DEQ-CFW_00063696

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DEQ-CFW 00063696

eAF f?
EFFLUENT
R17JDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH
FACILITY NAME DuPont - Fayetteville Works CLASS 3
OPERATOR IN
RESPONSIBLE CHARGE (ORC) Robert J. Geddie
CERTIFIED LABORATORIES (1) Aaua Tsbh Environmental Laboratory
(2)
Decembet FF`R-:ApC j�-
COUNTY Bladen
GRADE 4 PHONE [phone]
Burlington Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
�
DIV. OF ENVIRONMENTAL MANAGEMENT
G��iu/,/ �/
X Z
(SIGNATURE OF OPERIWOR IN RESPONSIBLE CHARGE) DATr
DEHNR
P.O BOX 29535
�,a 4;
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
R'
RALEIGH, NC 27626-0535
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE , f
t
50050
00010 1
00400
00310 1
00530
00556
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0.710
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2.0
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DEM Form MR -I (12/93)
DEQ-CFW 00063697

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
'-� II t� and sampling frequencies do NOT meet permit requirements
9 U r�-.�
Noncompliant
MAR 19 1997
If the Wii.snoncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintg�%W time table for improvements to be made.
FFICE
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of -the person or persons who manage the system, or those
persons directly: responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. M&Rerry - Site
Permittee (Pleasd print 009D
l
gniture
_NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
00080
Color (Pt -Co)
006 i0
Ammonia Nitrogen
01092
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
1lexavalent Chromium
01147
00300
Dissolved Oxygen
01034
Chromium
31616
00310
BODS
O(1665
Total Phosphorous
32730
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
00400
ptl
00745
Total Sulfide
01042
Copper
34481
00530 Total Suspended
00927
Total Magnesium
38260
Residue
00929
Total Sodium
01045
Iron
39516
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Nickel
Silver
Zinc
Aluminum
Total Selenium
Fecal Coli form
Total Phenolics
Benzene
Toluene
MBAS
PCBs
Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliforin is to Ix: reported as a GEOMETRIC mean. Use only units designated in the retxtrting
facility's perntit for reporting data. L6 I i [I P
* ORC must visit facility and document visitation of fauliFtya`,krequired per=15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the perrnittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063698

' EFFLUENT i FES 191997
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH December YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
C�4ECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
RALEIGH, NC 27626-0535
x -�:j ' K 11-;2 -) /4'
&Z — 64 'L-p-j/ -�
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
00951
00655
00600
00310
00340
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HRS
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Y/N
MGD
C
UNITS
Lb/Day
mg/L
mg/L
mg/L
mg/L
Ow
MAT
2
08001
24
Y
14.809
16
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14.809
13
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12
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26
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10
7.4
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28
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24
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EWE
30 osoo
24
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14.035
15
7.9
"...,
AVERAGE
14.335
12.8
1440
0.30
2.54
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I -
0.30
2.54
MINIMUM
13.913
10
6.8
804.2
... .......:.....:....
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i�.�._..
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Monthly Limit
Daily Limit
6-9
7917
DEM Form MR -I (12193)
DEQ-CFW 00063699

Facility Status: (Please check :ne of the following)
All monitoring data and sampling frequendes meet permit requirements ©�
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements I�
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
1 certify, under penalty of law, that this document and ai attachments were prepared under my direction or
supervision in ,accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of. the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are sijnificant penalties for submitting false information,
including the possibility of fines and imprisonment for Itnowrig violations.'
Micbael E. Maybeia - Sfte
t°ermittee (Please-bW or tvp
'/2-g /5' -1
re of
NC Hwy 87 South, Fayetteville, NC, 28306 "10) 678-1400 May 31, 2001
Permittee Address Phone Number Permit Exp. C
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 p1l
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total arsenic
006i0 Ammonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 ilexavalent Chronuum
01034 Chronuum
W665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067
Nickel
50060
Total
01077
Silver
Residual
01092
Zinc
Chlorine
01105
Alununum
01147
Total Selenium
71880
Formaldehyde
31616
Fecal Coli form
71900
Mercury
32730
Total Phenolics
81551
Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal colifon t is to Ix: reported as a GEOMETRICreporting
mean. Use only units designated in the rerting
facility's permit for reporting data. L6 i ;, !Vr
L jt'
* ORC must visit facility and c uinaertat visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the hermiuee, delegation of sigiratv4y authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063700

• EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO.
006 MONTH
December
YEAR 1996
FACILITY NAME DuPont - Fayetteville Works
I CLASS 3
COUNTY
Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie
GRADE
4 PHONE
[phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory
(2) Burlington Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES
Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
RALEIGH, NC 27626-0535
x ,�� i� - '44�
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DATE
50050
00400
00310
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RS
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MGD
UNITS
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DEQ-CFW 00063701

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements 0
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South
Permittee Address
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BODS
00340
COD
00400
pill
00530 Total Suspended
Residue
00545
Settleable Matter
Michael E. MavbB= - Site
of
NC, 28306 (9-M) 678-1
Phone Nurr
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
006 i0 Ammonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 llexavalent Chromium
01034 Chromium
W66.5 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
31.2001
Pe
01067
Nickel
50060
Total
01077
Silver
Residual
01092
Zinc
Chlorine
01105
Aluminum
01147
Total Selenium
71880
Formaldehyde
31616
Fecal Coli form
71900
Mercury
32730
Total Phenolics
81551
Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal colifonn is to be. reported as a GEOMETRIC.mean. Use only units designated in the reporting
facility's permit for reporting data. L5 �; ! IIV
* ORC must visit facility and document visit*w!! of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
o_ .. ,j,
** If signed by other than the pertnittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063702

NPDES NO: INC 0003573 DISCHARGE NO: 002 MONTH: December YEAR: 1996
r FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear Hlver
LOCATION: DuPont River Pump Station
Upstream
STREAM: Cape Fear River
LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
Downstream
00010
00300
00095
00951
Enter Parameter Code above
Name and Units Below
d
o
U
0)
o m
v
CL
d`o
>tm
c
cu
U
x
D O
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m
2
4
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6
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8
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10
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12
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14
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16
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110
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8.8
10.2
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7
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00300
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00951
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MAR 19 199T
FRfEz_ T TEVILE
�r�=v�=
REG.
DEQ-CFW 00063703

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of -the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information_ ,
including the possibility of fines and imprisonment for knowing violations."
Michael E.
niture
NC Hwy 87 South, Fayetteville, NC, 28306
Permittee Address
Number
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
00082
Color (ADMD
00625
Total Kjeldhal
01027
Cadmium
01105
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
1lexavalent Chromium
01147
00300
Dissolved Oxygen
01034
Chromium
31616
00310
BODS
W665
Total Phosphorous
32730
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
00400
pli
00745
Total Sulfide
01042
Copper
34481
00530
Total Suspended
00927
Total Magnesium
38260
Residue
00929
Total Sodium
01045
Iron
39516
00545
Settleable Matter
00940
Total -Chloride
01051
Lead
50050
Nickel
Silver
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCBs
Flow
31, 2001
tit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliforn is to be reported as a mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of fac8i1yas Veduir1g4; S}15 aYFAC 8A .02U2 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b)
(2) (D).
DEQ-CFW 00063704

January 29, 1997
NC Dept. of Environment, Health & Natural Resources
Division of Environmental Management
Central Files
DEHNR
P. 0. Box 29535
Raleigh, NC 27626-0535
AIAR 19 1997
11
vI'.se---a
REa
Attached is the DuPont Fayetteville Works Discharge Monitoring
Report for December, 1997.
If you have any questions, please contact Robert Geddie at (910)
678-1219.
RJG:apm
Attachment
cc: M. E.
Gell
- ENGR, Charlotte
R. J.
Geddie
- FW
J. E.
Hagle
- FW
M. G.
Batton
- FW
M. E.
Johnson
- FW
D. G.
Sorensen
- FW
File:
F-1-3-4
DEQ-CFW 00063705

L6 c,
Ij
DEQ-CFW-00063706

Y � '
EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH NOVEMBER 1 96
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddle / Kenneth M. Hall
Mail ORIGINAL and ONE
ATTN: CENTRAL FILES
131V. OF ENVIRONMENTAL MANAGEMENT
DEHNR L 199 (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
5005 r
'---p0Q!Q
00310 1
00530
00556
TG3F
FLOW
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DEM Form MR -I (12/93)
7.6 1 30.7 1 61.5
DEQ-CFW 00063707

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L�
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that thete are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number ' Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
0009.5
Conductivity
00300
Dissolved Oxygen
00310
BODS
00340
COD
00400
pl1
00530
Total Suspended
Residue
00545
Settleable Matter
PARAMETER CODES
00.556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
00610 Anunonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 Ilexavalent Chrontium
01034 Chromium
0066.5 Total Phosphorous
00720
Cyanide
01037 Total Cobalt
00745
Total Sulfide
01042 Copper
00927
Total Magnesium
00929
Total Sodium
01045 Iron
00940
Total Chloride
01051 Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene '
38260 MBAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehydz
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GIAMIi'1'ItIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitaLir3i a a(% as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the perntiuee, deleygftu, srgnkBrrQ Aodty must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).tt<�
DEQ-CFW 00063708

EFFLUENT .,1r .
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH NOVEMBER YEARS
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES j�G�,,I�
bIV. OF ENVIRONMENTAL MANAGEMENT X ��JJ
DEHNR (SIGNATURE OF OPERATO)f IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
aei Glru Mr. 97A9a_nra_9; ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DEM Form MR-1(12/93)
DEQ-CFW 00063709

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number ' Permit Exp. Date
PARAMETER CODES
00010 Temperature 005.56 Oil & Crease 00951 Total Fluoride 01067
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077
00080 Color (Pt -Co) 00640 Anunonia Nitrogen 01092
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium 01105
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 IIexavalent Chromium 01147
01034 Chromium
0(1G6.5
00720
00745
OU927
00929
ou94o
Total Phosphorous
Cyanide
Total SnlriJe
Total Magnesium
Total Sodium
Total Chlorite
01037 Total Cobalt
01042 Copper
01045 Iron
O1U51 Leal
Nickel
Silver
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCBs
Flow
50060 Total
Residual
Chlorine
71880 Formaldehydc
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal Coliform is to be reported as GEOMETRIC mean. Use only units designated in (fie reporting
facility's permit for reporting data. L6
* ORC must visit facility and document visitation of fac5i1MsG0aed per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the perntittee, delegation of signatory authority must be on rile with the state per 15A NCAC 2B .0506 (b)
(2) (D).
00300
Dissolved Oxygen
31616
00310
BODS
32730
00340
COD
34235
00400
pf I
34481
00530 Total Suspended
38260
Residue
39516
00545
Settleable Matter
50050
DEQ-CFW 00063710

EFFLUENT -�
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 006 MONTH NOVEMBER YEAR 199
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES g/��
DIV. OF ENVIRONMENTAL MANAGEMENT X f�®C�✓ '�"'
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DEQ-CFW 00063711

