DEQ-CFW_00085666

a
i
Analytical Data Form
RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/21/06 Project : DuPont2006 Source Name: BEI
Run: 3 Test For: APFOA/PFOA
Terence Method 2 Calculations
Average Stack Velocity T s
Vs = 85.49 Cp APavg VpsMs 33.76ft/sec
Actual Flow Rate
Qa = Vs As 60 12,032 ACFM
Average Stack Volumetric Flow Rate Qsd = 3600 [1 - Bws] Vs A Tstd 1 r Ps 1
Tstk J L Pstd J 686,923.5 dscf/hr
arence Method 3 Calculations
Molecular Weight, Dry Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + %N2)
28.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 -Bws) + 18 (Bws)
28.61 lb/lb-mole
Reference Method 4 Calculations
Sample volume, Standard Conditions Pbar + AH
Vm(std) = 17.64 Tm Y Vm 13.6
S 211.533 dscf
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i] 3.0 ft^3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wi] 1.5 ft^3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
[Vwc(std) + Vwsg(std) + Vm(std) 0.0208
Reference Method 5 Calculations
Percent Isokinetic (0.002669) (Vic) + I Tm I (Pbar + AH/ 13.6)
I = 100Ts l /l
60 B Vs Ps An 97.1 %
Concentration
Cs 0.0154 gr Mn
[ mg [Vm(std)] APFO 0.00007891 gr/dscf
Mass Emission Rate E J (Cs) (Qsd) 1 PFOA 0.00007565 gr/dscf
7,000 gr / dscf
APFO 0.00774361b/hr
PFOA 0.0074237lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 568000 678000 336694.8 904650.7
PFOA 544000 651000 323286.6 867244.2
Cond. Tare Final Net
63.5 560.1 496.6
Page 57 of 126
DEQ-CFW 00085666

11
c
RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/22/06 Project : DuPont2006 Source Name : BEI
Run: 4 Test For: APFOA/PFOA
Reference Method 2 Calculations
Average Stack Velocity
Vs = 85.49 Cp APavg Ts
32.4 ft/sec
Actual Flow Rate
Qa = Vs As 60 11,547 ACFM
Average Stack Volumetric Flow Rate Q sd = 3 600 [1 - Bws] Vs A Tstd Ps
[Tstkl [Pstd]
667,893.1 dscf/hr
Reference Method 3 Calculations
Molecular Weight, Dry Md = 0.44 (%CO2) + 0.32 (1.02) + 0.28 (%CO + %N2)
28.84 lb/lb-mole
Molecular Weight, Wet Ms = Md(1 - Bws) + 18 (Bws)
28.61 lb/lb-mole
Reference Method 4 Calculations
Sample volume, Standard Conditions AH
o Pbar +
Vm(std) = 17.64 Y Vm Tm 13.6 206.787 dscf
g
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i] 2.9 ft"3/ml
Water Vapor Volume Collected Vwsg(std) = 0.04715 [Wf - Wil
1.8 ft"3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
[Vwc(std) + Vwsg(std) + Vm(std) 0.0208
:rence Method 5 Calculations
Percent Isokinetic
(0.002669) (Vic + I r Y Vrnl (Pbar + 4II/ 13.6)
I=100Ts \ Tm 97.8%
60 B Vs Ps An
Concentration
Cs = [0.0154gr J [Vm(std)]
MnAPFO 0.00010813 gr/dscf
mg
Mass Emission Rate E J _ [ (Cs) (Qsd) 1 PFOA 0.00010389 gr/dscf
7,000 gr / dscf APFO 0.010317 Ib/hr
PFOA 0.0099125lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 766000 970000 473554 1239510
PFOA 736000 932000 455002.4 1190960
Cond. Tare Final Net
65.2 553.4 488.2
Page 58 of 126
DEQ-CFW 00085667

A
RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/21/06 Project: DuPont2006 Source Name: BEI
Run: 5 Test For: APFOA/PFOA
Reference Method 2 Calculations
le Stack Velocity
Flow Rate
ie Stack Volumetric Flow Rate
:rence Method 3 Calculations
Vs = 8 5.4 9 Cp -APavg Ts
V7Ps Ms
Qa = Vs As 60
Qsd = 3600 [1 - Bws Tstd Ps
Vs A [Tstk] [Pstd ]
31.47 ft/sec
11,216 ACFM
640,328.3 dscf/hr
Molecular Weight, Dry Md = 0.44 (%CO2) + 0.32 (1/602) + 0.28 (%CO + 0/.N2)
28.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 -Bws) + 18 (Bws)
28.61 lb/lb-mole
:rence Method 4 Calculations
Sample volume, Standard Conditions
Pbar + �H
13.6
Vm(std) = 17.64 Tm Y Vm
g 204.042 dscf
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i] 2.9 ft"3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wil 1.3 ft"3/g
Moisture Volume Fraction of Stack Gas
Bws _ Vwc(std) + Vwsg(std)
— [Vwc(std)
+ Vwsg(std) + Vm(std) 0.0208
arenre Method 5 Calculations
Percent Isokinetic (0.002569) (Vic) + Tm ( Pbar + AI3/ 13.6)
I = 100Ts
60 B Vs Ps An 100.5 %
Concentration
gr Mn
Cs = [0.0154 mg] [Vm(std)] APFO 0.00011212 gr/dscf
Mass Emission Rate [ E (Cs) (Qsd) PFOA 0.00010767 gr/dscf
7,000 gr / dscf
APFO 0.01025621b/hr
PFOA 0.0098492lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 804000 965000 481342 1285298
PFOA 772000 927000 462387.6 1234345
Cond. Tare Final Net
63.5 562.3 498.8
Page 59 of 126
DEQ-CFW 00085668

t!
Run 1
Example Calculations
1) Dry Gas Volume, Standard Conditions (68 F and 29.92 in. Hg), DSCF
o Pbur+ OH
Vmsrd = C17.64 Hg) (Y) (V—) T 13.6
1.94
Vmstd = (17.64) (1.013) (182.272) 29.90 +
13.6
554
2) Volume of Water Vapor Collected, SCF
VW,: = 0.04707 (V f - Vi )
Vwc(std) = 0.04707 ( 354.8 — 300.0)
V sg = 0.04715 (V f - Vi )
Vwsg(std) = 0.04715 ( 825.1 — 801.6)
3) Proportion of Water Vapor, by Volume
Vwc(std) + Vwsg(std)
Bws = I Vwc(std) + Vwsg(std) + Vm(std)
Bws = (2.6) + (1.1)
(2.6) + (1.1) + (176.540)
4) Absolute Stack Gas Pressure, in. H
Ps= Pbar + Pg
13.6
PS = 29.90 -}-
-1.5
13.6
Page 60 of 126
= 176.54 dscf
2.6 scf
1.1 scf
= 0.0205
= 29.79 in. Hg
DEQ-CFW 00085669

a
Run 1
Example Calculations
5) Dry Molecular Weight of Stack Gas, lb/lb-mole
Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + %N2)
Md = (0.44) (0.00) + (0.32) (20.90) + (0.28) ( 79.10)
"all Zeros indicate an assumption per 40 CFR part 60 subpart I =
6) Wet Molecular Weight of Stack Gas, lb/lb-mole
28.84 lb/lb-mole
Ms = Md (1- Bws) + 18 (Bws)
Ms = 28.84 ( 1 — 0.0205 ) + 18 ( 0.0205) = 28.62 lb/lb-mole
7) Average Stack Gas Velocity, ft/sec
TS
Vs = (85.49) (Cp) (�a,$) (MS) (PS)
V, = (85.49) (0.84) (0.49) (546.0) = 28.16 ft/sec
(28.62) (29.79)
8) Average Stack Gas Dry Volumetric Flow Rate, DSCF/Hr
Qsd = 3600 11- BwsI Vs A
[ Tstd Ps Tstk Pstd
Qsd = (3600) ( 1 — 0.0205) (28.16) (5.94) 528 29.79
546 F2992
567,905.7 dscf/hr
9) Actual Volumetric Flow Rate, ACFM
Qa = Vs As 60
%= (28.16) (5.94) (60)
Page 61 of 126
10,036 ACFM
DEQ-CFW 00085670

Run 1
Example Calculations
10) Isokinetics, Percent
(0.002669) (Vic)+[� Yi Vm ( Pbar + OH/13.6)
I=100Ts Tm
60 0 Vs Ps An
I = (100) (546)
11) Concentration, gr/dscf
(0.002669) (78.30) + (1.013) (182.272) ( 29.90 + 1_94
554 13.6
Cs= 0.0154 gr
] [ Mn
Mg Vn (std)
CS = 0.0154
27218254
176.540
12) Emission Rate, lbs/hr
E _ r (Cs) (Qsd)
L7,000 gr/dscf
E _ (0.0000) (567905.7)
7,000
(60.0) (240.0) (28.16) (29.79) (0.000459)
Page 62 of 126
100.6 %
= 0.00002374 gr/dscf
0.0018481 Ib/hr
DEQ-CFW 00085671

i
Summary Test Data
DuPont fayetteville
Sampling Train Data
1 Sampling time, minutes
2 Sampling nozzle diameter, inches
3 Sampling nozzle cross-section area, ft^
4 Isokinetic variation
5 Sample gas volume --standard condition
6 Average meter temperature OR
7 Average orifice pressure drop, in H2O
Velocity Traverse Data
8 Stack area, ft^2 As
9 Absolute stack gas pressure, inches Hg. Ps
10 Barometric pressure, inches Fig. Pbar
11 Average absolute stack temperature, OR Ts
12 Average sqrt. velocity head, (Cp = .84) VXT
13 Average stack gas velocity, ft/second Vs
Stack Moisture Content
14 Total water collected by train, ml Vic
15 Moisture in stack gas, percent % Bws
Emissions Data
16 Stack gas flow rate, dscf/hr Qsd
17 Stack gas flow rate, cfm acfm
18 APFO concentration, gr/dscf Cs
19 PFOA concentration, gr/dscf Cs
20 APFO emissions, Ib/hr E
21 PFOA emissions, Ib/hr E
PROJECT: )uPont200( Test For: APFOA/PFOA
Location: BEI
Run #1 Run #2
Date 06/21 /06 06/21 /06
start 08:54 14:35
6 240 240
Dn 0.2900 0.2900
2 An 0.000459 0.000459
1 100.6 107.7
s dsft^3 Vm(std) 176.540 192.682
Tm 554 545
AH 1.94 1.97
Run #3 Run #4 Run #5
06/21/06 06/22/06 06/22/06
20:42 01:34 06:09
240 240 240
0.2940 0.2940 0.2940
0.000471 0.000471 0.000471
97.1 97.8 100.5
211.533 206.787 204.042
542 538 541
2.56 2.45 2.25
Average
100.8
198.317
544
2.23
5.94
5.94
5.94
5.94
5.94
5.94
29.79
29.79
29.79
29.79
29.79
29.79
29.90
29.90
29.90
29.90
29.90
29.90
546
545
541
534
541
541.4
0.49
0.50
0.59
0.57
0.55
0.54
28.16
28.73
33.76
32.40
31.47
30.90
78.30
97.70
95.60
101.10
90.80
92.70
2.05
2.38
2.08
2.08
2.08
2.13
567,905.7 578,508.5 686,923.5 667,893.1 640,328.3
10,036 10,239 12,032 11,547 11,216
0.0000237 0.0000513 0.0000789 0.0001081 0.0001121
0.0000228 0.0000492 0.0000757 0.0001039 0.0001077
0.0019260 0.0042355 0.0077436 0.0103170 0.0102562
0.0018481 0.0040644 0.0074237 0.0099125 0.0098492
Page 63 of 126
628311.8
11014
0.0000748
0.0000718
0.0068957
0.0066196
DEQ-CFW 00085672

