WQ0000601_Final Permit_20100222

TRANSPORTATION
J. R. Gardner
Plant Manager
Environmental Control
Rail Transport Group
Route 1, Box 191-A
Hamlet, NC 28345
Bus. [phone] Ext. 279
Res. [phone]

TRANSPORTATION
Carl A. Gerhardstein, P.E.
AVP Environmental Systems and Sustainability
[phone]
North Carolina Department of Natural Resources
Division of Water Quality
Attn: Information Processing Unit
1617•Mail Service Center
Raleigh, North Carolina 27699-161
Public Safety & Environment
500 Water Street, J275
Jacksonville, FL 32202
September 13, 2010
File. 9613703
.� ®EIVR-SRO
SEP 2 -1 2010
DWQ
Permit No. W00000601, Richihond County �
CSX Transportation, Inc. (CSXT), Hamlet, NC
Dear Sir or Madam: I
Enclosed are revised Non Discharge Wastewater Monitoring Reports (NDMR) for the CSXT Hamlet, NC
facility (permit WQ0000601). The reporting format has been corrected to use the NDMR forms as specified in
Section IV. 4. and 7 of our permit. Future tri-annual reporting will be completed using the NDMR form. We
have included reports for January through July, 2010. Please note that we have collected more',frequent
samples than required by our permit to demonstrate compliance with our best management procedures. Extra
parameters were also tested and are reported on the monitoring reports and designated as "Extra Sample
Per requirements stated in Section IV. 3. of our permit, our facility has not removed any residuals from the
wastewater treatment system during the last 12 months. We will maintain a log of any future removal"events.
If you have any questions or comments, please do -not hesitate to contact me at [phone]
Sily
arkerhardstein, P.E.
AVP Environmental Systems and Sustainability
�1
.Enclosures
SEP-16 2010.
i �i1tQFtll.'�c t)i"� .•^-;�?t:y:c::;�itCa �?lit
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ATTACHIVIENT A — LIMITATIONS AND MONITORING
REQUIREMENTS
Permit Number;
WQ0000601
Version: 3.0
PPI 001— WWTF Effluent
EFFLUENT CHAR.aCTEPJSTtCS
Parameter Description —Parameter Code EFFLUENT LIMITS
MONITORING REQUIREMENTS
Monthly average Weekly Average Flow, in conduit or thru treatment plant — 50050
1.0
Daily Maximum
Monitoring Frequent Y
Sample Type
mgd
Solids, "total Dissolved— Igo Deg.C— 70300
151C)o
c .
Continuous
Recorder
pl i— 00400
S °�
M L
3 X year
'Grab
Carbon, Total Organic (TOC ) — 00680
3 X year
Grab
Nitrogen, Nitrate Total (as N) — 00620
J.
h.� L.
3 X year
Grab
Barium, Total (as Ba) — 01007•
3 X year
Grab
Cadmium, Total (as Cd) — 01027
3 X year
Grab
Chromium, Total (as Cr) — 01034
3 X year.
Grab.
Lead, Total (as Pb) — U 1051
3 X year
Arsenic, "Total (as t1s) — O l UO2 _
d • DG$o1.
/n 1,
3 X year -
Grab
Grab
3 k year monitoring shall be conducted in March, July
G - GOG /
L
3 X year
Grab
and November.
WQ0000601 Version 3.0
Attachment A
pan. t -Ir i

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL Y ICAO. REPORT
Job Number: 680-54502-1
Job Description: CSX Hamlet, NC WWTP Monthly
For:
CSX Transportation
500 Water Street
Jacksonville, FL . 32202
Attention: Mr. Mike Gregory
0Ajy(y`� 4 /j aawwae raease.
Kathryn SmitIth
ll 1 Project Manager I
2/0/2010 2AO PM
Kathryn Smith
Project Manager I
[e-mail]
02/03/2010
1 '
cc: Mr. Jerry Cato
Mr. Alan Pinnix
L W O N-E N V000002 7258HP roj ect-R000 011790
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This'report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A21-A: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT: ' PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353, KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC; 249; NV: GA00006;
NJ: GA769; NM; NY: '10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www t sr tarMerir.-ic ccLm
Page 1 of 19

