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HomeMy WebLinkAboutDEQ-CFW_00079862The Chemours Company 910-483-46810 Fluoroproducts chemours corn 22828 NC Highway 87 W Fayetteville, INC 28306-7332 CERTIFIED MAIL ARTICLE NUMBER 7002 0860 0006 9104 7828 RETURN RECEIPT REQUESTED Ms. Wren Thedford NCDEQ Division of Water Resources NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SUBJECT: NPDES Permit Renewal Applicati NPDES Permit No. NCO003573 I Dear Ms. Thedford: MAY O'S 7016 Nuum The Chemours Company — Fayetteville Works is requesting renewal of NPDES Wastewater Discharge Permit No. NC0003573. Since the issuance of the last permit, the ownership of this facility changed from the DuPont Company to The Chemours Company FC, LLC. Also, two separate companies, Kuraray America Inc. and the DuPont Company, are operating manufacturing units and are treating and discharging their wastewaters under the Chemours' NPDES Permit. Enclosed are the original and two copies of the General Information Form I (Form 3510-1), Wastewater Discharge Information Form 2C (Form 3510-2C), and additional required supporting documentation for renewal of the subject permit by the NC Division of Water Resources. Included in the permit application are the following supplemental information documents: Sludge Management Plan, Current Facility Wastewater Management, Current Facility Operating Conditions, Alternate Application Schedule for §316(b) of the Clean Water Act, Elimination of Monitoring Requirement for PFOA, and the non -reporting of bis(chloromethyl) ether. If you have any questions or need additional information, please contact me at (910) 678-1155. V;nr-rrAx7 DEQ-CFW-00079862 'ptei-e Drint or tvDe in the unshaded areas only Form Approved OMB No 2040-0086 FORM U S. ENVIRONMENTAL PROTECTION AGENCY I EPA I D NUMBER 1 GENERAL INFORMATION r a 777 Ill Consolidated Permits Program F NCD 047 368 642 D GENERAL (Read the "General lmtructions" before starling) 2 13 1,1 1 1s GENERAL INSTRUCTIONS LABEL ITEMS If a prepnnted label has been provided, affix it in the designated space Review the information carefully, if any of it is incorrect, cross through it and enter the correct data in the I. EPA I D NUMBER ' appropriate fill-in area below Also, if any of the preprinted data is absent (the area to the left of the label space lists the III. FACILITY NAME PLEASE PLACE LABEL IN THIS SPACE information that should appear), please provide it in the proper ' fill-in area(s) below If the label is complete and correct, you need not complete Items I, III, V, and VI (except VI-8 which V. FACILITY MAILING ADDRESS must be completed regardless) Complete all items if no label has been provided Refer to the instructions for detailed item for the legal authorizations under which this VI FACILITY LOCATION VI FACILITY LOCATION data collected data II POLLUTANT CHARACTERISTICS INSTRUCTIONS Complete A through J to determine whether,you need to submit any permit application forms to the EPA If you answer "yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the question Mark "X" in the box in the third column if the supplemental form is attached If you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements, see Section C of the Instructions See also, Section D of the instructions for definitions of bold-faced terms Mark ")C Mark 'X' SPECIFIC QUESTIONS YES No FORM ATTACHED SPECIFIC QUESTIONS YES NO FORM ATTACHED A Is this facility a publicly owned treatment works which B Does or will this facility (either existing or proposed) results in a discharge to waters of the U.S? (FORM 2A) X include a concentrated animal feeding operation or aquatic animal production facility which results in a 16 i] 1e 19 20 21 discharge to waters of the U.3? (FORM 2B) C Is this a facility which currently results in discharges to �/ X �/ X D Is this a proposed facility (other than those described in A X waters of the U.S. other than those described in A or B or B above) which will result in a discharge to waters of above? (FORM 2C) 22 23 24 the U.S.? (FORM 2D) 25 w 27 E Does or will this facility treat, store, or dispose of F Do you or will you inject at this facility industrial or hazardous wastes? (FORM 3) X municipal effluent below the lowermost stratum X containing, within one quarter mile of the well bore, 28, underground sources of drinking water? (FORM 4) 31 32 „ G Do you or will you inject at this facility any produced water H Do you or will you inject at this facility fluids for special or other fluids which are brought to the surface in processes such as mining of sulfur by the Frasch process, connection with conventional oil or natural gas production, X solution mining of minerals, in situ combustion of fossil X inject fluids used for enhanced recovery of oil or natural fuel, or recovery of geothermal energy? (FORM 4) gas, or inject fluids for storage of liquid hydrocarbons? (FORM 4) 34 35 36 37 1 3a 39 1 Is this facility a proposed stationary source which is one J Is this facility a proposed stationary source which is of the 28 industrial categories listed in the instructions and �/ X NOT one of the 28 industrial categories listed in the X which will potentially emit 100 tons per year of any air instructions and which will potentially emit 250 tons per pollutant regulated under the Clean Air Act and may affect year of any air pollutant regulated under the Clean Air Act 40 41 42 43 44 u or be located in an attainment area? (FORM 5) and may affect or be located in an attainment area? (FORM 5) III NAME OF FACILITY c 1 SKIP C emours Company - Fayetteville Works 15 18 - 29 30 IV FACILITY CONTACT A NAME & TITLE (last, first, & ade) B PHONE (area code & no) J2Johnson, Michael, Environmenta Manager ( 1)6 8-1 5 15 16 45 46 48 49 51 52- SS V. FACILTY MAILING ADDRESS A STREET OR P O BOX G 3 22828 NC Highway 87 W 15 15 45 B CITY OR TOWN C STATE D ZIP CODE a Fayettevi le C 2 3 6 15 1 16 40 41 42 47 51 VI. FACILITY LOCATION A STREET, ROUTE NO OR OTHER SPECIFIC IDENTIFIER 45 c 5 2 8 8 NC ighway 8 5 i6 B COUNTY NAME Bladen 20 C CITY OR TOWN D STATE E ZIP CODE F COUNTY CODE (if known) s F y t evi 1 C I 2 3 6 3 0l'7 95 16 40 41 42 47 51 52 -SG EPA Form 3510-1 (8-90) CONTINUE ON REVERSE DEQ-CFW 00079863 ipn rP(')M THE Fpr)rJT VII SIC CODES 4-di it, in order ofprioni�K) A FIRST B SECOND (specify) INDUSTRIAL ORGANIC CHEMICALS C I I I (specify) LAMINATED PLASTICS PLATE, SHEET, AND PROFILE SHAPES Jc 7 2 8 69 3083 C THIRD D FOURTH -.2-A I I l(specity)uNSUPPORTED PLASTICS FILM AND SHEET c (specify) PLASTIC MATERIALS AND RESINS 713081 1 NOTEKurar.y E.tarite ButaciteO and SentryGlasO sheeting 2821INOTE: DuPont PVF resin process units 1 i6 process units15 �7 - ---------- Vill OPERATOR INFORMATION A NAME B. Is the name listed in Item I T__7_ I VIII-A also the owner? 77,777 Jc 8Thel Chemours Company FC, LLC 0 YES ONO 5 16 55 M C. STATUS OF OPERATOR (Enter the appropriate letter into the answer box if "Other, 'specifv) D PHONE (area code & no) F = FEDERAL M = PUBLIC (other thanfederal Orstate) (specify) A (302) 773-1000 S = STATE 0 = OTHER (specify) �P P = PRIVATE -J 15 16 - 18 119 - 21 �22- 26 ---------- E STREET OR P 0 BOX AO� EUTettrUltl I I I I I I I I I I I I I I I I 1 1 2. 55 F CITY OR TOWN G STATE H ZIP CODE IX INDIAN LAND c I . . . . Is the facility located on Indian lands? B]Wilmington DE 19898 0 YES 121 No M -- - IT — - ti- 47 . 