Analytical Data Form
Project No. DuPont2006
Source: BES
Test for: APFOA/PFOA
Plant
DuPont fa etteville
Ambient Temp(°F)
76
Impinger 11
Vol. (ml)
Silica Gel
Weight, (g)
Location Fayetteville, NC Barometric Pressure(in. Hg) 29.98
Operator
JP
Assumed Moisture
1
Final
Date
6/21/2006
Probe length (ft)
4
Initial
MMI
Run
1
Probe Heater setting
Diff.
Sample Box No.
26-2
Nozzle Diameter (in.)
0.2770
Filter No.
Meter Box No.
Nozzle Area(ft^2)
0.000418
02
20.90
Meter OHa
1.7583
Leak rate (ft^3/min)
.015 5"
CO2
C Factor
0.997
Static Pressure (in. H2O)
2.3
CO + N2
79.10
Pitot Cp
0.84
Stack Diameter (in)
30
As (ft^2)
4.91
Test Time(start/finish)
8:50:00
Stack Dimensions(in) L x W
As (ft^2)
Test Time (total)
240
Multiplier 6.288
Traverse
Points
Stack
Temp
(Ts)
Velocity Head
(in. H2O)
(OP)
Pressure Diff.
Orifice (in. H2O)
(4H)
Dry Gas
Volume (ft^3)
(Vm)
Gas Sample
Dry Gas Meter (°F)
Inlet Outlet
623.810
1
86
0.28
1.76
90
2
87
0.30
1.89
91
3
87
0.27
1.70
92
4
87
0.23
1.45
93
5
87
0.27
1.70
93
6
88
0.45
2.83
93
7
88
0.37
2.33
93
8
88
0.34
2.14
94
9
88
0.31
1.95
94
10
89
0.35
2.20
94
11
89
0.39
2.45
94
12
89
0.42
2.64
94
1
89
0.35
2.20
94
2
89
0.37
2.33
95
3
90
0.34
2.14
96
4
90
0.31
1.95
96
5
90
0.32
2.01
97
6
91
0.32
2.01
98
7
91
0.35
2.20
99
8
91
0.34
2,14
101
9
91
0.35
2.20
102
10
92
0.43
2.70
103
11
92
0.33
2.08
104
12
92
0.32
2.01
828.640 105
Average
TS(°R)
Avera ec
Average
off (in. H2O)
Average
I Vm(ft^3)
Average
I Tm(°R)
_
AM! I
549 0.58 2.12 204.830 556
Page 64 of 126
DEQ-CFW 00085673

Analytical Data Form
Project No. DuPont2006
Source: BES
Test for: APFOA/PFOA
Plant
DuPont fa etteville
Ambient Temp ff)
94
Impinger
1 Vol. (ml)
Silica Gel
Weight, (g)
Location Fayetteville, NC Barometric Pressure(in. Hg) 29.98
Operator
JP
Assumed Moisture
1
Final
376
868.4
Date
06/21/06
Probe length (ft)
4
Initial
300
841.8
Run
2
Probe Heater setting
0
Diff.
76.0
26.6
Sample Box No.
26-2
Nozzle Diameter (in.)
0.2770
Filter No.
Meter Box No.
0
Nozzle Area (ftA2)
0.000418
02
20.90
MeterAHa
1.7583
Leak rate (ftA3/min)
.000 14"
CO2
C Factor
0.997
Static Pressure (in. H2O)
2.3
CO + N2
79.10
Pitot Cp
0.84
Stack Diameter (in)
30
As (ftA2)
4.91
Test Time(start/finish)
14:42:00
Stack Dimensions(in) L x W
As (ftA2)
Test Time (total)
240
Multiplier 6.288
Traverse
Points
I Stack
Temp
(Ts)
I Velocity Head
(in. H2O)
(AP)
Pressure Diff.
Orifice (in. H2O)
I (AH)
I Dry Gas
Volume (ftA3)
I (Vm)
Gas Sample
Dry Gas Meter (°F)
I Inlet I Outlet
0
830.235
1
94
0.31
1.95
103
2
94
0.30
1.89
103
3
93
0.33
2.08
104
4
93
0.34
2.14
104
5
93
0.30
1.89
104
6
93
0.32
2.01
104
7
93
0.31
1.95
103
8
93
0.31
1.95
102
9
83
0.32
2.01
70
10
78
0.45
2.83
64
11
70
0.42
2.64
54
12
66
0.45
2.83
55
1
76
0.46
2.89
56
2
76
0.45
2.83
56
3
76
0.45
2.83
57
4
67
0.37
2.33
60
5
83
0.37
2.33
76
6
84
0.34
2.14
78
7
84
0.36
2.26
80
8
84
0.35
2.20
81
9
84
0.35
2.20
82
10
84
0.37
2.33
82
11
84
0.37
2.33
82
12
84
0.37
2.33
1,035.368 82
Average
Average_
Average
Average
Average
Ts(°R)
AH (in. H2O)
Vm(ftA3)
I Tm(°R)
544 0.60 2.30 205.133 541
Page 65 of 126
DEQ-CFW 00085674

Analytical Data Form
Project No. DuPont2006
Source: BES
Test for: APFOA/PFOA
Plant
DuPont fa etteville
Ambient Temp(°F)
72
lmpinger
Vol. (ml)
Silica Gel
Weight, (g)
Location Fayetteville, NC Barometric Pressure(in. Hg) 29.98
Operator
JP
Assumed Moisture
1
Final
F 371.4
829.3
Date
06/21/06
Probe length (ft)
4
Initial
300
797.E
Run
3
Probe Heater setting
0
Diff.
71.4
31.7
Sample Box No.
26-2
Nozzle Diameter (in.)
0.277
Filter No.
Meter Box No.
0
Nozzle Area(ftA2)
0.000418
02
20.90
Meter AHa
1.7583
Leak rate (ftA3/min)
.001 10"
CO2
C Factor
0.997
Static Pressure (in. H2O)
2.3
CO + N2
79.10
Pitot Cp
0,84
Stack Diameter (in)
30
As (ftA2)
4.91
Test Time(start/finish)
20:45:00
Stack Dimensions(in) L x W
As (ftA2)
Test Time (total)
240
Multiplier 6.288
Traverse
Points
IStack
Temp
(Ts)
Velocity Head
(in. H2O)
(AP)
I Pressure Diff.
Orifice (in. H2O)
(Z
I Dry Gas
Volume (ftA3)
I (Vm)
Gas Sample
Dry Gas Meter (°F)
I Inlet I Outlet
0
35.671
1
84
0.37
2.33
78
2
84
0.35
2.20
80
3
84
0.30
1.89
80
4
84
0.29
1.82
80
5
84
0.32
2.01
81
6
84
0.35
2.20
82
7
84
0.35
2.20
82
8
84
0.37
2.33
82
9
84
0.36
2.26
82
10
84
0.35
2.20
83
11
84
0.30
1.89
83
12
84
0.30
1.89
83
1
84
0.32
2.01
82
2
84
0.30
1.89
81
3
84
0.34
2.14
81
4
84
0.29
1.82
81
5
84
0.29
1.82
82
6
84
0.28
1.76
82
7
84
0.31
1.95
82
8
84
0.31
1.95
82
9
84
0.31
1.95
82
10
84
0.29
1.82
82
11
84
0.31
1.95
82
12
84
0.30
1.89
224,365 82
Average
Avera a
Average
Average
Average
I
Ts('R)
4H (in. H2O)
Vm(ftA3)
Tm(°R)
544 0.57 2.01 188.694 542
Page 66 of 126
DEQ-CFW 00085675

Project wn.oupont2oua
anunm: aEG
Test for: APFOA/PFOA
Vol- (ml) IlWeight,
(g),
Location Fayetteville, NC Barometric Pressure(in, Hg) 29.98
-Operator
JP
Assumed Moisture
1
Final
359.4
M877.3]
Sample Box No.
26-2
Nozzle Diameter (in.)
0.277
Filter No.
[Test Time (total)
240
Multiplier 6.288
Traverse
Stack
Velocity Head
Pressure Diff,
I Dry Gas
I Gas Sample
Points
Temp
(in. H20)
Orifice (in. H20)
Volume (ftA 3)1
Dry Gas Meter ('F)
O
226140
1 Oo
0.35
luO
ro
2 82
0.34
214
76
3 81
0.30
228
77
4 02
0.33
2.08
78
5 81
0.35
220
78
8 81
0.35
220
79
7 01
0.34
2.14
00
8 81
0.33
2.08
80
9 82
8.35
220
81
10 82
8.87
2.33
81
11 82
0.37
2.33
82
12 01
0.37
2.33
82
1 81
0.37
2.33
82
2 81
0.33
208
88
3 81
0.32
2.01
83
4 02
U5
2,20
83
n Dz
0.33
2.08
83
O 02
0.34
2.14
OS
7 82
0.33
2.08
83
8 82
0.35
2.08
02
8 82
0.35
220
82
10 82
0.32
2.81
02
11 82
0.30
1.89
Do
Average
Average
Average
Average
Average
Page 67 ofl26

