DEQ-CFW_00076391

09/26/91 12: D'8 _ "r3` IEA, CARP 004
J Q
PA
Fi LE (�59�
Sample ID: 951-011-1 EFF-001
A. purgeable (Volatile organic) Fraction, EPA'Method $240
Number of chemical$ detected in Fraction 1
Fraction sTORET Number 84085
STORET
compound Quantitation Quantitation
Humber
L4 it
Target, Limit*
/J
Pollutants to be analyzed fOrz (ug/L) (ug/D)
t
34210
Acrolein
100
34215
Acrylonitrile
100
34030
Benzene
5
32101
Bramodichloromethahe
5
32104
Bromaform
5
34413
Bromomethans
10
32102
Carbon tetrachloride
5
34301
Worobenzene
6
34311
Chloroethane
10
34576
2-Chloroethyl vinyl ether
10
32106
chloroform
5
34418
chloromethane
10
32106
Dibromochloromethane
5
34.496
1,1-Dichloroethane
5
34531
1,2-Dxchloroethane
5
34501
1,1-Dichloroethylene
5
34546
trans-1,2-Dichloroethylene 5
34541
1,2--Dichloropropane
6
34704
cis-1,3-Dichloropropane
5
34699
trams-1,3-Dichloropropene
5
34371
Ethylbenzene
s
34423
Methylene chloride
5
34516
1,1,2,2-Tet.rachloroethane
7
34475
Tetrachloroethylene
5
34010
Toluene
6
34506
1,1,1-Trichloroethane
5
34511
1,1,2-Trichloroethane
5
39180
Trichloroethylene
5
34488
Trichlorofluoromethane
10
39175
Vinyl chloride
10
*If
different from quantitation
limit target
Page 2 of 9
Concentration
Detected
(ug/L )
4100
<100
<5
<5
<5
<10
<5
<6
<10
<10
<5
<10
<5
<5
<5
<5
<5
<6
<5
<5
<8
18
<7
<5
<6
<5
<5
<5
410
c10
GC/MS
confirmation?
Yes No
1
DEQ-CFW 00076391

09/26/91 i2:v9 IEA, CARY a 006
sample I.D.s951-011(0)-1 EFF-001
S. Acid Fatrantarile 3raction,
EFP► Method 8270
Page 4 of 9
Number of
chemicals detected in ,Fraction 1
Fraction
STQRET Number 45582
STOMT
CxXUPQund
Quantitation Quantitation
concentration WKS .
Number
Limit Tar at LiMlt*
Detected
Confirmation?
Pollutants
to be analyzed for:
t
(Ug/�) (ug/L)
(u5f/L)
Yea Na
y
34452
4-Chloro-3 methylphenol 10
<10
x
34586
2-Chlorophenol
10.
<10
x
34601
2,4-Diahloraphanol-
10
<10
x
34606
2,4-Dimethylphenol
10
<10
x
34616
2,4-Diui-trophenol
50
<50
X
34657
2-Methyl-4,6-dinitrophenol 50
<50
X
3458.1
2-Nitrophe4ol _
10
<10
X
34646
4-Nitrophenol
50
<50
x
39032
Pentachlorophenol.
's0
<50
X
34694
Phenol
1.0
<10
x
34621
2,4,6-Trichlorophenol
10
<10
X
*If different from quantitation limit target
r in) A
--"3
49 OCT
CENTRAL FILC COPY
DEQ-CFW 00076392