51 X EXISTING ENVIRONMENTAL PERMITS A NPDES (Dischar es to Surface ��,ej D PSD(Airl,'missions from Pro osedSource,$) cTT 9 N _T 1 NC0003573 c 9 T 1PI I I NC Title V Permit 03735 B U I C (Undewound E OTHER sect y) C T I I qecyn Vltads) ' A N c T I W 0 3 4 1 1 1 1 1 1 1 1 J1 y) Land Application Permit (specify) � 15 J 16 17118 C RCRA Hazardous Wastes E OTHER (spe fy) T I I _1 I N D047368642 C 9 T I 1 _7 (specfy) 9 R 151 16 17118 M 15 16 1 17118 30 XI MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements XII. NATURE OF BUSINESS (provide a bnefdescnption) The Chemours Company - Fayetteville works (formerly the DuPont Company - Fayetteville Works) is a fluorinated chemicals manufacturer situated on'a. 2,200-acre property in northwestern Bladen County, NC. The Chemours, products produced at the facility include fluorinated monomers and fluorinated vinyl ethers, Nafion" membranes and dispersion, and fluoropolymer processing aids. Chemours operates two natural gas / fuel oil -fired boilers, which provides steam for the entire facility. Also located at this facility are two tenant companies: Kuraray America Inc. and the DuPont Company. Kuraray operates the Butacite® polyvinyl butyral (PVB) thermoplastic sheet and resin manufacturing unit and the SentryGlasO ionoplast interlayer manufacturing unit. DuPont operates two polyvinyl fluoride (PVF) resin manufacturing units. Chemours receives and treats all of the Kuraray and DuPont process wastewater, sanitary wastewater, and contact stormwater in the Chemours' owned and operated wastewater treatment plant, and discharges that treated wastewater through Outfall 001 under the Chemours' NPDES Wastewater Discharge Permit (Permit No. N00003573). The Kuraray and DuPont non -contact cooling waters and stormwaters are discharged through Outfall 002 under the Chemours' NPDES Wastewater Discharge Permit. X111 CERTIFICATION (see instructions) I certify under penalty of law that / have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the applicatio!l i believe that the information is true, accurate, and complete I am aware that there are significant penalhes for submitting false information, including the possibility of finyand imprisonment A. NAME & OFFICIAL TITLE (type orprint) Ellis H. McGaughy - Plant Manager B SI ATURE C DATE SIGNED COMMENTS FOR OFFICIAL USE ONLY 1C 55 EPA Form 3510-1 (8-90) DEQ-CFW-00079864 DEQ-CFW 00079865 CHEMOURS, COMPANY FA ETT°E TILE WORDS LOCATIONS OF INTAKE AND DISCHARGE STRUCTURES DEQ-CFW 00079866 EPA I D NUMBER r-w Form Appra*ved ON1B No. 2Q40-0086 mint or fvrip in the. unshaded areas cnle N 0 4 39-6 642 1 Approval expires 3,31-98 FORM U S ENVIRONMENTAL PROTECTION AGENCY APPLJC.;%TION FOR PERMIT TO DISCHARGE VVAS1-EVVATER 2C Soo E PA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS NPOES Pro, OUTFALL LOCATION — ----- -------- — ------- For each outfafl, list the o� its: 5 '�.d :ii'. narsx'. <s> tix "'VaW, ......................... ------------------- - ..... .... ........... ........ ....... ------------ A OUITALL NUMBER, 6 LATITUDE LONGITUIDE . . ................... ...... ..... . D. RE—CEIVING WATER (,�aow) ... ..... ... .......... -2 NI I N SFC, 1 CF MiN "I S F. C 50.00 2 , 9 3 21 0 30.6b E 1.1.47 Car�e Feat' Rivur . ......... - ----------------------------------- -- - ------------------ 34 --- ----------- — ------------------- - ............... 31% 49.00 ----- 2c�.70 - — ----- ............... Cape Fear River ............ ---- - ------------------------ . ......... ------------------------ . .............. . ................ — — — ----- ------------ -------------------------------------------- ------- ... . ................. ----------- - ------------- I P10',,VS. SOURCES OF POLLUTION AND TREATMENT TECH N(j-LQG: ES — - ------------------ - A Attach a tinedrawingshcvqng the water flow thfough the facility. Indicate sokr _sc, and ;realry ?W t labeled to correspond to the rofe detailed descnpt:ons in stem .5. Construct a wale., ba:anc--the hric dtawing by ,nowinq ae,erage f:ows be:ween intikes, clpelat:orls units. and OUtfal:S If a water balance cannot be determined (e g, for certain, mining 6ctivit!es)pmvide a pictorial descriptiorl (if the nature and amount of any ate ) or treatment measures ,ourcesofw� rand any coilectio, . ... . . .............. . ............... ........... ....................... I--- ... .. . ................ 8 For each out"allwovide a desciwtion of: (1) All operations contribut;ng wastewater to the effluent, including process wastewater. sanitary wastewater, cooling water, and stomwaie!funoff: f !he average flow contributed by each operation and (3) The treatment received by the waMewaler Confinue on additional sJherz,.'s if ne-cessary 0 U 2 OPERATIO.YSi CONT R:BLITING FLOVV 3 TREATMENT FALL '40 (;'Id a, OPERATION (h,i, b AVERAGE FLOIA' f;,, "ur i" ., ,i DESCRIPTION LIST CODES F-PO%1 TABLE 2`1-1 ........................ -A . ... . ......... ... . .. . .... ... ............... .... . ......... . ...... ........ . ....... . . .......... ... . ..... .................. .............. OFFICIAL USE. ONLY ---------------- EPA Form 3510-2-0 (8-93) PAGE I of 4 CONTINUE ON REVERSE DEQ-CFW-00079869 r-hM -WI lr=r) rWt')O T;-+ P7P,)t-IT C Exnept for storm runaff, leaks, or spills are any of tne discharges de&,-nbed ri tem. s it ar E intermilterit Gr seasona!9 YES h,- lr 0 NO i-- iii) ....................... . ...... I a rR---QUENC,� - ---- - ------------------- i 4 E. TOTAL VOLUME a DAYS PER 2 OFERAIjON(s) AEFK o MONTHS o Fly,,,',, PA -i; w,; I C)IiTFA: L CI',-)NTRIBL;`.ING FLO'vv PER YEAR ICIfiCTER'M 2 MAXIMUtv' 1 LONGTERM 2 MAXiMUM C DJRATIOt� N:- � r,rry i,-AVER, ,C VFR A G E ....DAILY ............... M PR(,DJCTION - - ----------------------- A, Does in effli;era W':" P:I 0�1 -::-'at Cl buw0;4 0 ,ar; Aot Ac: u: NO YES B Are the I - '11:tat ion s in the. applicable elf: uent guideline e. x pfessed n e: ril & of Prodtjctbn (or titherure of op6,ta iyon YES ;Vi, 'i V , ;-) . . ...... . . . ............... . C. if you ariswemd 'yes' to Rem III hst te quantity r,,hich repteSe.nIs ari actua; measurement of your level of produ,.:ian <zxpressed in the terms and emits user in the applii-abie effluent gu:dehne, and indicate the affected ouffaGls ----------------------------------- . ................... ----------- . ........... . .. ... ........ - ........... 1. AVERAGE DAlLY PRODUCTI(DN 2 AFFECTED OUTFALLS c CiPEIRATION. PRODUCT MATERIAL E TC a QUAN-TY PER DAY : b. UNITS OF MEASURE :V !MPROVEMIEN A Are you now req�i:red ny �w,, ol 'r 01XIi,::10:? trealment equipmem. or pf;aGt;Ces U. arly 01hei- eri'vifljnrnenial pfogac wli0i fnay alfect ti--e dischxges desciibed in tl:s I his vid: des. bul i& nljMte-', permit Lid ir izi,stiztsve cir enfDrcempnt oiders, enfarn.ement cxmipliance rcliedulc letters &tipuiatior15 court orders and want a, ioan Conditions, Ej YES N 0 S. ;DENTiFICATION OF CONDITIO-N 2, AFFEC'T ED OUTFALLS lEF DESCMPTIC a. BR N OF PROJECT 4 FINAL COMPL:ANCE LATE AGREE ETC. -_SCITE D: C HA R G E B OPTIONAL You may attach additional sheets describing any additional water pollution control programs (or other erwronmental pqiects which may affact your I - - 9 -way or p!inr%ed, and ndicate your actuai or p:anned schedu:es for dtschiorge,sl you now have underway r,-,vvh:cn you p:an Indi-nale whether each pfooram is now uncei construction:. MIAR K 'X- iF DESCRIPTION OF ADDITIONAL C ROL P ROGRAMS 1 S AT TA(, HED Er,.A Form 3510-2(C f8-90, PAGE 2 of 4 CONTINUE ON PAGE 3 DEQ-CFW-00079870 EPA Form'3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE OEQ-CFVV_00079871 C.ONTiNUED FROM THE F-Rc,*)N*[ V�j THTING DA Do ym have any knoWeye w reaum W bdow ON a, WNW WW 01 mWe N W-C kw"Y Ws WwmWe sa A NO IWMMO - W a MWQ9 —W"� Wayn W ym"Bdwme mom Me Wst 3 Pam" N;O k�ai,:iina Ceriodaphnia Wranis Effluent Bioaosay vronWwre" 1z pertormod each vjow,�I in accordance with the reqvliremenc of condition AW of the facility's WDES Permit, 'rhe NCLEQ Divis-on of Waf.e-r Resoarces has copies of the Form AT-1 test resuLts that were submitted wit! the Vischarge Monitoring Reports during the period from �,'.,)12 thrc-,,,g�n FeoKuary 2016 Tke qvatterly chronic test performed during February 2012, failed foi tne dunia The reqoized monthly chronic tests performed in March and April 2012 both p,�-ssed� No other toxicity ten: faLlurns occurred during the five-year term of t.he omyrest permit, VW CONTRACT ANALYTWNFORNIATiC fAm a" &Me ampewspomd &Hot V pennned by a =W a4vamy W alf�sd=g 1"" YES (Aimcmmm whho, NO 00 �01,0 h hA—Sm4TPnn W.) ----- . . ........ . . ....... ------------------------------------------------- .................... .................... C TELEPHONE D. POLLUTANTS ANALYZED A NWE B ADDRESS Ost) ------- — - --------- — --------------------------------- --------------- . ........................ ... - - ------------------------------------------------------ TW West S--r�e" i 3 1 L 0,�Yqel: CQ!aform; alv:� Grca-�C, S"We As Soo rts; e Total Part 0 a-d T�a;- V.Ia—il, C�,"�Pcurds P a r t C GC �,I S Ac-,id Patt. C S W CERTRCATEN — - ----- — ----------------------------------- --- -- in&fy won PxQy of 115M.5 qs)aiii's-d personrei prope!ly plu W evaGam the wfor.maron sub.rnml,'ecd viased or) my inqufry of U�e perscr, or pem.f�ns� �vho manage toe. sy�stf�m or "hose Persons dmc§ ms;mnmble Ar gaMemW Me Obmava Us ViommBn WAtted A to Me best of my know!odq,� and belief t,'Ue. aC.CWWf�, E?0dCI0MPk.?tP. I 01P :31,v3le *170t th&�e am mpiitimat penaMs for wbANg We &KmaMR AcWWg Me pmabOty offine ano impfisonment for inowing viohitoos. 7NAME & OFFICIAL T7LE B PHONE NC� Lis v,, a I Nan* er '9101 67S C URE C, DATE SIGNED MAE, EPA F 3 5 1 2 C (8 - 9 0.) DEQ-CFW-00079872 VI N J, - I . 