DEQ-CFW_00083445

to
t33
A"!V e u rof i n s
1113 S. HIII S€meat
South Bond, IN 46617 Order#
Eaton Analytical F.1.674,2318247 Batch
Vdt1bU eztpt' pm!cY.S a€ CHAINOCUSTODY RECORD Page'---a..� of.... �
Shaded
area FrsrA axes as
REPORT Tt� SAMPLER f E na8ur� PWS 10 # � S r�TE (sampga srigh) ' PROJECT dL4Ahe � ..
......... ..
Jill®earey - Lab Manager � .... �--_- - «..
235 Govement Canter Dr. # � .. t�A %S SI €CR
mNC
Wilmington NG 23403 �
.. ... .._ ...._,..:.......... .......... .m..
PFC-1,4 Method
°tee m- Wg € ..............POPULA1"16 iEF? LB St URCEWAT€ R � ltiefJe7
.. ......... .......
CAPEFEARPke4-NC Finance COMPLIANCE 638 €ate€
235 Government banter [3r. MONITORING ll7is 135,20d Sxsrtea 4iJatar € a z
Wfminrattrn NC 23403 ..... € 0 £ �
«......_ ...
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LAB plumber COLLECTION �tdL�rsaFt�AtEF� 0 a�
SAMPLING SITE TEST NAME SAMPLE REMARKS « ....
ff� 0
CRATE TIME Are PM fkYES s tli3 a4 �
1 1 {. a ..:: �` ,iS�n eenr y Water Treatment Punt Post PF� 14 Method 53� � € 1 i31e►1 Sw
«::::::: ......... Oeslturra•aresurld «........�.
z `:,ti ion i"i �� lkjl1..._.,.Sweeney Water "Treatment Plant- Flaw PFC14 Method 3� ����€�€� X i CAW Sid€"'.
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EL fe3i HEl "((Siszmtu ,l BATE TIME RECE€VEDBY:(Signetare) DATE TIME LAB RES-MITsru4eo,.s TO RMRN UNUSEUPORTtM.30F TO rue
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RELlpl«t tS€�ED �'Y.(w'sgricture) � BATE E`. � � EMI ill �i 6y.{�Igna.u.a) MATS Tlt�
RELINQUISHED BY:(Signaiure)._._ DATE �., TIME RECEIVED FOR LABORATORY BY: DATE TIME
t101Tl
.: €, UPON cal upan to A
AM Pry �� s PM ,
All"F;I COD s. TURN -AROUND TIME (T`AF 0 - SURCHARGES
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EV1f.E3CP0suRE,WA11ER : RW - Ranh wnllm; (5=r .116ng CI&vs) Ta% ° z S "ke:,rd, RdEidgg' CALL. t:xsn krt hrs�- a hald€ns V ne rF?�5k3dif{�t
SW SURFACE WATER
may ha su8s(�d§ ie sddienstsE rhsrCles.
'.'1"d,P,y,.#. W1d"MR 'w'$RT° : rr.ga 3hsd kd 3xona~a CA3<#r
vrV-WASTE WATER Please edit expedited service net avMIants for all testing
- --- -3..L?-Fi1435 lsstfs m,43 EffsasXiveF3aw 1"t
Sample analysts wili In predlded according la me standard EEAPNamr .Services Terms, which sae ava€€able span requesi, Any ofte rarrrs proposed by Oustrzmer are deemedrRa4ersai etteradlrles and era mjact at unless expressly ag, ae to in edsWrrg by
EEA.

DEQ-CFW 00083446

If you have any questions concerning this report, please do not hesitate to call us at
8{'233-4777.
This report may not be reproduced, except in tu#, without written approval from EEA.
Page 1 of 13
DEQ-CFW 00083447

eurof ins
Eaton Analytical
Revision date: 05/15/2017
DEQ-CFW 00083448

Eaton Analytical
110 South Hill Street
South Bend, IN 46617
Tel: [phone]
F&x: [phone]
1 800 332 4345
Client: Cape Fear Public Utility Authority
Aftn: Jill Deaney
235 Government Center Drive
Wilmington, NC 28403
Report:
Priority:
Statue:
PW8 ID:
393030
Immediate Verbal
Final
NC0465010
EEAEEA Client ID
Method Collected
Collected
Received
I[
_.
Cate t Time
13y;
Date i Time
37333633 -- Sweeney Un#r Plant -post
3733354 Sweon�y1eEer
537 07113/17 0814
Client
07114117 0 :30
ry Plars#-���r
537 07113I17 03:49IienE
0719 3117 03:30
Detailed quantitative results are presented on the following pages. The results presented relate only to the samples provided for
analysis.
We appreciate the opportunity to provide you with this analysis. If you have any questions concerning this report, please dry not
hesitate to call Joseph Mattheie at [phone].
Note: This report may not be reproduced except in full, without written approval from EEA
0711912017
Authorized Signature Title Date
Client Marne: Cape Fear Public Utility Authority
Report #: 393030
Page 1 of 3
Page 3 of 13
DEQ-CFW 00083449