Job Narrative
680-54502-1
Comments
No additional comments.
r
Receipt
All samples were received in good condition -within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry.
No analytical or quality issues were noted.
Page 2 of 19

METHOD SUMMARY
Client: CSX Transportation
Job Number. 680-54502-1
Description
Lab Location Method Preparation Method
Matrix Water
Metals (ICP)'
TAL SAV 40CFR136A 200.7 Rev 4.4
Sample Filtration, Field
TAL SAV FIELD_FLTRD
Preparation, Total Metals
TAL SAV EPA 200.7
Preparation, Total Recoverable Metals
.
TAL SAV
EPA 200.7
Nitrogen, Nitrate -Nitrite
TAL SAV MCAWW 353,2
Solids, Total Dissolved (TDS)
TAL SAV 'SM SM 2540C
Organic Carbon, Total (TOC)
. TAL SAV SM SM 5310E
Lab References:
TAL SAV = TestAmerica Savannah ,
Method References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal
Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For. Chemical Analysis Of Water And Wastes",
EPA-60014-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater", '
i �-
0
TestAmerica Savannah
a
Page 3 of 19

METHOD / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-54502-1
- Method
Analyst
Analyst ID
40CFR136A 200.7 Rev 4.4
Bland, Brian
BCB
MCAWW 353.2
Ross, Jan
JR
SM SM 2540C
Jackson, Michelle S
MSJ
SM SM 5310E
Blackshear, Kim
KB
TestAmerica Savannah
Page 4, of 19

SAMPLE SUMMARY
Client: CSX Transportation
Job Number: 680-54502-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-54502-1 Water Sample Water 01/25/2010 0900 01/26/2010 1010
it
TestAmerica Savannah
Page 5 of 19

Client: CSX Transportation
Analytical data
Job Number: 680-54502-1
Client Sample ID:
Water Sample
Lab Sample ID:
680-54502-1
Date
Sampled:-01125/2010 0900
Client Matrix:
Water
Date
Received: 01/26/2010 1010
200.7 Rev'4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-159539
Instrument ID:
1CPD
Preparation:
200.7
Prep Batch: 680-159407
Lab File ID:
N/A
i Dilution:
1.0
Initial WeighWolume:
50 mL
Date Analyzed: '.
01/28/2010 1920
Final WeighWolume:
50 mL
Date Prepared:
01/28/2010 1200
Analyte
Result (mg/L)
Qualifier MDL
RL
Arsenic
0.0061
J
0.0046'
0.020
Barium
0.036
-0.0023
0.010
Cadmium
0.0050
U
0.0020
0.0050
Chromium
0.0048
J
0.0012
0.010
Lead
0.0082
J
0.0040
0.010
200.7 Rev 4.4 Metals (ICP)-Dissolved
Method:
200.7 Rev 4.4
Analysis Batch: 680-159539
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-159408
Lab File ID: '
NIA
Dilution:
1.0
Initial Weight/Volume:
50 mL
Date Analyzed:
01/28/2010 1757
Final Weight/Volume:
50 mL
Date Prepared:
01/28/2010 1203
-
Analyte
Result (mg/L)
Qualifier
-MDL
RL
Arsenic
0.020
U
0.d10
0.020,
Barium
0.037
0.0020
0.010
Cadmium
0.0050
U
0,0020
0.0050
Chromium
0.0046
J
0.0020
0.010
Lead
0.0070
J
0.0034
0.010
TestAmerica Savannah Page 6 of 19

