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HomeMy WebLinkAboutHISTORICAL BEFORE 2017F2( Smithfield Packing Co., Inc. Tar Heel Facility 2016 Annual Report Residuals Land Application Permit No. WQ0014868 Prepared By: EMA Resources, Inc. Phone 3369751@1441 —Fax 336*751*1442 755 Yadkinville Rd — Mocksville, NC 27028 R-D -\EMA ' Resources, Inc. t� February 27,2017 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2016 Annual Report — Smithfield Packing Co. Treatment and Land Application of Residuals Permit No. WQ0014868 pp!-�,c/l/ �0 MA9 p Dear Sir or Madam:fDk Enclosed are three copies of the 2016 Annual Report for the above referenced land d h'GU/�n application permit. During 2016 EMA Resources, Inc. land applied 527.99 dry tons of wastewater residuals to 329.4 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, a Brent Collins Director of Technical Services brent.collins(2cmaresourcesinc.com RECEIVED DEQ/DWR MAR 14 2017 ROS FAYE17EVILLE REEGIiONAL OFFICE Phone 336-751.1441 — Fax 336-751.1442 755 Yadkinville Road — Mocksville. NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: W00014868 County: Facility Name (as shown on permit): Land Application Operator: Bladen EMA Resources Inc. Year: 2016 Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: 336-751-1441 Total number of application fields in thepermit: 37 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 527.99 Total number of acres utilizes for land application during the year: 329.4 Part B - Annual Comniance Statement: Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. _ 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." I Kyle Narron - General Manager ' Permit4ee N e and Title (type or print) Signatgre of Permittee Date Z I`1 1/30/2017 1 Signa a 6f Preparer* Date Signature of Land Applier Date l _ (if different from Permittee) (if different from Permittee and Prepamr) * Preparer is defined in 40 CFR Part 503.9 (r) and, 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) - - - ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0014868 Facility Name: Smithfield Packing Company Residual Source WQ # or NCO078344 NPDES #: WWTP Name: Tarheel Plant WWTP 12acidnal Analveie data Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Conc. Limit m /k a Sam le or Composite Date North 3/31/16 South 4/21/16 South 4/21/16 South 5/9/16 11/3/16 11/30/16 Percent Solids (%) NA 4.66 4.04 2.81 3.65 1.21 0.44 Arsenic 75 3 3 3 3 3 3 Cadmium 85 2 2 2 2 2 2 Copper 4,300 1240 901 1150 983 62.9 183 Chromium NA 104 70 63 79 9.18 12.6 Lead 840 10 8 8 8 5 5 Mercury 57 0.4 0.4 0.4 0.4 0.4 0.4 Molybdenum 75 17 19 16 19 13 9.85 Nickel 420 58 51 38 58 5.24 7.35 Selenium 100 5 5 5 5 5 5 Zinc 7,500 3090 2710 2750 2820 100 311 Total Phosphorus NA 18200 16500 15600 17700 19000 19300 TKN NA 75100 95800 1 87900 1 1080001 54900 1 80000 Ammonia -Nitrogen NA 9440 10900 12500 13700 13900 80000 Nitrate and Nitrite NA 2 2 2 2 1.05 1.07 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I,certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaltie:Mmitting false information, including the possibility of fines and imprisonment for knowing violations." AAZEI -I/rin Cionatnre f lVreAsre.r * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00014868 Facility Name: Smithfield Packing Company Residual Source NCO078344 NPDES # or WQ#: WWTP Name: Tarheel Plant WWTP Residual Analvsis Data Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter 1'11 :'11 :.11 1111 M, islyly,1 ------ ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signif1panj pgnalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) -, ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report icility Name: =it #: Operator: :res Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): W00014868 Cation Exchange Capacity (non 503 only): Steve Dunham Owner: Steve Dunham Predominant Soil Series: 21.6 Acres Permitted: 21.6 Site #: SF03 Field #: 8.1 1 '. 0.-ideal Analvsis Data (Heavv Metals and Total Phosphorus use mL,/ke, % Solids use Raw Percent #): ., - ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". I"jgnature of Land Applier 1/30/2017 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized: _ Land Owner: Steve Dunham Annual Dry Tons Applied:` fi „k 56 S1M Site #: SF03 Acres Permitted: Operator: Steve Dunham Predominant Soil Series: LaB Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN: 21.6 21.6 8.1 "Cond. Volume applied Volume Residual Sources Sod Precip. > o�• ' z Nitrate PAN Applied pP Name of Crop Type 19 (enter one) Solids/ % Applied per (NPDES #, WQ#, Past 24 '° ,°_^_, =; TKN c and (Ibs/acre) Receiving Residual O Liquid Solids Acre Pert, Animal dry' His. c : �' �. Nitrite Application A Waste, etc) Moist „V"w,, ft Cu. Yds Gallons (Dry Tons/AC) inches 7 a mgtkg mglkg mglkg Crop 1 Crop 2 Crop 1 Crop 2 4/5 58500 3.79 , : ;0; 28 ,' Tazheel WWTP Dry <5" S 0.5 0.2 91700 11635 2 1 I8 Bermuda 4/6 130000 379 "i0:951, :« TazheeIWWTP Dry <,5" S 0.5 0.2 91700 11635 2 41'S.33^i,'NAE1';iBernmda 4/7 58500 3.79 " QA28`,;,, TazheeIWWTP Dry <,5" S 0.5 0.2 91700 11635 2 �'18.y90 °NAB;",Bermuda 4/8 110500 3.79 0 809 „`, Tarheel W WTP I Dry <•5"1 S 0.5 1 0.2 1 91700 11635 1 2 if; 35.303 t r uNA „`, Bermuda 0,000 .: O;QQO 0000, " t 0:000 ai r° 0:000 ` 0:000.� 0:000,. 0.00N 01000,° Of000 i 0.600" ;0.O,66 ) a0'.000 �'.OI000 0 000 .: t��„ ,,,''• ; y,,, �: 1 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) p TOTAL �, , 0 X'�35noa -; As Cd Cu Cr Pb H Mo Ni Se Zn P 1F14:2X7 r p0 000� Lime A lied Date lbs/ac Annual . : , . .... ... ;: . . .... .... .... .. .. . "''''. ""''""•'...'. Prior Years Cumulative lbs/ac 0.153 0.065 27:652 1.538 0.504 0.017 0.968 3.068 0.206 135 722 2000 Current Cumulative lbs/ac t011`69„ ° , ,O r075 I 33.242 i, 1.9513 •' 0 548! ; !. +0 019 E ;, 1:Ob1 , Permitted C. P. L. R.**** 9 250 1000 250 500 Permit PAN Limit l st/2nd Crop p ': i : i.> :: i' ;: v.'- ;"::: >:': ;? ;> ;:: ;::: r; ::::: '>: ' 1r :1'47„ i ? "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed. to assure that qualified personnel properly gathered and evaluated the information submitted. tam aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report�a Bcdity Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual) r, E�- 25.68 ermit #: WQ0014868 Cation Exchange Capacity (non 503 only): 7 Operator: cres Used: esidual Ana Com- I"posite Date Avg , Solids 3.79 Arsenic 3 -admium 2 topper 1068.5 Chromi 79 Lead 8.5 Zercury 0.4 Mo1yb- -, enum 17.75 Nickel 51.25 Selenium 5 Zinc 2842.5 Total Phos- 17000 Steve Dunham Owner: Steve Dunham Predominant Soil Series: Ce 13.3 Acres Permitted: 13.3 Site #: SF03 Field #: 2 Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent Total 1 2 3 4 5 6 7 8 9 10 11 12 `IT/Ac./ o H _ _'APp• Event 1.93 " - Lrsenic 0O'01�2't ; 01000s i 0 000, "i0 000 ;0 000 O'._000 0 009 %a0000` 4, aduuum 4, 008;R 0 000 O'000 000 0 000 0 000 r0 OUO 0 000. 0 OOQ.; `Ot000e,.'°,0 000 :0 000- X--008<s ; ,'„0 , , r Copper ` 4 12', 0 0,00,, ; 0 OQO,,, fl 0 000" ;0 0000000 0.0g0 ',0 009 OOO;s 0 OOOt ` 0 000 0 OOQ 4 12 7" , , KO , ` "iLoLn 0 3054' 0 000':" 0 000,, 000 000, 0 uQ00 O':QQO OOQ' 0 00,0 0 000 0 000 000E v O 3,05 -;0 ,'0 z_0 , .':0 Leado-033 x,0 000 „; 0 000,E O,OOx 0 000 '0;;0,00, O,OQO0 ' 0 000 0 000 : �0'000 w 0 000';0033 ,0 , 00,0 %00Z = W00.- goo 0004,. 0„OOO$ jaO00 = O000 O OOO `- O OOO' Woo WOOO', OOO 0O2 _Mercury � j ,FO`0005 �O e O O'069 s 0 000°E r 0 OOOFry O OQO Q 000 Oj000 0 000 ' 0 00 O'000 0 OOO4 - 0 000 0 000 'Q OM69 ennm .. w Nickel 60'>198^", 0 000 AW W0.00, . 0 M, �O OOQ` �0 000 s0 OQQ3, 0 000E r 0`000,z,' v 0 000 . ;; U OOOs Q 1Q8, ';lenium 0 019 0 000.:, 0 000 0002 A`000 ; ' 0 000 0.000„ 0, 000 0 000 OF000 0`000; 0019 „0 _ ;0000, Zinc 10 978v 0 000 = 0 000 ; „0 000, _Q 000 , y, 0 0,60, , 0 OQO,' O,R_O,O,Q4 , 0 ODOR , 0 000 u0 000, , `0 000 "0 978 Total " x_ +w ]r +1 t1 h, ,Phos- 65 654� �b0 000' V, 0 000 3 ' Oe000 y 0 000 3` +Fli 0 OOOg ht �, 0 000 t 0 000 .2 0 000 j'i- 0 0001 O'000 py 0 Q00 FEy 65 654 +4 - 3s S Y WryixiR , c�>-` � t` h �.,,�z,�ru, chorus >,�.�����?�h � .t wm>s .,��...��;�-,;zne.�,���:?� 4 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 'tm aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/30/2017 z'ignature of Land Applier Date DENR FORM MFLSF (12/2006) -) 1 Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 2 Acres Utilized: Steve Dunham Annual D Tons Applied: i 25 68 °334 „ Site #: SF03 Acres Permitted: Dry PP t ... �.. - _ Steve Dunham Predominant Soil Series: Ce Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 168 Crop 2 Name: Crop 2 Max. PAN: 13.3 13.3 7 ° -C °3 0 A Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre D Tons/AC (Dry ) Residual Sources DES #, W #, Q Fert., Animal Waste, etc) Sod Cond. (Dry, We st Moist) Precip. Past 24 Hrs. inches 9 � ro 0 E " o a �. x 0 w —" . 5 a m Fo �G. ,• �" 0 TRN Mg/kg z w ° y ? w' mgncg Nitrate and Nitrite mglkg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 4/29 78000 3.79 0.927 ,- Tarheel WWTP Dry <,5" S 0.5 0.2 91700 11635 2 40'.472 Bermuda 4/30 84500 379 1_i004-•'; TarheelWWTP Dry <,5" S 0.5 0.2 91700 11635 2 43;844 Bermuda 0:000': ; 0:'000 i 0.606 g Q 000 0!000 0.000 ; 000 "' -;4.600b.06 0 000!? .._.-... _.._. Residuals Applications totals on FORM FSF su attach FORM FSF su to this form): ""` TOTALS: N e',:'.o Fl•62soo ; :::: As Cd Cu Cr Pb Hg I Mo I Ni Se I Zn P 84r316 .0:o00ru Lime Applied Annual lbs/acre i {0`012,w ;0008, ,. 4:1=27; c' , 0 305;': ' Ox033` !, -'0 002 , `0''069 P f 0w1'9.8 0 019' j 10 978 r=65 654 ` , .• , ;:; :::;;:':::::y::; ;::::i:::< ;:::: ::::::2<:: .::..:::. •. •...... • ...::.. • . ....... ....... ... '' "•'"'''''''' "''"''''""'"''' Date Ibs/ac Prior Years Cumulative ibs/ac 0.162 0.054 33.283 1.345 0.615 0.017 0.968 3.545 0.197 141.758 Current Cumulative lbs/ac +0+174. O'062 3,7 410, `1°650'.'.;` 0 ¢4S, , r 0 019 w 1. 10;037 , 3:343, '0.216: j152 73¢s Permitted C. P. L. R.**** 9 250 1000 250 1 500 Permit PAN Limit 1st/2nd Crop:.:.:•i1:2•:..: •::<1:•::..::.:1i;:::>.:: >1v.:•i.:: `:: i :; : i>: `i;::;: ;::"i1.': i1:'iii.:•ii::: iS;i::': i:i>, ..:.,•. ....................................................................................................... (y: 68... < w,,,El 1. .- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date * ` Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading: Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report '—icility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): ,& .rmit #: W00014868 Cation Exchange Capacity (non 503 only): 4.7 Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series: Ce ores Used: 21.3 Acres Permitted: 21.3 Site #: SF03 Field #: 3 xesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 3 4 6 6 7 8 9 10 11 12 __2j 0 T/Ac./ App. Event 2.17 ow 0W 0---Aki, 0 IliOi000 0.000 ' ' 0 0009 0 000'- 0 xsenic ,0 , idmium 0 009s"r0 000p 000 +0`000 _ 0000 �0 000, " O:000r 0 000' 0 000 e , f0 000, ;_0, 000 O'009; Copper ` 4 637_`* 0"000 Y OOO k < 0 000 -A 000',, O000 0 000 tr,A00.0 ;. 0 000__ 0, 000 >'0 000•a 14`637: ; ,r0 . ; , u0.0,00 romi 0 343.`' `0 ,000_ `t0 000 0 000 `, 0 000 F0000 ,0:000 0.060 ' 0 OOOT , -0 000,' 0 0„000 000, :0:-343 Lead 0 037`' 0 000- 0 000: S Q 000 <0 000 0 000- O'000 O.000} O'000' 0 00,0:`,•' 0 000' ;0 000 0.037�, , Mercury 0 002' a 0 000 , 0 000 , 0 000 ,Os000 0000 , 0:000 `0 000t _ 0 00K0 000 :'0 000 0, 002r l nlum 0 077;p E 0 000 ` 0 000 0 000 0 000 r 0 000 u0 000 0 000 " 0 000 0 000% 0 000 _:0 000, 40 077 ; Nickel ` 0 222 0 000;'' 0 000 =0 000` 'r 0 000 0000 b'000 000_ 0 000 '0 000` 0 000> 0 000 U`222A' , , , t,0 ; ;lenium 0 022' 0 000 0 000* 0 000 :0 000 a , V-Aw,, t 0 000,. 0. 000, 0 000' 0.000 0 OQO >0 000 0 022" <-' Zinc 12 33,6 y'0 000 _ 0 090 0_000i r0 000 , 0000 , 0;000 `_0 00,0 ' 0 000':; 0 O'O,Ox", 0 000 ` 0 000 12 336E Total �Phos- 7380,�0 000 , 0 0000 0000 000 r0 000 0 000� 0 000 �0 000� 0 000 0 0000 000 73 780 ;3 C] y •` S f'�llungmaw .r ,"` _..v.. ..v F 41'.. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance �dh a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. mi aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 4;f 1/30/2017 "�gnature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized: Steve Dunham Annual Dry Tons Applied: t 46 22 Yj Site #: SF03 Acres Permitted: Steve Dunham Predominant Soil Series: Ce Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 168 Crop 2 Name: Crop 2 Max. PAN: 21.3 21.3 4.7 „ ' V m A Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume A Led per Applied p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet Moist) Precip. Past 24 Hrs. Inches Y a o o -• t n c w �' �, ; C' . ? W : �,• • w # c. TKN mg/kg z a o 0 mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of CropType yP Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/26 52000 3.79 0 386i Tarheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 116•.847 :NA •AN Rye 4/27 65000 3.79 , '•0.`482 `' Tarheel WWTP Dry <5" S 0.5 0.2 91700 11635 2 21.659 j 11, 14A is' Rye 4/28 84500 3.79 0b27'; . Tarheel WWTP Dry <5" S 1 0.5 1 0.2 91700 1 11635 1 2 ' 27`377 NA_ ;I Rye 4/29 39000 3.79 `.0`289�,�'s Tarheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 i If.636 NA! ,! Rye 5/5 52000 379 t '0:386..i TarheeIWWTP Dry <,5" S 0.5 0.2 91700 11635 2 '�'1G:847NAj"�; Rye 0:000 0:000 0 000,a! •�.00� : 0I)0 0.000 0.066"". 0.000; , 0:000 . ° Oi000 . 0:'000i'i - 0:000' I:-0000 0 000'.- ` " r ' �, e," ' -,,,, Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) - - " ' .. ..'. ... ..'..'. TOTALS: �. ;v :� ;o ,,` z9zsoo .:: As Cd Cu Cr Pb HP Mo Ni I Se I Zn P 4 9,t767, .0 000,i Lime A lied Annual lbs/acre .-OQ13 y, 0 009 � _ . �4:63T . Os343'; ' 0.037„ j'b 002 ' ; w0A77 _ 0:222. ..- ""O b22- : ,•12 336 ;73 780: • • • .....i :....::; :::. - - .................. ::: i>:»:::::: 2 .. ;:;, ,: «;•:• ........ ;: is ... •.•.•.: .... .... ""``'"''`'`"' Date ]bs/ac Prior Years Cumulative lbs/ac 0.129 0.061 25.21 0.858 0.451 0.013 0.74 2.62 0.149 ] 10.039 Current Cumulative lbs/ac 0.`l42 ", : 0!070 29,:843 1.201(„ 0.488. `'0' O15 " 0:817 ; 2:842', 0.171 " 122 373; Permitted C. P. L. R.**** 9 250 1000 250 500 Permit PAN Limit lst/2nd Crop .1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report icility Name: i `:rmit #: Operator: ^.res Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual) `j 77 WQ0014868 Cation Exchange Capacity (non 503 only): -4.8 Steve Dunham Owner: Steve Dunham Predominant Soil Series: WmB 37.2 Acres Permitted: 37.2 Site #: SF03 Field #: IHesidual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ^'ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. _'am aware that there are significant penalties for submitting false information, including the possibility of fines and ,imprisonment for knowing violations". 1/30/2017 1—�ignature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 7 Acres Utilized: 37.2 Land Owner: Steve Dunham Annual Dry Tons Applied:" 77 04s' r _ Site #: SF03 Acres Permitted: 37.2 Operator: Steve Dunham Predominant Soil Series: WmB Cation Exchange Capacity (non 503): 7.2 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 210 Crop 2 Name: Crop 2 Max. PAN: H Volume applied Volume Residual Sources Soil Precip. � ,� 0 5` Z Nitrate PAN A lied Name of Crop Type j (enter one) Solids/ % Applied per (NPDES #, WQ#,Cond Past 24 =. ^. TKN w o and (lbs/acre) Receiving Residual Liquid Solids Acre Fert.,Animal We' firs. , a w ,' p w• Nitrite Application Ca Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Moist) Inches C o c mglkg mglkg mglkg Crop I Crop 2 Crop 1 Crop 2 4/19 117000 3.79 A;497"'•{�` Tarheel WWTP • Dry <•5" S 0.5 0.2 91700 11635 2 21.705 NAr„',�. Bermuda 4/20 136500 3.79 `6:580': -• Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 .25:322 ',.NA. 'i Bermuda 4/21 136500 3.79 0380 , Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 25 322 ". NA, !Bermuda 4/22 52000 3.79 -.0 M Tarheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 %9.646 NA.', Bermuda 4/24 19500 3.79 0;083.,', Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 3.617 NA "Bermuda 4/26 26000 3.79 f 0±1'10 ` ' Tarheel WWTP Dry <,5" S 0.5 0.2 91700 11635 2 4,823 NAC'" Bermuda wo 0.000 VOW, O'060 0600','' 'a0m ........ ; ,,.. ,.. ; , .. . , , _, ,.;_,,, Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form). • • • ' TOTALS: k ,. o as75oo •:: As Cd Cu Cr Pb H Mo Ni Se Zn P i,90.436, 0 00Q'! Lime Applied Annual lbs/acre 4.4n6 ,0:327i -1 0 635 •+;*i0 002 .0,074 ,.0:213 0 021 °' I;11774 , 70 ; Date lbs/ac Prior Years Cumulative lbs/ac 0.095 0.048 19.692 3.174 0.62 0.011 0.604 2.294 0.131 95.354 2000 Current Cumulative lbs/ac 0;07, ' C,:0:056 ; • 24.14 3.361V ,1, Y016551, , 0 0,13 , �,0:,678 t 2.506', f 0?152:,! 907 128' Permitted C. P. L. R.**** 9 250 1000 250 500 Permit PAN Limit 1 st/2nd Crop ................................................................................... . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date `** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report "'acility Name: i 'ermit #: Operator: -'cres Used: L.esidual Ana Com- 'posite Date Avg o Solids i. Arsenic 3.79 3 7admium 2 ,opper 1068.5 r—O— 79 -, Lead 8.5 u+Iercury VMolyb- 0.4 -lenum 17.75 ;Nickel 51.25 Selenium 5 S Zinc 2842.5 Total Phos- 17000 Smithfield Farmland Corp. Total Dry Tons Applied (Annual): W00014868 Cation Exchange Capacity (non 503 only): Steve Dunham Owner: IW Burney Predominant Soil Series: 21.8 Acres Permitted: 21.8 Site #: SF07 Field #: 13.5 Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent Metal AaA 1 Total 1 11 2 L 3 4 5 6 7 LBJ 9 10 11 12 - IT/Ac./ App. n Event 2.50 " Arenic u0'O15 ` 0 000 0.000`, fro 000 0 000 0 000 P0"000 ° 0 000 ' 0 OOOi 0 000 r 0 000_ r e-5bA , v _n 0 O15w admium 0 o l6t,Ij OOOf" 0 OOOu; p 0 00,0 0 000 000 s0"000_ 0 090 0 000 0 0,00, ; 0 000 =0 000 O10 „ „Q ,, , ;„0 Copper z5 338' 0 00.0;' 0 OOOt' 0 000 0 000 } Ob00? O:000,0 0„00' 0,0000 OQO, O'000E OOOs Q , ,`$'338 Tomi A 3QSx f0 000 : 0 000 0`006 000 000 0:000 0`00'0� 0 000 0 000' 000 0 000 =: , ,0 ��0 �0 0 395 Lead 0`042- s O'000 0 000. `0 0000 000 ' �,0 000 0; 000, 000 0;0.042 `'_' , s,0 ,AWO 1,1,046k ,,_0 Mercury0 002 Q000 OOOk',0'000 z0 OOOx "iOOQu 50"000 0. y0 , Ylolyh 0 0890 i Yuc 000 ' E 000f iT` ,r1 F K & T 4W' C5w":y Oq0 ++c t .SAC J'. ^ ` 11 rt h AE Ai4 M1 f h 'tr✓ `'0 0 7 ..0 000 0 000 0 000 0 000 O 0 000 0 000 0 000� 1A 000 089 < lenum, n ,_t ae xi ax v ,_ 4 > . , s s v�+ a , . Nickel 0 256' ; 00000" 0 000R 0°000,0 000, O'_000ff 0 000 ;OQQQ 0`000 0 000;`; 00 OOQ ;lenium 0, 025r 0 OOQ s 0 000_;0 OQO '.;0 000 0§000 0000 0 000_, 0 000 0000 0 000 0 000 ;'0 025 Zinc 14 201 0 000 0 000,0 000 0 000 0000 0.000 OOOr �Q 000 4 0 000 `_,0 000; z1'4 20ny s _ , r_0'000 , 0 ;, Total % 2lra�" t Vier 3 �ahr 5iz rl r r Y� u x ar 11` ± _ _ •,Phos- 84 932 �} 0 000 § 0 000a 000 0 000> 0 000 0 000 O'tj00 0 000 0 000. Ot000 0 00084 932 -0 ; )horns it ceriny, under penairy of taw, tuat tors document was prepared under my direction or supervision in accordance with system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am vare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". r� 1/30/2017 O.-pature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized: 21.8 Land Owner: JW Burney Annual Dry Tons Applied: r ' ''S4 46 Site #: SF07 Acres Permitted: 21.8 Operator: Steve Dunham Predominant Soil Series: AaA Cation Exchange Capacity (non 503): 13.5 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 207 Crop 2 Name: Crop 2 Max. PAN: o A 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDES #, WQ#, Fert, Animal Waste, etc ) Sod Cond. (Dry, e ' k moist) Precip• Past 24 Hrs. inches 9 ^y " '� 5 », ` o 7 o �, o F,,�• " ; ` �• c ,TKN mg/kg z i o ? mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/14 136500 3.79 Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 ,43,210 NA;,,°' Bermuda 4/15 130000 3.79 `6:q& .7 Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 `.41:152 NA ; Bermuda 4/18 78000 3 79 9:565 „', Tarheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 24 691 15A.: Bermuda ,0;000N: ` OMO 0.000, i 0000 0:000 0 000 OI000 `'} 0000 0,000,' Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) p TOTALS: Sin ,. o nji 3445g0.. <:::: As Cd Cu Cr Pb H2 Mo Ni I Se Zn P 4_W9r. 54 i O.00,V` Lime A• lied Annuallbs/acre 9..-,10015' .. ��0'0.10` S:33$i, .. `0395_�, 0042-,.,�0002: ,`Ob89,, _._ 0:256r 0.025-';•14'201, ?84932!i ,;:;:;:.<�i:;> ...... ......... ...................... • , ;;:;::: ;:.v. '.;: ;:::;::':y:'.;:: Date lbs/ac Prior Years Cumulative 'lbs/ac 0.15 0.223 93.79 0.882 1.255 0.018 1.008 2.255 0.239 284.041 Current Cumulative lbs/ac Oif65 O'233 99 128I' I-29:T 1.29T ; ".0.020., , 41097 . 2.Sl4,- , 0:264, ' 298 242' Permitted C. P. L. R.**** 9 250 1000 250 500 Permit PAN Limit 1st/2nd Cr 0 P .......... ................ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report )cility Name: irmit #: Operator: res Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual) ;c 47:25 W00014868 Cation Exchange Capacity (non 503 only): 10.2 Steve Dunham Owner: JW Burney Predominant Soil Series: WmB 19.3 Acres Permitted: 19.3 Site #: SF07 Field #: ',ioc;final Analvcic 71afa rueavv Metals and Total Phosnhorus use mgAt=., % Solids use Raw Percent #): 9 9 10 11 12 " ample or 1 2 3 4 5 6 7 �_om- Avg posite --IDate Solids 3.79 Arsenic 3 �ldmhnnl 2 �opper 1068.5 Chromium 79 'Lead 8.5 -_.lercury 0.4 Molyb- 17.75 lenum Bickel 51.25 Selenium 5 � Zinc 2842.5 -Total Phos- 17000 )horns 1 _ unual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 H ' �iT/Ac./ _ App. w Event 2.45 arsenic ia, 0 000 a OF000 `K 000 '.`-0 00e 00 0 OQO 0 00 r 0 000 ' 04000 0 000 P 0 015 = j , ,' _ admium 0 O10•,0 OOOh, 0.000,` ;, w0 000_ ,0 OOOy ,-,OF000' Q 000, , 0 0,09 ` -0 000 .:.0 000,;; 0 000 A" 00,0 �.0 O10 Copper _ 5 231 x 0 000'4 !'0 000 r x 02000. 'Of000 y0 000 .0 000 0.000, 0 OOq; ; 0 000; s' ,0 000 0 000 ��5 231'` ! �0 000 0 000 OO,Or 000 0 000, 0 000 0 000 ' 0 000: '?0 000 0387, 'Wonuum,�,0.387�, 0- _r QO_0. __0 =O ,0 , , - -'Lead 0 042 - 0 000: ` 0 000,. ; p 000 0 000 t Os`00_0 ` 0000 0:000 , 0 000 0 000 0 000 � 0 000_ MAN2`: _Mercury 0 002 _ 0 OOOF 0 000, _ WOW 00,0,_0 000,- -, Q! 000, Oi000 �« a0 000 0 000.. 0 0000 000.' ;0 000 O'002; r'J01 b y 't dF 0 087z f 000 ¢" 0 OOO�t F_Lq M1 ` 0 000 i d `4 0 000" V d.'a6 0 4 0 000 P ' n Ot000 fS':' It Po 000 r0 000'� 0 000 0 000� t 0 087 ;. ienum {0 ,000 _ F 50 251;'` u. 0 000 0 000" �%0 000 = 0 000 ` �0 000,,E `:0 W �0 000 t 0 000, 0 000 , 0 OOOF ' 0 000 0 251. _Nickel elenium 0 024`; 0 000'. =0 000 d0 000 - 4 0 W _A`000 r 0000 O.000i _0 OQO_ ;0 000 ` O'000 -'_0 000 0 024 Zinc 13{97 2 0 000 , 0 000 - 0 000' "0 000 -0000; 0000 s0:OQ0', 0, 00.0, , x_0,00,0,%' `0 OQO, , 0 000 •13 917 a�1 T0161 , , r�:PP Gtli TEST x i �t�x .. } t ? x "i 1.,4,i i� '9 W -th V S L' »�= .+ '.. i 4`` e i <ar �F } x aR'� pY'2U£ Phos- ..,� %9U 83 232 0 000 ; i eiS 000 nb 0 000 < 0 000 f X� 0 000 9 0 000 ] £ 0 000 t( 3t5 , Oi000 piG, �0 000 0°000 0 OOOF 83 232. ,0 - homs,. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance Ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. ,,dam aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". d1z� 1/30/2017 signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. Land Owner: JW Burney Operator: Steve Dunham Crop 1 Name: Bermuda -Pasture WQ Permit M WQ0014868 Field #: Annual Dry Tons Applied:' Site #: Predominant Soil Series: WmB Crop 1 Max. PAN: 210 Crop 2 Name: 6 Acres Utilized: 19.3 SF07 Acres Permitted: 19.3 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 10.2 w q(NPDES m A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre D Tons/Ac (Dry ) Residual Sources #, WQ#, Fert., Animal Wes° etc) Sod Cord. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches > �. � ^ o� m ~ ° o " * w o o ,�, " �° �' N. .. o N mg/kg z 00 o �. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving g Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/11 19500 3.79 ", Q' ;'160�'� Tarheel WWTP Dry <,5" S 0.5 0.2 91700 11635 2 ,. 6.972 . NA' `, Bermuda 4/24 104000 379 , ' 0:852". ` TarheelWWTP Dry <.5" S 0.5 0.2 91700 11635 2 °37.186 '. PA `Bermuda 4/25 156000 3.79 "..1i277_".; Tarheel WWTP Dry <,5" S 0.5 1 0.2 91700 1 11635 2 , 55.780 NA,,,'- Bermuda 4/26 19500 3.79 0!d'60 . •. Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 `:6.912 • NA.' - Bermuda Oi000 , O ow, :000- ,•,'=Oi0001,,,, ' 0.000 0.000-1 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) TOTAIS: .� . `.� io�.;, 299000 ,:; : As Cd I Cu Cr Pb Hg I Mo I Ni Se I Zn P•10691"10:000- Lime Applied Annuallbs/acre :'0lO15 0.070 5.23J1 - ' ( 0 387" ; 0 042 : r, 0 002 ;0;0"87 = ..0 251 O.b24' 13 917 `i83 232 , ......':; :"': ;;:: ::::..:.:.:.....:......... .............. . ::::.:::.::.::.•. .. ... ""'• "•'• • Date lbs/ae Prior Years Cumulative lbs/ac 0.232 0.232 99.787 5.789 1.741 0.025 1.465 14.595 0.307 352.374 Current Cumulative ]bs/ac O;i247 _02,42 .105.01�8 6,176;",', 1 783 i;,0 027 ; 1:55WJ,`, '4.546 0�33`)±'�'366 29P Permitted C. P. L. R.**** 9 250 1000 1 250 1 1 500 Permit PAN Limit 1sU2nd C re P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 01 *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report "acility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): ermit #: W00014868 Cation Exchange Capacity (non 503 only): Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: AaA Icres Used: 12.1 Acres Permitted: 12.1 Site #: SF07 Field #: E esidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 7-lmple or 1 2 3 a 5 6 7 8 9 10 11 12 ,Com- itposite Avg Date i Solids 3.79 Arsenic 3 'cadmium 2 .opper 1068.5 lChromium 79 Lead 8.5 4ercury 0.4 Molyb- 17.75 'lenum 14 1 Nickel 51.25 Selenium 5 Zinc 2842.5 Total IPhos- 17000 )borus nnual Heavy Metal Field Loadings (Calculated in lbs/acre): I Total 1 11 2j 3j 4 5j 6 7 8 9 10 11 12 y iT/Ac./ App. y Event 2.55 Asenic 0 O15a' 0 OOd= 0 00,0k 0 OOOs 0 000 f0'000, 0 000_ 0`000 0.000; 0 000 000 0 00.0.,. , , UO ,"0'O1 admiumOQUt1,6 OOQf r2 000 p.QQO Q OOR.; U OOQc 0 0004 _0`QOU _ .'U'QQO x;:OQ10 Copper 5 443 "0 000 0,000 r'; 0`000, 0 000 ; 0.000� _M 'o„" `0 00;0 0 000: 0 0'R 0 000,,. ,0'000r romi 0 402 000 ;' O000 0 000 ;0 000r ?0 000 =0:0_00_, 0 OQO, 0 000 O OOO;a 000 '- 000`, `0 402 11 i3O : Lead 0 043 r 0 000"= 0 0000'000" ':_0{000-_0.:000 0 `000 000_0 000 0 000 000 10 043' _ , a0.000 _0 ;-0 5 0.002x 0 000_ Ww w0 000_ �G am W& AW M00 000; ` 0 0W NOW _Mercury a >0 •ZQw Rolyb 0 090 0 000 f' 0 000 " 000M 0 000r 0`000+ 0 000 0 000 i0'000 ; 0`0W iib 000� '0 000,, 0 090 'lenum �.Ye ,�N;..-: ti � ,<l .� r Sa,.o._. _ Nickel 0 261- 0 00.0;' 0 000 F 0 000' 0 000 0 000 O'060 } 0 QW 10 000 ` oft0, 0 000, ' ,0000', , , „0'261 ;lenium 0 025rK 000= , 0 000 c`0'000., 0,000, 0,000 MW 9;000, u0 000 0 OOO ;`0 OOOX M0 ,fw Zinc 74„48O.L ; 9 000,; 0 000 20300 O OO,On aX& 0 000 M 0 000 - 0610' 0 OOQ, 0 000, -- ,Or000„ , , I0 , ; bl'4:480_ Total t z 'G:+ �r x, 3y s J � ry r s 4fl i� c rfl >; fl �cw t Ord -1 r.."4's x ' °rah Y r a % ht' s, Phos- 86 598 0 000 ' 0 000 0 000 0 000 K0,000 y?° 01.000,41 0 000 0 000f 0 000,¢ 0 000 0 000 86 598 :horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. km aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations". "'gnature of Land Applier 1/30/2017 Date DENR FORM MFLSF (12/2006) PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 8 Acres Utilized: 12.1 Land Owner: 3W Burney Annual Dry Tons Applied: , " 82 Site #: SF07 Acres Permitted: 12.1 v i Operator: Steve Dunham Predominant Soil Series: AaA Cation Exchange Capacity (non 503): 11.1 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 207 Crop 2 Name: Crop 2 Max. PAN: 0 o A5. Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES#,WQ#, Fert., Animal µre etc) SO1l (Dry� Wet, Moist Precip. Past24 airs. inches > � • o w a o• '� o `•. . N • ?: w 'w � TRN mg/kg 2 o E• °' mg/kg Nitrate and Nitrite mg/kg P�,b� reed Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/11- 143000 3.79 ='1868 ' Tarheel WWTP Dry <5" S 0.5 0.2 91700 11635 2 8P{557 NQ; . Bermuda 4/13 32500 3.79 " '0.424.,," . ' Tarheel W WTP Dry <.5" S 0.5 0.2 91700 11635 2 18C536, NA , '- Bermuda 4/26 19500 379 ¢; Tarheel WWTP Dry <.5" S 0.5 0.2 91700 11635 2 ]d°421 NA,, ; Bermuda .060" i �,O?OOO` i .Oi000 ,'O`.000!Ff ,r0:000 - 5- _ _ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form). i TOTALS: � y , t ;o f 19so0d : ' ':::: As Cd Cu Cr Pb I Hg I Mo Ni I Se I Zn P =fil1('L14. ,- 0.000- Lime Applied Annual Ibslacre `Q 015 , . 1, 0 ,' r 5:4'43 0:403` 1 0 043-` .. :0.002 1''0',090^; 0.261 r,V. 5',' - , 14.480�" �-`86 598 ;; .. ;.: .... ......... .......... ....................::.•.> ..... Date Ibs/ac Prior Years Cumulative lbs/ac 0.127 0.05 21.205 34:4 -0.623 0.014 0.78 2.431 0.182 104.813 2000 Current Cumulativelbs/ac y0;,1142,` O'0602"G t ,,0016 '0:870 ^2692 0,20Z,; I19293'.,:: Permitted C. P. L. R.**** 9 250 1000 250 500.......... Permit PAN Limit 1 st/2nd Crop ............:: ::::::..... ................ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) r ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report ,acility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual) " 52:40 permit #: W00014868 Cation Exchange Capacity (non 503 only): 4.7 Operator: cres Used: esidual Ana Com- I Avg Iposite Date 'u Solids 3.79 Arsenic 3 idmium 2 topper 1068.5 romium 79 Lead 8.5 lercury 0.4 17.75 Nickel 1 51.25 Selenium 5 Ziuc 1 2842.5 Phos- 1 17000 Richard Dunham Owner: JW Burney Predominant Soil Series: 21.3 Acres Permitted: 21.3 Site #: SF07 Field #: Data (Heave Metals and Total Phosphorus use ma/kg, % Solids use Raw Percent Heavv Metal WmB 9 Total 1 11 2 L3J 4 L5J L6J7 8 9 10 11 12 J aT/Ac./ o APp•' Event 2.46 irsenic s'0 Ol'S 0 000u 0 000 ;FO 000,. ;.;0 000 p;0000 _ 0:0,00 0 000^ 0 000, 0 000=a ; 0 000 ;Q 000 : A 013 idmmm x0 OJAI dt0 02, 0 QOO.t 0 000 r V.QP,, .0:00,N 4W."00I Y0 000� -. r 0 OOOz ` 0 O,QO,v . 0 000 0 000 Copper 5 257 b z O 000 ' 0 000`n ^;�0 dw is 000"� Q 0001 `i0, 000 ,0�00;0' �0 000,E 0 00,0"'; -n0 000, 0 000, .. y.5 25T- ^'romi 0 389,„? _0 000,„ 0 000 g`0 000 _ ;0 000 j 0000 O;ObO" Ox000 1 O'00.0', 0 000''' , 0 000, 0 000t Lead 0 042" 0 000` 0 000 ..0 000 '0 000� 2 0000 , O'000 0 00,0 -0 000,; 0 0,00;, , 0 000 ' l0 000 _ _ 0 042` M_ ercury 0.002. _ 0.000 >; w0 000 , r 0 000, 0 000. 0000 0000 ,0 000 ; 0 0000 000; 0 000, 0 000, 0,002,' dolyb 000, 0 000 0 000� 000' t O'b00' O00 '0 000 0 000' ``0 000' 10 000 : O'087 A plenum � r - � �� _ . ,x.- ,0 -F � � _.�' ;;� .�� w ,,� I ,�x0'000 t Nickel 0 252'` 7A,000: _' . 0 000 0 000 :0 000 Ot000� 0,000 0 -0 ,0AWL" 0 000 ° _ 2000_, r;denium 0 025' g 0 000 0 000„ ; 0 000 . 0 000 ,0 000 0:`000n, 0 000 0 001T , 0 000; FO 000, 0 000; O'025 ZincO,OO , `0 000 _ s 0 OOQ, 0";000 , 0 000_ 0 O;OOu 0 000= ,0 000 k 0 000 0 000, _ 13 ;985t Total SK z Y§ a hos- , 83 640 0 000 . 0 000 ^JO 000 n �`0 000 h 0 000� 0`000 0 OOOw 0 000 i 0 OOO , 0 000 + 0 000� 83 640' .hnrus , _ . i cernty, under penalty of taw, that tuts document was prepared under my direction or supervision in accordance ^th a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. `m aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/30/2017 ;nature of Land Applier ;I Date DENR FORM MFLSF (12/2006) J --- _-� �_ - : -- _) - -J --J -- - �-7 --I -� --1 = - ? �7 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. Land Owner: JW Burney Operator: Richard Dunham WQ Permit #: WQ0014868 Field #: Annual Dry Tons Applied: Site #: Predominant Soil Series: WMB Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 210 Crop 2 Name: 9 Acres Utilized: 21.3 SF07 Acres Permitted: 21.3 Cation Exchange Capacity (non 503): 4.7 Crop 2 Max. PAN: ,. 'y q ALiquid Volume applied PP enter one Solids/ ( ) Cu. Yds Gallons /o " Solids Volume Applied per Acre o Tons/Ac (Dry ) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Sod Cond. W�, Moist) Precip. Pas[ 24 Hrs. inches a 'd " 4. c x a o %� �, w _ w' n 3 5' W fD « ��;; 6" o TKN mg/kg yyyy z I ] w. mg/kg Nitrate and Nitrite mgacg PAN Applied PP (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/9 136500 3.79 :1+f013o-" ' .. Tazheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 4,4.224 NA, .:i Bermuda 4/10 195000 3.79 1.447,,� Tazheel WWTP Dry <,5" S 0.5 0.2 91700 11635 2 6108i •NA ' .' Bermuda ILI 0;000 ILI 'dq � , �QQQ 0,000', 0:000 ., f=0.000� 0.000�. U:000 a ,0"00, 0.000t y 4,.09 Vbov ,0.'000.'.. ...0.000 . ••.0.000 0:0001 '' .0.600 ' .0:000, o Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) TOTALS: ,w, o_ F' , 33Tsoo ..: As Cd I Cu I Cr I Pb I Ha I Mo I Ni I Se I Zn P 10W,402' , 0 000.''i Lime Applied Annual IbS/acre ' • Q:015 Oi'O10' S.25T , 0 389' `, 0 042'; , . '-0.002 , , 0" 087 A252_- 0�023'. ..: is a;• 'i:::::ii::::5.•'? :>: •i Prior Years Cumulative lbs/ac 0.149 0.084 23.032 3.353 0.679 0.015 0.859 2.849 0.176 124.16.............. 2000 Current Cumulative lbs/ac Oi 164' ,4,' lb j s`28t289' 3:742,''y " 0 721, i' O Ol7 • I', 0:'946 , '3,1015` " 0 201' "'438 145, Permitted C. P. L. R.**** 9 250 1000 250 500' Permit PAN Limit 1st/2nd Crop ............... r "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report f7acility Name: 'ermit #: Operator: ;I cres Used: residual Ana ICorn- posite Date o Solids Avg 3.79 Arsenic 3 admium 2 topper 1068.5 Chromi 79 Lead 8.5 ercury 0.4 Molyb- —'lenum 17.75 Nickel 51125 Selenium 5 Zinc 1 2842.5 Phos- 1 17000 Smithfield Farmland Corp. Total Dry Tons Applied (Annual): W00014868 Cation Exchange Capacity (non 503 only): Steve Dunham Owner: JW Burney Predominant Soil Series: 7.5 Acres Permitted: 7.5 Site #: SF07 Field #: Data (Heald Metals and Total Phosphorus use nnual Heavy Metal 5.7 % Solids use Raw Percent LaB 14 Total Ill 2 j 3 L_j 4 L5J L6J7 8 9 10 11 12 T/Ac./ c App. m Event 2.60 y 0 Ol_6'r- 0 000 0 000" ; 0 000 000 i)`bk '�0'.000 ' 0 000 0 000 0 000 '0, arsenic ,''_0 , F EOA00 ; t 000, ;;0 016'? idmium 0 0102 ? 0 000 •, 0 000. ? 0 000 . 0 000 ;0'e000ti ,0,000 {O.000e 000, 0 000„ 0 000 ;0 OOQ .,;,Q Ol0 za Copper 5 5,60t 0 000 ?0 000,,0 000 0 000,0'b0000004 000 000 0 00'00 OOOt 000,5 ;;0 ,0 ,,TO 'romi 0 41w1", ; 0 000 ti 0 000 ' r 0 000 `0 000 K 000 + +0'000 0 000 t,0 000 0 000 0 000 '1-0 000 =0 411< . _ _ Lead 0 04.4 , 0 000? -0 000 , ;`0 000 , "Q 000 s A'000 0000 ' O.OQO 0 000 0 000 `: 0 000 -;`0 000 , 0 044;'- ,Mercury 0 002 Y'0 000: 0 000 , O 000, ,=0 600+ ow 0:000> _ 0 000, 0 000' 0 000, ` ,0 000,, b 000 �K002' �aolyb- �� 0 092V tW 000 0 000 0°000 " � 0 000' �0 000 v 0 000 0 000 0"OOO r 0 000 ` 0 000 �0 OOb £ 0 092 I._ ;1enntn ....vsai .Z / .` •.. - .4. .?i i..n ... r -. _ .:..- +"ieai'1 r�++t # ✓ .a'l * Nickel 0 267 * 0 00,0 000 :':'0 000 =0 000 0 000 0 Q00 0 "000 '0 OOOF x 0 000, ': 0 OOQ- , 0 0,00 267 .0 0 ` 'Jenium T,0 OOO.;i 0 000;, ` 0 000 ;'0 000, I `'000 -ov ; _ `Zinc 14 M' i0 000 ` -` 0 OOOe ,0 000' 40 000 �0'9,00 ?0; 000 , 0 OOQx, #0 000 0 000,` x 0 000. ,',0 000 Total - + e Y u k £ p j a �,'i i' T Z 1 t ry^��r',t x -y-. VZI '�."#4�Pv. r.� '+- i : y X FK'vi .aS' i'kt"rt/u+' '� D Y �: q'✓a- 1P 4 ple 3 11^S ,� 1 J : sY YS { '�r.� e 41 i - d ti a �`y i K?�'. - ^Phos- 88 468 1 0 000 : 0 000 0 000 0 000 T 0 000 '0 000 0 000 0 000{ 000 K 0 000 0 000 0 88 468 L '"- # *'z .s Yy-5' Y�'- tax" .+w :.� - lLyyY� ..s L2 `< �-0` i `. ,horns rn_.:,: a ..., 3= i cernry, miner penany of taw, tnat tms document was prepared under my direction or supervision in accordance with (7iystem designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am 1 dare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/30/2017 �'' pature of Land Applier Date DFNR FnPM mm cG tt)i,)nnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM .PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: W00014868 Field #: 14 Acres Utilized: 7.5 Land Owner: JW Burney. Annual Dry Tons Applied: ` } 19 52 _ Fo Site #: SF07 Acres PBurney.rmitted: 7.5 Operator: Steve Dunham Predominant Soil Series: LaB Cation Exchange Capacity g p ty (non 503): 5.7 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 147 Crop 2 Name: Cron 2 Max_ PAN - ., Volume applied PP (enter one) Solids Volume Applied Residual Sources Soil Cond. Precip. 9 < 0 Z Nitrate PAN Applied Name of CropType -4 ° % per (AIPDES #, WQ#, Past 24 � ,� TRN c and Receiving Residual 8 � Liquid Solids Acre Fert., Animal (Dry' His. o �' : �' : °r° o 5 w• Nitrite (lbs/acre) Application A Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) ) Wet, Moist) inches o, �. 7 * T a « a mgBg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 4/8 52000 3 79 s :'15096 `+' Tazheel WWTP Dry <•5" S 0.5 0.2 91700 11635 2 '47.847 NA `•; Bermuda 4/9 71500 3.79 1507 Tazheel WWTP Dry <,5" S 0.5 0.2 91700 11635 2 65:789 NA"'' Bermuda 0:000 . 0:000 OOO;.p ' 0!000 ' 0.000 0 000_, 0'"000 0.000` O'000.2 av °0".000r Oi000il, 0:000;, 6.6001 6i000r;r 1 01000 ill. 01006, 0.000 0.000,". :•:<•>:»: ' , ( •._... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) ::.:%� '• TOTALS: As Cu Cr Pb H Mo Ni Se Zn P 1 3J696 ,oiOW ° Lime Applied Annual Ibs/acre 0016'• , .560i • 0!411: ` r 0 04a' "YO 002 1, 0092. ' 0:264 ,.0 026" I .14 792 :'88 468 s • , ..:.:5;: ;;..:;;:. Date ]bs/ac Prior Years Cumulative Ibs/ac o.1141 0 '`.7,t a0.0459 .1718 1.7029 I 2.11'4.. 0.5333 0,379f : 0.013 0 O15k 0.7474 0 8'401.184'.' 2.5921 0.1582 107.161 d121 953 :::: 2000 Cumulative lbs/ac 25orient 0 1000 250 Soo ';:. ;; ;;: :.: ...:::.....• ;.; ;.• ;. Permitted C. P. L. R. **** Permit PAN Limit ist/2 nd Crop 147i,'z'� ,,. . E_ 1 cCL Lily, arruCr PCrrau.y or raw, inat tors document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/30/2017 **Volatilization Rate: Surface - 0.59 Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1. annerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): ermit #: W00014868 Cation Exchange Capacity (non 503 only): Operator: Hinton King Owner: Hinton King Predominant Soil Series: fcres Used: 89.5 Acres Permitted: 89.5 Site #: _ SF08 nesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, Field #: MaA % Solids use Raw Percent #): ^unple or to 1 2 3 4 5 6 7 8 9 10 11 12 �Co I1/3/16 11/30/16 posite Date o Solids 1.21 0.44 Arsenic 3 3 --�admium 2 2 �;opper 62.9 183 Chromium 9.18 12.6 Lead 5 5 lercury 0.4 0.4 Molyb- fenum 13 9.85 Nickel 5.24 7.35 Selenium 5 5 'Zinc 100 311 Total I Phos- 19000 19300 )horns + nnual Heavy fetal Loadings (Calculated in lbs/acre): Total Ill 2 3 L4J 5 6 7 8 Lj 9 10 11 12 'iT/Ac./ o App. Event 0.61 0.05 irsenic 0 004`x0 000 0 OQO 0 000 ?I"0'000< 0000; O':0003 0 D00` 0 000 0 000__ 0 000, `0004- , . .0000 . idmium 0 002 0, 000 i 0 000;; x 0 000 0 000 , ,1U`000; 0 000 0 OQOr 0.000! ° 0 000 � � 0 000. 0 000r° ,,„01003 Copper *OQ7,6 Y0 019' YO OOOA nQ1000 ,=0 000 �"0 90'O.c <U;0_00 O OOOr 0 OOq 0 000`:, x 0 000 0 OOO,x , ;Q09,G romium0 Ol,l;; , 0 OOl . ;n0 000 . `;;O 000, ;O OQO: 0.000 O 000 . _,0 000, t 0 OOQr 0 OOO;r0 000-O 0,00 `0:012>' 'Lead �0 006' 0 001, ° 0 000 :0 000,. , 0' 000 Os,000 0000O OOO ,. 0 OQO; , r0 000 0 000,0 000 .,.O,.00Z;° Mercury OQO 0 000.= 0 000 0 000 + 6;0_Ol' , 0 000 Qolyb- 0 016 3s0 001 0 OOU- 0 0�0 0 000 0000` 0 000lenurn 0009� r0 OOOa SO 000 t 0 OOOs'0'000 0 �017'- Nickel FO 00`6h r0',001 0 Q00 _0 000, r ,0 000 0,000 0000 ,0:0`000 000-` YO`0001 0 000._ 0 000_ sg000T ';lenium 0 006=; , 0 001 r 0 000 0 000 F,.O 000O 000 a0:000' 0.000 0 000' s 0 000 `_'; 0 000_y `0 OOO Qi007 - -'Zinc 0 122= Y 0_Q32 r, 0 000,, ,, 0 000 , `0 000; 10:000 , 0 000 r0,00Q; , 0.0,00 ' 0 OOOY,k_ ?,0 000 5;0 000 t`0=,154 Total y Mxih 5 i5j wZfiY� Phos- 23Jti.104t 2 007 R OOOR itY�` 000 0 OOOa 0 000 £� jS3�(:i �0 000 0 000 0 000 0 000 0 000 0 000 25 1°l l' I}lONS ^+If'a [: t } �. �':.v_,�.Sf,.Y I €'aL 4 �,0 eX'x'`y :; <Y. a "f y Or �6 "C e✓.vSn..«u r } ,` =�3'[� ,3,' M fa. R ty4 ei t <r<�az _ .H�: _ ... ..-.✓'3 $C.. mow:=. Ca�s..<..�<.:, � £:k.,Na. rE.x_ "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance h a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. L_ in aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ' 1/30/2017 F" gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. Land Owner: Hinton King Operator: Hinton King Crop 1 Name: Wheat WQ Permit #: WQ0014868 Field #: Annual Dry Tons Applied: r,l ' 359 07 Site #: Predominant Soil Series: MaA Crop 1 Max. PAN: 121 Crop 2 Name: Acres Utilized: SF08 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 89.5 89.5 3.2 [ e ° q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NpDES #, WQ#, Fert, Animal Waste, etc) Sod Cond. wry' Wet, Moist Precip. Past 24 Hrs. Inches 9 b a �. i O ^' o BL S' " ♦ ti TKN mg/kg 54900 z ct o o w. mg/kg 13900 Nitrate and Nitrite mg/kg 105 PAN Applied (Ibs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 11/16 123500 121 Tarheel WWTP Dry <.5" S 0.5 0.2 •• 2.44(f" -NA ,! Wheat 11/17 117000 1 21-O'056',; Tarheel WWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 ` 1:999 'NA"" Wheat 11/18 110500 1.21 v`/Oi062 `' Tarheel WWTP Dry <.5" S 0.5 0.2 54900 1 13900 105 . 1,888 NA:° ' Wheat I1/21 136500 1.21 . '0077'-- Tarheel W WTP Dry <,5" S 0.5 0.2 54900 13900 1.05 2332 .. NA..." Wheat 11/22 117000 121 l 0066 Tarheel WWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 . 1.999 ,NA•,. Wheat I1/23 117000 121 , 0066 ','i Tarheel WWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 1,999 ` NA"+ Wheat 11/28 104000 121 ,-6!059%, Tarheel WWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 t777 NA`?;i Wheat 11/29 136500 1.21 Oi077,., TarheeIWWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 Wheat 11/30 117000 121 0`066' •.,; Tarheel WWTP Dry <,5" S 0.5 0.2 54900 13900 1.05 : 11999 NA-"' ' Wheat 12/1 149500 0.44 " - 0!031' Tarheel WWTP Dry ¢5" S 0.1 0.2 80000 80000 1.07 2:452-, NA•.- Wheat 12/2 104000 044 110211 _ ., Tarheel WWTP Dry <,5" S 0.5 0.2 80000 1 80000 1 07 1.1'706 Nkl: Wheat a 0000 0;001, ' 0 ,` NA: Wheat ::•: :•:: - Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form) ""' '"•""'" TOTALS: , I , s0 : 1332500 As Cd Cu Cr I Pb Hg I Mo I Ni Se I Zn P .'225 -0'000-; Lime Applied Annual lbs/acre -; 0 004 Ot'003 j 0`.096` 0 012 _: �', 6.667, °. = IVoff 0.617 ' ( 0.007� 0.007 ' i 0 154' : �35 11 F., • , • . :::: : ::::::: : :: ............................ :: :•: •.•.::.:.:: •:: :•::: •.:•:: ................................. �..-.y.• .� Date lbs/ac Prior Years Cumulative lbs/ac 0.049 0.023 10.477 1,365 0.18 0.006 0.323 1.125#0�.L0214 50.13 2000 Current Cumulative Ibs/ac 0:0531:, Permitted C. P. L. R.**** 9 250 1000 250 500 2 Permit PAN Limit 1st/ nd Crop - - '�12It "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �Jf *Application Method: S - Surface, IN - Injection, INC - Incorporation ���""""`� 1/30/2017 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, annerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* • .1 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Vcility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual) O 0 F ermit #: W00014868 Cation Exchange Capacity (non 503 only): 3 Operator: Hinton King Owner: Hinton King Predominant Soil Series: NoA F`cres Used: 64.5 Acres Permitted: 64.5 Site #: SF08 Field #: 4 i_esidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): c�mple or 1 2 3 4 5 6 7 6 9 10 11 12 ICom- posite 11/3/16 Date ;i Solids 1.21 "Arsenic 3 ^3dmium 2 I opper 62.9 lChromim 9.18 —Lead 5 ;lercury 0.4 Molyb- 13 ,lenum Nickel 5.24 Selenium 5 Zinc 100 Total ` Phos- 19000 --)horns ,nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 0 "?T/Ac./ App. � y Event 0.92 lsenic 0 005' , 0 000c , 0 000,- ;' 0 000 , -A 000 0 000 , 0:000 F 0 000a 0 000, 0 000'•_' , 0 000 . ' 0 000f, ,,0 005:- admium :_ _ 0 0,,q t 0 000: 0 000� k 0 000 j 000 ` 0 000 __ , 0.000 . 