ClientName: Cape Fear Public Utility Authority Report #: 393030
Sampling Point: Sweeney Water Plant -Post PW5 ID; NCO455010
Sampling Point: Sweeney Water Plant -Raw
Analyte ° Analyte
M thod Reg
MRLt
Result
IJnite
ID # Limit
2991-6" N-ethyl Perfluoroactanesu€fenamidoacetic acid (NBFCC
537 -
2.0
< 2.0
ng1L
235 39-=s hi -methyl �er�uerecr to esuffeanarflldearatleacld {N�Ae
537 -
2.0
< 2.0
ng1L
$75 73 5 Perftuorobutanesu4fonlc acid (PFBS)
537 -
2.0
3.7
ngiL
M&76-2 PerfBuorodecanoic acid (PF®A)
537 -
2.0
< 2.0
ng1L
$75-85-9 Perfluorohegtanoic acid (PFHpA)
537 W
2.0
9.0
ngfL
355-46-4 Perfiuorohexanesuifonic acid (PFHxS)
537 -
2.0
6.7
ng1L
307-24 4 PerCluorohexaflcic acid (PFFixA)
537
2.0
54
ng1L
307-55-9 Per€tuaarclaudc acid (PFDoA)
537
2.0
< 2.0
ngfL
376 0 -7 I Pernuoromyris$ic acid (PFTA)
537
2.0
£ 2.0
ng1L
375-95-1 Pe¢0ucrcnonancic acid (PFNA)
5:a7
2.0
< 2.0
ngfL
,. :: .. ......
1763.23-1 Perfluamcdane suffonate (PFOS)
517 -
.4
15
r3git.
:
335 67-1 Perfiu#r# Ear of acid (PFOA} �
537 �
2.0 �
9.2
... i
ngik. i
72629-94-8 � Perflucrotrlafancic acid il'Firl7A �
537
2.0
2,0
n,
2058-94.8 6 PertiuOeaandecanolc acid (PFUnA)
537 ""-
2.0
< 2.0
ngiL
t EEA has demonstrated it can achieve these repod limits in reagent
grater, but can not document there in
all sample matrices.
Reg Llm t Type: MCL
SMG;.
AL
91rr�nbol.
a
�
Preparation
Date
07118/17 06:20
07118117 08:20
07118117 08:20
07118117 08:20
07118/17 08:20
07118117 0&20
07118117 08:20
07118117 08:20
07118117 08:20
07113117 08:20
07118117 08:20
07118117 08 20
07119r 17 0f3 20
07118117 08:20.
Analyzed
Date
07119f 17 04:09
07119117 04:09
07119117 04:09
07119117 04:09
071/9117 04:09 '
07119/17 04:09
OV19117 04:09
07119117 04:09
07/19117 04:09
07119i 17 04 09
07'16117 04:09 >
0711 Si t 7 04 0g
07119117 04:09
07119117 04:09
EIA
In g
3733364
3733354
3733364
3733364
3733364
3733364
3733364
3733364
3733364
3733364
.3733364
3733364
37.31,364
3733364
Page 2 of 3
Page 4 of 13
DEQ-CFW 00083450

