NCG030127_Letter RE Sample Results_20180821

G
IW
August 21, 2018
Semi -Annual Summary Stormwater DMR
NPDES Permit No. NCG030000
Certificate of Coverage No. NCG030127
Dear Administrator:
1709 Jake Alexander Blvd
Salisbury, NC 28146
Tel [phone]
Fax [phone]
Enclosed are two signed copies of the monthly Stormwater Discharge Monitoring Report (DMR) for the
Granges Americas, Inc Salisbury Plant covering the period of August 2018. The report covers monitoring
results for all July 2018. As required by General Permit No. NCG030000, samples are taken on a monthly basis
after measureable rainfall events, due to the exceedances for Copper and Zinc, above the benchmark values.
As of the September 2014 sampling event, we exceeded the benchmark values for both copper and zinc for a
fourth time. We made the proper notifications and received a letter back from Zahid S. Khan, a Regional
Engineer. We continue to conduct monthly monitoring and have initiated an Engineering Study to better
understand any sources of copper and zinc that may be affecting our monitoring results.
Should you have questions or comments, please contact me at [phone].
Ronnie Britt
Environmental Engineer
Granges Americas Inc- Salisbury, NC Site
Email: [e-mail]

aceAnalXical
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August 12, 2018
Robin Tolliver
Granges Americas
1709 Jake Alexander Blvd.
Salisbury, NC 28146
RE: Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Dear Robin Tolliver:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on August 02, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Terry Furr, Granges America, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 27

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Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 2 of 27