Project No. DuPnnt2OoO
Source: BES
Test for: APFOA/PFOA
'Plant
DuPont fayetteville
Ambient Temp(*F)
75
1 Impinger
Vol- (ml)
Silica Gel
Weight, (g)
Location Fayefteville, NC Barometric Pressure(in. Hg) 29.98
Operator
JP
Assumed Moisture
I
Final
358.5
852.8
'Sam, pie Box No.
26-2
Nozzle Diameter (in.)
0.277
Filter No.
4.91
ITest Time (total)
240
Multiplier 6.288
Traverse
' Stack
Velocity Head
Pressure Diff.
Dry Gas
Gas Sample
Points
Temp,
(in. H20,)
Orifice (in.zH20)
Volume (ftAa,)�
Dry Gas.Meter (*f,)
O
421.5#O
1 81
0.50
1.89
75
2 81
028
1.70
75
3 01
031
1.35
76
4 81
0.33
2.08
77
5 01
0.34
2]4
78
0 81
0.35
2.20
79
7 82
0.30
1.89
79
O 02
0.38
2.08
80
8 82
028
1.76
80
10 82
027
170
82
11 02
0.33
2.08
82
12 83
0.35
2.20
83
1 83
027
1.70
84
z 0
0.30
1.89
ou
3 03
0.30
1.88
80
4 84
0.28
1.82
91
5 84
0.80
1.89
02
8 04
0.29
1.82
SO
7 85
029
1.82
nn
8 85
0.33
2.08
88
8 85
0.33
2.08
80
10 85
0.83
2.08
SO
11 00
0.83
2.08
SU
12 OO
0.33
2.08
608.075 SO
Average
Average
Average
I Average
I Average
Page 68 of|26

Analytical Data Form
RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/21/06 Project : DuPont2006 Source Name: BES
Run : 1 Test For : APFOA/PFOA
Reference Method 2 Calculations
Average Stack Velocity
Vs = 8 5.4 9 Cp APavg Fps
sM s 33.23 ft/sec
Actual Flow Rate
Qa = Vs As 60
9,790 ACFM
Average Stack Volumetric Flow Rate ITstdr Ps Qsd = 3600 [1 - Bws Vs A L J
Tstk Pstd 557,237.0 dscf/hr
!rence Method 3 Calculations
Molecular Weight, Dry
Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + %N2) 28.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 - Bws) + 18 (Bws) 28.61 lb/lb-mole
wence Method 4 Calculations
Sample volume, Standard Conditions °R Pbar + OH
Vm(std) = 17.64 195.252 Y Vm Tm 13.6
g dscf
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i] 2.9 ft^3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wi] 1.3 ft^3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
[Vwc(std) + Vwsg(std) + Vm(std) 0.0211
arence Method 5 Calculations
Percent Isokinetic Yi VTmm
(0.002669) (Vic + ( )
(Pbar + pH { 13.6)
I = 100 Ts 60 B Vs Ps
An
102.9
Concentration
Cs = [0.0154 gr r Mn 1
mg L Vm(std) J
APFO
0.00002326 gr/dscf
Mass Emission Rate (Cs) (Qsd) 1
PFOA
0.00002231 gr/dscf
E _ [
7,000 gr / dscf J
APFO
0.0018516
PFOA
0.001776lb/hr
Filter
Cond.
Cond.
Total
ng
ng/L
ng
ng
APFO 192000
204000
103000
294955.5
PFOA 184000
196000
98960.4
282918
Cond. Tare
Final
Net
63.2
568.1
504.9
Page 69 of 126
DEQ-CFW 00085678

Analytical Data Form
RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/21/06 Project : DuPont2006 Source Name: BES
Run: 2 Test For: APFOA/PFOA
Drente Method 2 Calculations
Average Stack Velocity
Vs = 8 5.4 9 C p VAPavg s34.24 ft/sec�:Ms
Actual Flow Rate
Qa = Vs As 60 10,087 ACFM
Average Stack Volumetric Flow Rate Qsd = 3 600 [1 - Bws] Vs A Tstd r Ps
I1
Tstk Pstd J 577,852.9 dscf/hr
rence Method 3 Calculations
Molecular Weight, Dry
Md = 0.44 (0/.CO2) + 0.32 (%02) + 0.28 (%CO + °/uN2)
28.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 - Bws) + 18 (Bws) 28.58 lb/lb-mole
Reference Method 4 Calculations
Sample volume, Standard Conditions Pbar + AH
Vm(std) = 17.64 BH Y Vm Tm 13.6
g 201.051 dscf
Water Vapor Volume Collected
Vwc(std) = 0.04707 [V f - V i] 3.6 ft^3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wil
1.3 fi^3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
I Vwc(std) + Vwsg(std) + Vm(std) 0.0238
Reference Method 5 Calculations
Percent Isokinetic (0.002669) (Vic) + ( Yi VTmm (Pbar + AH / 13.6)
I = 100 Ts
60 0 Vs Ps An 102.2 %
Concentration
Cs 0.0154 gr Mn
[ mg [Vm(std)] APFO 0.0000661 gr/dscf
Mass Emission Rate r E (Cs) (Qsd) PFOA 0.00006352 gr/dscf
L7,000 gr / dscf APFO 0.0054566 Ib/hr
PFOA 0.0052436lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 620000 446000 218138.6 838094.5
PFOA 596000 428000 209334.8 805292.4
Cond. Tare Final Net
63.6 552.7 489.1
Page 70 of 126
DEQ-CFW 00085679

Analytical Data Form
RAMCON Environmental Corporation Emissions Calculations
Test Date: 06/21/06 Project : DuPont2006 Source Name: BES
Run: 3 Test For: APFOA/PFOA
erence Method 2 Calculations
Average Stack Velocity
Vs = 85.49 Cp APavg s�sT
M s 32.53 ft/sec
Actual Flow Rate
Qa = Vs As 60 9,583 ACFM
Average Stack Volumetric Flow Rate
Qsd = 3600 [1 - Bws Tstd Ps Vs A Tstk] Pstd]
547,813.0 dscf/hr
�rence Method 3 Calculations
Molecular Weight, Dry Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + %N2)
29.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 - Bws) + 18 (Bws)
28.56 Ib/Ib-mole
�rence Method 4 Calculations
Sample volume, Standard Conditions Pbar + AH
Vm(std) = 17.64 m Tm Y V13.6
S 184.468 dscf
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i] 3.4 ft^3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wi] 1.5 ft^3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
[Vwc(std) + Vwsg(std) + Vm(std) 0.0259
rence Method 5 Calculations
Percent Isokinetic (0.002669) (Vic) + I Tm (Pbar + AH/ 13.6)
I = 100Ts
60 B Vs N An 98.9 %
Concentration
Cs 0.0154 gr Mn
mg [ Vm(std) ] APFO 0.00005577 gr/dscf
Mass Emission Rate [ E J (Cs) (Qsd) 1 PFOA 0.00006117 gr/dscf
7,000 gr / dscf
APFO 0.00436451b/hr
PFOA 0.0047871lb/hr
Filter Cond_ Cond_ Total
ng ng/L ng ng
APFO 512000 411000 195142.8 707098.7
PFOA 588000 395000 187546 775503.6
Cond. Tare Final Net
63.4 538.2 474.8
Page 71 of 126
DEQ-CFW 00085680

RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/22/06 Project : DuPont2006 Source Name : BES
Run: 4 Test For: APFOA/PFOA
Reference Method 2 Calculations
e Stack Velocity
Flow Rate
e Stack Volumetric Flow Rate
Reference Method 3 Calculations
Vs = 85.49 Cp APavg �'T
Ms
Qa = Vs As 60
Qsd = 3600 [1 - Bws] Vs A [Tstk]
Tstd[Pstd]
Ps
33.04 ft/sec
9,734 ACFM
454.7 dscf/hr
Molecular Weight, Dry
Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + %N2)
28.84 lb/lb-mole
Molecular Weight, Wet Ms = M d (1 - Bws) + 18 (Bws)
28.56 lb/lb-mole
Reference Method 4 Calculations
Sample volume, Standard Conditions
Vm(std) = 17.64 OR Y Vm Tm 13'6 191.383 dscf
B
Water Vapor Volume Collected
Vwc(std) = 0.04707 [V f - V i] 2.8 ft"3/ml
Water Vapor Volume Collected Vwsg(std) = 0.04715 [Wf - Wi]
1.8 ft^3/g
Moisture Volume Fraction of Stack Gas Bws _ Vwc(std) + Vwsg(std)
I Vwc(std) + Vwsg(std) + Vm(std) 0.0259
vence Method 5 Calculations
Percent Isokinetic r
(0.002669) (Vic) + I Y Vml (Pbar + AH/ 13.6)
I = 100Ts 60 0 VmPS An 100.4
Concentration rr 1 [Vm(std)]
Cs = 10.0154 EJ MnAPFO 0.00010138 gr/dscf
mg
Mass Emission Rate r E (Cs) (Qsd) 1 PFOA 0.00009759 gr/dscf
7,000 gr / dscf IL J
APFO 0.008088 Ib/hr
PFOA 0.0077857lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 1080000 440000 205348 1285304
PFOA 1040000 423000 197414.1 1237372
Cond. Tare Final Net
62.9 529.6 466.7
Page 72 of 126
DEQ-CFW 00085681

RAMCON Environmental Corporation Emissions Calculations
Test Date : 06/21/06 Project : DuPont2006 Source Name : BES
Run: 5 Test For: APFOA/PFOA
Reference Method 2 Calculations
Average Stack Velocity
Vs = 85.49 Cp APavg Ts
P s M s 31.93 ft/sec
Actual Flow Rate
Qa = Vs As 60 9,407 ACFM
Average Stack Volumetric Flow Rate Tstd Ps
Qsd = 3600 [l - Bws Vs A Tstk Pstd
538,699.1 dscf/hr
?rence Method 3 Calculations
Molecular Weight, Dry Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + 0/.N2)
28.84 lb/lb-mole
Molecular Weight, Wet
Ms = Md (1 -Bws) + 18 (Bws)
28.56 Ib/Ib-mole
wence Method 4 Calculations
Sample volume, Standard Conditions
OR Pbar + AH
Vm(std) = 17.64 m Y VTm 13.6
g
181.621 dscf
Water Vapor Volume Collected
V wc(std) = 0.04707 [V f - V i]
2.8 ft^3/ml
Water Vapor Volume Collected
Vwsg(std) = 0.04715 [Wf - Wil
1.4 ft^3/g
Moisture Volume Fraction of Stack Gas
Bws _ Vwc(std) + Vwsg(std)
[Vwc(std)
+ Vwsg(std) + Vm(std)
0.0259
wence Method 5 Calculations
Percent Isokinetic (0.002669) (Vic + I Tm (Pbar + AU 13.6)
I = 100Ts 60 0 Vs Ps An °
98.7 /o
Concentration
Cs 0.0154 gr Mn
[ mg [ V m(std) ] APFO 0.00009527 gr/dscf
Mass Emission Rate E _ [ (Cs) (Qsd) 1 PFOA 0.00009142 gr/dscf
7,000 gr / dscf J
APFO 0.00733171b/hr
PFOA 0.0070354lb/hr
Filter Cond. Cond. Total
ng ng/L ng ng
APFO 1030000 390000 177957 1207913
PFOA 988000 375000 171112.5 1159070
Cond. Tare Final Net
65.2 521.5 456.3
Page 73 of 126
DEQ-CFW 00085682