Client Name: Cape Fear Public Utility Authority Report : 393030
Continuing Calibration Check Standard (CCC) I Continuing Calibration Verification (CCV) I Initial Calibration
Verification Standard (ICV) I Initial performance Check (IRC) 4 is a standard containing one or more of the target
analytes that is prepared from the same standards used to calibrate the instrument. This standard is used to verify
the calibration curve at the beginning of each analytical sequence, and may also be analyzed throughout and at the
end of the sequence. The concentration of continuing standards may be varied, when prescribed by the reference
method, so that the range of the calibration curve is verified on a regular basis. CCL, CCM, and CCH are the CCC
standards at lour, raid, and high concentration levels, respectively.
Internal Standards (IS) n are pure compounds with properties similar to the analytes of interest, which are added to
field samples or extracts, calibration standards, and quality control standards at a known concentration. They are
used to measure the relative responses of the anaiytes of Interest and surrogates in the sample, calibration standard
or quality control standard.
Laboratory Duplicate (LC) - is a field sample aliquot taken from the same sample container in the laboratory and
analyzed separately using identical procedures. Analysis of laboratory duplicates provides a measure of the
precision of the laboratory procedures.
Laboratory Fortified Blank (LFS) I Laboratory Control Sample (LCS) e is an aliquot of reagent water to which
known concentrations of the analytes of interest are added, The LFB is analyzed exactly the same as the field
samples. LFBs are used to determine whether the method is in control. FSL, FBM, and FISH are the LFR samples at
low, mid, and high concentration levels, respectively,
Laboratory Method Blank (LMB) I Laboratory Reagent Blank (LRB) a is a sample of reagent grater included in the
sample batch analyzed in the same way as the associated field samples. The LMB is used to determine if method
analytes or other background contamination have been introduced during the preparation or analytical procedure.
The LMB is analyzed exactly the same as the field samples.
Laboratory Trip Blank (L'TS) I Field Reagent Blank (FRS) Q is a sample of laboratory reagent water placed In a
sample container in the laboratory ;and treated as a field sample, including storage, preservation, and all analytical
procedures. The FRB/LTB container follows the collection bottles to and from the collection site, but the FRBILTB is
not opened at any time during the trip. The FRB/LTO is primarily a travel blank used to verify that the samples were
not contaminated during shipment.
Matrix Spike Duplicate Sample (MSD) I Laboratory Fortified Sample Matrix Duplicate (LFSMC) n is a sample
aliquot taken from the same field sample source as the Matrix Spike sample to which known quantities of the
analytes of Interest are added in the laboratory. The MSD is analyzed exactly the same as the field samples.
Analysis of the MSD provides a measure of the precision of the laboratory procedures in a specific matrix. SDL,
SDM, and SDH I LFSMDL, LFSMDM, and LFSMDH are the MSD or LFSMD at low, raid, and high concentration
levels, respectively.
Matrix Spike Sample (MS) I Laboratory Fortified Sample Matrix (LFSM) n is a sample aliquot takers from field
sample source to which known quantities of the anaiytes of interest are added in the laboratory. The MS is analyzed
exactly the same as the field samples. The purpose is to demonstrate recovery of the anaiytes from ;a sample matrix
to determine if the specific matrix contributes bias to the analytical results. MSL, MSM, and MSH I LFSML, LFSMM,
and LFSMH ;are the MS or LFSM at love, mid, and high concentration levels, respectively.
[duality Control Standard (OCS) I Second Source Calibration Verification (SSCV) - is a solution containing
known concentrations of the analytes of interest prepared from a source different from the source of the calibration
standards. The solution is obtained from a second manufacturer or lot if the lot can be demonstrated by the
manufacturer as prepared independently from other lots. The QCS sample is analyzed using the same procedures
as field samples. The QCS is used as a check on the calibration standards used in the method on a routine basis.
Reporting Limit Check (RLC) I initial Calibration Check Standard (ICCS) - is a procedural standard that is
analyzed each day to evaluate instrument performance at or below the minimum reporting limit (MRL),
Surrogate Standard (SS) I Surrogate Analyts (SUR) a is a pure compound with properties similar to the analytes of
interest, which is highly unlikely to be found in any field sample, that is added to the field samples. calibration
standards, blanks and quality control standards before sample preparation. The SS is used to evaluate the efficiency
of the sample preparation process.
Page 3 of 3
Page 5 of 13
DEQ-CFW 00083451

FELI in I E (s nalun.')
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DATE PEC IVED' "'�:�SE�n=�t-10)
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DATE ' Ti,s
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BY:
15
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REGFP Q �ISHE5 By(S3gnalure)
DATE i€e RECEVVED FOR LABORATORY
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rar°=3mar'";at& Wr".ttw ;3 axxMv d*p) 125%
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GVY-GROUND WATER
EINd EXPOSURE WATER
RAP Rwa W:+tim M lmrkirg dare) 73%
* L�taax8rut'i, E '>�� GRE.E-
thnfl d8 tt9ut55 3:D°�inq time rr�tcc$�ri��
may W r'c snv<grmS chvgg� '
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a^d sre rejecters ueles� re Y agree ;u €€3 esrr B3a d gY
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Eaton Analytical
Run Log
Run
ID: 231826 Method: 637
jyRe
samplO.
Semite
Matrix
Instrument lit
Anglysls.Date
Calibration File
CCL
3734274
Os
FL
07/1912017 00:14
071817M537a-FL-PFC14.rndb
LRB
3734263
RW
FL
07/1912017 00:46
071817M537a-FL-PFC14.mdb
FELL
3734264
RW
FL
07119/2017 01:04
071017M 537e-FL-PFC14.mdb
FS
3733363
Sweeney Water Plant -Post
1:3W
FL
0711912017 03:35
071817M 537a-FL-PFC14.mdb
FI3
3734266
Sweeney Water Plant -Past
CtW
FL
0711912017 03:52
071817iw1537a-FL-PFC14.mdb
FS
3733364
Sweeney }dilater Plant -Pawn
SW
FL
07119/2017 04:09
071817M537a-FL-PFC14.rndb
CCm
3734275
Cis
FL
07119/2017 04:42
071317M537a-FL-PFCr14.mdb