0.000a 0:000_ 0 000 `- 0 000 h " 000 ; ' 0 604�' Copper <0 ).15 0 000;• ¢ 0 000 0 OOOv 0000 0:000 ° 0 000' 0 OOO Id: 0 OOOv_?0 000 1,0 1,15;~; .0:000, , )y0.000 — romi 0 017`, ; 0 000' 0.000 '" 0 000 _- 0 000 , 0000,0:000 O.000m 0 000', 0 000 ° 0.000 `. 0 000 `;0 017 Lead 0 000.r _0 000y 0 000` ',`'0 000 0 000 0_:000 O';000 = 0:000 0t000 0 000;< < 0 000' a 0 000 _ `,0_:009'' Mercury r CA 0 000 . 0 000': 0 0,00' 0 000 , 0 000 ,0:000. 0.040s 0 000 0 000° 0 000, _±0 00-6 '0.001'. Qolyb 0 024'' i 0 000 -, �0 000 a 0 000f , �0)000 a0"000 0 000 r 0 000 t 0 OOOY 0 000; 0 000$ `0 000 0 024= lenum Nickel 6010, ` � 0 000 , 10 000 , 0 000 -_ 000 °0;000 _ � 0 000 , ,0 000 0.000 0 000 0 000, "0 000 ,:0 Oj O-; " ",lenium 0.0091= 0 000; _ 0 000 j;0 000 •`;0 000 , „0 000. _0.000 0 000 0 OOOt, _ 0 000=i t0 000 ,'0 000, 0 009`• Zinc 0 183a+ 0 000%„ 0 000 f 0 000 °;0 000 `0;' 00(r 0 000_ 0[000 000 ;, ' 0 000 O 000, _ ,0.000, .0 `A.183'? Total �Fi Phos- 34 770 nQ 000 ` 0 000 0 000 0 Oo 0,000 ) 0 000 s 0 000 0 000' t 0 000 '30 J600 0 000 34 770' F LS -S F H 4t I f r F` :•.a "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". +� 1/30/2017 {v ,gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Smithfield Farmland Corp. Land Owner: Hinton King Operator: Hinton King Crop 1 Name: Wheat PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0014868 Field #: Annual Dry Tons Applied:S9 02 „��,� Site #: Predominant Soil Series; NoA Crop 1 Max. PAN: 125 Crop 2 Name: SF08 Acres Utilized: 64.5 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 64.5 2.9 a,e Volume applied Volume Residual Sources Sod Cond. Pn:cip. 9 o �• z Nitrate PAN Applied pP Name of Crop Type ° (enter one) Solids/ % Applied per (NPDES #, WQ#, Past 24 t, rr- y .- `�° i9 �, TKN o and (Ibs/acre) Receiving Residual Liquid Solids Acre Fert., Animal (Dry,, His. 0 w *, �' Y Nitrite Application A Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) inches * o ° 7 * ^. a mg/kg 54900 mgtkg 13900 mg/kg 105 Crop 1 Crop 2 Crop 1 Crop 2 10/31 78000 121 kP.,006Pr TarheelWWTP Dry <.5" S 0.5 0.2 t,1ed9I NA- Wheat I1/1 136500 1.21 Tarheel WWTP Dry <.5" S 0.5 0.2 54900 13900 1.05 Wheat 11/2 136500 1 21 ,``0107;,"�*_ Tarheel WWTP Dry <.5" S 0.5 0.2 54900 13900 1 OS 3.236 , NA i_:� Wheat 11/3 136500 121 0:-=107 �:� TarheelWWTP Dry <.5" S 0.5 0.2 54900 13900 105 •3:236 NA::y', Wheat 11/4 45500 121 0,'036 '; TarheelWWTP Dry <,5" S 0.5 0.2 54900 13900 105 ;LM, NA*;:f Wheat 11/7 104000 1.21 Tarheel WWTP Dry <.5" S 0.5 0.2 54900 13900 1.05 Wheat 11/8 97500 121 _0081.r„ , 0Z176 �, Tarhee1 WWTP Dry <,5" S 0.5 0.2 54900 13900 1 OS 2`3T1 ,NAT Wheat 11/9 130000 1.21 , ' O:rJ02 � Tarheel WWTP Dry <.5" S 0.5 0.2 54900 13900 1 05 ,,3'b82 4 l NA,= Wheat 11/10 136500 121 O'�107 ';+ Tarheel WWTP Dry <.5" S 0.5 0.2 54900 13900*J',:' 36 "rNP:4 Wheat 11/12 78000 1.21 ^0106J „ Tarheel WWTP Dry <.5" S 0.5 0.2 54900 1390049 , ,NA��'.'? Wheat 11/14 6500 121 . ,,605', fi TarheelWWTP Dry <,5" S 0.5 0.2 54900 1390054 1 +NA'1" Wheat Tarheel WWTP D <.5" S 0.5 0.2 54900 1390003 ? Wheat 11115 84500 121 _`•' Oi066 .:' .'NA lT, ' ��. h, ..:: , , , _)n , Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this r +„'>1:.:YTOTALS:o „PnooOo .::i > As Cd Cu Cr Pb H Mo Ni Se Zn?34 * 0.000xt Lime A lied Annual lbs/acre009`* 0=01'9 „ 0 009:-' on183., :;;;: :;:; :, •. >';;; > : ; " " . Date lbs/ac Prior Years Cumulative lbs/ac 0.033 0.015 77219 0.55 0.122 0.004 0.247 0.731 0.059 36.926 2000 Current Cumulative Ibs/ac b 038e „ ` 0:019 , Iz o.&4 , 0 567•'., I rOs131 a r'0 005 , Ot271` - ,0,7,41t `0 06$ 2 ; 37 109"' Permitted C. P. L. R.**** 9 250 ]000 250 500 Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation t /IWIM1 7 **Volatilization Rate: Surface - 0.5 Iniectiou/Incorporation -1.0 Signature of Land Applier Date , *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) Page: 1 of 2 Report Number: 16-092-0205 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 56497 Sample Id: NORTH BASIN Waypoint_ ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/31/2016 13:30:00 Date Received: 04/01/2016 00:00 Date Reported: 04/05/2016 Total Solids ` 4.66 46600 100.0 JM 04/01/2016 15:00 SM-254OG Moisture' 95.34 100.0 JM 04/01/201615:00 SM-254OG Total Kjeldahl Nitrogen 7.51 75100 10.0 JM 04/04/2016 08:39 SM-4500-NH3C-TKN Total Phosphorus 1.82 18200 100 KM 04/04/2016 14:06 SW 6010C Total Potassium 0.37 3730 100 KM 04/04/2016 14:06 SW 6010C Total Sulfur 1.77 17700 100 KM 04/04/2016 14:06 SW 6010C Total Calcium 1.90 19000 100 KM 04/04/2016 14:06 SW 6010C Total Magnesium 0.19 1920 100 KM 04/04/2016 14:06 SW 6010C Total Sodium 0.87 8740 100 KM 04/04/2016 14:06 SW 6010C Total Iron 14300 100 KM 04/04/2016 14:06 SW 6010C Total Aluminum 10400 100 KM 04104/201614:06 SW 6010C Total Manganese 382 5 KM 04/04/2016 14:06 SW 6010C Total Copper 1240 5 KM 04/04/2016 14:06 SW 6010C Total Zinc 3090 5 KM 04/04/2016 14:06 SW 6010C Ammonia Nitrogen 0.94 9440 10.0 JM 04/04/2016 08:39 SM-4500-NI3C Organic N 6.57 65660 10.0 04/04/2016 08:39 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 04/04/2016 08:40 SM-450ONO3F Total Cadmium <2.0 2.0 KM 04/04/201614:06S/W/6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmports and letters am far the exclusive and confidential use of ourclients, and may not be reproduced in whole orpart, normay any reference be made to the work, the results, orthe company in any adwr lsing, news mlease, orotherpublic announcements without obtaining purprior written authorization. Debbie Halt -0,R§ TT� ITKGY----, -A&L Eastem is S 621,Whitepine Road Richmon il'VA,23237,Tchg()� ENIA RESOURCES INC 16 SWTHRELO-TAR IIFEL. I, 1R. EMA R,6sbiurces Inc' '-F-MA Resourc'eslnc 755 Yadkinville Rd '35.5.Y.AdIdnville Rd Mocks-vUle,NC 27028 T 1 fopksville, NC 270,28. a I N =6`1 EWE -F Ogg qk—rg rr�qg� W It, 142 R AYS "Vill 00 1 It wvy 'lira% N OR 'Gr k/-z omposite I U .4;qt 7-- _Grab PIM Glass 0 P"L mint. qt •_Glass.` ,_pint —born poslbail P­ 49 SLI.- Total Solids (Moisture) Total 10jel(w Nitrogen, Pliosphorms and Potassium, SL2; Basic'TesISLIAlas suffix,6alcium.Magn miumAodium. Iran, Aluunl6m, Manganese, Copper And Zinc 56 Me6lavArsdrilo., Cadmium, Chromium, Mercury, Molybdenum, Lead. Nickel, Selenium. & Zino Included In d2) .(Copper Nitrogen Sari= Total Neldahl, Ammonium. Nitrate &Organic Nitrogen. GCE -:Calcium Caitionatti r=qUWldnt or Tctsl�neutrallzafion Value (For Unne Treated Sludge) rya _. -_� ���"} _�.� �-_ 1 •ate; t- _� _ _=i _-_-_� '-� { �� �.��7 ,-�"�> t:� �y��l t` T-1 __-�_ .-_) Page: 1 of 2 Report Number: 16-113-0215 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE, NC 27028 • 0. Waypoint. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 • Fax 804-271-6446 www.waypointanalytical.com Project: SMITHFIELD TAR HEEL -SOUTH NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/21/2016 11:20:00 Date Received: 04/22/2016 00:00 Lab Number: 56869 Date Reported: 04/29I2016 Sample Id: SOUTH LAGOON 4.04 40400 100.0 JM 04/22/201615:35 Total Solids 100.0 JM 04/221201615:35 Moisture' 95.96 9.58 95800 10.0 JM 04/28/2016 08:39 Total Kjeldahl Nitrogen 100 KM 04/25/2016 13:08 Total Phosphorus 1.65 16500 0.36 3620 100 KM 04/25/2016 13:08 Total Potassium 18000 100 KM 04/25/2016 13:08 Total Sulfur 1.80 1.62 16200 100 KM 04125/2016 13:08 Total Calcium 1750 100 KM 04/25/2016 13:08 Total Magnesium 0.18 100 KM 04/25/2016 13:08 Total Sodium 0.67 6740 14700 100 KM 04/25/201613:08 Total Iron 8400 100 KM 04/25/2016 13:08 Total Aluminum 5 KM 04/2512016 13:08 Total Manganese 353 5 KM 04/25/2016 13:08 Total Copper 901 5 KM 04/25/2016 13:08 Total Zinc 2710 1.09 10900 10.0 JM 04/26/2016 09:09 Ammonia Nitrogen 10.0 04/26/2016 09:09 Organic N 8.49 84900 <2.00 2.00 JM 04/25/2016 08:50 Nitrate+Nitrite-N 2.0 KM 04/25/2016 13:08 Total Cadmium <2.0 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-2540G SM-254OG SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NI3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 16-113-0215 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE, NC 27028 Lab Number: 56869 Sample Id: SOUTH LAGOON Waypoi ntn 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9402 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: SMITHFIELD TAR HEEL -SOUTH NC CERT#257 REPORT OFANALYSIS Date Sampled: 4/21/2016 11:20:00 Date Received: 04/22/2016 00:00 Date Reported: 04/29/2016 Total Chromium 70 5 KM 04/25/2016 13:08 SW 6010C Total Nickel 51 5 KM 04/25/2016 13:08 SW 6010C Total Lead 8 5 KM 04/25/2016 13:08 SW 6010C Total Arsenic <3.0 3.0 KM 04/25/2016 13:08 SW 6010C Total Mercury <0.4 0.4 KM 04/25/201609:00 SW-7471B Total Selenium <5.0 5.0 KM 04/25/2016 13:08 SW 6010C pH (Standard Units)8.04 2.00 JM 04/26/2016 08:50 SW-9045D Total Volatile Solids 82.33 823300 100.0 JM 04/22/2016 15:35 SM-254OG Total Molybdenum 19 5 KM 04/25/2016 13:08 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI", "Fe", "P", "K", "S", AND "Zn". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmpods and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made to the work, the results, orthe company In any advertising, news release, or otherpublic announcements without obtaining ourprtor written authorization. Debbie Holt e : �Yfi. >•aFT�" t ,t:63s-•..� a.k• - - f.}.�t'tAl� �(y+7*1' i ,S}t`�GACCOUt�n;,etfvNN J: 04'22 } 1355A11 ... �� 7621 WbrtepmeRoadRrchmondVA23237 Te1:804,743� a,AtzEsotmcEs'l� d ® .. sN3rHFlELOTAR HEELSOl1TH Ca,�l} f tv g c-a.�ts r v�xsrr'w z+.4w ':p4" � �+*' �Mrs� z � r sto�rte�jlnforrt,adon' +MS?� ��ij2''�ub�li;ad�Byx �o^sg�y��t�;W,�iyY'�?.,g«,n�,rr ➢Cl�.p..`t �' a ay. .+{ ;kdR!4Srr%�:i1`44.'f r.",�5 ara�, i;Tr•^o+t, s, i+t �:fr F f:, �*F.. nw '.<+�.. EMA Resources Inc EMA'Resources Iric 755 Yadkinville Rd 755 yadkinville Rd Mocksyille, NC 27028 IVI0Cksl0q, NC 27028 s 5u tiGrab 5 �101t, �raoa 1 _ Grab composite Grab a .If I y� Y' 2 M..i TestlP.aokai a Beieils x., _at its :a "x'{c'-r ' ' rusan SLl Total Solids (MmsturejTolal Kjeldalil-Nitrogen, Phosphorus'ond Potassmm Sodium, Iron, Aluminum, Manngphhsc, Copper And 2mc SL2: Basic Tast'$LI plusiSulrur, Calcium, Magnesium, Molybdenum, Lead, Nldml, Selenium. 503 Mstate- Arsenic, Cadmium; Chmmlum,Meicury, (Copper&7lncincludedinSL2) rn ' Nltragen:5crics Total Kjelde6i, Ammamum,Nitrate& organic Nitrog=. Velue tFor.L'cne Treated Sludge] `. CCEc Czlaum;CadwnateEguivalentorTotel neuhalim6on a P age. 1 of 2 G . Report Number: 16-113-0214 • Account Number: 46245 Waypoi nt. 7621 ain 804-7 Road, Richmond, 27 -6446 Main 804-743-9401 0Fax 804-271-fi446 ANALYTICAL www.waypointanalytical.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 56868 Sample Id: NORTH LAGOON Project: SMITHFIELD TAR HEEL -NORTH NC CERT#257 REPORT OFANALYSIS Date Sampled: 4/21/2016 10:30:00 Date Received: 04/22/2016 00:00 Date Reported: 04/28/2016 Total Solids 2.81 28100 100.0 JM 04/22/2016 15:35 SM-2540G Moisture' 97.19 100.0 JM 04/22/201615:35 SM-2540G Total KJeldahl Nitrogen 8.79 87900 10.0 JM 04/25/2016 08:50 SM-4500-NH3C-TKN Total Phosphorus 1.56 15600 100 KM 04/25/201613:08 SW 601CC Total Potassium 0.30 2980 100 KM 04/25/2016 13:08 SW 6010C Total Sulfur 1.78 17800 100 KM 04/26/2016 13:08 SW 6010C Total Calcium 1.99 19900 100 KM 04/25/2016 13:08 SW 6010C Total Magnesium 0.18 1750 100 KM 04/25/2016 13:08 SW 6010C Total Sodium 0.73 7280 100 KM 04/25/2016 13:08 SW 601CC Total Iron 13900 100 KM 04/25/201613:08 SW 601CC Total Aluminum 8600 100 KM 04/25/2016 13:08 SW 6010C Total Manganese 327 5 KM 04/25/2016 13:08 SW 6010C Total Copper 1150 5 KM 04/25/2016 13:08 SW 6010C Total Zinc 2750 5 KM 04/25/2016 13:08 SW 601CC Ammonia Nitrogen 1.25 12500 10.0 JM 04/25/2016 08:50 SM-4500-NH3C Organic N 7.54 75400 10.0 04/25/2016 08:50 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 04/251201608:50 SM450ONO3F Total Cadmium <2.0 2.0 KM 04/25/2016 13:08 SW 601CC All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. &Ue_� Ourreports and letters are for the exclusive and confidential use of our clients, and may not be mpmduced in whole or pan, normay any reverence be made (y? to the work, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourpdor written authorization. Debbie Holt _i _ - _l -� ' �. Page: 2 of 2 Report Number: 16-113-0214 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 56868 Sample Id: NORTH LAGOON • Wayporntn ` 7521 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: SMITHFIELD TAR HEEL -NORTH NC CERT#257 REPORT OFANALYSIS Date Sampled: 4/21/2016 10:30:00 Date Received: 04/22/2016 00:00 Date Reported: 04/28/2016 Total Chromium 63 5 KM 04/25/2016 13:08 SW 6010C Total Nickel 38 5 KM 04/25/2016 13:08 SW 6010C Total Lead 8 5 KM 04/25/2016 13:08 SW 6010C Total Arsenic 3.0 3.0 KM 04/25/2016 13:08 SW 6010C Total Mercury <0.4 0.4 KM 04125/201609:00 SW-7471B Total Selenium <5.0 5.0 KM 04/25/2016 13:08 SW 6010C pH (Standard Units)8.04 2.00 JM 04/25/2016 08:50 SW-9045D Total Volatile Solids 80.92 809200 100.0 JM 04/22/2016 15:35 SM-2540G - Total Molybdenum 16 5 KM 04/25/2016 13:08 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ai", "Fe", "P", "K", "S", AND "Zn". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourpdor wdhen authodwtion. Debbie Holt M�6§ x.a w11�6AIr'�y,. Mvm.Mf 1}L,li A&L "Ea 7621 Whitepine Road Richmond VA23237' III���I�IhIIiID01�N19NN INIDIINIpN�lehl 5 ;s , ,.; . ..v M9i ti#-imp NORTH TARHEEL an'iSg�, r. ? 1€rk a"=i5i i k 41 r�SfibmlCteaBy'a;1� _ is. -ISM f'C x . h .n. , s„�ii'82r_.t*.F +:ae....,, .Cv ml.anPs.Yr. Sh'.. ;�gPYzto„a wu4,«n nt� M6a_,.. __.�.e.,-.,-�rr:�ae'- :.-c ., t.._ _ .�•rY,r EMA Resources Inc EMAResources Inc 755 YadkinviIle Rd 755 'YadkinvWe Rd MocksviUe, NC 27028 MuckwMe, NC 27028 e w ra:,! nT x- r x, mom. rm a .. r"Ye a 4 ll . ,xma cxrc MIT .. a NI >1-.;�, N*r *"'"�i.r`,',"�'rf '�.. ,,'d"G'`bnlaner� rm�U,onlsa.°nm4 a#i:tm �-�.:,i�$�'(eeckDea rT„, .?nt;.� 'race, 4X r't'?E+"F,''n.r"QC,411edionlnfofniO.n.fiSY'aaw., ...� .F a r!" .a. K r-•-, ^F*•,.w �"� _ eb`+`tif't ,�-+ rq, ,.... S r.r[ a'^'.F'i r�H e�'i.�a, iiY "FG.`.i �e Pis'7.�a' �''� t ,'n�i r r h;� wS�AT*. ?S+ifk' yr �.6"t�. AS' i ,r?�rN. , `S IO"+rNch'tr"'3'�m-ge`.�'4� ai$'35�{4M$'• 'W''"''Kn:«'-,"..� r.le'4t603rg t<08en-a+Tt',".ia VOWhe+te^ygl*k,�ur. ,4 13 "�6 t. ; N u y e ;", r r ;y x ;: olume SL1 T71pa .e.t a .r +, c+» n, n% .k.o-sGl H gCCE3 AgMf t { .nt Dab3 Ii S P. a �r1 NIP IteSr4y ,1C+'11, f�i��.tt?fiayg�w, 'I i. _k'knae 2+` ,7 t10a1a$n{..�T.W l �w. q+ xio-y"��YY m...� .w+1Di Ivc' Y 1in. Nil:::, +'.'4. _lw"U S694viS'4ki A'S�+LSi �++a'i -5x' _3£Y 3d x`"ui+v'f.WV.Y:L a..•= r2 .'4.a, ril .ss. i4y' c,*s}1.,„. .: j..,. oz Glass compositeqt _Glass co — _Grab — Composite _Plastic —lnl t _ Grab Gam _. oz Pint _ Composite Plastic _ Grab mYpostiwt.eaC Plastic h" _ dN�m ' 5t4.J, r Wr �Iiin�rPu�l.'411 ^mdbye�5�✓1" �I2.iF.'�nI 6C�k10 !. i n �1 yG'1 1?rf iM+1p� Y�Yi �OR }l"xil��r 'S—k^tiMkgityqp�Q YiAn{)t�.. 'T; 1'1RI'%r'"„WrJ,p 0e z3l.yr�r,:k.r^',t�`hktnR4 a Si nature „ ; rB r-S east IristN� diens.br:Remarks € . zkh :Bo AM u f 5,. � .CDC.._ MI + Er zra"z �s,.":..�_ SLI: Total Solids;(Moiatum) Total Kletdal4lNjtrugen,`Phophorua end Potassium SLY: Basic Test SL I plus Sulfur, Calemn%Magneslum,Sodium, Irou, Aluminum,Manganese, Copper And 2me 503'Metals- Arsenlq'Cadmium; Chromium, Mercury, Motybden_um, Lead,Nickel, Selenium. (Copper & 7.�nc ipdoded in SL2) _ Nitrogen Series: Total Kjeldahl Ammonium, Nitrate & Organic:Nilrogen. CCM Calcium Carbon aleEgui, lent orTetal neutratmdon Value (For lame Treated Sludge)`' Page: 1 of 2 Report Number: 16-131-0203 Account Number: 46245 Way 7621 Whitepine Road, Richmond, VA 23237 Y/�O' �ry ' Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE, NC 27028 Project: Smithfield Tar Heel NC Cert#257 REPORT OF ANALYSIS Date Sampled: 5/912016 19:00:00 Lab Number: 57191 Date Received: 05/10/2016 00:00 Sample Id : Smithfield Tar Heel SB Date Reported: 05/13/2016 Total Solids 3.65 36500 100.0 JM 05/10/2016 15:20 SM-254OG Moisture' 96.35 100.0 JM 05/10/201615:20 SM-2540G Total Kjeldahl Nitrogen 10.80 108000 10.0 JM 05/11/2016 09:29 SM-4500-NH3C-TKN Total Phosphorus 1.77 17700 100 KM 05/11/2016 11:23 SW 6010C Total Potassium 0.44 4400 100 KM 05/11/2016 11:23. SW 6010C Total Sulfur 1.97 19700 100 KM 05/11/2016 11:23 SW 6010C Total Calcium 1.79 17900 100 KM 05/11/2016 11:23 SW 6010C Total Magnesium 0.19 1920 100 KM 05/11/2016 11:23 SW 6010C Total Sodium 0.80 8000 100 KM 05/11/2016 11:23 SW 6010C Total Iron 1.47 14700 100 KM 05/11/2016 11:23 SW 6010C Total Aluminum 1.00 10000 100 KM 05/11/2016 11:23 SW 6010C Total Manganese 0.04 386 5 KM 05/11/2016 11:23 SW 6010C Total Copper 0.10 983 5 KM 05/11/2016 11:23 SW 6010C Total Zinc 0.28 2820 5 KM 05/11/2016 11:23 SW 6010C Ammonia Nitrogen 1.37 13700 10.0 JM 05111/201609:29 SM-4500-NI3C Organic N 9.43 94300 10.0 05/11/2016 09:29 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 05/11/201609:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/11/2016 11:23 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourreports and letters are forth& exclusive and confidential use of ourdlents, and may not be reproduced in whole or part, normay any reference be made to the work, the results, or the company In any advertising, news release, orotherpublic announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 16-131-0203 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE, NC 27028 Waypoint. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 • Fax 804-271-6446 www.waypointanalytical.com Project: Smithfield Tar Heel NC Cert#257 Lab Number; 57191 REPORT OFANALYSIS Date Sampled: 5/9/2016 19:00:00 Date Received: 05/10/2016 00:00 Sample Id :Smithfield Tar Heel SB Date Reported: 05/13/2016 Total Chromium 79 5 Total Nickel KM 05/11/2016 11:23 SW 6010C Total Lead 58 5 KM 05/11/2016 11:23 SW 6010C Total Arsenic 8 5 KM 05/111201611:23 SW 6010C Total Mercury 3.0 3.0 KM 05/11/2016 11:23 SW 6010C Total Selenium <0.4 0.4 KM 05/12/2016 09:00 SW-7471 B pH (Standard Units) • <5.0 5.0 KM 05/11/2016 11:23 SW 6010C Total Volatile Solids 8.00 2.00 JM 05/11/201609:29 SW-9045D 82.00 820000 100.0 JM 05/10/2016 15:20 SM-254OG Total Molybdenum 19 5 Comments: KM 05/11/2016 11:23 SW 6010C SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Ni". THE MATRIX SPIKE WAS OUT OF LIMITS FOR -Al-. ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourreports and letters are for the exclusive and conlidendal use of our clients, and may not be reproduced in whole orpart, normay any reference be made to the work the results, or the company in any advenising, news release, or other public announcements without obtaining our pdor wnften authodzaflon. Debbie Holt 'BIOxSOLIDS�SI'� ^� �'� �TR�:4NS�V1'i'srT A&L .Eastem' 7621 Whitepine Road Richmond VA 23237 Tel: 804- Il�l��lull�l�l IHI��IIII�IIu�IIII�II�IIIuIIIIII��IIIIIIII 16-131-02 g5°ti zeta EWRESOORCES'INC 13:3343 Smilhrield Tar Heel EMA Resources Inc I EMA Resources Inc 755 Yadkinville Rd 755 Yadkinville Rd Mocksvipe, NC 27028 D � t� tti,5S�� .S 5'�T'^i+. P'`7 a%....L' /, i � � IR 4� �� '4 2�J A" P L r3 ," .3.J d'F�.'6,t G vry.YyW '...,��i' i � i �/i. S {�* "i. 1 2 1CRy f ti� ..'.e � 'F r'. ��� T li•Y* 4H i' l�f„[r�.r.� e��' 4�a;?�a.�+�l. ����•�a��Sa[n le?Information�U�."�?.µ.t��s ,�_Tr'�t�{'a�xe:�rx,�M� ,�x,�.§�.>z� l f� ._4,><,: h;_.�i..��j•��,�� ,yLeliiNu`S+CollecUori ����,�_3�,�..t�. Inionn' a an M;+ { �"; lay <Coritamelslnfortrjallon?"rly') rt..:.:.e S "fK S H \�:, { "•�x„� R 1 ..�Z d "_} xr"`..sntdDawF,'TYP.a..r a,.: uLLMGrab Composite q �tpGrab . 40l ^sL'c_PGlass t 7.—Plasfic GlassComposite—piastic —int tGrah _ Glass — oZ int Composite Plastic fit Grab _Glass — oZ joqt lt Composite c Total Solids (Moisture) Total Kjeldahl Nitrogen, phosphorus and Potassium : Basic Test SLI plus Sulrur, Calcium, Magnesium,Sodium, Iron, Aluminum, Manganese, Copper And Zinc Metals: Arsenic. Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc included In SL2) -open Series: Total Kjeldnld, Ammonium, Nitrate 8: Organic Nitrogen. E: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) D ---3 ----_� Page: 1 of 2 Report Number: 16-309-0201 Account Number: 46245 Send To: EMA Resources Inc 755 Yadkinville Road Mocksville , NC 27028 Lab Number: 60531 Sample Id : Smithfield Tar Heel Waypoint0 d ANALYTICAL 7621 Whitepine Road,Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: Smithfield Tar Heel NC Cart #257 REPORT OF ANALYSIS Date Sampled: 11/3/2016 07:00:00 Date Received: 11/04/2016 00:00 Date Reported: 11/14/2016 Total Solids • exce as noted 1.21 12100 100.0 R D 11/04/2016 14:40 Moisture • 98.78 100.0 R D 11/04/2016 14:40 Total Kjeldahl Nitrogen 5.49 54900 10.0 SJB 11/07/2016 09:20 Total Phosphorus 1.90 19000 100 SJB 11/09/2016 12:11 Total Potassium 0.61 6130 100 SJB 11/09/2016 12:11 Total Sulfur 1.58 15800 100 SJB 11/09/2016 12:11 Total Calcium 0.91 9130 100 SJB 11/09/2016 12:11 Total Magnesium 0.23 2280 100 SJB 11/09/2016 12:11 Total Sodium 2.72 27200 500 SJB 11/10/2016 12:54 Total Iron 1320 100 SJB 11/09/2016 12:11 Total Aluminum 74200 100 SJB 11/09/2016 12:11 Total Manganese 115 5.00 SJB 11/09/2016 12:11 Total Copper 62.9 5.00 SJB 11/09/2016 12:11 Total Zinc 100 5.00 SJB 11/09/2016 12:11 Ammonia Nitrogen 1.39 13900 10.0 SJB 11/07/2016 09:20 Organic N 4.10 41000 10.0 11/07/2016 09:20 Nitrate+Nitrite-N <1.05 1.05 SJB 11/071201613:28 All values are on a d wei ht basis t b t N k D SM-2540G SM-2540G SM-4500-NH3C-TKN 6010C 6010C 6010C 6010C 6010C 6010C 6010C 6010C 6010C 6010C 6010C SM-4500-NH3C CALCULATION 4500NO3F-2011 ry 9 p y as eras . e ec on in on a series is on a wet asis. Our aspens and letters are for the exclusive and confidential use of ourcllents, and may not be reproduced in whole orpan6aftm, normay any reference be made to the work, the results, orthe company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization. Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-309-0201 Account Number: 46245 Send To: EMA Resources Inc 755 Yadkinville Road Mocksville, NC27028 Waypo0 G int. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Project: Smithfield Tar Heel NC Cert #257 Lab Number: 60531 REPORT OFANALYSIS Date Sampled: 11/3/2016 07:00:00 Date Received: 11/04/2016 00:00 Sample Id : Smithfield Tar Heel Date Reported: 11/14/201s ---...._... 14.vv Total Chromium 9.18 Total Nickel 5.24 Total Lead <5.00 Total Arsenic <3.00 Total Mercury <0.400 Total Selenium <5.00 pH (Standard Units) • 7.72 Total Volatile Solids 72.97 729700 Total Molybdenum 13.0 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. z.UU SJB 11/09/2016 12:11 601OC 5.00 SJB 11/09/2016 12:11 6010C 5.00 SJB 11/091201612:11 6010C 5.00 SJB 11/09/2016 12:11 6010C 3.00 SJB 11/09/2016 12:11 6010C 0.400. JM 11/11/201612:45 SW-7471B 5.00 SJB 11/09/2016 12:11 6010C JM 11/07/2016 09:20 SW-9045D 100.0 R D 11/04/2016 14:40 SM-2540G 5.00 SJB 11/09/2016 12:11 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis. Ourmports and letters are for the exclusim and confidential use of ourclients, and may not be reproduced in whole orpart, normay any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our priorwritten authorization. Debbie Halt Laboratory Supervisor — v BIOSOLIDS SAMPLE !'CUSTODY I Account# L III�IIIII�1111IN111111111�111111llll�10111111111;� 2015 s, Inc. B 7621 WhitepineRoad Ri EMAResources1no 12.49s8 ' flicc@al-labs-eastem.com Smithfield Tar Heel Submitted By >_Cfiatge To Copy To EMA Resources Inc EMA Resources Inc 755 Yadkinville Rd 755 Yadkinville Rd \ �//Mocksville, NC 27028 Mocksville, NC 27028 Project geed Sample Information Lab Number •(Lab Collection In6tma'on Container Iriforma& Please Check Desired Tests Sample ID • . • Use " Only)' Type Date Torre • Number Type; h� ,,Voipme SL1 SL2 503 NI ' en.. pH 'CCE Ag CI Volatile •, ''Others otBali Metals, Sane.`. Sol'ida ` 1 t�Grab _Composite 1r/31�L 7'f�/tfl. I f� ✓PlasOe oz t / V , / V Vz ' / — o2 _Grab _Composite _Glass Plastic -dim , — t _ Grab Glass — Oz — Composite _ Plastic —pint — t _Grab — °Z — Composite _Glass Plastic —pint — t SLI: Total Solids (Moisture) Total Kieldahl Nitrogen, Phosphorus and Potassium SL2: Basic Test SL I Plus Suirur, Calcium, Magnesiuln,Sodium, Iron, Aluminum, Manganese, Copper And Zinc 503 Metals: Arsenic, Cadmium, Chromium,Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc Included in SL2) Nitrogen Series: Total Kjeldaht, Ammonium, Nitrstc & Organic Nitrogen. CCE: Calcium Carbonate Equivalent or Total. neutralization Value (For Ume Treated Sludge) Page: 1 of 2 Report Number: 16-336-0205 Account Number: 46245 Send To: EMA Resources Inc 755 Yadkinville Road Mocksville , NC 27028 Lab Number: 61015 Sample Id : Smithfield Tarheel • Waypoint. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Smithfield Tarheel NC Cert#257 REPORT OFANALYSIS Date Sampled: 11/30/2016 08:00:00 Date Received: 12/01/2016 00:00 Date Reported: 12/09/2016 Total Solids 0.44 4400 100.0 JM 12101/201616:00 Moisture' 99.55 100.0 JM 1210112016 16:00 Total Kjeldahl Nitrogen 8.00 80000 10.0 SJB 12/07/2016 09:00. Total Phosphorus 1.93 19300 100 JTR 12/06/2016 13:55 Total Potassium 1.62 16200 10000 JTR 12/07/2016 19:31 Total Sulfur 1.35 13500 100 JTR 12/06/2016 13:55 Total Calcium 0.92 9180 100 JTR 12/06/2016 13:55 Total Magnesium 0.26 2640 100 JTR 12/06/2016 13:55 Total Sodium 10.70 107000 1000 JTR 12/06/2016 14:00 Total Iron 2250 100 JTR 12/06/2016 13:55 Total Aluminum 50700 1000 JTR 12106/201614:00 Total Manganese 149 5.00 JTR 12/06/2016 13:55 Total Copper 183 5.00 JTR 12/06/201613:55 Total Zinc 311 5.00 JTR 12/06/2016 13:55 Ammonia Nitrogen 8.00 80000 10.0 SJB 12/02/2016 09:20 Organic N 0.00 0 10.0 12/02/2016 09:20 Nitrate+Nitrite-N <1.07 1.07 SJB 12/02/201613:46 SM-2540G SM-254OG SM-4500-NH3C-TKN 6010C 6010C 6010C 601OC 6010C 601OC 6010C 601 OC 6010C 6010C 6010C SM-4500-NH3C CALCULATION 450ONO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmi ods and letters are forthe exclusive and confidential use of ourcllents, and mey not be n:produced in whole orpad, normay any reference be made &UMA to the work, the results, orthe company in any advedising, news release, orotherpublic announcements without obtaining our pdor mitten authodmtion. Debbie Holt Laboratory Supervisor 7T_� Pa e: 2 of 2 9 Report Number: 16-336-0205 Account Number: 46245 GWaypoint 7621 ain80 -7 3-94010Fax8 4VA-6446 Main 804.743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: EMA Resources Inc Project : Smithfield Tarheel 755 Yadkinville Road NC Cert#257 Mocksville , NC 27028 REPORT OFANALYSIS Lab Number: 61015 Sample Id : Smithfield Tarheel Total Cadmium <2.00 Total Chromium 12.6 Total Nickel 7.35 Total Lead <5.00 Total Arsenic <3.00 Total Mercury <0.400 Total Selenium <5.00 pH (Standard Units) ` ' 8.19 Total Volatile Solids 45.00 450000 Total Molybdenum 9.85 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. Date Sampled: 11/30/2016 08:00:00 Date Received: 12/01/2016 00:00 Date Reported: 12/09/2016 2.00 JTR 12/06/201613:55 6010C 5.00 JTR 1210612016 13:55 6010C 5.00 JTR 12/06/201613:55 6010C 5.00 JTR 12/06/201613:55 6010C 3.00 JTR 12/06/201613:55 6010C 0.400 JM 12/05/201611:00 SW-7471B 5.00 JTR 12/06/201613:55 6010C 1.00 SJB 12/02/2016 09:20 SW-9045D 100.0 JM 12/01/201616:00 SM-2540G 5.00 JTR 12106/201613:55 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourmports and letters are forthe exclusive and confidential use of ourcllents, and may not be reproduced in whole orpart, normay any reference be made to the work, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourpnorwdtten authorization. Debbie Holt Laboratory Supervisor trm—r BIOSOLIDS SAMPLE TR.4NSIVI�^"I�pp'-pp''I-I�ppl�nn�-�pp"IIII•�""ppI�'I""''II""T A&L E3 IWIIIIIIIIIuINl�llllllul'III��III11lIII�II�Illlllllllll 2zo,s con45 7621 Whitepine Road Rtebmond VA 23237 'f EMAResauices lnc _ ,32233 17— .., ,...,,.......is. SmilhrieW Tarheel IAccount# Submitted By __,.y To ENIA Resources Inc EMA Resources Inc 755 Yadkinville Rd 755 Yadkinville Rd Mocksville_ NC 27028 Mocksville, NC 27028 Sam le Information ; Lab Number Collectionlnfoanatlan containerlriforma6on :• Please. CheckDesiredTeats Sampla'ID ' (Lab Use n Only)"T .. YPe' r• Date ' - Tma Number r Typo ' �. Volume{ ; SW SI2 " 603TK :, Utals. N,uragen4 PH CCE' `.A9 a Volatile Solids '. Otheta ofBotfles 4, ..$ .�.. r,.... . ;', Series, : , AWAM Il�ol1(0 $_o0A}4 1 �o �t ��� —Composite. / _Glass,'--✓q°=t _Grab — Composite — plastic _mint t _Grab _ Glass — oZ blot —Composite _ply at I _Grab _Glass —aZ Tr —Compositetit Plastic ---P,pt Total Solids (Moisture) Total Kleldgltl Nitrogen, Phosphorus and Potassium Basic Test SLI Plus Sulfur, Calcium, tylagoesium,5odium, Iron, Aluminum, Manganese, Capper And Zinc latals: Arsen'i. ,.Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper &Zinc Included In Sl2) gcn Series: Total NcIdahl, Ammonium, Nitrate.@ Organic Nitrogen. Caldum Carbonate EquWalentorTotallneutralimtlon Value (For Lime Treated Sludge) )ESC ANALYTIICAL REPORTAprmyESC EMA Resources Sample Delivery Group: Samples Received: Project Number: Description: L827065 04/01/2016 Smithfield Tar Heel Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By: &UV Terrie Fudge Technical Service Representative ' Restii6 relate only to the Items tested or calibrated and are reported as rounded values This test report shall not be c reproduced, except in full, without written approval of the laboratory. Where applicable, sampling mnduded by ESC is performed per guidance provided in laboratory standard operating procedures: 060302. 060303, and 060304. .t .. w TABLE OF CONTENTS ONE LAB. NATIONWIDE. q I 'Cp: Cover Page 2Tc: Table of Contents 'Ss: Sample Summary 4Cn: Case Narrative 5Sr: Sample Results SMITHFIELD TAR HEEL L827065-01 60c: Quality Control Summary Wet Chemistry by Method 9012 B Wet Chemistry by Method 9b34-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010C Volatile Organic Compounds (GC/MS) by Method 8260B Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081 Semi Volatile Organic Compounds (GC/MS) by Method 8270D 7GI: Glossary of Terms 6AI: Accreditations & Locations 'Sc: Chain of Custody 1 �Cp 2 3 q 3 Ss 5 5 4Cn 7 5Sr 7 8 6QC 9 10 [GI 11 6AI 12 13 9SC 15 16 17 19 20 21 ACCOUNT: PROJECT: SDG: DATHrIME PAGE.. EMA Resources L827065 04A1/1617:29 2 0f 21 SAMPLE"SUMMARY' °; c Collected by Collected dateltime 5MITHFIELD TAR HEEL L827065-01 Waste Roy Whitaker 03/31/1613:30 Method Batch Dilution Preparation dateldme Analysis dateltlme ;Chlorinated Acid Herbicides (GC) by Method 8151A WG863014 1 04/09/1611:09 04108/16 22:12 "'Mercury by Method 7470A WG863038 1 04I0BA610:24 04/08/1613:32 'lMetals(ICP) by Method 6010C WG862909 1 04/07/1621:12 04/0811600:19 r P� l3esticides(Gq by Method 8091 WG862926 1 04/0911608A7 0411VI614:08 I Preparation by Method 1311 WG862422 1 04/0611617:04 04106/1617:05 Preparation by Method 1311 WG862591 1 04/07A611:12 04/07A611:13 1 Gemi Volatile Organic Compounds (GCfMS) by Method 8270D WG862923 1 041OM613:13 04/11/1606:09 ` Wiatile Organic Compounds(GC/MS) by Method 8260E WG863024 1 04/09/1622:24 0410911622:24 Wet Chemisty by Method 9012 B WG852124 1 04/0411614:38 04105/1615:39 Wet Chemistry by Method 9034-90308 WG862076 1 04/08116 08:52 04/08116 08:53 rt Chemistry by Method 9045D WG861594 1 04/041610:10 04104/1610.11 t Chemistry by Method D93/IOtOA WG861862 1 04/071616:21 04/07/1616:21 r-� l� f 1 t 1 It 1 i I / r'1 I� L 11 i t by P" ACCOUNT: PROJECT: SDG: DATE7TIME: EMA Resources L827065 04/11/1617:29 LAB: NATIONWIDE 4V - Received dateltime 04/0116 09:00 t C P Analyst 2Tc BE1 NJB LTB ADF UN BG JF ACG DR a SF JSS Ed MZ 7GI aAl aSc PAGE: " 3 of 21' iA CASE NARRATIVE ONELAB.NATIONwIDE. J* !' All MDL (LOD) and RDL (LOG) values reported for environmental samples have been corrected for the Cp dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the ZTc sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been Identified by the laboratory, and no Information or data have been knowingly withheld that aSs would 'affect the quality of the data. �I {'^r 5 ( Sr aQC (. 7GI Terrie Fudge A_ Technical Service Representative Project Narrative 9Sc I I 1 I � I I l r F1 All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B. All Reactive Sumde results reported in the attached report were determined as totals using method 9034/903013. Case Narrative: Due to sample matrix, standard ZHE container could not be used. A 500ml amber glassjar was used Instead. Zero headspace cannot be guaranteed due to the sample matrix issues. Sample Handling and Receiving the following samples were prepared and/or analyzed past considered min ESC Sample ID L827065-01 Project Sample ID SMITHFIELD TAR HEEL Method 9045D �I + f ACCOUNT: PROJECT: EMA Resources SDG:- DATErnme. PAGE: L827065 04d1/1617:29 4of21 j )SMITHFIEGQ TAR HEEL SAMPLE RESULTS - 01 " ONE tae,MAnoNwioE;' Collected datelttme: 03/31/16 13:30 ' - LB27065- - .-.. �- Preparation by Method 1311 C J Result Qualifier Prep Batch p Analyte date/tlme 2 ^"TCLP Extraction - 4(62016 5:04:58 PM WG862422 TC ITCLP ZHE ExueStioh : ; _ . ^ - 4(/20161112:16 AM WG862591 'Wet Chemistry by Method 9012 B aSs Result Qualifier RDL Dilution Analysis Batch — 4Cn Analyse mg/kg mg/kg date/time /-)Reactive Cyanide ND 0.250 1 04105/201615:39 WG852124 i 'Wet Chemistry by Method 90349030E 6 Result Qualifier RDL Dilution Analysis Batch QC Analyte mglkg mg/kg date/time 1 I'ReactNeSulfide ND 25.0 1 04/08/201608:53 WG862076 7GI ! !Wet Chemistry by Method 9045D BAI - Result Quardter Dilution Analysis Batch 4 Analyte date/tlme a / CorrosNity Non -Corrosive 1 04104/201610:11 WG861594 $C � v ' Wet Chemistry by Method D93/1010A �r Result Qualifier Dilution Analysis Batch l �Amdyte Deg.F date/time Ignitabilhy, DNI at 17OF 1 041071201616:21 WG861862 Mercury by Method 7470A Result Qualifier RDL Limit Dilution Analysis Batch � Analyte mgA mgA mg4 date lttme IMercury ND 0.0100 0.20 1 04/08/201613:32 WG863038 � Metals (ICP) by Method 6010C 4 % Result Qualifier RDL Limit Dilution Analysis Batch •,_-�Analyte mgA mgA mgA date/time Arsenic ND OA50 5 1 04/08/201600:19 WG862909 {nBarium-. ND - 1.35 100 1 64108/20160099 W6862909 A ;Cadmium ND 0.450 1 1 04108201600:19 WG862909 Chromium - - ND OA50 5 1 04108201500:19 WG862909 Lead ND OA50 5 1 04/08201600:19 WG862909 !Selenium NDOA50 1 1 04/08/201600:19 WG862969 f. Silver ND OA50 5 1 04/08/201600:19 WG862909 Volatile Organic Compounds (GC/MS) by Method 8260E l Result Qualifier RDL Llmh Dilution Analysis Batch Analyte mgA mgA mgA date/time `Benzene ND 0.0500 0.50 1 04/09201622:24 WG863024 tCartiodtetrachlorlde ' ND- 0.0500 0.50 1 041091201622:24 WG863024. Chlorobenzene ND 0.0500 100 1 04/09201622:24 WG863024 Chloroform ND. 0.250 6 1 04/09/201622:24 WGB63024 12Dichloroethane ND 0.0500 0.50 1 04/09/201622:24 WG863024 1,1-DIc'hloroethene _- ;�°" ND� 0.0500 0.70 1 041091201622:24 WG863024�' 2-6utanone(MEK) ND 0.500 200 1 04109201622:24 WG863024 etrachlorodhene •. - ND 0.0500. 0.70 1 04/091201622:24- WG8630A , It Trichloroethene ND 0.0500 0.50 1 04109/201622:24 WG863024 Vinyl chlonde ND 0.0500 0:20 1 04109201622:24 WG863024.• , ACCOUNT: PROJECT: SDG: DATErrIME: PAGE l - _ EMA Resources L827065 001116772of S:ot 21 , �SAMPERESLTS 'ONE AE - „,Collected date/t(me; ;03/31/16 ,13:30. - .. - - - 1-827066- Organic Compounds (GC/MS) by Method 8260E Cp �Volatile !. Result Qualifier RDL Limit Dilution Analysis Batch Analyte - mgll mgA mgf date/time (S) Toluene -a 102 90.0.115 114 0410920162224 WG863024 z-�C I ` /SJ,DibromafluoromeNone 94.8 79.0-121 125 0410920162724 WGS63024 f (S) a,,o,a-TnBuorotoluene 98.4 90.4-116 114 04109201622:24 WG863024 aSS N. (SJ4-Bromolluorobenzene 102 80.1-120 128 04109120162224 WG863024 t _)Chlorinated Acid Herbicides (GC) ✓ by Method 8151A 4Cn Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg4 mg4 mg4 date/time j `2A,5-TP(SlNe4 ND 0.00200 1 1 04/08/201622:12 WG863014 �2,4-DND 0.00200 10 1 04/081201622.12 WG863014 6 nIS) 2,4D/chlompheny/AcetIcAdd 63.2 18.2-146 04108201622.12 WG863014 Qc r d-'Pesticides 1GI (GC) by Method 8081 Result Qualifier RDL Limit Dilution Analysis Batch •Anatyte mgll mgfi mgA date/time aAl Chlordane ND 0.00500 0.03 1 001201614:08 WG862926 Endrin ND 0.00500 0.02. 1 041IV201614:08' WG862926 r jieptachlor ND 0.00500 0,0080 1 04/11201614:08 WG862926 SC 1 04/711201614'08' WG862926 2 :undane ND 0J]) 00 0.40.. Methoxychlor ND 0.00500 10 1 041IV201614:08 WG862926 1Toxaphene- •_ ND 0.0100 0.50. 1 04111201614:08 WG862926 , (SJDeccchlorobiphenyl 84.1 10.0-156 122.60 04117201614.08 WG862926 - ) • (9%Telrochloro-&Wlene 93.0 13.9-137 114.20 041IV201614:08 WG862926 - Semi Volatile Organic Compounds (GC/MS) by Method 8270D t-: Result Qualifier RDL Limit Dilution Analysis Batch Anahyte mg8 mgA mgh date/time 14-Dichlorobenzene ND 0.100 7.50 1 0411/201606:09 WG862923 ntrotoluene ND 0.100 0.13: 1 ,04MO1606:09 WG862923. . Hexachlorobenzene ND 0.100 0.13 1 04/IV201606:09 WG862923 <-Mexachloro-13diu[adlene ND - 0.100 0.50 1 04/11201606:09 WG862923 I Hexachlomethane ND 0.100 3 1 04111201606:09 WG862923 iobediene - ND. 0.500 2 1 041111201606:09 WG862923 .. .Pyridine ND 0.500 5 1 0411V201606:09 WG862923 PM -Methyl Phenol ND 0.100 400 1 04/11/201606:09 WG862923' i2-Methylphenol ND 0.100 200 1 04/111201606:09 WG862923 Pentachlorophenol ND 0.100 100 1 04/111201606:09 .WG862923 /�2.4,5-Trichlorophenol ND 0.100 400 1 04AII201606:09 WG862923 t24;fi-Tdchlorophenof ND 0.100 2 1 O4111/201606:09 W6862923-- ' (S)2-Pouorophenol 44.3 10.0-77.9 87 041IV201606:09 WG862923 (3)Phenold5 32.1 5.00770.1 62 041IV201606:09 WG862923 (sJNivobenzene-d5 81.5 1t8-723 120 041IV20160609 WG862923 15J247uoroblphenyt 77.6 29.5-131 722 � 04/111201606:09 WG862923 i (5J2,4,6-Tribromophenol 70.4 11.1-130 148 041IV201606:09 WG862923 ("n (SJp-TeryhenyWl4 -'" 77.1 29.3-137 149 041111201606:09 WG862923 - ACCOUNT: EMA Resources PROJECT: SDG: L827066 DATE/TIME 04/11A617t29.. Gof21 .- v 8oc'124` 7 } 1 ) ( caTl-c Nir �77775 M`f,. -� — ,f�NEf.-• Wet.Chemistry by Method 9012 B. _ _ L827065.01 Method Blank (MB) (Mal R3126450-1 04/05/1615:20 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mglkg mg/kg, Reactive Cyanide U 0.0390 0.250 Original Sample (OS) • Duplicate (DUP) (OS) L827065-01 04/05/1615:39 • (DUP) R3126450-5 04/05/1615:40 Original Result DUPResult Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg % % Reactive Cyanide ND ND 1 0.000 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3126450-2 04/05/1615:21 • (LCSD) R3126450-3 04/05/1615:28 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mglkg mglkg mglkg % % % % % Reactive Cyanide 48.4 49.4 60.2 102 124 50.0450 20.0 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L827065 0411V1617:29 7 of 21 }�8-,.<J7CQI ITl- JN 1'riJL ��rJI:Mr�r�'.Y —� Wet Chemistry by Method 9034.90308 L827065-01 - Method Blank (MB) (MB) WG862076-1 04/08/16 08:53 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Sulfide U 7.63 25.0 Original Sample (OS) • Duplicate (DUP) (OS) L827280-02 04/08/16 08:53 • (DUP) WG862076-4 04/08/16 08:53 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mglkg % % Reactive Sulfide ND ND 1 0.000 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) WG862076-2 04/08MG 08:53 • (LCSD) WG862076-3 04/08/16 08:53 Spike Amount LCS Result LCSD Result LCS Rea LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Reactive Sulfide 100 95.4 91.2 95.4 91.2 70.0-130 4.50 20 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATEMME: 04AIA617:29 PAGE: 8of21 v r J U 1'ay 4 -� 8 1N'L Wet Chemistry by Method 9045D L827065-01 Original Sample (OS) • Duplicate (DUP) C (OS) L827014-01 04/04/1610:11 • (DUP) WG861594-3 04/04/1610:11 P Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits ZTC Analyte % % on-Corrosiv 1 Comosiviry - - --- - - 0.000 10 - eeon-Corrosiv aSS Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 4Cn (LCS) WG861594.1 04/04/1610:11 • (LCSD) WG861594-2 04/04/1610:11 Spike Amount LCS Result LCSD Result LCS Rec LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits s Analyte ... % % % % % Sr ._..._..._ _.. ._,__.____. 634 ,... _..... _. ,. 6.35 _._... ._ .-_-..ry Cor rosivi6.43 _ .-.,.98.6 - ._...98.6__ ._ 02 ... ...._ . ____. ... .. --___0.158.__...,_ _-__. 98.5-110 .__ 7GI aAl 9Sc ACCOUNT: PROJECT: SDG: DATE7TIME: PAGE EMA Resources L827065 04/11/1617:29 9 of 21 8' 52 r (-_ )Q'L-DTI`= JN'- JL�--,vIM.: _ .) .._ Nel �.�n0— 1 Wet Chemistry by McMod D93/1010A L827065-01 Original Sample (OS) • Duplicate (DUP) Cp (OS) L827034-01 04/07/161621 • (DUP) WG861862-3 04/07/1616:21 Original Result DUP Result Dilution Analyte Deg. F Deg. F DUP RPD DUP Qualifier % DUP RPD Limits % TC Ignitability DNI at 170E DNI at 170E 1 0.000 10 Original Sample (OS) • Duplicate (DUP) (OS) L827036-01 04107/1616:21 • (DUP) WG861862-4 04/07/1616:21 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte Deg. F Deg. F % % Ignitability DNI at 170E DNI at 170E 1 0.000 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) WG861862-1 04/07/1616:21 • (LCSD) WG861862-2 04/07/1616:21 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte Deg. F Deg. F .. Deg. F % % % % % Ignitabiliry 82.0 84.10 84.10 163 103 93.0-107 0.000 20 3C$ 4Cn 6Sr] 7GI aAl aSc ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATE/TIME: 04AIA61729 PAGE: 10 of 21 f } '- 7 1 h �. r _1 -_ t ) _J C- _� 0NE'3—,o . .�8'� -3� Qlrr;��Tl` c JN`I R�L �or�lNVHrf brioy..G�. Mercury by Method 7470A L827065-01 Method Blank (MB) (Ma) R3127450.1 04/08/1612:54 Cp MB Result MB Qualifier MB MDL MB ROL Analyte .mg/i _ mgA mgA _ .. .._._,_ MercuryU 0.00333 0.0100 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127450-2 04/08/1612:57 - (LCSD) R3127450-3 04/08/1613:00 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgA mgA mgA % % % % % Mercury 0.0300 0.0325 0.0324 108 108 80-120 0 20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L826964-01 04/08/1613:03 . (MS) R3127450-4 04/08/1613:06 . (MSD) R3127450-6 04/08/1613:21 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits Analyte mgA mg/I mgA mgA % % % Mercury 0.0300 0.000282 0.0321 0.0316 106 104 1 75-126 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L827712-01 04/08/1613:15 - (MS) R3127450-5 04/08/1613:18 - (MSD) R3127450-7 04/08/1613:24 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mgA mgA mgA mgA % % Mercury 0,0300. 0.000310 0.0334 0.0344 110 114 aSS 4Cn _..__ SSr 7GI MS Qualifer MSD Qualifier RPD RPD Limits % % AI 1 20 9Sc Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 75-125 3 20 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATE/TIME: 04p1A617:29 PAGE: 11 of 21 - J--�1/riITY 1 � � _--,)NEL�_-.»fior.-..:_�. 