NH3 C
18.61 mg/kg
09/15/2017
Report #:: 2017-12878
Page 5 of 15

Civil Works Contracting Date of Report: Sep 20, 2017
1404 Chadwick Drive Customer PO #:
Sneads Ferry NC 28460 Customer ID: 16090025
Attention: Report #: 2017-12878
Project ID:
Total Phosphorus SM 4500 P F 89.4 mg/kg 09/05/2017
Mercury SW8467471B 0.0590mg/kg 08/29/2017
TCLP Metals
Arsenic
EPA 200.7
<1.0mg/L
09/11/2017
Barium
EPA 200.7
<1.0mg/L
09/11/2017
Cadmium
EPA 200.7
<1.0 mg/L
09/11/2017
Chromium
EPA200.7
<1.0mg/L
09/11/2017
Lead
EPA 200.7
<1.0 mg/L
09/11/2017
Selenium
EPA 200.7
<1.0 mg/L
09/11/2017
Silver
EPA 200.7
<1.0 mg/L
09/11/2017
Mercury
EPA 245.1
<0.0020 mg/L
09/08/2017
Report #:: 2017-12878 Page 6 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Lab lD Sample ID:
Collect Date/Time Matrix Sampled by
17-30878 Site: 3
8/28/2017
10:40 AM Solid/Sludge Eric McHorney
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.02 mg/L
09/08/2017
Endrin
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor
SW 846 Method 80818/3510
<0.0005 mg/L
09/08/2017
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Methoxychlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Toxaphene
SW 846 Method 8081B/3510
<0.05 mg/L
09/08/2017
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3610
<0.050 mg/L
09/06/2017
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
09/06/2017
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
09/12/2017
2,4-D
SW846 Method 8151A
<0.003 mg/L
09/12/2017
1, 1 -Dichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Benzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Report #:: 2017-12878
Page 7 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Methyl ethyl ketone
SW846 Method 8260/5030
<0.05 mg/L
09/12/2017
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
09/12/2017
301
Ignitability
EPA 1030
<0.8 mm/sec
09/06/2017
Cyanide
EPA 335.4
<0.1144 mg/kg
09/07/2017
Sulfide
SM 4500 S D
<0.2289 mg/kg
09/11/2017
pH
SW 846 Method 9045D
4.32 units
09/07/2017
Sludge Residuals
Aluminum
EPA 200.7
18500 mg/kg
09/12/2017
Arsenic
EPA 200.7
3.44 mg/kg
09/05/2017
Cadmium
EPA 200.7
<1.30 mg/kg
09/05/2017
Calcium
EPA 200.7
411 mg/kg
09/11/2017
Chromium
EPA 2007
21.3 mg/kg
09/05/2017
Copper
EPA 200.7
2.53 mg/kg
09/05/2017
Lead
EPA 200.7
5.55 mg/kg
09/05/2017
Magnesium
EPA 200.7
1180mg/kg
09/11/2017
Molybdenum
EPA 200.7
<1.30 mg/kg
09/05/2017
Nickel
EPA 200.7
2.94mg/kg
09/05/2017
Potassium
EPA 200.7
740 mg/kg
09/11/2017
Selenium
EPA200.7
<1.30mg/kg
09/05/2017
Sodium
EPA 200.7
269mg/kg
09/11/2017
Zinc
EPA 200.7
12.5 mg/kg
09/05/2017
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
224 mg/kg
09/05/2017
Nitrate+Nitrite-Nitroggen
EPA 353.2
<0.36 mg/kg
09/15/2017
Reporting limit a evated due to matrix interference.
Total Solids (%)
SM 2540 B
74.2 %
08/28/2017
Report #:: 2017-12878 Page 8 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Ammonia Nitrogen SM 4500 NH3 C
48.18 mg/kg 09/15/2017
Total Phosphorus SM 4500 P F
70.2 mg/kg 09/05/2017
Mercury SW8467471B
<0.026mg/kg 08/29/2017
TCLP Metals
Arsenic
EPA 200.7
<1.0mg/L
09/11/2017
Barium
EPA 200.7
<1.0mg/L
09/11/2017
Cadmium
EPA 200.7
<1.0mg/L
09/11/2017
Chromium
EPA 200.7
<1.0 mg/L
09/11/2017
Lead
EPA 200.7
<1.0mg/L
09/11/2017
Selenium
EPA 200.7
<1.0 mg/L
09/11/2017
Silver
EPA200.7
<1.0mg/L
09/11/2017
Mercury
EPA 245.1
<0.0020 mg/L
09/08/2017
Report #:: 2017-12878 Page 9 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
17-30879 Site: 4
8/28/2017
10:45 AM Solid/Sludge Eric McHorney
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.02 mg/L
09/08/2017
Endrin
SW 846 Method 8081 B/3510
<0.0005 mg/L
09/08/2017
Heptachlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor epoxide
SW 846 Method 8081 B/3510
<0.0005 mg/L
09/08/2017
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Methoxychlor
SW 846 Method 8081 B/3510
<0.0005 mg/L
09/08/2017
Toxaphene
SW 846 Method 8081 B/3510
<0.05 mg/L
09/08/2017
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
09/06/2017
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
09/12/2017
2,4-D
SW846 Method 8151A
<0.003 mg/L
09/12/2017
1, 1 -Dich loroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Benzene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Report #:: 2017-12878
Page 10 of 15

ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way Wilmington, NC 28405 o 910.392.0223 Lab a 910.392.4424 Fax
710 Bov4sertown Road, Nlanteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
info(rx;eiivironmentalchemists.com
Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Methyl ethyl ketone
SW846 Method 8260/5030
0.07 mg/L
09/14/2017
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
RCI
Ignitability
Cyanide
Sulfide
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
EPA 1030
EPA 335.4
SM 4500 S D
SW 846 Method 9045D
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 2007
EPA 200.7
EPA 200.7
EPA 200.7
EPA 2007
EPA 200.7
EPA 200.7
Zinc EPA 200.7
Total Kjeldahl Nitrogen (TKN) EPA 351.2
Nitrate+Nitrite-Nitrogen EPA 353.2
Reporting limit a evated due to matrix interference.
<0.8 mm/sec
<0.1099 mg/kg
<0.2199 mg/kg
5.58 units
18300 mg/kg
3.92 mg/kg
<1.65 mg/kg
731 mg/kg
31.2 mg/kg
2.60 mg/kg
5.87 mg/kg
1080 mg/kg
<1.65 mg/kg
3.92 mg/kg
722 mg/kg
<1.65 mg/kg
205 mg/kg
13.2 mg/kg
482 mg/kg
<0.39 mg/kg
09/06/2017
09/07/2017
09/11/2017
09/07/2017
09/07/2017
09/07/2017
09/07/2017
09/11/2017
09/05/2017
09/07/2017
09/07/2017
09/11/2017
09/07/2017
09/07/2017
09/11/2017
09/07/2017
09/11/2017
09/07/2017
09/05/2017
09/15/2017
Total Solids (%)
SM 2540 B
89.7 %
08/28/2017
Report #:: 2017-12878 Page 11 of 15

Civil Works Contracting Date of Report: Sep 20, 2017
1404 Chadwick Drive Customer PO #:
Sneads Ferry NC 28460 Customer ID: 16090025
Attention: Report #: 2017-12878
Project ID:
Ammonia Nitrogen SM 4500 NH3 C 27.08 mg/kg 09/15/2017
Total Phosphorus SM 4500 P F 98.2 mg/kg 09/05/2017
Mercury Sw846 74718 <0.022 mg/kg 08/29/2017
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
09/11/2017
Barium
EPA200.7
<1.0mg/L
09/11/2017
Cadmium
EPA 200.7
<1.0 mg/L
09/11/2017
Chromium
EPA 200.7
<1.0mg/L
09/11/2017
Lead
EPA 200.7
<1.0mg/L
09/11/2017
Selenium
EPA 200.7
<1.0mg/L
09/11/2017
Silver
EPA 200.7
<1.0mg/L
09/11/2017
Mercury
EPA 245.1
<0.0020 mg/L
09/08/2017
Report #:: 2017-12878 Page 12 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
17-30880 Site: 5
8/28/2017
10:50 AM Solid/Sludge Eric McHorney
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 8081B/3510
<0.02 mg/L
09/08/2017
Endrin
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Methoxychlor
SW 846 Method 8081B/3510
<0.0005 mg/L
09/08/2017
Toxaphene
SW 846 Method 8081B/3510
<0.05 mg/L
09/08/2017
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
09/06/2017
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
09/06/2017
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
09/12/2017
2,4-D
SW846 Method 8151A
<0.003 mg/L
09/12/2017
1,1-Dichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Benzene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Report #:: 2017-12878
Page 13 of 15

Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 16090025
Attention:
Report #: 2017-12878
Project ID:
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Methyl ethyl ketone
SW846 Method 8260/5030
<0.05 mg/L
09/14/2017
Tetrachloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
09/14/2017
RCI
Ignitability
EPA 1030
<0.8 mm/sec
09/06/2017
Cyanide
EPA 335.4
<0.1156 mg/kg
09/07/2017
Sulfide
SM 4500 S D
<0.2313 mg/kg
09/11/2017
pH
SW 846 Method 9045D
4.24 units
09/07/2017
Sludge Residuals
Aluminum
EPA 200.7
30100 mg/kg
09/07/2017
Arsenic
EPA 200.7
6.15 mg/kg
09/05/2017
Cadmium
EPA 200.7
<1.58 mg/kg
09/05/2017
Calcium
EPA 200.7
466 mg/kg
09/11/2017
Chromium
EPA 200.7
43.3mg/kg
09/05/2017
Copper
EPA 200.7
5.15 mg/kg
09/05/2017
Lead
EPA 200.7
7.71 mg/kg
09/05/2017
Magnesium
EPA 200.7
1600mg/kg
09/11/2017
Molybdenum
EPA200.7
<1.58mg/kg
09/05/2017
Nickel
EPA 200.7
4.64 mg/kg
09/05/2017
Potassium
EPA 200.7
1080mg/kg
09/11/2017
Selenium
EPA 2007
<1.58 mg/kg
09/05/2017
Sodium
EPA 200.7
412mg/kg
09/11/2017
Zinc
EPA 2007
20.5 mg/kg
09/05/2017
Total Keldahl Nitrogen (TKN)
EPA351.2
915mg/kg
09/05/2017
Nitrate+Nitrite-Nitrogen
EPA 353.2
<0.39 mg/kg
09/15/2017
Reporting limit a evated due to matrix interference.
Total Solids (%)
SM 2540 B
60.9 %
08/28/2017
Report #:: 2017-12878 Page 14 of 15

6602 Windmill Way, Wilmington, NC 28405 o 910.392.0223 Lab & 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910,347.5843 Lab/Fax
[e-mail]
Civil Works Contracting
Date of Report: Sep 20, 2017
1404 Chadwick Drive
Customer PO #:
Speeds Ferry NC
28460
Customer ID: 16090025
Attention-
Report #: 2017-12878
Project ID:
Ammonia Nitrogen
SM 4500 NH3 C
39.68 mg/kg
09/15/2017
Total Phosphorus
SM 4500 P F
119 mg/kg
09/05/2017
Mercury
SW846 74718
0. 0610 mg/kg
08/29/2017
TCLP Metals
Arsenic
EPA 2001
<1.0 mg/L
09/11/2017
Barium
EPA 2007
<1,0 mg/L
09/11/2017
Cadmium
EPA 200.7
<1,0 mgIL
09/11/2017
Chromium
EPA 200.7
<1.0 mg/L
09/11/2017
Lead
EPA 200.7
<1 .0 mg/L
09/11/2017
Selenium
EPA 200,7
<1.0 mg/L
09/11/2017
Silver
EPA 200.7
<1.0 mg/L
09/11/2017
Mercury
EPA 245.1
<0,0020 mg/L
09/08/2017
Comment- Sludge residuals results reported on a dry weight basis,
pH reported on an as received basis.
A Al
Reviewed by: W ViLLCtrL I
Report #': 2017-12878 Paw 15 of 15

Analytical & Consulting Chemists
6602 Windmill Way Wilmington, NC 28405
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-0223 FAX [phone]
NCDENR: DWO CER71FICA71ON # 94 NCDHHS: DLS CERTIFIrATION # 37729 In"onvironmentalchemistecorn
COLLECTION AND CHAIN OF CUSTODY
CLIENI.�:,rV�
PROJECT NAME:
REPORT NO. 4 -7
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
1COPY
TO:
6711:j
41 r2 P7 I Wj
Sample Identification
=&n. I r7m
MM
mulnualum
M
M
�"NM111111
DII, SL = Sludge, Other:
ANALYSIS REQUESTED
Transfer Relinquished By. Datemme Received By. Datarriff te
1.
2. -A-
Temperature when Received: —Accepted: —
R t _ Re—samp-e Requested:Delivered By: Received y: Date:k Time:
TURNAROUND:

ENCLO SURE 6

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