0
f'
0
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0
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SardpRe
raaEy4a
Method
MR: Client In
Result Amount
Target
Units
e6 Recovery R%PO R%PD DO
Extracted
AnaRyzed EEA
lygye
Rag
Recovery Recovery Limits Limit Factor
E0 9
CC1-
ES-€ .MeFOSAA-d3
537
i' A '..
k524Ja 00
4a24 J
t alL
1q: aq - n.lq --._ .... 10
07118f201712 51
0711912017 00:14 aM4274
_
COL
�
I&PFCA-13C:2 -_-,
a97 _.
.� R€fA
2a3302q.gd4
3t- 2g3C?:0
rqL
10a .'.-:54 -- -.. 1.0
07118109712'S1
0Y1191201700'1�4 2Y3�1k
CCL
13i.;4 €
_._�:..
5 ;}7
R rA
4119i9.0a
- 41 c1''
>tprR.
100 ��0 #50 ... .-- 10
07l18120171259
a7i19f209700'94 373427k
_ CCL
SS-, 1E4 O,5 A-da �. .�
..
fl37
€ 0. M -
�10.8310
a
i r�±L,
915 7^- 30 .�. -.. 171
0
07l1812017 12 51
.......................................................
07l1912017 00.14 �' 44274
_ ..
531
WA
�
9aT4
q
g19f264T 1281
071911700:1k7E
CCL
S PFHxA-13C2
€
Flo, 1112
530
rA-L
--
0
0711912097 92'51
07191201700:14 34
t1i Pe^uoraacanasulicnamidoae5 acid(NEFO{
537
2,2357
:
a
�_µm-
nvi
,,,..,. .,.... ..._._ __ :..:.
#9i 5i0 10
a73209792'511
am�f44CCL
079C1700.14 .Y4
GG
pf Pealiuraron.,4anasu drdrradr^ace cacid'iN.Me'B
537
�
2.1998
fl x3
nglL
19a 5i3- 1a:1 g L 0
a7f98l2a1712:51
47119J241700.14 9
CC
ner uaro5u€a eesa.Efari ac d (P Ba}
,...
5x7
...'
0
..
2.0493
.
2 rS
t�4rL
'€a2 5a - 15a {(--- E - i q
'a.,., ��...�Af...a.....��.....,.-
g7f93f2iB17 42 51
071i3J�017 0aS.14
�C4dL
-�
Psr^uoradacanoic acid 4PPDA3
37
1.901)1
2 0
'i r:..
..
95 50 15a -- - 1,0
�.,,,,,,,,.M�......,,..._
-
0719Bt2017 12 51
07119P2017 00:14 .� 37:4274
.. �,m.
-----.._...
CCL
PQr44i:oroha 4anrfc cold (} FH fi`
P P
Sir (( 2 0 E -
1.9676
�* u
w
sr 'L
�" 98 "�° .^q - lriq 9 w- 1
L� €�a
0711812017 12 51
07f19f2017 a0.14 ar274
CCL
_
P ruaao'+raxanasaEl%n:c acid,PFHxS} `0
537
2.0 -
2.i3054
:3 1a
^t lL
:.. Mm9Qa ^q-15i 9.f;
._:
0✓f1Bf201712&1
07119i26170a:t4 .'� k
CCL
Pcrfluoroha .anoic add €PF€ixR} -
53i
.:
2.0 2 ---
fl�
2 03.99
:_�
� .:.
�102 .....Ea'�-50 - 15 � � 9 =3 f
�`:
07i18iPg9712'S1
81209712:51
i1Y11912g9 P 00:#4
a711912017 00:14 `=7342, r`
,.L
Perflacrolaun add (.PFDcA)
537
_-_
2.0696
_Le.00: L ,,
90 a
103 5� .. #5t? 1 3
07i1
CB�
Par .ucr:smin tfo said (PFTA)
_
537
__. _
-
_
2.1301
u
4>sYN4 .,,.
te4°L
907 50-#5!3
07118t201712.51
07F1912a1700.14 97362rj
CCL
-- ., €
Pa�93uorvranarr a•d'PFFA) ..
.. 537
..,�0 ,�
20
_
1.9-0.%5
F 26
..
nrVL
9r 5 15a 'E i?
g7198f2g3'712:51
oTi9312017 Q0:1k ,#k2Y4
Parfluorddrare sud ode (PFOS)
537