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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
STORMWATER SAMPLES
92394219
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92394219001
SW01
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA 625.1
PKS
59
PASI-C
EPA624.1
GAW
35
PASI-C
SM 2540D-2011
CEH
1
PASI-A
EPA 9040C
RLO
1
PASI-A
92394219002
SW03
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA625.1
PKS
59
PASI-C
EPA 624.1
GAW
35
PASI-C
SM 2540D-2011
CEH
1
PASI-A
EPA 9040C
RLO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Sample: SW01 Lab ID: 92394219001 Collected: 07/31/1804:12 Received: 08/02/1811:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND
mg/L
5.0
1
08/10/18 04:13
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
20.6
ug/L
5.0
1
08/10/18 04:30
08/11/18 18:07
7440-50-8
Lead
ND
ug/L
5.0
1
08/10/18 04:30
08/11/18 18:07
7439-92-1
Zinc
51.0
ug/L
10.0
1
08/10/18 04:30
08/11/18 18:07
7440-66-6
625 MSSV
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Acenaphthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
83-32-9
Acenaphthylene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
208-96-8
Anthracene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
120-12-7
Benzidine
ND
ug/L
49.0
1
08/06/18 10:19
08/08/18 18:47
92-87-5 L2
Benzo(a)anthracene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
56-55-3
Benzo(a)pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
101-55-3
Butyl benzylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08108/1818:47
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
111-44-4
2-Chloronaphthalene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
91-58-7
2-Chlorophenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
7005-72-3
Chrysene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
4.9
1
08/0611810:19
08/08/18 18:47
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
24.5
1
08/06/18 10:19
08/08/18 18:47
91-94-1
2,4-Dichlorophenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
120-83-2
Diethylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
84-66-2
2,4-Dimethylphenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
105-67-9
Dimethylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
131-11-3
Di-n-butylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
19.6
1
08/06/18 10:19
08/08/18 18:47
534-52-1
2,4-Dinitrophenol
ND
ug/L
49.0
1
08/06/18 10:19
08/08/18 18:47
51-28-5
2,4-Dinitrotoluene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
121-14-2
2,6-Dinitrotoluene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
606-20-2
Di-n-octylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08108/1818:47
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
117-81-7
Fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
206-44-0
Fluorene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
87-68-3
Hexachlorobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
77-47-4
Hexachloroethane
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
67-72-1
REPORT OF LABORATORY ANALYSIS
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Date: 08/12/2018 11:13 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Sample: SW01
Lab ID: 92394219001 Collected: 07/31/18 04:12
Received: 08/02/18 11:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qua]
625 MSSV
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
193-39-5
Isophorone
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
78-59-1
Naphthalene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
91-20-3
Nitrobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
98-95-3
2-Nitrophenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
88-75-5
4-Nitrophenol
ND
ug/L
49.0
1
08/06/18 10:19
08/08/18 18:47
100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
86-30-6
Pentachlorophenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
87-86-5
Phenanthrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
85-01-8
Phenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
108-95-2
Pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 18:47
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 18:47
88-06-2
Surrogates
Nitrobenzene-d5 (S)
65
%
10-120
1
08/06/18 10:19
08/08/18 18:47
4165-60-0
2-Fluorobiphenyl (S)
65
%
15-120
1
08/06/18 10:19
08/08/18 18:47
321-60-8
Terphenyl-d14 (S)
54
%
11-131
1
08/06/18 10:19
08/08/18 18:47
1718-51-0
Phenol-d6 (S)
35
%
10-120
1
08/06/18 10:19
08/08/18 18:47
13127-88-3
2-Fluoropheno] (S)
47
%
10-120
1
08/06/18 10:19
08/08/18 18:47
367-12-4
2,4,6-Tribromophenol (S)
69
%
10-137
1
08/06/18 10:19
08/08/18 18:47
118-79-6
624 Volatile Organics
Analytical Method: EPA624.1
Acrolein
ND
ug/L
5.0
1
08/08/18 22:27
107-02-8 L1
Acrylonitrile
ND
ug/L
50.0
1
08/08/18 22:27
107-13-1
Benzene
ND
ug/L
2.0
1
08/08/18 22:27
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
08/08/18 22:27
75-27-4
Bromoform
ND
ug/L
2.0
1
08/08/18 22:27
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/08/18 22:27
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
08/08/18 22:27
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
08/08/18 22:27
108-90-7
Ch]oroethane
ND
ug/L
2.0
1
08/08/18 22:27
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
08/08/18 22:27
110-75-8 c2
Chloroform
ND
ug/L
2.0
1
08/08/18 22:27
67-66-3
Chloromethane
ND
ug/L
2.0
1
08/08/18 22:27
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
08/08/18 22:27
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:27
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:27
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:27
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
08/08/18 22:27
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
08/08/18 22:27
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
08/08/18 22:27
75-35-4
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
08/08/18 22:27
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
08/08/18 22:27
78-87-5
cis-1,3-Dich]oropropene
ND
ug/L
2.0
1
08/08/18 22:27
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.0
1
08/08/18 22:27
10061-02-6
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except in full,
Date: 08/12/2018 11:13 PM
without
the written consent
of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01 Lab ID: 92394219001 Collected: 07/31/18 04:12 Received: 08/02/18 11:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH at 25 Degrees C
Date: 08/12/2018 11:13 PM
Analytical Method: EPA 624.1
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
110
120
93
%
Analytical Method: SM 254OD-2011
7.4
mg/L
Analytical Method:
EPA 9040C
6.9
Std. Units
2.0
1
08/08/18 22:27
100-41-4
2.0
1
08/08/18 22:27
75-09-2
2.0
1
08/08/18 22:27
79-34-5
2.0
1
08/08/18 22:27
127-18-4
2.0
1
08/08/18 22:27
108-88-3
2.0
1
08/08/18 22:27
71-55-6
2.0
1
08/08/18 22:27
79-00-5
2.0
1
08/08/18 22:27
79-01-6
2.0
1
08/08/18 22:27
75-01-4
70-130
1
08/08/18 22:27
460-00-4
70-130
1
08/08/18 22:27
2037-26-5
70-130
1
08/08/18 22:27
17060-07-0
2.9
1
08/03/18 22:54
0.10
1
08/10/18 21:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Sample: SW03
Lab ID: 92394219002
Collected:
07/31/18 04:52
Received: 08/02/18 11:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND
mg/L
5.0
1
08/10/18 04:13
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
12.8
ug/L
5.0
1
08/10/18 04:30
08/11/18 18:19
7440-50-8
Lead
ND
ug/L
5.0
1
08/10/18 04:30
08/11/18 18:19
7439-92-1
Zinc
76.5
ug/L
10.0
1
08/10/18 04:30
08/11/18 18:19
7440-66-6
625 MSSV
Analytical Method: EPA 625.1 Preparation Method:
EPA 625.1
Acenaphthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
83-32-9
Acenaphthylene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
208-96-8
Anthracene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
120-12-7
Benzidine
ND
ug/L
49.0
1
08/06/18 10:19
08/08/18 19:16
92-87-5 L2
Benzo(a)anthracene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
56-55-3
Benzo(a)pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
101-55-3
Butyl benzylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
4.9
1
08/06/18 10:19
08108/1819:16
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
111-44-4
2-Chloronaphthalene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
91-58-7
2-Chlorophenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
7005-72-3
Chrysene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
24.5
1
08/06/18 10:19
08/08/18 19:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
120-83-2
Diethyl phthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
84-66-2
2,4-Dimethyl phenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
105-67-9
Dimethylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
131-11-3
Di-n-butylphthalate
ND
ug/L
4.9
1
08/0611810:19
08/08/18 19:16
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
19.6
1
08/06/18 10:19
08/08/18 19:16
534-52-1
2,4-Dinitrophenol
ND
ug/L
49.0
1
08/06/18 10:19
08/08/18 19:16
51-28-5
2,4-Dinitrotoluene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
121-14-2
2,6-Dinitrotoluene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
606-20-2
Di-n-octylphthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
117-81-7
Fluoranthene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
206-44-0
Fluorene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
87-68-3
Hexachlorobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
77-47-4
Hexachloroethane
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
67-72-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2018 11:13 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 27