4vv8;L�^'OrJ-' ,)N'r',�.L ;-jvlvlMr,rc-i, Metals (ICP) by Method 6010C L827065-01 Method Blank (MB) r Cp (MB) R3127224-1 04/08/16 00:10 MB Result MB Qualifier MB MDL MB RDL 2TC Analyte mgA mgA mgA Arsenic U 0.15 0.450 - Barium U 0.45 1.35 aSS Cadmium U 0.15 0.450 Chromium U 6.15 0.450 4 Lead U 0.15 0.450 Cn Selenium U 0.15 0.450 Silver U 0.15 0.450 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127224-2 04/08/16 00:13 • (LCSD) R31272243 04/08/16 00:15 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS OuallRer LCSD Qualifier RPD RPD Limits 7GI Analyte mgA mgA mgA % % % % % - ...,_. ._...... ... ... 10.0 _ ... .... `8.62 ._.. _...91 _.... _. 87 .. 20_..... ... _.. _........ _ . ._.. ..... _ .. _,..._ _.. ...20.., . .. -... _ ...,, __.. ......... aAl Sarum 10.0 9Arsenic 68 80420 1 20 Cadmium 10.0 9.01 8.93 90 89 80420 1 20 eSC Chromium 10.0 8.78 8.68 88 87 80-120 1 20 Lead 10.0 9.08 9.02 91 90 80420 1 20 Selenium 10.0 9.07 8.97 91 90 80420 1 20 Silver 10.0 8.64 8.54 86 85 80420 1 20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L827065-01 04/08/16 00:19 • (MS) R3127224-5 04/08/16 00:25 • (MSD) R3127224-6 04/08/16 00:28 Spike Amount Original Result MS Result MSD Result MS Rec. Analyte mg/l mgA mgA mgA % Arsenic 10.0 0.0125 8.87 8.86 89 Barium 10.0 0.0326 8.94 8.90 89 Cadmium 10.0 0.00108 9.08 9.05 91 Chromium 10.0 0.00140 8.62 8.54 86 Lead 10.0 0.00517 9.12 9.09 91 Selenium 10.0 0.0120 9.38 9.41 94 Silver 10.0 ND 8.62 8.56 86 MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 89 1 75-125 0 20 89 1 75-125 0 20 90 1 75-125 0 20 65 1 75425 1 20 91 1 75-125 0 20 94 1 75-125 0 20 86 1 75425 1 20 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATErnME: 04/1111617.29 PAGE 12 of 21 -wt�866u24__, Volatile Organic Compounds (GCIMS) by Method 82608 Method Blank (MB) .-- L827065-07 (MB) R3127778-7 0410911619:45 MB Result MB Qualfer MB MDL MB RDL Analyte mgh mgR mgh Benzene U 0.0167 0.0500 Carbon tetrachloride U 0.0167 0.0500 Chlorobenzene U 0.0167 0.0500 Chloroform U 0.0833 0,250 1.2-Dichloroethene U 0.0167 0.0500 1.1-Dichloroethene U 0.0167 0.0500 2-Butanone (MEK) U 0.167 0.500 Tetrachloroethene U 0.0167 0.0500 Trichloroethene U 0.0167 0.0500 Vinyl chloride U 0.0167 0.0500 IS) Toluene-d8 104 90.0415 (S) Dibromofluoromethone 99.2 79.0-121 (S) u.ixo-Trifluorotoluene 99.1 90.4-116 (S)4-Bromofluorabenzene 101 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127778-1 04/09/1615:20 • (LCSD) R3127778-2 04/09/1615:43 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Benzene 0.0250 0.0241 0.0237 96.5 95.0 73.0-122 1.66 20 Carbon tetrachloride 0.0250 0.0229 0.0229 91.8 91.4 70.9-129 0.390 20 Chlorobenzene 0.0250 0.0264 0.0265 106 106 79.7-122 0.340 20 Chloroform 0.0250 0.0257 0.0249 103 99.5 73.2425 3.11 20 1,2-Dichloroethene 0.0250 0.0274 0.0261 109 104 65.3-126 4.79 20 1,1-Dichloroethene 0.0250 0.0243 0.0241 97.0 96.3 60.6-133 0.720 20 2-Butanone (MEK) 0.125 0.178 0.154 142 123 46.4-155 14.2 20 Tetrachloroethene 0.0250 0.0252 0.0254 101 102 73.5-130 0.860 20 Trichloroethene 0.0250 0.0248 0.0247 99.3 98.9 79.5421 0.420 20 Vinyl chloride 0.0250 0.0216 0.0214 86.4 85.7 61.5-134 0.830 20 (S)Toluene-d8 103 102 90.0-115 (S) Dibromofluoromethone 976 95.2 79.0-121 (3)a,a,a-Trifluorotaluene 98.7 98.4 90.4-116 (S) 4-Bromofluorabenzene 102 102 80.1-120 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L827065 04AI/1617:29 13 of 21 s_.^ - T.-_.�NEv -Ql,r;LrTY-c.JN � RvL w�1M,-,R--� �s_i Volatile Organic Compounds (GC/MS) by Method 8260E L827065.01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) Cp (OS) L827923-02 04/09/16 20:07 - (MS) R3127778-3 04/09/1617:51 • (MSD) R3127778-4 04/09/1618:14 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits zTC Analyte .._nzene _..__ .... mgA mgA mg/I mgn % % % % % .. .. .. _.�.___ Be _.. .. ND 1.17 _.._ ......__ 0.9221.25 _ _93.9 .. _..73.7 ..... _ 1 1 58.6-133 J3 24.1 20 Carbon tetrachloride 1.25 ND 1.12 0.905 89.8 72.4 1 60.6.139 J3 21.4 20 aSS Chlorobenzene 1.25 ND 1.34 1.12 107 89.7 1 70.1-130 17.6 20 Chloroform 1.25 0.00427 1.24 1.09 98.9 87.1 1 66.1-133 12.7 20 4 1,2-Dichloroethane 1.25 ND 1.31 1.07 105 85.5 1 60.7-132 J3 20.3 20 Cn 1,1-Dichloroethene 1.25 ND 1.19 0.816 95.1 65.2 1 48.8-144 J3 37.3 20 2-Butanone(MEK) 6.25 ND 7.71 6.61 123 106 1 45.0-156 15.3 20.8 Fri 1.25 ND 1.27 0.950 102 76.0 1 57.4-141 J3 29.1 20 Trichloroethene 1.25 ND 1.22 0.966 98.0 77.3 1 48.9-148 J3 23.6 20 Vinyl chloride 1.25 ND 1.06 0.608 84.7 48.6 1 44.3-143 J3 54.1 20 (S) Toluene-d8 103 102 90.0-115 (S) Dibromofluoromethane 95.7 95.5 79.0-lb 7GI (S)a,a,o-Trlfluorotoluene 99.8 100 90.4-116 (S)4-Bromofluorobenzene 104 103 80.1-120 aAl Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) aSc (OS) L827031.01 04/09/16 20:30 • (MS) R3127778-5 04/09/1618:37 • (MSD) R3127778-6 04/09/1618:59 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Llmlts Analyte mg/I mgA mgll mgA % % % % % Benzene 125 0.118 1.02 1.06 72.0 75.2 1 58.6.133 3.76 20 Carbon tetrachloride 1.25 ND 0.887 0.916 71.0 73.3 1 60.6-139 3.20 20 Chlorobenzene 1.25 ND 1.09 1.13 86.9 90.4 1 70.1-130 3.99 20 Chloroform 1.25 ND 1.06 1.11 84.4 88.8 1 66.1-133 4.99 20 1,2-Dichloroethane 1.25 ND 1.08 1.08 86.2 86.2 1 60.7-132 0.0400 20 1,1-Dichloroethene 1.25 ND 0.812 0.842 65.0 67.4 1. 48.8-144 3.69 20 2-Butanone (MEK) 6.25 ND 4.88 4.95 78.0 79.3 1 45.0.156 1.59 20.8 Tetrachloroethene 1.25 ND 0.909 0.959 72.7 76.7 1 57.4-141 5.35 20 Trichloroethene 1.25 ND 0.903 0.937 72.2 75.0 1 48.9-148 3.71 20 Vinyl chloride 1.25 ND 0.599 0.632 47.9 50.5 1 44.3-143 5.36 20 (S)Toluene-d8 103 102 90.0-115 (S)Dibromofluoromethane 94.3 94.9 79.0-121 (S)cta,o-Trifluorotoluene 98.3 100 90.4-116 (S)4-BromoBuorobenzene - 101 103 80.1-120 ACCOUNT: PROJECT: SDG: DATEMME: PAGE EMA Resources L827065 04/1111617:29 14 of 21 J 1 lU � l 12 J w1 _ :J wC8Esu 4'-__R -- Chlorinated Acid Herbicides (GC) by Method 8151A L827065-01 Method Blank (MB) Cp (MB) R3127987-1 04/08/16 21:33 MB Result MB Qualifier MB MDL MB ROL Analyte mgA mg8 mg8 2,4D U 0.000667 0.00200 2,4,5-TP (Silvex) U 0.000667 0.00200 (S)2,4-DichlorophenylAcet1cAc/d 72.2 28.2-146 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127987-2 04/08/16 21:46 • (LCSD) R3127987-3 04/08/16 21:59 Spike Amount LCS Result LCSD Result LCS Rec LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg8 mgA mg8 % % % % % 2,4D _ 0.00500 0.00369 0.00356 73.8 71.3 31.1436 3.38 28.6 2,4,5-TP (Silvex) 0.00500 0.00389 0.00454 77.8 90.9 46.3427 15.5 29.5 (S)Z4-DIchlorophenylAcedcAcid 72.9 72.1 28.2-146 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L827065-01 04/08/16 22:12 • (MS) R3127997-4 04/08/16 22:26 • (MSD) R3127987-5 04/08/16 22:39 Spike Amount Original Result MS Result MSD Result MS Rec. Analyte mg/I mg8 mg/l mg8 % 2,4-6 0.0500 ND 0.0349 0.0336 69.8 2,4,5-TP (Silvex) 0.0500 ND 0.0383 0.0374 76.7 (5)2,4-DichlorophenylAcedcAdd 68.6 MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 67.2 1 . 31.1.136 -- - 3.79 74.8 1 46.3-127 2.52 67.3 28.2-146 RPD Limits 28.6 29.5 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATHrIME: 04/11/1617:29 PAGE: 15 of 21 vvu86�y26 ---'---Qurxt=l-FY i Pesticides (GC) by Method 8081 Method Blank (MB) (MB) R3127979-1 04/11A612:15 MB Result MS Qualifier MB MDL MB RDL Analyte mg4 mgh .... mgll..-....... .. Gamma BHC U 0.00167 0.00500 Endrin U 0.00167 0.00500 Heptachlor U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 Chlordane U 0.00167 0.00500 Toxaphene U 0.00333 0.0100 (S) Decochlorobiphenyl 109 10.0.156 (S)Tehachloro-m-xylene 92.1 13.9-137 NI-Ro L827065.01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127979-2 04/itA6ll:38 • (LCSD) R3127979-3 04/11/1611:50 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier Analyte mg/l mg/I mg/I % % % Gamma BHC 0.00100 ND ND 91.7 99.4 54.7-125 Endrin 0.00100 ND ND 101 107 50.1-131 Heptachlor 0.00100 0.000873 0.000817 87.3 81.7 20.7-127 Methoxychlor 0.00100 0.000984 0.00107 98.4 107 48.2-144 (S)Decochloroblphenyl 106 107 10.0.156 (S)Tetrachloro-m-xyfene 89.3 91.6 13.9-137 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L827281-01 04/11/1614:20 • (MS) R3127979-4 04/11/1614:33 • (MSD) R3127979-5 04/11/1614:45 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Analyte mgll mgh mgll mgll % % Gamma BHC 0.0100 ND 0.00673' 0.00980 97.8 98.0 Endrin 0.0100 ND 0.0102 0.0101 102 101 Heptachlor 0.0100 ND 0.00961 0.00714 96.1 71.4 Methoxychlor 0.0100 ND 0.00980 0.00962 98.0 96.2 (S) Decochforobiphenyl 76.9 73.2 (S)Tetrochloro-m-xyfene 90.5 86.8 LCSD Qualifier RPD ... _ " 8.06 5.88 6.61 8.80 Dilution Rec Limits MS Qualifier 1 54.7-125 1 50.1-131 1 20.7-127 1 48.2-144 10.0-156 13.9-137 RPD Limits 21.1 29.1 30.5 27.8 MSD Qualifier RPD RPD Limits 0.760 29.1 29.4 30.5 1.90 27.8 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATEmME: 0411111617:29 PAGE: 16 of 21 _� '__� ,_-� -o. �8f;��,2377 - __ -� __ �__ -- � _ 11 .ter TY . �N� RwL _ r- -�J _� �cna7MFaR-r Semi Volatile Organic Compounds (GC/MS) by Method 8270D L827065-01 Method Blank (MB) (MB) R3127820-3 04/11/16 02:38 MB Result MB Qualifier MBMDL MB RDL Analyte mgfl mg8 mg8 1,4-Dichlorobenzene u 0.0333 0.100 2,4-Dinitrotoluene u 0.0333 0.100 Hexachlorobenzene u 0.0333 0.100 Hexachloro-11,3-butadiene u 0.0333 0.100 Hexachloroethane u 0.0333 0.100 Nitrobenzene u 0.0333 0.100 Pyridine u 0.0333 0.100 2-Methylphenol u 0.0333 0.100 3&4-Methyl Phenol u 0.0333 0.100 Pentachlorophenol u 0.0333 0.100 2,4,5-Trichlorophenol u 0.0333 0.100 2,4,6-Trichlorophenol u 0.0333 0.100 (S) Nflrobenzene-dS 84.7 21.8-123 (S) 2-Fluoroblphenyl 82.9 29.5-131 (S)p-Terphenyl-dN 89.1 29.3-137 (S) PhenoFdS 40.0 5.00-70.1 (S) 2-Fluorophenol 56.7 10.0-77.9 (S)1,4,6-Tribromophenol 88.3 112-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3127820-1 04/11/16 01:27 - (LCSD) R3127820-2 04/11/16 01:51 SpikeAmount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mgll % % % % % 1,4-Dichlorobenzene 0.0500 ND ND 55.6 61.7 21.0-89.4 10.3 32.6 2,4.Dinitrotoluene 0.0500 0.0418 0.0430 83.6 85.9 31.2-105 2.74 22 Hexachlorobenzene 0.0500 0.0408 0.0426 81.6 85.2 38.5-116 4.23 20.1 Hexachloro-1,3-butadiene 0.0500 ND 0.0345 62.1 69.1 16.1.104 10.7 31.2 Hexachloroethane 0.0500 ND ND 56.4 64.1 16.5-89.8 12.7 30.7 Nitrobenzene 0.0500 0.0379 0.0405 75.8 81.0 31.4-106 6.60 25.7 Pyridine 0.0500 ND ND 42.3 45.0 13.5-58.9 6.27 32.5 2-Methylphenol 0.0500 ND 0.0334 63.2 66.8 26.4-86.9 5.51 26.5 3&4-Methyl Phenol 0.0500 ND 0.0345 65.0 68.9 27.9-92.0 5.90 27 Pentachlorophenol 0.0500 ND 0.0355 63.3 71.0 10.0-97.4 11.5 35.1 2,4,5-Tdchlorophenol 0.0500 0.0362 0.0384 72.4 76.8 34.9-112 5.97 23.9 2,4,6-Trichlorophenol 0.0500 0.0352 0.0385 70.4 77.0 29.8-107 9.04 24.1 ACCOUNT: PROJECT: SDG: EMA Resources L827065 DATE/TIME: 00111617:29 PAGE: 17 of 21 8E��23' -7 V fY 'N7 S� M/ �1 __ �1E� : }ION. . .�U ;� i� Semi Volatile Organic Compounds (GC/MS) by Method 8270D L827065.01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) C (LCS) R3127820-1 04/11/16 01:27 • (LCSD) R3127820-2 04/11/16 01:51 p Spike Amount LCS Result LCSD Result LCS Rea LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 2TC Analyte mgA mgA mgA % (SJ Nitrobenzene-tl5 810 _..._._...._%__.. 84.0 _ 1t8-123 ...__......._.._..___%_.........%...__. (S)2-Fluorobiphenyl 77.6 8t4 29.5-131 a$S (S)p-Terphen&14 82.8 87.9 29.3.137 (S)PhenoWS 32.9 34.4 5.00-70.1 4Cn (S)2-Fluorophenol 42.5 44.2 10.0-77.9 (S)2,4,6-Tribromophenol 88.9 100 11.2-130 6Sr Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L826964-01 04/11/16 03:01 • (MS) R3127820-4 04/11/16 03:25 - (MSD) R3127820-5 04/11/16 03:48 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 7GI Analyte mgA mgA mgA mgA _ % % % % % 1,4-Dichlorobenzene 0.500 NO 0.297 0.326 59.3 65.1 1 14.0-104 9.26 36.4 2,4-Dinitrotoluene 0.500 NO 0.407 0.472 81.4 94.5 1 16.2-135 14.9 20.6 oAl Hexachlorobenzene 0.500 NO 0.399 OA56 79.8 91.1 1 31.9-135 13.2 20 Hexachloro-1,3-butediene 0.500 ND 0.332 0.360 66.4 71.9 1 15.7-109 7.96 37.6 a$C Hexachloroethane 0.500 ND 0.304 0.332 60.9 66.4 1 10.4-105 8.68 40 Nitrobenzene 0.500 ND 0.377 0.422 75.5 84.3 1 23.1-121 11.1 29 Pyridine 0.500 NO 0.179 0.200 35.8 39.9 1 10.0-77.8 11.0 38.8 2-Methylphenol 0.500 ND 0.312 0.358 62.4 71.6 1 10.0-133 13.7 .40 3&4-Methyl Phenol 0.500 NO 0.322 0.372 64.4 74.5 1 17.4-100 14.5 27.7 Pentachlorophenol 0.500 NO 0.376 0.463 75.2 92.6 1 10.0-108 20.8 40 2,4,5-Tnchlorophenol 0.500 ND 0.360 0.418 72.0 83.7 1 30.6-120 15.0 33.8 2,4,6-Trichlorophenol 0.500 NO 0.360 0.415 72.0 82.9 1 19.1-114 14.1 29.9 IS) ffitrobenzene 6 79.1 88.6 21.8-123 (S)1-Fluorobiphenyl 76.8 87.1 29.5-131 (SJp-Terpheny1-d14 82.1 94.5 29.3-137 (S) Phenol-d5 30.1 36.1 5.00-70.1 (S)2-Fluorophenol 40.7 47.8 10.0-77.9 (S)1,4,6-Tribromophenol 93.9 105 11.2-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L827065 04110617:29 18 0121 -) GLOSSARY OF TERMS 0NELAB.NAn0NWIDt3 r-, Abbreviations and Definitions p SDG Sample Delivery Group. MDL Method Detection Limit _ , Tc RDL Reported Detection Limit ND,U- Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. the be on a dry 3Ss 7(dry) Results are, reported based on the dry weight of sample, [this will only present 'i report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) Cn ❑ from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard)-Malytes added to everyblank, sample, Laboratory Control s Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring Sr recovery: Surrogates are not expected to be detected in all environmental media: Rec. Recovery. 6Qc n SDL Sample Detection Limit. +. MQL Method Ouantitation Limit. Unadj. MQL Unadjusted Method Ouantitation Limit. n 8AI Qualifier Description J3 The associated batch OC was outside the established quality control range for precision. s Sc - ACCOUNT: `EMA Resources PROJECT: SDG: L827065 DATEMME 04AM6.1749 PAGE 19 of 21 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. >� ESC Lab Sciences is the only environmental laboratory accredited(cemfed to support your work naBanWdefrom one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country Our capacity and capability from our single location laboratory is comparable to the collective totals of the CP network laboratories in our industry. The most significant benefit to our 'one location' design is the design of our laboratory campus. The model E conducive to accelerated productivity, decreasing turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE ' Not all codifications held by the laboratory are applicable W the results reported In the allached report 2 State Accreditations Alabama 40660 _ Nevada TN-03-2002-34 SS] Alaska. _ _ UST-OBO New Hampshire 2975_ Arizona AZO612 New Jersey—NELAP TNO02 _ Arkansas 88-0469 New Mexico _ TN00003 4C� California 01157CA New York 11742 n Colorado TN00003 North Carolina Env375 6 t Conneticut PH_0197 North Carolina DW2i704 Sr Florida E87487 North Carolina ° _ _ 41 _ Georgia NELAP North Dakota R-140 Georgia' 923_ Ohio—VAP CL0069 QC ❑ _ Idaho TN00003 Oklahoma 9915 Illinois 200008 Oregon TN200002 7GI Indiana C-TN-01_ Pennsylvania 68-02979 ❑ Iowa 364 Rhode Island 221 r I Kansas E-10277 South Ciro_Iina 84064 I 1 Kentucky' 90070 South Dakota nla Kentucky' 16 Tennessee" 2006 Louisiana A130792 Texas T104704245-07-TX o Maine_ TN0002 Texas' - LAB0152 $C I Maryland INUtah 6585858 - 157 - Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 109 —% Minnesota 047.999-395 Washington C1915 Mississippi TN00003 West Virginia 233 - Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming AKA 1-7 Nebraska NE-OS45-05 Third Party & Federal Accreditations A2LA—ISO 17025 1461.01 AIHA 100789 A2LA—ISO 17025' 1461.02 DOD 1461.01 Canada 1461.01 USDA S-67674 - EPA—Crypto TN00003 ,-� `Drinking Water 1 Undergmund Storage Tanks 'Aquaticroxichy `chemicaVMiaobwogical 'Mold ^ Accreditation not applicable I I Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please r contact our main off ice. ESC lab Sciences performs all testing at our central laboratory. WA MT NO ME OR MN T tO SD T WI NY T - NE 1A T PA. T T N� T �qN "T t T T U' T OOT KS MS WV VAT n, T KV T •aR I • T� NM Olt All?N T SC T T s It c-A T T (� T TX w T j T T • t- ^ AK T T • r ' ll l; B HI { I - ACCOUNT: PROJECT: SDG: DATHTIME PAGE EMA Resources - L827065 04(111161729 20 of 21 , ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) f-� 1 ' Facility Name: Smithfield Packing Company WWTPName: Tarheel WWTP Monitoring Period: From 4/1/2016 To WQ Permit Number: W00014868 NPDES Number: NCO078344 4/1/2016 Pnthnoen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ Alt_ C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ............ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ 1 Heat Treatment ❑ Thermopbilic ❑ Beta Ray ❑ aRa Gamma [3 Pasteurization ❑ Pas .................. . . Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Nurn er o Excee- en Frequency of Analysis Y Sample Type Analytical Tech-ni ue q inimu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 610 112902 428954 MPN/G 0 Quarterly G SM92210E- 2006 CF 1000 mpn per gram of total solid (dry weight Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) 0 jAlt. 2 (40-day bench) ❑Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ 1 Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ JAR. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A.NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Prepaz r T rQand 'le ( pe or print) —40n rut Si ture 6fPreparer* Date Brent Collins: Director of Technical Services Land Applier Name and Title(ifapplicable)(type or print) 1/30/2017 Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date 1—� DENR FORM PVRF 02T (12/2006) 1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTIO� FORM (02T Rules) Facility Name: Smithfield Packing Company WQ PermitxNumber: W00014868 NVVATP Name: Tarheel WWTP NPDES N amber: NCO078344 I I Monitoring Period: From 4/19/2016 To 4/19/2016 • ,I r-, I I �d i� i- I i ij r1 I � �a I! i i Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tern) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray Pasteurization n ❑ Class B: jAlt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting ❑ Aerobic Digestion ❑ stio Anaerobic D1 e n ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level inSlud a g Pathogen Density Number o Excee- oces Frequency of Analysis Y Sample Type Analytical Tech-ni que inimu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids NON 749 777 803 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Rl Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) [3 Alt. 6 (Allr Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ jAlt. 10 (Incorporation) :❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are (--- i significant penalties for false certification including fine and imprisonment." JeffMusselwhite - Environmental Coordinator Pre r e and)itle (type or rint) kA r--} Sibbire ofPreparer* Date Brent Collins; Director of Technical Services Land Applier Name and Title(ifapplicable)(type or print) 1/30/2017 Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) r-r DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) r-I II i Fr I Facility Name: Smithfield Packing Company WQ Permit Number: W00014868 WWTPName: TarheelWWTP NPDESNumber: NCO078344 Monitoring Period: From 4/19/2016 To 4/19/2016 Pathouen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ I Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray❑ Gamma Ray❑ Pas ❑ Pasteurization .......................... Class B: JAIL (1) Fecal Density Ell Alt (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion El If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level inSlud a g Pathogen Density Numuer or Ex Frequency of Analysis Sample YP Type Analytical Tech-nique inimu Geo. Mean imu Units Fecal Colifortn 2 x 10 to the 6th power per gram of total solids MPN 669 729 855 MPN/G 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) El Alt. 2 (40-day bench) ❑ jAlt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (AIL Stabilization ❑ 1 Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ fl CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Brent Collins; Director of Technical Services Pre are ame an Titl (type or print) Land Applier Name and Title (if applicable)(type or print) ,;9! fZ (�"/ 1/30/2017 Signature ofPreparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) i j DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Smithfield Packing Company WQ Permit Number: W00014868 WWTPName: TarheelWWTP NPDESNumber: NCO078344 F'11 Monitoring Period: From 5/10/2016 To 5/10/2016 4 PnfhnuPn Rednetinn (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: f ,-z �1 Class A: Alt- A (time/temp) ❑ Alt B (Aik Treatment) ❑ Alt. C (Prior Testing) ❑ :: A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying [3Heat Treatment ❑ Thermophilic [3;<;::: Beta Ray ❑ Gomm a RaY [3 eu ' lion ❑ Past nza Class B: lAlt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ gestion i estion [3An aerobe Di If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level inSlud a g Pathogen Density um er o Excee- Frequency of Analysis Y Sample T e Type Analytical Tech-ni ue q inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids 725 1708 6009 MPN/g 0 Quarterly G SM92210E- 2006 rCF 1000 mpn per gram of total solid (dry weight) . I I I ---T I Salmonella bacterial (in lieu of fecal coliform __ 3 MPN per 4 grams total solid (dry weight) I Vector Attraction Reduction (15A NCAC 02T .1107)-Please indicate alternative performed: Alt.l (VS reduction) 21 Alt. 2 (40-day bench) ❑ jAlt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ 1 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) - "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Prep a ame and Title (type or print) W tM Siinaltire of Prepazer* Date Brent Collins; Director of Technical Services Land Applier Name and Title(ifapplicable)(type or print) ZOQ 1/30/2017 Signature of Land Applier (if applicable) *Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) �f ll Ir, ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Smithfield Packing Company WQ Permit Number: WQ0014868 WWTP Name: Tarheel WW'fP NPDES Number: NCO078344 Monitoring Period: From 11/3/2016 To 11/3/2016 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A7 Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ :.::..:•...:.......... A1t.D (No Prior Test) [3 Process to Further Reduce Pathogengs [3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma G ❑ Y Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ c Anaerobe Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Nurn er o EX e- Frequency of Analysis Y Sample Type Analytical Tech-ni ue q inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MFN 2353 2957 3571 MPN/g 0 Quarterly G SM2006 006 - CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) 211 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ 1 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ JAX 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Brent Collins; Director of Technical Services ri Prepare EN and Title (type or print) / Land Applier Name and Title(ifapplicable)(type or print) // / 41el ` 1/30/2017 Z Signature Jf Preparer* ate Signature of Land Applier (if applicable) Date I` • *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Smithfield Packing Company WQ Permit Number: W00014868 WWTPName: TarheelWWTP NPDESNumber: NCO078344 Monitoring Period: From 12/1/2016 To 12/1/2016 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt C (Prior Testing) ❑ A1t.D (No Prior Test) . ❑ Process to Further Reduce Pathogengs ❑ ............. If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ .............. If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAcrobic Digestion ❑ 'e s ❑ Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter TLevel in Sludge Pathogen Density um er oowable ce Frequency Analysis Sample Type Analytical Tech-nique Minim Geo. Mean aximu Unitsdmof Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 1351 1460 1563 MPN/g 0 Quarterly G SM92210E- 2006 CFU 1000 mpn per gram of total solid (dry weight Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) r❑ JAR. 2 (40-day bench) ❑ 1 Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (AIL Stabilization ❑ 1 Alt 7 (Drying -Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ jAlt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 17 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator (i Pre ;;Tre and Title (type or print) n Signature ofPreparer* Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) -dd 1/30/2017 D eateat Signature of Land Applier (if applicable) lY *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date t , DENR FORM PVRF 02T (12/2006) 4 Analytical Results EMA Resources, Inc. 755 Yadkinville Rd. k Mocksville, NC 27028 l � ,tea �N Receive Date: Reported: For: Comments: 160401-03-01 160401-03-01 160401-03-02 160401-03-02 160401-03-03 160401-03703 160401-03-04 160401-03-04 160401-03-05 160401-03.05 160401-03-06 160401-03-06 160401-03-07 160401-03-07 0410112016 04104/2016 Smithfield Tar Heel Parameter Fecal Colifonns Percent Solids Fecal Coliforms Percent Solids Fecal Colifonns Percent Solids Fecal Collforms Percent Solids Fecal Coliforms Percent Solids Fecal Coliforrns Percent Solids Fecal Colifonns Percent Solids Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert#37755, EPA #NC00909 Sample ID Unit Method Analyst 1 417,755 MPWg SM92210E-2006 04/01/2016 WL 1 3.83, % SM254OB-1997 04I01/2016 WL 2 252,809 MPWg SM92210E-2006 04/01/2016 WL 2 3.56 % SM264OB-1997 04/01/2016 WL 3. >444,444 MPWg SM92210E2006 04/01/2016 WL 3 3.60 % SM254OB-1997 0410112016 WL 4 138,504 MPN/g SM92210E-2006 04/0112016 WL 4 3.61 % SM2540B-1997 04/01/2016 WL 5 428,954 MPWg SM92210E-2006 04/01/2016 WL 5 3.73 % SM25408-1997 04101/2016 WL 6 146,628 MPWg SM92210E-2006 04/01/2016 WL 6 3.41 % SM254OB-1997 ' 04/01/2016 WL 7 416,667 MPWg SM92210E-2006 04/01/2016 WL 7 3.84 % SM254OB-1997 04/01/2016 WL PO Box 228 • Statesville, NC 28687.7041872/4697 Page 1 of 3 i, Analytical Results EMA Resources, Inc. . 755 Yadkinville Rd: _ ti Mocksville, NC 27028 ^. Receive Date' 0411,812016 Reported: 04119/2016 For: Smithfield Tar Neel Comments: Sample Number Parameter Semple ID Result Unit Method Analyzed Analyst _ _ .. 160416-0401 Y Y Fecal661korms SF-1 <810 MPWg,'"SM92210E-2D116" 04%1$1201fi WC 160418-0"1 Percent Solids SF-1 3.28 % SM254OB-1997 04/1812016 WL � 4 Respectfully submitted, Dena Myers NCCert#440, ! I NCDW Celt #37755, EPA'#NCOO9O9 � r 1� L j4� h C M rt 'I I a CI PO Box 228 • Statesville, NC 28687 •704/872/469.7 Page 1 of 2 ('1 i 5 i. . AIC P702-Y LaWD 0 Relinqulshed,by: Received by: Relinquished by: Received by: Composite Sampling #1 Time begin— am, pm Date Time end —am, pm Date Composite Sampling #2m Time begin— am, pm Date Time end am, pm Date Lab (704) 872-4697, (11MG DaW) CustodgRecord Time �:R<-ram)pm Date-ZLL/2L Sampled by: Time QP In Date Transported by: . I Time am, pm Date Holding times met: Time am, pm Date Compliance work: Non-compliance work: Analytical Results EMA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Dater 04119/2016 Reported: 04/20/2016 For: Smithfield Tar:Heel North Lagoon Comments: Geometric Mean <777 MPWg Sample Number Parameter Sample ID Result Unit Method 160419.15-01 Fecal Coliforms 1 749 MPWg SM92210E-2606 160419-15-01 Percent Solids 1 2.67 % SM25408-1997 160419-15-02 Fecal Coliforms 2 <803 MPWg SM92210E-2006 160419-15-02 Percent Solids 2 2.49 % SM254OB-1997 160419-15-03 Fecal Coliforms 3 <800 MPWg SM92210E-2006 160419-15-03 Percent Solids 3 2.50 % SM254OB-1997' 160419-15-04 FecalColifonns 4 794 MPWg SM92210E-2006 160419.15-04 Percent Solids 4 2.52 % SM254OB-1997 160419-16-05 FeralColiforrns 5 <760 MPN/g SM92210E-2006 160419-15-05 Percent Solids 5 2.63 % SM254OB-1997 160419-15.06 Fecal Coliforms 6 <760 MPWg SM92210E-2006 160419-15-06' Percent Solids 6 2.63 % SM2540B-1997 160419-15.07 FecalColiforrns 7 <775 MPWg SM92210E-2006 160419-15-07 Percent Solids 7 2.58 % SM2540B-1997 Respectfully submitted, Dena Myers NC Cart#440, NCDW Cert#37755, EPA #NCOOf309 1� 04119/2016 WL 04/19/2016 WL 04/19/2016 WL 04/19/2016 WL 04/19/2016 WL 04/19/2016 WL 04/1912016 WL 04119/2016 WL 04/1912016 WL 04/19/2016 WL 04/1912016 WL 04/19/2016 WL 04/19/2016 WL 04/19/2016 WL PO Box 228 • Statesville, NC 28687.704/87214697 Page 1 of 3 j Client: STATF.9MLEANAMIMICAL P.0110X328 Slaa%Ole.'NC, 207, 'Address:12,MurtStrcet (704) 872-4697 Contact Person: Phone FAX* Wy Chain of Cusodytecord quisitioned by; (Time Date) Customer sample [Do Lab-1UN TlmqSampled (Grab Only) Date Sampled (Grab Only) at &';ii; —W—T —M Paramete re requested [or analysis. 100415-15-01 !:IVPA Vh /ram 02 3:'( 3 ?,-k 411's I sr -ter -3 03 j F� OU Relinquished by: a Dapm te Sampled by., Received by: Time p S am pm Date j _61 _I(0 Transported by. 19d*?;j16L Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date Compliance work: 6o�nooslte Sampling #11; Time begin— am, pm Date Non-compliance work: Time end —am, pm Date Lab comments: Composite Sampling #2: Time,begln— am, pm Qate—J--J—, ,Time end —am, j pm Date --J—J— ' Analytical Results EMA Resources,, Inc. 755 Yadkinvilie Rd. Mocksville, NC 27028 G' Receive Date: 04/19/2016 ■ Reported: 04/20/2016 For: Smithfield Tar Heel South Lagoon Comments: Geometric Mean <729 MPN/g sample Number Parameter Sample ID Result Unit Method Analyzed Analy ,J 1604194-01 -Fecal Coli-fourris f- <676 — MPWg SM922iCE2006 W19/2016 WL 160419-14-01 Percent Solids 1 2.96 % SM2540B-1997 04/19/2016 WL I 160419-14-02 Feral Coliforms 2 851 MPWg SM922.10E-2006 04/19/2016 WL 160419-14-02 Percent Solids 2 2.35 % SM2540BA997 04119/2016 WL 160419-14-03 Fecal Coliforms 3 855 MPWg SM02210E-2006 04/19/2016 WL 160419-14-03 Percent Solids 3 2.34 % SM2540B-1997 04/19/2016 WL 160419-14-04 FecalColifonns 4 692 MPNIg. SM92210E-2006 04/19/2016 WL j 160419.14-04 Percent Solids 4 2.89 % SM2540B4997 04/19/2016 WL 160419-14-05 Fecal Coliforms 5 <694 MPN/g SM92210E-2006 04/19/2016 WL 160419-14-05 Percent Solids 5 2.88 % SM254OB-1997 04/19/2016 WL 160419-14-06 Fecal Coliforms 6 669 MPN/g SM92210E-2006 04/19/2016 WL ` 160419-14-06 Percent Solids 6 2.99 % SM2540B-1997 04/19/2016 WL 160419-14-07 Feral Coliforms 7 <690 MPN/g SM92210E-2006 04/19/2016 WL ' 160419-14-07 Percent Solids 7 190 % SM254OB-1997 04/19/2016 WL Respectfully submitted, a- - Dena Myers NC Cart #440, NCDW: Cert#37755, EPA #NC00909 r PO Box 228 • Statesville, NC 28687 •704/872/4697 1. Page 1 of 3 L i r Client C 2ccC YS'kATBSYtLLE'ANALYI7CAI. ]22Cour[Saeei P.O.Bofi-228 Address: "'' S • 7 ZG Ct- Smoesville;NC,28687% 8724697 oc KS V<'c tC AIC 70 2, ContactPerson: J Phone .�c� .. — -Shy FAX# — ?3G - S/ �y�.2 Chainof Custody Record PO # T sA�URsquisI.tIed S�Z rz6z /l DW7 ! �� by: Ewe): Customer Sample 10# lab-tD# Time Sampled (Grab.Only) Date Sampled (OrabOnly) MaTl Parameters requested(oranatysls w' vm ' N` 612- `f : "v3 -?�CA I� C=5 -1 0 - e-f �=s 7 Relinquished by: Time m, m Date K /L/1� Sampled by o� Time � • �� �rr Date �J_!� i J n 'Received by: m —1.(� Transported Relinquished by: Time am, pm Date Holding times met. i Received by: 'Dime am, pm Date �_J Compliance work: _z Composite Sampling #1: Time begin am, pm Date —J—J— � Non-compliance work: Time end am, pm Date _J—J— I Lab Comments: Composite. Sampling #2: Time begin . am, pm Date /_/ i Time end. -- am; pm .Date _/_/ am, J Analytical Results EMA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Date: 05/10/2016 Reported: 05/11/2016 For: Smithfield Tar Heel South Basin Comments: Geometric Mean 1,708 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 160510-14-01 Fecal Collfonns SF-1 2,448 MPN/g BM92210E-2005 960/2016 WC _ 160510-14-01 Percent Solids SF-1 2.86 % SM254OB-1997 05/10/2016 WC 160510-14-02 FecalColifonns SF-2 6,009 MPN/g SM92210E-2006 05/1012016 WC 160610-14-02 Percent Solids SF-2 2.33 % SM264OB-1997 05/10/2016 WC 160510-14-03 Fecal Colifonns SF-3. <725 MPN/g SM92210E-2005 05/10/2016 WC 160510-14-03 Percent Solids SF-3 2.76 % SM254OB-1997 05/1012016 WC 160510-14-04 Fecal Coilfodns SF-4 <1,111 MPNIg SM92210E-2005 05110/2016 WC 160510-14-04 Percent Solids SF-0 1.80 % SM254013-1997 05/10/2016 WC _ 160510-14-05 FecalColifomts SF-5 1,208 MPN/g SM92210E-2006 05/16/2016 WC 160510A4-05 Percent Solids SF-5 3.31 % SM254OB-1997 05/10/2016 WC 160510-14.06 FecalColifdrms SF-6 2,108 MPN/g SM92210E-2006 05/10/2016 WC 160510.14-06 Percent Solids SF-6 3.32 % SM254OB•1997 05/102016 WC 160510-14-07 FecalColiforrns SF-7 1,404 MPN1g SM92210E-2006 05/102016 WC 160510-14-07 Percent Solids SF-7 2.85 % SM254OB-1997 05/10/2016 WC Respectfully submitted, Dena Myers _ NC Cart #440, NCDW Cart #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 3 Clienk WC. S1'ATESVELLEANALYT16E, 122CourtSupet - 'P.O.Box22V Staumville;NC 28687' (704),872AM Address: 7� W,) X 7-,V 1/7-c C v- A4 VC ks L/zr ( cc- Contact Pars v 'Tn' Ptfone.# 33'e. 7:�-I- 4) Chak of i Custody Record Mro, # Requisitioned by (pipe Date) �Cuatprwr iSarnpfo to# Lab -ID 0 ad Date Sampled. G(mbdn�) Matlix Parameters requested to r analysts atria.. W I S5 Z- 09) 7: ,13 P M 05 7:,5�?vA V/ F -,q 7.-'3 9 P M 5-19A, 7:' J/5- ?M is % ,Relinquished by: Time 2.*j_<ra3pm Sampled by: F.)W11;rz'f Al,-':2 "Received by: q Time qL,�O@Ppm Date—_�—p Transported by. — Relinquished by: Time am, pm Date _J__J_ 1--, Holding times met. 1 ,'-.,Received by: Time am, pm Date _J_J_ Compliance work: ,Ctomposite.Saml;lllng #1 Timebegin am. pm Date No.n-compliance work: Time end am, pm Date Composite Sampling #2: Lab Comments: Tirne begin— am, pm Date _J_`TiJ_ me end —am, pm Date f Results i EMA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Date: 11/03/2016 Reported: 11/04/2016 For: Smithfield Tarheel P I Comments: Geometric Mean <2957 MPN/g r i4 Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst - 161103-18-01 Fecal Coliforms 1-SF <2857 MPWg see=ICE-M 11103/2016 WC 161103-18-01 Percent Solids 1-SF f1.70 % Sin26409-1997 11/03/2016 WC 161103-18-02 Fecal Coliforms 2-SF <3030 MPN/g SM9221cEa006 11/03/2016 WC 161103.18-02 Percent Solids .2-SF 0.66 % sm2mus-Im 11/0312016 WC -1 161103-18-03 Fecal Coliforms 3-SF <3279 MPWg- smm'cE-zm 11/03/2016 WC 161103-18-03 Percent Solids 3-SF 0.61 % SM25409-1sw 1110312016 WC 161103-18-04 Fecal Coliforms 4-SF <2941 MPN1g W92i1cE-2068 11103/2016 WC 161103-18-04 Percent Solids 4-SF 0.68 % SM2S409-1997 11/03/2016 WC 161103-18-05 Fecal Coliforms 5-SF <2353 MPN/g s"m'1cE.2D°6 11/0312016 WC _ 161103-18-05 Percent Solids 5-SF 0.85 % SM2540IM997 11103/2016 WC 161103-18-06 Fecal Coliforms 6SF <3571 MPN/g W92210E-2ws 11103/2016 WC - 161103.18-06 Percent Solids 6-SF 0.56 % SM254sa1997 11/03/2016 WC- - 161103-18-07 Fecal Coliforms 7-SF <2817 MPN/g sm9z21cE4ss 11/03/2016 WC 161103-18-07 Percent Solids 7-SF 0.71 % SMU40&1W 11/03/2016 WC Respectfully submitted, Dena Myers NC Cert#440, NCDW Cert#37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687.704/872/4697 Page 1 of 4 r—� m Ie11L STAIESMIZANALY)ICAL - .5 . ,J 7 "D z;,OJrCC' E 173„StNaviOe.NC um � t0i=.'9 Chain of 6 ✓4 ,.r .CoMedPemn: ,r FAX L- r S voa se R3 Cusdq'Record o. � ImiD� (or-borA .. Pmamorn,ogwmEM�n?M+K F: I I 02 , K ^ l \. N n iN✓ �. ll, Rolirqulshed by: Recelved b)r Relinquished by. Recehred by: CCompoalte Somollrw Time begin limeend .Complift SamlifIng Tlmebegin lame end \� \�,r( �'�J� 81: am, pm Date JJ am,pm Date JJ 1112, am;pm DataJJ— am, pm Date _JJ Time 2 - amo Dale 1%J.3J1-G Sampled by: a Time am, pm Data JJ Ilansported Time am, pm Date —J—J—1 Holding times met: Time. L m Date Comprww work: Noncompilanee work LOComments; Analytical Results EMA Resources, Inc. 755 Yadkinville Rd. _ Mocksville, NC 27028 �i Receive Date: 12/01/2016 1 j Reported: 12/02/2016 � � 1 For: Smithfield Tarheel Comments: i Geometric Mean <1,460 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst e ) 161201-12-01 Fecal Coliforms 1 <1351 MPN/g SM92210E-2005 12/01/2016 WC 161201-12-01 Percent Solids 1 1.48 % SWWB-1997 12/01/2016 WC 161201-12-02 Fecal Coliforms 2 <1361 MPN/g sM9221cE-2006 12/01/2016 WC 161201-12-02 Percent Solids 2 1.47 % SM25406-1997 12/01/2016 WC 161201-12-03 Fecal Coliforms 3 <1504 MPN/g sM9221cE-2005 12/01/2016 WC 161201-12-03 Percent Solids 3 1.33 % SM25466-1997 12101/2016 WC 161201-12-04 Fecal Coliforms 4 <1563 MPN/g SM92210E-2006 12/01/2016 WC 161201-12-04 Percent Solids 4 1.28 % sM2s4n6-1997 12/01/2016 WC 161201-12-05 Fecal Coliforms 5 <1460 MPN/g sM9221cE-2006 12/01/2016 WC _ 161201-12-05 Percent Solids 5 1.37 % SM2546a1997 12/01/2016 WC 161201-12-06 Fecal Coliforms 6 <1460 MPN/g SM92210E-2006 12/01/2016 WC - 161201-12-06 Percent Solids 6 1.37 % SM2540&1997 12/01/2016 WC - 161201-12-07 Fecal Coliforms 7 <1538 MPN/g sM9221cE-2006 12/01/2016 WC i 161201-12-07 Percent Solids 7 1.30 % SM2540e-1997 12/01/2016 WC Respectfully submitted, Dena Myers 0 NC Cert #440, NCDW Cert #37755, EPA#NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Client ✓� a C (S u.Qci�S :z/C.. srnresvur.e ANwxr[cAr. 1x7 C5iamsvilllle1,NC 286887 Address: .J�KL�JGCCC R o� A1OGK5-VCU--` C 2'7 oA 8 (70837U67i Contact Person: ;�-7 y �� &)2 Phone ,g33E-75' 9r/ "?FC-7a7 / FP'X - Chain of Custody Record Po" RZAWLequisitioned by. ome) Customer - Sample IDM �b.1Of eaempled IGmb Only) Date Semplsd tGr - we• Mahe - w ww Peramptem nque wtsr enaly619 9:00 hal k a03 SF- 03 , , u1A1, SF'C. S W ✓ ✓, S F- ; rI AVA+� Relinquished by: Received by: Relinquished by: Received by: Composite Samolina #t: Time begin- am, pm Date Time and am, pm Date _/_/ .Composite Samalina #2: Time,begin am, pm Date _/,_/ Time end - _am, pm- Date -/,_/ Time 9 • em)pm Date./,417/'--1j, Time �.35 �m, pm Data Time am, pm Date .��_ Time am, pm Date _/ ,_ lab Comments: Sampled by: o,' Transported by' Holding times met L/ compliance work: Non-compliance Non-compliance waric l Smithfield Farmland - Tar Heel ANL Volatile Solids In st��` t' DAF �'-z DAFE, �, Digester In i* ��� i�,. erg k'"SSmg/l�#TvSS �}i to ML^' iMontti ar.+M � gll'' , mgll Yoltitlle Solids IV 9' Feb 2016 54,300 50,925 94 Maw20161`i Apr 2016 75.925 74,900 99 Jun 2016 75,200 71,550 95 Aug 2016 68,625 65,200 95 *Ow i6i._.IN 681433M, iiZA A Oct 2016 68,100 64,575 95 Nov 20,1`6� Yid- �6fl��400 ;.' S 5`1S 90 Dee 2016 54,625 51,100 94 Mmimums,anr . k54�300: 50T92'5 Maximum 85,925 80,975 Tptal 78,- 075: Average 68,693 65,090 94 Volatile Solids Out Volatile Solids IN average % Reduction 3/31/16 North 79.49 94 75.26 4/21/16 South 82.33 94 70.26 4/21/16 North 80.92 94 72.93 5/9/16 South 82 94 70.92 11/3/2016 72.97 94 1 82.77 11/30/2016 45 94 94.78 r- -_ j ---) -- ---I . I Page 1 of 1 Report No: 16-137-0644 Account No: 46245 Advisor: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 Waypoint. ANALYTICAL Client: S. Dunham 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanaiytical. com Farm ID: Date Received: 05/16/2016 _ Date of Report: 05/17/2016 Lab No Field ID Sam le to Soil Class HM% WN, pH � AaP-1 K-1 Sf Mn-1-­Zn-l: `Zn-Al �Cri4 . CEC BS/•, Ca/ ,Mg/ ESP: Na, SS f'N y 19900 1 MIN 1.5 5.8 1.5 442 43 31 131 1375 1375 295 8.1 81 65 12 0.6 0.1 12 Comment: Test result units = CEC and Na in meq/100cm3; NQ�N in mg/dm3; WV in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shovm on this report are performed in accordance within NCDA guidelines, Analysis prepared by Waypoint Analytical Virginia, Inc. - - - -� - �- Page 1 of 1 - - Report No 16-358-0666 W Account No: 46245 aypoint.. ANALYTICAL Advisor. EMA Resources Inc Client: Mack King 755 Yadkinville Road SF08 Mocksville INC 27028 - 1 7621 Whitepme Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalVtfcal.com Farm ID: Date Received: 12123/2016 Date of Report: 01/04/2017 Lab No Field ID ` Sample lD' t Soil Class HM% W/V pH Ac �P-I . K--1 S-1 Mn-1 Zn-1 � Zn-AI -Cu-1 '� CEC BS%- Ca%.'. Mg% ESP--, Na SS-f 4N0im ,^ 01961 3 MIN 1.0 5.6 1A 358 34 44 169 895 895 640 6.0 77 54 15 4.3 0.3 12 01962 4 MIN 0.9 5.2 1.0 87 25 25 69 345 345 105 3.0 65 48 11 2.0 0.1 10 Comment: Test result units = CEC and No in meq/100cm3; NC3-N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoinl Analytical Virginia, Inc. 7 Site Smithfield Farmland Corp. - Tar Heel Division - WQ0014868 - Lime Log Lime pH from Soil Applied - Report Ibs/acre Date Applied SF03-01 5.8 2000 2/19/2016 SF03-07 5.6 2000 2/19/2016 SF07-08 5.9 2000 2/20/2016 SF07-09 5.7 2000 2/20/2016 SF07-14 4.6 2000 2/20/2016 SF08-03 5.6 2000 12/29/2016 SF08-04 5.2 20 00 12/29/2016 r- 0-16 —Resources, Inc. Smithfield Packing Co., Inc. Tar Heel Facility 2014 Annual Report Residuals Land Application Permit No. WQ0014868 Prepared By: EMA Resources, Inc. Phone 336*75191441 —Fax 336*751.1442 755 Yadkinville Rd — Mocksville, NC 27028 a M i `Resources, Inc. February 19, 2015 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2014 Annual Report — Smithfield Packing Co. Treatment and Land Application of Residuals Permit No. WQ0014868 Dear Sir or Madam: � 0FIV FES 21 '2015 DWR SECTION INFORMATION PROCESSING UNIT Enclosed are three copies of the 2014 Annual Report for the above referenced land application permit. During 2014 EMA Resources, Inc. land applied 1088.27 dry tons of wastewater residuals to 409.2 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincere y, enit"C/ollinS4;2;� Director of Technical Services brent.collins&emaresourcesinc.com Phone 336.751.1441 — Fax 336.751.1442 755 Yadkinville Road — Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#:. WQ0014868 County: Facility Name (as shown on permit): Land Application Operator: Bladen Year: 2014 Smithfield Packing Company EMA Resources Inc. Phone: 336-751--1441 Land application of residual solids as allowed by the permit occurred during the past calender year? 0 Yes ® No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of.application fields in permit: 1 37 Total number of fields land application occurred during the year: 10 Total amount of dry tons applied during the year for all application sites: 1088.27 Total number of acres land application occurred during the year: 409.2 Part B: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. RJ Yes ® Nc If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. -- 1. Only residuals approved for this permit were applied to the permitted sites. - 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. -- 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief; true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Kyle Narron - General Manager � IAOUI.,—��— Permittee Name and Title (type or print) Sign atUL o Permittee Date Signat re o' Preparer* Date Signiture of Land. Applier Date (if di erent from Pernttee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r). DENR FORM ACF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0014868 Laboratory: 1) A&L Labs Facility Name: Smithfield Packing Company 2) NPDES # or NCO078344 3) WQ#: 4) WWTP Name: Tarheel Plant WWTP 5) Residual Analvsk Data Sample or Composite Date 3/26/14 Port 1&2 3/26/14 Port 3&4 4/24/14 Port 5&6 4/24/14 Port 7&8 March Average 10/13/14 North 10/13/14 South Fall Average Percent Solids 5.19 4.89 3.78 3.14 4.25 5.6 5.59 5.595 Arsenic 3 3 3 3. 3 3 3 3 Cadmium 2 2 2 2 2 2 2 2 Chromium 104 80 100 102 96.5 100 106 103 b Copper 459 477 614 598 537 699 748 723.5 Lead 9 9 14 13 11.25 12 12 12 Mercury 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 fD Molybdenum 17 17 20 22 19 17. 