Run 1
Example Calculations
1) Dry Gas Volume, Standard Conditions (68 F and 29.92 in. Hg), DSCF
r o Pb-4-OH
Vmsca = 117.64 Hg) (Y) (V-) T 13.6
2.12
Vmstd = (17.64) (0.997) (204.830) 29.98 +
13.6
556
2) Volume of Water Vapor Collected, SCF
V we = 0.04707 (V f - Vi )
Vwc(std) = 0.04707 ( 361.3 — 300.0)
V sg = 0.04715 (V f - Vi )
Vws9(std) = 0.04715 ( 819.0 — 791.7)
3) Proportion of Water Vapor, by Volume
Bws = Vwc(std) + Vwsg(std)
[Vwc(std) + Vwsg(std) + Vw(std)
BWs = (2.9) + (1.3)
(2.9) + (1.3) + (195.252)
4) Absolute Stack Gas Pressure, in. Hg
Ps= Pbar + Pg
13.6
Ps = 29.98 + 2.3
13.6
Page 74 of 126
195.252 dscf
= 2.9 scf
= 0.0211
= 30.15 in. Hg
DEQ-CFW 00085683

Run 1
Example Calculations
5) Dry Molecular Weight of Stack Gas, lb/lb-mole
Md = 0.44 (%CO2) + 0.32 (%02) + 0.28 (%CO + 0/.N2)
Md = (0.44) (0.00) + (0.32) (20.90) + (0.28) ( 79.10)
all Zeros indicate an assumption per 40 CFR part 60 subpart 1 = 28.84 lb/lb-mole
6) Wet Molecular Weight of Stack Gas, lb/lb-mole
Ms = Md (1- Bws) + 18 (Bws)
MS = 28.84 ( 1 — 0.0211 ) + 18 (0.0211) = 28.61 lb/lb-mole
7) Average Stack Gas Velocity, ft/sec
Ts
V5 = (85.49)(Cp)(�a,g)
(Ms) (Ps)
VS _ (549.0)
(85.49) (0.84) (0.58) 33.23 ft/sec
(28.61) (30.15)
8) Average Stack Gas Dry Volumetric Flow Rate, DSCF/Hr
Qsd = 3600 11- BwsI Vs A Tstd Ps
Tstk Pstd
Qsd = (3600) ( 1 — 0.0211) (33.23) (4.91) 528 r30.15
F549 F29.92
557,237.0 dscf/hr
9) Actual Volumetric Flow Rate, ACFM
Qa = Vs As 60
Qa= (33.23) (4.91) (60) = 9,790 ACFM
Page 75 of 126
DEQ-CFW 00085684

Run 1
Example Calculations
10) Isokinetics, Percent
(0.002669) (Vic)+ Yi Vm ( Pbar + AH/13.6)
Tm
I=100Ts
60 0 Vs Ps An
= (100) (549)
11) Concentration, gr/dscf
(0.002669) (88.60) + (0.997) (204.830) ( 29.98 + 2.12
556 l 13.6
Cs= 0.0154 gr
] [ Mn
Mg Vn(std)
CS = 0.0154 •2949555
195.252
12) Emission Rate, lbs/hr
E_ (Cs) (Qsd)
7,000 gr/dscf
E _ (0.0000) (557237.0)
7,000
(60.0) (240.0) (33.23) (30.15) (0.000418)
Page 76 of 126
102.9 %
0.00002326 gr/dscf
0.001776 1b/hr
DEQ-CFW 00085685

Summary Test Data
PROJECT: )uPont200(
Test For:
APFOA/PFOA
DuPont fayetteville
Location:
BES
Sampling Train Data :
Run # 1
Run # 2
Run # 3
Run # 4
Run # 5
Average
Date
06/21/06
06/21/06
06/21/06
06/22/06
06/22/06
start
08:50
14:42
20:45
01:35
06:10
1 Sampling time, minutes
9
240
240
240
240
240
2 Sampling nozzle diameter, inches
Dn
0.2770
0.2770
0.2770
0.2770
0.2770
3 Sampling nozzle cross-section area, ft^2
An
0.000418
0.000418
0.000418
0.000418
0.000418
4 Isokinetic variation
1
102.9
102.2
98.9
100.4
98.7
100.6
5 Sample gas volume --standard conditions dsft^3
Vm(std)
195.252
201.051
184.468
191.383
181.621
190.755
6 Average meter temperature °R
Tm
556
541
542
541
544
545
7 Average orifice pressure drop, in H2O
AH
2.12
2.30
2.01
2.14
1.95
2.10
Velocity Traverse Data
8 Stack area, ft^2
As
4.91
4.91
4.91
4.91
4.91
4.91
9 Absolute stack gas pressure, inches Fig.
Ps
30.15
30.15
30.15
30.15
30.15
30.15
10 Barometric pressure, inches Hg.
Pbar
29.98
29.98
29.98
29.98
29.98
29.98
11 Average absolute stack temperature, °R
Ts
549
544
544
542
543
544.4
12 Average sqrt. velocity head, (Cp = .84)
VT�T
0.58
0.60
0.57
0.58
0.56
0.58
13 Average stack gas velocity, ft/second
Vs
33.23
34.24
32.53
33.04
31.93
32.99
Stack Moisture Content
14 Total water collected by train, ml
Vic
88.60
102.60
103.10
96.60
87.30
95.64
15 Moisture in stack gas, percent %
Bws
2.11
2.38
2.59
2.59
2.59
2.45
Emissions Data
16 Stack gas flow rate, dscf/hr
Qsd
557,237.0
577,852.9
547,813.0
558,454.7
538,699.1
556011.3
17 Stack gas flow rate, cfm
acfm
9,790
10,087
9,583
9,734
9,407
9720
18 APFO concentration, gr/dscf
Cs
0.0000233
0.0000661
0.0000558
0.0001014
0.0000953
0.0000684
19 PFOA concentration, gr/dscf
Cs
0.0000223
0.0000635
0.0000612
0.0000976
0.0000914
0.0000672
20 APFO emissions, Ib/hr
E
0.0018516
0.0054566
0.0043645
0.0080880
0.0073317
0.0054185
21 PFOA emissions, Ib/hr
E
0.0017760
0.0052436
0.0047871
0.0077857
0.0070354
0.0053256
Page 77 of 126
DEQ-CFW 00085686

APPENDIX D - Field Data
Page 78 of 126
DEQ-CFW 00085687

VIM-
0
N
/a5o
/O56
Mull
to anon
01y rator
(Tate
Run No. /
Sample Box No. -?
Meter Box No. - 5-
Meter H a
C Factor -
Punt Tube Coelliclent Cp 4 f�
Schematic of Stack Crass Section
RAMCON Environmental Corporation
Im der
SilicaGel
Ambient TemperatureBarometric
Pressure q yG
iDifference
�p
Assumed Moisture, %
Probe tengllt, m (ft) li
D U
Robe Heate'Selting.4d.' -w.� L/00
7,.3
Nozzle Idendfiation No.
Avg. Calibrated Nozzle Dia., (in.) 444,094—
(
Leak Rate, mrlmin. (dm) . d / , ''
OVA 4
Static Pressure, mm Hg On. ft tJ. 3
Filter No. /3.4 5 - /
r,v�,A cvl • i
��� Tor
/,3L
Source Name: = 5 /'),,•
Tmverse
Pow
No.
Sampling
Time
(a) min.
Vacuum
hL Hg
stack
Temperature
(rs)'F
Velocity
Head (Ps}
in H2O
Pressure Diff.
Orf. Meter
In H2O
Gas Sample
Volume, fP
Gas Sample Temperature at
Dry Gas Meter 'F
Filter Holder
Temperature
•F
Probe
Filter
•F
lad
lmpbger
'F
Inlet
Outlet
v
.?
. 7C
G 3. o
D
--•��! -
ti �
9�
!Q
' 3
/. G'
. i'
S '
8
a. 37
, 33
G .a -
3V
yf
18
SC
b
70
3,
$
e, '/
I?e
s-
f
v
fl b
O, 3 /
Z,
C
C
f/
/oa
/
Fla
O .
7.� s'
(j.3`/
,7./ Ff
%3j.77S
fe,
t' \l,wMS\18-00001.NED
AH - 846.72 (DO (Cp)2 (1-8wo)2 AN a Md Tam ft &P
Ms Ts Prn-

RIIMCON enimiom test lob tixN, t ont Gate
%ration
eta
7el(iJrs
Traverse
Sampling
stack
Velocity
Pressure Diff.
Gas Sample Temperature at
Fiber Holder
Probe
Lad
Pain*
Time
VACun1
Temperature
Head (Ps)
Orf. Meter
Gas Sample
Dry Gas Meter OF
Temperature
Filter
Irryirrder
Na
(e)Min,
in. Hg
(Ts)OF
in HZO
in HZO
Volume, W
Inlet
Outlet
Of
OF
•F
32
76*/.
5F7
9�
Ica
F7
7>7.
-9
s Yv
. b-
190
, / 3
7b . !/ 5
se"
'S
as
7 g Y 7
9 fr
5-7
.7 le
3
0, -el
SO 3
.19
a. 33
5-eto
1a
s-
30
y
v. 3 2
� `Y,
v- 7
,?,•1 S
o�
�6.Ofl
^-v-f -
, v
r8•b
S3,�s
MA T'Et
AH — *t46J2 (Dr1)'t (Cp)2 (14;wo)2 �H a mg-t
PC AP
F-'Vtxms\1 A-00001.NFD

n
/I/`/.Z
b
0
N
A014)
i7 30
I
n
n
I
0
0
0
w
ch
rn
m
0
t`ti15t 21
()IrtYak�r .il>
mi. —Kly C
Run No.
sample Box No.
Meter Box No. ,*f� 4 .
Melfr H a
C f actor
Pilot Tube Coefficient Cp 4, k9-
RAMCON Environmental Corooration
scnematK: 91 sraoK crass se=n
Source Name: 13 -e -- 5
lmpkV-
Volume,
Silica Gel
Weight' g
Ambient Temperature 9<�
!!t
Barometric Pressure J% PO
Assumed Moisture, %Probe lengd+, m #10 'i r
b
8,41- 8
Probe Heater Setting A, 4 �A,,i ;/o" Difference
Nozzle klenlitiation No.
Avg. Calibrated Nozzle Dia., (in.)
Leak Rate, tni/min. (cfm) D. Pow
Static Presstm, mm Hg On. Hg) s .7
Filter No. /3',L S - 7
Fn� $V j -7
* ;r G '? y
Traverse
row
No.
Sampling
Tune
(N min.
vacuum
in. Hg
Stack
Temperature
(1-s) OF
Velocity
Head (P,)
in H2O
Pressure DIf. .
OrE Meter
In H2O
Gas Sample
Voles' fti
Gas Sample Temperature et
Dry Gas Meter OF
Filter Holder
Temperature
OF
Probe
Filter
OF
Last
Impi'iger
OF
Inks
Outlet
'Cr
��
0.3
% 5�
b%30.
0IL9<
.8`t
93 ,v s"
/03
/os-
/05-
/o -5—
/aS—
S
*70,
Ms—
Sr/
7
c,
78, "/.7
7v
G. a
bo
l
3
Z.
y 70
70
G0
78
0. Y5,—
00.
&"
/ate
7
//. s-
y
o -
/0 s-
•74,
8- 3
S'
s
a S
�t1J"
�✓i'
3
/`/d
0. z�S-
s'0 . -
/05-
T:U'ormsU a-0000 t .NED
AH — 846.72 (Dri)4 (Cp)2 (1-8wo)2 AH a Md Trr Ps AP
Ms Ts Pm•