11 - I I - I . Flow Units: Gallons per Day Basis: (1) All Manufacturing Units operating (2) Maximum 30-day average of measured flows (2013 - 2015) DEQ-CFW-00079873 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information rEPA LD NUMBER (copvfrom Item I of Form 1) on separate sheets (use the same format) instead of completing these pages SEE INSTRUCTIONS, NCD 047 368 642 V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 ofForm 2-C) OUTFALL NO. ooi PART A -You must provide the results of at least one analyses for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 3. UNITS 4. INTAKE 2. EFFLUENT (specify r%blank) (opnona( b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM a MAXIMUM DAILY VALUE (tfararlable) (tfmadable) AVERAGE VALUE 1. POLLUTANT d. NO. OF a. CONCEN- b. NO. OF CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES a. Biochemical Oxygen Demand (BOD) 71.0 0 675.9 26. B 207. 1 5.8 37. 8 465 m L g/ lb. n a / n a / n a / b. Chemical Oxygen Demand (COD) 32.1 1 313.2 2 1 m g/L lb. n/a n/a n/a c. Total Organic Carbon (TO(} 84.9 828.4 1 mg/L lb. n/a n/a n/a d. Total Suspended Solids (TS.Cj 44 . 0 387. 8 22 . 0 177 . 0 9. 8 54 . 6 465 m /L g lb. n/a n/a n/a e.Ammonia (asN) 0.414 4.0 1 mgfL lb. n/a n/a n/a f.Flow VALUE 1.627 VALUE 1.133 VALUE 0.907 1095 MGD MGD VALUE n/a n/a g Temperature VALUE VALUE VALUE VALUE (granter) 26.0 22.2 18.4 118 °C n/a n/a h. Temperature VALUE VALUE VALUE VALUE (summer) 32.0 30.6 29.0 118 °C n/a n/a MINIMUM MAXIMUM MINIMUM MAXIMUM i• pH 6 .37 8.47 n/a n/a 374 STANDARD UNITS PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, on an effluent limitations guideline, you must provide the results of at least one analyses for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opuonal 1. POLLUTANT AND b. MAXIMUM 30 DAY VALUE c LONG TERM AVRG. VALUE a. LONG TERM AVERAGE a b a. MAXIMUM DAILY VALUE a available (f ) (rfm�minble) VALUE CAS NO. BELIEVED BELIEVED d. NO. OF a. CONCEN- b NO. OF (1) (1) (1) (rfavatlable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES a. Bromide (24959-67-9) b Chlorine, Total Residual X 0.03 0.3 1 mg/L lb. n/a n/a n/a c. Color 10 n/a 1 PCU n/a n/a n/a n/a d. Fecal Coliform \X X est . 2 n/a 1 col/dL n/a n/a n/a n/a e. Fluoride (16984-48-8) X 170 1659 1 mgfL lb. n/a n/a n/a f. (as'A/)te-Nitre?e X 0.065 0.6 1 mg/L lb. n/a n/a n/a EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE DEQ-CFW 00079874 �41 ITEM V-R CONTINUED FROM FRONT 2. MARK"X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. VALUE a. LONG TERM AND a, b a. MAXIMUM DAILY VALUE (tj'avadable) (ifavadable) AVERAGE VALUE CAS NO. BELIEVED BELIEVED d. NO. OF a. CONCEN- (1) b. NO. OF (1) (1) (1) (favadable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES g. Nitrogen, Total Organic (a, 1.016 9.9 1 mg/L 1b. n/a n/a n/a N) I I h. Oil and x <5.6 <50.0 5.2 42.5 0.26 1.87 36 Mg/L 1b. n/a n/a n/a Grease i Phosphorus (as P), Total X 12.4 121.0 1 mg/L 1b. n/a n/a n/a (7723-14-0) I. Radioactivity (1) Alpha, Total x (2) Beta, Total x (3) Radium, x Total (4) Radium 226, x Total k. Sulfate (asSO,) x 1083 10568 1 Mg/L 1b. n/a n/a n/a (14808-79-8) I. Sulfide (Gc S) x m. Sulfite (- SW x (14265-45-3) n. Surfactants x 3.07 30.0 1 Mg/L 1b. n/a n/a n/a o. Aluminum, Total x 0.19 1.9 1 mg/L 1b. n/a n/a n/a (7429_90_5) 1 p. Barium, Total (744()-39-3) x q. Boron, Total (7440-42-8) x I r. Cobalt, Total x (7440-48-4) s. Iron, Total x 0.28 2.7 1 mg/L 1b. n/a n/a n/a (7439-89-6) I. Magnesium, Total X 2.26 22.1 1 mg/L 1b. n/a n/a n/a (7439-95-4) u. Molybdenum, Total x (7439-98-7) v. Manganese, Total x <0.005 <0.049 1 mg/L 1b. n/a n/a n/a (743996-5) w. Tin, Total (7440-31-5) x. Titanium, Total (7440-32-6) EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 DEQ-CFW-00079875 EPA I.D. NUMBER (copyfronillem I ofEonn 1) OUTFALL NUMBER ('ONTINI IFn FROM PArF 'A OF FORM 9-r, NCD 047 368 642 1 001 1 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully Complete one table (all 7pages) for each outfall See instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b C. a. MAXIMUM DAILY VALUE (ifavadable) VALUE (ifavadable) AVERAGE VALUE - - CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b NO. OF (1) (1) (1) (ifavadable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENW)RATION (2) MASS ANALYSES TRATION b MASS CONCENTRATION`[ (2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total X <0.002 <0.020 1 mg/L 1b. n/a n/a n/a (7440-36-0) 2M. Arsenic, Total X <0 . 005 <0. 049 1 mg/L 1b. n/a n/a n/a (7440-38-2) 3M Beryllium, Total X <0 . 001 <0.010 1 mg/L 1b. n/a n/a n/a (7440-41-7) 4M. Cadmium, Total X <0.002 <0.020 1 mg/L 1b. n/a n/a n/a (7440-43-9) 5M. Chromium, X 0.010 0.070 0.010 0.070 0.004 0.034 4 mg/L 1b. n/a n/a n/a Total (7440-47-3) 6M. Copper, Total X 0.007 0.050 0.007 0.050 0.0055 0.047 4 Mg/L 1b. n/a n/a n/a (7440-50-8) 7M, Lead, Total X <0.003 <0.029 1 Mg/L 1b. n/a n/a n/a (7439-92-1) I I 8M Mercury, Total X <0.0002 <0.002 1 mg/L 1b. n/a n/a n/a (7439-97-6) 9M. Nickel, Total X 0.012 0.090 0.012 0.090 0.0083 0.065 4 mg/L 1b. n/a n/a n/a (7440-02-0) 10M. Selenium, X <0.005 <0.049 1 mg/L 1b. n/a n/a n/a Total (7782-49-2) 11 M Silver, Total X <0.002 <0.020 1 mg/L 1b. n/a n/a n/a (7440-22-4) 12M Thallium, <0 . 005 <0. 049 1 mg/L 1b. n/a n/a n/a Total (7440-28-0) 1 13M. Zinc, Total X 0.042 0.390 0.042 0.390 0.0343 0.286 4 mg/L 1b. n/a n/a n/a (7440-66-6) I I I 14M. Cyanide, Total (57-12-5) X <0. 005 <0.049 mg/L 1b. n/a n/a n/a I 15M. Phenols, X =,O , 0400 <0.390 1 mg/L 1b. n/a n/a n/a Total DIOXIN 2,3,7,8-Tetra- DESCRIBE RESULTS Not applicable chlorodibenzo-P- X Dioxin (1764-01-6) EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE DEQ-CFW-00079876 r(')MTIMI irn I=P()kA THE FRONT 2. MARK "X" 3 EFFLUENT 4. UNITS 5. INTAKE (apnnnaC 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b c a. MAXIMUM DAILY VALUE (ifavadable) VALUE (ifewadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEW OF (1) (ifavadable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION -2- MASS ANALYSES GC/MS FRACTION -VOLATILE COMPOUNDS 1V. Accrolein x <0.0500 <0.488 1 Mg/L 1b. n/a n/a n/a (107-02-8) 2V. Acrylonitrile (107-13-1) x <0.0100 <0.098 1 Mg/L 1b. n/a n/a n/a 3V. Benzene (71-43-2) v ^ <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a 4V. Bis (Chloro- methA Ether x Not Req iced per NCDWR NPDES Permitt'g Unit (542-88-1) 5V. Bromoform x <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a (75-25-2) 6V Carbon Tetrachloride x <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a (56-23-5) 7V. Chlorobenzene <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a (108-90-7) 8V. Chlorodi- bromomethane <0.00100 <0.10 1 Mg/L 1b. n/a n/a n/a (124-48-1) 9V. Chloroethane x <0.00500 <0.049 1 Mg/L 1b. n/a n/a n/a (75-00-3) 10V, 2-Chloro- ethylvinyl Ether x <0.0500 <0.488 1 mg/L 1b. n/a n/a n/a (110-75-8) I 11 V. Chloroform (67-66-3) x <O.00SOO <0. 049 1 mg/L 1b. n/a n/a n/a 12V. Dichloro- bromomethane x <0.00100 <0.10 I Mg/L 1b. n/a n/a n/a (75-27-4) 13V. Dichloro- difluoromethane x <0.00500 <0 . 049 1 Mg/L 1b. n/a n/a n/a (75-71 -8) 14V. 1,1-Dichloro- <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a ethane (75-34-3) 1 15V. 1,2-Dichloro- x <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a ethane (107-06-2) 16V. 1, 1 -Dichloro- <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a ethylene (75-35-4) 17V. 1,2-Dichloro- x <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a propane (78-87-5) 18V. 1,3-Dichloro- propylene x <0.00100 <0.10 1 Mg/L 1b. n/a n/a n/a (542-75-6) 19V Ethylbenzene x <0.00100 <0.10 1 mg/L 1b. n/a n/a n/a (100-41-4) 20V Methyl x <0.00500 -0 . 049 1 Mg/L 1b. n/a n/a n/a Bromide (74-83-9) 21V. Methyl A <0.00250 <0.024 1 Mg/L 1b. n/a n/a n/a Chloride (74-87-3) EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5 DEQ-CFW-00079877 CONTINHFr) FROM PArF V-4 2. MARK"X" 3. EFFLUENT 4. UNITS 5. INTAKE (opunnan 1 POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG ' a. LONG TERM AND a. b c a MAXIMUM DAILY VALUE (ifavadable) VALUE (ifava lable) I AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a CONCEW b. NO. OF (1) (1) -(1) (ifavadable) REQUIRED PRESENT ABSENT CONCENTRATION 1 (2) MASS CONCENTRATION 1 (2) MASS CONCENTRATION 1 (2) MASS 1ANALYSES TRATION b MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION -VOLATILE COMPOUNDS (continued) 22V. Methylene <0. 00500 <0.049 1 Mg/L 1b. n/a n/a n/a Chloride (75-09-2) 23V. 1,1,2,2- Tetrachloroethane x <0.00100 <0 . 010 1 mg/L 1b. n/a n/a n/a �79-34- ) 24V. Tetrachloro- x <0.00100 <0 . 010 1 mg/L 1b. n/a n/a n/a ethylene (127-18-4) 25V Toluene x <0. 