DEQ-CFW_00062198

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NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH October YEAR 2007
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. die GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Labor umb on) (2)
CHECK BOX IF ORC HAS CHAP I PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard
Mail ORIGINAL and ONE CO to: _� u �at�
ATTN: CENTRAL FILES rt�
DIV. OF WATER QUALITY `N X
DENR D Y'� (SIGNATURE OF OPERATORV RESPONSIBLE CHARGE) E
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS �n07
RALEIGH, NC 27699-1017 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE r r EB
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HRS
HRS
Y/N
MGD
'G
UNITS
Lb/Day
mg/L
mg/L
ug/L
mg/L
mg/L
1
o8o-o
24
B
16.179
26 :
7.35
2
osoo
24
Y
17.005
26
7.32
1357
0.56
30.10
3
osoo
24
Y
15.744 .
27
7.38
4
osoo
24
Y
15.652
28
7.38
0.12
5
osoo
24
Y
17J044.
28
7.40
6
10800
24
16.008
7 ,
osoo
24
15.980
8
osoo
24
Y
17.420
28
7.32
9
o800,
24
Y
16.264
29 , y
7.39
868'
10
osoo
24
Y
16.653
28
7.34
11
0so0
24
Y
16.983 .
27
7-40
1210800
24
Y
16.549
27
7.45
13
0800
24
14132
14
osoo
24
15.117
15
'0800
24 _
Y
1,4.552
26 _
7.65'
16
osoo
24
B
14.918
25
7.44
1170
17
osoo
24
Y
14.772 `
24
7.45
18
osoo
24
Y
19.409
26
7.46
13
osoo
24
Y
14..032
27
7.39
20
osoo
24
13.225
21
0800
24
13.381
22
osoo
24
Y
13.561
25
7.41
23
0800
24
Y
13.536 ' .
24
7.35' .
881
24
osoo
24
Y
13.091
26
7.33
25
0800
24
Y
+11.929
26
osoo
24
Y
27
oso®
24
*
;
28
0800
24
29
0800
24
Y
30
08001
24 1
Y
31
08a0
24 1
Y
6.033 _
21
7.00
AVERAGE
14.999
26
1069
0.56
30.10
0.12
MAXIMUM
19.409
29
7.65:
1357
0.56
30.1.0
0.12
MINIMUM
6.033
21
7.00
868
0.56
30.10
0.12
Comp. (C) Grab (G)
G
G
C
C '; '
C
C
C
C
Monthly Limit
Daily Limit
6-9
7917
DEM Form MR-1 (12/93)
* Plant Shutdown- No Flow
DEQ-CFW 00062198

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105 Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616 Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235 Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481 Toluene
00530
Total Suspended
00927
Total Magnesium
38260 MBAS
Residue
00929
Total Sodium
01045
Iron
39516 PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 213 .0506
(b)(2)(D)
LO S— 3�0
DEQ-CFW 00062199

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH October YEAR 2007
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES - -—
DIV. OF WATER QUALITY X
1
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
1 00010
00400
1 00310
00530
1 00556
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DEM Form MR -I (12/93)
*Plant Shutdown- No Flow
DEQ-CFW 00062200

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
. , A 1 0
cl/ ;(.Zjp
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00556
00600
00610
00625
00630
PARAMETER CODES
Oil & Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal
Nitrogen
Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
LO S- 330
DEQ-CFW 00062201

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: October YEAR: 2007
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
� o
DWQ Form MR-3 (Revised 7/2000)
00010
00400
00310
00610
00530
00094
U
N
N
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C
U
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(D
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0
HRS
oc
units
mg/L
mg/L
#/100ml
gmhoicm
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
2'5
26
-27
28
29
30
31 .
Average
Maximum
Minimum
DEQ-CFW 00062202

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements u
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
11/3c�
Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082
Color (ADM[)
00625
Total Kjeldhal
01027
Cadmium
01105 Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616 Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235 Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481 Toluene
00530
Total Suspended
00927
Total Magnesium
38260 MBAS
Residue
00929
Total Sodium
01045
Iron
39516 PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
LO G— 33
DEQ-CFW 00062203

4M.
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DuPont Fluoroproducts
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
November 30, 2007
DISCHARGE MONITORING REPORT — October 2007
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of October 2007.
If you have any questions, please contact Robert Geddie at [phone].
RJG: sns
Attachment
cc: Ken Cook - ENGR, Old Hickory
R. J. Geddie - FW
M. E. Johnson - FW
G. G. Santiago- FW
File: F-1-3-4
E.I. du Pont de Nemours and Company
DEQ-CFW 00062204