0
0
n
n
I�
0
O
O
00
gWCQN erne nom test io8
ram. +cant Date
f/
tocatiow
Sampiin6
Stack
Velocity
Prenure Diff.
Gas Sample Temperature at
Filter Holder
Pratt
l.ad
E
Time
Vaewm
Temperature
Head (Ps)
Orf. Meter
Gas Sample
D
Gar Meter 'F
Temperature
Filter
lmpkwf
(e)min.
M• HE
(T,) OF
in H2O
in H2O
Voiame,it'
idea
Outkt
OF
OF
OF
`l
/,6,0
er 7
e. 47
1, 3 5
!s y. s Dr
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AH 846.72 (D-04 (CP)2 (14*0)T AH.8 1A � Ap
Flher Holder
Probe
lad
Temperature
Filter
lmpho"
.F
'F
-F
�r
y'
5-3
5.3
9�i
y�i
s 3

I4j-I IMj/�•�I
STACS ISOKINETIC SAMPLING FIELD DATA SHEET
tI30
t4
..
C
Traverse.
Point
Number
Orifice
Press.
Stack
Temp
Probe
Temp
JL(F)
Fifte
Temp
(F)
Impinger
Temp
Dry Gas Meter
�_ Temp.
Vacuum
H
�®
Qom.
ir7sT���S'����F�li%��lC��Ei,��i'�
�■irme�r���r��r����c�v�
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.. Point
7 Ul
hn
s5 t f
DEQ-CFW 00085708

$TACS ISOKINETIC SAMPLING FIELD DATA SHEET
S ! � -07_
_
r� .A
- .-
•
•. ..9
MA
�W-�
FA F-w-WA I VA
Inus -verse�.
Point Number
•
•
•
Probe
'
�®
i66i��
EWAr1.fa��E
4r�
��r�r,�n��a�����c����■©ram
■r.�r�r��r�r��c���c���©ram
rs�■r.,
�:
r�
VA ,
®•;
IQ:�I�'��'�.'/fil�iiF�l�'i�
►�l=!!!tom
�r��a�r�r��,��r�r�n■�c��r�v�r.�
■�s�a�r��►�r�ra�
;
�c��r�so
� � i����������
©
.. -.Ws
-. ..
",Note:
Nearest upstream disturbance or exit must be 2 duct diameters
away to use 6 points per traverse.
rine
�5 101Cko
W'Ay
DEQ-CFW 00085709

STACS ISOKINETIC SAMPLING FIELD DATA SHEET
-.
Number
- ..
..
-ir
Vacuum
• •
ME Uto
Ogg "ON
Wi
" ,
W-1212
�Mwam-�
W�NEA,=F��
OWN
��
'a
• •
f�3101WOMMEMii`�t7�
iA
MRM
.
�Mmffimmw(•_f�EWZ-=
E 2WA�s�i���
of
���i
� i
�
����ri
�i■
ire©�5tTotal
Traverse Point
Note: Nearest upstream disturbance or exit must be 2 duct diameters
1 CLS. 1V1 Vi t<V
DEQ-CFW 00085710

STACS ISOKINETIC SAMPLING FIELD DATA SHEET
MMW
-..
r
..
M.
Leak Check:
-.
Number
Reading
Vrri
OrificeFinal
Press.
Probe
ZO,Wm.....:I
dam
' M
• e
Np_M
KAMw=
KrAMO
INMffM
Z
W=
' "
E
M%0`11'w�_
rumd
©
,.
-RY.
r "WAM
ar:=s�MEWaOMEWMIU�w�
®s
otal TraversePoint
rttyc IV/ u, ,/-v
DEQ-CFW 00085711

STACS ISOKINETIC SAMPLING FIELD DATA SHEET
n
dot
02
�
GIIL•1
• rStock
g
Traverse
Point
Number
no
Orifice
"112
Stack
1�
(F)_][
Probe
(F) J_
I
(F)
Dry Gas Meter
vacuum
��NZAMRUWR
NOW"
•
rim• i
�
f �
�/���Q��_�
m
91"i
�WW�="N
1:2
mvm�=
t�!
Z1�it L0
790ME
�-WJWWA
M�s
E'�'':�Q�1iJlli��i
�1►1���l�if,�f�SE���A�©
��-f
JWA
Point
Note: Nearest upstream disturbance or exit must be 2 duct diameters
away to use 6 points per traverse.
rage lUJ 01 1G0
DEQ-CFW 00085712

e
Obi
09�
a101
rp5'f
m
p
C�
n
Io
0
O
tb
ch
v
MIIA
to allon
eat+erawr
i)ate
BPI-
RM
Sample Box No.
Meter Box No.
Meter H Q
C ('actor
PiMrt Tube Coefficient Cp
Lem.A_— eiae-d
RAMCON Environmental Corporation
C..►,.....w. ,.r C1�It f`mew Swclten
Cnfsrwe 11j"M a- Z C
Slika Gel
Wefg11(, g
AmblentTemperature Zi
Barometric Pressure
Assumed Molsture, % ,� ZProbe
MDifference,�gi
length, m (h1
Probe Heater 5edh►g %y�
4�3 s
Nozzle Identification No. ---���
Avg. Calibrated Nozzle Dia., (in.)�
teak Rate, mlimin. (c(m) Do
�/
Static Pressure, men Hg On. VW
Filter No.
ff
�y
fk I
f, RF � (9 ,
AAIA-L 511:Ci
1
i
Velocity
In a
1
•
r
Ternimature
•
mum
�r��©E��r�
•
r�rr
_
r�r
�r
� 1,rr�r
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•
-
rrrrrrrrt
rrrom
E
rr �KM
■�'
r.
�•f_�r���
E
iG�
`
KN•
�rrr
r�■rr
+�
r�rrEMM
1':V orms\1 E•OOOOI .t11:q
AH — 846.72 0614 (Cp)2 (1-8")2 AH a --"'A Tm Ps pp
Ms Ts Pm -
le
W

m
p
n
I
0
0
0
00
rr
v
f linrmA!A-0000i.1'E0
5
Vacumn
in. HS
Stack
Temperature
(T,) •F
Velocity
Head (P,)
in HZO
Prenure Diff-
Orl. Meter
in HZO
Gar Sanp1e
Volume, W
.t53
09
g
VVI
LZ
S
gG
•l
1?; '76
67
.17
120. �'
Gar Sample Temperature at
Filter Holder
Probe
Lad
Dry Gas Meter'F
Temperature
filter
WON@ -
Inlet
Outlet
•F
•F
'F
i
1�A
AIA
Cod
AH — B4b.T2 ((i�l't (Gp1i (1 � �H a ilk M El 4P
Ms is Prri•

0
M
p
n
I�
0
0
0
w
ch
14
rim,A- �
tcx anon
()prralor
Date
Run No.
Sample Box No.
Meter Box No.
MAPS H
C Factor O
Mot Tube Coefficient Cp
lJ�$
o
i-4
Igo,
i -V'otms\18-OOOOt.tdE4
SCnemeno or SLACK Loross oactouR
dur- ame:
RAMCON Environmental Corporation
I
Ambient Temperature r"
Barometric Pressure -
Assumed Moisture, %
Probe lengh m (it)
Probe Heater Setting
Nozzle Identification No.
Avg. Calibrated Nozzle Dia., (in.)
leak Rate, Wimin. (0m)
Static Pressure, mm Hg On. HO
Fllter No.
S$R U5.y
AH - 846.72 (Di)4 (Cp)2 (1-8wo)2 Ali a Md Am- -ft AP
Ms Ts Pm -
Silks Gel
WeW4 g
Lad
impingcr
'F
cn . J

. RAMCt7N rntission� tesE lag s)xet, carte, T1ite
l otaticyn
t ett Nd
. . . . .
Traverse
S"fing
Stack
Velocity
PrMure [)if(.
Gar Sample Temperature at
Fiber Holder
Probe
Last
Point
Time
vacuum
Temperature
Head (Pj)
Orf. Meter
Gas Sample
Dry
Go Meter'F
Temperature
F'ba
tfo
(e) min.
in. Hg
(Ts)'F
in H2O
in HZO
volume, fts
Inlet
Outlet
'F
'F
'F
, ola
3
7S
N40
f sr,Z,
(:a
'Z
-
3
Y .7
r
?0
1147
-1 r
1
S i
b G3
�?
r9r';
zip. z-
EZ,
7
-4 2
252.
(-?q?
10
ZZG
'T
973
. !
ova
i
Z
b
3
I.OL
of-
to f-
4V yr"�4�
nH — 846.72 (1:)11)4 (Cp)2 (fd3we)2 AH a MsAP
f ATorms\lA.000OI.NED

b
co
co
0
GC
0
N
n
I�
0
0
O
00
ch
v
Schematio of Stack Gross Section
t'tanl t,
i.oc ation
(),wator
Dale ti t 17--1 i V a
Run No. 22
SanjAe Box No. AZ
Meter Box No.
Meter H a
C ractor _ 2-
i,irel cube Coefficient Cp
f: - �.
KAMCON Environmental Corporation
? f)Otl2. �a
Ambleni Temperature
Barometric Pressure '
Assumed Moisture,
Probe Length, m (1)
Probe Heater Setting
Nozzle Identification No.
Avg. Calibrated Nozzle Dia., (in.)
Leak Rate, ms/rein. (cfm)
Static Pressure, mm.Hj On. Hg)
Filter No.
ici6 t,
f .
velocity
_
Pressure Diff. �1
In H-PO
In H20
51
wrm
AH — 846.72 (Drt)4 (Cp)2 (I-Swo)2 AH a —MA Trr Ps ap
Ms Ts Pm•

md
at; — 846.72 OA)4 (CPT tla"*)l QH a , eP
Ms is Prn•
i 1Fc,rms\18-00001.NE()