00500 <0.049 1 Ing/L 1b. n/a n/a n/a (108-88-3) 26V. 1 2-Trans- Dichloioethylene x <0.00100 <0 . 010 1 mg/L 1b. n/a n/a n/a (156 60-5) 27V. 1,1,1-Trichloro- X <0.00100 <0.010 1 mg/L 1b. n/a n/a n/a ethane (71-55-6) 28V 1,1,2-Trichloro- X <0.00100 <0 . 010 1 mg/L 1b. n/a n/a n/a ethane (79-00-5) 29V Trichloro- <0.00100 <0. 010 1 mg/L 1b. n/a n/a n/a ethylene (79-01-6) 30V. Tnchloro- fluoromethane x <0.00500 <0.049 1 mg/L 1b. n/a n/a n/a (75-69-4) 31V. Vinyl Chloride x <0.00100 <0 . 010 17 mg/L 1b. n/a n/a n/a (75-01-4) GC/MS FRACTION - ACID COMPOUNDS IA. 2-Chlorophenol <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (95-57-8) 2A. 2,4-Dichloro- <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a phenol (120-83-2) 3A. 2,4-Dimethyl- <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a phenol (105-67-9) 4A. 4,6-Dinitro-0- x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a Cresol (534-52-1) 5A. 2,4-Dinitro- x <0.0100 <0.098 1 Mg/L 1b. n/a n/a n/a phenol (51-28-5) 6A. 2-Nitrophenol x <0.0100 <0.098 I mg/L 1b. n/a n/a n/a (89-75-5) 7A. 4-Nitrophenol <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (100-02-7) BA. P-Chloro-M- <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a Cresol (59-50-7) 9A Pentachloro- X <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a phenol (87-M5) 10A. Phe6oll x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (106-95-2) I 1 IA. 2,4,&Trichloro- x <0098 . T 1 Mg/L 1b. I n/a n/a n/a I phenol (88-05-2) - - EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE DEQ-CFW-00079878 rONTINliFn FROM THE FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1 POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b C. a MAXIMUM DAILY VALUE (rfmwdable) VALUE (ifavailable) I AVERAGE VALUE CAB NUMBER TESTING BELIEVED BELIEVED --.OF '1'J ' a.CONCEN- b NO. OF (1) (1) (1) (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION1 (2)MASS RATIONJ CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b. MASS CONCENTRATION1 (2)MASS ANALYSES GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1 B. Acenaphthene x <0.00100 <0.01 I I mg/L 1b. n/a n/a n/a (83-32-9) 2B. Acenaphtylene x <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a (208-96-8) 3B. Anthracene x <0.00100 <0.01 I mg/L 1b. n/a n/a n/a (120-12-7) 4B. Benzidine (92-87-5) <0 . 0100 <0 . 098 1 mg/L 1b. n/a n/a n/a 5B, Benzo (a) Anthracene <0.00100 <0.01 I mg/L 1b. n/a n/a n/a (56-55-3) 6B Benzo (a) x <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a Pyrene (50-32-8) 7B. 3,4-Benzo- fluoranthene x <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a (205-99-2) 8B. Benzo (glu) x <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a Perylene (191-24-2) 9B Benzo (k) Fluoranthene x <0.00100 <0.01 1 Mg/L 1b. n/a n/a n/a (207-08-9) 10B. Bis (2-Ch1nm- cihw�v) Methane x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (111-91-1) 11 B. Bis (2-Clyloff)- edryo Ether x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (111-44-4) 12B. Bis (2- Chlorolvopropyf x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a Ether (102-80-1) 1313. Bis (2-Elln-1- hego Phthalate x <0.00300 <0.029 1 mg/L 1b. n/a n/a n/a (117-81-7) 14B 4-Bromophenyl Phenyl Ether x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (101-55-3) 15B. Butyl Benzyl x <0 . 00300 <0.029 1 mg/L 1b. n/a n/a n/a Phthalate (85-68-7) 16B. 2-Chloro- naphthalene x 0.00100 <0.01 1 mg/L 1b. n/a n/a n/a (91-58-7) 17B. 4-Chloro- phenyl Phenyl Ether <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (7005-72-3) 18B Chrysene x <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a (218-01-9) 19B Dibenzo (a,h) Anthracene A <0.00100 <0.01 1 mg/L 1b. n/a n/a n/ja (53-70-3) I 20B. 1,2-Dichloro- <0.00100 <0.01 1 mg/L 1b. n/a n/a n/a benzene (95-50-1) 1 1 21 B. 1,3-Di-chloro- x <0.0010 I 1 mg/L I 1b. n/a n/a n/a I benzene (541-7a-1) EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 DEQ-CFW-00079879 CONTINUED FROM PAGE V-6 2. MARK "X" 3 EFFLUENT 4. UNITS 5 INTAKE (optionan 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c.LONG TERM AVRG, a. LONG TERM AND a. b. c a. MAXIMUM DAILY VALUE (ffavadable) I VALUE (Ifulflilable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- )NO.OF (1) (ifavad REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS NTRATION ICONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION 1 (2) MASS JAALYSES N GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continueef) 22B. 1,4-Dichloro- x <0.00100 <0.001 1 Mg/L 1b. n/a n/a n/a benzene (106-46-7) 23B. 3,3-Dichloro- <0.0100 <0.098 1 Mg/L 1b. n/a n/a n/a benzidine (91-94-1) 248. Diethyl Phthalate (84-66-2) A <0.00300 <0 . 029 1 mg/L 1b. n/a n/a n/a 25B. Dimethyl Phthalate <0.00300 <0.029 1 mg/L 1b. n/a n/a n/a 26B. Di-N-Butyl x <0.00300 <0.029 1 Mg/L 1b. n/a n/a n/a Phthalate (84-74-2) 27B. 2,4-Dinitro- x <0.0100 <0.098 1 mg/L 1b, n/a n/a n/a toluene (121-14-2) 28B. 2,6-Dinitro- x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a toluene (606-20-2) I 29B. Di-N-Octyl Phthalate (117-84-0) x <0.00300 <0.029 1 mg/L 1b. n/a n/a n/a 30­B. 1,2-Diphenyl- hydrazine (as Azo- x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a benzene) (122-66-7) 31B Fluoranthene (206-44-0) x <0.00100 <0.001 1 mg/L 1b. n/a n/a n/a 32B. Fluorene (86-73-7) x <0.00100 <0.001 1 mg/L 1b. n/a n/a n/a 33B. Hexachloro- benzene (118-74-1) x <0.00100 <0.001 1 mg/L 1b. n/a n/a n/a 34B. Hexachloro- butadiene (87-68-3) x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a 7-B. Hexachloro- cyclopentadiene x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (77-47-4) 36B Hexachloro- ethane (67-72-1) x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a 37B. Indeno (1,2, 3-cd) Pyrene x <0.00100 <0.001 1 mg/L 1b. n/a n/a n/a (193-39-5) 38B Isophorone x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (78-59-1) I 39B. Naphthalene x <0.00100 <0.001 1 mg/L 1b. n/a n/a n/a (91-20-3) 40B. Nitrobenzene x <0.0100 <0.098 1 mg/L 1b. n/a n/a n/a (98-95-3) 41B. N-Nitro- sochmethylarnme x- <0.0100 <0.098 1 Mg/L 1b. n/a n/a n/a (62-75-9) 1 1 428. N-Nitrosodi- N-Propylamine x <0.0100 <0.098 1 Mg/L n/a n/a n/a (621 -64-7) EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE DEQ-CFW-00079880 rnNTINIIFn FROM THE FRONT 2 MARK "X" 3 EFFLUENT 4. UNITS 5 INTAKE (opnonal) 1. POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b c a. MAXIMUM DAILY VALUE (rfavmlable) VALUE (favadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF 1 1 1 1 (favailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION - BASEINEUTRAL COMPOUNDS (connnuet� 43B. N-Nitro- sodiphenylamine <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (86-30-6) 44B Phenanthrene A <0.00100 <0.001 1 mg/L lb. n/a n/a n/a (85-01-8) 4 (129-00-0) 9-00-0) <0.00100 <0.001 1 mg/L lb. n/a n/a n/a 468. 1,2,4-Tn- chlorobenzene <0.0100 k.0981 1 mg/L lb. n/a n/a n/a (120-82-1) GC/MS FRACTION - PESTICIDES 1P.Alddn (309-0D-2) <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a 2P.a-BHC X <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a 4-6 (319-8) HC 319-6 (319-85-7) <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a 4Py-BHC N, z <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (58-89-9) 5P.6-BHC <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (319-86-8) 6P.Chlordane <0.000050 <0.005 1 mg/L lb. n/a n/a n/a (57-74-9) 7P.4,4'-DDT <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (50-29-3) 8P.4,4'-DDE (72-55-9) <0.040050 <5e-4 1 mgJL lb. n/a n/a n/a 9P.4,4'-DDD <0.000050 <5e-4 1 mgJL lb. n/a n/a n/a (72-54-8) 10P. Dieldnn (60-57-1) <0.000050 <5e-4 1 mgJL lb. n/a n/a n/a 11P.a-Enosulfan v <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (115-29-7) 12P. (3-Endosulfan (115-29-7) <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a 13P Endosulfan Sulfate <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (1031-07-8) 14P Endrin <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (72-20-8) 15P.Endnn Aldehyde <0.000050 <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (7421-93-4) 16P. Heptachlor (76-44-8) �/ ^ <0.000OSQ <5e-4 1 mg/L lb. n/a n/a n/a EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 DEQ-CFW 00079881 AIR 9 Ed I will) EPA I D. NUMBER (copyfroin hein I ofTorin 1) OUTFALL NUMBER rONTIMliFn FRnM PA(' F V-8 I NCD 047 368 642 1 001 1 2. MARK "X" 3. EFFLUENT 4 UNITS 5. INTAKE (opuonaO 1. POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b. c a. MAXIMUM DAILY VALUE (ifavaihible) VALUE (favadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF --T (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION 1_(2) MASS ANALYSES GC/MS FRACTION - PESTICIDES (continuee! 