19 18 y Nickel 63 55 65 64 61.75 78 82 80 Selenium 5 5 5 5 5 5 5 5 Zinc 2920 2970 3470 3420 3195 3330 3530 3430 Total Phosphorus 24400 21700 34600 34800 28875 34100 35700 34900 TKN 82500 84000 71200 62400 75025 49300 48100 48700 Ammonia -Nitrogen 8090 -10600 12400 12100 10797.5 8040 7510 7775 Nitrate and Nitrite 9.63 8. 88 63.5 60.5 135.4525 2 2 2 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant enalties for bmitting false information, including the possibility of fines and imprisonment for knowing violations." f Signa4re lok Preparer Date F DENR FORM RSSF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0014868 Laboratory: 1) A&L Labs Facility Name: Smithfield Packing Company 2) NPDES # or 3) WQ#: NC0078344 4) WWTP Name: Tarheel Plant WWTP 5) Residual Analvsis Data Composite Date W. Mt ME 01 My M. F "IMM, 10/13/14 South "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." P� Signafg,reparer Date DENR FORM RSSF-B (5/2003) Field pH Tons per acre applied SF03-07 6.5 0 SF06-06 5 1 SF07-03 5.9 1 SF07-06 5.3 1 SF07-08 5.7 1 SF07-09 5.5 1 SF08-03 5.3 1 SF08-04 5.7 1 SF12-0 1 6.5 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 63.35 Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series: WmB Acres Used: 37.2 Acres Permitted: 37.2 Site #: SF03 Field #: 7 xesicival Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 March Average 2 31 177 8 9 10 11 12 % Solids 4.25 Arsenic 3 Cadmium 2 Copper 96.5 lChromiurr 537 Lead 61.75 Mercury 0.4 IMolyb- denim 19 Nickel 61.75 Selenium 5 Zinc 3195 Total IPhos- horus 28875 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total I DT/Ac./ App. Event 1-1 1.70 2 3 4 5 6 7 8 9 10 11 12 c y Arsenic 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.010 Cadmium 0.007 0.000 0.000 6.000 0.000 0.000 0.060 0.000 0.000 0.000 -0.000 0.000 1 0.007 Copper __ 0.329 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.329 C hromium L829 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 1.829 Lead 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.210 0.001 0.000 6.000 0.000 0.000 0.000 0.000 0.000 0.0000.0000.0000.0000.001 Mol0..065 r 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 0.210 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.210 0.017 .0.000 0.000 0.000 0.000 0.000 0.000 0.000. -0.000 0.000 0.000 0.000 0.017 Zinc .10.882 0.000 0.000 0.060 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 10.882 ITotal Phos- horus 98.348 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 98.348 'I certify, under penalty of law, that this document was prepared under my direction or sunervision in aconrdnnr,- with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/22/2015 Signature of Land Applier Date r11=nIR Gr,,Dhll RAM CC /-101nnncx ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 7 Acres Utilized: 37.2 Land Owner: Steve Dunham Annual Dry Tons Applied: 63.35 Site #: SF03 Acres Permitted: 37.2 Operator: Steve Dunham Predominant Soil Series: WmB Cation Exchange Capacity (non 503): 7.2 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 210 Crop 2 Name: Crop 2 Max. PAN: o ill'. N � 't � o A Volume applied PP (enter one) Solids/ Liquid Cu Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. �D Wet Moist) Precip. past 24 Hrs. inches o c? '2 o' 2" w. o �', ; -- * w ; = # w 0 TKN mg/kg 75025 Z > o � as 0 � :. mg/kg 10797.5 Nitrate and Nitrite mg/kg 35.45 PAN Applied (]bs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/13 273000 4.25 1.301 Tarheel WWTP Dry <.5" S 0.5 0.27 1 47.549 NA Bermuda 4/14 84500 4.25 0.403 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 14.718 NA. Bermuda 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ........ ...... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): .... .......... TOTALS: 01 357500 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 62.2 77 0.000 Lime Applied Annuallbs/acre 0.010 0.0845 0.095 0.007 0.0415 0.048 9 0.329 19.3631 19.692 250 1.829 1.3451 3.174 0.210 0.4098 0.620 1000 0.001 0.0093 0.011 0.065 0.5388 0.604 0.210 2.084 2.294 250 0.017 0.1139 0.131 10.882 84.4715 95.354 500 98.348 :: ::: ::::::::::::::::::::':::::::: ::::: ........................... ::::::::::::::::::::::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2ndCrop .................................... 2 10 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* f Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: 'Permit #: r Operator: -Acres Used:. Smithfield Farmland Corp. Total Dry Tons Applied (Annual): WQ0014868 Cation Exchange Capacity (non 503 only): Vance Tyson Owner: Vance Tyson Predominant Soil Series: 79 Acres Permitted: 79 Site #: SF06 Field #: 162.42 De 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or C'om- iposite Date 1 Fall Average 2 3 4 5 6 7 8 9 10 11 ,12 % Solids 5.6 Arsenic 3 Cadmium 2 Copper 723.5 lChromium 103 Lead 12 Mercury 0.4 I Molyb- denum 18 Nickel 80 Selenium 5 Zinc 3430 Total IPhos- horus 34900 :knnual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 2.06 2 3 4 5 6 7 8 9 10 11 12 H 0 �^ Arsenic ° :'.O:Q12 0:000 }, 0;00 ; , 0;000 0"000; :: 0 000 „,""°.0 000., 0 000 . = ..0 000:..:.0`.,OAO - 0:000 0000", , Cadmium < 0 008 0 000 0 000 -` 0 000 0 000 '. 0000 0 000 : 0 000, O.OQO;„ ;,0 000. 0 000 0000:;. 0:008' Copper ' 2 975. 0 000 0 000 ;- .' ,0 000: 0, 000 0,;000 ; .00.0 . 000 ;; 0 000 , 0000 .' 2.975'- ^hromium 4° Or000 ;0: 000 ,; 0 000= 0 000 OOOOr ::0 000; 0,000 , „ 0`000 _ .'0 000-;; 0 OOp <0`.000. " O':424 Lead " 0' 049, ; 0`000.' '":;0 000 ", 0 000, --,0 000 O:,OOO ;i : }0 000, ;-,, ' O.00p , r 0:000' , , 0 060 . 0 000'. -,.0000 ; ,.0.049 Mercury ; O:,OQ2 0:000 a 0. 000 O OOU; 0.000 , : 0, 0 0 000: 0 000 0:000 ,, 0.000` . 0 000 0 000 : ": 0.002` Molyb- denum 0 074` 0 000 0` 000 0 000' 0 000 0`000 '0 000 0 OQ'0 0 000 0 000 ; 0 00;0 0:0.00_ 0 074 Nickel ;'0329-. ;,0:0.00 :.0 000 ` 0:0.00`;: 'Of1;00 , A;000:`: .;0.000. 0 00,0 Q000 0 000.' 0 000; O':000.; 0.329 Selenium 0 021-. 0 000 Q000 O'000: O OUO 0000 . 0 000 0 000 . 0:0,00, . ,,0 000 0;000, 0°:000 -0.021 Zinc =14 104 0 000. %r 0 000 , 0:0'00 0 000 0.000 °, 0 000= 0 000 0:0.00 O OOQ : 0 000 0"000.'- '14.104; Total P - ho s horus 9 ,0.. 0 0.000 0 00.0 _ _ , 0.000. . 0.000 : - .0 000. ? 0,000 0,:000.-. , ; 0 000 .: M0:000 . 0:000 . ,143;509 -'I certify, under penalty of law, that this document was prepared under my direction or supervision in aceordanre„ with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 6 Acres Utilized: Vance Tyson Annual Dry Tons Applied: 162:42 Site #: SF06 Acres Permitted: Vance Tyson Crop 1 Name: Small Grain Predominant Soil Series: Crop 1 Max. PAN: 100 De Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 79 79 11.5 5 C- Ll Volume applied (enter one) Solids/ Li uid 9 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Co it �D' Wet , Moist) Dry Precip. Past 24 Hrs. inches <.5" ' o w a o N' # o � 0.5 '. g Li N , I* 0.2 TKN mg/kg 48700 Z J o S mg/kg 7775 Nitrate and Nitrite mg/kg 2 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application PP Crop 1 Crop 2 Crop 1 Crop 2 10/22 208000 5.6 0.615 Tarheel WWTP S 14.848 NA I SG 10123 182000 5.6 0.538 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 12.992 NA SG 10/24 195000 5.6 0.576 . Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 11920 NA SG 10/25 110500 5.6 0.327 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 7.888 NA SG 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 695500 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 49.647 0.000 Lime A lied Annuallbs/acre 0.'012 0.008 2.975 0.424 0.040 0.002 0.074 0.329 0.621 14.104 .143.509::::::::::::::::::::::::: ............................ ::::::::::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.0396 0.0224 10.4789 0 0.1529 0.0037 0.2314 1.3362 0.0365 35.6488 2000 Current Cumulative lbs/ac 0.052 0.031 13.454, 0.424 0.202. 0.005 0.305 1.665 0.057 49.753 Permitted C. P. L. R.**** 9 250 1000 250 500 e it Limit lst/2nd Crop P rm PAN P1E .................. ................................100 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 x*x Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 27.65 Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Acres Used: Steve Dunham 12.3 Owner: JW Burney Predominant Soil Series: AaA Acres Permitted: 12.3 Site #: SF07 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Coin- Iposite Date 1 March Average 2 3 4 5 6 7 8 9 10 11 12 % Solids 4.25 Arsenic 3 Cadmium 2 Copper 96.5 [Chromium 537 Lead 61.75 'Mercury 0.4 I Molyb- denum 19 Nickel 61.75 Selenium 5 Zinc 3195 Total IPhos- horus 28875 !annual I Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2.25 2 3 4 1 61 7 8 9 10 11 12 0 Arsenic 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.013 Cadmium 0.009 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.434 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.434 hromi 2.414 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.414 Lead 0.278 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.278 Mercury 0.002 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum denum 0.085 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.085 Nickel 0.278 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.278 Selenium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Zinc 14.365 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.365 Total Phos- horus 129.822 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 129.822 "I certify, under penalty of law, that this document was nrenared under my direction or supervision in acenrrlanep with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violatiioon�s". 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized: JW Bumey Annual Dry Tons Applied: 27.65 Site #: SF07 Acres Permitted: Steve Dunham Predominant Soil Series: AaA Cation Exchange Capacity (non 503): Crop 1 Name: Fescue -Pasture Crop I Max. PAN: 138 Crop 2 Name: Crop 2 Max. PAN: 12.3 12.3 8.6 o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES # W # rt. Animal ' Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. inches a 410 ° o w o o ?: * N' � 70 � w w * Y TKN mg/kg 75025 Z Y 4 El o � °4 ° P. mg/kg 10797.5 Nitrate and Nitrite mg/kg 35.45 PAN Applied (lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 4/12 117000 4.25 1.686 Tarheel WWTP Dry <.5" S 0.5 0.2 61.632 NA Fescue 4/13 39000 4.25 0.562 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 20.544 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000_ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORMTSF supp ( attach FORM FSF supp to this form): TOTAL&I 01 156000 ::::::::;:j::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 82.176 0.0oo ' Lime Applied Annuallbs/acre 0.013 0.061 0.074 0.009 0.0247 0.034 9 0.434 12.9188 13.353 1 250 2.414 0 2.414 0.278 0.2381 0.516 1000 0.002 0.0075 0.009 0.085 0.4302 0.516 0.278 1.4473 1.725 250 0.022 0.1029 0.125 14.365 66.6504 81.015 500 129.822:::::::::::::;:: ::::::::::::::::::::::: :::: ............................ :: - ................... I ................ . Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 18 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 70.27 Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: WmB Acres Used: 19.3 Acres Permitted: 19.3 Site #: SF07 Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): _ sample or Com- posite I Date 1 March Average 2 3 4 5 6 L71 8 9 10 11 12 % Solids 4.25 Arsenic 3 Cadmium 2 Copper 96.5 lChromium 537 Lead 61.75 Mercury 0.4 IMolyb- denum 19 Nickel 61.75 Selenium 5 Zinc 3195 Total Phos- horus 28875 nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DTVA c./ App. Event 1 3.64 2 3 4 5 .6 7 8 9 10 11 12 i y Arsenic 0.022 '0.000 0.000 0.000 0.000 0.000 0.000 1, 0.000' 0.000 0.000 1 0.000 0.000 1 0.022 ,admium 0.015 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.015 Copper 0.703 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.703 lChromium 3.910, 0.000 0.000 0.'000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.910 Lead 0.450 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.456 Mercury 0.003 0'.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.003 Molyb- denumd enum 0.138 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.138 Nickel 0.450 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.450 Selenium 0.036 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Zinc 23.266 0.000 0.000 0.000 0.000 0.000 0.000 `0.000 0.000 0.000 0.000 0.000 1 23.266 Total I Phos- horus 210.268 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 210.268 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". _ 1/22/2015 Signature of Land Applier Date f1FNR F()RAA RAGI CG' do/onnm Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A'"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ001.4868 Field #: 6 Acres Utilized: JW Burney Annual Dry Tons Applied: 70.27 Site #: SF07 Acres Permitted: Steve Dunham Predominant Soil Series: WmB Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 210 Crop 2 Name: Crop 2 Max. PAN: 19.3 19.3 7.8 o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D (n� Wet, Moist Precip. past 24 Hrs. inches a � : °" p �' # .1 w �. P • Z 4 � 5 g 9 * m o p TKN mg/kg 9 75025 Z t - uo° o CD Z �, mg/kg 10797.5 Nitrate and Nitrite m nc g 9 35.45 PAN Applied lbs/acre ( ) Name of CropType - ReceivingResidual Application Crop 1 P Crop 2 P Crop 1 P Crop 2 P 4/6 32500 4.25 0.298 Tarheel WWTP Dry <.5" S 0.5 0.2 10.911 1 NA Bermuda 4/9 1 52000 4.25 0.477 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.51 35.45 17.457 NA Bermuda 4/10 117000 4.25 1.074 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 39.278 NA Bermuda 4111 104000 4.25 0.955 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 34.914 NA Bermuda 4/12 91000 4.25 0.836 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 30.550 NA Bermuda 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .......... TOTALS: 01 396500:::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 133.110 0.000 Lime A lied - Annual lbs/acre 0.022 0.2106 0.232 0.015 0.217 0.232 9 0.703 99.0846 99.787 250 3.910 1.879 5.789 0.450 t1.2912 41 00 0.003 0.0225 0.025 0.138 1.3268 1.465 0.450 14.145 14.595 250 0.036 0.2702 0.307 23.266 329.108::::::::::-:.......................Current 352.374 500 210.268:::::::::::::::::::=:::::::: Date lbs/ac Prior Years Cumulative lbs/ac Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 stl2nd Crop 210 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date p y g *** Mineralization Rates: Compost -0.1, anaerobiall digested -0.2 aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 20.74' WQ0014868 Cation Exchange Capacity (non 503 only): Steve Dunham Owner: JW Burney Predominant Soil Series: AaA 12.1 Acres Permitted: 12.1 Site #: SF07 Field #: 8 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 March Average 2 3 4 5 6] ;_7j 8 9 10 11 12 % Solids 4.25 Arsenic 3' Cadmium 2 Copper 96.5 Chromium 537 Lead 61.75 Mercury 0.4 Molyb- denum 19 Nickel 61.75 Selenium 5 Zinc 3195 Total I Phos- horus 28875 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ITotal DT/Ac./ App. Event 1 1.71 2 3 4 5 6 7 8 9 10 11 12 o 14 Arsenic ' 0.010 0.000 0.000 1 0.000 0.000, 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.010 'Cadmium 0.007 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.331 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.331 -hromium 1.841 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.841 Lead 0.212 0.000 0.000 .0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.212 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.001 Molyb- denum 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.1000 0.000 0.000 0.000 0:000 0.065 Nickel 0.212 0.000 0.000 0.000 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.212 Selenium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.017 Zinc 10.952 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 10.952 I Total Phos- horus 98.984 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 98.984 "I certify, under penalty of law. that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. l am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 8 Acres Utilized: 12.1 Land Owner: JW Burney Annual Dry Tons Applied: 20.74 Site #: SF07 Acres Permitted: 12.1 Operator: Steve Dunham Predominant Soil Series: AaA Cation Exchange Capacity (non 503): 8.6 Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 207 Crop 2 Name: Crop 2 Max. PAN: � +� o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume A lied er PP P Acre (Dry Tons/Ac) Residual Sources (Np Q DES #, W #, Fert., Animal Waste, etc) Soil Cond. wry' Wet, Moist) Precip. Past 24 Hrs. inches y �'� 5 o� c � � 7y P N 0 TKN mg/kg 75025 Z Y o o c mg/kg 10797.5 Nitrate and Nitrite mg/kg 35.45 PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2, Crop 1 Crop 2 4/6 117000 4.25 1.714 Tarheel WWTP Dry <.5" S 0.5 0.2 62.650, NA Bermuda 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 117000 As Cd Cu Cr Pb Hg Mo Ni - Se Zn P 62.650 0.000 Lime Applied Annuallbs/acre 0.010 0.1025 0.113 0.007 0.0356 0.042 9 0.331 17.7708 18.102 250 1.841 1.68 3.521 0.212 0.3784 0.590 1000 0.001 0.0111 0.012 0.065 0.6481 0.713 0.212 2.0252 2.237 250 0.017 0.1424 0.160 10.952 83.6545 94.607 500 98.984:: :::::::::::::::::: :::::::::::::::: ........................... ............................ :::::::::::::::::: .............................. Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd CroP p 2 07 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/13/2014 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): WQ0014868 Cation Exchange Capacity (non 503 only): Richard Dunham Owner: JW Burney Predominant Soil Series: 21.3 Acres Permitted: 21.3 Site #: SF07 Field #: 51.84 WmB 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 March Average 2 3 4 5 6 7 8 9 10 11 12 % Solids 4.25 Arsenic 3 Cadmium 2 Copper 96.5 Chromi 537 Lead 61.75 Mercury 0.4 I Molyb- denum 19 Nickel. 61.75 Selenium 5 Zinc 3195 ` Total 'Phos- horus 28875 knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total I DT/Ac./ App. Event 1 2.43 2 3 4 5 6 7 8 9 10 11 12 c Arsenic ; 0.0,15 ; 0,000,, . `0 000 .. 0 000 0 000:'-: 0 000 . 0.000 :' =`;0;000 '- ` OA00 :.0:000; ` r0:000 ; ,1000'. ,' 0.015. �admium : 0 O1Q, 0 0.00 0 000 . :0 000 0 ,0,00 .0:000 ._ ;0 000 „ , 0 00,0 0 000, 0 000' 0 00:0 .0 000 ' . 0:010 ` Copper 70. OOgO , :OOOO.r;000 ; 0 000 0000:0000 0.0.00 ° °:.0 4.7U..; ^,hromium :2:61,4 0 Q00 ; 0' 000, : ' 0 OOq= 0:0.00 O'000 : ,;. 0 00,0 0 00'0 , , 0;000 0. Lead ; 0, 30,1- „ 0 ;000 0 000 " ;- 0 006' 0:000 ,O U00 -0 000'.` 0000 0 000 O U00 : 0 00.0 ' ; ;0:000:' .;?0.301 Mercury ;= 0 KZ; ='0 U00; ..,O.OQO„ O OOU , 0:000 002' Molyb- denum 0 092 0 0:00 0; 000 0 000; 0 0.00 -'. 0:00,0,- 0 000 0 000 0 000 0 000 .Y 0 000" :, 0.000 0 092; Nickel -,0, :1 `. ;. 0:000 0.000 : "0.301 Selenium ' 0 024~` : 0 000 0,000; 0;000:. .' O'.000 0. 000, :'0;,000 0 000,`." 0 OQO :: ' °0:000`.. 0:024 Zinc 5 553 0.000 `:0 000 ', ` 0 000., O OQO 0"000, :.`0 000 0 000 O:O,O:U,' `:0 000- . ; `O;:OQO :0;000. 15:553 ITotal Phos- horus 4,40:564 0:000 0 000 _ '= 0 00;0 A'000 ..r0:000.' `;: 0 000 :; 0 000 0:000 . '."-6 -0:000'. ` 0:006 1.40.564 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance xvith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information,, including the possibility of fines and imprisonment for knowing violations". 'Z5;�e 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 9 Acres Utilized: 21.3 Land Owner: JW Burney Annual Dry Tons Applied: 51.84 Site #: SF07 Acres Permitted: 21.3 Operator: Richard Dunham Predominant Soil Series: - WMB Cation Exchange Capacity (non 503): 4.7 Crop 1 Name: Corn -Grain Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN: .40 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons "�u Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Anneal Waste, etc) Soil Cond. (Dry, Wet,ao Moist Precip, Past 24 Hrs. inches Y cD 0 o o m o �; N *? w ., N #m o � TKN mg/kg 9 75025 Z o �; a i5 m /k 9 9P 10797.5 Nitrate and Nitrite mg/kg. 35.45 PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application PP Cro 1 Crop 2 P Crop 1 P Crop 2 P 415 175500 4.25 1.460 Tarheel WWTP Dry <.5" S 0.5 0.2 53.385 NA Corn 4/6 117000 4.25 0.973 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 35.590 NA Corm 0.000 0.000 0.000 0.000. 0.000 j 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. , 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 292500 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 88.975 1 0.000 Lime Applied Annuallbs/acre 0.015 0.1241 0.139 0.010 0.0686 0.078 9 0.470 20.3597 20.829 250 2.614 0.5814 3.196 0.301 0.3558 0.656 1000 0.002 0.0121 0.014 0.092 0.7192 0.812 0.301 2.4105 2.711 250 0.024 0.1354 0.160 15.553 101.361 116.915 500 140.564 :::::::::::::::....:.:.::::::: :'::;""'*"*""".:'."" :""":::::::::::::.:.:...:. ........................... :::.55"`::<::::::::::;:`:::::::: Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit P m' AN Limit 1stl2nd Crop P 4 11 "I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Comp y g Compost -0.1 anaerobiall digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Hinton King Owner: Hinton King Predominant Soil Series: Acres Used: 89.5 Acres Permitted: 89.5 Site #: SF08 Field #: 336.97 MaA 3 . Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 Fall Average 2 3 4 5 6 7 8 9 10 11 12 % Solids 5.6 Arsenic 3 Cadmium 2 Copper 723.5 ICmi 103 Lead 12 Mercury 0.4 I Molyb- denum 18 Nickel 80 Selenium 5 Zinc 3430 Total I Phos- horus 34900 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 3.77 2 3 4 5 6 7 8 9 10 11 12 H c ?. Arsenic0000:.,0;,000 0 0,00"` ;.:`0,000 : ; .000.0 ; 0 000 ; . 0:000`:; r 0:023 Cadmium'` 0 015. 0,000`'` °0'000, ; 0 000:;0000,, "..0,000 . 0 000 0:000 -0-015'" Copper 5 44.8 0 000 0 000. , :- ,0 OQO 0 0_U01 O:;ObO 0 000 ° .:' 0:000 0 00Q„ 0 000 - 0 000 0 Q00 'S 44.8; ^hromium > 0 776: 0 000 .:..,0 000., ; 0 000,` , 0 0.00 0:000 :0 000 0;.0,0;0; 0.000 ' ,.0, 000 .' 0,000 77.6"" Lead.0 000000 _ 0:000 ._ 0.090:. Mercury .,; 0 003. :R0, 0 Q 000 0 000._ 0:000, ; 0 000 ,ti0 000 ` 0 0,00 , , ,0.000 :: ,0 000 ,: 0 0.00 0 000 :6.003. Molyb- denum 0 136 0 000 0:000 0 000. 0 000 0 `000 0 0OA O'000 0 000 : 0 OOQ 0.000".:_ 0.136 Nickel ;:0602: 0 0;00,:: 0.000 0 00¢ 0 0U0 0:000 0' 0°OQ 0 000 ' .0"000 ,0,000 , . 0:00,0,0:.602.; Selenium 0 038< 0:000 0:000" 0 000; `O.000 ;0, 000. 0 OU0 ' , 0 00.0 0000 ; _'0, 0,00., 0 000„. ''"000 ` :-OQ3'8' Zinc ;25:828'`:0:000, `: `"0:000 * 0 000t, , 0 0"OOf' ,0000. 0:000 ° 0 00:0 0000 0 000 • 0 000 0:00.0;". "25:828 Total Phos- horus .262797: "0:000.'.r.0:000 : 0 000.; 0 000 0:000 '0 000 \ 0 000 00" 000 _ 0 000 0:000.,: 262:797 ''I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance -vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ie 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #•• W 0014868 Field #• Q 3 Acres Utilized: Land Owner: Hinton King Annual Dry. Tons Applied: 336.97 Site #: SF08 Acres Permitted: Operator: Hinton King Predominant Soil Series: MaA Cation Exchange Capacity (non 503): Crop 1 Name: Rapeseed Crop 1 Max. PAN: 140 Crop 2 Name: CroD 2 Max. PAN: 89.5 89.5 3.2 ° +� ° ° ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Moist) Precip. Past 24 Hrs. inches y b° co Et o o m a * c �y w w ; -- N �, � cc �' * 0 TKN mg/kg 48700 Z q o °° ° ° � �• mg/kg 7775 Nitrate and Nitrite mg/kg 2 PAN Applied lbs/acre ( ) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 9/30 45500 5.6 0.119 Tarheel WWTP Dry <.5" S 0.5 0.2 2.867 NA Rapeseed 10/2 136500 5.6 0.356 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 8.601 NA. Rapeseed 10/3 162500 5.6 0.424 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 10.239 NA Rapeseed 1015 286000 5.6 0.746 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 18.020 NA. Rapeseed 10/6 292500 5.6 0.763 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 18.430 NA Rapeseed 10/7 221000 5.6 0.577 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 13.925 _ NA Rapeseed 10/8 201500 5.6 0.526 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 12.696 NA Rapeseed 10/9 97500 5.6 0.254 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 6.143 NA Rapeseed 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 1443000 ::.?:.':;`: AS Cd Cu Cr Pb I HR Mo Ni. Se Zn I P 90.921 0.000 Lime Applied Annuallbs/acre 0.023 0.026 0.049 1 0.015 0.0077 0.023 9 5.448 5.0294 10.477 1 250 1 0.776 0.5899 1.365 0.090 0.0901 0.180 1000 0-003 0.0032 0.006 1 0.136 0.1873 0.323 0.602 0.5222 1.125 250 1 0.038 0.0462 0.084 25.828 24.3024 50.130 500 262.797 :.:.:::.:.:::.:.:::::.:.::::::::::::::::::::::::::: ...........I ................ Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Per Permit PAN Limit is t/2nd Crop P 140 -i cernty, unaer penalty of iaw, tnat tors document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/fncorporation - 1.0 *** Mineralization Rates: Compost -0.1 anaerobiall digested -0.2 Signature of Land Apptier Date p � y g aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) i' ANNUAL. METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 127.52 WQ0014868 Cation Exchange Capacity (non 503 only): Hinton King Owner: Hinton King Predominant Soil Series: NoA 64.5 Acres Permitted: 64.5 Site #: SF08 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 Fall Average 2 3 4 5 6 7 8 9 10 11 12 % Solids 5.6 Arsenic 3 Cadmium 2 Copper 723.5 Chromi 103 Lead 12 Mercury 0.4 IMolyb- denum 18 Nickel 80 Selenium 5 Zinc 3430 Total Phos- horns 34900 nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 1.98 2 3 4 5 6 7 8 9 10 11 12 c a y Arsenic - 0 012:.. 0:000 0.000 0:00.0: `.>.0:0.00.: ,:0:000. `=>0 000:;`v'0'0.0.0=` , :.0.000 ,.0 000'LL;,. .admium 0:00. 0.000 .:v:0:0.00; 0 000 .0;000 : =0 000;u 0 OO;Q , 0;;000 0 000,: 0,000 0:000 :.0 008:- Copper :' 2 861., 0 00,0.': 0,00 0 000 :0 000 0 OQO ; 0000` . ,t'0 OOQ': 0 00:0 0,000= hromi 0 407 0 Ob0 0' 000 < 0_QOU 0 000 0000 U 000 `: O O,QO 0 :000 ` ; 0 000,'- 0 000' , .0:0:00 ; 0 40.7: Lead 0 047 0.000 0_,t000 ', 0 000: 0.0:00' 0 000... 0:00,00:047` Mercury O'002; 0 000 0; 000 ' Oa000 00,00, ' 0:000000„ 0 Q00 0:000 .; 0:002 Molyb- denum 0 07L 0 000 0 OOU ` 0 000 0 Oq0 0 U00 40 000 : 0 00,0 0 000 0 00071 ; Nickel>>.00QO 0:0,00 ° = 0 000. 0:000 0:000 0 000 0 000 0.0.00 0 000, : O'.000.. Selenium 0 020, ' 0 0"00 0;000 '`'.0:000= , 0 OQO 00.00` ` ; 0 000 :° 0 QQO 0:000 :0 000,' ':0:000'., " 0:000 0 020: Zinc 13 562 U 000 0.000 20;000 13:5.62. ITotal Phos- horus ~l37 995 0 000 0:000 ;' 0 000 0 U00`.` : . ; 0.000 ".0 000 ' 0 O .. = 0.000 0 000 : 0 000 :, 0.000 ,137.995 Al certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Zfz 4; 24- 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 4 Acres Utilized: Land Owner: Hinton King Annual Dry Tons Applied: 127.52 Site #: SF08 Acres Permitted: Operator: Hinton King Predominant Soil Series: NoA Cation Exchange Capacity (non 503): Crop 1 Name: Rapeseed Crop 1 Max. PAN: 140 Crop 2 Name: Crop 2 Max. PAN: 64.5 64.5 2.9 � o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons ova Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) SoilPrecip. Cond. D (Dry, Wet' Moist) Past 24 Hrs. inches y c� :? �' o0 W_ o o %`� w = * w � $ =4 i P. * N # K : TKN mglkg 48700 Z � o as o cl �. mg/kg 7775 Nitrate and Nitrite mg/kg 2 PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/9 227500 5.6 0.824 Tancccl WWTP Dry <.5" S 0.5 0.2 19.890 NA Rapeseed 10/10 195000 5.6 0.766 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 17.049 NA Rapeseed 10/13 97500 5.6 0.353 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 8.524 NA Rapeseed 10/.14 26000 5.6 0.094 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 2.273 NA Rapeseed 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... ........ . TOTAL&I 01 546000 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 47.737 1 0.000 Lime Applied Annuallbs/acre 0.012 0.0207 0.033 1 0.008 0.0071 0.015 9 2.861 4.3587 7.219 250 0.407 0.1424 0.550 0.047 0.0747 0.122 1000 0.602 0.0028 0.004 0.071 0.1758 0.247 0.316 0.415 0.731 250 0.020 0.0389 0.059 13.562 23.3636 36.926 500 137.995 ::::::::::::::::::: ::::::::::::: :: ::::::::: ........................... ............................ :::::::::':::::::::::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 140 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ;e'LsiG;2'L *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* r ! Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 56.45 Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Douglas Musselwhite Owner: Douglas Musselwhite Predominant Soil Series: WaB Acres Used: 25 Acres Permitted: 25 Site #: SF09 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/k2, % Solids use Raw Percent #): Com- Iposite Date % Solids Arsenic March Average 4.25 3 Cadmium Copper [Chromium 2 96.5 537 Lead Mercury IMolyb- denum Nickel Selenium 61.75 0.4 19 61.75 5 Zinc Total i Phos- 3195 28875 nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total App•Event r2.26 5 6 7DT/Ac./ y Arsenic 0.014 0.000 0.000 1 0.000 0.000 0.000 1 '0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.014 'admium 0.009 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper OA36 0.000 0.000 0.000' .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.436 ^1romium 2.425. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.425 Lead 0.279 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.279 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum : 0.086' 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.086 Nickel 0.279 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.000 0.000 0.279 Selenium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Zinc 14.429 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 14.429 ITotal Phos- 130.4001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 130.40( AI certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations``". 2!�r 4�', _ 1/22/2015 Signature of Land Applier Date i DENR FORM MFLSF (12/2006) ` - - L___ ' L - J - -- ` Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 4 Acres Utilized: Douglas Musselwhite Annual Dry Tons Applied: ;`56'.45'.:'; ,:. Site #: SF09 Acres Permitted: Douglas Musselwhite Predominant Soil Series: WaB Cation Exchange Capacity (non 503): Crop 1 Name: Soybeans Crop 1 Max. PAN: 109 Crop 2 Name: Crop 2 Max. PAN: 25 25 4.0 QLiquid V1.olume applied (enter one) Solids/ Cu. Yds Gallons % Solids Volume Applied per pP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc ) Soil Cond. We ' Moist) Precip. Past 24 Hrs. inches y cc o c , * w' 7y w -, # w TKN mg/kg 75025 Z ct o El w. mg/kg 10797.5 Nitrate and Nitrite mg/kg 35.45 PAN Applied (Ibs/acre) Name of Crop Type, Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/4 260000 4.25 2:843,:.'': Tarheel WWTP Dry <.5" S 0.5 0.2 67.384 NA Beans 4/5 58500 4.25 .;^04I5, ;.; Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 15.161 NA Beans 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 MOO 0.000 0.000- 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 1: ,,_, ; `0 318500 ;:;:;>:.:.:: AS Cd Cu Cr Pb H Mo Ni Se Zn P 82.546 0:000 Lime A lied lbs/acre , 0.0154 0` 029 : - . ' 0.0051 0:014 `. 9 .¢: 3.5566 %:3.:992 'i. 1 250 0.394 _:--`2:819 : 1 1 0.0614 0;340'" 1000 0.002 ":0:004':'t 0.1228 . ..... 0:209;F: 1 0.3633 . .... ... i`:'0.642'. 250 , 0.0205 ?`. 0043............. _ 16.8209 1 500 :::::' :00Annual : :::::::::: ::: :::::: ::::::: ........................... ,.......•. .:.:.:.:.:;:.:_:.:.:_: Date 1bs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 10 9 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) 4 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): Operator: Hinton King Owner: Hinton King Predominant Soil Series: Acres Used: 49 Acres Permitted: 49 Site #: SF12 Field #: 171.06 NoA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- Iposite Date 1 March Average 2 Fall Average 3 4 5 6 7 8 9 10 11 12 % Solids 4.25 5.6 Arsenic 3 3 Cadmium 2 2 Copper 96.5 723.5 Chromi 537 103 Lead 61.75 12 Mercury 0.4 0.4 I Molyb- denum 19 18 Nickel 61.75 80 Selenium 5 5 Zinc 3195 3430 Total Phos- horus 28875 34900 nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App• Event 1 1.79 2 1.70 3 4 5 6 7 S 9 10 11 12 14 Arsenic 0.011 0.010 0.000 .0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 admium 0.007 0.007 0.000 0.000 .0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.014 Or Copper 0.345 2.466 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.811 ^,hromi L09 0.351 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 2.270 Lead 0.221 0.041 0.000 0..000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.262 Mercury 0.001 0.001 0:000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.068 0.061 0.000 0.-000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 Nickel 0.221 0.273. 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.493 Selenium 0.018 0.017 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.000 0.035 Zinc 11.419 11.689 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 23.108 I Total Phos- horus 103.199 118.939 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 222.138 •'I certify, under penalty of law, that this document was Arenared.under my direction or supervision in accnrdance -vith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ''?!f.e 4�_ 1/22/2015 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: I Acres Utilized: Land Owner: Hinton King Annual Dry Tons Applied: 171.06 Site #: SF12 Acres Permitted: Operator: Hinton King Predominant Soil Series: NoA Cation Exchange Capacity (non 503): Crop 1 Name: Com-Grain Crop 1 Max. PAN: 131 Crop 2 Name: Wheat Crop 2 Max. PAN: 49 49 4.5 50 y Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (DryQ We Moist) Precip. Past 24 Hrs. inches Y c� o w a o c D r , N' r, * TTCN mg/kg 75025 Z Y o o cc � �. mg/kg 10797.5 Nitrate and Nitrite mg/kg 35.45 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 4/1 13000 4.25 0.047 Tarheel WWTP Dry <.5" S 0.5 0.2 1.719 NA Corn 412 208000 4.25 0.752 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 27.504 NA Corn 4/3 273000 4.25 0.987 Tarheel WWTP Dry <.5" S 0.5 0.2 75025 10797.5 35.45 36.099 NA Corn 10/20 123500 5.6 0.589 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 Na 14.213 Wheat 10/21 234000 5.6 1.115 Tarheel WWTP Dry <.5" S 0.5 0.2 48700 7775 2 Na 26.930 Wheat 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 ......... ...... . Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 01 851500 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 65.321 41.144 Lime Applied Annual lbs/acre 0.021 0.0181 0.039 1 0.014 0.0062 0.020 9 2.811 3.8059 6.616 1 250 1 2.270 0.1278 2.398 1 0.262 0.0652 0.327 1000 1 0.003 0.0025 0.005 0.129 0.1532 0.282 1 0.493 0.3627 0.856 250 0.035 0.0338 0.069 1 1 23.108 20.3725 43.481 500 222.138::::::::::::::::....::::::;:::::; :::::::::::::::::::::::::: ........................... ............................ :::: .................... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop 31 1 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/22/2015 **Volatilization hate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ' ****C.P.L.R,: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Page: 1 of 2 Report Number: 14-086-0202 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 98609 Sample Id: NORTH PORTS 1 & 2 �L A &L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743 9401 Fax (804) 271 6446 www.aleastem.com Project: SMITHFIELD-TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/26/2014 10:00:00 Date Received: 03/27/2014 00:00 Date Reported: 04/03/2014 Total Solids * 5.19 51900 100.0 JM 03/27/2014 14:50 SM-2540G Moisture * 94.81 - 100.0 JM 03/27/2014 14:50 SM-254OG Total Kjeldahl Nitrogen 8.25 82500 10.0 JM 03/28/2014 07:45 SM-4500-NH3C-TKN Total Phosphorus 2.44 24400 100 KM 03/28/2014 11:46 SW 6010C Total Potassium 0.45 4510 100 KM 03/28/2014 11:46 SW 6010C Total Sulfur 1.64 16400 100 KM 03/28/2014 11:46 SW 6010C Total Calcium 3.72 37200 100 KM 03/28/2014 11:46 SW 6010C Total Magnesium 0.19 1910 100 KM 03/28/2014 11:46 SW 6010C Total Sodium 0.88 8770 100 KM 03/28/2014 11:46 SW 6010C Total Iron 14600 100 KM 03/28/2014 11:46 SW 6010C Total Aluminum 7600 100 KM 03/28/2014 11:46 SW 6010C Total Manganese 430 5 KM 03/28/2014 11:46 SW 6010C Total Copper 459 5 KM 03/28/2014 11:46 SW 6010C Total Zinc 2920 5 KM 03/28/2014 11:46 SW 6010C Ammonia Nitrogen 0.81 8090 10.0 JM 03/28/2014 07:45 SM-4500-NH3C Organic N 7.44 74410 10.0 03/28/2014 07:45 CALCULATION Nitrate+Nitrite-N 9.63 2.00 JM 03/28/2014 07:45 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/28/2014 11:46 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt r_ I Page: 2 of 2 Report Number: 14-086-0202 �L A &L Eastern Laboratories, Inc. Account Number: 46245 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-WG Submitted By: ROY WHITAKER winrwaleastem.com Send To: EMA RESOURCES INC Project: SMITHFIELD-TAR HEEL 755 YADKINVILLE RD NC CERT#257 MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Lab Number: 98609 Sample Id: NORTH PORTS 1 & 2 Date Sampled: 3/26/2014 10:00:00 Date Received: 03/27/2014 00:00 Date Reported: 04/03/2014 Total Chromium 104 5 KM 03/28/2014 11:46 SW 6010C Total Nickel 63 5 KM 03/28/2014 11:46 SW 6010C Total Lead 9 5 KM 03/28/2014 11:46 SW 6010C Total Arsenic 3.0 3.0 KM 03/28/2014 11:46 SW 6010C Total Mercury <0.4 0.4 KM 03/31/2014 09:00 SW-7471B Total Selenium <5.0 5.0 KM 03/28/2014 11:46 SW 6010C pH (Standard Units) * 7.65 2.00 JM 03/28/2014 07:45 SW-9045D Total Volatile Solids 76.30 763000 100.0 JM 03/27/2014 14:50 SM-254OG Total Molybdenum 17 5 KM 03/28/2014 11:46 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Cr", AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are 'for the exclusive and confidenfial use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements rdthout obtaining our prior written authorization. Debbie Holt I ;4 BiOSOLIDS SAMPLE TRANSMITTAL FORNWHAIN OF CUSTODY Account A&L Eastern Agricultural Laboratories, laic. 762 INhitepine, Road Richmond VA23231 Tel: 804-743-9401 Fax; 804-271 6446 Email: offs eeO a14abs-easternxom CUstorner Informabon $ubm1tted,B y Charge, Ta 14-086-0202 r 111111 Jill 111111111111111111 4 '245 EMA ResourcQsfilc EMA Resources Tile EMA RESOURCES INC 03�27-2014 - 755 Yadki.nville Rd. 755 Yadkinville Rd SMITHFIELD-TAR HEEL 13:14�38 Morksville., NC 27028 Mock swil-le, NC 27028 Project `Aim Sample Information Lab Number Collection Informatibn Con"a Iner Jnforrvaildh Please Ch6ck Desired Tests Type Date Thle Number �of Type Volume SLi ;SL2 503 metals Nitrogen, Series pH GCE Ag C1 Solids. Volatile, others Sample ID (Lab Use Only) Bottles MAIN Prab C;�Composde Glass —01a stic int ::fqt Glass oz n V o V/ Grab OR-Composil.e 3 —vislastio q t Grab Glass oz Composite 0 —plastic; __pint ____�,tnl Grab Glass Plastic oz int composite ilnqUP [W.Jay:A,'Jignature), Date Tyne Received By: (Signature) Date Tmie Ilk F�( J, q� �s Special lnsfructions or RerTiarks' Test Package 17etalls SL I: Total Solids (Moisture) Tixaf Kjeldahl.Nitrogen2 Phosphorlis and Potassium SI,2-. Basic Test SL I plus Sulfur; Calcium, tvlagnesium,Sadiurn., Iron, Aluminum, Manganese. Copper And -Zinc 603 Metals: Manic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium, (popper &Zinc included in SL2) Nit ragcn,Seirles: Total KJcIdahl. Ammonium. Nitrate & Organic Nitrogen. CCE Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) Page: 1 of 2 Report Number: 14-086-0203 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 98610 Sample Id: NORTH PORTS 3 & 4 AILA&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 co wwwt aleastem.com Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/26/2014 11:00:00 Date Received: 03/27/2014 00:00 Date Reported: 04/03/2014 Total Solids * 4.89 48900 100.0 JM 03/27/2014 14:50 SM-2540G Moisture * 95.11 100.0 JM 03/27/2014 14:50 SM 2540G Total Kjeldahl Nitrogen .8.40 84000 10.0 JM 03/28/2014 07:45 SM-4500-NH3C-TKN Total Phosphorus 2.17 21700 100 KM 03/28/2014 11:46 SW 6010C Total Potassium 0.48 4800 100 KM 03/28/2014 11:46 SW 6010C Total Sulfur 1.73 17300 100 KM 03/28/2014 11:46 SW 6010C Total Calcium 2.83 28306 100 KM 03/28/2014 11:46 SW 6010C Total Magnesium 0.19 1900 100 KM 03/281201411:46 SW 6010C Total Sodium 0.92 9180 100 KM 03/28/2014 11:46 SW 6010C Total Iron 14400 100 KM 03/28/2014 11:46 SW 6010C Total Aluminum 7900 100 KM 03/28/2014 11:46 SW 6010C Total Manganese 398 5 KM 03/28/2014 11:46 SW 6010C Total Copper 477 5 KM 031281201411:46 SW 6010C Total Zinc 2970 5 KM 03/28/2014 11:46 SW 6010C Ammonia Nitrogen 1.06 10600 10.0 JM 03/28/2014 07:45 SM-4500-NI3C Organic N 7.34 73400 10.0 03/28/2014 07:45 CALCULATION Nitrate+Nitrite-N 8.18 2.00 JM 03/28/2014 07:45 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/28/2014 11:46 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential p use of our clients, and may not be reproduced y in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-086-0203 Account Number: 46245 Submitted By: ROY WHITAKER wwwaleastern.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/26/2014 11:00:00 Lab Number: 98610 Date Received: 03/27/2014 00:00 Sample Id : NORTH PORTS 3 & 4 Date Reported: 04/03/2014 Total Chromium 80 5 KM 03/28/2014 11:46 5vv buIUU Total Nickel 55 5 KM 03/28/2014 11:46 SW 6010C Total Lead 9 5 KM 03/28/2014 11:46 SW 6010C Total Arsenic 3.0 3.0 KM 03/28/2014 11:46 SW 6010C Total Mercury <0.4 0.4 KM 03/31/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/28/2014 11:46 SW 6010C pH (Standard Units) * 7.68 2.00 JM 03/28/2014 07:45 SW-9045D Total Volatile Solids 78.98 789800 100.0 JM 03/27/2014 14:50 SM-2540G Total Molybdenum 17 5 KM 03/28/2014 11:46 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Cr", AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt IIIIIMIIIIIII�lllllllllll1161lillllllllll[�IIIIII�Il11�111111114624 -0; 3 PILL ��F:J 1� �Lid V' PLF T 11V rJ L 1 46295A&L ES.steM EMA RESOURCES INC 13:1621 SN11THFIELC TAR HEEL 7621 Whitepine Iioad Ricllrnond VA 23237 TO: 904 Customer InforiTIOL., Submitted By Charge To Copy To EMA Resources Inc ETWA Resottirces Inc 755-'-Adkirlville Rd 755 Yadlanviile Rid Mocksville, NC 2702$ Mocksvil.le, NG 27028 Project ruz7i�fi '� -rAr2 4Egc Lab Number Sample ID (Lab Use Only) ArAM /44-fe¢ fbos 34' Coliection Information Container Information Number 603, .Nitrogenolatile b®r Type Date Tim of Bottles barType Volume SL1 SLZ t+eotals 5orlea pN GCF Ag. ClCI t3allds _, rab _ Glasa "—' oz 8'Gomposfte � f i. �� 10 ! 