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements L �J
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of.the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that thete are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South
Permittee Address
Michael E. Mavberry -
Sionitbre
28306
910 678-1400
Phone N
PARAMETER CODES
r '
) Zl1.10K
00010 Temperature
00556
Oil & Grease
009.51
Total Fluoride
01067
Nickel
00076 Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032
Ilexavalent Chromium
01147
Total Selenium
00300 Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
00310 BOD5
W66.5
'total Phosphorous
32730
Total Phenolics
00340 COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400 pH
00745
Total Sulfide
01042
Copper
34481
Toluene '
00530 Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545 Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
31.2001
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Cale assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal colifonn is to be reported as a GEOMETRIC mean. Use only units designated in'the reporting
facility's permit for reporting data.
* ORC must visit facility and dooLkerkvtAffmon of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than tliM_trtt g*dt'Mignatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063712

NPDES NO: NC 0003573
FACILITY: DuPont - Fay1
STREAM: Cape Fear Rh
LOCATION: DuPont River
DISCHARGE NO: 002 MONTH: NOVEMBER YEAR: 1996
COUNTY: Bladen
STREAM: Cape Fear River
LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
Downstream
DEQ-CFW 00063713

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0`
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and. a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that thete are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (t't-Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
13O11)5
00340
COD
00400
pl f
00530 Total Suspended
Residue
00545
Settleable Matter
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
00610 Anunonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 llexavaleut Chromium
01034 Chromium
W665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal colifonn is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data. * ORC must visit facility and document visitation of facility as required per 1j/6NdT ,`4A .0202 (b) (5) (B).
** If signed by other than the permitlee, delegation of signatory authority must be towel WASMate per 15A NCAC 213 .0506 (b)
(2) (D)•
DEQ-CFW 00063714

EFFLUENT -
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH OCTOBER YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
.CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall ;
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES G�✓"" (!'1� /J n e J l/� �?/��
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 NN-� 1 I BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535
FLOW
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::::::::...�::;:
©
1:11
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. a
DEM Form MR -I (12193)
DEQ-CFW 00063715

RECEIVED Facility Status: (Please check one of the following)
DEC 3 �Pt�oritoring data and sampling frequencies meet permit requirements
uu 7777vv Compliant
FAYEP R g data and sampling frequencies do NOT meet permit requirements
AEG r Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
!t r
i
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of.the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00.556
Oil & Grease
00951
Total Fluoride
01067
Nickel
50060
Total
00076 Turbidity
00600
Total Nitrogen
01002
'Total Arsenic
01077
Silver
Residual
00090 tolor (It -Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095 Conductivity
00630
Nitrales/Nitrites
01032
1lexavalent Chromium
01147
Total Selenium
71880
Formaldehyde
00300 Dissolved Oxygen
01034
Chromium
31616
Fecal ColifOrm
71900
Mercury
00310 BODS
W665
Total Phosphorous
32730
Total Phenolics
81551
Xylene
00340 COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400 p1l
00745
Total Sulfide
01042
Copper
34481
Toluene
00530 Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545 Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assistance may obtained by calling the
Water
Quality Compliance Group at (919)
733-5083, extension 581 or 534.
The monthly average for fecal colifonn is to be rcIQLjgc(C. s� 1- t., -)ME-" TRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the perniittee, delegation of signatory authority must be on rile with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063716

EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 — MONTH OCTOBER YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS. 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie l Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
'DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
Ilium.
MCMM=
EMMEN
mmm"
MCMIMES
McMw2=
DEM Form MR-1 (12193)
DEQ-CFW-00063717

RECEIVEDFacility Status: (Please check one of the following)
DEC 3 0 ftonitoring data and sampling frequencies meet permit requirements
Compliant
FAY(i.�-Emg data and sampling frequencies do NOT meet permit requirements C�
REG. ��+� Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E.
P/ f sl�6
of
NC Hwy 87 South, Fayetteville, NC, 28306 (910) 678-14W May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil Si. Grease
00951
Total Fluoride
01067
00076 `I'mbidity
00600
'Total Nitrogen
01002
'Total Arsenic
01077
00080 Volor (I't-Co)
00610
Ammonia Nitrogen
01092
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032
1lexavatent Chromium
01147
00300 Dissolved Oxygen
01034
Chromium
31616
00310 BODS
W66.5
'Total Phosphorous
32730
00340 COD
00720
Cyanide
01037
Total Cobalt
34235
00400 pit
00745
Total Sulfide
01042
Copper
34481
00530 Total Suspended
00927
Total Magnesium
38260
Residue
00929
Total Sodium
01045
Iron
39516
00545 Settleable Matter
00940
Total Chloride
01051
Lead
50050
Nickel
Silver
Zinc
Aluminum
Total Selenium
Fecal ColifOrrn
Total Phenolics
Benzene
Toluene
MBAS
PCBs
Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Croup at [phone], extension 581 or 534.
The monthly average for fecal colifoim is to be mean. Use only units designated in the reporting
facility's permit for reporting data.
* Otte runs( visit facility and document visitation of facility its rectWed per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other thau the penniltee, delegation of signatory authority roust be on file with the state per 15A NCAC 213 .0506 (b)
(2) (U)•
DEQ-CFW 00063718

EFFLUENT Ca"NOV 2 7 W6
NPDES PERMIT NO. INC 0003573 DISCHARGE NO. 006 MONTH OCTOBER YEAR 1996
FACILITY NAME DuPont - Fayetteville Works , CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) A ua Tech En ironmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES `
biv. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 � ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
S
FLOW
I= Y
o
®
EFF X
W
F
2 o
E
0
INIF
F C
�
Q c
1=
O
rp N
m
W
O
J F
o
O
a g
• • � � :BdG'O•!A•
DEQ-CFW 00063719

^. : facility Status, (Please check one of the following)
rz it
All monitoring data and sampling frequencies meet permit requirements
DEC 3 0 1996 Compliant
FAYj-=WjW &g data and sampling frequencies do NOT meet permit requirements 0
REG. OFFICE Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made. .. '
v jy�
Y
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Maybe
Pegnittee (Please
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 'I`urbidity
00080 tolor (I't-Co)
00082 Color (ADM I)
00095
Conductivity
00300
Dissolved Oxygen
00310
BODS
00340
COD
00400
plI
00530'I'otal Suslrended
Residue
00545
Settleable Matter
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 llexavalent Chromium
01034 Chromium
W665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parauneter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
Tlie monthly average for fecal coliform is to be repoiLed as a. ;IiOME' 1'RIC mean. Use only units designated in the reporting
facility's permit for reporting data'.
* ORC must visit facility and document visitation of facility as. requited per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with (lie state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063720

NPDES NO: NC 0003573 DISCHARGE NO: 002 MONTH: OCTOBER YEAR: 1996
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
Downstream .
�MMMMWMM
Enter Parameter Code above
Name and Units Below
A
o
DEQ-CFW-00063721

Facility Status: (Please check one of the following)
ru �..,.a T
All monitoring data and sampling frequencies meet permit requirements EET
UtG 3 0 1996 Compliant
FAy ll AM Noncompliant
data and sampling frequencies do NOT meet permit requirements
Noncompliant
REG. OFFICE
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of. the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Mavberrv-- Site
of
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
00010 'Temperature
00076 'I'mbidity
00080 Color (1't-Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
1301)5
00340
COD
00400
pll
00530 Total Suspended
Residue
00545
Settleable Matter
PARAMETER CODES
00556
Oil & Grease
00951
Total Fluoride
00600
'Total Nitrogen
01002
'Total Arsenic
00610
Ammonia Nitrogen
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00630
Nitrates/Nitrites
01032
I lexavalent Chromium
01034
Chromium
W665 'Total Phosphorous
00720 Cyanide
01037 'Total Cobalt
00745 Total Sulfide
01042 Copper
00927 Total Magnesium
00929 Total Sodium
01045 Iron
00940 Total Chloride
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 WAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to lx: reported as a GE'0M1 FRIG mean. use only units designated in the reporting
facility's permit for reporting da(a. 0- } „
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213 .0506 (b)
(2) (D)•
DEQ-CFW 00063722

R
aUPONT
DuPont Automotive
DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
November 18, 1996
NC Dept. of Environment, Health & Natural Resources
Division of Environmental Management
Central Files
DEHNR
P. 0. Box 29535
Raleigh, NC 27626-0535
Attached is the DuPont Fayetteville Works Discharge Monitoring
Report for October, 1996.
If you have any questions, please contact Robert Geddie at (910)
678-1219.
RJG:mam
Attachment
cc: M. E. Gell
R. J. Geddie
J. E. Hagle
M. G. Batton
M. E. Johnson
D. G. Sorensen
File: F-1-3-4
- ENGR, Charlotte
- FW
- FW
- FW
- FW
- FW
E. I. du Pont de Nemours and Company ® Printed on Recycled Paper
FF-9522 Rev. 5/93
DEQ-CFW 00063723

"l,VE
DEC 3 0 1996
FAY �'dL�.E
RGi. �FF-iCE
e- (, 7
''J vL ritJi--�
DEQ-CFW 00063724

EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH SEPTEMBER YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
DEM Form MR -I (12/93)
(SIGNATURE OF OPERATOR IN
BY THIS SIGNITURE, I CE
ACCURATE AND COVANWTC
ONSIBLE CHARGE)
THE REPORT IS
DEQ-CFW 00063725

Facility Status: (Please check one of the following)
II m nt oring data and sampling frequencies meet permit requirements
NOV 2 b 1996 Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements 0
Fs� � t..,, F - .. Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made. '
•
"I certify, under penalty of law, that this doct�ent and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of -the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayberry - Site Manager
Permit ee On r t p)
Sigure o rmitt ate nat
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride
00076 'I'ilrbidity 00600 Total Nitrogen 01002 'Total Arsenic
00080 Color (I't-Co) 00610 Ammonia Nitrogen
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Ilexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BODS
W665 Total Phosphorous
00340
COD
00720 Cyanide
01037.
Total Cobalt
00400
pill
00745 Total Sulfide
01042
Copper
00530 Total Suspended
00027 Total Magnesium
.
Residue
00929 Total Sodium
01045
Iron
00545
Settleable Matter
00940 Total Chloride
01051
Lead
01067 Nickel 50060 Total
01077 Silver Residual
01092 Zinc Chlorine
01105 Aluminum
01147
Total Selenium
71880 Formaldehyde
31616
Fecal Coliform
71900 Mercury
32730
Total Phenolics
81551 Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
Parameter Code assistance may obtained by calling the Water duality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal colifotm is to be repotted m a GEOM1 TR1C mean. Use only units designated in the reporting
facility's permit for reporting data. ,
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** if signed by other than the permitice, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063726