Analytical Data
Client: CSX Transportation Job Number: 680-54502-1
General Chemistry
Client Sample ID: Water Sample
Lab Sample ID: 680-54502-1
Date Sampled: 01/25/2010 0900
Client Matrix: Water.
Date Received: 01/26/2010 1010
Analyte Result
Qual Units MDL
RL
Dil Method
Nitrate as N 0.26
mg/ L 0.010
. ..........
0.050
_. _..... 1_ _._.._. .
.0 353.2
Analysis Batch: 680-159557
Date Analyzed: 01/26/2010 1742
Total Organic Carbon 5.5
mg/L 0.50
1.0
1.0 SM 5310E
Analysis Batch: 68.0-159858
Date Analyzed: 02/02/2010 1437
Analyte Result
Qual Units RL
RL
Dil Method
Total Dissolved Solids 52
mg/L 5.0
.5.0
.•.-..
1.01 SM 2540C
Analysis Batch: 680-159316
Date Analyzed: 01/27/2010 1518
1
n
TestAmerica Savannah , Page 7 of 19

DATA REPORTING QUALIFIERS
Client: CSX Transportation Job Number: 680-54502-1
Lab Section Qualifier Description
Metals
U Indicates the analyte was analyzed for but not detected. .
J Result is less than the,RL but greater than or equal to the
MDL and the concentration is an approximate value.
General Chemistry
U ' Indicates the analyte was analyzed for but not detected.
i
TestAmerica Savannah
Page 8 of 19

Quality Control Results -
a
Client: CSX Transportation
Job Number: 680-5450271._.
Method Blank - Batch: 680-159407
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID: MB 680-159407/5-A
Analysis Batch: 680-159539
Instrument ID: ICP/AES -'D
Client Matrix: Water
Prep Batch: 680-15940.7
Lab File 10: N/A
Dilution: 1.0
Units: , mg/L
Initial Weight/Volume: 50 mL
Date Analyzed: 01/28/2010 191'0
Date Prepared: 01/28/2010 1200
Final Weightolume: 50 mL
Analyte
Result
Qual
MDL RL
Arsenic
Barium
0.020
U
... ... .... .._ . ... .. .
0.0046 0.020
Cadmium
0.010
U
0.0023 0.010
Chromium
0.0050
U
O:OOZO 0.0050
Lead
0.010
U
t).0012 0.010
0.010
U
0.0040 0.010
Lab Control Sample - Batch: 680-159407
Method: 200.7 Rev.4.4
Preparation: 200.7
Lab Sample ID: LCS 680-159407/6-A
'
Analysis Batch: 680-159539
Instrument ID: - D
Client Matrix: Water
Prep Batch: 680-159407
,ICP/AES
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weightolume: 50 mL
Date Analyzed: 01/28/2010 1915
Date Prepared: 01/28/2010 1200
Final Weight/Volume: 50 mL
Analyte
Spike Amount Result
% Red.
Limit
Arsenic
2.00 1.94
97
85 - 115
Barium
Cadmium
2.00 2.05
103
85 - 115
Chromium
0.0500 0.0493
99
85 - 115
Lead
0.200 0.201
100
85 - 115
0.500 0.492
98
85 - 115
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 9 of 19

Client: CSX Transportation
Matrix.Spike/
Matrix.Spike Duplicate Recovery Report - Batch: 680-159407
MS Lab Sample ID: 680-54502-1 Analysis Batch: 680-159539
Client Matrix: Water Prep Batch: 680-159407
Dilution: 1.0
Date Analyzed: 01/28/2010 1936
Date Prepared: 01/28/2010 1200
Quality Control Results
Job Number: 680-54502-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICP/AES -.D
Lab File ID: N/A
Initial Weight/Volume: 50 mL
Final WeighWolume: 50 mL
MSD Lab Sample ID: •
680-54502-1
Analysis Batch:
680-159539
Instrument ID: ICP/AES - D
Client Matrix:
Water
Prep Batch: 680-159407
Lab File ID: • N/A
Dilution:
1.0
Initial Weight/Volume: 50 mL
Date Analyzed:
01/28/2010 1941
Final Weight/Volume: 50 mL
_ Date Prepared:
01/28/2010 1200
% Rec.
Analyte
MS MSD
Limit
RPD
RPD Limit MS Qual MSD Qual
Arsenic
94 99
75 - 125
5
20
Barium
100 105
75 - 125
5
20
Cadmium
95 100
75 - 125
5
20
Chromium
96 102
75 - 125
6
20
Lead
94 100
75 - 125.
5
20
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 10 of 19