00 AVA Mastic. t Grab + % Composite 3Ab a 1�G f I � d ' Grab Composite. ..,_., Gtab —Composite Glass antic ---- oz 7 t / t/ _ Glass '—'—' oz _ Plastic — atnt _ Glass oz '—' �Irtf Date Total Solids (Moisture) Total Kieldahl Nitrogen, Phosphorus and Potassium Basic Test SLI plus.sulfirr, Calcium,' Magnesium,3odium,.Iran, Aluminum, Manganese Copper And Zinc Metals: Arsen(e, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium, (Copper & Zinc included In 512) "gee Series: Total Kjeldald, Ammonium, Nitrate & Organic Nitrogen. Calcium Carbonate Equivalent or Total neutralizatidn Value (For Lime Treated Sludge) Account # Dthors Page: 1 of 2 Report Number: 14-115-0209 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 55035 Sample Id: SOUTH LAGOON 5 & 6 wwwaleastern.com A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271.6446 Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Total Solids * 3.78 37800 100.0 JM Moisture * 96.22 100.0 JM Total Kjeldahl Nitrogen 7.12 71200 10.0 JM Total Phosphorus 3.46 34600 100 KM Total Potassium 0.37 3690 100 KM Total Sulfur 1.79 17900 100 KM Total Calcium 3.57 35700 100 KM Total Magnesium 0.26 2550 100 KM Total Sodium 0.88 8760 100 KM Total Iron 20400 100 KM Total Aluminum 24100 100 KM Total Manganese 864 5 KM Total Copper 614 5 KM Total Zinc 3470 5 KM Ammonia Nitrogen 1.24 12400 10.0 JM Organic N 5.88 58800 10.0 Nitrate+Nitrite-N 63.5 2.00 JM Total Cadmium <2.0 2.0 KM Date Sampled: 4/24/2014 07:30:00 Date Received: 04/25/2014 00:00 ,Date Reported: 04/30/2014 04/25/2014 14:30 04/25/2014 14:30 04/28/2014 09:40 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 13:09 04/28/2014 09:40 04/28/2014 09:40 04/28/2014 09:40 04/28/2014 13:09 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization �. Debbie Holt SM-2540G SM-2540G SM-4500-NH3C-TKN SW 601 OC SW 601 OC SW 601 OC SW 601 OC SW 601 OC SW 601 OC SW 6010C SW 601.0C SW 601 OC SW 601 OC SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 601 OC Page: 2 of 2 Report Number: 14-115-0209 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 55035 Sample Id: SOUTH LAGOON 5 & 6 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 �7 vm aleastem.com Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/24/2014 07:30:00 Date Received: 04/25/2014 00:00 Date Reported: 04/30/2014 Total Chromium 100 5 KM 04/28/2014 13:09 SW 601OC Total Nickel 65 5 KM 04/28/2014 13:09 SW 601OC Total Lead 14 5 KM 04/28/2014 13:09 SW 601OC Total Arsenic 3.0 3.0 KM 04/28/2014 13:09 SW 601 OC Total Mercury <0.4 0.4 KM 04/28/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/28/2014 13:09 SW 601OC pH (Standard Units) * 7.96 2.00 JM 04/28/2014 09:40 SW-9045D Total Volatile Solids 66.31 663100 100.0 JM 04/25/2014 14:30 SM-2540G Total Molybdenum 20 5 KM 04/28/2014 13:09 SW 601OC Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work. the results, or the cornpany in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt 10SOLTDIS' SAMPLE TRANS $ Account # At AFL Easl Illlllllllllllllllllllilll1IIIIIIIIIIIIGIflllllllllllllllflllll{l 04-i5�a1ag t� 7621 M11itepinc Road Richmond VA 2"iZ+7 Te EMA RESOURCES INC li:09:00 I SNtiTHFIELD TAR HEEI15&6 — CLIStOMe( Infoi Submitted By Copy 1 a EMA Resources lne EMA I'Lesources. Inc 755 Yadkinville Rd 755 Yadkinville Rd NC 27028 cksville, NC 27028 Iroject -� 'Mocksvilie, Sample Information Lab Number Collection Information. Container Information Please Check Desired Tests Type Date. 7 m� of [tNumber Battles rYlae Volume 5L1 SL2 503 Metals Ntrogen� ( Series pH CCE Ay Cl Volatile Solids Others Sample. ID (Lab Use Only) A91ed oaat V'. � �'rab Glass Mastic D — pint ,f d :h tio" Composite Yt � 7.'30 AK m at 3rab Composite kfby I ' 3� ss �`Plasticint_ D — int ed t Grata _ Glass — oZ — Composite — Plastic ___pint t Grab —Composite Glass — oz Pinf — — Plastic t elinquished a r: (Signature) Date Tcne Received By; (Signature) Date_ The F41, t/t , -6- - Re ;L1: Total Solids (MoiMure) TQW Kieldahl Nitrogen, Phosphorus and Potassium iL2: Basie'rest5LI plus Sulfur, Calcium. tvlagncshtm.Soilinm, Iron, Aluminum, k40112anese, CopperAnd Zinc )03 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nirkel, Selenium. (Copper & Zinc included in SL2) Orrogen Series: ['Dial K,icldahi, A.m.monium, Nilrate & Organic Nitrogen. ,C -Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) Page: 1 of 2 Report Number: 14-115-0210 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 55036 Sample Id : SOUTH LAGOON 7&8 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 wwwaleastem.com Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/24/2014 08:30:00 Date Received: 04/25/2014 00:00 Date Reported: 04/30/2014 Total Solids * 3.14 31400 100.0 JM 04/25/2014 14:30 SM-2540G Moisture * 96.86 100.0 JM 04/25/2014 14:30 SM-2540G Total Kjeldahl Nitrogen 6.24 62400 10.0 JM 04/28/2014 09:40 SM-4500-NH3C-TKN Total Phosphorus 3.48 34800 100 KM 04/28/2014 13:09 SW 6010C Total Potassium 0.34 3390 100 KM 04/28/2014 13:09 SW 6010C Total Sulfur 1.76 17600 100 KM 04/28/2014 13:09 SW 6010C Total Calcium 3.96 39600 100 KM 04/28/2014 13:09 SW 6010C Total Magnesium 0.25 2500 100 KM 04/28/2014 13:09 SW 6010C Total Sodium 0.82 8160 100 KM 04/28/2014 13:09 SW 6010C Total Iron 20500 100 KM 04/28/2014 13:09 SW 6010C Total Aluminum 21700 100 KM 04/28/2014 13:09 SW 6010C Total Manganese 878 5 KM 04/28/2014 13:09 SW 6010C Total Copper 598 5 KM 04/28/2014 13:09 SW 6010C Total Zinc 3420 5 KM 04/28/2014 13:09 SW 6010C Ammonia Nitrogen 1.21 12100 10.0 JM 04/28/2014 09:40 SM-4500-NI3C Organic N 6.03 50300 10.0 04/28/2014 09:40 CALCULATION Nitrate+Nitrite-N 60.5 2.00 JM 04/28/2014 09:40 SM-450ONO3F Total Cadmium <2.0 2.0 KM 04/28/2014 13:09 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made k�L(`�? to the work the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-115-0210 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 AFL Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (B ) 271-6446 www.aleastem.com Project: SMITHFIELD TAR HEEL NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/24/2014 08:30:00 Lab Number: 55036 Date Received: 04/25/2014 00:00 Sample Id: SOUTH LAGOON 7&8 Date Reported: 04/30/2014 Total Chromium 102 5 KM U4/26/2U14 "IS:UU bvv ou-1UL. Total Nickel 64 5 KM 04/28/2014 13:09 SW 6010C Total Lead 13 5 KM 04/28/2014 13:09' SW 6010C Total Arsenic 3.0 3.0 KM 04/28/2014 13:09 SW 6010C Total Mercury <0.4 0.4 KM 04/28/2014 09:00 SW-7471 B Total Selenium 5.0 5.0 KM .04/28/2014 13:09 SW 6010C pH (Standard Units) " 7.98 2.00 JM 04/28/2014 09:40 SW-9045D Total Volatile Solids 66.14 661400 100.0 JM 04/25/2014 14:30 SM-2540G Total Molybdenum 22 5 KM 04/28/2014 13:09 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made io the work, the results. or the company in any advertising, news release, or otherpublic announcements without obtaining our prior written authorization. Debbie Holt .:; BIOSOLIDS SAMPLE TRA SNUTTAL, F ORM/Cl-LMN OF CUSTODY I Account A ,� us ` A&L Eastem Agricultural Laboratories, inc. 7621 Whhepine Road Richmond VA 13237 Tel: 804-743-g4Q1 Fay: 8Q4-271-Gdtid Ernaif: oJtic n -fobs easiern,oam Customer Information Submitted By Charge To I Illllllllllllllllilllil�llllIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII 5 �z4o EMA. Resources Inc a424 ENTA Resources Inc 5-..01 EMA RESOURCES INC 755 Yadkinville Rd SMITHFIELD TAR HEEL,7&8 11:13:33 755 Yadlcinville Rd Mocksville, NC 27029 Mocksville, NC 27025 ))ect Sample Information Lab Number Collection Information Container Information Please Check Desired Tests Type Date Titus Number of Bottles Type Volume SLfi : 8L2 III Metals Nitrogen Series pH CCE Ag CI Volatile Solids Others ample ID (Lab Use only) 9wd rab ✓�y � Glass �� — oz ant / l re�o•J v%Gomposite 7-'-rAK 1.�Ylastic . W'dD�< rob Composite 1 t� ss �" Plastic oz pint �r r (t ' - os' t Grab Gfess, — oz Composite Plastic ____pint t _ Grab _ Glass — oz Composite Plastic ----pint 0 elinqulshed B : (Signature) Date TWO Rocslved By (Signature) Date Turin Test Package Details special instructions at HemarKS l: Total Solids (Moisture) Total Kjeidahl Nitrogen, Phosphorus and Potnssiurn 2: Basic Test SLI plus Suilhri Calcium, Mognesium,Sodium, Iron, Aluminum, htflnganese, Copper And Zinc 3 Metals: Arsenic; Cadmium, Chromium, Mercury, Molytadenum, Lead, Nickel, Selenium. (Copper & Zinc tilcluded In SL2) trogen Scries: Total Kjcidahi. Ammonium. Nitrate & Organic Nitrogen. :E: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) Page: 1 of 2 Report Number: 14-287-0200 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 9son9, A&L Eastern Laboratories, inc. 7621 Whitepine Road Richmond, Vlrgfnla 23237 (804) 743-9401 Fax (804) 271.696 wwwaleastem.com Project: SMITHFIELD TAR HEEUNORTH NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/13/2014 12:30:00 Lab Number: 58090 Date Received: 10/14/2014 00:00 Sample Id: SMITHFIELD TAR HEEL NORTH Date Reported: 10/22/2014 Total Solids * 5.60 bbuuu -i uu.0 111VI , VI I' tGv I- -- Moisture * 94.40 100.0 JM 10/14/2014 09:00 Total Kjeldahl Nitrogen 4.93 49300 1.0.0 JM 10/15/2014 08:39 Total Phosphorus 3.41 34100 100 KM 10/17/2014 14:44 Total Potassium 0.34 3380 100 KM 10/17/2014 14:44 Total Sulfur 1.78 17800 100 KM 10/171201414:44 Total Calcium 4.22 42200 100 KM 10/17/2014 14:44 Total Magnesium 0.29 2920 100 KM 10/17/2014 14:44 Total Sodium 0.98 9840 100 KM 10/17/2014 14:44 Total Iron 18200 100 KM 10/17/2014 14:44 Total Aluminum 21700 100 KM 10/17/2014 14:44 Total Manganese 949 5 KM 10/17/2014 14:44 Total Copper 699 5 KM 10/17/2014 14:44 Total Zinc 3330 5 KM 1-0/17/2014 14:44 Ammonia Nitrogen 0.80 8040 10.0 JM 10/16/2014 08:44 Organic N 4.13 41260 10.0 10/15/2014 08:39 Nitrate+Nitrite-N <2.00 2.00 JM 10/15/2014 08:40 Total Cadmium 2.0 2.0 KM 10/17/2014 14:44 t t d b t risk Detection limit on all N series is on a wet basis. SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6040C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3G CALCULATION SM-450ONO3F SW 6010C All values are on a dry weight basis excep as no e y as e C our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made to the work. the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary -1 1 Page: 2 of 2 Report Number: 14-287-0200 Account Number: 46245 Submitted By: ROY WHITAKER wwaaleastent.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 Project: SMITHFIELD TAR HEEL/NORTH NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/13/201412:30:00 Lab Number: 58090 Date Received: 10/14/2014 00:00 Sample Id: SMITHFIELD TAR HEEL NORTH Date Reported: 10/22/2014 Total Chromium 100 Total Nickel 78 Total Lead 12 Total Arsenic <3.0 Total Mercury <0.4 Total Selenium <5.0 pH (Standard Units) 7.93 Total Volatile Solids 66.05 660500 Total Molybdenum 17 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 5 tcoti iu/, rtzu t4 I4:,+,+ .wv ov rvv 5 KM 10/17/2014 14:44 SW 6010C 5 KM 10/17/2014 14:44 SW 6010C 3.0 KM 10/17/2014 14:44 SW 6010C 0.4 KM 10/15/2014 09:00 SW-7471 B 5.0 KM 10/17/2014 14:44 SW 6010C 2.00 JM 10/15/2014 08:39 SW-9045D 100.0 JM 10/14/2014 09:00 SM-2540G 5 KM 10/17/2014 14:44 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 607 Our reports and letters are for the exclusive and confidential use of our clients, and may not Be reproduced in whole or paR, norm any reference be made to the work. the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary l�Y T i s-�. '� J1.'Y-� r� Y T!'t m � ti� S r ' B10SO IDS S WLE T.�.L- 1,4SM_FT.�, . r a , Account RL L Ea., 1111111111111111111111111111111111111111111111111IIII111 � 45°2�° t 7621 Whitepine Road Riclunond VA 23237 '1 EMA RESOURCES Vb sa ta•zoi 08:25:5,1 < UStOsllc�f Inb SMITHi IELDTAR'HEELtpMORTH SLd3milted By �____ ,_ . _. ra EMA Resources Inc. EMA Reso-urces Inc 755 YadkinviHe Rd 755 Yadkinville Rd Mocksville, NC 27028 Mocksville, NC 27028 Project'2'�L Sample Information Lab Number Collactlori Information Container Information Please Check Desired Tests Sample ib (Lab Use Number 503 Nitrogpn Volatile Only) Type Date Tmw of goitles Type Volume SLi SL2 Metals Series pH CCE Ag Cl Solids Others 1T ✓ Grab Glass — oz rfc� J Composite ID XV / 2; 3o Piet ( L antic --pint �/ ✓ fJott.'H —' qt S'VjG7('k6) �1Grab Glass -- oz � r ?lt2au�r _Composite 1013 !'f �; Ofl A+ L�Ia5tic—�^ptnt i�/ / V Grab _ Glass ---- 0Z !•f Composite — Plastic ----pint t _Grab —Glass --` Qz —Composite _ Plastic plat t _Iln u' a Ignature) Dgto/ TM Received By: (Signature)_ Date Tana P �G7 / 0� I '•frV �t�l y �Y Cj�. 7 1 �& L «. Test Package Details SL I: Total Solids (Moisture) Total Kjoidahl Nitrogen, Phosphorus and Potassium SL2: SasicTest SL I plus Sulfur, Calcium, Ivlagnesiuun,Sodium, iron, Aluminum, lvtangwicse, Copper And 'Zinc 503 Metals; Arsenic, Cadmium, Chromium, Mercury, Malybdertum, Lead, Nickel, Selenium.. (Copper & Zinc Included in SL2) Nitragen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen. CCE:Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) 3ecial Instructions or Re Page: 1 of 2 Report Number: 14-287-0201 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743.9401 Fax (e04) 271.6446 www.aleastem.com Project: SMITHFIELD TAR HEEUSOUTH NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/13/201413:00:00 Lab Number: 58091 Date Received: 10/14/2014 00:00 Sample Id: SMITHFIELD TAR HEEL SOUTH Date Reported: 10/22/2014 Total Solids * 5.69 55900 100.0 JM Moisture * 94.41 100.0 JM Total Kjeldahl Nitrogen 4.81 48100 10.0 JM Total Phosphorus 3.57 35700 100 KM Total Potassium 0.37 3660 100 KM Total Sulfur 1.91 19100 100 KM Total Calcium 4.37 43700 100 KM Total Magnesium 0.29 2940 100 KMI Total Sodium 1.08 10800 100 KM Total Iron 18900 100 KM Total Aluminum 21800 100 KM Total Manganese 920 5 KM Total Copper 748 5 KM Total Zinc 3530 5 KM Ammonia Nitrogen 0.75 7510 10.0 JM Organic N 4.06 40590 10.0 Nitrate+Nitrite-N <2.00 2.00 JM Total Cadmium 2.0 2.0 KM All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 10/14/2014 09:UU 10/14/2014 09:00 10/15/2014 08:39 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/17/2014 14:44 10/16/2014 08:44 10/15/2014 08:39 10/15/2014 08:40 10/17/2014 14:44 Our reports and letters ate for the exclusive and confidential use of our clients, and may not be reproduced in whole, or part, nor may any reference be made fo the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt 5M-2b4UU SM-2540G SM-4500-N H3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NI3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-287-0201 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 58091 Sample Id: SMITHFIELD TAR HEEL SOUTH S�V A &L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwwialeastem.com Project: SMITHFIELD TAR HEEUSOUTH NC CERT#257 REPORT OF ANALYSIS Total Chromium 106 Total Nickel 82 Total Lead 12 Total Arsenic <3.0 Total Mercury <0.4 Total Selenium <5.0 pH (Standard Units) * 7.95 Total Volatile Solids 67.94 679400 Total Molybdenum 19 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. Date Sampled: 10/13/2014 13:00:00 Date Received: 10/14/2014 00:00 Date Reported: 10/22/2014 5 KM 10/17/2014 14:44 SW 6010C 5 KM 10/17/2014 14:44 SW 6010C 5 KM 10/17/2014 14:44 SW 6010C 3.0 KM 10/17/2014 14:44 SW 6010C 0.4 KM 10/15/2014 09:00 SW-74718 5.0 KM 10/17/2014 14:44 SW 6010C 2.00 JM 10/15/2014 08:39 SW-9045D 100.0 JM 10/14/2014 09:00 SM-2540G 5 KM 10/17/2014 14:44 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the excursive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ce the work. the results, or the company in any advertising. news release, orother public announcernents without obtaining our prior written authorization. Debbie Holt .t( a A. ,> - --- 762t White lne Road Richmond I 14 ?s7-o_a t 111111111111II`I Ill�l11111►I11�it�i�,�ji���►��e����l io is 2014 EMA RESOURCES MC 12:53:53 SMITHFIELD TAR HEEUSOUTH r _ -10D /YICCOEi11t S-C,3R[arfl.COJit Submitted By Charge To Copy To EMA Resources Inc El'w'IA Resources Inc 755 'Yadkinville Rd 755 Yadkirnville Rd moobville, INC 27028 Mocksville, NC 27028 Project Sample Information Sample ID Lab Number (Lab Use Only) Collection Information Container information Please Check Dasired Tests Type pate Time Number of Boliies Type Volume SL1 SL2 505 Metals Nitrogen Series pH CCf; Ag Cl Volatile Solids Others OW�✓D i'9R Itea p2.7K Jo goo- iao �JQ u �� Grdb Composite —` _ZGrab Composite Grab ^Composite �fJ�� � ir�jd3� l g. � 8o f� t ; dA f to ( i Glass Mastic Glass Mastic Glass Plastic '^ o7-z �t —�t t ---- oz --pint t �i v V V VX Grab Composite _ _, Glass Pies( ----- °z ---pint Date Tfrr Special instructions or Remarks fin u e nature) D to Time Received icy. Slg attire) L Test Package DetaHs SU, Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus; and Potassium SL2: Basic Test SL i puts Sulfur, Calcium, Magnosium,Sodium, troll Aluminum, Mangunese, Copper And Zinc 503 Metals: Arsahic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc included In SL2) rg1tragen Series; Total Kjoldahl, Ammonium, Nitrate & Organic Nitrogen. CCE; Calcium Carbonate Equivalent or Total neutralization Value (For lime Treated Sludge) OESC 1 Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 Report Summary Friday May 02, 2014 Report Number: L6955O9 Samples Received: 04/25/14 Client Project: ion: SMITHFIELD TAR HEEL 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have an questions regarding this data package, please do not hesitate to caly l. Entire Report Reviewed By: Terrie Fudge/, ESC FVpresentative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each -scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory, standard operating procedures: 060302, 060303, and 060304. Page 1 of 5 OESCl•A•S 5•G•1•E•R1•C•E•S REPORT OF ANALYSIS Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 May 02,2014 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Date Received April 25, 2014 Description SMITHFIELD TAR HEEL Sample ID SMITHFIELD TAR HEEL LAGOON Collected By Roy Whitaker Collection Date 04/24/14 08:30 Parameter Result Det. Limit Units ESC Sample Site ID.: Project Limit Method # : L695509-01 Date/Time By Dil Corrosivity Non-Corrosiv 9045D 04/28/14 1516 MGM 1 Ignitability See Footnote Deg. F D93/101 04/30/14 1615 DR 1 Reactive CN (SW846 7.3.3.2) BDL 0.125 mg/kg 9012B 04/29/14 2006 MCG 1 Reactive Sulf.(SW846 7.3.4.1) BDL 25. mg/kg 9034/90 04/29/14 1614 DR 1 TCLP Extraction - 1.311 04/28/14 09.30 LJN 1 Mercury BDL 0.0010 mg/1 0.20 7470A 04/29/14 1242 BRJ 1 Arsenic BDL 0.45 mg/l 5.0 6010C 04/29/14 1912 ALT 1 Barium BDL 1.4 mg/l 100 6010C 04/29/14 1912 ALT 1 Cadmium BDL 0.45 mg/l 1.0 6010C 04/29/14 1912 ALT 1 Chromium BDL 0.45 mg/l 5.0 6010C 04/29/14 1912 ALT 1 Lead BDL 0.45 mg/1 5.0 6010C 04/29/14 1912 ALT 1 Selenium BDL 0.45 mg/l 1.0 6010C 04/29/14 1912 ALT 1 Silver BDL 0.45 mg/l 5.0 6010C 04/29/14 1912 ALT 1 TCLP ZHE Extraction - 1311 04/28/14 0930 LJN 1 TCLP Volatiles Benzene BDL 0.050 Carbon tetrachloride BDL 0.050 Chlorobenzene BDL 0.050' Chloroform BDL 0.25 1,2-Dichloroethane BDL 0.050 1,1-Dichloroethene BDL 0.050 2-Butanone (MEK) BDL 0.50 Tetrachloroethene BDL 0.050 Trichloroethene BDL 0.050 Vinyl chloride BDL 0.050 Surrogate Recovery Toluene-d8 98.3 Dibromofluorome.thane 92..2 a,a,a-Trifluorotoluene 104. 4-Bromofluorobenzene 98.8 TCLP Pesticides Chlordane BDL 0.0050 Endrin BDL 0.0050 Heptachlor BDL 0.0050 L695509-01 (IGNITABILITY) - Did Not Ignite @ 170 F mg/l 0.50 8260B 04/29/14 1707 JC 1 mg/l 0.50 8260B 04/29/14 1707 JC 1 mg/l 100 8260B 04/29/14 1707 JC 1 mg/1 6.0 8260E 04/29/14 1707 JC 1 mg/1 0.50 8260B 04/29/14 1707 JC 1 mg/1 0.70 8260B 04/29/14 1707 JC 1 mg/l 200 8260B 04/29/14 1707 JC 1 mg/l 0.70 8260B 04/29/14 1707 JC 1 mg/l 0.50 8260B 04/29/14 1707 JC 1 mg/l 0.20 8260B 04/29/14 1707 JC 1 % Rec. 114. 8260E 04/29/14 1707 JC 1 % Rec.. 125. 8.2605 04/29/14 1707 JC .1 % Rec. 114. 8260B 04/29/14 1707 JC 1 % Rec. 128. 8260B 04/29/14 1707 JC 1 mg/l 0.030 8081A 05/02/14 1257 CBB 1 mg/l 0.020 8081A 05/02/14 1257 CBB 1 mg/1 0.0080 8081A 051/02/14 1257 CBB 1 Page 2 of 5 OESC 1 "rCS'UR LAS OFCHOICE REPORT OF ANALYSIS Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 Date Received April 25, 2014 Description SMITHFIELD TAR HEEL Sample ID SMITHFIELD TAR HEEL LAGOON Collected By Roy Whitaker Collection Date 04/24/14 08:30 12065 Lebanon Rd, Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 May 02,2014 ESC Sample # L695509-01 Site ID .: Project : Parameter Result Det. Limit Units Limit Method Date/Time By Dil Lindane BDL 0.0050 mg/l 0.40 8081A 05/02/14 1257 CBB 1 Methoxychlor BDL 0.0050 mg/l 10. 8081A 05/02/14 1257 CBB 1 Toxaphene BDL 0.010 mg/l 0.50 8081A 05/02/14 1257 CBB 1 Surrogate Recovery Decachlorobiphenyl 104. % Rec. 123. 8081A 05/02/14 1257 CBB 1 Tetrachloro-m-xylene 75.5 % Rec. 114. 8081A 05/02/14 1257 CBB 1 TCLP Herbicides 2,4,5-TP (Silvex) 2,4-D Surrogate Recovery 2_,4-Dichlorophenyl Acetic Acid TCLP Semi-Volatiles 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachloroethane Nitrobenzene Pyridine 3&4-Methyl Phenol 2-Methylphenol Pentachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Surrogate Recovery 2-Fluorophenol Phenol-d5 Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol p-Terphenyl-d14 BDL 0.0020 mg/1 1.0 8151A 05/01/14 1758 KLM 1 BDL 0.0020 mg/l 10. 8151A 05/01/14 1758 KLM 1 71.0 % Rec. 8151A 05/01/14 1758 KLM 1 BDL 0.10 mg/l 7.5 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 0.13 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 0.13 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 0.50 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 3.0 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 2.0 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 5.0 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/1 400 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 200 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 100 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/l 400 8270D 04/30/14 0349 KMF 1 BDL 0.10 mg/1 2.0 8270D 04/30/14 0349 KMF 1 49.0 % Rec. 87.0 8270D 04/30/14 0349 KMF 1 33.3 % Rec. 67.0 8270D 04/30/14 0349 KMF 1 56.0 % Rec. 120. 8270D 04/30/14 0349 KMF 1 67.1 % Rec. 122. 8270D 04/30/14 0349 KMF 1 87.3 % Rec. 148. 8270D 04/30/14 0349 KMF 1 73.0 % Rec. 149. 8270D 04/30/14 0349 KMF 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 05/02/14 15:49 Printed: 05/02/14 16:12 L695509-01 (IGNITABILITY) - Did Not Ignite @ 170 F Page 3 of 5 Sample Work Number Group L695509-01 WG718297 I H Attachment A List of Analytes with QC Qualifiers Sample Type Analyte SAMP Silver Run ID Qualifier R2912086 01 Page 4 of 5 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning 01 (ESC) The analyte failed the method required serial dilution test and/or subsequent post -spike criteria. These failures indicate matrix interference. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 5 of 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Smithfield Packing Company Permit Number: WQ0014868 WWTP Name: Tarheel WWWTP NPDES Number: NC007$M44 Monitoring Period: From Port 1&2 - 4/24/14 To Port 1&2 - 4/24/14 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alterative 1 [3 Alternative 2 ® Alterative 3 y ® .... ' ..... . . . ' ' .:.:.:.:.:....:.:.:.:.:.:.:.: Alterative 40 Alterative 5 ® Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost EIT Heat Drying ® Heat Treatment ® Thermophilic ............................ ... ...........:.:..::................... . Beta Ra Ga mma aroma Ray ® Y Pasteurization Class B: Alterative 1 R1 Alternative 2 ® Alternative 3 If applicable to alternative performed (Class B on! ) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ® Composting ® jAerobic Digestion Anaerobic D iQ est' ion® If applicable to alternative performed (Class A or Class B) complete the following monito Jug data: Parameter Allowable Level en Pathog Density Number o Frequency Sample Analytical in Sludge Excee- de ces of Analysis Yp Type Tech-ni ue q Minimunl Geo. Mean MaximulT Units 2x 10tothe 6t power MPN per 592 1976 61453 MPN/g 0 60 days G SM92210E gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) (dry weight Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 21 Option 2 i3 Option 3 ® Option 4 ® y Option 5 El Option 6 ® Option 7 ®Option 8 ® Option 9 ® Option 10 No vector attraction reduction options were performed erformed p U KIIr11;A_HVIN N'tAl1+.'1V1LA T (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Brent Collins - Director of Technical Services Prepare N and Title (type or print) Land App19 e and tle applicable)(type or print) -• . -� j �41/22/201 s Signa e o Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Smithfield Packing Company Permit Number: WQ0014868 WWTP Name: Tarheel WWWTP NPDES Number: NCO078344 Monitoring Period: From Port 3&4 - 4/24/14 To Port 3&4 - 4/24/14 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1® Alternative 2 ® AlternativE30 Alternative 4® Alterative 5 ® Alternativ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 11 Heat Drying ® Heat Treatment ® Thermophilic 13 Beta RayG ® aroma Ray Y Pasteurization a n Class B: Alternative 1 R1 Alternative 2 ® Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying [I Composting osting E3 Aerobic Digestion D Anaerobic Digestion® If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Parameter Allowable Level in in Sludge Pathogen Density Number o de- entes Frequency of Anal sis Sample Type i Analytical Tech - n' ue MinimumGeo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power WN per gram of total solids or 2 x 10 to the 6th power CFU per,gram of 533 1533 19074 MPN/g 0 60 days G SM92210E 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 R1 Option 2 ® Option 3 E3 70ption 4 ® Option 5 El Option 6 ® Option 7 ® Option 8 ® Option 9 ® Option 10 No vectorattraction to reduction options were performed p CERTIFICATION STATEMENT (please check the appropriate statement) 21 " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the. system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Brent Collins - Director of Technical Services Preparer N e d Title (type or print) Land dApplhr Name and Title (if applicable)(type or print) IALR- SignatuO'e f reparer Date Signature of Lan Applier (if applicable) Date DENR FORM RF (512003) ANNUAL PATHOGEN AND VECTOR ATTRACTION RED'UCTION FORM Facility Name: Smithfield Packing Company Permit Number: WWTP Name: Tarheel WWWTP NPDES Number: Monitoring Period: From North - 10/14/14 To North - 10/14/14 WQ0014868 NCO078344 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 10 Alternative 2 ® Alternative 3 El Alternative 40 Alternative 5 ® Alternative 6 11 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ® Heat Drying ® Heat Treatment ® Thermophilic El Beta Ray El Y Gamma Gamma 0 Pasteurization Class B: Alternative 12 Alternative 2 ® Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying E3 Composting ® Aerobic Digestion El Anaerobic Die stion g ................................................................................................................................... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- deuces Frequency of Analysis Sample Type Analytical Tech - e Minimum Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 4751 5744 6623 MPN/g 0 60 days G SM92210E 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 Rl Option 2 ®Option 3 ® Option 4 ® Option 5 Option 6 ® Option 7 E3 I Option 8 ® Option 9 ® 10ption 10 0 No vector attraction reduction were options performed 13 p CERTIFICATION STATEMENT (please check the appropriate statement) Ri "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector .attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) `This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jeff Musselwhite - Environmental Coordinator Brent Collins - Director of Technical Services Preparer Name and Title (type or print) Land App ' Name and itle if applicable)(type or print) Signat e f reparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) - ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM: Facility Name: Smithfield Packing Company Permit Number: WQ0014868 WWTP Name: Tarheel'WWWTP NPDES Number: NCO078344 Monitoring Period: From South-10/14/14 To South - 10/14/14 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 10 Alternative 2 ® Alternative:3 Alternative 4® Alternative 5 ® Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ® Heat Drying ® Heat Treatment ® Thermophilic El Beta Ray Gmma Ray Pasteurization Class B: Alternative 121 Alternative 2 ® Alternative 3 El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ® Composting ® Aerobic Digestion, Anaerobic D i estion® If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Erequency of Anal sis Sample Type Analytical Tech - ni ue Minimum mu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 4484 5639 6600 MPN/g 0 60 days G SM92210E 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 WN per 4 grams total solid I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 21 Option 2 ®Option 3 ® Option 4 ® Option 5 13 Option 6 ® Option 7 ® Option 8 ® Option 9 ® Option 10 No vector attraction reduction options e e performed were CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." JeffMusselwhite - Environmental Coordinator Brent Collins - Director of Technical Services Preparer Name and Title (type or print) Land A pppliaoV&anae and 14tie CW applicable)(type or print) Si a Prepare; �Si �ature of Land Applier (if applicable) Date DENR FORM RF (5/2003) Analytical Results EIVIA Resources, Inc. 755 Yadkinville Rd. Mocksville NC 27028 Entered 412412014 Reported: 4/28/2014 For: Smithfield TarheeI Sample ID Parameter Cust ID Result Units Date Method ,Analyzed Analyst 14.0424-8.1 % Solids N12-I 3.38 % SM254OB-1997 4/24/14 CL 140424-8.1 Fecal Conform MTF N 12-1 592 MPN/g SM92210E-2006 4/24/14 CL 140424-8.1 Geometric Mean N 12-1 1.976 MPN/g dry wt. basis 4/25114 CL 140424-8.2 % Solids N12-2 3.30 % SM254OB-1997 4/24/14 CL 140424-8.2 Fecal Coliform MTF N12-2 <606 MPN/g SM92210E-2006 4124/14 CL 140424-8.3 % Solids N 12-3 3.28 % SM254OB-1997 4/24/14 CL 140424-8.3 Fecal Coliform MTF N12-3 610 MPN/g SM92210E-2006 4/24/14 CL 140424-8.4 % Solids N12-4. 3.29 % SM254OB-1997 .4/24/14 CL 140424-8.4 Fecal Coliform MTF N12-4 <608 MPN/g SM92210E-2006 4/24/14 CL 140424-8.5 % Solids N12-5 3.22 % SM2540B-1997 4/24/14 CL 140424-8.5 Fecal Conform MTF N12-5 <621 MPN/g SM92210E-2006 4/24/14 CL 140424-8.6 % Solids N 12-6 3.58 % SM254OB-1997 4/24/14 CL 140424-8.6 Fecal Coliform MTF N 12-6 61,453 MPN/g SM9221 CE-2006 4/24114 CL 140424-8.7 % Solids N12-7 3.45 % SM254OB-1997 4/24/14 CL 140424-8.7 Fecal Coliform MTF N 12-7 23,188 MPN/g SM9221 CE-2006 4124/14 CL P.O. Box 228 a Statesville, North Carolina 28687 9 7 04/8 7 2/4697 EIVIA Resources, Inc. 755 yadkinville Rd. Mocksville - Entered 4/24/2014 Reported: 4/28/2014 For: NC 27028 Date Sample ID Parameter Cust ID Result Units Method Analyzed Analyst Respectfully submitted, V Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.O. Box 228 a Statesville, North Carolhia 28687 0 704/872/4697 Mll Client: ""'' . 3­--7) i E STAT'SVfLLE ANAINTICAL 122 Court Street - P.O. Vix 228 Address: Slatesville.NC 28687 (704) 8724697 Chain of Custody Record Contact Person: Phone # FAX# PO # Requisitioned by: (Time Date) Customer Lab -ID # Time Sampled Date Sampled a E Matrix Parameters requested for analysis shrigo w I VM Sample 'D# (Grab Only) (Grab Only) 1V I J /7 A Al F\` V -7 ­111V q Relinquished by: Time am,, pm Date V Sampled by: '4: Received by: X Time ampM' Date Transported by: Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date Compliance work: Composite- Sampling #1: Time begin- am, pm Date Non-compliance work: Time end am, pm Date Lab Comments: composit ampling #2: Time begin- am, pm Date Time end am, pm Date i Analytical Results EIVIA Resources, Inc. \ 755 Yadkinville Rd. Mocksville NC 27028 Entered 4/24/2014 Reported: 4/28/2014 For: Smithfield Tarheel Date Sample ID Parameter Cust ID Result Units Method Analyzed Analyst 140424-9.1 % Solids N34-1 3.67 % SM2540B-1997 4/25/14 CL 140424-9.1 Fecal Coliform MTF N34-1 19,074 MPN/g SM92210E-2006 4/25114 CL 140424-9.1 Geometric Mean N34-1 1533 MPN/g dry wt. basis 4/28114 CL 140424-9.2 % Solids N34-2 3.72 % SM254OB-1997 4/25/14 CL 140424-9.2 Fecal Coliform MTF N34-2 13,441 MPN/g SM92210E-2006 4/25/14 CL 140424-9.3 % Solids N34-3 3.75 % SM254OB-1997 4/25114 CL 140424-9.3 Fecal Coliform MTF N34-3 533 MPN/g SM92210E-2006 4/25/14 CL 140424-9.4 % Solids N344 3.27 % SM254OB-1997 4/25/14 CL 140424-9.4 Fecal Coliform MTF N344 <612 MPN/g SM92210E-2006 4/25/14 CL 140424-9.5 % Solids N34-5 3.56 % SM254OB-1997 4/25/14 CL 140424-9.5 Fecal Coliform MTF N34-5 562 MPN/g SM9221 CE-2006 4/25/14 CL 140424-9.6 % Solids N34-6 3.24 % SM254OB-1997 4/25/14 CL 140424-9.6 Fecal Coliform MTF N34-6 617 MPN/g SM92210E-2006 4/25/14 CL 140424-9.7 % Solids N34-7 2.92 % SM254OB-1997 4/25114 CL 140424-9.7 Fecal Coliform MTF N34-7 <685 MPN/g SM92210E-2006 4/25/14 CL Rn. Box 228 • Statesville, North Carolina 28687. 704/872/4697 r EIVIA Resources, Inc. L 755 Yadkinville Rd. Mocksville NC 27028 1` Entered 4/24/2014 Reported: 4/28/2014 For: Sample ID Parameter Cust ID Result Units ®ate Method Analyzed Analyst Respectfully submitted, Dena Myers NC Cert #440., NCDW Cert #37755, EPA NCOO9O9 P.O. Box 228 • Statesville, North Carolina 28687 c 704/872/4697 M Client: STATESVILU ANALYTICAL 122CourtStwet - RO.Box228 Statesville. NC 28687 (704) 87241697 Address: f 77,77 Contact Person: Phone FAX4 Chain of E F (lime Date) � Custody Record PO # Requisitioned by: Customer Time Sampled Lab -ID # Date Sampled Matrix Parameters requested for analysis Sample IDU (Grab Only) (Grab Only) sludgOW I ww l Al '2 41 4 � Al' Relinquished by: Time /,;4 am -.pT Date Sampled by: Received by: A V 7 Time / am,, Date / Transported by: r. Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date Compliance work: Composite Sampling #11: Non-compliance work: Time begin- am, pm Date Time end am, pm Date Lab Comments: Comi2osite Sampling #2: Time begin- am, pm Date Time end- am, pm Date Analytical Results EIVIA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Date: 10/1412014 Reported: 10/16/2014 For: Smithfield Tar Heel Comments: Geometric Mean = <5744 MPN/g Sample Number parameter Sample ID Result Unit Method Analyzed Analyst 141014-19-01 Fecal Coliforms SFN-1 <5714 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-01 Percent Solids SFN-1 3.5012 % SM2540B-1997 10/14/2014 MD 141014-19-02 Fecal Coliforms SFN-2 <4938 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-02 Percent Solids SFN-2 3.2452 % SM25406-1997 10/14/2014 MD 141014-19-03 Fecal Coliforms SFN-3 <6116 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-03 Percent Solids SFN-3 3.2716 % SM2540B-1997 10/14/2014 MD 141014-19-04 Fecal Coliforms SFN-4 <6623 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-04 Percent Solids SFN-4 3.024 % SM2540B-1997 10/14/2014 MD 141014-19-05 Fecal Coliforms SFN-5 <6135 MPN/g SM9221 CE-2006 10/14/2014 CL I 141014-19-05 Percent Solids SFN-5 3.2572 % SM2540B-1997 10/14/2014 MD 141014-19-06 Fecal Coliforms SFN-6 <4751 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-06 Percent Solids SFN-6 42108 % SM25408-1997 10/14/2014 MD 141014-19-07 Fecal Coliforms SFN-7 <6192 MPN/g SM92210E-2006 10/14/2014 CL 141014-19-07 Percent Solids SFN-7 3.2268 % SM2540B-1997 10/14/2014 MD Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 s Statesville, NC 28687 ® 704/872/4697 Page f of 3 Client: C C , S'rATESVILLE ANALYTICAI, 122 Court Street - P.O. Box 229 Address: Staiesville. NC 28687 (704),02-4097 Contact Person: Phone# 7 FAX# Chahi of PO 11 Requisitioned by: (Tim e oat©) Custody Record -T— Customer I Ime Sampled Lab ID 4 Date SampledMatrix Parameters requested for analysis Sample 10ft (Grab Only) (Grab Only) h- 71 0" tv� -`5 r1r IV I < —7- !0' t -S J -------------- Relinquished by: -9/ Time Date arn�'D'm,) a e L�L / -:�V Sampled by: Received by: am ate' E-4Li Transported by: Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date compliance work: L Composite Sampling #11. Non-compliance work: Time begin— am, pm Date Time end am, pm Date Lab Comments: Composite. Sampling #2: Time begin— am, pm Date Time end_ am, pm Date �Analytical Results EINIA Resources, Inc. 755 Yadkinville Rd. Mocksville, NC 27028 Receive Date: 10/14/2014 Reported: 10/16/2014 For: Smithfield Tar Heel Comments: Geometric Mean = <5639 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 141014-18-01 Fecal Coliforms 1-SFS <4484 MPN/g SM92210E-2006 10/14/2014 CL 141014-18-01 Percent Solids 1-SFS 4.4624 % SM254OB-1997 10/14/2014 MD 141014-18-02 Fecal Coliforms 2-SFS <6024 MPN/g SM92210E-2006 10/14/2014 CL 141014-18-02 Percent Solids 2-SFS 3.3188 % SM254OB-1997 10/14/2014 MD 141014-18-03 Fecal Coliforms 3-SFS <6042 MPN/g SM9221 CE-2006 10/1412014 CL 141014-18-03 Percent Solids 3-SFS 3.31 % SM254OB-1997 10/14/2014 MD 141014-18-04 Fecal Coliforms 4-SFS <6600 MPN/g SM9221 CE-2006 10/14/2014 CL 141014-18-04 Percent Solids 4-SFS 3.034 % SM2540B-1997 10/14/2014 MD 141014-18-05 Fecal Coliforms 5-SFS <4608 MPNIg SM92210E-2006 10/14/2014 CL 141014-18-05 Percent Solids 5-SFS 4.3444 % SM2540B-1997 10/14/2014 MD 141014-18-06 .Fecal Coliforms 6-SFS <6192 MPN/g SM92210E-2006 10/14/2014 CL 141014-18-06 Percent Solids 6-SFS 3.2312 % SM254013-1997 1.0114/2014 MD 141014-18-07 Fecal Coliforms 7-SFS <5899 MPN/g SM92210E-2006 10/14/2014 CL 141014-18-07 Percent Solids 7-SFS 3.3864 % SM2540B-1997 10/14/2014 MD Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 - Statesville, NC 28687-704/872/4697 Page 1 of 3 Client: 'Aj- _)J_" "XTICAL STATE'sVIIAX ANAt 122 Court Streci - RO. Box 229 Address: c" p Statesville.W 1-8687 (704) 8724097 Chain of Contact Person: -7 Phone FAX# VI r. PO # �*.qFr' "I __Y�_ Requisitioned by: A (rime Date) Custody Record Customer Lab -ID Time Sampled Date Sampled Ri Matrix Parameters requested for analysis %,j VN, Sample IN (Grab Only) (Grab Only) 3 NIIIV71 Relinquished by: Time amp Date /1) Sampled by Received by: Time/ Al 4'e 411 am, I#n A)ate,"�,"' -�'Z-/t_Z Transported b Y: X Relinquished by: Time am, pm Date Holding times met: L ... ..... Received by: Time am, pm Date Compliance work: Composite Sampling #1: Time begin- am, pm Date Non-compliance work: Time end ------am, pm Date Lab Comments: ComposIte, Sampling 42, Time begin- am, pm Date Time end am, pm Date t-age1 of`I y Report Number: 14-323-0728 Account Number: 46245 3 U Send To: EMA RESOURCES INC Wwwaleasiem.com 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 11/19/2014 Date Of Analvsis: 11/20/2014 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: WILLIAM DUNHAM Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 11/20/2014 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number o /o Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm. Rate ppm . Rate ppm Rate p H Index meq/100g meq/100g 7 20677 2.8 M 96 238 VH 35 VL 243 VH 892 M 26 VL 6.5 0.5 7.2 NC=198 NC=18 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI Field ID % % % I % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 7 17 M 28.7 VH 113 VH 274 VH 6.1 VH 0.4 L 0.13 VL 1.2 28.1 61.9 1.6 ' 7.4 NC=35 NC=717.5 1 NC=706 NC=305.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. ?uric ifc GOw� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. i C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary raye 1 of I Report Number: 14-323-0713 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 www.aleastem.com Date Received: 11/19/2014 Date Of Analysis: 11/20/2014 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: VANCE TYSON SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 11/20/2014 Farm ID: Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number ° ENR /° Rate Mehlich 3 Reserve K Mg - Ca Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate -ppm Rate ppm Rate p H Index megl100g megl100g 6 125 VH 115 M 136 L 1046 L 31 VL 20658 15.2 VH 150 1 5.0 6.46 4.7 11.5 NC = 104 NC = 59 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NOsN S Zn Mn Fe Cu B SS Cl Al % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 6 30 H 16.4 VH 7 L 395 VH 1.9 H 0.4 L 0.2 VL 2.6 9.9 45.5 1.2 40.9 NC=62 NC=410.0 NC=44 NC=95.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Ppp/ic Vmc Gad H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by:ABL Eastern Laboratories, Inc. [f C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 14-323-0726 I( Account Number: 46245 U Send To: EMA RESOURCES INC Wuuwaleastem,com 755 YADKINVILLE RD MOCKSVILLE NC 27028 nafp Rprpivpd- 11/19/2014 Date OfAnalvsis: 11/20/2014 AFL Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: J BURNEY Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 11/20/2014 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate lbs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm' Rate ppm Rate PH Index meq/100g meq/100g 3 20671 3.6 M 110 149 VH 55 VL 246 H 956 M 29 VL 5.9 6.78 1.5 8.6 NC=124 NC=28_ 6 20672 3.3 M 105 845 VH 1173 VH 1121 M 1 756 L 129 VL 6.3 6.69 2.4 7.8 NC = 704 NC = 88 1-8 20673 3.5 M 108 555 VH 108 M 175 H 985 M 24 VL 5.7 6.75 1.8 8.6 NC = 462 NC = 55 9 20674 1.4 L 71 1680 VH 60 L 72 M 536 M 120 VL 5.5 6.81 1.2 4.7 NC=567 NC=31 14 20675 3.0 M 102 569 VH 26 VL 99 M 1643 M 19 VL 5.5 6.78 1.5 5.6 NC=474 NC=13 Percent Base Saturation I Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS CI Al Field ID % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm- 3 18 M 24.5 VH 229 VH 229 VH 7.5 VH 0.4 L 1.6 23.8 55.5 1.5 17.1 NC = 37 NC = 612.5 1 NC = 1431 1 1 NC = 375.0 6 H 76.4 VH VH 338 VH VH VL 5.7 12.9 48.5 1.6 30.9 �26 NC = 54 NC = 1910.0 165 NC = 406 121.2 NC = 1060.0 10.3 g 19 M VH H VH VH 0.4 L 3.2 17.0 57.3 1.2 21.0 168.5 125 1359 19A NC=40 NC=1712.5 NC=156 NC=470.0 g 15 L 50.8 VH 19 M 386 VH 13.9 VH 0.2 VL 3.3 12.8 57.0 1.9 26.0 NC=31 NC=1270.0 NC=119 NC=695.0 14 L 72.5 VH 11 M VH VH 0.2 VL 1.2 14.7 57.4 1.5 26.0 114 NC=29 NC=1812.5 NC=69 �289 122.3 NC=1115.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g mapmum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble. Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary rctye 1 Of 1 _ Report Number: 14-287-0658 Account Number: 46245 Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 10/14/2014 A&L Eastern Laboratories e, 7621 Whitepine Road .Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastem,com Grower: MACK KING Farm ID: 6fS SOIL ANALYSIS REPORT Analytical'Method(s): Mehlich 3 Date Of Analysis: 10/15/2014 Date Of Report: 10/15/2014 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Rate ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 3 116 VH 103 H 37 L 317 L 14 VL 24531 1.9 L 83 5.3 6.83 1.0 3.2 NC=97 NC=53 4 M 59 L 52 M 323 M L 24532 1.9 L 84 �49 115 5.7 6.87 0.6 2.9 NC=41 NC=30 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl Al % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 3 19 MI10.9 VH 8 L 194 VH 2.8 H 0.3 VL 0.09 VL 8.3 9.6 49.5 1.9 31.2 NC = 40 NC. = 272.5 NC = 50 NC = 140.0 4 12 L VH 9 L VH 1.6 H VL VL 5.2 14.9 55.7 2.2 20.9 18.4 1NC �135 FO2 10.07 NC=25 NC=210.0 56 NC=80.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Nage 1 of i Report Number: 14-323-0714 Account Number: 46245 t� wwwaleastem.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 Date Received: 11/19/2014 Date Of Analvsis: 11/20/2014 A&L Eastem Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: MCCALL KING SOIL ANALYSIS REPORT Date Of Report: 11/20/2014 Analytical Method(s): Mehlich 3 Farm ID:5GiZ, Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g 1 20659 1.1 L 66 210 VH 59 L 1 77 M 658 H 17 VL 6.5 0.3 4.5 NC = 175 NC = 30 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS CI AI Field ID % % I % % % Pp m Rate PP m Rate PP m Rate PP m Rate Pp m Rate PP m Rate PP m Rate ms/cm Rate Pp m Rate pp m 1 13 L 9.0 VH 14 M VH 1.8 H 0.2 VL 0.11 VL 3.4 14.3 73.1 1.6 7.4 �150 NC = 27 I NC = 225.0 NC = 88 NC = 90.