26/91 13:06 a IEA,CARY
008
Sample I.D.: 951-011(0)-1 EFF-001
C. BaBa/Neutral Praction, EPA Method 8270 Page 6 0£ 9
Number of chemicals detected in Fraction 5
praction STORET Number 45583
STORBT Commpound
Quantitation
Quantitation
concentration
relmS
Number
Limit Target
Limit*
Deteoted
confirmation?
pollutants to be analyzed for.
(ug/L)
(ug/L)
(ug/L)
Yes No
34205
Acenaphthene
10j1/
34200
Acenaphthylene
1.
34220
Anthracene
10
39120
Benzidine
56
34526
Henzo (a) anthracene
10
34247
Benzo (a) pyrene
10
34230
Benzo (b) fluoranthene
10
34521
Benzo (ghi) perylene
10
34242
Benzo (k) fluoranthene
10
34278
His (2-chloroethoxy)methane
10
34273
Blo (2-chloroethyl)ether
10
34283
Bis(2-chlorcisopropyl)ether
10
39100
Bis(2-ethylhexy1)phthalate
10
34636
4-Bromophenyl phenyl ether
10
34292
Butyl benzyl phthalate
10
34581
2-Chloronaphthalene
10
34641
4-Chlorophenyl phenyl ether
10
34320
Chryaenes
10
34556
Dibenzo(a,h) anthracene
10
34536
1,2-Dichlorobenzone,
10
34566
1,3-Dichlorobenzene
10
34571
1,4�Diehlorobenzene
10
34631
3,3-Dichlorobenzidine
20
34336
Diethyl phthalate
10
34341
Dimethyl phthalate
10
39110
Di-n-butyl phthalate
10
34611
2,4-Dinitrotoluene
10
34626
2,6-Dinotrotoluene
10
34596
Di-n-octyl phthalate
10
34346
1,2-Diphenylhydrazine**
10
34376
1+"luoranthene
10
34381
Fluorene
10
39700
Hexachlorobenzene
10
34391.
Hexachlorabutadtana
10
34386
Iiexachlorocyclopentadiene
10
34396
Hexachloroethane
10
34403
iadeno(1,2,3-c4)pyrene
10
34408
Isophorone
1.0
34696
Naphthalene
10
34447
Nitrobenzene
10
34438
N-nitrosodimethylamine
10
34428
N-nitroso-di-n-prapylamine
10
34433
N-nitrosodiphenylamine
10
34461
Phenanthrene
10
34469
Pyrene
10
34551
1,2,4-Trichlorobenzene
10
*if
different from quantitation target
**As
A-zabenzene
<10
<10
<10
<50
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
c1.0
<10
<10
<10
<10
<10
<10
<20
<10
<10
-C10
<10
<16
<10
<10
<10
{10
<10
<10
<10
<10
<10
<10
<10
E10
<10
<10
<1.0
<13�:jAglg 21
<1 oc$ j
CENTRAL FILE CQpy
DEQ-CFW 00076393

09/26/91 13:01
0
IEA,CARY
010
i
Sample IA: 951-011
N/R = Not Requested
D. Organochlorine/Organophosphorus Pesticides and PCB'e
Number of chemicals detected in Fraction
Fraction STET Number 00188
Page 6 of 9
STORET
Compound Quantltation Quantitation ConcentratiQn confirmation?
Number
Limit Target Limit*
Detected Dual Column GC/MS
i.Pollutants to be analyzed for:
(ug/L) (ug/L)
(ug/L) you No yes No
Organochlorime Festicides/Fc8's:
SPA xet�j od 0080
39330
Aldri.n
0.05
N/R
39337
alpha-BHC
0.05 y
N/R
39338
Beta -SEC
0.05
N/R
34259
Delta-BHC
0-1
N/R
39340
Gamma-BHC (Li.ndaae)..
0.05
N/R
39350
Chlordane
0.2
N/R
39310
4,4'-DDD
0.1
N/R
39320
4,4'-DDE
0.1
N/R
39300
4,4'-DDT
0.1
N/R
39380
iiieldrin
0.02
N/R
34361
Endosulfan I (alpha)
0.1
N/R
34356
Rndosulfan II (beta)
0.1
N/R
34351
Endosulfan sulfate
0.7
N/R
39390
Endrin
0.06
N/R
3436E
Endrin aldehyde
0.2
N/R
39410
Heptachlor
0.05
N/R
39420
Heptachlor epoxide
0.8
N/R
39480
Hethoxychl.or
0-6
N/R
39755
Hirex
0.2
N/R
39400
Toxaaphene
2.4
N/R
34671
PC$ 1016
0.5
N/R
39488
PCs 1221
0_5
N/R
39492
PCB 1232
0.5
N/R
39496
PCB 1242
015
N/R
39500
FCB 1248
0.5
N/R
39504
PCB 1254
1.0
N/R
39508
PCB 1260
1.0
N/R
Organophoephorue Pesticides : EPA Method 8080
39660 Demetcn 2.5
39540 parathion (ethyl) 0.6
E. Herbicides, EPA Method 8150 N/R - Not Requested
Number of chemicals detected in Fraction
Fraction STORET Number 00148
N/R
N/R
STORET
Compound
QuUmmtitation Quantitation
concentration
confirmation?
Number
Limit Target Limit*
Detected
Dual Column
Pollutants to be analyzed for; (ug/1') (ug/L)
(ug/L)
yes No
39730
39045
2, 4-D
silvex
12
2
N/R
N/R
SC f �r 1 Z
C !L�g1'l
39740
2,4,5-T
2
N/R
&
,.
*If different from
quantitation limit target
CPAT14L Flu copy
DEQ-CFW 00076394