rgi
a7116i201712 51
3`1.9035
07199217 00.14CCL
CCL
Peffuorooctandc acid(PFCA,
537
140
.
07f18120171251
0711912017014 °373�41 27744
,. ..
_
CCL �Pe^Pua o ^ide..anoic add :PFTrDA r `
837�
..
� "• -.
2.0628
2 0
d�r3.
1aa 50 �� 1:�+^+ @ ? 0
076181201712:61
07i1912a17 00' 94 -, 34?7r4
Perfluorcundecanoicacid(� UM)
537
1.9533
W20,-,-
nO:'L
fl0-9fl," ��E ,......3
iP711af201712:51
07199t201e00.14 373st274
LPG
IS-PlPAaFiiSAAd9
537
PdfA
42930.97a
462430
;1q*L
95 50-159 1.0
0779aM1708:20
0711=17W48 3734MS
LRB
IS-PF43A-13C2
537
$a!A
1089950.0q
bi33g2B2
ng1L
03 50-150 10
a"7t19MI70820
OW19Zq1700:48 3734i83
LRB
IS-PFOS-13C4
537
NIA
379M00
411919
n91L
922 60151i 1'0
07113J2a17 #if€.20
0711%417 WAS 9734203
LRB
SS-NFtFCISAA-d5
;;. 537
N/A
193.2750
: 200
t1grL :
96 70:_ 130 : 1.0
071IW201700.20
07119120170045 3734M.
LRB
SS-PFCBA-13C2
;;. 537
hd1,4
a9. 220
100
ngPL :-
90 70-"€0i4 i.q
0711!?U2a1709:20
07119V20174A 6 3'F3+4263
LRB
SSPPFxA-13C2
537
4d1A
5€.1298
q.@
agiL
102 70-130 1,0
971951201708:20
0711WO17W40 3734263
LRB
ayl acid (NEFC)
537
2.0
a 2,0
i1wL :-
1,0
07118F2 ITOO:20
0 IIW2017 W.4a 3734M
LRB
ryR B�erBuoreaci ae d;su€fenaonl¢Ere�crkc add {NM&F
537
2.0
� 2,0
nWL :
1,4
di7118Y201706:2C
£47I79121k17 a0 4i§ 3734283
L326
Porflu+src0u4arseauRStanle add (PFhS)
537
2.0
< 2O
n
to
07118=17a8:2O
07119120174a:49 3734M
i R8
Pad uoradacanoRc exact (PFCaA)
537
2.0
2 0
n7fL
1.0
Wi18f2A17 M.20
07119i2017 M40 3i 83
LRB
i+er8uoa epiaraa€c acid (PFHPA)
537
2.0
2,0
WL :
1,0
17/1812017 0t1:20
07119t2CJ170q:48 37342a3
LRB
'werfiueroheuerseaclfu3tie acid (PF1ixS)
337
2.0
2 0
1.0
0711WO17 08:20
07110=17 0GAS 373420
LRB
ParflaaarohexaaoRoadd (PFFixA)
537
20
'r .. 2:0
MIL
1.0
071101209708:20
g7P19t201700:43 3734 3
LRB
Per3asaroBeuaic said {PFDoA)
: 537
2.0
K 20
rfwL
: 1.a
a7€'RRFl20974b8:2a
i371i1ir2g1700'�ti0 973+42'03
LR9
Pefluoromydsdc acid (PFTA)
537
2.0
< 2,0
agtL
M_ M. 10
Ci7f18P2017 08 20
07110?2017 00:48 3734280
L680
Paafluorgradrosnez€c Arad iF'FdilAj :
537
2.0
< - 20
1,0
97/1Si1017 08:20
07l19f2€}170OA8 37242W
-OLi80
Pe RRaBtxocsanaau}fonafa(PFCS)
537
2.0
< 2;0
nWL :
1.0
071143R20170620
071191201700:48 373428
LRB
: Perauordoctandr. acid (PFCA)
.: 537
2.0
r, 10
RgiL :-
- 1.0
07118QC17 08:20
07119*011 ata49 3734203
WLRS
Petlfuorotrid node acid (PFTrDA) `
537
2.0
1.0
07i19Bl2017 W20
B"7t191M700'48 373420E
Lff30
Paa4:uoruundecandcadd (PFUM)
537
2.0
%.0
oEA'r _:
1,0
07116=170&,20
07t19F2017483:411✓ 37342.?
t"�Page 2 of 5
_ _
EEA Run ID 2318251 EEA Deport # 393030