APPENDIX E - Calibration Data
Page 112 of 126
DEQ-CFW 00085721

Themocouple Calibration
Thermocouple No. ✓ / 3
Date l �J�-(( Calibrated By
Barometric Pressure, "Hg . O Ambient Temperature, (°F)
Calibration
System Used
Ref. Digital
Thermometer &
Thermocouple
I.)- Nos.
Reference
Thermocouple
Temperature
(Tr OF)
Test
Digital
Thermometer
I.D. No.
Test
Thermocouple
Temperature
(Tt °F)
Temperature
Diff., %
(Allowable:
< 1.551.)
ICE
BATH
BOILING
WATER
BOILING
OIL
Tr -Tt
Temperature Difference =---------- * 100
Tr + 460
Page 113 of 126
DEQ-CFW 00085722

Themocouple Calibration
Thermocouple No.
Ci
Date '� � Calibrated By
Barometric Pressure, "Hg Ito, y�z Ambient Temperature, (OF) 2 F
Calibration
System Used
Ref. Digital
Thermometer &
Thermocouple
I.D. Nos.
Reference
Thermocouple
Temperature
(Tr OF)
Test
Digital
Thermometer
I.D. No.
Test
Thermocouple
Temperature
(Tt OF)
Temperature
Diff., %
(Allowable:
< 1.50/0)
ICE
BATH
,112L
Oo
BOILING
WATER
!
a
BOILING
OIL
Tr - Tt
Temperature Difference =---------' 100
Tr + 460
Page 114 of 126
DEQ-CFW 00085723

Themocouple Calibration
Thermocouple No./ if
Date . / Calibrated By
Barometric Pressure, "Hg Ambient Temperature, (°F) _
Calibration
System Used
Ref. Digital
Thermometer &
Thermocouple
I.D. Nos.
Reference
Thermocouple
Temperature
(Tr OF)
Test
Digital
Thermometer
I.D. No.
Test
Thermocouple
Temperature
(Tt `F)
Temperature
Diff., %
(Allowable:
< 1.5%)
ICE
BATH
�
BOILING
WATER
BOILING
OIL
Tr - Tt
Temperature Difference =--------- • 100
Tr + 460
Page 115 of 126
DEQ-CFW 00085724

3�
nrt s rtmT tvK
t.N a lLl 1..) Ip 1; • t.] rt PR b.l
Sl11rRIK a[a[
1{) 1Kr0111tri OpTa FIYIIYI IirOr-atll[ Sfr1Mr10■,
Lrrlla a
Slwtla HOK ,STATIC ►KSSIII[
•Orrllla
J � I � IrrKr Fa.. r
"I"
MULE Oldta
(1) IIK nr*.. Tf PKC IIMT IIK ICt /■Ttlfllla WIW
"M O"I i A IPIT rrpltuAirL Itt rYLr
rllr I. 1 .40 FM IIK MULE FORT nAK
KWI l01—Ia U—
IKIr101 rK KllwrnlK
s, Fall tALctuna r
rrew. 1.1
Type S Pitot Tube Inspection
�t•• Lee.w«
F
Lou—
.. r1rA 1 •,M ,wl •,Iwf NII
rtrrr. 1.1 Mgrtr.l N.r..awpl. &W rr.►. PI.-W J--t'
L1rtt.rNN: 0, N- 1.41 A 2.93 a 11/le rrf
+et/l FLAK
_ an
Yy„«
10■{IT90t, . rA I.N 0{• 1 A.tf :,
" Atte I — -- I 11, • It
1, d •f, < f.ef Q 4SIa lLAtr
Wu I■l 'lyf I..) u)
M
1
I
KW{ NwItKIK LIAR t,LL{uurVICKAT
1K K+n.uir r. Tar ta r
I[twl Iy1tRrK Lt'/IL Menlo
10 KRMI■la h r.A 1r
CsT�
■eMI IeKlarr■t LIAR
M111wl 1r■ KT{Iwl■la L;•�J
rre„r. 1.1 I�leeri m o 41—osl.re lw...r.w.rt.
T■YirTat i
I •
nK JAI$
p) w rtd
ra'p.[ 1.f. /t.r.i17 e■0■tsret.f 77M f 01[r■ "/w. ■►■.r Lr
vi-, l- ;=1Me.01.w HrW�talar en t[w+.s..
ui■, 1►1 ew �i. r te. l.e.. �+r.11.L t. 1rAy14J1a.L
utrr 1<1 ■iN rL.•+r NN l.ve s NMar teMt► +M wnrlLw
mlmlbnt. "Ne►1- — rrt d WO
.■llr •[ f,N r7 4 .ui¢d Tr �ltr■ E■M■ rN■tL,KUK tilr
w7.
Level?
Obstructions?
Damaged?
-100 <a( <+100
.10' < a2 < +10°
-50 < P( < +50
-50 < D2 <+50
Y
9
A
z < 0.125" (z = A sin Y)
w < 0.03125" (w = A sin 8)
�,
0.413"SP„�0.591"
0.413" <_ PB � 0.591"
p
0.1875" 5 Dr Z 0.375"
See 40 CFR 60 Vol. 42 No. 160 EPA Method 2. Verify the minimum 2-inch setback of the thermocouple and the minimum
'/.-inch separation between the pitot tube and the nozzle as shown at the top of this page.
Comments:
I Certify that pitot tube number
applicable design features and is hereby
Was Pitot Tube damaged during test?
Signature:
meets or exceeAkll specifications, criteria and/or
,ned a pitot
Signature _
Date
Post Test Inspection
Yes --4— No
Date:
Page 116 of 126
DEQ-CFW 00085725

Type S Pitot Tube Inspection
T1Y•[ t "M Tw[ 1
trl.w to I U. I.. I itr D.- I.. c.11/l I..J
S.gRIK gull
t.) KIM 11M fgglw. AW" rum- Int 1tr wrid.
fiAiltw w
057�j=!m
OvLINK
114bUlw
p1 SIDE ILV. TO vRYl.f 71IDf T{tl[ Ipl IAIEpQii hlw
�S R 0/111K KNI[ 07 nt�ief TYI[�EA•YE 1[IlttAt
q1S d ttAaSTA[M ip III[ qAl[ [LI[S' [NtE
.Wt IwIGTIw Lull 1
NSII It• rot K'tMI— '
g. , ""ZIK It
Lw.w L.t (mnt111..41
J
I
wTY! IwIEatIK Ltli RtaRlo
/ea KTTMI.Iw T. iqv WLIAATIK a
I
tttrL IwIUTIw
rw ![nKInK t
CZ::ffi
neat[ Iw1GTIK toll
nitnw nt "It. -Mot
vLtva I.t fooa0.woo of 41r 1.n Yaa.r. t.
X Ica t..l�
w_Or. wi I I
i Iw[cnr s' IwanaM nt
w .I.w r•I. r�.
.-_
v[gm, a.7 "q"r" alr.+..wglA W w.►. v!•t.wwa to vnRla
Lpt.rl..rm+ Dt wLaw• t.it Ad t.7S o t7/U +ne
.Slot 'tM
LOKit-0Ilps� A _ vA
nK Ylt t —
�-S••
en:
'A'vt
D.fs d $.SIR PLW
`t
twit 1-1 wt I..) to)
,
TAIASRI6( � I •
tcJ nit
�'•DRt1K
ilA.[Y
4.) w na
►i i.f. )rcy.Tt) ewrttget.d L}Dg DimE eiw.. ADnD 1A1
j. W w+ [..'g .DCAEAg taslw McMDelwia t. tttmv.Lst
.. l►) t.v �iwt [Au aywlSM viart µY.11gl Y irgitwAWl
Aattl (cl Uec .it++ Md l.gt L wwl l..gt► AM oo-ra .
o1— of " .t..w Li" w den. SUAtt m tld t".
wow .[ D.w ..r a u.[gmd ce rive t[wA w..ta+weAa trt.
w[.
Level?
Obstructions?
Damaged?
-10° < a, <+10D
,2
-10' < aZ < +10°
.50 < P, < +50
2
-5° < Pz <+5D
i
Y
e
3
A
/
z < 0. 125" (z = A sin y)
w < 0.03125" (w = A sin 0)
;
0.413" 5 P, > 0.591"
v
0.413" 5 Pa 2: 0.591"KO
0.1875" 5 Dr Z 0.375"
See 40 CFR 60 Vol. 42 No. 160 EPA Method 2. Verify the minimum 2-inch setback of the thermocouple and the minimum
3/.-inch separation between the pitot tube and the nozzle as shown at the top of this page.
Comments:
I Certify that pitot tube number
applicable design features and is hereby
Was Pitot Tube damaged during test?
Signature:
i meets or
;ned a pitot tube ca�i
Signature
Post Test Inspection
Yes _� No
Date:
Page 117 of 126
criteria and/or
DEQ-CFW 00085726

311
�ci
•.) I.r 0 . 1.; a (InS-PII.t
1.) ■"" VIEW, o"IR -MIM■ /lt■r• Ing L()A411CM.
S1Y►tIM t0
SM{I.■ MOM - , LTATI�PK=AMC
Im
11■Aer nn..._
prl-IM
WIRE
Type S Pitot Tube Inspection
r.l I 1
[�()�'-f{j•. ■,p '�n.t t nut n. t nwr :w
`nw. r. r.as�t r1li
1
IIPY• r.J ..p.rtrM WatOCOv►l• W PavN ►ivn.eva !a ynMt
lv..r[-rrN: p, •. t.-.. ■.Il W t.T3 a. IS/{f .nd
A-slO[ MAM
TOM
lTUDEAllItt1�� 1
Tl■L Ns { � I■ h - h
nu.srvar
iM■ NIS
10
1 LR.Ii
• nAcs
(.) N Tsar
n9vt 1.3; SL-W,17 tOrytLKCN SYN ■ ►lt.t
1.1 -II v e.r: JM eP•ni.{ Pla1Me P--�L.r N trwrsns
u! ! 1.1 te► �Iwr: L•e• eya1M Plot ■-L+11•L N 1.g1,rP1[.+1
.II., le) Li" vi— Nth t.Pt -J •�y ltttyeA Ad .rt.rttlf•I
is IMIA"t. MM■ •{•-•d [[a- h.th .1d.t. ■.NSIIt p-elciPWt
glaMt L ■.N MJ it u.i*.•d IN ►itet tMt.- N-.tsucW this
-y.
Level?
Obstructions?
Damaged?
-100 < a, < +100
-100 < a2 <+100
T,Z
.50 < al <+50
-50 < Pz < +50
Y
9
A
z < 0.125" (z = A sin y)
/
w < 0.03125" (w = A sin 0)
Q
0.413" S P,l >_ 0.591"
0.413"5PB20.591"
0.1875" <_ Dr >_ 0.375"
See 40 CFR 60 Vol. 42 No. 160 EPA Method 2. Verify the minimum 2-inch setback of the thermocouple and the minimum
1/4-inch separation between the pitot tube and the nozzle as shown at the top of this page.
Comments:
I Certify that pitot tube number ,/�/� meets or exce all pecificat ions, criteria and/or
applicable design features and is hereby signasned pitot tube catibra i f or of 0.84.
Signature
Post Test Inspection
Was Pitot Tube damaged during test? Yes_ No
Signature: Date:
Page 118 of 126
DEQ-CFW 00085727