NPDES PERMIT NO. NC 0003573
FACILITY NAME DuPont - Fayetteville'
OPERATOR IN RESPONSIBLE CHARGE (ORC)
CERTIFIED LABORATORIES (1) Aqua Tech
CHECK BOX IF ORC HAS CHANGED C
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
RALEIGH, NC 27626-0535
EFFLUENT f `,
DISCHARGE NO. 002 MONTH SEPTEIbCER i �bVYPAO, 1996
CLASS 3 COUNTY Bladen
?rt J. Geddie GRADE 4 PHONE [phone]
rental Laboratory (2) Burlington Research
PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
00951
00655
00600
00310
00340
FLOW
yui
z
fE Y
c
m
EFF X
uw
oO
p
;?
W`
8
E
INF ED
y
a y
=
¢
a o
t
N
c
O
w W
CL
O a
z
O
V
m
o
a s
~
IL
O
0
0
G 0:
HRS
HRS I
Y/N
I MGD
I -C
UNITS
Lb/Day
mg/L
mg/L
mg/L
mg/L
»a.
2
o800
24
14.650
26
7.4
E4
7.4
o800
24
Y
14.650
28
6
o800
24
B
14.650
28
7.1
Em
8
o800
24
14.650
789
10
o800
24
Y
16.657
27
7,4
12
0800
24
Y
16.657
27
7.3
14
o800
24
16,657
7.4
16
o800
24
Y
16,035
28
18
o800
24
Y
16.035
28
7.3
7.4
20
o800
24
Y
16.035
26
IN
22
0800
24
16.035
1463
24
0800
24
Y
14,145
28
7.6
26
0800
24
Y
14,145
26
7.4
28
0800
24
14.145
4010800
24
B
13.429
26
7,3
0.56
$,29
AVERAGE
15.248
27.2
1501
MINIMUM
13.429
25
6,8
789
0.56
4.29
Monthly Limit
Daily Limit
6-9
7917
DEM Form MR-1(12193)
DEQ-CFW 00063727

Facility Status: (Please check one of the following)
IHW oring data and sampling frequencies meet permit requirements
NOV 2 6 1996. Compliant
_ All monitoring data and sampling frequencies do NOT meet permit requirements
' �` �+-.t , Noncompliant
-.
RI; C3F—F-iC;�
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayberry - Site Manager
Perm' to e)
00,
n2l �/20�v.
Si i ire o er10
'* Date
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil & Grease 00951 Total Fluoride
01067
00076 Turbidity
00600
Total Nitrogen 01002 Total Arsenic
01077
00080 Color (Pt -Co)
00610
Anunonia Nitrogen
01092
00082 Color (All
00625
Total Kjeldhal 01027 Cadmium
01105
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Ilexavalent Chromium 01147
01034 Chromium
00300
Dissolved Oxygen
31616
00310
1301)5
32730
00340
COD
34235
00400
pfl
34481
00530 Total Suspended
38260
Residue
39516
00545
Settleable Matter
50050
t)0665
00720
00745
00�27
00929
ou940
'total Phosphorous
Cyanide
Total Sulfide
Total Magnesium
Total Sodium
Total Chloride
O1037 Total Cobalt
U1042 Copper
01045 Iron
O1U51 Lead
Nickel
Silver
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCBs
Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Paraineter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The rrronthly average for fecal colifonn is to Im reported as a CIsOMl.."TRIC mean. Use only units designated in the reporting
facility's permit for reporting data. C "
ID J
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the frerrnittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (U)•
DEQ-CFW 00063728

4,-
EFFLUENT=
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 006 MONTH SEPTEMBER YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Biaden
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) Aqua Tech Environmental Laboratory (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Kenneth M. Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
�
#•:EE
{-
�
v-
f•>t£
^
°
t
..
..
•.
E
E :. E E
Emmmmmmmmommm
Im
E - #
.
Monthly Limit
DEQ-CFW 00063729

Facility Status: (Please check one of the following)
ononng data and sampling frequencies meet permit requirements
NOV 2 61996 compliant
qI' t nng, data and sampling frequencies do NOT meet permit requirements
-� Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made. •
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of -the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayberry Site Manager
Permi e I s Ft
f
Signi ure of ittee " ate
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 'Turbidity
00080 Color (P(-Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BODS
00340
COD
00400
plI
00530 Total Suspended
Residue
00545
Settleable Matter
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal 01.027 Cadmium
Nitrogen
00630 Nitrates/Nitrites 01032 I lexavalent Chromium
01034 Chromium
W66.5 'Total Phosphorous
00720
Cyanide
01037 Total Cobalt
00745
Total Sulfide
01042 Copper
00927
Total Magnesium
00929
Total Sodium
01045 Iron
00940
Total Chloride
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147
Total Selenium
31616
Fecal Col i f orm
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
50060 Total
Residual
Chlorine
71890 Formaldehyde.
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The nionthly average for fecal coliforin is to be reported as a GEOME-FRIC mean. Use only units designates( in the reporting
facility's permit for reporting data. J -
* ORC must visit facility and document visitation of facility it required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the lierniitlee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063730

NPDES NO: NC 0003573 DISCHARGE NO: 002 MONTH: SEPTEMBER YEAR: 1996
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall landing
to
Downstream
DEQ-CFW 00063731

EFacility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
NOV 2 61996
j, ,& _q Qrjtj data and sampling frequencies do NOT meet permit requirements
rri
Compliant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were, prepared under my direction or
supervision in accordance with a system designed to assure that qualifitrd personnel properly gather and evaluate
the information submitted. Based on my inquiry ofthe person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. M b - Site Manager
Per rr pe /9
Signiture of Permitt Date
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 2001
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
005.50
Oil & Grease
00951
Total Fluoride
01067
Nickel
50060
Total
00076
Turbidity
00600
'Total Nitrogen
01002
'Total Arsenic
01077
Silver
Residual
00080
Color (I't-Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
1lexavalent Chromium
01147
Total Selenium
71880
Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900
Mercury
00310
BODS
W665
Total Phosphorous
32730
Total Phenolics
81551
Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pll
00745
Total Sulfide
01042
Copper
34481
Toluene
00530 Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Pararneter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is (o be repoiled as a G(30MLTRfC mean. Use only unitsAesignated in (fie reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the perinittee, delegation of signatory authority must be on file with the state per 15A NCAC 213 .0506 (b)
(2) (U)•
DEQ-CFW 00063732

•
oUPONT
DuPont Automotive
DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
October 29, 1996
NC Dept. of Environment, Health & Natural Resources
Division of Environmental Management
Central Files
DEHNR
P. 0. Box 29535
Raleigh, NC 27626-0535
Attached is the DuPont Fayetteville Works Discharge Monitoring
Report for September, 1996.
If you have any questions, please contact Robert Geddie at (910)
678-1219.
RJG:mam
Attachment
cc: M. E. Gell
R. J. Geddie
J. E. Hagle
M. G. Batton
M. E. Johnson
D. G. Sorensen
File: F-1-3-4
- ENGR, Charlotte
- FW
- FW
- FW
- FW
- FW
E. I. du Pont de Nemours and Company ® Printed on Recycled Paper
FF-9522 Rev. 5/93
DEQ-CFW 00063733

NOV 2 6 1996
I J FEE CW- CE
DEQ-CFW-00063734

EFFLUENT '' �9
NPDES PERMIT NO. INC 0003573 DISCHARGE NO. 001 MONTH AUGUST YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) ( u ton Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLT ECTINO S P Rwert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:;
ATTN: CENTRAL FILES��`
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
FLOW
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DEM Form MR -I (12/93)
DEQ-CFW 00063735

ay
l A
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements
Compliant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of die person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E. MayNrry - Site Manager•
� /sv
of Permittee**
Hwy 87 South, Fayetteville, NC 28302 [phone] U l/ May 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
I lexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530 Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147
Total Selenium
31616
Pecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MB
39516
PCBs
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
8155-Lvd60he
50050 Flow 00
Pararneter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], e
The monthly average for fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in die reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063736

{
EFFLUENT Ak4e4VW 12C f4ld
NPDES FAHIMIT NQ. NC 0003573 DISCHARGE NO. 002 MONTH AUGUST YEAR 1996
FACILITY KIAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
bIV. OF ENVIRONMENTAL MANAGEMENT (6)W c 1)/7 ��1fTc�' '2 / 0 7_ Z
DEHNR (SIGNATURE'bF 6PERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
IW.
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HRS 1
HRS
Y/N
MGD
C
UNITS
Lb/Day
MG/L
MG/L
1 108001
24
Y
14.777
27
7
2 108001
24
Y
14.777
28
7.1
<2
<25
3 108001
24
14.777
4 108001
24
14.777
5
osoo
24
Y
15.595
29
6.9
6
osoo
24
Y
15.595
29
7
478.6
7
osoo
24
Y
15.595
29
7.1
8
osoo
24
Y
15.595
29
7.1
9
osoo
24
Y
15.595
29
7.1
10108001
24
15.595
11
08001
24
15.595
12
osoo
24
Y
14.359
30
7.2
13
08001
24
1 Y
14.359
27
7.3
1305
14
08001
24
1 Y
14.359
27
7.3
15
08001
24
1 B
14.359
29
7.4
16.08001
24
Y
14.359
29
7.4
17108001
24
14.359
18
osoo
24
14.359
19
osoo
24
Y
16.233
28
7.4
20
osoo
24
Y
16.233
29
7.7
1706
21
osoo
24
Y
16.233
29
7.5
22
osoo
24
Y
16.233
29
7.4
23
08001
24
Y
16.233
29
7.4
24
osoo
24
16.233
25
osoo
24
16.233
26
osoo
24
Y
13.624
29
7.5
-'
27
osoo
24
Y
13.624
30
7.7
1004
l
28
osoo
24
Y
13.624
29
7.5
a
.
29
osoo
24
Y
13.624
27
7.9
`
30
osoo
24
Y
13.624
28
7.5
31
osoo
24
13.624
AVERAGE
14.973
28.591
1124
0
0
MAXIMUM
16.233
30
7.9
1706
<2
<25
MINIMUM
13.624
27
6.9
478.6
<2
<25
Comp. (C) Grab (G)
G
G
C
C
C
Monthly Limit
Daily Limit
I5000
DEM Form MR-1 (12/93)
DEQ-CFW 00063737

Y
r1willty stotust meaff eheoit one of the following) .�
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of die person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E. Ma berr - Site Manager
P e (Ple mt o type)
Sig ature o Penmi ee** Date
Hwy 87 South, Fayetteville, NC 28302 [phone] MaY 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen 01092 Zinc Chlorine
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium 01105 Aluminum
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Ilexavalent Chromium 01147 Total Selenium 71880 Formaldehyde
00300 Dissolved Oxygen 01034 Chromium 31616 Fecal Coliform 71900 Mercury
00310 BODS 00665 Total Phosphorous 32730 Total Phenol4rj 55,1, I�ae =
00340 COD 00720 Cyanide 01037 Total Cobalt 34235 Benzenes „
00400 pI1 00745 Total Sulfide 01042 Copper 34481 Toluene tti
00530 Total Suspended 00927 Total Magnesium 38260 MBAS
Residue 00929 Total Sodium 01045 Iron 39516 PCBs QC�- 11 1996
00545 Settleable Matter 00940 Total Chloride 01051 Lead 50050 Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], exte A"r
s YAM.tyt� S a'idF'-:7}rK"•F ~�zF�.,
The monthly average for fecal coliforrn is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063738

i
oUPONT
DuPont Automotive
NC Dept. of Environment, Health, and Natural Resources
Division of Environmental Management
Central Files
P. O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. NC0003573
Discharge Monitoring Report - August 1996
Dear Sirs:
DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
October 3, 1996
Attached is the corrected August 1996 Discharge Monitoring Report for the DuPont -Fayetteville
Works' Outfall 002. This DMR should replace the incorrect report for Outfall 002, which was
submitted on September 30, 1996. All other information in the September 30th submittal is
correct and should not be changed.
The error on the original report was caused by a data entry in the software program which
generates the DMR. The Outfall 002 flow measurement entries were inadvertently off by one
week throughout the report, resulting in incorrect fluoride mass discharge determinations and
incorrect Outfall 002 flow indications. The error has been corrected in the attached report.
All monitoring data and sampling frequencies were compliant with permit requirements.
If you have any questions regarding this matter, please feel free to call me at [phone].
Attachment
cc: Ms. Kitty Kramer, Fayetteville Regional Office
Michael E. Johnson
Environmental Coordinator
E. I. du Pont de Nemours and Company
® Printed on Recycled Paper
FF-9522 Rev 5/93
DEQ-CFW 00063739

