DEQ-CFW_00062101

Y !
SENT
NPDES PERMIT NO. NC0003573 DISCHARGE N 0 T September YEAR 2008
FACILITY NAME DuPont - Fayetteville Works COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. G die GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumbe ) O 08
CHECK BOX IF ORC HAS CHANGED I� PERSON(S) COLLECTb $p WbES Robert J. Geddie / Ray Beard
Mail ORIGINAL and ONE COPY to: `
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
DENR (SIGNATURE OF OPERA IN RESPONS'�IBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RAI EIGH NC: 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
00310 1
00530
00556
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39700
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0
NRS
HRS
Y/N
MGD
'C
UNITS
Lb/Day
Lb/Day
mg/L
P/F
Ug/L
1
osaa4
14.1*
O'776
49 8
68.6
2 108001
24
Y
0.835
25
7.71
27.2
100.3
3
osoo:
24
Y
0,929
25
7 74
34.1
7777
4 108001
24
Y
0.693
25
7.60
5:
osoa
24
",Y
O'866
6
08001
24
0.846
7
osoo'
.24
0;764
8
08001
24
Y
0.821
28
7.70
15.1
38.3
9.
osoo
24
Y
0.889
27
7.72
-'25.2
32 6
<5 6
10
osoo
24 1
Y
0.851
27
7.77
31.2
73.8
11
osoo'
. 24
Y
0.922
12
0800
24
Y
0.845
13
oeool
..24
0:772,
77777
14
osoo
24
0.814
15
osoo
24
Y
0 766
28
7 50
22 4
94 5
16
osoo
24
Y
0.679
26
7.60
15.9
21.0
777777"
17
0800
24
Y
0 802
25
7 60
18
osoo
24
Y
0.744
19
osoa
24
Y
0 681
EE
20
0800
24
0.697
21
0800:
.24
0; 640
22
osoo
24
Y
0.721
22
7.51
22.8
33.1
23
osoo:
24
Y
0 733
21
7 40...
=97 7.
40.3 .
-
777
jr
24
osoo
24
Y
0.657
20
7.50
25.8
38.4
25
-osoo:
24
Y
0 997
26
0800
24
Y
0.717
27
osoo
24
0.804
28
osoo
24
0.700
29
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: 24 '
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0.732 =
23
7�86
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70 2
3o
0800
24
Y
0.840
23
7.50
33.6
91.1
31
Osoo
7A
Y
AVERAGE
0.784
25
27.5
66.7
<5.6
MAXIMUM
0 997
7 86
501
,<178 2;
. <5 6
MINIMUM
0.640
20
7.40
14.0 1
21.0
1 <5.6
Camp. (C Grab (G)
G
G
C,
C
G
Monthly Limit
2.0
191.3
317.8
PASS
DalYLimlt
6 S
508.2
,1030
0,5
DEM Form MR-1(12193)
* Holiday
DEQ-CFW 00062101

l V
Facility Status: (Please check one of p, following)
All monitoring data and sampling frequencies' meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
if the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
Residue
00545
Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032
Hexavalent Chromium
01034
Chromium
01037
Total Cobalt
01042
Copper
01045
Iron
01051
Lead
01092 Zinc
01105 Aluminum
01147
Total Selenium
31616
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], exten
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designa
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
581 or
in the i
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
no
DEQ-CFW 00062102

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH September YEAR 2008
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddle GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY )(
DENR (SIGNATURE OF OPERATOR WIRESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
a;FLOW
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HRS
Y/N
MGD
'C
UNITS
Lb/Day
mg/L
mg/L
ug/L
mg,
1
osoo
24
* -
- 1%002,
2 10800
24
Y
19.213
29
7.46
1179
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24
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18 7947i57
30
4 108001
24
Y
19.011
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7.20
5
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1 S 697
30
710 .
6 10800
24
18.537
7
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8
o800
24
Y
19.520
30
7.10
0.02
9
Y
Zt).437
28
6.90
1543
148
1 78
10
0800
24
Y
16.034
27
6.93
;a 1
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24
16
Y
1'3 506
26.
7 64
777
12
0800
24
Y
13.549
28
7.10
13
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24
13.501
14
0800
24
13.796
15
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24
Y-
1.3.893
29 -
7 02
-
16
08001
24
Y
13.993
29
7.29
635
17
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24
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18
08001
24
Y
13.418
29
7.15
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13,263
29
7 02
20
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24 1
12.868
21
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: 1'2 597
22
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24
Y
12.704
27
7.21
Y
7 43934
24
Y
12.574
26
7.30
2412.166
27
N.
24
Y
12.068
28
7.14
.
24
12.553
;24
Y'
' 12
24
Y
12.234
29
7.81
1005
12124
24..
AVERAGE
14.934
28
1059
1.48
1.78
0.02
MAXIMUM
20 437
30
7,81.
1543..:
1.48
1.78
0 0.2-
MINIMUM
12.068
23
6.90
635
1.48
1.78
0.02
mp. (C)Grab (Gj
G
G,
C
C
C
C
Monthiv Limit
DEM Form MR -I (12/93)
0
O
0
* Holiday
DEQ-CFW 00062103

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"i certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
. n i
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
Residue
00545
Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032
Hexavalent Chromium
01034
Chromium
01037
Total Cobalt
01042
Copper
01045
Iron
01051
Lead
01092
01105
01147
31616
32730
34235
34481
38260
39516
50050
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCB's
Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
80 91 i io
DEQ-CFW 00062104

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: September YEAR: 2008
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
00010
00400
00310
00610
00530
00094
51521
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d
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HRS
°C
units
mg/L
mg1L
#1100mi
µmhol—
ug/L
Average
<0.01
Maklmum
<0 01
Minimum
<0.01
DWQ Form MR-3 (Revised 7/2000)
2
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O
2
3
4
6
._......_.._.
..........___.
8
9'
......_...... _...
10
12
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14
15
.... _._____..
... ____...._
16
�17
18
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20
21
22
.23
.................
24
.____......_.
....__............
"251
........_..........
26
28
=29
30
00010
00400
00310
00610
00530
00094
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M
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e
i=
d
O
H
ti
V
00
HRS
°C
units
mg/L
mg/L
#/100ml
µmhoicm
Minimum
DEQ-CFW 00062105

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements �J
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
nn076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
81551 Xyiene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 213 .0506
(b) (2) (D) so 91 I.iO
DEQ-CFW 00062106

0M.
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DuPont Fluoroproducts
Fayetteville Works Plant
22828 NC Highway 87 West
Fayetteville, NC 28306-7332
October 14, 2008
DISCHARGE MONITORING REPORT — September 2008
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of September 2008.
If you have any questions, please contact Robert Geddie at [phone].
RJG: jlp
Attachment
cc: Ken Cook - ENGR, Old Hickory
R. J. Geddie - FW
M. E. Johnson - FW
M. M. Page - FW
File: F-1-3-4
E.I. du Pont de Nemours and Company
DEQ-CFW 00062107

�M �| |"nO
-_ ~,�°
OEQ-CFVV_00062108