Quality Control Results
Client: CSX Transportation
.
Job Number: 680-54502-1
Method Blank - Batch: 680-159408
Method: 200.7 Rev 4.4
Preparation: 200.7
Total Recoverable
Lab Sample ID: MB 680-159408/7-A
Analysis Batch: 680-159539
Instrument ID: ICP/AES - D
Client Matrix: Water
Prep Batch: 680-159408
Lab File ID: N/A
Dilution: 1.0
Units: mg/L'
Initial Weight/Volume: 50 mL
Date Analyzed: 01/28/2010 1747
Date Prepared: 01/28/2010 1203
Final Weight/Volume: 50 mL
Analyte
Result
Qual '
MDL RL
Arsenic
Barium
0.020 _
U
_. ........ _ ..
0.010 0.020
Cadmium
0.010
U
0.0020 0.010
Chromium
0.0050
U
0.0020 0.0050
Lead
0.010
U
0.0020 0.010
1
0.010
U
0.0034 0.010
Lab Control Sample - Batch: 680-159408
Method: 200.7 Rev 4.4
Preparation: 200.7
i
Total Recoverable
Lab Sample ID: LCS 680-15940818-A
Analysis Batch: 680-159539
Instrument ID: ICP/AES - D
Client Matrix: Water
Prep Batch: 680-159408
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial WeighWolume: 50 mL
Date Analyzed: 01/28/2010 1752
Final WeighWolume: 50 mL
Date Prepared: 01/28/2010 1203
Analyte
Spike Amount Result
% Rec.
Limit Qua]
Arsenic ^
2.00 1.98
99
85 - 115
Barium,
2.00 2.07
104
85 - 115
Cadmium
0.0500 0.0503
101
85 - 115
Chromium
0.200 0.204
102
85 - 115
Lead
0.500 0.504
101
85 - 115
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 11 of 19

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-159408
MS Lab Sample ID:
680-54502-1
Analysis Batch: 680-159539
Client Matrix:
Water
Prep Batch: 680-159408
Dilution:
1.0
Date Analyzed:
01/28/2010 1813
Date Prepared:
01/28/2010 1203
MSD Lab Sample ID:
680-54502-1
Analysis Batch: 680-159539
Client Matrix:
Water
Prep Batch: 680-159408
Dilution:
1.0
Date Analyzed:
01/28/2010 1818
Date Prepared:
01/28/2010 1203
Quality Controi Results
Job Number: 680-54502-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Dissolved
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Instrument ID: ICP/AES - D
Lab File ID: N/A
Initial WeighttVolume: 50 mL
Final Weight/Volume: 50 mL
% Rec.
Analyte
MS
MSD
Limit
RPD
RPD Limit MS Qual MSD Qual
Arsenic
98
99
75 - 125
1
20
Barium
102
102
75 -125
0
20
Cadmium
99
99
75 - 125
0
20
Chromium
100
100
75 - 125
0
20
Lead
98
99
75; 125
0
20
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page .12 of 19