aceAnalXical
J www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Sample: SW03
Lab ID: 92394219002 Collected: 07/31/1804:52
Received: 08/02/1811:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qua[
625 MSSV
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
193-39-5
Isophorone
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
78-59-1
Naphthalene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
91-20-3
Nitrobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
98-95-3
2-Nitrophenoi
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
88-75-5
4-Nitrophenol
ND
ug/L
49.0
1
08/06/18 10:19
08108/1819:16
100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
62-75-9
N-Nitroso-di-n-propy[amine
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
86-30-6
Pentachlorophenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
87-86-5
Phenanthrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
85-01-8
Phenol
ND
ug/L
4.9
1
08/0611810:19
08/08/18 19:16
108-95-2
Pyrene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
129-00-0
1,2,4-Trichoorobenzene
ND
ug/L
4.9
1
08/06/18 10:19
08/08/18 19:16
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
9.8
1
08/06/18 10:19
08/08/18 19:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
68
%
10-120
1
08/06/18 10:19
08/08/18 19:16
4165-60-0
2-Fluorobiphenyl (S)
68
%
15-120
1
08/06/18 10:19
08/08/18 19:16
321-60-8
Terpheny[-d14 (S)
45
%
11-131
1
08/06/18 10:19
08/08/18 19:16
1718-51-0
Phenol-d6 (S)
33
%
10-120
1
08/06/18 10:19
08/08/18 19:16
13127-88-3
2-Fluorophenol (S)
43
%
10-120
1
08/06/18 10:19
08/08/18 19:16
367-12-4
2,4,6-Tribromophenol (S)
64
%
10-137
1
08/06/18 10:19
08/08/18 19:16
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Acrolein
ND
ug/L
5.0
1
08/08/18 22:44
107-02-8 L1
Acrylonitrile
ND
ug/L
50.0
1
08/08/18 22:44
107-13-1
Benzene
ND
ug/L
2.0
1
08/08/18 22:44
71-43-2
Bromodich[oromethane
ND
ug/L
2.0
1
08/08/18 22:44
75-27-4
Bromoform
ND
ug/L
2.0
1
08/08/18 22:44
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/08/18 22:44
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
08/08/18 22:44
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
08/08/18 22:44
108-90-7
Ch[oroethane
ND
ug/L
2.0
1
08/08/18 22:44
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
08/08/18 22:44
110-75-8 c2
Chloroform
ND
ug/L
2.0
1
08/08/18 22:44
67-66-3
Chloromethane
ND
ug/L
2.0
1
08/08/18 22:44
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
08/08/18 22:44
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:44
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:44
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
08/08/18 22:44
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
08/08/18 22:44
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
08/08/18 22:44
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
08/08/18 22:44
75-35-4
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
08/08/18 22:44
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
08/08/18 22:44
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
08/08/18 22:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.0
1
08/08/18 22:44
10061-02-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/12/2018 11:13 PM
without the written consent of Pace Analytical Services, LLC.
Page 8 of 27

/ aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: STORMWATER SAMPLES
Pace Project No.: 92394219
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW03 Lab ID: 92394219002 Collected: 07/31/18 04:52 Received: 08/02/18 11:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH at 25 Degrees C
Date: 08/12/2018 11:13 PM
Analytical Method: EPA 624.1
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
108
114
92
%
Analytical Method: SM 254OD-2011
7.2
mg/L
Analytical Method: EPA 9040C
6.1
Std. Units
2.0
1
08/08/18 22:44
100-41-4
2.0
1
08/08/18 22:44
75-09-2
2.0
1
08/08/18 22:44
79-34-5
2.0
1
08/08/18 22:44
127-18-4
2.0
1
08/08/18 22:44
108-88-3
2.0
1
08/08/18 22:44
71-55-6
2.0
1
08/08/18 22:44
79-00-5
2.0
1
08/08/18 22:44
79-01-6
2.0
1
08/08/18 22:44
75-01-4
70-130
1
08/08/18 22:44
460-00-4
70-130
1
08/08/18 22:44
2037-26-5
70-130
1
08/08/18 22:44
17060-07-0
2.9
1
08/03/18 22:54
0.10
1
08/10/18 21:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
(�7
Page 9 of 27