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: { "t;c me Gwr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 14-323-0727 Account Number: 46245 WNWAleastem.cotn Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE NC 27028 n rune• r%-4-r% A....r-iiionion4A A &L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: DOUGLAS MUSSELWHITE Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 n.fn Af Rannrt• 91/9n/9f11A Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich3 . Reserve-. K Mg Ca Na Soil Buffer H Field ID Number % Rate lbs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meg1100g megi100g 4 248 VH 37 VL 49 M P27 M VL 5.8 6.85 0.8 4.0 20676 1.4 L 72 116 NC=207 NC=19 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI Field ID % % % % % Pp m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate ms/cm Rate PP m Rate ppm q 10 L 15.7 VH 16 M 158 VH 3.8 VH 0.2 VL 2.4 10.2 65.9 1.7 18.8 NC=21 NC=392.5 NC=100 NC=190.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) testea. jampies are retameu a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days, after testing. by: rAu��a mr G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. r o C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Pat McCrory Governor A ��`� NCDENR North Carolina Department of Environment and Natural Resources July 22, 2014 Kyle Narron, General Manager Smithfield Farmland Corporation — Tar Heel Division Post Office Box 99 Tar Heel, North Carolina 28392 Dear Mr. Narron: John E. Skvarla, III Secretary Subject: Permit No. WQ0014868 Smithfield Farmland Corporation — Tar Heel Division Land Application of Industrial by Product Residuals (Non - Dedicated) Bladen County In accordance with your Permittee name change and permit renewal request received May 28, 2014 and April 1, 2014 respectively, we are forwarding herewith Permit No. WQ0014868 dated July 22, 2014, to Smithfield Farmland Corporation — Tar Heel Division for the continued operation of the subject residuals management program. Please note that this renewed permit shall become effective on August 1, 2014 (i.e. the day after the expiration date of the existing permit), which differs from the date of this letter. Modifications to the subject permit include the deletion of the following fields from the land application program decreasing the total acreage from 1412.4 to 1179.8 acres: SFOI-01, SFO1-02, SFOI-03, SFO1-04 (85-60 acres) SF03-08 (41.0 acres) SF04-04, SF04-05, SF04-06, SF04-07, SF04-08, SF04-09, SF04-10 (106.0 acres) Please note the name of the Permittee has been changed from Smithfield Packing Company, Inc. — Tar Heel Division to Smithfield Farmland Corporation — Tar Heel Division. The owner of Fields SF03- 01, SF03-02, SF03-03, SF03-04, SF03-05, SF03-06 and SF03-07 has changed from William Dunham to Steve Dunham.. The owner of Fields 09-01, SF09-02, SF09-03, and SF09-04 has changed from Douglas Musselwhite to Melba Musselwhite. The owner of Field SF12-01 has changed from David S. Canady to Hinton King. This permit shall be effective from August 1, 2014 until July 31, 2019, shall void Permit No. WQ0014868 issued August 26, 2005 and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachments A for they may differ from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Phone: 919-807-64641 Internet: http:llportal.nrdenr.orgAyeblwa An Equal Opportunity 1 Affirmative Action Employer— Made in part wish recycled paper Mr. Narron July 22, 2014 Page 2 of 3 Please note that on September 1, 2006, North Carolina Administrative Code Title 15A Subchapter 02T — Waste not Discharged to Surface Waters was adopted. Accordingly, this permit incorporates the requirements of these rules, therefore, please take the time to review this permit thoroughly. The following conditions have been added, modified or deleted from those in the last permit issuance: y Condition 1.2. — Allows 90 days to notify the regional office of an intended land application Condition 1.3. — Allows 90 days to submit an Operation and Maintenance Plan i� Condition 1.4. — Allows 180 days to achieve compliance with site signage requirements °v Condition IL8. — Lists the setback distances for land application sites Y Condition 11.9. — Lists the setback distances for bulk residual applications ➢ Condition 11.11. — Describes appropriate methods for calculating agronomic application rates i Condition 11.12. — Describes the realistic nitrogen rate for hay crops on grazed pasture areas ➢ Condition I1I.4. — Outlines the requirements of an Operation and Maintenance Plan i' Condition 111.6. — Requires the permit and O & M Plan to be kept on site during applications ➢ Condition 111.7. — Requires spill control provisions during residuals transport and application i' Condition 111.11. --- Lists conditions under which bulls residuals are not allowed to be applied ➢ Condition II1.12. — Lists public access restrictions ➢ Condition 111.13. — Describes the signage requirements for each land application site Y Condition IV.7. Lists the recording requirements for all land application events y Condition 1V.8. — Requires the submission of an annual report each year Condition V.l. — Requires inspection and maintenance in accordance with the O & M Plan Condition V1.6. — Allows permit revocation or unilateral modification in certain situations v Condition V1.7. — Prohibits expansion of the program in certain instances If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699--6714. Unless such demands are made, this permit shall be final and binding. Mr. Narron July 22, 2014 Page 3 of 3 If you need additional information concerning this matter, please contact Alice M. Wessner at (919) 807-6425 or alice.wessner@ncdenr.gov. Sincerely, Thomas" A. Reeder, Director Division of Water Resources cc: Bladen County Health Department Cumberland County Health Department Roberson County Health Department Fayetteville Regional Office, Water Quality Regional Operations Section Roy L. Whitaker, EMA Resources, Inc. 755 Yadkinville Road, Mocksville, North Carolina 27028 Beth Buffington, Public Water Supply Section — Protection and Enforcement Branch Permit File WQ0014868 Notebook File WQ0014868 This Page Blank NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMIVIISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF INDUSTRIAL BY PRODUCT RESIDUALS PERMIT (NON -DEDICATED) In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Smithfield Farmland Corporation -Tar Heel Division Bladen County FOR THE continued operation of a residuals management program for the Smithfield Farmland Corporation -Tar Heel Division and consisting of the land application of Industrial By Product residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received April 1, 2014, and in conformity with other supporting data subsequently fled and approved by the Department of Environment and Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from August 1, 2014 until July 31, 2019, shall void Permit No. WQ0014868 issued August 26, 2005, and shall be subject to the following specified conditions and limitations: I. SCHEDULES I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0I05(d) requires an updated site map to be submitted with the permit renewal application. 2. The permittee shall be in full compliance with the regional office notification requirements established in Condition III.3. by October 22, 2014 (90 days from the effective date of this permit). 3. The permittee shall be in full compliance with the signage requirements established in Condition 111.13. by January 22, 2015 (180 days from the effective date of this permit). WQ0014868 Version 3.0 Shell Version 140324 Page I of 11 H. PERFORMANCE STANDARDS The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals to the site, contact the Fayetteville regional office supervisor, and take any immediate corrective actions. 2_ This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. 3. Only residuals generated by the facilities listed in Attachment A are approved for land application in accordance with this permit. 4. Only the sites listed in Attachment B are approved for residuals land application. 5. Pollutant concentrations in residuals applied to land application sites Iisted in Attachment B shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The Permittee shall determine compliance with the CPL.Rs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application have not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. 6. ResiduaIs that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A. 7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. WQ0014868 Version 3.0 Shell Version 140324 Page 2 of 11 8. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback feet Habitable residence or place of public assembly under separate ownership or not 100 to be maintained as part of the project site Property lines 50 Private or public water supply 100 Surface waters (streams -- intermittent and perennial, perennial waterbodies, and 50 wetlands Wells with exception to monitoring wells 100 All treatment and storage facilities were originally permitted prior to September 1, 2006 9. Setbacks for Class Bland application sites shall be as follows: Setback by application type (feet) Setback Description Vehicular Irrigation Surface Surface Injection Application Application Incorporation Habitable residence or place of public assembly under separate ownership or not to be maintained as 400 400 200 art of the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the 0 200 0 lessee/operator of the land to be maintained as part of the project site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, 100 100 50 perennial waterbodies, and wetlands) Surface water diversions (ephemeral streams, 25 100 25 waterways, ditches) Groundwater lowering ditches (where the bottom of 25 100 25 the ditch intersects the SHWT Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 100 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or 15 15 15 more in vertical height Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 WQ0014868 Version 3.0 Shell Version 140324 Page 3 of I I 10. Land application areas shall be clearly marked on each site prior to and during any residuals application event. 11. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http://nutrients.soil.nesu.cdu/,y_ields/index.php). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist_ ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 aLttp://v,rww.neagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards(ftp://ftp-fc.se.egov.usda.gov/Nl4Qpractice-standards/standards/590_pdf). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. 12. When residuals are Iand applied to grazed pasture, bay crop realistic nitrogen rate shall be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. 13. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer and rye grass in the winter with both crops to receive residuals), then the second crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (Ibs/ae/yr). This practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. 14. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum., etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall maintain written records of these recommendations and details of their implementation. 15. The compliance boundary for residual land application sites shall be specified in accordance with 15A NCAC 02L .0107(b). These sites were individually permitted on or after December 30, 1983; therefore, the compliance boundary is established at either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to remediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. WQ0014868 Version 3.0 Shell Version I40324 Page 4 of I I 16. In accordance with 15A NCAC 02L .0108, the review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L .0106. III. OPERATION AND MAINTENANCE REQUIREMENTS The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. 2. The Fayetteville Regional Office, telephone number (910) 433-3300, and the appropriate local government official (Le., county manager, city manager, or health director) shall be notified at Ieast 48 hours prior to the initial residuals land application to any new Iand application site. Notification to the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. 3. The Fayetteville Regional Office shall be notified via email or telephone, (910) 433-3300, at least 24 hours prior to conducting any land application activity. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) pursuant to 15A NCAC 02T A 110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a) Operational functions; b) Maintenance schedules; c) Safety measures; d) Spill response plan; e) Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit-, f) Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event_ The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). WQ0014868 Version 3.0 Shell Version 140324 Page 5 of]] Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition III. 4.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Technical Assistance & Certification Unit at (919) 733-0026. 6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the Iand application sites during land application activities. 7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. 8. Residuals shall not be stored at any land application site, unless written approval has been requested and received from the Division. 9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. 10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. 11. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. if the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations to the acceptable soil pH (6.0) will be noted in this permit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; j. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; WQ0014868 Version 3.0 Shell Version 140324 Page 6 of 11 k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals Iand application event. 13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a Iand application event, and for as long as the public access restrictions required under HI. 12 apply. I4. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period_ Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the Iand 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 38 months surface shall not be harvested for: 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (NRCS) or other State Agencies_ The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the Iand application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. WQ0014868 Version 3.0 Shell Version 140324 Page 7 of 11 IV. MONITORING AND REPORTING REOUIIMEMENTS 1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (I.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.00$) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (02) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the foll wing parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) WQ0014868 Version 3.0 Shell Version 140324 Page 8 of 11 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website(http://www.ncagr.gov/agronomi/pubs.htm). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exehan eable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. 7. The Permittee shall maintain records tracking all residual land application events. At a minimum, these records shall include the following: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number as listed in Attachment B); d. Approximate areas applied to (acres); e. Method of land application; f. Weather conditions (e.g., sunny, cloudy, raining, etc.); g. Predominant Soil Mapping Unit (e.g., CbB2); h. Soil conditions (e.g., dry, wet, frozen, etc.); i. Type of crop or crops to be grown on field; j. Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years); k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet ton per acre; Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or wet tons per acre; m. Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, djy ton per acre, or wet tons per acre; and WQ0014868 Version 3.0 Shell Version 140324 Page 9 of I i n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy metal (e.g., shaIl include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each held. Three copies of an annual report shall be submitted on or before March 1'. The annual report shall meet the requirements described in the Instructions_ for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http://.portal.nedenr.or web/wq/gps/lau/reportiniz, or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 9. Noncompliance Notification The Permittee shall report by telephone to the Fayetteville Regional Office, telephone number (910) 433-3300, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the land application program resulting in the land application of significant amounts of wastes that are abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to surface waters. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. WQ0014868 Version. 3.0 Shell Version 140324 Page 10 of 11 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215.6C. 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in ISA NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A NCAC 02B _0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. 5. In the event the residuals program changes ownership or the Permittee changes their name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. 6_ This permit is subject to revocation or unilateral modification upon 60 days notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revolve this permit pursuant to 15A NCAC 02T .0I05(e)(3)_ Permit issued this the 22"d day of July 2014 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION r ThomaV . Reeder, Director Division of Water Resources By Authority of the Environmental Management COMMISSiOn Permit Number WQ0014868 WQ0014868 Version 3.0 ShelI Version 140324 Page It of 1 I THIS PAGE 13LANK Page 1 of 1 ATTACHMENT A - Approved Residual Sources Smithfield Farmland Corporation —Tar Heel Division Certification Date: July 22, 2014 Permit Number: WQ0014868 Version: 3.0 Maximum Monitoring Monitoring Monitoring Frequency for Approved Owner Facility Name County Permit I3ivlagieal Dry TonNumber Frequency for frequency for Pathogen & Mineralization Residuals Per Year ear I Non -hazardous Metals and Vector Attraction Rate Characteristics z Nutrients 315 4, 5, 6 lE�edi1Ct16n5 Smithfield Farmland Corporation — Tar Heel Tar Heel WWTP Bladen NCO078344 Yes 2,050 Annually See Table Below See Table Below 0.20 Division Total 2,050 1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition I V.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Generated short tons per ear Monitoring Frequency Established in 40 C]a l2 503 and 15A NCAC 02T .1111 <319 1/Year =>319 - <1,650 1! guarter 4 times 2er ear _> 1,650 - <16,500 1/60 Days 6 times 2er ear =>16,500 1/month 12 times per ear 6. Industrial By Product residuals are exempt from meeting the vector attraction reduction requirements in Condition 1VA, provided they are not mixed with residuals that have been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Industrial By Product residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in 15A NCAC 02T .l 102(6). If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. Page I of I This Page Blank ATTACHMENT B - Approved Land Application Sites Smithfield Farmland Corporation — Tar Heel Division Certification Date: July 22, 2014 Permit Number: WQ0014868 Version: 3.0 Field Owner Lessee County latitude Longitude Net Acreage Dominant Soil Series Footnotes SF03-01 Dunham. Steve Bladen 340 44' 06" 780 43' 07" 21.60 Lakeland sand, I-7% slopes SF03-02 Dunham, Steve Bladen 34° 44' 15" 780 43' 12" 13.30 Centenary sand 3 SF03-03 Dunham, Steve Bladen 340 44' 18" 780 43' 20" 21.30 Centenary sand SF03-04 Dunham, Steve Bladen 340 44' 12" 780 43' 26" 19.00 Wasda muck SF03-05 Dunham, Steve Bladen 340 44' 08" 78" 43' 21" 8.00 Lakeland sand, 1-7% slopes SF03-06 Dunham, Steve Bladen 340 44' 02" 780 43' 33" 32.00 Lakeland sand, 1-7% slopes SF03-07 Dunham, Steve Bladen 340 43' 28" 780 44' 21" 37.20 Wickham fine sandy loam, 1-6% slopes 3 SF07-01 Burney, J W Dunham, Steve Bladen 340 43' 11" 780 44' 26" 21.8 Altavista tine sandy loam, 0-3% slopes 3 SF07-03 Burney, J W Dunham, Steve Bladen 340 43' I5" 780 44' 10" 12.3 Altavista fine sandy loam, 0-3%slopes 3 SF07-06 Burney, J W Dunham, Steve Bladen 340 43' 29" 780 43' 53" 19.3 Wickham fine sandy loam, 1-6%slopes SF07-08 Burney, J W Dunham, Steve Bladen 340 43' 37" 78043' 44" 12.1 Altavista fine sandy loam, 0-3% slopes SF07-09 Burney, J F Dunham, Richard Bladen 34" 43' 44" 780 43' 44" 21.3 Wickham fine sandy loam, 1-6%slopes SF07-14 Burney, J F Dunham, Richard Bladen 340 43' 55" 780 43' 27" 7.5 Lakeland sand, 1-7% slopes 3 SF07-15 Burney, 3 F Dunham, Richard Bladen 340 43' 51" 780 43' 41" 3.0 Lakeland sand, 1-7% slopes 3 SF l0-01 Butler, Murdock M Bladen 34" 46' 32" 780 49' 19" 53.00 Norfolk loamy fine sand, 0 to 2% slopes SF 10-02 Butler, Murdock, M, Bladen 340 47' 30" 78" 49' 48" 45.0 Autryville loamy sand, 0-3% slopes SF 10-03 Butler, Murdock M Bladen 340 47' 23" 780 49' 54" 31.00 Norfolk loamy fine sand, 0 to 2%slopes SF12-01 King, I -Linton McCall Bladen 34° 48' 19" 78° 51' 46" 49.00 Norfolk loamy fine sand, 0 to 2%slopes Total acreage far Bladen County 427.7 SF06-O i Tyson, Vance Cumberland 340 55' 43" 780 50' 24" 5.5 Autryville loamy sand, 0-3% slopes SF06-02 Tyson, Vance Cumberland 340 55' 48" 780 50' 14" 31.1 Autryville loamy sand, 0-3% slopes SF06-03 Tyson, Vance Cumberland 34Q 55' 29" 780 50' 14" 64.5 Deloss loam 3 SF06-04 Tyson, Vance U Cumberland 340 55' 43" 780 50' 24" 35.0 Deloss loam 3 SF06-05 Tyson, Vance U Cumberland 34" 55' 48" 780 50' 14" 34.00 Deloss loam 3 SF06-06 Tyson, Vance U Cumberland 340 55' 29" 780 50' 14" 79.00 Deloss loam 3 SF06-07 Tyson, Vance U Cumberland 340 55' 50" 780 49' 41" 77.00 Deloss loam 3 ATTACHMENT B - Approved Land Application Sites Smithfield Farmland Corporation -- Tar Heel Division Certification Date: July 22, 2014 Permit Number: WQ0014868 Version: 3.0 Field Owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Footnotes Total acreage for Cumberland County 326.10 SF08-01 King, Hinton McCall Robeson 340 44' 50" 78" 53' 29" 7.5 Goldsboro loamy sand, 0 to 2% slopes SF08-02 King, Hinton McCall Robeson 340 44' 44" 780 53' 21" I7.00 Goldsboro loamy sand, 0 to 2% slopes SF08-03 King, Hinton McCall Robeson 340 45' 0I" 780 53' I2" 89.50 Marlboro sandy loam, 0 to 2% slopes S F08-04 King, Hinton McCall Robeson 34" 43' 18" 780 55' 15" 64.50 Norfolk loamy sand, 0 to 2% slopes SF08-05 King, Hinton McCall Robeson 340 43' 22" 780 56' 02" 46.00 Goldsboro loamy sand, 0 to 2% slopes SF08-06 King, Hinton McCall Robeson 340 43' 50" 780 56' 00" 21.50 Norfolk loamy sand, 0 to 2% slopes SF08-07 King, Hinton McCall Robeson 340 43' 21" 780 56' 47" 37.00 Goldsboro loamy sand, 0 to 2% slopes SF08-09 King, Hinton McCall Robeson 340 46' 35" 780 58' 06" 45.00 Coxville loam 3 SF09-01 Musselwhite, Douglas Robeson 340 4740" 78" 55' 56" 36.00 Wagram loamy sand, 0 to 6% slopes 1 SF09-02 Musselwhite, Douglas Robeson 340 47' 49" 780 56' 06" 27.50 Goldsboro loamy sand, 0 to 2% slopes 2 SF09-03 Musselwhite, Douglas Robeson 340 47' 21" 78" 55' 53" 9.50 Wagram loamy sand, 0 to 6% slopes SF09-04 Musselwhite, Douglas Robeson 34° 47' 12" 1 78° 55' 59" 25.00 Wagram loamy sand, 0 to 6% slopes Total acreage for Robeson County 426.00 Total Land Application Area 1179.8 l . A reduced setback front a residence under separate ownership has been approved for this land application sitc. Mile Road regardless of whether a surface or a subsurface application method. 2. A reduced setback from a residence under separate ownership has been approved for this land application site. 20, regardless of whether a surface or a subsurface application method 3. Residual land application events on these fields shall be prohibited from December through March inclusive. separation between the depth of the residuals land application and the water table is less than three feet. Residuals may be land applied within 200 feet ol'the residences along Barker Ten Residuals may be land applied within 200 feet of the residences along Highway No residuals shall be land applied to these fields when the vertical A4a 4 Aja NCDENR North Carolina Department of Environment and Nati Division of Water Quality —3everly Eaves Perdue Coleen H. Sullins Governor Director March 10, 2010 Mr. Larry Johnson, General Manager Smithfield Packing Company — Tar Heel Plant P.O. Box 99 Tar Heel, North Carolina 28392 SCANNED DATE: 2 /;/t S RECEIVED / DENR / DWQ Aquifer protection Section MAR 16 2010 Dee Freeman Secretary Subject: Permit Extension Permit No. WQ0014868 Smithfield Packing Co. WWTP Land Application of Residual Solids (503 Exempt) Bladen County Dear Mr. Johnson: On August 5, 2009, Session Law 2009-406, entitled "An Act to Extend Certain Government Approvals Affecting the Development of Real Property Within the State," was enacted by the General Assembly and signed into law. The Act, known as the Permit Extension Act of 2009, extends the expiration date of certain government approvals and permits. For additional information, the following website ( http:/portal.ncdenr.org/web/wqlaps/lau#extension ) can be viewed to address this statute and affected DWQ permits. Non -discharge permit, WQ0014868, issued by the Division of Water Quality falls within the scope of this Act and is therefore being extended until 31 July 2013. Please note per your permit, a renewal application must still be submitted six months in advance of the extended expiration date. if Smithfield Packing Company needs to modify, upgrade, retrofit infrastructure at this facility which would require modification of the permit; a permit application can be submitted for review and the necessary modified permit issued. If you have any questions regarding this letter, please contact Division staff in the Fayetteville Regional Office at (910) 433-3340 or Central Office at (919) 733-3221. Thank you in advance for your cooperation. Sincerely, .JJ rt R4R0--6F-- Jim Barber Aquifer Protection Section cc: Fayetteville Regional Office, Aquifer Protection Section WQ0014868 Permit File WQ0014868 Notebook File Bladen County Health Department Technical Assistance and Certification Unit AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699.1636 Location, 2728 Capital Boulevard. Raleigh, North Carolina 27604 Phone: 919-733.3221 1 FAX 1: 919.715-0588; FAX 2: 919-715-60481 Customer Service: 1-877-623-6748 Internet: www.ncwalerauality.org An Equal 6pponunny %AtfirmaliveAcVon Employer 011C NorthQuolina 4 NCDENR North Carolina Department of Environment and Division of Water Quality Beverly Eaves Perdue Coleen H, Sullins Governor Director March 10, 2010 Mr. Larry Johnson, General Manager Smithfield Packing Company — Tar Heel Plant P.O. Box 99 Tar Heel, North Carolina 28392 Dear Mr. Johnson: SCANNED Natl DATE: /L /1 S Dee Freeman Secretary RECEIVED / DENR / DWQ Aquifer Protection Section MAR 16 2010 Subject: Permit Extension Permit No. WQ0014868 Smithfield Packing Co. WWTP Land Application of Residual Solids (503 Exempt) Bladen County On August 5, 2009, Session Law 2009-406, entitled "An Approvals Affecting the Development of Real Property Within the Assembly and signed into law. The Act, known as the Permit 1 expiration date of certain government approvals and permits. For website ( http:/portal.ncdenr,org/web/wq/aps/lau#extension ) can bf affected DWQ permits. Act to Extend Certain Government State," was enacted by the General 3xtension Act of 2009, extends the dditional information, the following viewed to address this statute and Non -discharge permit, WQ0014868, issued by the Division of Water Quality falls within the scope of this Act and is therefore being extended until 31 July 2013. Please note per your permit, a renewal application must still be submitted six months in advance of the extended expiration date. If Smithfield Packing Company needs to modify, upgrade, retrofit infrastructure at this facility which would require modification of the permit; a permit application can be submitted for review and the necessary modified permit issued. If you have any questions regarding this letter, please contact Division staff in the Fayetteville Regional Office at (9 10) 433-3340 or Central Office at (919) 733-3221. Thank you in advance for your cooperation. Sincerely, .JJ►"� E4;IZ- Jim Barber Aquifer Protection Section cc: Fayetteville Regional Office, Aquifer Protection ,Section WQ0014868 Permit File WQ0014868 Notebook File Bladen County Health Department Technical Assistance and Certification Unit AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604 Phone: 919-733.3221 1 FAX 1: 919-715-0588; FAX 2: 919-715-6048 i Customer Service: 1-877-623-6748 One OneNohh�al"C?.�.111a Internet: v�uvw.ncuvate uali .o ���l,�ary +�� An Equal Opportunity 1 Affirmative Action Employer fL WATF Michael F. Easley, Governor Obwd C AI William G. Ross Jr., Secretary T North Carolina Department of Environment and Natural Resources Alan W, Klimek, P.E., Director Division of Water Quality September I5, 2008 RECEIVED / DENR 1 DVVQ Aquifer Protection Section MR. LARRY JOHNSON, GENERAL MANAGER SEP 19 2008 SMITHFIELD PACKING CO. — TAR HEEL PLANT PO Box 99 TAR HEEL, NORTH CAROLINA 28392 Subject: Attachment B Certification Permit No. WQ0014868 Smithfield Packing Co. Inc Tar Heel Plant Residuals Land Application Program (503 Exempt) Bladen County Dear Mr. Johnson: In accordance with your permit modification application package received on 25 July 2008 in the Fayetteville Regional Office, as well as the additional information received on 18 August 2008; we are forwarding herewith a modified Attachment B, certified I I September 2008 to the Smithfield Packing Company for the subject residuals land application program. This certification is being issued to modify Attachment B to: ♦ Approve of a new sites owned by Murdock Butler, David Canady and William Dunham in Bladen County; Vance Tyson in Cumberland and Hinton McCall King & Douglas Musse1white in Robeson County for land application of residuals under this program. These sites total 870.00 net acres as shown on the buffer maps prepared by EMA Resources, Inc, in the 25 July 2008 application. Please replace the existing Attachment B of Permit No. WQ0014868, previously certified on 26 August 2005 with this modified Attachment B. Note that only the vicinity and buffer maps for any new land application sites are attached to this modified Attachment B. It is the Permittee's responsibility to insure a complete permit is created by inserting this modified Attachment B (with vicinity and buffer maps) into Permit No. WQ0014868 issued on 26 August 2005 and making sure to retain any vicinity and buffer maps for any existing and unmodified land application sites. This modified Attachment B shall be effective from the date of certification until 31 July 2010; shall void Attachment B of ,Permit No. WQ0014868, that was previously certified on 26 August 2005 and shall be subject to the conditions and limitations as specified therein and well as those specified in the above -referenced permit. As always, remember to take the time to review this modified Attachment B thoroughly, as some of the conditions contained therein may have been changed since the last certification. Note that this modified Attachment B is hereby incorporated by reference into Permit No. WQ0014868 issued on 26 August 2005. Nor Carolina Ivatcrra!!y Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Phone (919) 733-3221 Customer Service www.ncwaterquality.org 2728 Capital Boulevard Raleigh, NC 27604 Fax (919) 715-0588 1-877-623-6748 Fax (919) 715-6048 An Equal Opportunity/Affirmative Action Employer — 50% Recycled/10% Post Consumer Paper WQ0014868 15 September 2008 Page Two If any parts, requirements, and/or limitations contained in this certification or modified Attachment B are unacceptable, you have the right to request an adjudicatory hearing upon written request within 30 days following receipt of the certification. This request shall be in the from of a written petition, conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need any additional information concerning this matter, please contact Jim Barber by telephone at 910-433-3340 or via e-mail atjim.barbet@ncmail.net Sincerely, 3 ,for Cole H. Sullins, Director cc: EMA Resources Inc. — Roy Whitaker Bladen County Health Department Cumberland County Health Department Robeson County Health Department Jeff Musselwhite — Smithfield Tar Heel Plant Environmental Manager APS FRO Files: Smithfield Packing Co. WQ0014868 APS Central Files — Raleigh Central Office APS LAU Files: Ed Hardee ATTACHMENT B - Approved Land Application Sites Permit Number: WQ0014868 Version, 2.10 Smithfield Packing Company Inc Smithfield Packing (Tar Heel Division) Field/Zone Id owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Condition IVA Restriction SFO1-01 SFOI-02 SFO1-03 SFO1-04 SF03-01 Smithfield Packing Company, Inc. Smithfield Packing Company, Inc. Smithfield Packing Company, Inc. Smithfield Packing Company, Inc. IDunham, William Dunham, Steve Bladen Bladen Bladed Bladen Bladen 34045'51" 34045'39" 34045'27" 34°45'29" 34'44'06" 78048'22" 78048'18" 78`4F10" 78048-22" 78°43'07" 22.50 14.00 31.10 18.00 21.60 Norfolk Norfolk Norfolk Rains Lakeland GW-,q GW-B GW-A GW-B GW-A SF03-02 Dunham, William Dunham, Steve Bladen 34044'15" 78043'12" 13.30 Centenary GW-B SF03-03 SF03-04 Dunham. William Dunham, William Dunham, Steve Dunham, Steve Bladen Bladen 34044'18" 34044'12" 78°43'20" 78043'26" 21.30 19.00 Centenary Wasda GW-A GW-A SF03-05 Dunham, William Dunham, Steve Bladen 34°44'08" 78`43'21" 8.00 Lakeland GW-A SF03-06 Dunham, William Dunham, Steve Bladen 34044'02" 78°43'33" 32.00 Lakeland GW-A SF03-07 Dunham, William Dunham, Steve Bladen 34043'28" 78044'21" 37.20 Wickham GW-B SF03-08 Dunham, William Bladen 34043'46" 78044'01" 41.00 Wickham fine sandy loam, I to 6% slopes GW-A SF04-04 Patterson, Russell Bladen 34'48'39" 78`51'13" 9.00 Norfolk GW-A SF04-05 Patterson, Russell Bladen 34°48'33" 78050-05" 8.60 Norfolk GW-A SF04-06 Patterson, Russell Bladen 34048'23" 78049'42" 13.50 Norfolk GW-B SF04-07 Patterson, Russell Bladen 34048'20" 78'49'55" 15.00 Norfolk GW-A SF04-08 Patterson, Russell Bladen 34048'09" 78'49'57" 25.80 Norfolk GW-A SF04-09 Patterson, Russell Bladen 34`47'59" 78°50'03" 12.60 Norfolk GW-A SF04-10 Patterson, Russell Bladen 34°48'01" 78°50'13" 2L50 Norfolk GW-A SF06-01 Tyson, Vance Bladen 34'55'49" 78051-03" 5.50 Autryville GW-A SF06-02 SF06-03 Tyson, Vance Tyson, Vance Bladen Bladen 34°55'42" 34°55'38" 78051'03" 78-50-21" 31.10 64.50 Autryville Autryville GW-A GW-B SF07-01 Burney, J W Bladen 34-4311" 78-44-26" 21.80 Altavista GW-B SF07-03 Burney, J W Bladen 34°43'15" 78°44'10" 12.30 Altavista GW-B 5F07-06 Burney, J W Bladen 34043'29" 78043'53" 19.30 Wickham GW-A SF07-08 Burney, J W Bladen 34'43'37" 78'43'44" 12.10 Altavista GW-A SF07-09 Burney, J F Bladen 34°43'44" 78043'44" 21.30 Wickham GW-A SF07-14 Burney, J F Bladen 34°43'55" 7804327" 7.50 Lakeland GW-B SF07-15 Burney, J F Bladen 34043'51" 78043'41" 3.00 Lakeland Gw-B SF10-01 Butler, Murdock M Bladen 34046'32" 78'49'19" 53.00 Norfolk loamy fine sand, 0 to 2% slopes GW-A SFI 0-02 Butler, Murdock M Bladen 34'47'30" 78°49'48" 45.00 Autryville GW-A SFIO-03 Butler, Murdock M Bladen 34°47'23" 78049'54" 31.00 Norfolk loamy fine sand, 0 to 2% slopes GW-A SF12-01 Canady, David S Bladen 34°48'19" 1 78°5F46" 49.00 Norfolk loamy fine sand, 0 to 2% slopes GW-A COUNTY 'TOTAL BLA ID EN 761-40 Permit No. WQ0014868 1 Certification Date: 09/11/2008 SF06-04 Tyson, Vance U Cumberland 34°55'43" 78°50'24" 35.00 Deloss loam GW-B SF06-05 Tyson, Vance U Cumberland 34°55'48" 78050'14" 34.00 Deloss loam GW-B SF06-06 Tyson, Vance Cumberland 34°55'29" 78°50'14" 79.00 Deloss loam GW-B SF06-07 Tyson, Vance Cumberland 34"55'50" 78049'41" 77.00 Deloss loam GW-B COUNTY TOTAL CUMBERLAND 225.00 SF08-01 King, Hinton McCall Robeson 34, 44'50" 78053'29" 7.50 Goldsboro loamy sand, 0 to 2% slopes GW-A SF08-02 King, Hinton McCall Robeson 34044'44" 78'53'21" 17.00 Goldsboro loamy sand, 0 to 2% slopes GW-A SF08-03 King, Hinton McCall Robeson 34'45'01" 78053,121, 89.50 Marlboro sandy loam, 0 to 2% slopes GW-A SF08-04 King, Hinton McCall Robeson 34'43' 18" 78*55'15" 64.50 Norfolk loamy sand, 0 to 2% slopes GW-A SF08-05 King, Hinton McCall Robeson 34043'22" 78°56'02" 46.00 Goldsboro loamy sand, 0 to 2% slopes GW-A SF08-06 King, Hinton McCall Robeson 34043'50" 78056'00" 21.50 Norfolk loamy sand, 0 to 2% slopes GW-A SF08-07 King, Hinton McCall Robeson 34043'21" 78°56'47" 37.00 Goldsboro loamy sand, 0 to 2% slopes GW-A SF08-09 King, Hinton McCall Robeson 3404635" 78058'06" 45.00 Comille loam GW-B SF09-01a Musselwhite, Douglas Robeson 34-47-40" 78°55'56" 36.00 Wagram loamy sand, 0 to 6% slopes GW-A SF09-02a Musselwhite, Douglas Robeson 34-47-49" 78°56'06" 27.50 Goldsboro loamy sand, 0 to 2% slopes GW-A SF09-03 Musselwhite, Douglas Robeson 34*47'21" 78055'53" 9.50 Wagram loamy sand, 0 to 6%slopes GW-A SF09-04 Musselwhite, Douglas Robeson 34047'12" 78055'59" 25.00 Wa am loamy sand., 0 to 6%slopes GW-A CO UNTX 'TOTAL ROBESON 426-00 Total I 1,412.40 A reduced buffer of 200' has been approved for residences under separate ownership along Barker Ten We road for this land application field due to the proposal for residuals to be injected on Field SF09-01. A reduced buffer of 200' has been approved for residences under separate ownership along Hwy 20 for this land application field due to the proposal for residuals to be injected on Field SF09-02. Permit No. WQ0014868 2 Certification Date: 09/1 112008 SUE LUC;ATIUN MAY MURDOCK BUTLER x 'x_ p 1" = 3,906.3 ft Data Zoom 12-1 SF 10-01,02,03 s, Inc. I e,,j� :Y�Y' ➢ �Nv owner: &R�>oc.K bu�i E,g Scale: l = Y00 Site: S r1 o Field #: 09 Legend: Total Acres: S..S Applicable Acres: V�ro lL , -Stream -Slope/Buffer -Slope/Buffer -Drainage -Application Area 11 -House/Building (9) -Rock Outcrop 0 -Well © -Soil Boring (E)-Pond/Water -Unsuitable Soils ,.--- -Fence -Forested Area —Resources, Inc. ,I l , i Y 11. _! Owner: Pu0oc1S U7«R Scale:l"= qoo Site: 6F10 Field #: b 3 Total Acres: licable Acres: 3 1, o Legend: -Stream -Slope/Buffer -Drainage -Application .Area -House/Building -Well -Pond[Water -Fence -Rock Outcrop -Soil ]Boring -Unsuitable Soils -Forested Area Street Atlas USAO12007 Plus A v AVE �. P �J �f nux�nxxunxw�nxx�+iwxr �_ XV�1HIpiPBw�iNF&�1 ��iW ip ira�w;arnwiwi � . 4�� 87 DR ALTER , i � QKQ l( g CUSTQN RD � , r 20 20 l'�Buies Neck Ln v ('unp 'L Cuk� Rb :i OL( "�gi"x"mM«nr„x�n + i i\\ CDG i i VERSAW CIR O f TOtarsville \ C'drn._ i --Y--------------------- I_ SITE LOCATION MAP "H Scale 1 : 46,875 o DAVID S. CANADY A k f 1'h z 0fj SP 12-01 1 ° = 3,906,3 ft Data Zoom 12-1 A ,Resources. Inc. APPLICATION AREA MAP Owner: ��u�, S. �s 7Y. Scale: I"= Q Site: S� Field #: O i Total Acres: S— . Q Applicable -Acres: Legend: -Stream-House/Building -Rock Outcrop -Slope/Buffer -Well -Soil Boring -Drainage-Pond/Water -Unsuitable Soils -Application Area -Fence -Forested Area Street Atlas USA® 2007 Plus ESQ m N 53 TAR1+��L F�R�Y C[?OSSING o� . G py P White Oak apRNf� RD 5� 15 HILL LN P � f 2nIV ro A. YMy Tar Heel �? r Heel SF6&OS g�R��Ro 53 - • 8u ney ' 87 131 (tn rF• qy �O 2 JAG? p0 pl�G� GRIMES SINGI ETARY�RD J¢ 07 �2 F� TM Scale 1 : 46,875 SITE LOCATION MAP Y ,yiil� 9 x tx 2 W. DUNHAM & ANN DUNN 1 = SF03-08 s,sos.s tt Data Zoom 12-1 APPLICATION AREA MAP Owner: �TA"A_m "bu,Kw,% 4- AMN 1 1 "oj es, Inc. Scale: l "= qgo Site: _,�5F"03 Field #: D Total Acres: .S Applicable Acres: 0 Legend: ----Stream -Slope/Buffer �--- --� -Drainage -Application Area 11 -House/Building -Rock Outcrop 0 -Well p -Soil Boring (2)-Pond/Water JAMARt- -Unsuitable Soils --- -Fence CD -Forested Area 5 03 an a KING HlRAMhD -A c/c, 0 A p ,,Vtlo ,so Ap Jj7 Z C5, �ap ol 13tS All p Ok I-V T RI- pTli DR '-'r'R'CJA'DR v op DIR _j BEA AMP DR r ALLIANCE s-r � ; A 1�,'yd dW�tlt .... z,1-" • � ��oa� 1 � , are; y0 �.�`:, ,_/ f � \ apy"') lop cli. rn as zl)De! -10 N, � aR -llk 101 � vo lop -60 to k ld(k3'�l DIMS "da -SH;aR61 INIVS ---,—A,3- S ST APPLICATION AREA MAP a Owner: _ gtrcc l so/l, Scale: I"= qoo Site: SFo(o Field #: 0 Total Acres: 38.® Applicable Acres: 3,. o Legend: �ti 6 -,--Stream -SlopeMuffer -- -Drainage -Application Area Inc, 19 -House/Building. 0 -Rock Outcrop 'f -Well © -Soil Boring 0-Pond/Water --%W -Unsuitable Soils -„- -Fence �ZD -Forested Area --Resources, Inc, APPLICATION AREA MAP Owner: Scale:Site: Field #: 05- Total Acres: 3 % a Applicable Acres: Legend: /-Stream -Slope/Buffer -Drainage -Application Area .3 51o 0-House/Building (9) -Rock Outcrop -Well © -Soil Boring -Pond/Water J-2265tr -Unsuitable Soils x--,v -Fence CD -Forested Area. m Street Atlas USA& 2007 Plus ST SF08.09 �cf`Y IQ �4 � Q iRig,R� 1 .y Q' +P �N CN RO GREAT NfRRi $Fff&d8 TM SITE LOCATION MAP IENTON McCALL KING SF08-01,02,03,04,05,06,071*09 —im RD i fJ � 2 t't pp iBules Necit ` � w z `+ o a w I el w� 4� Cw1P�RD SF08-01,02,03 r5 _fALlNA@E R[ �.i po �4 .y r, Scale i . 46,875 s w x x + V = 3,906.3 ft Data Zoom 12-1 APPLICATION AREA MAP Owner: Psrj-roN AV',C� zNcr __-- Scale:l"= qoo ' Site: 5FDa Field #: 0 I Total Acres: $ Applicable Acres: %. .- Legend: --Slope/Buffer --- = -- -Drainage -Application Area Inc. it -House/Building ( -Rock Outcrop 0 -well © -Soil Boring -Pond/Water _V%RF -Unsuitable Soils ,x—* * -Fence CD -Forested Area Inc. APPLICATION AREA MAP Owner:- AzIj -;"0& KC-4 I-L k�,,) C, Scale:l" _ qpo " _ Site: Sro ? Field #: Da Total Acres: /9. o Applicable Acres: /Z o Legend: -o"---Stream -Slope/Buffer --� -Drainage -Application Area 0-House/Building & -Rock Outcrop fi� -Well © -Soil Boring -PondlWater -Unsuitable Soils -x - — -Fence CD -Forested Area Inc. A PPIAC A'T'ION AREA MAP Owner: �V�J_folv Mc ac. Scale: I,,— qoc> ' Site: 5r_0 S Field #: 03 Total Acres: 7 o Applicable Acres:_ 469. S Legend: �.� .. • -/'--Stream 11 -House/Building ® -bock Outcrop -Slope/Buffer fiJ -Well ® -Soil Boring Drainage (E)-Pond/Water _�MW -Unsuitable Soils -Application Area -Fence 4ZD -Forested Area A nInW W d" ♦ tnXE1Ar ■ "171 A A S A _n Owner: Ac CAS 66)U Scale:1 "= 0 Site: s, Inc. SFo g Field #: 041 Total Acres: 6 2. ® Applicable Acres: 6 q.-5- Legend: �_ • -/�_-Stream -Slope/Buffer -- -•-� -Drainage -Application Area 0-House/Building. (9) Rock Outcrop 0 -Well © -Soil Boring (E)-Pond/Water -Unsuitable Soils x--.Y, * -Fence -Forested Area APP1,1CATION ARF,A MAP Owner: t A :,Q Cr Field #: b.' Total Acres: Legend: -Slope/Buffer --�— —�- -Drainage -Application Area Inc. Scale:l"= qoo Site: 5 Fo � �d • 6 Applicable Acres: V(o , O JS -House/Building 0 -Rock Outcrop fi� -Well © -Soil Boring Q-PondlWater -Unsuitable Soils 4_4t_-� -Fence = -Forested Area Inc. %,PP LICATIONN AREA MAP Owner: sr•►Tonl Mxa« Scale:l"= qoo ' Site: S P:-o S Field #: 0& Total Acres: .0 Applicable Acres:/ S Legend: -/---Stream 11 -House/Building -Rock Outcrop -SlopeBufFer 0 -Well Q -Soil Boring --4- ° --= -Drainage 0-Pond/Water -Unsuitable Soils -Application Area -,.