Client: CSX Transportation
Method Blank -Batch: 680-159557
Lab Sample ID:
MB 680-15955711
Analysis Batch: 680-159557
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: - mg/L
Date Analyzed:
01/29/2010 1414
Date Prepared:
N/A
Analyte
Result
Nitrate as N
0.050
Lab Control Sample - Batch: 680-159557
Lab Sample ID: LCS 680-15955712 Analysis Batch: 680-159557
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 01/29/2010 1414
Date Prepared: N/A
Quality Control Results
Job Number: 680-54502-1
Method: 353.2
Preparation: N/A
°
Instrument ID:, KoneLab2
Lab File ID: N/A
Initial Weight/Volume: 2
mL
Final Weight/Volume: 2
mL
Qual MDL
RL
U 0.010
0.050
Method: 353.2
Preparation: N/A
Instrument ID: KoneLab2
Lab File 10: N/A
Initial Weight/Volume: 2
mL
Final Weight/Volume: 2
mL
Analyte Spike Amount Result % Rec. Limit
Qual
Nitrate as N 0.989 1.02 103 90 - 110
Matrix Spike/ Method: 353.2
Matrix Spike Duplicate Recovery Report - Batch: 680-159557 Preparation: N/A
MS Lab Sample ID: 680-54321-F-1 MS
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
01/29/2010 1414
Date Prepared:
N/A
MSD Lab Sample ID:
680-54321-F-1 MSD
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
01/29/2010 1414
Date Prepared:
N/A
Analysis Batch: 680-159557
Prep Batch: N/A
Analysis Batch: 680-159557
Prep Batch: N/A
% Rec.
Analyte MS MSD Limit
Nitrate as N 92 96 90 - 110
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 13 of 19
Instrument ID: KoneLab2
Lab File ID: N/A
Initial Weight/Volume: 10 mL
Final WeightlVolume: 10 mL
Instrument ID: KoneLab2
Lab File ID: N/A
Initial Weight/Volume: 10 mL
Final WeighWolume: 10 mL
RPD RPD Limit MS Qual MSD Qual
2 10

Client: CSX Transportation
Method Blank - Batch: 680-159316
Lab Sample ID: MB 680-159316/1 Analysis Batch: 680-159316
Client Matrix: Water Prep -Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 01/27/2010 1518
Date Prepared: N/A
Quality Control Results
Job Number: 680-54502-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte
Result,
Qual RL RL
Total Dissolved Solids
5.0
U 5.0 5.0
Lab Control Samplel
Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680-159316
Preparation: N/A
LCS Lab Sample ID:
LCS 680-159316/2
Analysis Batch:
680-159316
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: NIA
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed:
01/27/2010 1518
Final Weight/Volume: 100 mL
Date Prepared:
N/A
LCSD Lab Sample ID:
' LCSD 680-159316/3
Analysis Batch:
680-159316
! Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: ,-
1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed:
01/27/2010 1518
Final Weight/Volume: 100 mL
Date Prepared:
N/A
% Rec.
Analyte
LCS LCSD
Limit
RPD RPD Limit LCS Qual LCSD Qual
Total Dissolved Solids
85 85
80 - 120
1 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 14 of 19

Quality Control Results
Client: CSX Transportation Job Number: 680-54502-1
Duplicate -Batch: 680-159316 Method: SM 2540C
Preparation: N/A
Lab Sample ID: 680-54502-1 Analysis Batch: 680-159316 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial WeightfVolume: 100 mL
Date Analyzed: 01/27/2010 1518 Final WeightNolume: 100 mL
Date Prepared: N/A
Analyte Sample ResulUQual Result RPD Limit Qual
Total Dissolved Solids 52 59.0 13 25 .
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAriterica Savannah Page 15 of . 19

Client: CSX Transportation
Method Blank - Batch: 680-159858
Lab Sample ID:
MB 680-159858/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
02/02/2010 1042
Date Prepared:
NIA
Analysis Batch: 680-159858
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-54502-1
Method: SM 5310B
Preparation: N/A
Instrument ID: Total Organic Carbon Analyze
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Analyte
Result
Qual MDL RL
Total Organic Carbon
1.0
.... ........
_ _....... _ ....... .. _
U 0.50 1.0
Lab Control SampleV
Method: SM 5310B
Lab Control Sample Duplicate Recovery Report - Batch: 680-159858
Preparation: N/A
LCS Lab Sample ID:
LCS 680-15985814
Analysis Batch:
680-159858
Instrument ID: Total Organic Carbon Analyze
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 25 mL
Date Analyzed:
.02/02/2010 1115
Final Weight/Volume: 25 mL
Date Prepared:
N/A
LCSD Lab Sample ID:
LCSD 680-159858/5
Analysis Batch:
680-159858
Instrument ID: Total Organic Carbon Analy:
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 25 mL
Date Analyzed:
02/02/2010 1128
Final Weight/Volume: 25 mL
Date Prepared:
NIA
% Rec.
Analyte
LCS LCSD
Limit
RPD RPD Limit LCS Qual LCSD Qual
Total Organic Carbon
98 99
80 - 120
1 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 16 of 19