�4vk
r
F 996
FILM
DEQ-CFW 00063740

EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH AUGUST YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
,CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
RALEIGH, NC 27626-0535
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
w
i= Y
$
O
=
O
M
y
O
O
50050
00010
00400
00951
00310
00340
FLOW
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¢ y
W W
2 V
UJI
=
G.
w
7
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v
N
C
o0
c
V
EFF X
INF
J F
HRS 1
RS
Y/N
MGD
'C
UNITS
Lb/Day
MG/L
MG/L
1 108001
24
Y
15.595
27
7
2 108001
24
Y
15.595
28
7.1
<2
<25
3 108001
24
15.595
4 108001
24
15.595
5 108001
24
Y
14.359
29
6.9
6
0800
24
Y
14.359
29
7
440.7
7
o800
24
Y
14.359
29
7.1
8
o800
24
Y
14.359
29
7.1
9
o800
24
Y
14.359
29
7.1
10
o800
24
14.359
11108001
24
14.359
12108001
24
Y
16.236
30
7.2
13108001
24
1 Y
16.236
27
7.3
1476
14108001
24
1 Y
16.236
27
7.3
15
08001
24
1 B
16.236
29
7.4
16
08001
24
Y
16.236
29
7.4
17
0800
24
16.236
18
08001
24
16.236
19
08001
24
Y
13.622
28
7.4
20
o800
24
Y
13.622
29
7.7
1431
21
0800
24
Y
13.622
29
7.5
22
o800
24
Y
13.622
29
7.4
23
o800
24
Y
13.622
29
7.4
24
o800
24
13.622
25108001
24
13.622
26108001
24
Y
14.650
29
7.5
27108001
24
Y
14.650
30
7.7
1080
28
08001
24
Y
14.650
29
7.5
29
0800
24
Y
14.650
27
7.9
30
0800
24
Y
14.650
28
7.5
31
0800
24
14.650
AVERAGE
14.832
28.591
1107
0
0
MAXIMUM
16.236
30
7.9
1476
<2
<25
MINIMUM
13.622
27
6.9
440.71
<2
<25
Comp. (C) Grab (G)
G
G
C
C
C
Monthly Limit
Daily Limit
1
5000
DEM Form MR-1 (12/93)
DEQ-CFW 00063741

Y
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E. Ma berr — Site Manager
Pe ittee (Plea a pr )
Signature of Permittee** ate
Hwy 87 South, Fayetteville, NC 28302 [phone] May 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951
Total Fluoride
00076 Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300 Dissolved Oxygen
01034
Chromium
00313 &- )�
00665
Total Phosphorous
00340 CC
00720
Cyanide
01037
Total Cobalt
00400 e:i-.
00745
Total Sulfide
01042
Copper
00530 Total Suspender:
0007-7
'., otal Magnesium
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
50060 Total
Residual
Chlorine
01147 Total Selenium 71880o aldehyde
31616 Fecal Coliform ., %r ry
32730 To Phe q j44
34235 Ben
34481 Tolue 1g96
38260 MBA
Residue 0 : Total Sodium 01045 Iron 39516 PCBs
00545 Settleable Matter 00940 Total Chloride 01051 Lead 50050 Flow N 'f��'�`\►�S
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], �iuteiis vn 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5)IB).
** U igned by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
DEQ-CFW 00063742

3
EFFLUENT
NPDES PERMIT NO. NC 0003573
DISCHARGE NO. 001 MONTH JULY
YEAR
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY
Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC)
Robert J. Geddie GRADE 4 PHONE
[phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC)
(2) Burlington Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S),COLLECTING SAMPLES Robert J. Geddie ! K. Mark Hall
Mail ORIGINAL and ONE COPY to:
V
'
ATTN: CENTRAL FILES
-DIV.
}
4?61f�J6j-
OF ENVIRONMENTAL MANAGEMENT
X
DEHNR ;'
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
'16AT "
P.O BOX 29535
BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535
...� ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
CO)
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UNITS
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1.148
27
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24
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104.3
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.:.:.:.:.:.:.:..:.:.:.:.:.:.:..:.:.:.:.:.:.:.::.:.:.:.:.:.:.::.:.:.:.:.:.:.:..;.;.;.;.;.;
28
o800l
24 1
0.687
.........................................................::::::..........
2........
..
::::::::
tI,89::::.::.::::3?[{91
.
�
30
o800
24
Y
0.743
28
7.5
264.6
55.8
77777
AVERAGE
0.662
27.4
68.3
99.9
24.5
0.5
0
1hFI� XI�M111fA:::::�:::.p�:qq.pp.:::;;:s/.�y.nn.:::::
�':::::.:}•!.......:M!..........:.:..:.:.�
s:4.!tD..:..:.:.!F3;.:.
:,:,;g:�}:�q(:::ss�}�T:
.,:. �,xi!.:.::.k??;
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:::::::::::::::::
:.:.::?y+i:.:.:
;.;.;.;.;.;.;.;..;.;.;.;.;.•
MINIMUM
0.000
26
7.4
<18.3
55.8
24.5
0.5
<5
Monthly Limit
2.0
175.4
292.3
PASS
Daily Limit
1
6-9
467.7 1
950.1
DEM Form MR -I (12/93)
FAYETTEVILLE REG, OFFICE`
.�-
DEQ-CFW 00063743

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet ps rrftit requirements
r
Compliant
Noncompliant
1.
°.v
If the facility is noncompliant, please comment on corrective actions being;Aenp res otequipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E. Maybkr} y - Si
Signature of Permittee**
87 South, Fayetteville, NC 28302 [phone]
Address
Phone Number
PARAMETER CODES
00010
Temperature
00556
Oil & Grease 00951 Total Fluoride
00076
Turbidity
00600
Total Nitrogen 01002 Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal 01027 Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites 01032 l lexavalent Chromium
00300 Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530 Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Date
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147
Total Selenium
31616
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at (919)
lay 1996
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
_extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units d3jl ,ked in the reporting
facility's permit for reporting data. �" -
* ORC must visit facility tand document visitation of facility as required per 15A NCAC 8A .0202 i ) (B)•
** If signed by other than the pennittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063744

' 4
EFFLUENT
AM!' SEP 181996
NPDES PERMIT NO. NC 0003573
DISCHARGE NO.
002 MONTH
JULY YEAR 1996
FACILITY NAME DuPont - Fayetteville Works
CLASS 3
COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie
GRADE
4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC)
(2) Burlington
Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES
Robert J. Geddie I K. Mark Hall
1
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O BOX 29535
RALEIGH, NC 27626-0535
(SIGNATURE OF OPERAT R IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
a -kb ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
Q
p
1= Y
'e chi
ag
ii N
4)
0
or
E
°
0
M
e
o
a
O
50050
00010 1
00400
00951
1 00310
00340
FLOW
y
¢
Ww
2 V
F
a
wo
O
U.
a
y
p
m
OO
Q
EFF X
INF
J
a
HRS
1 HRS
Y/N
MGD
CI
UNITS
Lb/Day
MG/L
MG/L
1
0800
24
Y
17.391
33
7.3
2
08001
24
B
17.391
32
7.3
1566
3
08001
24
1 Y
17.391
30
7.4
4
08001
24
B
17.391
31
7.8
5
08001
24
17.391
30
7.4
6
08001
24
17.391
7
108001
24
17.391
8
08001
24
Y
15.145
31
7.3
9
08001
24
1 Y
15.145
33
7.3
1503
10
08001
24
Y
15.145
29
7
11
08001
24
Y
15.145
28
7.3
12
08001
24
Y
15.145
28
7.3
13
08001
24
15.145
14
08001
24
15.145
15
08001
24
Y
1 10.454
30
7.7
16
08001
24
Y
10.454
17
08001
24
Y
10.454
18
08001
24
Y
0
19
osoo
1 24
Y
0
20
0800
24
10.454
21
osoo
24
10.454
22
osoo
24
Y
15.441
28
7.5
23
o800
24
Y
15.441
28
7.2
749.5
24
osoo
24
Y
15.441
28
7.2
25losool
24
Y
15.441
28
7.1
26
0800
24
Y
15.441
27
7.2
27
osoo
24
15.441
28
0800
24
15.441
29
osoo
24
Y
14.777
28
7.1
30
osoo
24
Y
14.777
30
7.2
253.9
31108001
24
Y
14.777
30
7.1
AVERAGE
13.950
29.579
1018
MAXIMUM
17.391
33
7.8
1566
MINIMUM
0.000
27
7
253.9
Comp. (C) Grab (G)
G
G
C
C
C
Monthly Limit
Daily Limit
5000
DEM Form MR-1 (12193)
DEQ-CFW 00063745

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meevrfmit requirements
Noncompliant
E -
If the facility is noncompliant, please comment on corrective actions being take in raspece o•equiment, operation, maintenance, w
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, we, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayberry -Rite Manager
Signature of Pdrmi*e**
t)wv 87 South, Fayetteville, NC 28302 (910)678-140
Address
Phone Number
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
Nickel
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
00080
00082
Color (Pt -Co)
Color (ADMI)
00610
00625
Ammonia Nitrogen
Total Kjeldhal 01027
Cadmium
01092
01105
Zinc
Aluminum
00095
Conductivity
00630
Nitrogen
Nitrates/Nitrites
01032
l lexavalent Chromium
01147
Total Selenium
00300
Dissolved Oxygen
01034
Chromium
31616
32730
Fecal Coliform
Total Phenolics
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530 Total Suspended
00927
Total Magnesium
38260
39516
MBAS
PCBs
Residue
00929
Total Sodium
01045
Iron
50050
Flow
00545
Settleable Matter
00940
Total Chloride
01051
Lead
lay 1996
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyd
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data. ��,�`'
* ORC must visit facility !and document visitation of facility as required per 15A NCAC 8A .0202 (b) (J)\(B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213 .0506 (b)
(2) (D)•
DEQ-CFW 00063746