Sample Method MRL Client ID Result
Type
Pkrea sdatt
Target
L€n9ta
%
Recovery RPD RPD 4Q99 �astracted
F9e
Re very
Limits
L9atait ;"ee*� ,
Analyzed
EFs5
fS PFi3A-13G2
537
537
3dlA
'A
..
1111.1
0 fl 00
45..0.....0......2......0.........0..0..
'S kau
,..
............4......6......2...
ngrL
�tg
&0 9u
_ ...,
- �'j 1.fl 07MW.0170820
071i912D170104
9 .M264
PF�iS-1UC4
,..
1978400.g0
2Q,1 "fl,20 :
::
n9iL
3
5q aq
: ......a�........,,fl.... Q7f1ii#201708.20
g7r'93y2Q1T 0i:09
3738254
_l
5S PliFiJAA-d5-.....__.
537
::: 53T
_., E~ifA
ilA
d07425.0Q
4t?f}:g
ng1L
99
W 9 Q
.:.
:.. �- q,,. :.3rli Qr2047082q
07199f2017 01:04
: v73a425ti
S�'PFLtA-13i2
::
F
--_
...
•p95.8200
2i?0
nglL
'9B
70130
3 S} 0711812U170S 2q
0711912097 fb1:t'%A
: 5T34Ls34
SS-PFHxi4t3D2
53T
NA�
','
--
93.6007
1^fl
ng/L
3
70 €0u
D ^{} OTi1812017DB20
071991201703:04
37342Ek
53T
597
t9lA.
M�
--
49.7278
50,1
nglL
93
70 f�0
-� 0711$i2617082D
07i19f2017Q1:D4
3734264
_ayiPerBdarcccianenU€fdn�reFadvtacaBcaGid{Pi'ciF�a
c. tp Pgr•�a4fddd4 ne u3fcnamidrsa 5d acid {F91`d
.......-_
537
__ ...
..
--
2.1107
1.9989
2Q
-.:
2.fl
ng1L
10q
5Q 15fl
..4 1u O7l13i2g17D820
0Tr19i2D1701:94
37:,284.
-.-_- �......,,
sdr"ur3rddUfc3nffsuieraFvic acid ( F'flw}
63i
-,
2.0
...
_-
2.1025
2.fl
n9fl-
'QD
? 9'�fl
1ru g711 Bf2017082q
$£'' 'j€
07199{2017 flF9:614
: 37'.3�`...'1�br4
PE3diF Grudsr,.aeet acid {PF�}Rj
537
_
j��j""""
2.0
1.9724
2-fl
n0
505
5fl t S:
0 Q7l1Bt201708 "'D
07f10l2917 01:04
3734204
i; 0 r •a randp4np c acid tPFFipAj 3
537
.3
2 Q
_-
2.0053
2 0
m01L
9r
Q;< fl
xq 07!'P£612g1T382D
0T119120'P7 Q3:04
;xrbi269
E eN udrdh�x��esi Efu�F c,3 id IPFHxSl,
587
2.0401
0
giL
INO
1 �fl
'� „q 7f15i2Q 17 08:23
-
07119 D17 01:94
37 �1284
{f PdrxuGrrs3laxa 7ctc ecd {PFHatAj -
_.,
'
2 q
t
2.0874
fl
NIL
i0,7
5fl Ise
:� -. 1 q .Q7ri Bf2017 g820
D7fT+3f26i17 g1:Q4
: 3734?i3d
va. ....�
E9 PeffluOr0
..
nOtL
..
T04
r:
5fl 1 au
.�. Q7r1Br2dP97 4i8.2a
JTi19!'�3'97 Q1:o4
37:iF2$�9
OU c acid gPFDdA%
i537
2 Q
�
1.9723
,� .0
atgtL
99
-
,.- T50
_..
f.0 07It8i20170820
.. ..
07119120170104
373d2B4
Psr'ducrGn ynsbd eG.l9 P 4
-
Psr"saGr.,nd'terc
2.0
M
:� t,
19515
2.0
ngil-
'3F
50 `50
==1,0 07Ii812017 gi%20
OT19012g17 fl1:Q4
�t'rg4?84
c acid ,F F9fif�4
Perlu rtsecla^td to €d�aie (cFj
537
537
2 D
E Q
_
2.0555
2.0
ngiL
1fl30
9r's0
�....p...�.... 1 C }', .OTiTBl2017 09 20
07t1ra12017 D104
:?73A284
��_. ..
-
2.g352
2 0
ngrL
Tfl2
xiq -ISO
3 r 07#18l2D17 03:2q
07l19#2017 01:g4
9734284
adEF.n�ddc3$n4M1F add r,F'FC)Aj
E'rrdiuo dbriddcani>ic Acid tPFTd)A) �
537
2.0
.,�
21305
2 Q
ngFL
10
5.,-'95u
r fl D7f48l2D17 03 20
....�
07/1912017 01'Q4
3 3T;;42Q4
..
537
2 fl
---
� �
1.9+814
2 0
ngiL
37
50: ?50
Tr1S! 0t7 QB 20
g7193#2Q17 01.0+p
3. 392Qd E
F�
dstrauddvcnnEG acid iPs-Ee'rtAj
53T
....
1.3334
.E.q
ng1L
35
50 -15Q4Y
37118!'t017 09 2q