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-159858
Quality Control Results
Job Number:* 680-54502-1
Method: SM 5310B
Preparation: N/A
MS Lab Sample ID:
680-54490-H-2 MS
Analysis Batch: 680-159858
Instrument ID: Total Organic Carbon
Client Matrix:
Water
Prep Batch: N/A
Lab Fife ID: N/A
Dilution:
1.0
Initial Weight/Volume: 25 mL
Date Analyzed:
02/02/2010 1620
Final Weight/Volume: 25 mL
Date Prepared:
N/A
MSD Lab Sample ID:
680-54490-H-2 MSD
Analysis Batch: 680-159858
Instrument ID: Total Organic Carbon Analyze
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Initial Wefght/Volume: 25 mL
Date Analyzed:
02/02/2010 1633
Final WeighttVolume: 25 mL
Date Prepared:
N/A
% Rec.
Analyte
MS MSD Limit
RPD RPD Limit MS Qual MSD Qual
Total Organic Carbon
97 -98 80 -120......
.. .... 2 ' 25,
Duplicate -Batch: 680-159858
Method: SM 5310B
Preparation: N/A
Lab Sample ID: 680-54517-H-3 DU
Analysis Batch: 680-159858
Instrument ID: Total Organic Carbon Analyze
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial WeightNolume: 25 mL
Date Analyzed: 02/02/2010 1803
Final Weight/Volume: 25 mL
Date Prepared: N/A
Analyte
Sample Result/Qual Result
RPD Limit Qual
Total Organic Carbon
1.0 U , 1.0
NC 25 U
Calculations are performed before rounding to avoid round -off errors In calculated results.
TestAmerica Savannah Page 17 of 19
I
I

-
CHAIN OF
C"m
TRANSPORTATION C U STO �Y
LABORATORY INFORMATION
COC #:
O TestAmeriea Savannah - 5102 LaRuctre Avenuo, Savannah, GA 31404 P: 912-354-7858 F: 912-352-0'165
O restAmerica North Canton - 4101 Shultet Drive N%V. North'Canton, OH 44720 P- 330-497-939a F: 330-497-0772
Q TestAmerua Tampa - 6712 Benjamin Ruad, Suite IOG. 7antpe; FL 33634 P: d13.865-74Z7 F: 813 885-70 i9
❑ TestAmerica Pensacola - 3355 tdcLemore Drive. Pensacola, FL 32514 P: 850-474-1001 F: 850-'478.2671
Q TestAnterica Bullato - 10 Hazelvieod Drive. Suite 106, Nhheist. Ny 14228 'P: 715-691-2600 F: 716.96t-7991
Q Tesu+nenca Chicago - 2417 Bond Slreet, University Park IL 60466- P: 709-534-5200 F: 708.534-5211
SHIPMENT INFORMATION.
Shipment Method:
Shipment Tracking No.
CSXT PROJECT INFORMATION Pro]. State (State 01 Origin)
CONSULTANT INFORMATION Project H:
CSXT Project Number; ." Proj. City:
Company: PM:.'
CSXT Project Name: J ` ` L
^1
Address: Emaik . -
CSXT Contact: LWON: _ /
City, Slate, 2rp: Phone; Fax:
Turnaround Time: El Standard 6-13 Days
❑ A Day Rush Specity.9 Days _-
❑ 2 Day Rush Standard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: 3 = Sulfuric Acid Note too,
0 = No Preservatives 4 -'Sodium Thiosulfale Pres.
1 = Hydrochloric Acid ' 5 = Sodium Hydroxide Code
2 = Nitric Acid 6 = Other
2- L
COMMENTS
LAB USE
METHODS FOR ANALYSIS
J
,
Deliverables: ❑ .Other Deliv: __-__
❑ CSXT Standard (Level II) _ • •�.,_�
❑ Level III ❑ EDD Required, Format:
❑ Level IV
Matrix Codes: SO = Soil LIQ = Liquid
GW = Groundwater SL = Sludge
WW = Waste Water OI = Oil
SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION
Sample )denuitcauon
Containers
Sample Collection
Filtered
I Type
Matrix
Number &
Type
Date
Time
Sampler
Y or N
Comp"
or Grab
Code
— r — 7� _
2-T-0
ll5i
Q
_,
.
vvw
11
IZSat(
Relinquished By:
Date/l-ime:
Race a
el-rime:�3
Comments & Special Analytical Requirements: "
n
Relinquished By:
Dale(Tirna:
Received By;
aieCTime:
Relinquished By:
DaieFTime:
Received By.
Date(Fime:
co end By Laboratory:
1 ll is
Datemme:
- 1- C
L
-. •
LA13 USE: Cuslody Intact
❑Yes .❑No
Custody Seal It
'b.
LAB Log Number:: .
- E
UHIUNAL-Ht I UHN I ULAbUKAIt1KY VVIFgbAhtt"r.tb 1 tU nvvut.CmUaI at avnMlldtu- IV lrbA I vvI I HUrAIUI ALUVU TnL-%06(0509)