17P. Heptachlor Epoxide A <0.000050 <5e-4 1 Mg/L lb. n/a n/a n/a (1024-57-3) 1 8P. PC B-1 242 x <0.000500 <0.005 1 mg/L lb. n/a n/a n/a (53469-21-9) 19P. PCB-1254 x <0.000500 <0.005 1 mg/L lb. n/a n/a n/a (11097-69-1) 20P. PCB-1221 <0.000500 <0.005 1 Mg/L lb. n/a n/a n/a (11104-28-2) 21P. PCB-1232 (11141-16-5) x <O.00OSOO <0.005 1 mg/L lb. n/a n/a n/a 22P. PCB-1248 (12672-29-6) <0.000500 <0.005 1 mg/L lb. n/a n/a n/a 23P. PCB-1260 (1 1096-82-5) x <0.000500 <0.005 1 Mg/L lb. n/a n/a n/a 24P. PCB-1016 (12674-11-2) x <0.000500 <0-005 1 mg/L lb. n/a n/a n/a 25P.Toxaphene (8001-35-2) 1 A I I <0.000500 I <0.005 I I 1 mg I /L lb. n/a n/a I n/a EPA Form 3510-2C (8-90) PAGE V-9 DEQ-CFW-00079882 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copvfrom Ifem I ofl,arm 1) on separate sheets (use the same fonnaf) instead of completing these pages. NCD 047 368 642 SEE INSTRUCTIONS. OUTFALL NO. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) 002 PART A -You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 3. UNITS 4. INTAKE 2. EFFLUENT (spec{fv fblank) (apllonaO b. MAXIMUM 30 DAY VALUE c LONGTERM AVRG. VALUE a. LONG TERM a. MAXIMUM DAILY VALUE (ifavadabde) (rfavailable) AVERAGE VALUE d. NO OF a. CONCEN- b. NO. OF 1 1 1 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES a. Biochemical Oxygen 3.9 762.1 3.9 762.1 1.4 185.7 12 mg/L lb. n/a n/a n/a Demand (BOD) b. Chemical Oxygen 33.7 4898 33.7 4898 4.37 458.6 12 mg/L lb. n/a n/a n/a Demand(COD) c. Total Organic Carbon 12.8 1135 1 mgJL lb. n/a n/a n/a Totald. Suspended Solids(7SS� Solids 10.6 939.7 1 mg/L lb, n/a n/a n/a e. Ammonia (asl) 0.410 36.3 1 mgJL lb. n/a n/a n/a f.Flow VALUE 34,791 VALUE 26.813 VALUE 14.556 1095 MGD MGD VALUE n/a n/a g. Temperature VALUE 22.0 VALUE 18.8 VALUE 14.1 188 °C VALUE n/a n/a (uanrer) h Temperature VALUE 33.0 VALUE 31.1 VALUE 30.0 19 0 °C VALUE n/a n/a (summer} MINIMUM MAXIMUM MINIMUM MAXIMUM I. pH 6.11 8.16 n/a n/a 647 STANDARD UNITS PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present Mark "X" In column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2 MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opuonal) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG VALUE a. LONG TERM AVERAGE AND a b a. MAXIMUM DAILY VALUE (favadable) (favadable) VALUE CAS NO. BELIEVED BELIEVED d. NO. OF a. CONCEN- b. NO. OF (1) (1) (1) (1) (afavardable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b MASS CONCENTRATION (2) MASS ANALYSES a. Bromide (24959-67-9) b. Chlorine, Total �/ X 0.14 12.4 1 mg/L lb. n/a n/a n/a Residual C.Color X 27 n/a 1 PCU n/a n/a n/a n/a d Fecal Coliform est . 2 n/a 1 col/dL n/a n/a n/a n/a e. Fluoride (16984-48-8) X 35.1 4110 35.1 4110 17.3 1783 12 mg/L lb. n/a n/a n/a f.Nitrate-Nitnte 2.4 442.9 2.4 442.9 1.04 127.5 36 mg/L lb. n/a n/a n/a (as M EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE DEQ-CFW 00079883 A�• ITEM V-B CONTINUED FROM FRONT 2. MARK"X" 3. EFFLUENT 4. UNITS 5. INTAKE (opnona! 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. VALUE a. LONG TERM AND a b. a. MAXIMUM DAILY VALUE (ifavadable) (favejdable) AVERAGE VALUE CAS NO. BELIEVED BELIEVED d NO. OF a. CONCEW b. NO. OF (1) (1) (1) (1) — (ifavadable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES_ g. Nitrogen, Total Organic (as X 0.362 32.1 1 mg/L 1b. n/a n/a n/a N) h. Oil and x �'4 76 <422 I Mg/L 1b. n/a n/a n/a Grease . i. Phosphorus (as P), Total x 1.2 154 1.2 154 0.8 85.8 36 mg/L 1b. n/a n/a n/a (7723-14-0) 1 I. Radioactivity I (1) Alpha, Total x (2) Beta, Total A (3) Radium, x Total (4) Radium 226, x Total k. Sulfate (also,) x 105 9309 1 mg/L 1b. n/a n/a n/a (14809-79-8) I. Sulfide (-,9 x m. Sulfite (-SO-0 x (14265-45-3) n. Surfactants x 0.552 48.9 1 mg/L 1b. n/a n/a n/a o. Aluminum, Total x 1.27 112.6 1 Mg/L 1b. n/a 11/a n/a (7429-9()-5) p. Barium, Total (7440-39-3) x q Boron, Total 'y (7440-42-8) r. Cobalt, Total x (7440-48-4) s Iron, Total x 1.15 102.0 1 mg/L 1b. n/a n/a n/a (7439-89-6) I. Magnesium, Total X 2.26 200.4 1 mg/L 1b. n/a n/a n/a (7439-954) u. Molybdenum, Total x (7439-98-7) v. Manganese, Total x 0.069 6.12 1 mg/L 1b. n/a n/a n/a (7439_96_5) w. Tin, Total (7440-31-5) A x. Titanium, Total x (7440-32-6) 1 EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 DEQ-CFW-00079884 i ' 14 EPA I.D. NUMBER (copy from loem 1 ofFonn 1) OUTFALL NUMBER r nkl-rlkl"Cn CDr10.A Denc v nc cnonA r INCD 047 368 642 002 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industnes, nonprocess wastewater outfalls, and nonrequrred GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant of you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl4, 6 dinatrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged Note that there are 7 pages to this part, please review each carefully Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opaonal) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. . a. LONG TERM AND a b c a. MAXIMUM DAILY VALUE (rfavadable) VALUE (ifavadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b NO OF (ifavadable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b MASS CONCENTRATION (2} MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1M. Antimony, Total <0.002 <0.177 1 mg/L lb. n/a n/a n/a (7440-36-0) 2M Arsenic, Total <0.005 <0.443 1 mg/L lb. n/a n/a n/a (7440-38-2) 3M. Beryllium, Total <0.001 <0.089 1 mg/L lb. n/a n/a n/a (7440-41-7) 4M Cadmium, Total X <0.002 <0.177 1 mg/L lb. n/a n/a n/a (7440-43-9) 5M.Chromium, <0.005 <0.433 1 mg/L lb. n/a n/a n/a Total (7440-47-3) 6M. Copper, Total 0.005 0.443 1 mgfL lb. n/a n/a n/a (7440-50-8) 7M. Lead, Total <0.003 <0.266 1 mg/L lb. n/a n/a n/a (7439-92-1) 8M Mercury, Total \/ X <0.0002 <0.018 1 mg/L lb. n/a n/a n/a (7439-97-6) 9M. Nickel, Total <0.005 <0.433 1 mg/L lb. n/a n/a n/a (7440-02-0) 10M.Selenium, <0.005 <0.433 1 mgfL lb. n/a n/a n/a Total (7782-49-2) 11 M. Silver, Total �,/ <0.002 <0.177 1 mg/L lb. n/a n/a n/a (7440-22-4) 12M. Thallium, <0.005 <0.433 1 mg/L lb. n/a n/a n/a Total (halliu 8-0) Zinc, Total 0. 008 0. 709 1 mg/L l b. n/a n/a n/a (7aa (744o-ss-s) 14M. Cyanide, <0.005 <0.433 1 mg/L lb. n/a n/a n/a Total (57-12-5) 15M. Phenols, 0.0433 3.84 1 mg/L lb. n/a n/a n/a Total DIOXIN 2,3,7,8-Tetra- \ / dESCRIBE RESULTS Not applicable chlorodibenzo-P- Dioxin (1764-01-6) /}�\ EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE DEQ-CFW 00079885 F61011TRIFITIN CONTINUED FROM THE FRONT 2 MARK"X" 3. EFFLUENT 4 UNITS 5. INTAKE (opuona� 1 POLLUTANT ib. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b c a MAXIMUM DAILY VALUE (i(avadable) VALUE (tfavadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b NO. OF (1) (l (1) (1) (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION1 (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b. MASS CONCENTRATION I (2)MASS ANALYSES GC/MS FRACTION -VOLATILE COMPOUNDS 1V. Accrolein (107-02-8) 'y <0 . 0500 <4 . 433 1 mg/L 1b. n/a n/a n/a 2V. Acrylonitrile (107-13-1) x <0 . 0100 <0.887 1 mg/L 1b. n/a n/a n/a 3V. Benzene (71-43-2) A <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 4V. Bis (Chloro- meil�vr Ether x Not Req ired per NCDWR NPDES PermittIg Unit (542-88-1) I 5V Bromoform (75-25-2) x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 6V. Carbon Tetrachloride x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (56-23-5) 7V. Chlorobenzene x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (108-90-7) 8V. Chlorodi- bromomethane x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (124-48-1) 9V. Chloroethane (75-00-3) x <0.00500 <0.443 1 mg/L 1b. n/a n/a n/a 1 OV. 2-Chloro- ethylvinyl Ether <0.0500 <4.433 1 mg/L lb. n/a n/a n/a (110-75-8) /AY\ 1 1V. Chloroform (67-615-3) x 0.0248 2.199 1 mg/L 1b. n/a n/a n/a 12V. Dichloro- bromomethane x 0.00422 0.374 1 mg/L 1b. n/a n/a n/a (75-27-4) 13V, Dichloro- difluoromethane x <0.00500 <0.443 1 mg/L 1b. n/a n/a n/a (75-71-8) 14V. 1,1-Dichloro- ethane (75-34-3) x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 15V. 1,2-Dichloro- ethane (107-06-2) A <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 18V. 1,1-Dichloro.- x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a ethylene (75-35-4) I 17V. 1,2-Dichloro- propane (78-87-5) \ / A <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 18V. 11,3-Dichlorc, propylene x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (542-75-6) I I 19V. Ethylbenzene x <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (100-41-4) 20V Methyl A \ Z <0.00500 <0.443 1 Mg/L 1b. n/a n/a n/a Bromide (74-83-9) 21V. Methyl X_ <0.00250 <0.222 1 Mg/L 1b. n/a n/a n/a Chloride (74-87-3) EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5 DEQ-CFW-00079886 r'nNITIMI IPM 97PnRA D&r'r: %I -A 2. MARK "X" 3. EFFLUENT 4. UNITS 5 INTAKE (opaona! 