RAMCON Environmental Temperature Di play Calibration
Meter Box: 4iLk
Date: 4 Calibrated By:
Temperature Settings
M04M.0
=OEM
U'
111!--�Mtulfl
r�� 7g,
k90
P
F 7,-1,11,
,.(aqf
R�"\'w�mzurd
Y^t^£•�l.ni..�a
7�xyxd

RANICON Environmental
Temperature Display Calibration
Meter Box:
Date: - 62z _—Zs-� - Calibrated By: Xk
Temperature Settinas
��
t.
'"i }��,.. �'•�"�
�i+ti,f4lTaa
�"�•✓}.w:P+
..unA�i:r1...
.a ai 3.e�+M
�,.�.w
!'�' �'�tf
L���
SALTEK52SP
CERT,IFICATEOFCALIBiA�6�'.,z-�',�-'-
Thisis to cerffy thatyourAftek Unithas been- calibrated using
are traceable ft the liationaL[nsftteratstandertfsanciTechngf6iiwitft!i>:iC��.,It -'qt(e`
NIST Calibration ServIces. Actual records portairffngto these scmde
available for examination
CerRecommend imis
tifi9&by.AlhekbWU&trfwCbrw ffecartbria6
Wade( Niumber— 2 2 — k 2 t c c f reewrl CS
Calibration Due -Z
2
1084450
Serial Numb
CC BECEAPATION; OF: C0146I lly,'t
Tfiwibowsignatur F, i;Corp-36Vantag*PbrritUrNmRocfwsur>.1&- 14674*6
Declares that the equipment specified complies with standards ENMIXT-isr4 tN5dWt.
The product compries with Ow assentilat roquirements, of therEM Cr)
X

Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/19/2006 Orifice ID Y Calibration
Delta H @ Cal.
Vac
Meter Box: A2 48 pass
pass
pass
Technician: MAD 73 pass
pass
pass
40 pass
pass
pass
55 pass
pass
pass
63 pass
pass
pass
PART 1: Orifice Calibration
Calibration Orifice Set:
D1 Critical
Vacuum:
13.9
Barometric Pressure
( in. Hg ):
29.950
Collected Data
Initial
Final Meter
Init Final
[nit Final
Amb
Run
K
Orifice
Run
Delta H
Meter
Volume
Volume (
Meter Meter
Temp Temp
Amb
Temp Temp
Time
Factor
Vac
ID
#
(
cu ft )
mnsec
i
cult
F F
F F
48
1
0.65
13.925
22.150
66.00 66.00
60.00 61.00
18
0
0.3485
20
48
2
0.65
22.150
26.257
66.00 66.00
61.00 61.00
9
0
0.3485
20
73
1
3.70
29.913
44.783
57.00 63.00
57.00 58.00
14
0
0.815
15
73
2
3.70
44.783
50.648
61.00 64.00
58.00 57.00
5
30
0.815
15
40
1
0.30
50.648
56.733
62.00 60.00
58.00 59.00
19
30
0.2396
22
40
2
0.30
56.733
62.345
60.00 60.00
59.00 60.00
18
0
0.2396
22
55
1
1.15
62.865
72.440
60.00 63.00
60.00 59.00
16
0
0.4606
19
55
2
1.15
72.440
79.034
62.00 64.00
59.00 60.00
11
0
0.4606
19
63
1
1.95
79.034
92.198
63.00 67.00
59.00 60.00
17
0
0.5945
17
63
2
1.95
92.198
103.068
66.00 67.00
60.00 61.00
14
0
0.59
17
Calculated Data
Corrected
Orifice
Run
Meter
Meter
Meter
Ave Meter Ave Amb
Delta H
ID
#
Volume
Volume
Volume
Temp (F) Temp (F)
Y
@
(cu ft)
( std cu ft)
(stdcuft)
48
1
8.225
8.27443
8.23496
66 60.5
0.9952
1.7608
48
2
4.107
4.13168
4.11551
66 61
0.9961
1.7625
AVE
0.9957
1.7617
73
1
14.87
15.24510
15.02198
60 57.5
0.9854
1.8709
73
2
5.865
5.98418
5.90149
62.5 57.5
0.9862
1.8619
AVE
0.9858
1.8664
40
1
6.085
6.17501
6.14531
61 58.5
0.9952
1.7262
40
2
5.612
5.70597
5.66713
60 59.5
0.9932
1.7328
AVE
0.9942
1.7295
55
1
9.575
9.72757
9.68385
61.5 59.5
0.9955
1.7998
55
2
6.594
6.67986
6.65765
63 59.5
0.9967
1.7946
AVE
0.9961
1.7972
63
1
13.164
13.31062
13.28021
65 59.5
0.9977
1.8268
63
2
10.87
10.95975
10.92613
66.5 60.5
0.9969
1.8251
AVE
0.9973
1.8260
Average for All Runs 1
0.9938 1
1.7962
Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/20/2006
Meter Box: A2
Technician: MAD
PART 2: Thermocouple Calibration
T/C Calibrator Make: Tegam T/C Calibrator Model: 840A
Calibrator
Meter
Error
( Allowable
Output ( F)
ReaFding
F)
Error ( F)
Result
0.0
2
2
9.24
pass
32.0
33
1
9.88
pass
70.0
72
2
10.64
pass
100.0
103
3
11.24
pass
200.0
204
4
13.24
pass
500.0
504
4
19.24
pass
1200.0
1203
3
33.24
pass
1995.0
1999
4
49.24
pass
Page 121 of 126
DEQ-CFW 00085730

Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/8/2006 Orifice ID
Y Calibration
Delta H @ Cal.
Vac
Meter Box: A4 40
pass
pass
pass
Technician: MAD 73
pass
pass
pass
48
pass
pass
pass
55
pass
pass
pass
63
pass
pass
pass
PART 1:
Orifice Calibration
Calibration
Orifice Set:
D1
Critical
Vacuum:
13.9
Barometric Pressure ( in. Hg ):
29.760
Collected Data
Initial Meter
Final Meter
Init Final
Init Final
Run
Orifice
Run
Delta H
Volume (
Volume (
Meter Meter
Amb Amb
Time
K
Vac
ID
#
cu ft)
cu ft)
Temp Temp
Temp Temp
min1sec
Factor
F F
F F
40
1
0.29
45.347
60.654
69.00 68.00
67.00 66.00
49
0
0.2396
25
40
2
0.29
60.654
70.029
68.00 68.00
66.00 69.00
30
0
0.2396
25
73
1
3.40
70.029
79.418
69.00 72.00
69.00 66.00
9
0
0.815
19
73
2
3.40
79.418
86.744
72.00 73.00
66.00 66.00
7
0
0.815
19
48
1
0.63
86.826
93.102
73.00 70.00
66.00 66.00
14
0
0.3485
24
48
2
0.63
93.102
97.600
70.00 69.00
66.00 65.00
10
0
10.3485
24
55
1
1.10
97.600
105.286
69.00 68.00
65.00 65.00
13
0
0.4606
23
55
2
1.10
105.286
110.603
65.00 68.00
65.00 65.00
9
0
0.46061
23
63
1
1.85
110.603
116.699
68.00 69.00
65.00 65.00
8
0
0.5945
20
63
2
1.85
116.699
122.028
69.00 69.00
65.00 63.00
7
0
0.5945
20
Calculated Data
Corrected
Orifice
Run
Meter
Meter
Meter
Ave Meter
Ave Amb
Delta H
ID
#
Volume
Volume
Volume
Temp (F)
Temp (F)
Y
@
(cu ft)
(std cu ft)
(stdcuit)
40
1
15.307
15.21555
15.22708
68.5
66.5
1.0008
1.6810
40
2
9.375
9.32782
9.31386
68
67.5
0.9985
1.6857
AVE
0.9996
1.6833
73
1
9.389
9.36911
9.50434
70.5
67.5
1.0144
1.7263
73
2
7.326
7.28303
7.40279
72.5
66
1.0164
1.7149
AVE
1.0154
1.7206
48
1
6.276
6.20850
6.33098
71.5
66
1.0197
1.7176
48
2
4.498
4.46643
4.52428
69.5
65.5
1.0130
1.7225
AVE
1.0163
1.7200
55
1
7.686
7.65536
7.77715
68.5
65
1.0159
1.7273
55
2
5.317
5.31592
5.38418
66.5
65
1.0128
1.7339
AVE
1.0144
1.7306
63
1
6.096
6.08292
6.17725
68.5
65
1.0155
1.7502
63
2
5.329
5.31254
5.41025
69
64
1.0184
1.7453
AVE
1.0169
1.7478
Average for All Runs 1
1.0125
1.7205
Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/8/2006
Meter Box: A4
Technician: MAD
PART 2: Thermocouple Calibration
T/C Calibrator Make: Tegam T/C Calibrator Model: 840A
Calibrator
Meter
Error
( Allowable
Result
Output ( F )
Reading
( F)
Error( F)
0.0
2
2
9.24
pass
32.0
34
2
9.88
pass
70.0
73
3
10.64
pass
100.0
103
3
11.24
pass
200.0
202
2
13.24
pass
500.0
502
2
19.24
pass
1200.0
1204
4
33.24
pass
1995.0
1997
2
49.24
pass
Page 122 of 126
DEQ-CFW 00085731

Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/3/2006 Orifice ID Y Calibration
Delta H @ Cal.
Vac
Meter Box: A5 73 pass
pass
pass
Technician: MAD 40 pass
pass
pass
48 pass
pass
pass
55 pass
pass
pass
63 pass
pass
Dass
PART 1:
Orifice Calibration
Calibration
Orifice Set:
D1
Critical
Vacuum:
13.9
Barometric Pressure ( in. Hg ):
29.970
Collected Data
Initial
Final Meter
Init Final
Init Final
Run
Orifice
Run
Delta H
Meter
Volume (
Meter Meter
Amb Amb
Time
K
Vac
ID
#
Volume (
cu ft)
Temp Temp
Temp Temp
min sec
Factor
cult
F F
F F
73
1
3.50
47.199
57.769
62.00 62.00
59.00 58.00
10
0
0.8150
17
73
2
3.50
57.769
65.175
62.00 62.00
58.00 58.00
7
0
0.8150
17
40
1
0.29
65.175
71.361
62.00 62.00
58.00 58.00
20
0
0.2396
24
40
2
0.29
71.361
77.549
62.00 60.00
58.00 59.00
20
0
0.2396
24
48
1
0.63
77.549
86.994
60.00 60.00
60.00 57.00
21
0
0.3458
23
48
2
0.63
86.994
95.193
60.00 60.00
57.00 60.00
18
0
0.3458
23
55
1
1.15
103.380
111.693
60.00 60.00
57.00 57.00
14
0
0.4606
22
55
2
1.15
112.306
117.054
60.00 59.00
55.00 55.00
8
0
0.45061
22
63
1
1.90
117.054
123.925
59.00 58.00
55.00 55.00
9
0
0.5945
20
63
2
1.90
123.925
130.010
58.00 58.00
55.00 55.00
8
0
0.5945
20
Calculated Data
Corrected
Orifice
Run
Meter
Meter
Meter
Ave Meter
Ave Amb
Delta H
ID
#
Volume
Volume
Volume
Temp (F)
Temp (F)
Y
@
(cu ft)
( std cu ft)
(stdcuft)
73
1
10.57
10.79700
10.72679
62
58.5
0.9935
1.7634
73
2
7.406
7.56505
7.51238
62
58
0.9930
1.7617
AVE
0.9933
1.7626
40
1
6.186
6.26951
6.31014
62
58
1.0065
1.6627
40
2
6.188
6.26357
6.30709
61
58.5
1.0037
1.6675
AVE
1.0051
1.6651
48
1
9.445
9.61733
9.55777
60
58.5
0.9938
1.7453
48
2
8.199
8.34860
8,19238
60
58.5
0.9813
1.7453
AVE
0.9875
1.7453
55
1
8.313
8.47546
8.49950
60
57
1.0028
1.7951
55
2
4.748
4.84545
4.76063
59.5
55
0.9825
1.8702
AVE
0.9927
1.8326
63
1
6.871
7.03844
7.06606
58.5
55
1.0039
1.7850
63
2
6.085
6.23930
6.28094
58
55
1.0067
1.7868
AVE
1.0053
1.7859
Average for All Runs
0.9968
1.7583
Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/3/2006
Meter Box: A5
Technician: MAD
PART 2: Thermocouple Calibration
T/C Calibrator Make: Tegam T/C Calibrator Model: 840A
Calibrator
Meter
Error
( Allowable
Output ( F )
ReaFding
F)
Error ( F)
Result
0.0
1
1
9.24
pass
32.0
33
1
9.88
pass
70.0
69
-1
10.64
pass
100.0
101
1
11.24
pass
200.0
202
2
13.24
pass
500.0
502
2
19.24
pass
1200.0
1203
3
33.24
pass
1995.0
1998
3
49.24
pass
Page 123 of 126
DEQ-CFW 00085732

Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/20/2006 Orifice ID Y Calibration
Delta H @ Cal.
Vac
Meter Box: Al 73 pass
pass
pass
Technician: MAD 40 pass
pass
pass
48 pass
pass
pass
55 pass
pass
pass
63 pass
pass
pass
PART 1: Orifice Calibration
Calibration Orifice Set:
D1 Critical
Vacuum:
13.9
Barometric Pressure
(in. Hg ):
29.950
Collected Data
Initial
Final Meter
Init Final
Init Final
Run
Orifice
Run
Delta H
Meter
Volume
(
Meter Meter
Temp Temp
Amb Amb
Temp Temp
Time
K
Factor
Vac
ID
#
(Volume
cu ft)
minjsec
cu ft
F F
F F
73
1
3.50
87.716
99.109
57.00 59.00
59.00 60.00
11
0
0.8150
19
73
2
3.50
99.109
112.583
59.00 65.00
60.00 61.00
13
0
0.8150
19
40
1
0.28
12.583
18.564
62.00 61.00
62.00 61.00
19
30
0.2396
25
40
2
0.28
18.564
25.628
61.00 61.00
61.00 60.00
23
0
0.2396
25
48
1
0.60
25.628
34.992
61.00 62.00
60.00 62.00
21
0
0.3485
24
46
2
0.60
34.992
39.898
162.00 63.00
62.00 62.00
11
0
0.3458
24
55
1
1.10
39.898
46.369
63.00 64.00
63.00 64.00
11
0
0.4606
23
55
2
1.10
46.369
51.668
64.00 65.00
64.00 63.001
9
1 0 10.4606
23
63
1
1.80
51.668
59.263
65.00 67.00
63.00 64.00
10
0 1
0.5945
20
63
2
1.80
59.263
66.091
67.00 68.00
64.00 65.00
9
0
0.59
20
Calculated Data
Corrected
Orifice
Meter
Run
Meter
Volume
Meter
Ave Meter Ave Amb
Y
Delta H
ID
#
Volume
Volume
Temp (F) Temp (F)
@
(cu ft)
(std cu ft)
(std cu ft)
73
1
11.393
11.71978
11.78025
58 59.5
1.0052
1.7817
73
2
13.474
13.75426
13.90873
62 60.5
1.0112
1.7714
AVE
1.0082
1.7766
40
1
5.981
6.06336
6.12761
61.5 61.5
1.0106
1.6187
40
2
7.064
7.16815
7.23438
61 60.5
1.0092
1.6172
AVE
1.0099
1.6179
48
1
9.364
9.50040
9.60285
61.5 61
1.0108
1.6406
48
2
4.906
4.96794
4.98631
62.5 62
1.0037
1.6663
AVE
1.0072
1.6534
55
1
6.471
6.54819
6.63216
63.5 63.5
1.0128
1.7277
55
2
5.299
5.35199
5.42631
64.5 63.5
1.0139
1.7244
AVE
1.0134
1.7261
63
1
7.595
7.66218
7.78198
66 63.5
1.0156
1.6948
63
2
6.828
6.86881
6.99711
67.5 64.5
1.0187
1.6932
AVE
1.0172
1.6940
Average for All Runs
1.0112
1.6936
Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/20/2006
Meter Box: Al
Technician: MAD
PART 2: Thermocouple Calibration
T/C Calibrator Make: Tegam T/C Calibrator Model: 840A
Calibrator
Meter
Error
( Allowable
Output ( F)
ReaFding
F)
Error ( F)
Result
0.0
0
0
9.24
pass
32.0
32
0
9.88
pass
70.0
70
0
10.64
pass
100.0
101
1
11.24
pass
200.0
201
1
13.24
pass
500.0
501
1
19.24
pass
1200.0
1203
3
33.24
pass
1995.0
1997
2
49.24
pass
Page 124 of 126
DEQ-CFW 00085733

Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/20/2006 Orifice ID Y Calibration
Delta H @ Cal.
Vac
Meter Box: A7 73
pass
pass
pass
Technician: MAD 40
pass
pass
pass
48
pass
pass
pass
55
pass
pass
pass
63
pass
pass
Dass
PART 1: Orifice Calibration
Calibration
Orifice Set:
D1 Critical
Vacuum:
13.9
Barometric Pressure ( in. Hg ):
29.990
Collected Data
Initial
Final Meter
Init Final
Init Final
Run
Orifice
Run
Delta H
Meter
Volume
(
Meter Meter
Temp Temp
Amb Amb
Temp Temp
Time
K
Factor
Vac
ID
#
(Volume
cu ft)
min1sec
cu ft
F F
F F
73
1
3.40
8.054
17.568
64.00 64.00
64.00 64.00
9
0
10.8150
17
73
2
3.40
17.568
27.116
64.00 65.00
64.00 65.00
9
0
10.8150
17
40
1
0.27
27.116
32.760
63.00 65.00
63.00 64.00
18
0
0.2396
24
40
2
0.27
32.760
39.341
65.00 64.00
64.00 63.00
21
0
0.2396
24
48
1
0.59
39.341
46.139
64.00 65.00
64.00 63.00
15
0
0.3485
23
48
2
0.59
46.139
54.102
64.00 64.00
63.00 64.00
17
30
0.3485
23
55
1
1.10
54.102
62.182
64.00 65.00
64.00 63.00
13
30
0.4806
22
55
2
1.10
62.182
69.368
64.00 65.00
63.00 64.00
12
0
0.4806
22
63
1
1.80
69.368
74.777
65.00 65.00
64.00 63.00
7
1 0
0.5945
19
63
2
1.80
74.777
80.184
65.00 65.00
64.00 63.001
7
1 0
1 0.59
19
Calculated Data
Corrected
Orifice
Run
Meter
Meter
Meter
Ave Meter Ave Amb
Y
Delta H
ID
#
Volume
Volume
Volume
Temp (F) Temp (F)
@
(cu ft)
(std cu ft)
(stdcuft)
73
1
9.514
9.68528
9.60972
64 64
0.9922
1.7226
73
2
9.548
9.71063
9.60514
64.5 64.5
0.9891
1.7226
AVE
0.9907
1.7226
40
1
5.644
5.70188
5.65298
64 63.5
0.9914
1.5573
40
2
6.581
6.64215
6.59514
64.5 63.5
0.9929
1.5558
AVE
0.9922
1.5565
48
1
6.798
6.86655
6.85192
64.5 63.5
0.9979
1.6095
48
2
7.963
8.05097
7.99390
64 63.5
0.9929
1.6110
AVE
0.9954
1.6102
55
1
8.08
8.17167
8.50424
64.5 63.5
1.0407
1.5818
55
2
7.186
7.26752
7.55933
64.5 63.5
1.0402
1.5818
AVE
1.0404
1.5818
63
1
5.409
5.47451
5.45466
65 63.5
0.9964
1.6958
63
2
5.407
5.47248
5.45466
65 63.5
0.9967
1.6958
AVE
0.9966
1.6958
Average for All Runs
1.0030
1.6334
Source Testing And Consulting Services
Meter Box Calibration
Calibration Date: 1/20/2006
Meter Box: A7
Technician: MAD
PART 2: Thermocouple Calibration
TIC Calibrator Make: Tegam TIC Calibrator Model: 840A
Calibrator
Meter
Error
( Allowable
Output ( F)
ReaFding
F)
Error ( F)
Result
0.0
2
2
9.24
pass
32.0
34
2
9.88
pass
70.0
72
2
10.64
pass
100.0
101
1
11.24
pass
200.0
200
0
13.24
pass
500.0
502
2
19.24
pass
1200.0
1201
1
33.24
pass
1995.0
1987
-8
49.24
pass
Page 125 of 126
DEQ-CFW 00085734

APPENDIX F — Plant Data
Page 126 of 126
DEQ-CFW 00085735