— * -Fence Forested Area Inc. MPLA�C_'ATIOPT AREA MA? Owner:- N%a« )6�Lj& Scale:P= qao' Site: Fog Field #: 07 Total Acres: �1/ 0 Applicable Acres: Legend: .. 8 _Stream P-House/Building -Rock Outcrop -Slope/Buffer -well ® -Soil Boring -Drainage -Pon ater -Unsuitable Soils Application Area ._Fence -Forested. Area Inc. APPLICATION AREA MAP f%R F „wl'.tn4 c: •. } - r - -.°. •acw \ II Owner: Y7 *4i- kCAQ C46- Scale:I"= q00 Site: FO8 Field #: 7 Total Acres: 5//. D Applicable Acres:___ 3_7 D Legend: lL • �-Stream 19 -House/Building (9) -Rock Outcrop -Slope/Buffer fiJ -Well © -Soil Boring --- ° ---= -Drainage Q-PondlWater -Unsuitable Soils -Application Area -Fence CD -Forested Area APPLICATION AREA MAP UP '-Resources, Inc. w Ir Owner: Y__rf1j_7_01J A-CPLL G Scale: l "= Ltoo ° Site: .5 F-b -z� Field #: 0�3 Total Acres: 'F.S Applicable Acres: 7-5- Legend: -'---Stream -Slope/Buffer -Ehainage -Application Area 19 -House/Building 0 -Rock Outcrop gl -Well a -Soil Boring -Pond/Water -Unsuitable Soils 4--w-Y- -Fence 4f� -Forested Area Inc. UFLICATION AREA MAP r � Owner: 9xaToN cCACC K z�G Scale:l."= qoof Site: SF-d S Field #: 09 Total Acres: �90 Applicable Acres: LS, D Legend: —_Stream -Slope/Buffer ---- ° —� -Drainage -Application Area ■-House/Building (9) -Rock Outcrop fi� -Well ® -Soil Boring --Pond/Water __AVRr- -Unsuitable Soils — - -Fence �= -Forested Area Ago N� 6 4� 45 A DR Ac� 0 SITE LOCATION MAP DOUGLAS MUSSELWME SF09-01,02,03,04 Street Atlas USAG 2007 Plus )rse Neck V Scale 1'. 31,250 204.2 ft Data Zoo APPLICATION AREA MAP 10 _F 44, XX ,r,4 x 6-1 x X Owner: o(,tccq:s U55C-CWKZ7C- Field #: 0 1 Total Acres: Legend: --,"-Stream -Slope/Buffer -Drainage -Application Area Inc. Scale: I "= q-oo' Site: 5P-09 qo.o Applicable Acres: 3 ( ,. C 11 -House/Building @ -Rock Outcrop ,0 -Well 0 -Soil Boring (2)-Pond/Water -Unsuitable Soils -Fence -Forested Area Inc. APPLICATION AREA MAP Owner: - s yr Scale:1 qcor Site: SF-4 ? Field #: 0,2 Total Acres: 3 I.O Applicable Acres: '� 7-5— Legend: �-Stream -Slope/Buffer y --= -Drainage -Application Area 11-House/Building (9) -Rock Outcrop -Well © -Soil Boring -Pond/Water -Unsuitable Soils 4-*-* -Pence CD -Forested Area A l LICATION AREA MAP 0 Inc. k T. N,�.Y, `-. tx•• ;x, �. �•'i`..r 1'SJ._� Its =� S _+.��.L�3�. i.,S:id-_� u _ '-.f_ Owner: bOUCCA.5 Scale:l = qco ' Site: Sro9 Field #: 03 Total Acres: O-S Applicable Acres: Legend: f -Stream -Slope/Buffer ---- --= -Drainage -Application Area 9.s 0-House/BuMmg Q -Rock Outcrop jor -Well © -Soil Boring -Pond/Water -Unsuitable Soils 4-4--o- -Fence CD -Forested Area APPLICATION AREA MAP Owner: I J0(AG A_5 mussC-cw��r '—Resources, Inc. .,� I a x . e- LU Old t ff,T R �f ib Scale: F'= 40b Site: S Fo 9 Field #: O q Total Acres: 6,0 Applicable Acres: S o Legend: I -Stream -Slope/Buffer --� -Drainage -Application Area it -HouseBuilding ( -Rock Outcrop j0 -Well p -Soil Boring (2)-Pond/Water JMME- -Unsuitable Soils — - v -Fence CD -Forested Area 0�0V V4 A 7-ER 'G } co i— a � Michael F. Easley. Governor William G. Ross Jr., Secretary North Carolina Depar£rnent of Environment and Natural Resources August 26, 2005 MR. LARRY JOHNSON, GENERAL MANAGER, TAP, HEEL PLANT SMITHFIELD PACKING COMPANY, INC. POST OFFICE Box 99 TAR HEEL, NC 28392 Dear Mr, Johnson: Alan W. Klimek, P.E. Director Division of Water Quality Subject: Permit No. WQ0014868 Smithfield Packing Company, Inc. Tar Heel, NC Division Residuals Land Application Program Land Application of Residual Solids (503 Exempt) Bladen County In accordance with your permit renewal request received on August 30, 2002 as well as additional information received on September 7, 2002 and July 17, 2003; we are forwarding herewith a renewed Permit No. WQ0014968, dated August 26, 2005, to Smithfield Packing Company, Inc. for the subject residuals land application program. This permit shall be effective from the date of issuance until July 31, 2010; shall void Permit No. WQ0014868, issued to Smithfield Packing Company, Inc. on October 30, 1998; and shall be subject to the conditions and limitations as specified therein. Make note of this permit's expiration date and the fact that a permit renewal application is due to the Division of Water Quality (Division) no later than six months prior to that date (i.e., see Condition VI. 7.), as the Division does not send reminders to apply for permit renewal. This permit approves the continued operation of the residuals land application program for another five-year cycle. At your request, several land application sites totaling 356.5 acres permitted in the previous issuance of this permit are being deleted in this issuance. As always, remember to take the time to review this permit thoroughly, as some of the conditions contained therein may have been added, changed, or deleted since the last issuance. Pay particular attention to the monitoring requirements in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. If any parts, requirements, and/or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within 30 days follovring receipt of this permit. This request shall be in the from of a written petition, conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such demands are made, this permit shall be final and binding. Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Internet: htip:A. 12o.em.swe.nc.us 2728 Capital Boulevard Raleigh, NC 27604 NorthCaralina Phone (919) 733.3221 Customer Service A?[Zwrally Fax (919) 715-0588 1-877-623-6749 Fax (919) 715-6049 An Equal OpponunilylAffirmative Action Employer— 50% Recycled110'A Posl Consumer Paper Mr. Larry Johnson August 26, 2005 Page 2 If you need any additional information concerning this platter, please contact i1�Ir. J. R. Joshi by telephone at (919) 715-6698, or via e-mail at jaya joshi@ncrnail.net. Sincerely for Alan W. Klimek, P.E. cc: Bionomic Services, Inc.; 516 Roundtree Road, Charlotte, NC 28217-2133 Bladen County Health Department Sampson County Health Department Mooresville Regional Office -Aquifer Protection Section Technical Assistance and Certification Unit APS Central Files APS Piles LAU Residuals Program Coordinator NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF RESIDUAL SOLIDS (503 EXEMPT) PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Smithfield Packing Company, Inc. Bladen County FOR THE continued operation of a residuals land application program consisting of the application of residuals generated by the residuals source -generating facilities listed in the most recently -certified Attachment A to the land application sites listed in the most recently -certified Attachment B with no discharge of wastes to surface waters, pursuant to your permit renewal request received on August 30, 2002 as well as additional information received on September 7, 2002 and July 17, 2003; and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until July 31, 2010; shall void Permit No. WQ0014868, issued to Smithfield Packing Company, Inc. on October 30, 1998; and shall be subject to the following specified conditions and limitations. 1. PERFORMANCE STANDARDS The residuals land application program shall be effectively maintained and operated as a non - discharge system to prevent the discharge of any wastes resulting from the operation of this program. 2. This permit shall become voidable if the soils of the land application sites fail to assimilate the residuals adequately and may be rescinded unless the land application sites are maintained and operated in a manner that will protect the assigned water quality standards of the surface waters and groundwater. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface waters or groundwater resulting from the operation of this residuals land application program. In the event that the residuals land application program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall cease land applying residuals to the site, contact the Aquifer Protection Section of the appropriate Division of Water Quality's (Division) regional office, and take any immediate corrective actions as may be required by the Division. Only the land application sites listed in the most recently -certified Attachment B of this permit are approved for residuals land application. When wastewater residuals are applied, the Class B pathogen requirements as defined in 40 CFR Part 503 or the Process to Significantly Reduced Pathogens (PSRP) as defined in 40 CFR Part 257 Appendix 11 shall be met. Additionally, an evaluation shall be performed which demonstrates the ability of the residuals to comply with this requirement. Upon request, a copy of this evaluation shall be submitted including all test results and calculations. When residuals from an animal processing facility are being land applied, one of the following shall be completed to control possible nuisance conditions: a. Subsurface injection of the residuals, b. Incorporation of the residuals into the soil within 24 hours of the application event, or c. Addition of sufficient lime to the residuals to create a uniform mixture and maintain a pH of 10 for a 30-minute period prior to being surface land applied. IX. OPERATION AND MAINTENANCE REQUIREMENTS 1. The facilities and land application sites shall be properly maintained and operated at all times. 2. Upon classification of the residuals land application program by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall designate a certified land application/residuals operator to be in responsible charge (ORC) of the program. The operator shall hold a certificate of the type classification assigned to the program by the WPCSOCC. The Permittee shall also designate a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8G .0202. 3. No residuals shall be stored at any land application site at any time, unless written approval has first been requested and obtained from the Division. 4. A copy of this permit shall be maintained in all manned equipment at the land application sites when residuals are being land applied during the life of this permit. A spill prevention and control plan shall be maintained in all residuals transport and application vehicles. 5. When land applying residuals to any land application site, the following buffer zones shall be maintained at all times: 400 feet from residences or places of public assembly under separate ownership for surface application methods; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the Aquifer Protection Section of the Mooresville Regional Office; K b. 200 feet from residences or places of public assembly under separate ownership for subsurface application methods; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the Aquifer Protection Section of the Mooresville Regional Office; 100 feet from any public or private water supply source, waters classified as SA or SB, and any Class I or Class Il impounded reservoir used as a source of drinking water for both methods, d. 100 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for surface application; e. 50 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for subsurface application; f. 50 feet from property lines for both surface and subsurface application methods; g. 50 feet from public right of ways for both surface and subsurface application methods; h. 10 feet from upslope interceptor drains and surface water diversions for both surface and subsurface application methods; and i. 25 feet from downslope interceptor drains, surface water diversions, groundwater drainage systems, and surface drainage ditches for both surface and subsurface application methods. 6. Maximum slope for land application of residuals shall be 10 percent for surface application methods and 18 percent for subsurface application methods. Specific residuals land application area boundaries shall be clearly marked on each land application site prior to and during a residuals land application event. 8. The lifetime loading rates (LLRs) of heavy metal loadings rates on any land application site shall not exceed the following for the corresponding soil cation exchange capacities (CEC): Parameter LLR for a Site with CFCs <5 (pounds per acre LLR for a Site with CECs 5 to 15 (pounds per acre) LLR for a Site with CECs >15 (pounds per acre) Cadmium 4.5 9 18 Copper 125 250 500 Lead 500 1,000 2,000 Nickel 125 250 500 Zinc 250 500 1,000 9. An acceptable pH shall be maintained in the soil, greater than 6.0, on all land application sites onto which residuals are land applied to ensure optimum yield for the crops specified in Condition U. 13. The agronomist shall provide information on the pH best suited for the specified crop and the soil type. 10. Should any of the residuals to be land applied contain a high salt content (i.e., high sodium adsorption ratio (SAR) of five or higher), the exchangeable sodium percentage (ESP) or other method as approved by the Division, using the results from the annual soils analysis as required by this permit, shall be monitored on all of the land application sites. The local Cooperative Extension Office, the Department of Agriculture and Consumer Services. the Natural Resource Conservation Service, a North Carol ina-Iicensed Soil Scientist; or other agronomist shall review the results and make recommendations regarding soil amendments (e.g., gypsum, etc.) or other ameliorative mechanism for maintaining the integrity of the site in terms of suitability for land application of residuals and maintaining conditions conducive to crop growth. The Permittee shall implement such recommendations accordingly and shall maintain written records of each monitoring event that includes details of the sites covered and rate of soil amendment application. 11. The Permittee shall be responsible for verifying the volume of residuals that may be land applied to the site such that the plant available nitrogen (PAN) loading rate for the specified crop (i.e., see Condition II. 13.) shall not be exceeded by all of the sources of PAN applied. Should the maximum PAN loading rate be met or exceeded, then no additional residuals shall be land applied to the site. 12. A suitable vegetative cover shall be maintained on land application sites onto which residuals are land applied in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist and as approved by the Division. 13. Residuals and other sources of PAN shall be land applied to all land application sites at agronomic rates in accordance with the crop management plan outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. Under no circumstances shall the following PAN loading rates land applied to any site exceed the following for the specified crops: PAN PAN Crop (pounds per Crop (pounds per acre er ear) acre per year) Alfalfa 200 Forest 75 (Hardwood or Softwood) Bermuda Grass 220 Milo 100 (Hay or Pasture) BIue Grass 120 Small Grain 100 (Wheat, Barley, or Oats) Corn 160 Sorghum or Sudex 180 (Grain) (Pasture) Corn 200 Sorghum or Sudex 220 (Silage) (Silage) Cotton 70 Soybeans 200 Fescue 250 Timothy, Orchard, or 200 Rye Grasses The Permittee shall apply for and receive a modification of this permit before Iand applying residuals on any land application site that is to be established in a crop other than those listed above. A maximum PAN loading rate for the desired crop shall be approved with the permit modification. If the land application sites are to be overseeded (e.g., bermuda grass in the summer and rye gxuass in the winter with BOTH crops to receive residuals), then the second crop shall receive an application of PAN at a rate of no greater than 50 pounds per acre per year. This practice shall be allowed as long as the second crop is to be harvested. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no residuals shall be land applied to these sites because the PAN ,,vill essentially be returned to the soil. Residuals shall not be land applied at rates greater than agronomic rates, unless authorized by the Division. 14. Animals shall not be grazed on any land application site for 30 days after any residuals land application event. Sites that are to be used for grazing shall have fencing that will be used to prevent access after each event. 15. Food crops, feed crops, and fiber crops that do not come in contact with the residuals shall not be harvested for 30 days after any residuals land application event. 16. Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) shall not be harvested for 14 months after any residuals Iand application event. 17. Food crops with harvested parts below the surface of the land (i.e., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for 20 months after any residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 18. Food crops with harvested parts belo.v the surface of the land shall not be harvested for 38 months after any residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 19. Turf shall not be harvested for one year after any residuals land application event. 20. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into any surface waters. Disking, seeding and other tillage operations on the land application sites shall be performed following the land contours to aid in controlling channeling of storm water. 21. Adequate procedures shall be provided to prevent surface runoff from carrying any land applied or stored residuals into any surface waters. 22. Surface -applied residuals shall be plowed or disced within 24 hours after land application on land application sites with no cover crop established. 23. For land application sites that are prone to flooding or within the 100-year flood elevation, residuals shall be land applied only during periods of dry weather. The residuals shall be incorporated into the soil within 24 hours after land application. 24. Residuals shall not be land applied during inclement weather or until 24 hours following a rainfall event of 0.5-inch or greater in 24 hours. Any emergency residuals land application measures shall first be approved in writing by the Division. 25. Residuals shall not be land applied to any land application site that is flooded, frozen, or snow-covered. 26. Appropriate measures shall be taken to control public access to the land application sites during active site use and for the 12-month period following the last residuals land application event. Such controls may include the posting of signs indicating the activities being conducted at each site. III. MONITORING AND REPORTING REQUIREMENTS Anyt monitoring (i.e., including groundwater, surface water, residuals, soil, or plant tissue '.S T]A 1�lCPC� IIPPTYfPI{ 3'7P�PCc9 T\f �1�1 tl'lP Ti��rt��`ln {'n Pn �lulrP nr��u�tiLrr,f tti.o o 3..,11 v ialiten" viil Jtiull established, and an acceptable sampling and reporting schedule shall be followed. 2. Residuals to be land applied shall be analyzed to demonstrate that they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). A corrosivity, ignitability, and reactivity analysis as well as a Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted on residuals to be land applied. The analyses shall be performed at the frequency specified in the most recently -certified Attachment A of this permit, and the results shall be maintained on file by the Permittee for a minimum of five years. If residuals generated by a particular residuals source -generating facility are land applied at a frequency less than that which is specified in the most recently -certified Attachment A of this permit, the analyses shall be required for each residuals land application event. Only residuals that are generated by the residuals source -generating facilities that are identified as being exempt from this condition in the most recently -certified Attachment A of this permit shall not be required to comply with this monitoring requirement. The TCLP analysis shall include the following parameters (i.e_, note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) o-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) 1,l-Dichloroethylene (0.7) Pyridine (5.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Endrin (0.02) Silver (5.0) Hexachlorobenzene (0.13) TetrachIoroethylene (0.7) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) Mercury (0.2) Vinyl chloride (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) After the residuals have been monitored as specified above for two years at an annual frequency or greater, the Permittee may submit a request to the Division for a permit modification to request a reduction of this monitoring requirement. In no case, however, shall the frequency of monitoring be less than once per permit cycle. 0 3. An analysis shall be conducted on residuals generated by each residuals source -generating facility listed in the most recently -certified Attachment A of this permit. The analysis shall be performed at the frequency specified in the most recently -certified Attachment A of this permit, and the results shall be maintained on file by the Permittee for a minimum of fire years. If residuals generated by a particular residuals source -generating facility are Iand applied at a frequency less than that which is specified in the most recently -certified Attachment A of this permit, an analysis shall be required for each residuals land application event. The analysis shall include, but shall not necessarily be limited to, the following parameters: Aluminum Potassium Ammonia -Nitrogen Nickel Cadmium 4 Nitrate -Nitrite Nitrogen Total Kjeldahl Nitrogen Percent Total Solids Zinc Copper PH Lead Phosphorus Plant Available Nitrogen (by calculation) After the residuals generated by a particular residuals source -generating operation have been monitored for two years at a frequency greater than annually, the Permittee may submit a request to the Division for a permit modification to reduce the frequency of this monitoring requirement. In no case, however, shall the frequency of this monitoring be less than once per year when a residuals land application event of residuals generated by the residuals source - generating facility occurs during that year. 4. Laboratory analyses as required by Condition 111. 2. and Condition 111. 3. shall be performed/gathered on the residuals as they are to be land applied. Furthermore, analytical determinations made pursuant to the monitoring and reporting requirements of this permit shall be made by a laboratory certified by the Division for the required parameter(s) under 15A NCAC 2H .0800 or 15A NCAC 2H .1100. 5. Proper records shall be maintained by the Permittee tracking all residuals Iand application events. These records shall include, but are not necessarily limited to, the following information: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number); d. Method of land application; e. Weather conditions (i.e., sunny, cloudy, raining, etc.); £ Soil conditions (i.e., dry, wet, frozen, etc.); g. Type of crop or crops to be grown on field; h. Volume of residuals land applied in gallons per acre, dry tons per acre, or kilograms per hectare; i. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or kilograms per hectare (if applicable); 7 j. Volume of soil amendments (i.e., lime, gypsum, etc.) applied in gallons per acre, dry ton per acre, or kilograms per hectare (if applicable); and lc. Annual and cumulative totals of dry tons per acre of residuals as well as animal waste and other sources of nutrients (i.e., if applicable), annual and cumulative pounds per acre of each heavy metal (Le., shall include, but shall not be limited to, cadmium, copper, lead, nickel, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each field. A representative annual soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site on which a residuals land application event in the respective calendar year has occurred, and the results shall be maintained on file by the Permittee for a minimum of five years. The Standard Soil Fertility Analvsi5 shall inclii6f-. hilt is not necessarily limited to, the following parameters: Acidity Exchangeable Sodium Percentage (by calculation) Calcium Magnesium Phosphorus Cation Exchange Capacity Manganese Potassium Copper Percent Humic Matter Sodium Base Saturation (by calculation) pH Zinc 7. All residuals included in this permit shall be monitored quarterly from the date of permit issuance, for compliance with Condition I. 6. and Condition I. 7. of this permit. Data to verify stabilization of the residuals shall be maintained by the Permittee. The required data shall be specific to the stabilization process utilized, but also shall be sufficient to demonstrate clear compliance with the Class B pathogen requirements as defined in 40 CFR Part 503 or the Process to Significantly Reduce Pathogens (PSRP) as defined in 40 CFR Part 257 Appendix II. Three copies of all required monitoring and reporting requirements as specified in Condition III. l., Condition III. 2., Condition III. 3., Condition III. 4., Condition III, 5., Condition III. 6., and Condition III. 7. shalI be submitted annually on or before March 1st of the year following the residuals land application event to the following address: NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 9. Noncompliance Notification: The Permittee shall report by telephone to the Aquifer Protection Section of the Division's Fayetteville Regional Office at telephone number (910) 496-1541, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the residuals land application program that results in the land application of significant amounts of residuals that are abnormal in quantity or characteristic. b. Any failure of the residuals land application program resulting in a release of material to receiving waters. Any time that self -monitoring information indicates that the residuals land application program has gone out of compliance with the conditions and limitations of this permit or the parameters on which the program system was designed. d. Any process unit failure, due to known or unknown reasons, that render the residuals land application program incapable of adequate residuals treatment. e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site. Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS Land Application Site Requirements: a. Each land application site identified with a GW-A in the most recently -certified Attachment B of this permit is dominated by soils with a mean seasonal high water table greater than three feet below the Iand surface. Residuals land application and reclaimed water irrigation events may occur on these sites throughout the year. b. Each land application site identified with a GW-B in the most recently -certified Attachment B of this permit is dominated by soils with a mean seasonal high water table between one and three feet below the land surface. Residual land application events on these sites shall be prohibited from December through March, inclusive. No residuals shall be ]arid applied to these sites when the vertical separation between the depth of residuals land application and the water table is less than three feet. 2. Applicable Boundary Requirements: a. The COMPLIANCE BOUNDARY for residuals Iand application progratns is specified by regulations in 15A NCAC 2L (i.e., "Groundwater Classifications and Standards"). The Compliance Boundary for each land application site is established at either 250 feet from the residuals land application area or 50 feet within the property boundary, whichever is closest to the residuals land application area. An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to inunediate remediation action according to 15A NCAC 2L .0106 (d)(2). b. The REVIEW BOUNDARY shall be established around each land application site midway between the Compliance Boundary and the perimeter of the residuals land application area. Any exceedance of Groundwater Quality Standards at the Review Boundary shall require action in accordance with 15A NCAC 2L .0106 (d)(2). Additional Requirements: a. Any additional groundwater quality monitoring, as deemed necessary by the Division, shall be provided. W V. INSPECTIONS Prior to each residuals land application event. the Permittee or his designee shall inspect the residuals storage, transport, and application facilities to prevent malfunctions and deterioration, operator errors, and discharges that may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Pernnittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority; upon request. Ali}% duly autizuriucu, offlWor, employee, or representative of rite Division may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the land application sites or facilities at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS This permit shall become voidable unless the residuals land application events are carried out in accordance with the conditions of this pernait, the supporting materials, and in the manner approved by the Division. 2. This permit shall be effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes § 143-215.6A through § 143-215.6C. 4. The annual administering and compliance fee shall be paid by the Permittee within 30 days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit; as specified by 15 NCAC 2H .0205 (c)(4). The issuance of this permit does not preclude the Permittee from, complying with any and all statutes, rules, regulations, or ordinances that may be imposed by other government agencies (i.e., local, state, and federal) which have jurisdiction, including, but not limited to, applicable river buffer rules in 15A NCAC 2B .0200, soil erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000, and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 15A NCAC .0500. 6. This permit may be modified, revoked, and/or reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to protect the environment and public health adequately. 10 The Permittee, at least six months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Division shall review the adequacy of the facilities and residuals land application program described therein, and if warranted, shall extend the permit for such period of time and under such conditions and limitations as it may deem appropriate - This permit shall not be automatically transferable. In the event that there is a desire for the residuals land application program to change ovmership or to change the name of the Permittee, a formal permit request shall be submitted to the Division documentation from the parties involved and other supporting materials as may be appropriate. The approval of this request shall be considered on its merits and may or may not be approved. Permit issued this the twenty-sixth day of August, 2005. NORTH CARMINA ENVD34NMENTAL MANAGEMENT COMMISSION Qr Alan W. Klimek, P.E.. Director Division of Water Quality By Authority of the Environmental Managemer t Commission Permit Number WQO-014868 ENS i Ock kA- "ter. MPS � 11 ATTACHM_EN_T A - Approved Residual Source -Generating Facilities Permit No. FVQ0014868 Sinithfteld Packing Company, Inc Tar heel, NC Division Residuals Land Application Prograin Owner Facility Name County Permit Issued Is 503? Maximum Monitoring Monitoring Approved ]Number BY DryTons Frequency for Frequency for Mineralization I Per Year Condition III. 2. Condiliou III.3. [fate Sinithriield Packing Company, Inc. Tarlieel Plant WWTP Bladen NC0078344 1)WQ non 503 2,050.00 Annually Every 60 days 0.20 Total I i i2,050.00 Permit No. WQ0014968 Page I of i Certification Date: August 26, 2005 U fJl ti ti L A N D C O U N T Y WM. O.N[/5KE k I•� .W'� LOCK AND DA yNHj T yl .a— ` tom! ti e nx L ` SITE SF4 RUSSELL PATTERSON T"Ar,] jlNLLE7ARY u]r ., - - uc] LANE � A u ,ygy � •, lio] BAKERS LAKE u ,m 3L' so \s1.1 1� t? 2• � is 15T F� 1 � 'µ ! 1p J •L l N L {' SITE SF3 STEVEN DUNHAM •� jLl .s 1�•. 1 `'ram SITE SFI SNHT1 FIELD PACKING �-- ' " `� /er �,f s+a s� � Y. , •k craw � _. i I�il i �M !• ] r � �1:3- it 1•? 9 ,]i, Irro � lul 'G PLANT LOCATION !V r lAle l,m �E L) �_S , _ w 1]fi Cn Ll7L x] ul ti „•:t - ].. SALTERS l 131 3s LIKE SITE SF7 JW AND JF BURNE) t2 ♦q Irfa 11 YAN III R v M—d- 0 all n 114 1191 •r' ., I,i .� eyY Yla t Pa.� • ♦ U11.Ifi+ F ll0 Z � tit r 11.1 yii �7i. 120 Q t'1v - t� lW >t,G• ., 4 �.. i ] •fir. .1 .] 1Nl + l 1 '� '] /•�rir ._ 1 H� 11.0. �iYrl Uj co W-2 Q LIID , 1 1NOLETARY I . of R J UU YONU 1 � T � 1r0 �1 .J a • Fir 11 ]. !Y \ l I][ ��• ry Itl1 � I 41 i1 •mil —70 11/Wlirp+ tY rf LIB61 'Is J . � It SMITHFIELD PACKING — TARHEEL DIVISION LAND APPLICATION PROGRAM (WQ0014868) FARM SITES - LOCATION MAP r 4 I] (Bladen County) - vm Scale 1 inch = approx. 2 miles CiL ` u L J �j trt t1Yt iulz �tA%� lil ATTACUMENT B - Approved Hand Application Sites Per»tit No. YYQ0014868 .Sndfhfield Packing Contpany,lttc. Tar Heel, NC Division .Residuals Land Application I'rogranr SiWField ID Landowner Lessee/Operator County latitude Longitude Net Acreage Applicable Restriction in Condition IV. 1, SFOI-01 Smithfield Packing Company, Inc. Maden 34045'51'° 78048'22" 22.50 QW-A SFOI-02 Smithfield Packing Company, Inc. Maden 34045-39" 78°48'1S" 14.00 CJW-I3 SFO1-03 Smithfield Packing Company, Inc. Maden 34'45'27" 7804S'10" 31.10 G W-A SFO1-04 Smithfield Packing Conlpairy, (nc. llladen 34045'29" 78'48'22" 18.00 GW-B SF03-01 Dunham, Jr., William Dunham, Steve llladen 34044'06" 7804TOT 21.60 GW-A SF03-02 Dunham, Jr., William Dunham, Steve ]]laden 34'44'15" 78043'12" 13.30 C;W I3 SF03-03 Dunham, Jr., William Dunham, Steve €]laden 34044'18" 78043'20" 21.30 GW-A 5F03-04 Dunham, Jr., William Dunham, Steve Illaden 34'44'12" 78°43'26" 19.00 GW-A SF03-05 Dunham, Jr., William Dunham, Steve Maden 34044'08" 78°43'21" 8.00 GW-A SF03-06 Dunham, Jr., William Dunham, Steve Illaden 34044106" 78°43`35" 32.00 C1W-A SF03-07 Dunham, Jr., William Dunham, Steve Maden 34°43'26" 78"43'26" 37.20 GW-B SF04-04 Patterson, Russell Maden 34'48'39" 7805I'l3" 9.00 GW-A SF04-05 Patterson, Russell ];laden 34048'33" 7F50'05" 8.60 CAW -A SF04-06 Patterson, Russell Bladen 34048'23" 78049'42" 13.50 GW-13 SF04-07 Patterson, Russell llladen 34°48'23" 78049'42" 15.00 GW-A SF04-08 Patterson, Russell I31ade❑ W48'09" 78049'57" 25.80 GW-A SF04-09 Patterson, Russell Maden 34°57'59" 78050'02" 12.60 OW -A SF04-10 Patterson, Russell Maden 34°47'59" 78°50'20" 21.50 GW-A 51`06-01 Tyson, Vance €]laden 34055'49" 7F5P03" 5.50 OW -A SF06-02 Tyson, Vance Maden 34055'42" 7905MY' 31.10 GW-A SF06-03 Tyson, Vance Illaden 34050'29" 78050'29" 64.50 GW-13 SF07-01 Burney, J W Illaden 34°4T11" W4426" 21.80 C1W-13 SF07-03 Burney, J W 111aden 34-43-15" 78-44'10" 12.30 (3W-B SF07-06 Burney, J W [.]laden. 34°43'29" 78'113'53" 19.30 GW-A SF07-08 Burney, J W Illaden 34043'37" 78043'44" 12.10 GW-A S11,07-09 Burney, J F Illaden 34043'44" 78043'44" 21.30 OW -A S1:07-14 Burney, J F I.iladen 34°43'55" 78043'27" 7,50 CYW-13 SF07-15 BUL-ney, J F 111aden 3404TS1" 7804341" 3.00 Gw-n Total For Cocrtzty Total f3larlen 542.40 542.41) Permit No. WQ0014868 Page 1 of 1 Certification Date: August 26, 2005 C U M S E; R L A N D C O U N T Y !1t7,f.O.HUSKE I _ I a LOCK AHP ut11H_ - I�A ° _. La—.. LITTLE SITE SF4 RUSSELL PATTERSON - SvYCLETARY E1" �. P LtixE •� 1 "Pr Aa r- •�_+ '� i4s JEJi BAKERS LAKE a •� nwr]. • + C) ! "- 3. r'' SITE SF3 STEVEN DUNHAM SITE SF1 SMITHFIELD PACKING 1 .Oak^_ r, �• :- AN 12j, J 1 ila PLANT LOCATION {' 9 e , t � Fit 11� � v L•� �.r k _ i5 f u sA1.rL'Rs' � •� lar au � Jwxe - _ SITE SFi JW AND JF BURNE) 1'a 1, 1 •�� .{' iAck :4•. .Ia LW _ sa suw.e.rw .! 'i ;y ...i., rs , L • �J '1 v :�r•. J .1 un 1F3 - It 1 1 ; ` w j- 131 m - im rNCLerARr �`� i LIU • POND A ui-_ J 1A ry4 ji" , J Itu 1190 nr a a �i� Jy u! ,us _10 —W1M ,ln Ur SMITHFIELD PACKING -- TARHEEL DIVISION ` LAND APPLICATION PROGRAM (WQ0014868) FARM SITES - LOCATION MAP ] (Blades County) 1 Seale cinch = approx. 2 miles + { r; rr�j: r� v Y n Eban,Lrrg'� bra Ch.. Is irn � I1 4 h 11! RESERVATION Olt,- J DMAT _ o aONHI£k 1 Ltf6 c o dOlWBAiV r r 5 TTT222I::-�. a�+ I-W ? �. c, C sFau Fw• f1t r ebl -a 11Irog ` FA`1LLF 1� i n BNnNSON E.� 8.] L] ! r� ,'I : .*: 4� '�` t � � �vwNOE1.� i41Rw �a' ��' rub •.q _ .r LLT �� w IQ4! - e1v ~r Ems. � m 14 'wu_ VI'erM1rille -p 72_ 9 Ali -i C6wb,d Municgof y �� w . •, 17 r°Cy � 1 0 Hart M{LLS FAI ;ZU 'Kr-S J FWD �L n^ L4ti a Cr 9 I3.i1 k l I d 192 ~ ` Y o, Sv ' 17� fist SITE SF6 VANCE TYSON S' 1q R— t 's 0 ,�^ Cyp,e,e Lvka ti i'.Z zm 73 �r 1 a. Tee. d,. ° ]01 91 * 93 a L Y'• zo to 1 Ii+ a nJ' A37 .v 1•7.` : "'�' 116' \ e7 = Vn:da C6. ZMV 1 v1.S 'r UD ! 3M o-.k tw L » 'zu;' .r Ch. _ 1E 2 1w. e _ 01L UR SMITHFIELD PACKING - TARHEEL DIVISION ° B L a LAND APPLICATION PROGRAM (WQ0014868) I N FARM SITES - LOCATION MAP 4 (Cumberland County) 42 Scale 1 inch = approx. 2 miles L U IVl b t M L IN a 1, U UHSEE v _ �' fn w�'n LDCIf aHD AhM L-L j Jl-IY ued„1r/ SITE SF4 RUSSELL PATTERSON :T "' L'�� SI GLE7'ARY LAKF Y. HORSESHOE BAKERS 4AK£ sj ^LAKE UL ]° CTk ?3U tw� SITE SF3 STEVEN DUNHAM SITE SF1 SMITHFIELD PACKING --s kpN ua} _ PLANT LOCATION "=' 'Luz V' � at JIr-� ., 2] 13, �•.. . r 1 Ir:. � S.fLTERS t a LAX£ SITE SF7 JW AND JF BURNED. 1.] sr LAi. I'll 1 iccvjti•'4�� L° r Rra v Mecdw+ 133. rnP i b l r 5 + 13:'_ Q -to wJaIM10N •I - J iA] , 1 r 1 .. -_II[ L •I ,] E7 ra Ll➢T — :m ` 'UM. — I O !=L 'jf ��"�° fill, {•-. INOLETARYn'- [� POND T AIM e r K r 111- 4 -f0 ]It .a-_- Lw r7 t •r '.r y lL'n I,i] Sandi'G.w. Ch - SMITHFIELD PACKING — TARHEEL DIVISION LAND APPLICATION PROGRAM (WQ0014868) o r� „ FARM SITES - LOCATION MAP 1 ' a ,,T (Bladen County) — ti Scale ai inch = approx. Z miles 1 ^'15.1 �, i � '-' -. ..'' '1't�'1•t•►. .trt � I Y.YS :.? ., fr.-.... r. F.a'^= •}:. r„_''�.,n �:' . i ySi:�S .i ,�S'ti "' � ' � .fr k`s �: _, ay_�"'tS .-r +•�.- Y � yaS. * '.. � r `� _�• f T f � r1 S : rll �' f �� � ,� ''^ �,. 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S y aY� - Y� � , .r!' ° r '- I- f I' 4 - ,r ., :t>� �`ii•r4..-I ,r. 1 � �1 Z; 1 _ •.iY�� VY � .�tiiti fr '-So 4 t( 5 tl I- �C /t1 c I< -� y7 ' � ° ' r n J r� ` •_. ;4rti••S ��.:. f._L_,r e, � /d-,... -y , a F..r`r�� r�-'J .r� x _ Ty � y r S„r* � 1. � � 3 •'L '�': SITE SFi SMITHFIELD PACKING Buffer Maps (Aug. 2002) AERIAL PHOTOGRAPH - FIELD FEATURES House/well Soil Boring (orange) (yellow) Buffer Area Water (stream or pond) 111 (red) ­__ (blue) r-7) r` C Field NirTi�_er (yellow) F of j R,--rd�_r (vallnv) Nt jr jr ` r Y' 3 It PC 1 V, r B •� Gr S rr but AV& 2oa1f5 -�U ?, j c3 SITE SF4 RUSSELL PATTERSON Buffer Maps (Aug. 2002) AERIAL PHOTOGRAPH - FIELD FEATURES of House/well Soil Boring �i (orange) (yellow) Buffer Area Water (stream or pond) CField Nurber (yellow) Field BcrLei l v�-1 1 nw ) 1--im _ ••�' •yam bL ti' ��.� � - _ `\ _ . _�`• -. _-_ ^�' ���. '�-� _ - ry•,`' , �• I'...'-r ..r \ �.. I a '-i :tip: ` _y-?•Tr. �:.�i' •5+.: °.6 r�: �.4i7 Z�- s.ILI tw i _ � ti � _ Y t' -�'_ � .ai. •'�' <.. _ :,:; art i'.:�•`._ .�. .J��'� � �' x_ :� ,T -- - �,- - •r"i,.Y far j �•_ —r F •, �".: _ RI -Y�lc �4w J � ate } -- , * _ -r L �` -N • gin' ��� -.. � I x "'mac .r .• - � :� . _ _ - - •' ' . �, i f _ ' . '� -' ,' • ��'` ., �t� �,i _- -- �*.�...-ter .. -• i - �' �! �, 'sue•' `'x �. �� _sr"r _�l11 ". - �� -�,� -;� ..'h: - 7c.��'�r I -4_ •tip +.� _aL Q� SATE SF4 RUSSELL PATTERSON Buffer Maps (Aug. 2002) AERIAL PHOTOGRAPH - FIELD FEATURES House/Nell Soil Boring (orange) (yellow) Field Number (yel 1 ow) Nj Buffer Area Water (stream or pond) Field Border (red) (blue) nw L:> (yellow) r k V 1. A-i r % L r L era sc—;�" f�; q f zi, Nf f j 'nit @2 z 44 0 to 61, ❑c F rd (L) " w 4� rci 7; z x fn W t / o SR 2z38 � / � i�OL z FIELD - 6-1 A o t n `* ACCESS i FIELD - 6-2 b Ej 4 LL a n iq a `ain r- �� 8 X r 1 0 0 z (� 7 u] a SITE SF6 VANCE TYSON Buffer Maps (Aug. 2002) ROW CROPS u�'ror� `�sar� s:onn ACCESS ®�2 I FIELD - 6-3 ACCESS Jrow CROPS i ti N CA f WOODS SITE SF7 JW AND JF BURNEY Buffer Maps (Aug. 2002) S CALF— Y • 95p /'� RIC NOMcC SERVLCES.oNC. W N SY: 0 AT=; Le^end N Dwelling Wooded Area v STu=re (Sam) --+ Drainage,rray Q Pond — Ac ess Road • Well -- Property Une /!! Buffer Area x-x-x Fence W Wet Area 0 viand Auger String S1v=IF ELD PACKLLNG FIGURE NO LAND APPLICATION PROCRAM SITE NO: Buvmr JOB NO: 1588-9"08 U.W �� ADJACENT I S= PFJZA T'rED (S« FIG. SA) I I MELD - 7-8 ADJACENT SITE FF-Fl, iITED SITE SF7 JW AND JF BURNEY Buffer Maps (Aug. 2002) � GALE t • � �. '-"ECK`�70 gy. BIO-NOPAIC SERVICES. INC. 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'•�e - t• '�:3�� I � �� ?. ` r C{l,=1'^.Y�: � t I�Y y,.r��a i ;rC NJ y��'" .i�• _ � -- . . . V t � •.•-,, _' �., i{,� 4 .tia� L� (D t O [J O Z� r CL4 (D `-- r� rLJ � O L � •rj 3 O a ~ t i O C14 } r-S >-I )•a a x O u] - a+ (n v L 41 Q i 4-j 4 R-, a W a) a) (� �rl w a) rd U7 W :j O 4-, a O v lll 1. �r4 44 =1-I State of North Carolina Department of Environment and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Direlctor October 30, 1998 William D. GilI, Assistant V.P., Environmental Affairs Smithfield Packing Company, Tar Heel Division Route 1, Box 189 PO Box 99 Tar Heel, NC 28392 Dear Mr. Gill: 7 1 ! •;% IT • NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES Subject: Permit No. WQ0014868 Smithfield Packing Company, Tar Heel Division Land Application of Wastewater Residuals Bladen County In accordance with your application received on August 6, 1998 we are forwarding herewith Permit No. WQ0014868 dated October 12, 1998 to Smithfield Packing Company, Tar Heel Division for the operation of a wastewater residuals land application program. This permit shall be effective from the date of issuance until February 28, 2003 shall void Permit No. WQ0014868 issued March 31, 1998 and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring and reporting requirements contained in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems_ If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforming to Chapter I50B of North Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447, Raleigh, NC 27611-7447. Unless such demands are made this permit shall be final and binding. If you need additional information concerning this matter, please ntact Sue Homewood at (919) 733- 5083 extension 502. Sincerely �[ reston Howard, Jr., P.E_ cc: Bladen County Health Department Bio-Nomic Services, Inc. Fayetteville Regional Office, Water Quality Section Fayetteville Regional Office, Groundwater Section Bob Cheek, Groundwater Section, Central Office Technical Assistance and Certification Unit Non -Discharge Compliance/Enforcement Unit PO Box 29535, Raleigh, North Carolina 27626-0535 Telephone (919) 733-5083 Fax (919) 733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/10% post -consumer paper NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH RESIDUALS LAND APPLICATION PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Smithfield Packing Company, Tar Heel Division Bladen County FOR THE operation of a wastewater residuals land application program consisting of the application of 2050 dry tons per year of residuals from the sources Iisted in Condition 115, to approximately 858.9 acres of land in Bladen County and Cumberland County with no discharge of wastes to the surface waters, pursuant to the application received on August 6, 1998 and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until February 28, 2003 shall void Permit No. WQ0014868 issued March 31, 1998, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS The Fayetteville Regional Office, telephone number 910-486-1541 and the appropriate local governmental official (county manager/city manager) shall be notified at least twenty-four (24) hours prior to the initial application of the residuals to a site so that an inspection can be made of the application sites and application method_ Such notification to the regional supervisor shall be made during the normal office hours from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. In addition, the Bladen County Manager's office or the Cumberland County Manager's office (according to the application site) must be notified prior to the initial application so that they will be aware that the operation has commenced. 