NPDES PERMIT NO. NC0003573 OUTFALL 001 JULY, 1996
DUPONT - FAYETTEVILLE WORKS PAGE 1 OF 2
Effluenf Characteristic
Monthly
Average
Limit
(lb/da)
Daily
Maximum
Limit
(lb/day)
Outfall
001
Discharge
(lb/day)
Method
Detection
Limit
(u /L)
Acena hthene
0.16
0.43
0
10
Acr lonitrile
0.70
1.77
0
5
Benzene
0.27
0.99
0
5
Carbon Tetrachloride
0.13
0.28
0
5
Chlorobenzene
0.11
0.20
0
6
1,2,4-Trichlorobenzene
0.50
1.02
0
10
Hexachlorobenzene
0.11
0.20
0
10
1,2-Dichloroethane
0.50
1.54
0
5
1, 1, 1 -Trichloroethane
0.15
0.39
0
5
Hexachloroethane
0.15
0.39
0
10
1,1-Dichloroethane
0.16
0.43
0
5
1,1,2-Trichloroethane
0.15
0.39
0
5
Chloroethane
0.76
1.96
0
10
Chloroform
0.15
0.34
0
5
2-Chloro henol
0.23
0.72
0
10
1,2-Dichlorobenzene
0.56
1.19
0
10
1,3-Dichlorobenzene
0.23
0.32
0
10
1,4-Dichlorobenzene
0.11
0.20
0
10
1,1-Dichloroeth lene
0.12
0.18
0
5
1,2-trans-Dichloroeth lene
0.15
0.39
0
5
2,4-Dichloro henol
0.29
0.82
0
10
1,2-Dichloro ro ane
1.12
1.68
0
6
1,3-Dichloropropylene
0.21
0.32
0
5
2,4-Dimeth 1 henol
0.13
0.26
0
10
2,4-Dinitrotoluene
0.83
2.08
0
10
2,6-Dinitrotoluene
1.86
4.68
0
10
Eth lbenzene
0.23
0.79
0
8
Fluoranthene
0.18
0.50
0
10
Methylene Chloride
0.29
0.65
0
5
Methyl Chloride
0.63
1.39
0
10
Hexachlorobutadiene
0.15
0.36
0
10
Naphthalene
0.16
0.43
0
10
Nitrobenzene
0.20
0.50
0
10
DEQ-CFW 00063747

DEQ-CFW 00063748

NPDES PERMIT NO. NC0003573 OUTFALL 001 JULY, 1996
DUPONT - FAYETTEVILLE WORKS PAGE 2 OF 2
Effluent Characteristic
Monthly
Average
Limit
(lb/day)
Daily
Maximum
Limit
(lb/day)
Outfall
001
Discharge
(lb/day)
Method
Detection
Limit
(u /L)
2-Nitrophenol
0.30
0.50
0
10
4-Nitrophenol
0.53
0.91
0
50
2,4-Dinitro henol
0.52
0.90
0
50
4,6-Dinitro-o-cresol
0.57
2.02
0
50
Phenol
0.11
0.19
0
10
Bis(2-eth lhex 1) hthalate
0.75
2.04
0
10
Di-n-but 1 phthalate
0.20
0.42
0
10
Diethyl phthalate
0.59
1.48
0
10
Dimeth 1 phthalate
0.14
0.34
0
10
Benzo(a)anthracene
0.16
0.43
0
10
Benzo(a)pyrene
0.17
0.45
0
10
3,4-Benzofluoranthene
0.17
0.45
0
10
Benzo(k)fluoranthene
0.16
0.43
0
10
Chrysene
0.16
0.43
0
10
Acena hth lene
0.16
0.43
0
10
Anthracene
0.16
0.43
0
10
Fluorene
0.16
0.43
0
10
Phenanthrene
0.16
0.43
0
10
P rene
0.18
0.49
0
10
Tetrachloroeth lene
0.16
0.41
0
5
Toluene
0.19
0.58
0
6
Trichloroeth lene
0.15
0.39
0
5
Vinyl Chloride
0.76
1.96
0
10
Total PAH's
n/a +-57.0
µg/L
<10 µg/L
10
DEQ-CFW 00063749

DEQ-CFW-00063750

Z-544 REV 10/89 a
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
August 27, 1996
NC Dept. of Environment, Health & Natural Resources
Division of Environmental Management
Central Files
P. 0. Box 29535
Raleigh, NC 27626-0535
Attached is the DuPont Fayetteville Works Discharge Monitoring
Report for July, 1996.
If you have any questions, please contact Robert Geddie at (910)
678-1219.
RJG:mam
Attachment
cc: M. E. Gell
R. J. Geddie
J. E. Hagle
M. G. Batton
M. E. Johnson
D. G. Sorensen
File: F-1-3-4
- ENGR, Charlotte
- FW
- FW
- FW
- FW
- FW
Better Things for Better Living
DEQ-CFW 00063751

DEQ-CFW-00063752

F ; EFFLUENT
NPDE3 PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH JULY YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED u PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mafk Hall
Mail ORIGINAL and ONE COPY to:
ATI-N: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.0 BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
w�
i= Y
N
O
N
=
E
C
O
cc
O
50050
00010
00400
00951 1
00310
00340
FLOW
W
y
w W
2 V
H
na
LU
M
0
U.
a
cmo
to
m
c�
EFF X
INF
} W
a Q
G
HRS
HRS
Y/N
MG
CI
UNITS
Lb/Day
MG/L
MG/L
1 108001
24
Y 1
17.391
33
7.3
2
osoo
24
B
17.391
32
7.3
1566
3
osoo
24
Y
17.391
30
7.4
4
osoo
24
B
17.391
31
7.8
5
osoo
24
17.391
30
7.4
6
080o
24
17.391
7 108001
24
17.391
8 losool
24
Y
15.145
31
7.3
9 JoBool
24
Y
15.145
33
7.3
1503
10
08001
24
Y
15.145
29
7
11
osoo
24
Y
15.145
28
7.3
12
osoo
24
Y
15.145
28
7.3
13
osoo
24
15.145
14
osoo
24
15.145
15
osoo
24
Y
10.454
30
7.7
16108001
24
Y
10.454
17108001
24
Y
10.454
18108001
24
Y
0
19
osoo
24
Y
0
20
osoo
24
10.454
21
osoo
24
10.454
22
osoo
24
Y
15.441
28
7.5
23
osoo
24
Y
15.441
28
7.2
749.5
24
osoo
24
Y
15.441
28
7.2
25
osoo
24
Y
15.441
28
7.1
26
osoo
24
Y
15.441
27
7.2
27
osoo
24
15.441
28
osoo
24
15.441
29
o800l
24
Y
14.777
28
7.1
30108001
24
Y
14.777
30
7.2
253.9
31108001
24
1 Y
14.777
30
7.1
AVERAGE
13.950
29.579
1018
MAXIMUM
17.391
33
7.8
1566
MINIMUM
0.000
27
7
253.9
Comp. (C) Grab (G)
G
G
C
C
C
-A 11
Monthly Limit
774�I
Daily Limit
5000
f
DEM Form MR-1 (12193) e4
DEQ-CFW 00063753

Facility Status: (Please check one of the following) 1,
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made. _ i
f
&V2-
"I-certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Michael E.
Permittee
Signature of Permlittee"
Hwy 87 South, Fayetteville, NC 28302 [phone]
Permittee Address Phone Number
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951
Total Fluoride
00076 Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032
1lexavalent Chromium
00300 Dissolved Oxygen
01034
Chromium
00310 BOD5
00665
Total Phosphorous
00340 COD
00720
Cyanide
01037
Total Cobalt
00400 pH
00745
Total Sulfide
01042
Copper
00530 Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545 Settleable Matter
00940
Total Chloride
01051
Lead
—Site Ma
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34491 Toluene
38260 MBAS
39516 PCBs
50050 Flow
lay 1996
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
f5
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .( 0211(b)
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063754

' DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
aUPONT
DuPont Automotive
August 30, 1996
Ms. Kitty Kramer
NC DEHNR - Division of Environmental Management
Water Quality Section
Wachovia Bldg. - Suite 714
Fayetteville, NC 28301
RE: NPDES Permit No. NC0003573
Dear Ms. Kramer:
Upon reviewing the July 1996 Discharge Monitoring Report, it has come to our attention that the
weekly monitoring of Fluoride at Outfall 002 was not conducted for the week of July 15th.
The entire site was in the midst of our annual shutdown, and the river water pumps were
shutdown during the early morning of July 17th, which would have been the end of the normal
composite sampling period for July 16th. Our Wastewater Treatment Operator failed to realize
that there was flow at Outfall 002 throughout the 24-hour period of the July 16th sample date,
and that the composite sampler could have and should have been sampled.
Because the Nafion® manufacturing division had been shutdown for several days prior to the
missed sample date, we are confident that the fluoride mass discharge was well below our
permitted limit, if not below the analytical detetion limit.
A revised Outfall 002 DMR (copy attached) is being submitted to the DEHNR Central Files to
reflect we were non -compliant with regard to the required monitoring frequency.
If you should have any questions, please feel free to call me at 678-1155.
cc: DEHNR Central Files, Raleigh
Michael E. Johnson
Environmental Coordinator
E. I, du Pont de Nemours and Company
® Printed on Recycled Paper
FF-9522 Rev 5/93
DEQ-CFW 00063755

DEQ-CFW 00063756

EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH JUNE YEAR9� 6,
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone] .,
CERTIFIED LABORATORIES (1) IEA (Cary, NC (2) Burlington Research
_CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR VI 5 2. (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 • BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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0.927
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24.5
119.7
36.9
4.52
0
88
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7::'.:
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MINIMUM
0.417
23
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Monthly Limit
2.0
175.4
292.3
PASS
Daily Limit
6-9
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950.1
DEM Form MR-1 (12/93)
DEQ-CFW 00063757

e ,s
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements u
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment'bWration, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of 'my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
HWY. 87 SOUTH, DUART, NC [phone] `/ MAY 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
Nickel
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
00310
BODS
00665
Total Phosphorous
32730
Total Phenolics
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
plf
00745
Total Sulfide
01042
Copper
34481
Toluene
00530 Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assistance
may obtained by calling the Water
Quality Compliance Group at (919)
733-5083�
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designat6 n the reporting
facility's permit for reporting data. _,
* kP
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b),(B).
-o
t Via.
**If signed by other than the permittee, delegation of signatory authority must be on file with the state pt�fiSA W g 6 (b)
(2) (D)•
DEQ-CFW 00063758

AUG 1 2 1996
EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH JUNE YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to: -' e Cj
ATTN: CENTRAL FILES
D V OF ENVIRONMENTAL MANAGEMENT X ��`/�'�
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
ill.'��®��ilil®IIII�®i®illlllllll����ililiiliiii•illlllllll�IIIIIIIIII�lilililil�iiililili�
DEM Form MR -I (12193)
DEQ-CFW 00063759

N
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet perr3ut requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and -evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of 'my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
MICHAEL E. MAYMWY
"ttee lease prin )
igna re of Permittee** ate
HWY. 87 SOUTH DUART NC [phone] MAY 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
Nickel
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530 Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assistance
may obtained by calling the Water Quality Compliance Group at [phone], ei
t
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
1 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units dWi ate4�ip the`c poiting
facility's permit for reporting data. iv—% r `s
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (B). tp
** If signed by other than the permittee, delegation of signatory authority must be on file with the state p 5A A&C 6 (b)
(2) (D)•
}
DEQ-CFW 00063760