09/26/91 13:01 $ IEA,CARY 11011
iL
-genic Analytical Informations Page 9 of 9
-genic Frnati.on Method GC operating Conditions Surrogates (spikes)
E traotion Column Description compound Recover
x
I)Atah ContinubUg Length A Xn, Film Thicknacss
;
Column Type, Cai'rieF Gag Z F1oW
gate, Temporature Program
8240 75m x 0.53mm,
1,2-Diohloroethnnm-d4
98
Lrgenble
3MM Da-624, us@ 12mt/min
woluene-d6
97
it-011-1
35 (Slain), 8 deg/min, 140
p-SromofluoroYengAne
103
:id Extrmctebl68
8270 x 30M x 0,32mm, 0.5um
Eheuol-d5
48
Da-625, Re@ 36cm/800e0
2-Fluorophenol'
48
il-all{a)-1
y
40 (4min),300 (10min),
2,4,6-Tribroav3phen01
67
10deg/min
Nitrobenzene-d5
45
2 Pluorobiphenyl
39
Lae/Neutral
6270 30m = 0.32mm, 0.5um
Terpisenyl-di6
36
etractable
DR-625, Reg 90cm/80sac
40 (4min),300 (10min),
10deg/min
-
VMS Library size (number of reference apactra): 49,000 * (RYBT)
!Metals and Other Chemicals
Mgr of metals and Other Chemicals(Be listed above) detected in Semple aa. - Not Raqueated
raction STMMT Number 78240
ToazT . Compound Quantitation Quantitatioa Concentration
amber Limit Target Limit* Detected
01jutants to be analyzed for (ug/L) (ug/L) (ug/L)
1104 Aluminum 50 a/R
1097 Antimony 50 W/R
1002 Arsenio 10 N/R
1012 Beryllium 25 R/R
1027 cadmium 2 N/R
1034 Chromium 5 N/R
NIR
1042 copper 2 M/�
1051 Lead 10
1900 mercury 0.2 R/R
-1067 Nickel 10 N/R
11147 Selenium 5 N/R
11077 silver 5 N/R
i1092 Zinc 10 N/R
tther Inorganio6/
►1007 cerium Soo NIR
10940 Chloride 1000 N/R
10720 Cyanide 20 N/R
10952 Fluoride 100 N/R
tSr different from.quantita.tion limit target
►nalytical Laboratory Representative:
Sign Date: =C !
?nail t o +rotor in Responsible Charge (OCg1=
C certify that this report is accurate and complete to the beat of my knowledge. � C•3
Date OCTD
4igned:
r "'JTRAL FILE Copy
DEQ-CFW 00076395