2. This permit shall become voidable if the soils fail to adequately assimilate the wastes and may be rescinded unless the sites are maintained and operated in a manner which will protect the assigned water quality standards of the surface waters and ground waters. 3. The land application program shall be effectively maintained and operated as a non -discharge system to prevent the discharge of any wastes resulting from the operation of this program. 4. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. In the event that the land application program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall cease applying residuals to the sites and take any immediate corrective actions as may be required by the Division of Water Quality (Division). 6_ Some of the buffers specified below may not have been included in previous permits for this land application operation. However, any sites or fields that are included in this permit, but were approved with different applicable buffers shall be reflagged to comply with the below buffers. The following buffer zones shall be maintained: a) 400 feet from residences or places of public assembly under separate ownership for surface application method; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the appropriate regional office, b) 200 feet from residences or places of public assembly under separate ownership for subsurface residual injection method; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and the appropriate regional office, c) 100 feet from any public or private water supply source, waters classified as SA or SB, and any Class I or Class II impounded reservoir used as a source of drinking water for both methods, d) 100 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for surface application, e) 50 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for subsurface application, fl 50 feet from property lines for both surface and subsurface application methods; g) 50 feet from public right of ways for both application methods, h) 10 feet from ups lope interceptor drains and surface water diversions for both application methods, i) 25 feet from downslope interceptor drains, surface water diversions, groundwater drainage systems and surface drainage ditches for both application methods. 7. A copy of this permit shall be maintained at the land application site when residuals are being applied during the life of this permit. A spill prevention and control plan shall be maintained in all residuals transport and application vehicles. 8. Specific residual application area boundaries shall be clearly marked on each site prior to and during application. 9. No residuals at any time shall be stored at any application site, unless approval has been requested and obtained from the Division. 10. Maximum slope for residual application shall be 10% for surface application and I8% for subsurface applications. II. OPERATION AND MAINTENANCE REQUIREMENTS I. The facilities and application sites shall be properly maintained and operated at all times. 2. A suitable vegetative cover, as listed in condition 114, shall be maintained in accordance with the crop management plan outlined by the local Extension Office, the Department of Agriculture, the Natural Resource Conservation Service, or other agronomist, and approved by this Division. An acceptable pH must be maintained in the soil, residual and lime mixture, greater than 6.0, on all land application sites to insure optimum yield for the crop(s) specified below. The agronomist shall provide information on the pH best suited for the specified crop and the soil type. 2 4. The application rates shall not exceed the following for the specified crops: Crop PAN (lb./acre/yr.) CKOP PAN (lb./acre/yr.) Alfalfa 200 Forest (Hardwood & Softwood) 75 Bermuda Grass (Hay, Pasture) 220 Milo 100 Blue Grass , 120 Small Grain (Wheat, barley, oats) 100 Corn (Grain) 160 Sorghum, Sudex (Pasture) 180 Corn (Silage) 200 Sorghum, Sudex (Silage) 220 Cotton 70 Soybeans 200 Fescue 250 Timothy, Orchard, & Rye Grass 200 If the approved land application sites are to be double cropped (i.e., a crop in the spring and a second crop in the fall, with BOTH crops to receive wastewater residuals), then the second crop shall receive an application of nutrients at a rate of no greater than 50 lbs/acre/yr. This practice will be allowed as long as the second crop is to be harvested_ If the second crop is to be planted for erosion control only, and is to be tilled into the soil, then no wastewater residuals shall be applied to these fields because the nitrogen will essentially be returned to the soil. 5. No residuals other than the following are hereby approved for land application in accordance with this permit: Permit Volume Source County Number (dry tons/,year) Smithfield Packing Company, Tar Heel Division Bladen NCO078344 2050 6. The lifetime heavy metal loadings (lbs./acre) shall not exceed the following for the corresponding Cation Exchange Capacities (CEC): Parameter CEC < 5 CEC 5 to 15 CEC > 15 Lead 500 1000 2000 Zinc 250 500 1000 Copper I25 250 500 Nickel 125 250 500 Cadmium 4.5 9 is Upon classification of the facility by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall employ a certified land applicationlresiduals operator to be in responsible charge (ORC) of the land application program. The operator must hold a certificate of the type classification assigned to the land application program by the WPCSOCC. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8A .0202. Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. 9. Surface applied residuals will be plowed or disced within twenty-four (24) hours after application on lands with no cover crop established. 10. For areas that are prone to flooding or within the 100-year flood elevation, residuals may be applied only during periods of dry weather. The residuals must be incorporated into the soil within twenty-four (24) hours after application. 11. Appropriate measures must be taken to control public access to the land application sites during active site use and for the 12-month period following the last residual application event_ Such controls may include the posting of signs indicating the activities being conducted at each site. 12. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals application area onto the adjacent property or into any surface waters. 13. Residuals shall not be applied in inclement weather or until 24 hours following a rainfall event of 1/2- inch or greater in 24 hours. Any emergency residuals disposal measures must first be approved by the Division. I4. Residuals shall not be applied to any land application site that is flooded, frozen or snow-covered. 15. Residuals shall not be applied at rates greater than agronomic rates, unless authorized by the Division. 16. Animals shall not be grazed on an application site for 30 days after residuals application. Application sites that are to be used for grazing shall have fencing that will be used to prevent access after each application. 17. Food crops, feed crops and fiber crops that do not come in contact with the residuals shall not be harvested for 30 days after residuals application. 18. Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (ex. tobacco, melons, cucumbers, squash, etc.) shall not be harvested for 14 months after residuals application. 19. Food crops with harvested parts below the surface of the land (root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for 20 months after application of residuals when the residuals remain on the Iand surface for four (4) months or longer prior to incorporation into the soil. 20. Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after application of residuals when the residuals remain on the land surface for less than four (4) months prior to incorporation into the soil. 21. Turf shall not be harvested for 1 year after residuals application if the turf is to be placed on land with a high potential for public exposure. III. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee tracking all application activities. These records shall include, but are not necessarily Iimited to the following information: a. source of residuals b. date of residual application c. location of residual application (site, field, or zone #} d. method of application e. weather conditions (sunny, cloudy, raining, etc.) f2 soil conditions g. type of crop or crops to be grown on field h. volume of residuals applied in gallons/acre, dry tons/acre or Hograms/hectare i. annual and cumulative totals of dry tons/acre of residuals, annual and cumulative pounds/acre of each heavy metal (which shall include, but not be limited to cadmium, copper, lead, nickel, and zinc), annual pounds/acre of plant available nitrogen (PAN), and annual pounds/acre of phosphorus applied to each field. A representative annual soils analysis (Standard Soil Fertility Analysis) shall be conducted on each site receiving residuals in the respective calendar year and the results maintained on file by the Permittee for a minimum of five years. The Standard Soil Fertility Analysis shall include, but is not necessarily limited to, the following parameters: Acidity Calcium Copper Magnesium Cation Exchange Capacity Manganese Percent Humic Matter PH Phosphorus Potassium Sodium Zinc Base Saturation (by calculation) 4. A residuals analysis will be conducted every 60 days from the date of permit issuance by the Permittee and the results maintained on file by the Permittee for a minimum of five years. If land application occurs at a frequency less than every 60 days, a residuals analysis will be required for each instance of land application. The residuals analysis shall include but is not necessarily limited to the following parameters: Cadmium Copper Lead Nickel Zinc Aluminum Ammonia -Nitrogen Nitrate -Nitrite Nitrogen % Total Solids pH Phosphorus Potassium TKN Plant Available Nitrogen (by calculation) After the residuals have been monitored for two years at the above frequency, the Permittee may submit a request to the Division for a permit modification for the reduction of the frequency of monitoring for pollutant concentrations and for the pathogen density requirements, but in no case shall the frequency of monitoring be less than once per year when residuals are applied to the land. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Cadmium (1.0) Chiorobenzene (100.0) o-Cresol (200.0) Cresol (200.0) 1,2-Dichloroethane (0.5) Endrin (0.02) Hexachlorobenzene (0. 13) Lead (5.0) Methoxychlor (10.0) Pentachlorophenol (100.0) Silver (5.0) Trichloroethylene (0.5) 2,4,5-TP (Silvex) (1.0) Barium (100.0) Benzene (0.5) Carbon tetrachloride (0.5) Chlordane (0.03) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) p-Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) 1, 1 -Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13). Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lindane (0.4) Mercury (0.2) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) . Pyridine (5.0) Selenium (1.0) Tetrachloroethylene (0.7) Toxaphene (0.5) 2,4,5-Trichlorophenol (400,0) 2,4,6-Trichlorophenol (2.0) Vinyl chloride (0.2) 6. Three copies of all required monitoring and reporting requirements as specified in conditions 111 1, 11I 2, 111 3, III 4, III 5, shall be submitted annually on or before March 1 of the following year to the following address: NC Division of Water Quality Water Quality Section Non -Discharge Compliance/Enforcement Unit Post Office Box 29535 Raleigh, North Carolina 27626-0535 7. Noncompliance Notification: The Permittee shall report by telephone to the Fayetteville Regional Office, telephone number 910-486- 1541 as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the land application program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to receiving waters_ Any time that self -monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site. Persons reporting such occurrences by telephone shall also file a written report in letter form within five (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS The COMPLIANCE BOUNDARY for the disposal system is specified by regulations in 15A NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary is for the disposal system constructed after December 31, 1983 is established at either (I) 250 feet from the waste disposal area, or (2) 50 feet within the property boundary, whichever is closest to the waste disposal area_ An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to immediate remediation action in addition to the penalty provisions applicable under General Statute 143-215.6A(a)(I). In, accordance with 15A NCAC 2L, a REVIEW BOUNDARY is established around the disposal systems midway between the Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards at the Review Boundary shall require remediation action on the part of the permittee. 2. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. 3. No land application of waste activities shall be undertaken during periods of prolonged rainfall, nor when the seasonal high water table is less than three feet below land surface. V. INSPECTIONS The Permittee or his designee shall inspect the residuals storage, transport, and application facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Pennittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenanae, repairs, or corrective actions taken by the Perth ittce. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority, upon request. 2. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the application site or facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS This permit shall become voidable unless the Iand application activities are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by this Division. 2. This permit is effective only with respect to the .nature and volume of wastes described in the application and other supporting data. 3. This permit is not automatically transferable. In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. 4. The following are approved sites for residuals application (see attached map[s]): Application Area [acres] Site No. Owner/Lessee excluding buffers Blades County SF I-1 Smithfield Packing Company 22.5 SF 1-2' Smithfield Packing Company 14.0 SF 1-3 Smithfield Packing Company 31.1 SF 1-4a Smithfield Packing Company 18.0 SF 2-1 White Pharr 10.0 SF 2-2 White Pharr 11.3 SF 2-3 White Pharr 19.0 SF 2-4 White Pharr 7.3 SF 2-5a John Willis / White Pharr 36.0 SF 2-5b John Willis / White Pharr 9.8 SF 2-6 John Willis / White Pharr 20.0 SF 3-1 W. M. Dunham, Jr. / Steven H. Dunham 21.6 SF 3-2' W. M_ Dunham, Jr. / Steven H. Dunham 13.3 SF 3-3 W. M. Dunham, Jr. / Steven H. Dunham 21.3 SF 3-4 w W. M. Dunham, Yr. / Steven H. Dunham 19.0 SF 3-5 W. M. Dunham, Jr. / Steven H. Dunham 8.0 7 SF 3-6 W. M. Dunham, Jr. / Steven H. Dunham 32.0 SF 3-7 a W. M. Dunham, Jr. / Steven H. Dunham 40.0 SF 4-1 Ethal Davis Estate / Russell (Rusty) Patterson 25.3 SF 4-2 Ethal Davis Estate / Russell (Rusty) Patterson 31.2 SF 4-3 Russell (Rusty) Patterson 22.0 SF 4-4 Russell (Rusty) Patterson 9.0 SF 4-5 f Russell (Rusty) Patterson 8.6 SF 4-6 a Russell (Rusty) Patterson 13.5 SF 4-7 Russell (Rusty) Patterson 15.0 SF 4-8 Russell (Rusty) Patterson 25.8 SF 4-9 Russell (Rusty) Patterson 13.5 SF 4-10 Russell (Rusty) Patterson 21.5 SF-7-1 a J.F. and J.W. Burney 21.8 SF-7-2 a J.F. and J.W. Burney 48.5 SF-7-3 a J.F. and J.W. Burney 12.3 SF-7-4 a J.F. and J.W. Burney 19.8 SF-7-5 J.F. and J.W. Burney 23.8 SF-7-6 J.F. and J.W. Burney 19.3 SF-7-7 J.F. and J.W. Burney 6.3 SF-7-8 J.F. and J.W. Burney 12.1 SF-7-9 J.F. and J.W. Burney 21.3 SF-7-10 J.F. and J.W. Burney 9.9 SF-7-11 a J.F. and J.W. Burney 6.3 SF-7-12 J.F. and J.W. Burney 18.6 SF-7-13 J.F. and J.W. Burney 25.3 SF-7-14a J.F. and J.W. Burney 7.5 SF-7-15 a J.F. and J.W. Burney 3.0 TOTAL ACRES IN COUNTY 795.4 Cumberland County SF 6-1 Vance Tyson 5.5 SF 6-2 Vance Tyson 33.5 SF 6-3 a Vance Tyson 64.5 TOTAL ACRES IN COUNTY 103.5 TOTAL AVAILABLE ACRES 898.9 a This land application site is partially covered in soils having a seasonal high water table'at depths ranging from zero to three feet below Iand surface. No residuals shall be applied to this field during the period from November through April, inclusive, unless augering on the site verifies that the apparent water table is greater than three feet below land surface. 5. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statute 143-215.6A to 143-215.6C. 6. The annual administering and compliance fee must be paid by the Permittee within thirty (30) days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205 (c)(4). 8 7. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local, state, and federal) which have jurisdiction. S. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 9. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to adequately protect the environment and public health. 10. This permit shall become voidable unless the agreements between the Permittee and the landowners/lessees are in full force and effect. The land owner agreements are considered expired concurrent with the expiration date of the permit and must be renewed at the same time the permit is renewed. Permit issued this the 3 ay of October, 19 8 NORTH C INA EN 0 AGEMENT COMMISSION c A. Preston Howard, Jr., P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0014868 State of North Carolina Department of Environment and Natural Resources Division of Water Quality .lames B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director March 31, 1998 William D. Gill, Assistant VP, Environmental Affairs Smithfield Packing Company, Tar Heel Division Route 1 Box 189, Post Office Box 99 Tar Heel, North Carolina 28392 Dear Mr, Gill: 4 NCDENR NORTH CAROL-INA DEPARTMENT OF ENVIRONMENT AND NATURAL RE50URCES Subject: Permit No. WQ0014868 Smithfield Packing Company, Tar Heel Division Land Application of Wastewater Residuals Bladen County In accordance with your application received on January 14, 1998, we are forwarding herewith Permit No. WQ0014868, dated March 31, 1998, to the Smithfield Packing Company, Tar Heel Division for the operation of a wastewater residuals land application program. This permit shall be effective from the date of issuance until February 28, 2003, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring and reporting requirements contained in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447, Raleigh, NC 27611-7447, Unless such demands are made this permit shall be final and binding. If you need additional information concerning this matter, please ntact Mr. Michael D. Allen at (919) 733-5083 extension 547. Sincere] Lax A. Preston Howard, Jr., P.E. cc: Bladen County Health Department Bio-Nomic Services, Inc. Fayetteville Regional Office, Water Quality Section Fayetteville Regional Office, Groundwater Section Bob Cheek, Groundwater Section, Central Office Technical Assistance and Certification Unit Non -Discharge Compliance/Enforcement Unit PO Box 29535, Raleigh, North Carolina 27626-0535 Telephone (919) 733-5083 Fax (919) 733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/10% post -consumer paper NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH RESIDUALS LAND APPLICATION PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO THE Smithfield Packing Company, Tar Heel Division Bladen County FOR THE operation of a wastewater residuals land application program consisting of the application of 600 dry tons per year of residuals from the sources listed in Condition II 5, to approximately 499.6 acres of land in Bladen County with no discharge of wastes to the surface waters, pursuant to the application received on January 14, 1998, and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until February 28, 2003, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS 1. The Fayetteville Regional Office, telephone number (910) 486-1541, and the appropriate local governmental official (county manager/city manager) shall be notified at least twenty-four (24) hours prior to the initial application of the residuals to a site so that an inspection can be made of the application sites and application method. Such notification to the regional supervisor shall be trade during the normal office hours from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. In addition, the Bladen County Manager's office must be notified prior to the initial application so that they will be aware that the operation has commenced. This permit shall become voidable if the soils fail to adequately assimilate the wastes and may be rescinded unless the sites are maintained and operated in a manner which will protect the assigned water quality standards of the surface waters and ground waters. The land application program shall be effectively maintained and operated as a non -discharge system to Prevent the discharge of any wastes resulting from the operation of this program. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. In the event that the land application program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall cease applying residuals to the sites and take any immediate corrective actions as may be required by the Division of Water Quality (Division). 6. Some of the buffers specified below may not have been included in previous permits for this land application operation. However, any sites or fields that are included in this permit, but were approved with different applicable buffers shall be reflagged to comply with the below buffers. The following buffer zones shall be maintained: a) 400 feet from residences or places of public assembly under separate ownership for surface application method; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the appropriate regional office, b) 200 feet from residences or places of public assembly under separate ownership for subsurface residual injection method; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and the appropriate regional office, c) 100 feet from any public or private water supply source, waters classified as SA or SB, and any Class I or Class 11 impounded reservoir used as a source of drinking water for both methods, d) 100 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for surface application, e) 50 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for subsurface application, f) 50 feet from property lines for both surface and subsurface application methods; g) 50 feet from public right of ways for both application methods, h) 10 feet from upslope interceptor drains and surface water diversions for both application methods, i) 25 feet from downslope interceptor drains, surface water diversions, groundwater drainage systems and surface drainage ditches for both application methods. 7. A copy of this permit shall be maintained at the land application site when residuals are being applied during the life of this permit. A spill prevention and control plan shall be maintained in all residuals transport and application vehicles. Specific residual application area boundaries shall be clearly marked on each site prior to and during application. No residuals at any time shall be stored at any application site, unless approval has been requested and obtained from the Division. 10. Maximum slope for residual application shall be 10% for surface application and 1 S% for subsurface applications. U. OPERATION AND MAINTENANCE REQUIREMENTS The facilities and application sites shall be properly maintained and operated at all times. A suitable vegetative cover, as listed in condition 114, shall be maintained in accordance with the crop management plan outlined by the local Extension Office, the Department of Agriculture, the Natural Resource Conservation Service, or other agronomist, and approved by this Division. An acceptable pH must be maintained in the soil, residual and lime mixture, greater than 6.0, on all land application sites to insure optimum yield for the crop(s) specified below. The agronomist shall provide information on the pH best suited for the specified crop and the soil type. 4 C' The application rates shall not exceed the following for the specified crops: Crop PAN (lb./acre/yr.) Crop PAN lb./acre/yr. AIfalfa Bermuda Grass (Hay, Pasture) Blue Grass Corn (Grain) Corn (Silage) Cotton Fescue Coastal Bermuda Grass 200 Forest (Hardwood & Softwood) 75 220 Milo 100 120 Small Grain (Wheat, barley, oats) 100 160 Sorghum, Sudex (Pasture) 180 200 Sorghum, Sudex (Silage) 220 70 Soybeans 200 250 Timothy, Orchard, & Rye Grass 200 350 If the approved land application sites are to be double cropped (i.e., a crop in the spring and a second crop in the fall, with BOTH crops to receive wastewater residuals), then the second crop shall receive an application of nutrients at a rate of no greater than 50 lbs/acre/yr. This practice will be allowed as long as the second crop is to be harvested. If the second crop is to be planted for erosion control only, and is to be tilled into the soil, then no wastewater residuals shall be applied to these fields because the nitrogen will essentially be returned to the soil. No residuals other than the following are hereby approved for land application in accordance with this permit: Permit Volume Source County Number (dry tons/year) Smithfield Packing Company, Tar Heel Division Bladen NC0078344 600 The lifetime heavy metal loadings (tbs./acre) shall not exceed the following for the corresponding Cation Exchange Capacities (CEC): Parameter CEC < 5 CEC 5 to 15 CEC > 15 Lead 500 1000 2000 Zinc 250 500 1000 Copper 125 250 500 Nickel 125 250 500 Cadmium 4.5 9 18 7. Upon classification of the facility by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall employ a certified land application/residuals operator to be in responsible charge (ORC) of the land application program. The operator must hold a certificate of the type classification assigned to the land application program by the WPCSOCC. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8A .0202. 8. Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored. residuals into any surface waters. 9. Surface applied residuals will be plowed or disced within twenty-four (24) hours after application on lands with no cover crop established. 10. For areas that are prone to flooding or within the I00-year flood elevation, residuals may be applied only during periods of dry weather. The residuals must be incorporated into the soil within twenty-four (24) hours after application. 11. Appropriate measures must be taken to control public access to the land application sites during active site use and for the 12-month period following the last residual application event. Such controls may include the posting of signs indicating the activities being conducted at each site. 12. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals application area onto the adjacent property or into any surface waters. 13. Residuals shall not be applied in inclement weather or until 24 hours following a rainfall event of 1/2- inch or greater in 24 hours. Any emergency residuals disposal measures must first be approved by the Division. 14. Residuals shall not be applied to any land application site that is flooded, frozen or snow-covered. 15. Residuals shall not be applied at rates greater than agronomic rates, unless authorized by the Division. 16. Animals shall not be grazed on an application site for 30 days after residuals application. Application sites that are to be used for grazing shall have fencing that will be used to prevent access after each application. 17. Food crops, feed crops and fiber crops that do not come in contact with the residuals shall not' be harvested for 30 days after residuals application. 18. Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (ex. tobacco, melons, cucumbers, squash, etc.) shall not be harvested for 14 months after residuals application. 19. Food crops with harvested parts below the surface of the land (root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for 20 months after application of residuals when the residuals remain on the land surface for four (4) months or longer prior to incorporation into the soil. 20. Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after application of residuals when the residuals remain on the land surface for less than four (4) months prior to incorporation into the soil. 21. Turf shall not be harvested for 1 year after residuals application if the turf is to be placed on land with a high potential for public exposure. III. MONITORING AND REPORTING REQUIREMENTS I. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. Proper records shall be maintained by the Permittee tracking all application activities. These records shall include, but are not necessarily limited to the following information: a. source of residuals b. date of residual application c. location of residual application (site, field, or zone 4) d. method of application e. weather conditions (sunny, cloudy, raining, etc.) f. soil conditions g. type of crop or crops to be grown on field h. volume of residuals applied in gallons/acre, dry tons/acre or kilograms/hectare i. annual and cumulative totals of dry tons/acre of residuals, annual and cumulative pounds/acre of each heavy metal (which shall include, but not be limited to cadmium., copper, lead, nickel, and zinc), annual pounds/acre of plant available nitrogen (PAN), and annual pounds/acre of phosphorus applied to each field. A representative annual soils analysis (Standard Soil Fertility Analysis) shall be conducted on each site receiving residuals in the respective calendar year and the results maintained on file by the Permittee for a minimum of five years. 4 The Standard Sol] Fertility Analysis shall include, but is not necessarily limited to, the following parameters: Acidity Calcium Copper Magnesium Cation Exchange Capacity Manganese Percent Humic Matter PH Phosphorus Potassium Sodiurn Zinc Base Saturation (by calculation) The Standard Soil Fertility Analysis (see above) and an analysis for the following pollutants shall be conducted once prior to permit renewal on soils from each site which has received residuals during the permit cycle. Cadmium Lead Nickel 4. A residuals analysis will be conducted quarterly from the date of permit issuance by the Permittee and the results maintained on file by the Permittee for a minimum of five years. If land application occurs at a frequency less than quarterly, a residuals analysis will be required for each instance of Iand application. The residuals analysis shall include but is not necessarily Iimited to the following parameters: Cadmium Copper Lead Nickel Zinc Aluminum Ammonia -Nitrogen Calcium Magnesium Nitrate -Nitrite Nitrogen % Total Solids PH Phosphorus Potassium Sodium TKN Plant Available Nitrogen (by calculation) A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Cadmium (1.0) Chlorobenzene (100.0) o-Cresol (200,0) Cresol (200.0) 1,2-Dichloroethane (0.5) Endrin (0.02) Hexachlorobenzene (0.13) Lead (5.0) Meth oxychlor (10.0) Pentachlorophenol (100.0) Silver (5.0) Trichloroethylene (0.5) 2,4,5-TP (Silvex) (1.0) Barium (100.0) Benzene (0.5) Carbon tetrachloride (0.5) Chlordane (0.03) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) p-Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) I,1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lindane (0.4) Mercury (0.2) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pyridine (5.0) Selenium (1.0) Tetrachloroethylene (0.7) Toxaphene .(0.5) 2,4,5-Trichlorophenol (400,0) 2,4,6-Trichlorophenol (2.0) Vinyl chloride (0.2) 6. Three copies of all required monitoring and reporting requirements as specified in conditions 111 1, III 2, 1113, III 4, and 111 5 shall be submitted annually on or before March 1 of the following year to the following address: NC Division of Water Quality Water Quality Section Non -Discharge Compliance/Enforcement Unit Post Office Box 29535 Raleigh, North Carolina 27626-0535 7. Noncompliance Notification: The Permittee shall report by telephone to the Fayetteville Regional Office, telephone number(910) 486-1541, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the land application program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to receiving waters. Any time that self -monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site. Persons reporting such occurrences by telephone shall also file a written report in letter form within five (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS The COMPLIANCE BOUNDARY for the disposal system is specified by regulations in 15A NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary is for the disposal system constructed after December 31, 1983 is established at either (1) 250 feet from the waste disposal area, or (2) 50 feet within the property boundary, whichever is closest to the waste disposal area. An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to immediate remediation action in addition to the penalty provisions applicable under General Statute 143-215.6A(a)(1). In accordance with 15A NCAC 2L, a REVIEW BOUNDARY is established around the disposal systems midway between the Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards at the Review Boundary shall require remediation action on the part of the perm ittee. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. No land application of waste activities shall be undertaken when the seasonal high water table is less than three feet below land surface. 6 V. INSPECTIONS 1. The Permittee or his designee shall inspect the residuals storage, transport, and application facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority, upon request. 2. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the application site or facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that trust be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS This permit shall become voidable unless the land application activities are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by this Division. 2. This permit is effective only with respect to the nature and volume of wastes described in the application and other supporting data. 3. This permit is not automatically transferable. In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. 4. The following are approved sites for residuals application (see attached map[s]): Application Area [acres] Site No. Owner/Lessee _(excluding buffers) Bladen County SF 1-1 Smithfield Packing Company 22.5 a SF 1-2 Smithfield Packing Company 14.0 SF 1-3 Smithfield Packing Company 31.1 a SF 1-4 Smithfield Packing Company 18.0 SF 2-1 White Pharr 10.0 SF 2-2 White Pharr 11.3 SF 2-3 White Pharr 19.0 SF 2-4 White Pharr 7.3 SF 2-5a John Willis / White Pharr 36.0 SF 2-5b John Willis / White Pharr 9.8 SF 2-6 John Willis / White Pharr 20.0 SF 3-1 W. M. Dunham, Jr. / Steven H. Dunham 21.6 SF 3-2' W. M. Dunham, Jr. / Steven H. Dunham 13.3 SF 3-3 W. M. Dunham, Jr. / Steven H. Dunham 21.3 a SF 3-4 W. M. Dunham, Jr. / Steven H. Dunham 19.0 SF 3-5 W. M. Dunham, Jr. / Steven H. Dunham 8.0 SF 3-6 W. M. Dunham, Jr. / Steven H. Dunham 32.0 a SF 3-7 W. M. Dunham, Jr. / Steven H. Dunham 40.0 7 Site No. Owner/Lessee Application Area [acres] (excluding buffers) SF 4-1 Ethal Davis Estate / Russell (Rusty) Patterson SF 4-2 Etha1 Davis Estate / Russell (Rusty) Patterson SF 4-3 Russell (Rusty) Patterson SF 4-4 Russell (Rusty) Patterson SF 4-5 Russell (Rusty) Patterson SF 4-6 a Russell (Rusty) Patterson SF 4-7 Russell (Rusty) Patterson SF 4-8 Russell (Rusty) Patterson SF 4-9 Russell (Rusty) Patterson SF 4-10 Russell (Rusty) Patterson TOTAL ACRES IN COUNTY TOTAL AVAILABLE ACRES 25.3 31.2 22.0 9.0 8.6 13.5 15.0 25.8 13.5 21.5 499.6 499.6 a This land application site is partially covered in soils having a seasonal high water table at depths ranging from zero to three feet below land surface. No residuals shall be applied to this field during the period from November through April, inclusive, unless augering on the site verifies that the apparent water table is greater than three feet below land surface. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statute 143-215.6A to 143-215.6C. The annual administering and compliance fee must be paid by the Permittee within thirty (30) days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit as specified by 15 NCAC 211 .0205 (c)(4). 7. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local, state, and federal) which have jurisdiction. 8. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 9. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring- requirements the Division deems necessary in order to adequately protect the environment and public health. Permit issued this the thirty-first day of March, 1998 NORTH CA LIMA ENV RONME�NTAL MANAGEMENT COMMISSION -A. Preston Howard, Jr., P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0014868 „v � �SuhS[8uOn 3• . Ga BM tag• Enbdm � �' � ,�+ ° ° ° i 1�•'i• -� -- 'ems --e _ Ll 0 Oo 1 _ r e _ Cgm `= r ` - a o ory .a 1Lock nn gas uo Radio •� I - I - A. ,Al Cem i TOPOGRAPHY MAP SCALE 1:24,000 BLUE COLOR INDICATES WATER Pond or Lake Stream or River Intermittent Stream gmpu• R «.!1 76.- c/ es -A 5F `I 7T17TJ)P - ---- - -�ti ----- —�—� �, � i{%orlS Bay 62 White Oak �,• ,.i��l � 1 BM •78 % , � -.. �I� .l1ao .Cam ,Cem - /' C Ch ur Cam - O l/, Cem \ J G �- /� /^, J J We Purdie Cem _- V 1 336 TOPOGRAPHY MAP N SCALE 1:24 00©0 BLUE COLOR INDICATES WATER Pond or Lake Stream or River Intermittent Stream FARM: S+�Jw `7i v,, �A 5F 3 FIELDS;_, / - 7 Mile so Ca �sa— uCarm l JC \ Vurdle Mt ' Cem HI Ger r - GLLM 3iCOBr•,s� V ; ti ::52 em 13�0 so IP pre Fl� TOPOGRAPHY HAP SCALE 1:24,-000 j BLUE COLOR INDICATES WATER Pond or Lake Stream or River Intermittent Stream FARM: Bo FA qXA z F Z FIELDS: S L s NL High Cem clalt chapel Tar\ffeel .S11b5I3 , c / • • , '32 �1CNeff EJ1'h 131, �I engert Cem - r c T. Fled Cb if' � 155 � _ & - Mil � err 22 Cem } Chipa 'a 149 gm 13 artch -_-- _ t1 r_ of r ; ,f v _ Ij y _ ' Cem 342 Cem_ / '`- _._ \ •.tom' r -ti Cem/ Bumey-- r-,Cem. i � { 1 TOPOGRAPHY HAP A SCALE 1:24,000 BLUE COLOR INDICATES WATER Pond or Lake Stream or River Intermittent Stream FARM: �o �kr+rt�t S �'�- FIELDS: �� 5� I 1 , f r ♦ 1 i - j� Ijl I. Curve. �— BM 137 I.� i 't, I I• x I 15 1 �1 SP B Br C Cem-- `� ` 51 Deed \ t 1 _ BM 151 MI a� j 5 D9 Bushy y M 138- "_ 1 1�n~ � v cC� rJ�a 5� 700 (TAR H6IFL) l01 tARNEEL 1.4M! 47' 30„ 5253 f11 NE ELfZA84-THTOWN 16 Mi. SCALE 1:24 000 MILLS 1000 0 1DDO 20W 3000 4000 5000 6Q0p 7000 &M 9000 10 000 cr- TOPOGRAPHY MAP N SCALE 1:24,000 BLUE COLOR INDICATES WATER Pond or Lake Stream or River I nt errrd tt en t Stream FARM: SrMt',�1<!d f�pc1��`�r SF/ FIELDS• �— y RATING SCALE FOR CLASSIFICATION *F WATER POLLUTION CONTROL SYSTEMS Name 'of Facility: 92`t ac, Co,,-2 4K I TA-�++jaa- 01M ,22 Owner or Contact Person, Gtu Asir VP, Mailing Address: i-jris I g«< lei 1.Po sax Icl 39L County: 3--*0e- Telephone:_ -1,15 Present Classification:New Facility ✓ Existing Facility NPOES Per. No. NC00 Nondisc. Per. No. WQp0,046 Health Oept. Per. Na — Rated by: Nm;+NeL A-,q� Telephone: Date: Reviewed by: Health Dept. Telephone: ReglonalOffice Telephone: Central Office Telephone: ORC: Grade: Teiephonel Check- Classification(s): Subsurface Spray Irrigation LandApplication Wastewater Classification: (Circle One) ( 11 III IV Total Points: >3 k:^P�xc GSA' pF�rRTYJ-1 A = N PART 1 ' %�y�c �eee�4,:tclTctT}i-t^ T.ie p c c nSi. Tt = 1!e K C 1C I- SLfd.S'JRrACE CLASSIF1CATOON (check all units tha; apply) 1 septic tanks 7 pump tanks 3. siphor, or pump -dosing systems 4-Sand fiilerl 5 grease trsprniemoplor 6 oillwaier separators 7 subsea face treatment and disposa: gravity pressure spj;v+Y imGATM CLAMFIGATICN (check all units that apply) 1-preliminary treatment (derrnliion no. 32 ) z lagoons 3. aeplic tanks 4, _,.., pump tanks 6-pumps G sand filters 7. _ Qrease Iraphnterceptor B oil/water separators 4. disinfection 10.,- chemicar addition for nutrientlalgae control it. spray irrigalion of wastewater Pretreatment of wastewater In excess of these components shall be rated using the polni rating system and will require an operator with an appropriate dual certification. LAND F�FP,ICFTI 11RESIDUALS CLASSIFICATION' (►',ppTes only to permit kidder) 1. Land Zrp!i:ation of biosolids, residuals or cantaminatsd soils on a designated site. WASTEWATER TREATMENT FAaLrlY C1 A5SIFZ4TON The to:!owing sys!en,s shall be assigned a Class I classiricalion, unfect the flow Is of a signiiicanl quanlity or she technology Is uiusuml:y complex, to regUlre ponsidti-Cion by the Commission on a Cast -by -case basis: (Check It Appropriate) 1 Oi!'ria?e Separator Systems consisting only of physic's! sepwat;on, pumps and disposal; 2. Sep;ic %-IVSand Filier Systems consisling onty of septic tanks, dosing apperi lus, pumps,sand fillers, disinfection and direct discharge; 3 Lzcoor, Systems consisting only or preliminary treatment, lagoons, pumps, disinlealion, necessary chemical Irea:ment for algae or nutrient control, and direct discharge; ,. CIDsee-loop Fecycle Systems: 6. Gfconewa!er Remediarion Systems censisiing only of pumps, a+r-stripping, carbon adsorption, dWnlect;on and disposal; 6 Fish farms wish discharge Ic sur+acc waters: 7."t.'a!er Pant sivdge baridiing and back; -wash walef treatment; S Sea'oy' pti:>-esaing consislirrg of saetning and disposal. - D. 5:nr�!e-Ia-r,ily discharging systems with the ezceplion or Aerobic Trealmenl Units, will be t)assiried if permitted afler July 1. 1443 or it upon inspection by the I)Wsion, F is found that the system Is not being adequately operated or maintained. SuJh systems will be notilied of the ciassificalion or rectasslticalionj�y the Commission, in writing.