1. POLLUTANT b, MAXIMUM 30DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b, c a. MAXIMUM_D_AIUYVALUEJ (ifavadabl VALUE (ifavadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEW b. NO OF (1) (1) (1) (ifavadable) REQUIRED PRESENT ABSENT CONCENTRATION 1 (2) MASS I CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION -VOLATILE COMPOUNDS (connnued) 22V. Methylene x <0.00500 <0.443 1 mg/L 1b. n/a n/a n/a Chloride (75-09-2) 23V. 1,1,2,2- Tetrachloroethane x <0 . 00100 <0.089 1 mg/L 1b. n/a n/a n/a (79- 4-5) 24V. Tetrachloro- x <0.00100 <0.0139 1 mg/L 1b. n/a n/a n/a ethylene (127-18-4) I I I I 25V. Toluene x <0.00500 <0.443 1 mg/L 1b. n/a n/a n/a (108-88-3) 26V. 1,2-Trans- Dichloroethylene x <0 . 00100 <0.089 1 mg/L 1b. n/a n/a n/a (1 5r�60-5) 27V. 1,1,1-Trichloro- \ / <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a ethane (71-5&6) A I 28V. 1,1,2-Trichloro- A \ / I <0 . 00100 <0.089 1 mg/L 1b. n/a n/a n/a ethane (79-00-5) 29V Trichloro- x <0. 00100 <0.089 1 Mg/L 1b. n/a n/a n/a ethylene (79-01-6) 30V. Trichloro- fluoromethane x <0.00500 <0.443 1 mg/L 1b. n/a n/a n/a (75-69-4) 31V, Vinyl Chloride X 00100 <0.089T 1 mg/L 1b. n/a n/a n/a (75-01-4) GC/MS FRACTION -ACID COMPOUNDS 1A. 2-Chlorophenol <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (95-57-8) 2A 2,4-Dichloro- x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a phenol (120-83-2) 3A. 2,4-Dimethyl- x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a phenol (105-67-9) 4A. 4,6-Dinitro-0- x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a Cresol (534-52-1) 5A. 2,4-Dinitro- x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a phenol (51-28-5) 6A, 2-Nitrophenol x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (88-75-5) 7A. 4-Nitrophenol x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (100-02-7) BA. P-Chloro-M- A <0.0100 <0.887 1 Mg/L 1b. n/a n/a n/a Cresol (59-5D-7) 9A Pentachloro- x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a phenol (87-86-5) 10A. Phenol x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (108-95-2) I - 11 A, 2,4,6-Trichloro- X <0.0100 <0.887 1 m /L 1 1b. 1 n/a n/a n/a phenol (88-05-2) EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE DEQ-CFW-00079887 CONTINUED FROM THE FRONT 2. MARK"X" 3. EFFLUENT 4. UNITS 5 INTAKE (optional} 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a. b C. a. MAXIMUM DAILY VALUE (ifenwilable) VALUE (ifavailahle) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO. OF a. CONCEN- b NO. OF (1) (1) (1) (1) (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION 1 (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1 B. Acenaphthene x I <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (83-32-9) 2B, Acenaphtylene x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (208-96-8) 3B. Anthracene x <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (120-12-7) 4B. Benzidine (92-87-5) x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a 5B. Benzo (a) Anthracene x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a (56-55-3) 6B Benzo (a) x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a Pyrene (50-32-8) 7B. 3,4-Benzo- fluoranthene x <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (205-99-2) 8B. Benzo (ghi) Perylene (191-24-2) x <0.00100 <0.089 1 mg/L 1b. n/a n/a n/a 9B. Benzo (k) Fluoranthene x 0.00100 <0.089 1 Mg/L 1b. n/a n/a n/ (207-08-9) 10B. Bis (2-Chfom- eiho)(y) Methane x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (111-91-1) 11B Bis(2-Chlom- eiki3O Ether <0.0100 <0. 887 1 mg/L 1b. n/a n/a n/a (111-44-4) 12B. Bis (2- Chloroaoprqpyn x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a Ether(102-80-1) 13B. Bis (2-Ethrl- ' vo Phthalate \ / <0.00300 <0.266 1 mg/L 1b. n/a n/a n/a 7hex (11-81-7) 14B. 4-Bromophenyl Phenyl Ether x <0.0100 <0.887 1 Mg/L 1b. n/a n/a n/a (101-55-3) 15B Butyl Benzyl x <0.00300 <0.266 1 mg/L 1b. n/a n/a n/a Phthalate (85-68-7) I 16B. 2-Chloro- naphthalene <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (91-58-7) 17B. 4-Chloro- phenyl Phenyl Ether x <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (7005-72-3) 188. Chrysene <0.00100 <0.089 1 Mg/L 1b. n/a n/a n/a (218-01-9) 1 19B. Dibenzo (a,h) Anthracene x <0 . 00100 <0.089 1 Mg/L 1b. n/a n/a n/a (53-70-3) I 20B. 1,2-Dichloro- x <0.00100 <0.089 1 mg/L 1b. n/a n/a benzene (95-50-1) I [21 B. 1,3-Di-chloro- I enzene (541-73-1) \ .11 A 77t <0.00100 I <0.089 1 mg/L 1b. I n/a n/a EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 DEQ-CFW-00079888 rr)MTI?d P:n PPOKA PAr r: W-A 2. MARK "X" 3 EFFLUENT 4. UNITS 5 INTAKE (optional) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. a. LONG TERM AND a b c. a. MAXIMUM DAILY VALUE (fmwarrable) VALUE (favatlable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d NO OF a. CONCEN- b NO. OF (favarlablc) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continuer) 22B.1,4-Dichloro- v <0.00100 <0.089 1 mg/L lb. n/a n/a n/a benzene(106-46-7) 238.3,3-Dichloro- \/ x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a benzidine(91-94-1) 24B Diethyl Phthalate (84-66-2) v <0.00300 <0.226 1 mg/L lb. n/a n/a n/a 256. Dimelhyl Phthalate <0.00300 <0.226 1 mg/L lb. n/a n/a n/a (131 -11-3) 26B.Di-N-Butyl <0.00300 <0.226 1 mg/L lb. n/a n/a n/a Phthalate (84-74-2) 27B.2,4-Dinitro- <0.0100 <0.887 1 mg/L lb. n/a n/a n/a toluene (121-14-2) 28B.2,6-Dinitro- <0.0100 <0.887 1 mg/L lb. n/a n/a n/a toluene (606-20-2) 29B.Di-N-Octyl <0.00300 <0.226 1 mg/L lb. n/a n/a n/a Phthalate (117-84-0) 30B 1,2-Diphenyl- hydrazine (as Azo- <0.0100 <0.887 1 mg/L lb. n/a n/a n/a benzene) (122-66-7) 31B.Fluoranthene <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (206-44-0) 32B.Fluorene <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (86-73-7) 33B. Hexachloro- <0.00100 <0.089 1 mg/L lb. n/a n/a n/a benzene(118-74-1) 34B.Hexachloro- <0.0100 <0.887 1 mgfL lb. n/a n/a n/a butadiene (87-68-3) 35B. Hexachloro- cyclopentadiene <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (77-47-4) 36BHexachloro- x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a ethane (67-72-1) '3-76. indeno (1,212,3-c-cd)Pyrene <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (193-39-5) 38B.Isophorone <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (78-59-1) 39B.Naphthalene <0.00100 <0.089 1 mgfL lb. n/a n/a n/a (91-20-3) 40B. Nitrobenzene v <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (98-95-3) ^ 416 N-Ndro- sodamethylamine <0.0100 <0.887 1 mgfL lb. n/a n/a n/a (62-75-9) 42B. N-Nitrosodi- - N-Propylamine <0.0100 <0.887 1 mgfL lb. n/a n/a n/a (621-64-7) EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE DEQ-CFW 00079889 CONTINliFn FROM THE FRONT 2. MARK "X" 3 EFFLUENT 4. UNITS 5. INTAKE (opnonan 1. POLLUTANT b. MAXIMUM 30 DAY VALUE C. LONG TERM AVRG. a. LONG TERM AND a b. c a MAXIMUM DAILY VALUE (ifavailable.) VALUE (ifavadable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. NO OF a CONCEN- (1) b. NO OF (1) 1 (ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION1 (2)MASS ICONCENTRATIONI (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b. MASS CONCENTRATION1 (2)MASS ANALYSES GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (conanieeco 43B. N-Nitro- sodiphenylamine x <0.0100 <0.887 1 Mg/L 1b. n/a n/a n/a (86-30-6) 44B Phenanthrene x <0 . 