DEQ-CFW 00063761

JUj
EFFLUENT
40J
h NPDES PERMIT NO. NC 0003573
DISCHARGE NO.
001 MONTH JUNE
YEAR 199C
FACILITY NAME DuPont - Fayetteville Works
CLASS 3 COUNTY
Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie
GRADE 4 PHONE
910 678-1219
CERTIFIED LABORATORIES (1) IEA (Cary, NC)
(2) Burlington Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
r
u
'/f`S✓/iC�
Ar Y.)
- DIV. OF ENVIRONMENTAL MANAGEMENT
X
DEHNR
(SIGNATURE OF OPER
IBLE CHARGE)
ItVIOT
DATE
BOX 29535
BY THIS SIGNATURE, IREPORT IS
EP.O
OF MY KNOWLEDGE
y�
M T -1
RALEIGH, NC 27626-0535
ACCURATE AND COMPLETE
TO THE BEST
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DEM Form MR-1 (12193)
DEQ-CFW 00063762

OF
Facility Status: (Please check one of the following)
LiT,
All monitoring data and sampling frequencies meet permit requirements
Compliant
rAbG 13 1596
All monitoring data and sampling frequencies do NOT meet permit requirements
ENV. MANAt�`�ilf;�li Noncompliant
FAYETTEViLLE REG. Ui`r Cr
If the facility iS nottcoippliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for itnptovements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false inforl tion, including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayb - Site anager•
Per le prin
ign re of Pernuttee** JV V() ate
Hwy 87 South, Fayetteville, NC 28302 [phone] May 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010
Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
Nickel
50060
Total
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
tlexavalent Chromium
01147
Total Selenium
71880
Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
11616
Fecal Coliform
71900
Mercury
00310
BOD5
00665
Total Phosphorous
30
Total Phenolics
81551
Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter rode assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly :Ege for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's pry - iur reporting data.
* ORC must visit facility and document visitation of facility as required 061�115A NCA+ 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signal,)ry authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063763

JUL 25199%
" EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH JUNE YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
y CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES 0 - ,_ / /
DIV. OF ENVIRONMENTAL MANAGEMENT X U
GG� 7
DEHNR (SIGNATURE OF OPERATOR I RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNITURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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23
Monthly Limit
2.0
Daily Limit
DEM Form MR4 (12193)
M
' . ,
&w"f
-
e
PASS
DEQ-CFW 00063764

Facility Status: (Please check one of the following)
BIC
All monitoring data and sampling frequencies meet permit requirements
'1 Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
ENV. MANAGEI\"ENT Noncompliant
`FAYETTEVILLE REG. OFFICE
s ,
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false infor, tion, including the possibility of fines and imprisonment for knowing violations."
Michael E. Maybe-ry - Site Mana
of Permittee" % I I Date
Hwy 87 South, Fayetteville, NC 28302 [phone] U May 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951
Total Fluoride
01067
Nickel
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
01077
Silver
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
1lexavalent Chromium
01147
Total Selenium
00300
Dissolved Oxygen
01034
Chromium
11616
Fecal Coliform
00310
11OD5
00665
Total Phosphorous
J0
Total Phenolics
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
p1l
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCBs
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Paramel—''ode assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly -1ge for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's p­ or reporting data.
* ORC must visit facility and document visitation of facility as required per 15AEN1, AC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of sign-wy authority must be on file with; the state per 15A NCAC 2B .0506 (b)
(2) (D)• '
DEQ-CFW 00063765

PI Or
r EFFLUENT JUN `Z l �J9A'�►
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH MAY YEAR
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddi k Hall
Malt ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES // '
DN. OF ENVIRONMENTAL MANAGEMENT X Gr/
DEHNR (SIGNATURE OF OPERATOR I RESPONSIBLE CHARGE) DATE
P.O BOX 29535 j BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-MS ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DEM Form MR4 (12193)
DEQ-CFW 00063766

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements Ea
t
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, of those persons directly responsible for gathering the information, the
information submitted is, to the best of -my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
HWY. 87 SOUTH, DUART, NC [phone] Cl/ MAY 31, 1996
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00676
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pff
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556
Oil & Grease
00951
Total Fluoride
00600
Total Nitrogen
01002
Total Arsenic
00610
Ammonia Nitrogen
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01034
Chromium
00665
Total Phosphorous
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
50060 Total
Residual
Chlorine
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
32730 Total Phenolics 81551 Xylene
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00745
Total Sulfide
01042
Copper
34481
Toluene
00927
Total Magnesium
38260
MBAS
00929
Total Sodium
01045
Iron
39516
PCBs
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063767

EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH MAY YEAR 19W
FACILITY NAME DuPont - Fayetteville Works CLASS 3 couNTY Bladen
- OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC (2) Burlington Research
,-CHECK BOX IF ORC HAS CHARRED PERSON(S) COLLECTING SAMPLES Robert J. Geddle / K. Mark Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.0 BOX 29535
RALEIGH, NC 27625-0636
X /C=Cx-
(SIGNATURE OF
IN RESPONSIBLE CHARGE)
BYTHIS SIGNATURE, i CERTIFY THATTHE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DATE
�••=�'
•t• •
•• ••Sri
•!-no
•tL •
••C '•
r
-
mm
DEQ-CFW 00063768

Facility Status: (Please check one of the following) ;
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
HWY. 87 SOUTH, DUART, NC
Permittee Address
00010
Temperature
00676
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 plf
00530 Total Suspended
Residue
00545 Settleable Matter
MICHAEL E.
of Pernfitted**
(910) 678-14
Phone Number
PARAMETER CODES
00556
Oil & Grease
00951
Total Fluoride
00600
Total Nitrogen
01002
Total Arsenic
00610
Ammonia Nitrogen
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01034
Chromium
00665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147
Total Selenium
31616
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
MAY 31, 1996
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063769

Industrial & Environmental Analysts, Inc. (IEA)
GC/MS BASE/NEUTRAL EXTRACTABLES EPA 625 COMPOUND LIST
IEA Project
Number: 2101-181
IEA Sample Number: 9605361-02
Date Received:
05/15/96
Client Name:
Dupont
Date Sampled:
05/15/96
Client Project ID: LFN-182117 Waste
Water Sample Date Extracted:
05/20/96
Sample Identification:
E60514
Date Analyzed:
05/24/96
Matrix:
Water
Analysis By:
Dixon
Dilution Factor:
1.0
Quantitation
Results
Limit Concentration
Number
Compound
(ug/L)
(ug/L)
1
Acenaphthene
10
BQL
2
Acenaphthylene
10
BQL
3
Anthracene
10
BQL
4
Benzo(a)anthracene
10
BQL
5
Benzo(a)pyrene
10
BQL
6
Benzo(b)fluoranthene
10
BQL
7
Benzo(g,h,i)perylene
10
BQL
8
Benzo(k)fluoranthene
10
BQL
9
bis(2-Chloroethoxy)methane
10
BQL
10
bis(2-Chloroethyl)ether
10
BQL
11
bis(2-Chloroisopropyl)ether
10
BQL
12
bis(2-Ethylhexyl)phthalate
10
13
4-Bromophenyl phenyl ether
10
BQL
14
Benzyl butyl phthalate
10
BQL
15
2-Chloronaphthalene
10
BQL
16
4-Chlorophenyl phenyl ether
10
BQL
17
Chrysene
10
BQL
18
Dibenzo(a,h)anthracene
10
BQL
19
1,2-Dichlorobenzene
10
BQL
20
1,3-Dichlorobenzene
10
BQL
21
1,4-Dichlorobenzene
10
BQL
22
3,31-Dichlorobenzidine
10
BQL
23
Diethyl phthalate
10
BQL
24
Dimethyl phthalate
10
BQL
25
Di-n-butylphthalate
10
BQL
26
2,4-Dinitrotoluene
10
BQL
27
2,6-Dinitrotoluene
10
BQL
28
Di-n-octylphthalate
10
BQL
29
Fluoranthene
10
BQL
30
Fluorene
10
BQL
31
Hexachlorobenzene
10
BQL
32
Hexachlorobutadiene
10
BQL
33
Hexachlorocyclopentadiene (3)
10
BQL
34
Hexachloroethane
10
BQL
35
Indeno(1,2,3-cd)pyrene
10
BQL
36
Isophorone
10
BQL
37
Naphthalene
10
BQL
FORM 625B (1) Rev. 081792
DEQ-CFW 00063770

DEQ-CFW-00063771

i
Industrial
& Environmental Analysts,
Inc. (IEA)
GC/MS BASE/NEUTRAL EXTRACTABLES EPA 625
COMPOUND LIST
IEA Project Number:
2101-181
IEA Sample Number:
9605361-02
Date Received:
05/15/96
Client Name:
Dupont
Date Sampled:
05/15/96
Client Project ID:
LFN-182117 Waste Water
Sample Date Extracted:
05/20/96
Sample Identification:
B60514
Date Analyzed:
05/24/96
Matrix:
Water
Analysis By:
Dixon
Dilution Factor:
1.0
Number Compound
Quantitation Results
Limit Concentration
(ug/L) (ug/L)
38
Nitrobenzene
10
BQL
39
N-Nitroso-di-n-propylamine
10
BQL
40
N-Nitrosodiphenylamine (1)
10
BQL
41
Phenanthrene
10
BQL
42
Pyrene
10
BQL
43
1,2,4-Trichlorobenzene
10
BQL
44
Benzidine
45
N-Nitrosodimethylamine
10
BQL
Comments:
*This compound is no longer provided as a normal target deliverable for
Method 625. Please contact your account representative for further
information.
Sample specific quantitation limits may be calculated by multiplying
the quantitation limit by the dilution factor.
(1) Cannot be separated from Diphenylamine
(3) Hexachlorocyclopentadiene does not recover by this method.
BQL = Below Quantitation Limit
FORM 625B (2) Rev. 081792
DEQ-CFW 00063772

EFFLUENT AM, MAY 2 p Epp
NPDES 15ERMIT NO. NC OW3573 DISCHARGE NO. 001 MONTH APRIL YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) lEA (Cary, ND(2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29M BY THIS SIGNAURE, I CERTIFY THAT THE REPORT IS
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DEM Form MR4 (12193)
DEQ-CFW 00063773

Facility Status: (Please check one of the'foliowing)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements 0
Noncompliant
If the facility is noncompliant please comment on corrective actions being taken in respect to equipment;: operation,
maintenance, etc., and a time table for improvements to be made.
t certify, under penalty of law, that this document and all attachments.were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel prop6dy.gather and evaluate
the information submitted, Basedon my.inquiryof the :person or persons who manage the system, or those
persons Wrectly responsible for. gathering. the information, the `information is, to the best of my_knowledge and belief,
true,. accurate, .and complete. I am aware that there are.significant penalties for submitting. false information,
including the possibility of fines andimprisonmentfor.knowing violations."
Michael E. Mayberry Site .Manager
Pe ittee (Ple r-ty e)
Si iture of P rrrt► ee*" _ Date
NC Hwy 87 South, Fayetteville, NC. 24306 91 678-14Q0_ May. 31, 1996
Permittee Address Phone'Number, Permit Exp. Date
PARAMETER CODES
DEQ-CFW 00063774

�1���
EFFLUENT MAY 2019r
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH APRIL YEAR 1996
FACILITY NAME DuPont - FayettevlHe Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
-DIV. OF ENVIRONMENTAL MANAGEMENT X /�- C�
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 296M BY THIS SIGNATURE, I CERTIFY THATTHE REPORT IS
RALEIGH, NC 276264M ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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DEM Forth MR4 (12193)
DEQ-CFW 00063775