0711912017 01:04
F734251
95-idF?,9F'C35EAda�d3
537
PF1A
sreeetvtgti4gt6rt'farrt-Aasc
4�ti4�iiiB.QO
:4�a e3Q
ngti.
9T
.50-160
: Ei.03 D7t18€2Csf'd"t2B.2Q
4#"FS1D1201'7ti3�r
1F88,5D
F9
90P6LSA-13C2
�}a
537
6V94
Sv�ay�eeerPxuNxaY
2Qpa3$TgiRfl
205509
50-$8
0,93 £7$82#97$B2FTi##
47035
57 :
F3
B3T
WA
rrrgiaYeri
4V10
r
itS3
5C3;i0Sb
0#33 07118d20474b920
07119P2097U33
37S2 3
F5
5NE4Fi3SAA-rtS
537
AdFi4
swreeneywesteaP t1-P Ff
17g.iBvaO
200
7g%
70,130
i335 Qit1982GS7€J8:231
Oi9 i31f03;3
375i393?
F
SS-13C2
537
pg#A
atveenay&s?s P9an-P8
95,e48k
i0gY
92
7O-19D
D.937f1i#20170B2O
Df#9Di73330
$a393
F3
_ 8$-PFPia,4-15 2
aa3T
FE#A
6vewneyWaterPfa�E-Pa®t
44:IW7
5D.0
ragtL �
95
7dF=1911
0.93 c�'Fir$;�017499.,2td
dF7'#i 7TFf3:3�
3733
ty9 Pardhaatraddr8er0avalfdrvasnl�in9cdilc add ehEEkEit:
: 0;7
2.0
:' aeney+4faesr Pint -Pave
a
2.83
n
�,�.
.-
-
.
F
. xy3 Pr�riir,FGrasOc'i�aaesuEfor6anreEtee r,�stsc add EAJhieF
:537
2.0
5wreeney atiacgs Ptaac-r�afff
w
2.p
w M., 0.'9=S ti7#'9 Oi29#17 ff19.2it
liii'1:9t 0�74.3:u"5
3'7'33.38
F°3
Pn18caGrdbu9atnesu6ffdrtic aGk# (F'F09) :.
537
2,0
SwasenayL&atrr P3a7t€-Ps�B
�,g
-
i3.9& g7t9982p-$7 tlat:20
0TF79}2(d-Ii 09;35
3'7.}3gS .
F
Pnt4ud Eac9nGGacd(PF33A
537
2,0
7YVa9 F€e¢et st
4,4
-
0.93 0714 Q1e"T£Ji3:20
07FtT D1...... 5
33`95353 3
FS
Ps Bdcsrotl4dnddadri(PPaipA}
537
2.fl
.....
mane Hate PanrPas
1
ra¢rL
sR93 C£fY8#201743620
D7#Ff3F2it7tA%:
3F a983:
F3
ac
Re¢f}u>tttmz rsn�aKsncF#(PFhllc)
a%7
2.0
:waeneyi�afe FrentimEi
B.i
ragf3
t.93 fXFI3BP2aA174b92}3
07#IIIT@"�:35
3 3859
...-
FS
Per9ddrdhexaraa€cadd ;PFf4xA
537
2,0
9areent�Jsta�rP3azt1-Pr+et
9'F
t� 8
090 4}T7PB2E38i4} 2iP
O IIH327i703:35
FS
Pdmraifsw'9G aced (flFOdA)
537
2.0
awsmdyVaeer F'BPasB
K
-
2.
ngft-
A�rL
D.93 t37P18dL4370;
-:
O7'i1Di703;33753385
._
--
F9
PeMdnF'urmp+ri&i3Gadd _(PFTA)
637
2.0
5sney�+rat67tf�ar-Past
x
2.9
dF 93 071=017 08 20
07f1wM7 Vt,135
37
0
FB
PdFfla.tnrrtPapn3Fxa9G acid (PFkdA)
597
2,D
sereeney iP7aYet Pl�ae-!*scat.T
ngsL
i4,9:5 tYT13892s3174RB:2dE
t371'19stYTg3;5.5
3723399i
fll
p
F3
PG49tktrrsetGiane su9tdr¢ (PFi'1)
: 537
2,0
9ureenay Vdats�r P1-PrFfi
2
m O�b9 0T1t�#2{317t€ 20
OTd1 O'1703,35
:: .:
57539BS
F$
%3
P�r?unt'mddi an a 4 add {PFL1rij
537
2,0
a x an»p #�Faear Fda t-PIDai
14
0.g& t3fiBF2lJf708,20
.
D7{101703,3733
E� F9
PargFtnrGGa¢9n,8.t4cticacdg6bFb"rCFAS
a57
2,q
enepviaterPFaror-t>otas
2.0
t
f8.93 Qif1Ba2O97 080
07dt€7iR 3
37339
jy FS
F9¢5ac nendscamncscdd{PFtireA}
537
2.Q
srmarwgVa a Fizz ao�c
c
2.0
t#.95 OB#18P2D1700 9
ki7d?DP201FO3,3Q
573&3
O
w FJ
ES-d4ieFC➢SAA 93 ��
v5$7
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3
4
d524x4
atgL
IL
_,
0,03 iBi#i1 PHPB 20
95 824
07110=17£i$w
Or/19t2U1703.82W
3MSM33
374200
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..
EEA Run ID 2313251 EEA RePo9t # 393030
En

