DEQ-CFW_00060752

EFFLU NT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH April YEAR 2010
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPCI� .GEF Jamie R. Lewis GRADE 3 PHONE [phone]
CERTIFIED'LABORATC I�� �ap� (Lumberton) (2) 1 _
CHECK BOX IF ORC HAS CHA�i M 13 �h n 1 PERSON(S) COLLECTING SAMPLES Jamie Lewis / Ray Beard ! Russ I otan
julu
Mail ORIGINAL and ONE COPY to:ATTN: CENTRAL FILES O7� A`l�
DIV. OF WATER QUALITY D •. X C� _%-) O
o""- -
DENR Oj A (SIGNATU E OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER n ry ry BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 S E r 8 LO�U ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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C
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FLOW
w
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~ a
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w W
20
Lu
C
a
EFF X
INF
}
Q I
�
HRS
HRS
YIN
MGD
'C
UNtTS
1
0800
24
Y
0.528
2
080o
24
0.512
3
08o0
24
0.544
4
o800
24
0.544
5
.o800
24
B
0.640
22
77W4
6
0800
24
B
0.752
23
7.73
7
0800
24
B
0.720
8
0800
24
B
0.752
9
0800
24
B
0.704
10
0800
24
0.672
11
o800
24
0.720
12
o800
24
Y
0.784
23
7.93
13
0800
24
Y
0.816
1410800
24
L Y
0.832
23
7.97
15
o800
24
Y
0.736
16
0800
24
Y
0.880
17
0800
24
0.864
18
0800
24
0.832
19
o800
24
Y
0.848
&22. ';
44111
111
2010800
24
Y
0.880
22
7.88
21
0800
24
Y
0.768
22
0800
24
Y
0.848
23
0800
24
Y
0.880
24
o800
24
0.864
25
0800
24
0.832
2610800
24
Y
0.672
23
7.72
27
oson
24
Y
0.848
22::
Rik7.70
28
0800
24
Y
0.720
21
7.63
29
0800
24 ''
Y
0.576
30
0800
24
Y
0.704
31
0800
24
AVERAGE
0.742
22
a
w w
a y
V Z W
N to p D
N 7 y f7
m Q _J
0 O
20.1 1 49.5
17.0 42.5
24.5 13.6
18.7 1 43.7
11.8 35.3
<14.1 40.3
<12.01 36.0
O z
F 2 N
v QUQ W
.O X CI
L =
U
PIF 1 uNL
MAXIMUM
0.880
2"
1..9
4L.4
�sr.a
co.0
MINIMUM
0.512
21
7.63
11.8
13.6
<5.0
Comp. (C) Grab (G)
G
G
C
C
G
C
Monthly Limit
2.0
191.3
317.8
PASS
Daily Limit
6-9
508.2
1030
05
DEM Form MR4 (12193)
* Holiday
DEQ-CFW 00060752

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01092
Zinc
Chlorine
01027
Cadmium
01105
Aluminum
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
01034
Chromium
31616
Fecal Coliform
71900 Mercury
32730
Total Phenolics
81551 Xylene
01037
Total Cobalt
34235
Benzene
01042
Copper
34481
Toluene
38260
MBAS
01045
Iron
39516
PCB's
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file w�hjthe state. per 15A NCAC 2B .0506 -
(b) (2) (D) _ I"
DEQ-CFW 00060753

f ` Al f `e OC -ed
EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH April YEAR 2010
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 3 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie Lewis / Ray Beard / Russell Rota
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY X GYVi:/L^� •
DENR (SIGNA.TUfZE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
00951
00665
00600
51521
1 00310
003,
FLOW
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0
0
Q
G
HRS
HRS
Y/N
MGD
"c
UNITS
Lb/Day
mg/L
mg/L
ug/L
mg/L
mg)
1
0800
24
Y
8.384
19
7.49
2
0800
24
7.896
3
oeoo
24
8.800
4
0800
24
8.248
6
108001
24 1
B
8.525 1
22
7.50
1 651
0.58
1 1.51
7
108001
24
B
8.824 124
7.62
0.05
8
08001
24 1
B
8.811
24
7.63
9
080o
24 1
B
8,862
23
1.51
10
0800
24
12.386
11
080o
24
13.056
=.
12
0800
24
Y
13.104
22
7.41
1310800
24
Y
13.120
21
7.51
623
1410800
24
Y
13.526
21
7.50
1510800
24
Y
-13.738
20 "
7.46
16108001
24
Y
13.120
21
7.41
17
08001
24 1
13.488
18
o800
24
1 13.373
19
oeoo
24
Y
1 13.587
21
7150
20
oeoo
24
Y
13.552
21
7.50
684
21
o800
24
Y
"12.704
21" ;
"I7,48 "
22
0800
24
Y
12.112
21
7.45
23
0800
24
Y
13.248
21
24
0800
24
13.718
25
0800
24
13.874
26
0800
24-1
Y
13.878
21
7.44
27
0800
24 "
Y
14.050
21"
7.43
28
0800
24
Y
14.214
21
7.39
761
29
0800
24
Y
13.978
.21
7.19
30
oeoo
24
Y
14.048
21
7.20
31
0800
24
AVERAGE
11.958
21
680
0.58
1.51
0.05
MAXIMUM
14.214
24
7.63
761
0.58
1.51
0.05
MINIMUM
7.896
19
7.19
623
0.58
1.51 1
0.05
mp. (C)' Grab (G)
G
G"
G
C
C
C
C
C
Monthly Limit
Daily Limit
6-9
7917
DEM Form MR-1 (12/93)
* Holiday
DEQ-CFW 00060754

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082
Color (ADM])
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
" ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
(b) (2) (D)
DEQ-CFW 00060755

4M.
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DuPont Fluoroproducts
Fayetteville Works Plant
22828 NC Highway 87 West
Fayetteville, NC 28306
August 12, 2010
DISCHARGE MONITORING REPORT - Amended April 2010
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Amended
001 and 002 Discharge Monitoring Report for the month of April 2010. The temperature
and pH readings were put on the opposite 001 and 002 spreadsheets.
If you have any questions, please contact Jamie Lewis at [phone].
JRL: j 1p
Attachment
cc: Ken Cook - ENGR, Old Hickory
J. R. Lewis - FW
J. L. Locklear - FW
File: F-1-3-4
E.I. du Pont de Nemours and Company
DEQ-CFW 00060756

DEQ-CFW-00060757