Facility Status: (Please check one of the following)
Al[ monitoring data and sampling frequencies, meet permit -requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
- Noncompliant
If the facility is noncompliant,'please comment on corrective actions being: taken in respect=to equipment, operation,
maintenance, etc., and a time table for improvements to be made. .
"I certify, under penalty -of law, that this document and all attachments were -prepared under ray direction or
supervision in accordance'with a system designed to assure that qualified personnel:properly gather, and evaluate
the informatlon submitted. Based on my inquiry of the person' or persons who manage the system,, or those
persons'directly responsible for gathering the information, the'inforn ation is, to the best of my knoy4edge and belief,
true; accurate; and complete..•I am aware that triere are Significant penalties for submittii' g falseinformation;
including the possibility of fines and imprisonment for knowing violations."
Mich Lei E. Ma Site Manager
P Mee (Pleas. ype) :.
_ Si niture of.Permittee" _ ate
NO Hwy 87 South; Fayetteville, NC; 28306 [phone] May, 31, 1996 ::
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
,
DEQ-CFW 00063776

,jr- Z�
EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 001 MONTH APRIL YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA Ca (2) Burlington Research
-CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddiei }- , Marcus Hall
t:
Mail ORIGINAL and ONE COPY to:
,.ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X ��L �✓'.�C G���tr S �.:� /f��j
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) BATE
P.O BOX 28535 BY THIS SIGNAURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NO 27626-05M ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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DEM Form MR4 (12193)
DEQ-CFW 00063777

n-,
Facility Status: (Please check one of the following).
All monitoring data and sampling frequencies meet permit requirements CJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law,' that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly -gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system,. or those
persons directly responsible for gathering the information, the information is, to the, best of my knowledge and belief,
true, accurate, and complete. I am aware that there are. signifcant.penalties for submitting false information,
including the possibility of fines and, imprisonment for knowing violations."
Michael E. Mayberry - Manager .
RO(nittee (Please p
1/6
Si niture of Permitte at
NC Hwy47 South,* Fayetteville, NC, 28306 (910)-678-140E1 - May 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES `"
DEQ-CFW 00063778

'F
EFFLUENT
NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH APRIL YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
-CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie f K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
,ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT X
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-035 ACCURATE AND COMPLETE TO THE KST OF MY KNOWLEDGE
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DEM Form MR41(12193)
DEQ-CFW 00063779

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements 0
Noncompliant
If the facility is noncompliant; please comment on corrective actions being taken in respect to equipment,' operatid'n,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the informationsubmitted. Based on my inquiry of the.person or persons who manage the system,_ or those
persons directly. responsible, for gathering the information, the information is, -to the pest of my knowledge and belief_,
true, accurate, -and complete.- I am aware that there are significant.penalties for submitting.false."information,
Including the possibNity of fines and imprisonment for knowing violations." .
- - Michael E. Mayberry Site manager
P ittee (Pleas t r type)
** Si 9 � iture of rmittee Date(
(._. _..
NC Hwy 87 South, Fayetteville, NC, 28366 [phone] May-31, 1996
Permittee Address Phone Number ;Permit Exp.' Date' "
PARAMETER CODES
DEQ-CFW 00063780

EFFLUENT
NPDES PERMIT NO, INC 0003573 DISCHARGE NO. 001 MONTH MARCH YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert I Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED L—J PERSON(S) COLLECTING SAMPLES Robe e / K. Marcus Hall
Mail ORIGINAL and ONE COPY to: t`{
ATTN: CENTRAL FILES ,/ /(� Y G� WJ 41/-Z /41,;57
DIV. OF ENVIRONMENTAL MANAGEMENT X G // / c•
DEHNR
P.O BOX 29535 r
RALEIGH, NO 27626-0535
a
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DATE
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DEM Form MR4 (12193)
DEQ-CFW 00063781

41
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements l
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant `
If the facility is noncompliant, please comment on corrective actions being taken in respect to, equipment, operation,
maintenance, etc., and a time table for improvements to be lnade.
"I certify; under penalty of law, that this document .and aU attachments were. prepared under my direction or
supervision in accordance with a system designed to. assure thatqualified personnel properly gather and evaluate
the information submitted. Based on my inqur of -the person or persons who manage the system, .or those
'ry pe pe y e
persons directly responsible for gathering the information; the information is, to the best: of my knowledge and belief,
true, accurate, and complete. I am aware that there are -significant penalties for submitting false information,
including the possibility of fines and imprisonment -for knowing violations."
Michael E. Mayberry.. - SeLManager
P ee lease print pe
ign• re,of Pe ittee** U61, o
NC Hwy 87 South, Fayetteville, NC, 28306 . (910) :678-1400 May 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER .CODES '
DEQ-CFW 00063782

k1AY 0619�r
EFFLUENT
NPDES PERMIT NO. NC 0003573
DISCHARGE NO. 002 MONTH
MARCH
YEAR 1996
FACILITY NAME DuPont - Fayetteville Works
CLASS 3
couNTY
Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE
4 PHONE
[phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC)
(2) Burlington
Research
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES
Robert J. Geddie / K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
��� / A,
�'
�(�
D OF ENVIRONMENTAL MANAGEMENT
X ✓" ' •
-�
DEHNR
(SIGNATURE OF OPERATOR RESPONSIBLE CHARGE)
DATE
P.O BOX 29535
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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DEM Form MR -I (12t93)
DEQ-CFW 00063783

I
r 6.
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements C�
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
NC Hwy 87 South
Michael E.
of Permittee*"
28306 (910) 678-140
Phone Number
PARAMETER CODES
31. 1996
DEQ-CFW 00063784

DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
DuPont Automotive
April 26, 1996
NC Dept. of Environment, Health, and Natural Resources
Division of Environmental Management
Central Files
P. O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. NC0003573
Discharge Monitoring Report - March 1996
Dear Sirs:
Attached is the DuPont -Fayetteville Works Discharge Monitoring Report for March 1996.
During the week of March 18, 1996, the Outfall 002 temperature was recorded three of the
required five days of that week.
The cause of this monitoring omission was due to a new operator in training at the wastewater
treatment plant who failed to record the temperatures on the required dates. The operator has
been contacted and the importance of recording required information has been emphasized.
We believe the above actions have corrected the problem, and future recurrence of this
monitoring omission is not expected.
If you have any questions regarding this matter, please feel free to call me at [phone].
Environmental Coordinator
Attachments
cc: Ms. Kitty Kramer, Fayetteville Regional Office
E. I. du Pont de Nemours and Company ® Printed on Recycled Paper
Z•544 Rev. 8/95
DEQ-CFW 00063785

DEQ-CFW 00063786

} EFFLUENT A
NPDES PERMIT NO. NC0003673 DISCHARGE NO. 001 MONTH FEBRUARY YEAR 1996 '( 1
FACILITY NAME DuPont - Fayettevjye Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) lEA (Cary, NC) (2) Burlington Research
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES /-� /,,,,. r �f /
` DIV. OF ENVIRONMENTAL MANAGEMENT X �v L/` '� " ` l�
DEHNR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE 1'
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
50050
00010
00400
50060
003'
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DEM Form MR4 (12193)
DEQ-CFW 00063787

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements
t
Compliant
0
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and -all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
E. Mavberr`r a Site
' SidAiture of
NC Hwy 87 South, Fayetteville, NC, 28306 (910) 678-14 1 May 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
DEQ-CFW 00063788

w
Effluent Toxicity Report Form - Chronic P�ss/Fail and Acute LC50 Date: 02l22196
acility: DUPONT H DES#: NC0003ST3 Pipe#: OM County: BLADEN
Aboratory Performing Test: BURLINGTON RESEARCH, INC.
r Comments:
Signat of opetlefor in Responsible Charge
s gn re of La ratory Supery sor * PASSED: -4.76% Reduction
)rk Order: 68227-001 ' Environmental Sciences Branch
MAIL ORIGINAL To: Div. of Environmental Management
N.C. Dept. of EHNR
44D1 Reedy Creek Road
! Raleigh, North Carolina 27607-6445
>rth Carolina Ceriodaphnia esults
Chronic Pass/Fail Reproduction ToxicityChronic Test R
Test Calculated t = -0.653
esutt$
Tabular t m 2.508
3NTROL ORGANISMS 1 2 3 4 5 6 7 '8 9 10 11 12 % Reduction = -4.76
% Mortality Avg.Reprod.
# Young Produced 18 30 26 27 33 26 19 15 29 23 26 22 8.33 24,50
Control Control
Adult Wive Mead L L L L L L L D L L L L 0.00 25.67
(fluent %: 3.3%
Treatment 2 Treatment 2
'REATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Controt%CV PASS FAIL
# Young Produced [23 30 23 23 31 25 2 27 23 24 22 30 % control orgsproducing 3rd
brood Check One t�•;, L ... L.. L j. L !: IL L 92%
let sample 1st sample 2nd sample Test St Complete
art ete•This For Either Test
)H
4/96
Control 7.61 7.72 E47 7.80 7.68 .7Collection (Start) Date
Sample 1: 02/12/96 Sample 2: 02/15/962nd
rreatment.2 7.72 7.73 7.83 7.85 .71 Sample Type/Duration 1st p!F
e s s Grab Comp. Dqhre
D
t e t e t le I S S
a n a n a In Sample 1 X U AM Mrd r d r jdt t t Sample 2 X T P P
let sample lst sample 2nd sa�pte 45
D.O. Hardness(mg/L)
Control 8.3 8.0 8.6 7.7 7.9 •3 Spec. Cond.(Nmhos) 124 SW 455
Treatment 2 L.
7.8 8.0 .4 ;,,,,,1
Chlorine(mg/l) ii?,alum n/a n/a
S le t at receipt(°C) ;''1i.b 1.S
LCSO/Acute Toxicity Test W amp•
(Mortality expressed as %, combining replicates) Mote: Please
% % % i
% % % % %
% Y. % % % % %
Concentration compisto This
Section Also
Mortality
start/end start/and
LC50 = % Method of Determination Control
95% confidence ;Limits Moving Average — Probit _
% -- % Spearman Karb r other _ _ High
Conc.
pH D.O.
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DEN form AT-1 (3/87) rev. 11?95 (DUBIA ver. 4.30)
APR 24 SO
ENV. M.AN UMENT
RAYUTEV) RAG.OF 1 5<
DEQ-CFW 00063789

AP? -1 gro
DEQ-CFW 00063790

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH FEBRUARY YEAR 1996
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) IEA (Cary, NC) (2) Burlington Research
CHECK BOX IFORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / K. Marcus Hall
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES � h�'
DIV. OF ENVIRONMENTAL MANAGEMENT XZ G� l � 3 Z 7
DEHNR (SIGNATURE OF OPERA OR IN RESPONSIBLE CHARGE) DATE
P.O BOX 29535 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27626-0535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DEM Form MR4 (12193)
DEQ-CFW 00063791

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Michael E. Mayberry QSite Manager
P ittee PI ase in ty e) _.
t4Sigrfture of P itt - 0 ate -0
NC Hwy 87 South, Fayetteville, NC, 28306 [phone] May 31, 1996
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
C- '
DEQ-CFW 00063792