0
0
n
n
�O
O
O
00
W
rn
a¢nple
Analyts
rs9ethcrt8
Ty
FD
I5-PFCA-13C2,
Mff
FO
IS-PFOS 13C4
5',
( FE3
eS-NPt f SAF d5
, .
53 ..__._._�
F0. 3t
8$-FF'GF 3f 2 _.. f
-537
FC
`;,PFF:xt.1o;:.2
537
I FD }rry3 acid (I'• EEO f ,.. ••-•i
i......,.
537
,.,.....
3yj Perfluoronctar,asu?onaF'3id oacatic a ad iNMsF
537
F0
Peftc.abutanesutcnr acid(PFE3�5�}3'
537
c>r
edlluorodecenmi., acid (PFCA)
..
a37
' C
,Peftormheptandc acid (FFHpA)
537 w.
FD
psr'li ern»sxssnssulien'c acid fPFNxS)
537
t �F€3 l
Perfluet'mhaxande acid (PFt1XF.i
53;
FD
_
Perfluorolaunc add WFOoA)
537
F0
Part:umromyr stic acid SPFTA)
537
F0.
W4
Per$umrdmmnaro c ac d PFMA
537
FD
W �
Pa-flumr000taa a aa3rar•a.a (PFCS) -..
..
537
FID 1•
Perflamrrrocta smic acid_ (PFCA% . ,-
M
I F0 r
Pell D o adeca7mi acid (PFTrCA)
537
I m F0 p�r0udrrr;ndecanoi acid (P 'UnAj . _
537
F6
IS-NMOFOSAA-d3
537
FS:
€S-PFOAs13C2. :
.;537
F3
IS-PFt?5-13fl4
..:. 637
FS
SS-NElFOiSAA-d5
537
F&.
SS-PFDA-93C2
.:537 ..
FS
... SS-:PFttxA-93C2
:..537
FS Ay{ Pa fluorn¢acEaaleeuPtmwra sitl4ac84 C Wd (NEIFC
537
FS acid (NMeF
537
FS.
Pedltxxmtx.naa¢i9adie acid (PF®fi)
'. 637
FS
parl9amrcadedafam¢c $add (PFDA)
. 537
F5:
t9atflucxch ptanraac aoW (PFHpA)
.537
F5
P ¢flumrataaxdnasulfmaie acid (PFHxS) ;
< 557
Fs
P fluc rahf xarm c acid (PFHxA)
537
FS
PeMuordaurlc acid (PFDQA)
637
Pas9umrotny a4c acid (PFTA)
537
FS
PeFftworiona oleacid.(PFNA)
637
F5
, Petflumrooc(ane Swonate (PFOS)
FS
Peftoroo tanalm acid (PFO4A)
537
FS
pardludnaflideAcaraoio add:. (P'F trt1A)
FS
Parl m aw-docarido add (PFUnA)
537
,�„OCtA
IS-NMeFiTw-d3
537
Im-
,IOCCIM
*-PFOA 93C2
537
wPage 4 of 5
R§ttL Client 963 Result I Amount Target
Ott, :.. $xee..cgtva;�rf ant-P• t.. 2047260 n 203xa20
Swefrgy rilat
2 a
..
o f Irt 3 n fast
4 30
...
2.q
5.3� naf,�t r Ian �e t
12 7
r
2
S,w-naAJaaf rPlaniFe_i
893
:.
2.
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17S
.
2 0
ew e ey Water
?7
x a eu W.t.,Pa tPvat
2.0:
..
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4.74
..
xeen y s+vAer 11a^4 Pax ,
14 4
.�
2q
,.
: tt •�
2a
.
_
N A - 431858 00 431.858
M A. ... ... 19442w.00 _ 194429C•
tintts
% Re"O ory RPO RPt3 Mt Extracted
Analyzed EEA
fteovvery Limita Ludt Factor
IR #
.. - 3... ._.j ... ____.
L.........l t3 9� 0711612017 06:20
..........
07119=17 03:52 3734285
rgrL
102 50 - 150 � q 95 OW1 ai201'7 0a:2q
071ISM1 r 03 52 342 ,6'
rg;L
70-'3a Oc5 07/18t201708:20
071IM0170352 3 34Mr,
r'glL
7q - 't3q � 5 0711812017 03:20
0711912017 03 52 VM266
ngk
..
7a - 130 ==0.95 07115D2017 ga:20
07119l2017 g3'S2 8 ;A2g0
ngrL
,,.�
E� 085 07t1912017aa:2..
07l19t20t70352 . 3734256
nglt---'
95 07119209700:20
0719012017 03.52 :37 z92
ftgDL
�� --• 795 071131201708:20
0711W201703:52 37342t36
_.:
-tit
0.2 3a +^, 95 07l9317017 08:20
0T119D20t T 03:52 37,.42
...
3giE.
1,5 3a 0,95 071IM01708:20
07l19D201703:52 M4M
_
2.9- ; a o 15 o7r1e12o1a a®:2o
07199 2017 03:52 3 42s
is
0711612017 06:20
07/1912017 0152 37V!266
ng L
Orilw2017 09:20
0711912017 03 52 37.3A266
F.........." �]� 07t1k}!?0'P70R:20
07f1012..... F '�a342Gn
nOtL
3 07113?2017 0$:20
07119M17 0$.52 37.A286
nOtL
_: =F7,250 q,SS 1 0711af20r 08:20
0711912017 03 52 .3734266
14 30 q.55 gaD1812017 M20
07A 201703:52 3734266
n
'-- _._ 7.t..'S gW2017 M20
71grL
:
OVIV20170352S7341,1,6
ngrt.
..,
� � 0.95 .: 07118t2017 08:20
07i99.f2017 03:52 ... ,4260
ng1L 10a 50 - 1 w 1.0 07i19l209 a 04 42 373A275
nglL 1q0 0q - 150- 1 0 0711q! 017 t2 51 0711.9f21J9i 64 42. 3734<75
EEA Run ICE 2318251 EEA Report # 303030

i Page 5 of 5 EEA Run ID 231825 / EEA Report # 393030

O
k
jy2e :�.
CCL
CCU
FD
FS
FBL
LRB
«
\
§
a
Sample ly.
«m€mlU«m>
dmlgnlU«mmw
Field Duplic!e
Field Sample
Fordfied Blank Low
Laboratory Reagent Blank

Fags 13 of 13
DEQ-CFW 00083459

DEQ-CFW 00083460