00100 <0.089 1 Mg/L 1b. n/a n/a n/a (85-01-8) 45B. Pyrene (129-00-0) x i <0.00100 <0.089 i I mg/L 16. n/a n/a n/a 46B. 1,24-Tri- chlorobenzene x 0.0100 k0.887 1 Mg/L 1b. n/a n/a n/a (120-82-1) GC/MS FRACTION - PESTICIDES 1P. Aldrin x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (309-00-2) 2P. a-BHC x <0.000050 <0.005 1 mg/L 1b. n/*a n/a n/a (319-84-6) 3P. P-BHC (319-85-7) x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a 4P. y-BHC x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (58-89-9) I - 5P - 5-BHC x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (31 M6-8) 6P. Chlordane <0.000050 <0.044 1 mg/L 1b. n/a n/a n/a (57-74-9) 1 1 7P. 4,4'-DDT x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (50-29-3) 8P. 4,4'-DDE (72-55-9) x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a 9P. 4,4'-DDD <O.00OOSO <0.005 005 1 mg/L 1b. n/a n/a n/a (72-54-8) /Y\ I I 1 OP. Dieldrin (60-57-1) x <0.000050 <0.005 1 Mg/L 1b. n/a n/a n/a 11 P. cc-Enosulfan x <0.000050 <0.005 1 Mg/L 1b. n/a n/a n/a (115-29-7) I 12P. P-Enclosulfan (115-29-7) \ / A <O.00OOSO <0.005 1 mg/L 1b. n/a n/a n/a 13P. Endosulfan Sulfate x 0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (1031-07-8) 14P Endrin x <0.000050 <0.005 1 mg/L 1-b. n/a n/a n/a (72-20-8) 15P. Endrin Aldehyde x <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (7421-93-4) 16P. Heptachlor A <0.000050 <0.005 1 mg/L 1b. n/a n/a n/a (76-44-8) . EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 DEQ-CFW-00079890 EPA I.D. NUMBER (copy.froin lie?n I ofl,'e)nn 1) OUTFALL NUMBER PnKITIKII 1CM CDnRA DAr-r k/ 0 1 NCD 047 368 642 1 002 1 2. MARK "X" 3 EFFLUENT 4. UNITS 5. INTAKE (nptionan 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c.LONG TERM AVRG a. LONG TERM AND a. MAXIMUM DAILY VALUE (ifmwilable) I VALUE (ifavailable) AVERAGE VALUE CAS NUMBER =TES�INGD BELIEVED � BELIEVED d. NO. OF a. CONCEW b NO. 0 F (ifavailable) REQUIRE PRESENT ENT ABSENT CONCENTRATION1 (2)MASS ICONCENTRATIONI (2)MASS ICONCENTRATIONI (2)MABJANALYSES S TPATION b.MASS r-.oNj(-.pNTRATI0Hl (2)MASS ANALYSES GC/MS FRACTION - PESTICIDES (continued) 17P Heptachlor Epoxide x <0.000050 <0.005 Mg/L lb. n/a n/a n/a (1024-57-3) 1 BP. PCB-1 242 x <0.000500 <0.044 mg/L lb. n/a n/a n/a (53469-21-9) 19P PCB-1254 <0.000500 <0.044 1 Mg/L lb. n/a n/a n/a (11097-69-1) 20P PCB-1221 x <0.000500 <0.044 1 mg/L lb. n/a n/a n/a (11104-28-2) 21232 <0.000500 <0.044 1 mg/L lb. n/a n/a n/a (11141-16-5) 22P. PCB-1248 (12672-236) x- <0.000500 <0.044 1 mg/L lb. n/a n/a n/a 23P. PCB-1260 (11096-82-5) x 1 1 <0.000500 <0.044 1 mg/L lb. n/a n/a n/a 24P. PCB-1016 (12674-11-2) A <0.000500 <0.044 1 Mg/L — lb. n/a n/a n/a - 25P.Toxaphene x <0.000500 <0 044 1 mg/L lb. n/a n/a n/a (8001-35-2) . I I EPA Form 3510-2C (8-90) PAGE V-9 DEQ-CFW-00079891 Chemours Company — Fayetteville Works NPDES Permit No. NCO003573 Supplemental Information — Permit Renewal Application — April 27, 2010 The Chemours Company — Fayetteville Works operates a Class 3 Wastewater Treatment Plant which is comprised of a single -stage activated sludge biological system. Excess sludge is removed from the system by diverting part of the Recycled Activated Sludge (at approximately 0.6% solids) from the clarifiers to a Dissolved Air Floatation ("DAF") unit for initial thickening. The sludge from the DAF (at approximately 3% solids) is transferred to a Mix Tank where polymer agents are added to enhance the dewatering process. The semi -thickened sludge is transferred from the Mix Tank to a Rotary Filter for final thickening, whereby the sludge is thickened to 6% solids. The thickened sludge is then transferred to a Screw Press where it is dewatered to a concentration of 9-20% solids. Following the Screw Press, the sludge is typically dried in steam heated dryers to a concentration of 40-55% solids. The dried sludge, or on occasion the dewatered sludge, is transported off -site to a commercial Subtitle D landfill. This sludge is currently being disposed of at the Waste Industries "Sampson County" Landfill near Roseboro, NC. In 2015, the average weekly quantity of generated wasted sludge was approximately 35,000 lb. DEQ-CFW-00079892 Chemours Company — Fayetteville Works NPDES Permit No. NCO003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Current Facility Wastewater Management Process wastewater and storrnwater from the various manufacturing areas are collected in the respective area sumps and ultimately conveyed via a gravity flow underground process sewer pipe to the facility's central wastewater treatment plant ("WWTP"). Sanitary sewage is conveyed via a separate underground sewer system to the WWTP. The permitted flowrate of the WWTP is 2.0 MGD, with an actual average flowrate of approximately 1.2 MGD. This untreated process wastewater is commingled in the WWTP Influent Sump where it is pumped to an 850,000-gallon Equalization Basin. The Equalization Basin is mixed with two floating submerged mixers. Three floating surface aerators in the basin cool and aerate the incoming wastewater. A 175,000-gallon Emergency Retention Tank is available for temporary storage of untreated wastewater which may need additional treatment or acclimation in the WWTP activated sludge process at a controlled rate that allows for proper biological treatment. Untreated wastewater from the Equalization Basin is normally pumped to a 250,000-gallon Predigester Tank in which initial biological activity with the WWTP activated sludge begins. The Predigester Tank is aerated. The partially treated wastewater from the Predigester Tank is pumped to a 1,700,000-gallon Aeration Tank. The Aeration Tank is the unit where the majority of the biological activity occurs. The Aeration Tank is aerated primarily by a diffused air system located in the bottom of the tank. The tank can have supplemental aeration via one or two floating Biomixersg that injects air through submerged rotors. The biologically treated wastewater is then sent to one of two in -ground clarifiers (119,000 gallons and 168,000 gallons respectively) or an above -ground 679,000-gallon clarifier; with all clarifiers being operated in parallel. The clarified treated effluent is discharged to and through Outfall 001. The wasted activated sludge is sent to a Dissolved Air Floatation (DAF) unit, then to a 47,000 gallon Sludge Storage Tank, and finally to a Rotary Filter for thickening. The thickened sludge is dewatered in a Sludge Press, and can be dried in a steam -heated dryer for additional moisture removal. The dewatered sludge or dewatered/dried sludge is transported off -site to a commercial Subtitle D landfill. Non -contact process cooling water and non -process stormwater are conveyed via surface ditches. In addition, excess riverwater flow and Outfall 001 effluent are discharged directly to a surface ditch. The combined, total flow of water from the site is discharged through and monitored at Outfall 002. The discharged treated wastewater is conveyed via an underground pipe to the Cape Fear River, where it enters the river at a point approximately 1,500 feet upstream of the William O. Huske Lock & Dam (aka Lock & Dam No. 3). DEQ-CFW-00079893 Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application April 27, 2016 I I # Chemours Fluoromonomers/Naflon@ Membrane Manufacturing Area: The Chemours Company — Fayetteville Works' Fluoromonomers / Nafiong Membrane manufacturing area produces several final products. ChemoursTM Nafion(b Membrane is a plastic film used in the chloroalkali industry and in electrochemical fuel cells. ChemoursTM Nafion(& Polymer Dispersions are used in the fabrication of thin films and coating formulations for fuel cells membranes, catalyst coatings, sensors, and a variety of electrochemical applications. The HFPO monomer and the Vinyl Ether monomers are used to manufacture various fluorochemical products such as ChemoursTM Teflon®. Wastewater generated from this manufacturing fLility is discharged to the Chemours' wastewater treatment plant. Chemours Polymer Processing Aid ("PPA") Manufacturing Area: The Chemours Company — Fayetteville Works' PPA manufacturing area produces a polymer processing aid. The processing aid produced in this unit is used in the manufacturing of fluoropolymers and fluorinated telomers,,but none of the produced processing aid is used at the Fayetteville Works site. All process wastewater generated from this manufacturing facility is collected and shipped off -site for disposal. No process wastewater from this manufacturing facility is discharged to the Chemours' wastewater treatment plant or to the Cape Fear River. Kuraray Butaciteg Manufacturing Area: The Kuraray America Inc. — Fayetteville Plant's Butacitel) manufacturing area produces two final products. KurarayTM Butaciteg Interlayer plastic sheeting is the final product used in safety glass such as automobile windshields. Polyvinyl butyral resin is shipped off -site as a transfer to other Kuraray locations for final processing. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Kuraray SentryGlasO Manufacturing Area: The Kuraray America Inc. — Fayetteville Plant's SentryGlas(k) manufacturing area produces KurarayTM SentryGlasg ionoplast interlayer laminate. SentryGlass interlayer is used for laminated safety glass in side, rear, and overhead automobile windows. It is also used in architectural applications desiring safety glass. There is no contact process wastewater generated from this manufacturing facility, therefore only sanitary waste from this area is treated in the Chemours' wastewater treatment plant. This manufacturing facility does discharge non -contact cooling water to a surface ditch and ultimately to Outfall 002. DuPont Polyvinyl Fluoride ("PVF") Manufacturing Area: The DuPont Company — Fayetteville Works' PVF manufacturing area produces polyvinyl fluoride resin that is used in the electronics industry as a backing for photovoltaic cells, as well as many other uses. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. DEQ-CFW-00079894 W Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27,201C. Alternate Application Schedule for §316(b) of the Clean Water Act Final regulations implementing §316(b) of the Clean Water Act, which establish requirements for cooling water intake structures at existing facilities, were published in the Federal Register on August 15, 2014 with an effective date of October 14, 2014. The Chemours Company — Fayetteville Works ("Chemours") operates a cooling water intake structure on the Cape Fear River that is subject to this new Federal Cooling Water Intake Structure Rule ("the Rule") as codified in 40 CFR Part 125. The Rule requires' the owner or operator of a facility subject to Subpart J whose currently effective permit expires after July 14, 2018, to submit to the Director the information required in the applicable provisions of 40 CFR 122.21(r) when applying for a subsequent permit. Pursuant to 40 CFR 125.95(a)(2), the owner or operator of a facility subject to Part 125 Subpart J, "Requirements Applicable to Cooling Water Intake Structures for Existing Facilities Under Section 316(b) of the Clean Water Act", whose currently effective permit expires prior to July 14, 2018, may request the Director to establish an alternate schedule for the submission of the information required in 40 CFR 122.21(r) when applying for a subsequent (renewed) permit. On October 20, 2015, a letter was sent from Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, to Dr. Sergei Chernikov, NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, requesting an alternate schedule whereby all the materials required by the Rule will be submitted with the 2021 renewal application. On February 26, 2016, a letter was sent from S. Jay Zimmerman, Director, NCDEQ Division of Water Resources, to Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, wherein the requested alternate schedule for submission of required CWIS information with the next permit renewal in 2021 was approved. A copy of Mr. Zimmerman's letter is attached to this application package. DEQ-CFW-00079895 Water Resources ENVIRONMENTAL QUALITY February 26, 2016 Mr. Michael E. Johnson, P.E. Environmental Manager Chemours Company 22828 NC Highway 87 West Fayetteville, North Carolina 28306-7332 PAT MCCRORY Goivnior �, ,,�'?- en Secrelcity S. JAY ZIMMERMAN Subject: Alternate CWA 316(b) Application Schedule NPDES Permit NCO003573 Fayetteville Works Bladen County Dear Mr. Johnson: Director The Clean Water Act Section 316(b) Cooling Water Intake Structure (CWIS) Final Rule outlines regulations and standards for the design and operation of cooling water intake structures under the NPDES program. Your current permit expires October 31, 2016, with renewal application due by May 4, 2016. Since your permit expires prior to July 14, 2018, under 40 CFR 125.95(a)(2), you have requested an alternative schedule for submission of CWIS permit application information required in 40 CFR Part 122.21( r). Based on Division review, an alternate schedule for submission of required CWIS information with the next permit renewal in 2021 is approved. This schedule date will be established in the 2016 permit renewal as well. Please note that facilities should begin to adapt their systems to comply with CWA Section 316(b) requirements. If you have any questions, please contact Tom Belnick-with the NPDES Permitting Unit at 919-807-6390 or via email: tom.beinick@ncdenr.gov Sinc.exely, S. Jay Zimmerman, P.G. Direc tor, r efDSirector, Division of Water Resources Cc: NPDES File Central File Ec: US EPA Region 4 US FWS NC WRC NC DWR/Fayetteville Region State ol'North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919 707 9000 DEQ-CFW-00079896 jt. Chemours Company — Fayetteville Works NPDES Permit No. NCO003573 In December 2002, the DuPont Company — Fayetteville Works began production of, ammonium perfluorooctanoate ("APFO"), which is the ammonium salt of perfluorooctanoic acid ("PFOA"). The renewed NPDES Permit No. NC0003573 that became effective on July 1, 2007, included a requirement for monthly monitoring of PFOA at Outfall 002. In 2006 the North Carolina Division of Water Quality ("DWQ"), in consultation with the North Carolina Division of Waste Management and the North Carolina Department of Health and Human Services, established an Interim Maximum Allowable Concentration ("IMAC") of 2 gg/L for PFOA, which was intended for the protection of groundwater as a source of drinking water. Following the issuance of this temporary health -based level, DWQ requested the assistance of the North Carolina Secretary's Science Advisory Board on Toxic Air Pollutants (*NCSAB") in reviewing the toxicological literature on PFOA and recommending to DWQ an update of the IMAC for PFOA in groundwater. On August 10, 2012, the NCSAB issued their recommendation to DWQ that the IMAC for PFOA in groundwater be reduced to I ptg/L. During the 3-year period from 2013 to 2015, the average monthly concentration of the final effluent discharge at Outfall 002 was 0.027 [tg/L PFOA, with a maximum concentration of 0.088 }Lg/L PFOA. During the same period, the average monthly concentration of the incoming water from the Cape Fear River to the site, which is 99% of the effluent flow at Outfall 002, was 0.012 ptg/L PFOA, with a maximum concentration of 0.031 µg/L PFOA. The production of APFO at this facility ceased in April 2013. The Chemours Company — Fayetteville Works (formerly the DuPont Company — Fayetteville Works) is requesting that the monthly monitoring requirement for PFOA at Outfall 002 be eliminated in the renewed NPDES Permit No. NC0003573 for the following reasons: • APFO is no longer manufactured at this facility and has not been produced at the facility since April 2013; • APFO is not and has never been used as a process aid or a raw material at this facility; • The 3-year average concentration at Outfall 002 was 0.027 Vg/L PFOA, versus the current NC-DWR IMAC of 2 gg/L PFOA and the NCSAB recommended I gg/L PFOA; and • PFOA is present at low concentrations throughout the Cape Fear River basin, and that background level of PFOA in the Cape Fear River water contributes to the concentration measured at Outfall 002. DEQ-CFW-00079897 J* Chemours- Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2010 Form 2C Permit Application — Bis(chloromethyl) ether Bis(chloromethyl) ether (CAS No. 542-88-1) was not analyzed for, and consequently was not reported on Page V-4 of Form 2C for both Outfall 001 and Outfall 002. On November 28, 2014, the State of Oregon's Department of Environmental Quality ("ODEQ") issued a memorandum (Note 1) addressing the issue of analyzing for bis(chloromethyl) ether ("BCME"). In this memorandum, ODEQ states: 66 Based on the chemical's rapid hydrolysis in water, there are no analytical methods to measure BCME in water samples. Currently, the only analytical techniques available for this compound are for air samples. Region 10 EPA staff queried its Manchester Environmental Lab in Port Orchard, WA about potential, analytical methods for BCME. Staff at the lab confirmed that there is no EPA method for BCME because of its rapid degradation in water." Because of the lack of an'EPA approved analytical method for bis(chloromethyl) ether in a water matrix, ODEQ concluded: Given its rapid hydrolysis in water, there are no recommended analytical methods for BCME in water samples. Because BCME is not quantifiable in wastewater, DEQ will not require permit holders to monitor or conduct reasonable potential analyses for this toxic pollutant." In an April 13, 2106, email from Tom Belnick, Super -visor of the NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, to Michael Johnson, Environmental Manager, Chemours Company — Fayetteville Works, Mr. Belnick stated: "I checked with our DWR analytical lab, and they concur with Oregon's position and are not aware of any labs using even R&D methods for this analyte. Therefore, you can omit this parameter from your application renewal." Note 1: http://www.deq.state.or.us/wq/standards/docs/toxics/BisChloromethylMemo.pdf DEQ-CFW-00079898