Industrial & Environmental Analysts, Inc. (IEA)
BASE/NEUTRAL EXTRACTABLES SW-846 METHOD 8270
IEA Project Number:
IEA Sample Number:
Client Name:
Client Project ID:
Sample Identification:
Matrix:
Number
Compound
2101-071
951176-05 Date Received: 11/29/95
Dupont Date Sampled: 11/29/95
Waste Water Treatment Date Extracted: 12/04/95
EFF (001) Date Analyzed: 12/07/95
Water Analysis By: Van Lare
Dilution Factor: 1.0
Quantitation Results
Limit Concentration
(ug/L) (ug/L)
1
Acenaphthene
10
BQL
2
Acenaphthylene
10
BQL
3
Anthracene
10
BQL
4
Benzo(a)anthracene
10
BQL
5
Benzo(b)fluoranthene
10
BQL
6
Benzo(k)fluoranthene
10
BQL
7
Benzo(g,h,i)perylene
10
BQL
8
Benzo(a)pyrene
10
BQL
9
Benzyl alcohol
20
BQL
10
bis(2-Chloroethoxy)methane
10
BQL
11
bis(2-Chloroethyl)ether
10
BQL
12
bis(2-Chloroisopropyl)ether
10
B L
13
bis(2-Ethylhexyl)phthalate
10
BQ
14
4-Bromophenyl phenyl ether
10
B L
15
Benzyl butyl phthalate
10
BQL
16
4-Chloroaniline
20
BQL
17
2-Chloronaphthalene
10
BQL
18
4-Chlorophenyl phenyl ether
10
BQL
19
Chrysene
10
BQL
20
Dibenzo(a,h)anthracene
10
BQL
21
Dibenzofuran
10
BQL
22
Di-n-butylphthalate
10
BQL
23
1,3-Dichlorobenzene
10
BQL
24
1,4-Dichlorobenzene
10
BQL
25
1,2-Dichlorobenzene
10
BQL
26
3,31-Dichlorobenzidine
20
BQL
27
Diethyl phthalate
10
BQL
28
Dimethyl phthalate
10
BQL
29
2,4-Dinitrotoluene
10
BQL
30
2,6-Dinitrotoluene
10
BQL
31
Di-n-octylphthalate
10
BQL
32
Fluoranthene
10
BQL
33
Fluorene
10
BQL
34
Hexachlorobenzene
10
BQL
35
Hexachlorobutadiene
10
BQL
36
Hexachlorocyclopentadiene (3)
10
BQL
37
Hexachloroethane
10
BQL
38
Indeno(1,2,3-cd)pyrene
10
BQL
39
Isophorone
10
BQL
FORM 8270B (1) Rev. 041795
DEQ-CFW 00063793

PR I
DEQ-CFW-00063794

Jar
Industrial
& Environmental Analysts,
Inc. (IEA)
GC/MS BASE/NEUTRAL EXTRACTABLES EPA 625
COMPOUND LIST
IEA Project Number:
2101-104
IEA Sample Number:
9602195-02
Date Received:
02/07/96
Client Name:
Dupont
Date Sampled:
02/07/96
Client Project ID:
LFN-182117
Date Extracted:
02/12/96
Sample Identification:
E60206
Date Analyzed:
02/18/96
Matrix:
Water
Analysis B •
Van Tar -
Number Compound
1 bis(2-Ethylhexyl)phthalate
J
Dilution Factor: 1.0
Quantitation Results
Limit Concentration
(ug/L) (ug/L)
10 BQL
Comments:
*This compound is no longer provided as a normal target deliverable for
Method 625. Please contact your account representative for further
information.
Sample specific quantitation limits may be calculated by multiplying
the quantitation limit by the dilution factor.
BQL - Below Quantitation Limit
FORM 625B (1) Rev. 081792
DEQ-CFW 00063795

APR - 1 95
DEQ-CFW 00063796

oUPONT
DuPont Automotive
NC Dept. of Environment, Health, and Natural Resources
Division of Environmental Management
Central Files
P. O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. NC0003573
Discharge Monitoring Report - February 1996
Dear Sirs:
DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
March 29, 1996
147Ell
APR 24 1996
ENV. MANAGEMENT
FAYETTEVILLE REG. OFFICE
Attached is the DuPont -Fayetteville Works Discharge Monitoring Report for February 1996.
Included is the Effluent Toxicity Report Form for the Chronic Bioassay Testing required for
Outfall 002.
Also included is the analytical testing results for bis(2-ethylhexyl) phthalate at Outfall 001 for
both the last quarter of 1995 and the first quarter 1996. This quarterly testing is required due
to the apparent presence of bis(2-ethylhexyl) phthalate detected during the 1995 annual
monitoring requirement for the OCPSF Priority Pollutants. In both of the submitted quarterly
tests, bis(2-ethylhexyl) phthalate was below the analytical detection limit.
If you have any questions regarding this matter, please feel free to call me at [phone].
Environmental Coordinator
Attachments
E. I. du Pont de Nemours and Company ® Printed on Recycled Paper
Z-544 Rev. 8/95
DEQ-CFW 00063797

RECCE f ' ;" t:11-.' - H CS
APR -1 e0
DEQ-CFW 00063798

EFFLUENT MAR 1819oe
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH Z-AA19 y YEAR 199
FACILITY NAME DU PONT - FAYETTEVILLE WORKS CLASS 3 COUNTY BLADEN
OPERATOR IN RESPONSIBLE CHARGE (ORC) ROBERT J. GEDDIE GRADE_ PHONE [phone]
CERTIFIED LABORATORIES (1) IEA. INC. (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES ROBERT J . GEDDIE
Mail ORIGINAL and ONE COPY to: /� r
ATTN: CENTRAL FILES
DIY. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF OPERAT R IN RESPONSIBLE CHARGE) DATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND OM ETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
II I
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II II
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Daily Limit
I r m Form MR-1 ! -'/93)
467.7 950.1
DEQ-CFW 00063799

R 10►
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements EiEr
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made. «
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
HWY. 87 SOUTH. DUART. NC
Permittee Address
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH'
00530 Total Suspended
Residue
00545
Settleable Matter
00556
00600
00610
00625
00630
00665
00720
00745
00927
00929
00940
MICHAEL E. YBERRY
P �'ttee�Ie�n �r)
Sig ature of Pemmi ** Da
(910) 67 �—)(O MAY 31, 1996
Phone Number
Permit Exp. Date
PARAMETER CODES
Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
Ammonia Nitrogen 01092 Zinc Chlorine
Total Kjeldhal 01027 Cadmium 01105 Aluminum
Nitrogen
Nitrates/Nitrites 01032 Hexavalent Chromium
01034 Chromium
Total Phosphorous
Cyanide
Total Sulfide
Total Magnesium
Total Sodium
Total Chloride
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility
�as7re❑❑q��uirred per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of gj i a&; AiArity must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)-
;�t'011d
SJ91i
DEQ-CFW 00063800

EFFLUENT " MAR 18199
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH 'An1U/--- YEAR 199 (0
FACILITY NAME DU PONT — FAYETTEVILLE WORKS CLASS_3 COUNTY BLADEN
OPERATOR IN RESPONSIBLE CHARGE (ORC) ROBERT J . GEDDIE - GRADE_ PHONE [phone]
CERTIFIED LABORATORIES (1) IEA. INC. (2)
CHECK BOX IF ORC HAS CHANGED 7 PERSON(S) COLLECTING SAMPLES ROBERT, J . GEDDIE
Mail ORIGINAL and ONE COPY to:
w ATTN: CENTRAL FILES x `Q v
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
DEQ-CFW 00063801

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements EEI�
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of -my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
MICHAEL E.
2
of
HWY. 87 SOUTH, DUART, NC [phone] MAY 31, 1996
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530 Total Suspended
Residue
00545
Settleable Matter
PARAMETER CODES
00556
Oil & Grease
00951
Total Fluoride
01067 Nickel
00600
Total Nitrogen
01002
Total Arsenic
01077 Silver
00610
Ammonia Nitrogen
01092 Zinc
00625
Total Kjeldhal
01027
Cadmium
01105 Aluminum
Nitrogen
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147 Total Selenium
01034
Chromium
31616 Fecal Coliform
00665
Total Phosphorous
32730 Total Phenolics
00720
Cyanide
01037
Total Cobalt
34235 Benzene
00745
Total Sulfide
01042
Copper
34481 Toluene
00927
Total Magnesium
38260 MBAS
00929
Total Sodium
01045
Iron
39516 PCBs
00940
Total Chloride
01051
Lead
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as u red per 15A NCAC 8A .0202 (b) (5) (B).
96 6 Z IJ
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)• r. 3 ,iS G032
DEQ-CFW 00063802

0
®VE 10 DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
QU PONT FEB 29 1996
DuPont Automotive ENV. MANAGEMENT
FAYETTEVILLE REG. OFFICE
February 28, 1996
NC Dept. of Environment, Health, and Natural Resources
Division of Environmental Management
Central Files
P. O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. NC0003573
Dear Sirs:
Attached is the DuPont -Fayetteville Works Discharge Monitoring Report for January 1996.
The January 10, 1996, Outfall 001 sample was measured as 2070 lb/day Total Suspended Solids
(TSS) versus the Daily Maximum permit limit of 950.1 lb/day.
That single daily exceedance resulted in a January Monthly Average of 302 lb/day TSS versus
the permit limit of 292.31b/day TSS.
During the second week of January, the site's Wastewater Treatment Plant experienced an upset
which resulted in bulking of the biomass in both clarifiers. Entrained air bubbles in the sludge
caused it to float, with the most severe problem occurring on January 10, 1996. The site's efforts
to enhance the settling with commercial settling agents during this period were unsuccessful.
The site formed a Task Group to identify and correct the cause of the poor settleability. Samples
of the sludge were sent to Dr. David Jenkins for analysis of the types and abundance of micro-
organisms present. Dr. Jenkins identified an abundance of Norcardia bacteria which are known
to cause floatation problems.
Some of the actions taken to solve the sludge settling problem were varying the types and
quantities of the polymer to enhance settleability, increasing the F/M ratio to reduce the
abundance of the Norcardia, removal of floating material from the clarifiers and foam from the
Aeration Tank to physically remove Norcardia from the system, and increasing the dissolved
oxygen in the Aeration Tank to inhibit any growth of filamentous bacteria.
A marked improvement in solids discharge was noted during the week of January 21, 1996, By
the week of January 28, 1996, the Outfall 001 TSS discharge had returned to a non -detectable
concentration.
E. I. du Pont de Nemours and Company
® Panted on Recycled Parer
DEQ-CFW 00063803

NC DEHNR
DEM - Central Files
February 27, 1996
Page 2
The low TSS discharge at Outfall 001 has continued through the month of February 1996. We
believe the above actions taken corrected the problem of the poor sludge settleability, and future
recurrence of this TSS exceedance is not expected.
If you have any questions regarding this matter, please feel free to call me at [phone].
Attachments
cc: Ms. Kitty Kramer, Fayetteville Regional Office
Michael E. Johnson
Environmental Coordinator
DEQ-CFW 00063804