Login Sample receipt Check List
Client: CSX Transportation
Login Number: 54502
Creator: Daughtry, Beth
List Number: 1
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with,
Samples,were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample coritainers have legible labels.
Containers are not broken or leaking.
Sample tollection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, in any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter,
If necessary, staff have been Informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
T / F/ NA Comment
N/A
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
N/A
True
N/A
N/A
False
True
TestAmerica Savannah
Page 19 of 19
Job Number: 680-54502-1
List Source: TestAmerica Savannah

WQ0000601 o CSX'T HAMLE'T9 NC
FEBRUARY 2010

ATTACHMENT A — LIMITATIONS AND MONITORING REQUIREMENTS
Permit
Number:
WQ0000601
'version: 3.0
PPI 001— WWTF Effluent
EFFLUENT CIIAR� 'TEI2IISTICS
Parameter Description -parameter Code
EFFLUENT LIMITS
iwi�1VITORIIVG REQUIRE
Monthly Average
Flow, in conduit or thru treatment plant - 50050
tm
9Weekly Average
Dae ly Maximum
Monitoring Frequency Sample P Type
1.0 mad
Solids, Total Dissolved - 180 Deg.0 - 70300
Continuous
Recorder
Of - 00400
%'i✓0
le L
3 X year
Grab
Carbon, 'Total Organic (•TOC) - 00680
3 X year
Grab
Nitrogen, Nitrate'I'otal-(as N) - 00620
L
3 X year
Grab
Barium, "Total (as Ba) - 01007
3 X year
Grab
Cadmium, Total (as Cd) - 01027
6. 011'
j% d.
3 X year
Grab .
Chromium, Total (as Cr) - U 1034
L O . bts
�.
3 X year
Grab
Lead, Total (as l'b) - 01051 -
t a • a i
py
3 X year
Grab
Arsenic, Total (as As)-'01002
3 X year
Grab
3 X year monitoring shall be conducted in March, July November.
3 X year
Grab
and
r -
WQ0000601 Version 3.0
Attachment A
Pale I of l

Test-Ait-me'rica
C
THE LEAOFR IN ENVIRONNIE..NrAL TESTING
ANALYTICAL REPOkT
Job Number: 680-55328-1
Job Description: CSX Hamlet, NC WWTP Monthly
.For:
CSX Transportation
500 Water Street
Jacksonville, FL 32202
Attention: Mr. Mike Gregory
Approved for release.
Kathryn Smith
Project Manager 1
315/2010 4:10 PM
Kathryn Smith
Project Manager I
[e-mail]
03/05/2010
cc: Mr. Jerry Cato
Mr. Alan Pinnix
L WON-ENV0000027258//Project-R000011790
The test results in'this report meet NELAP requirements for parameters for which accreditation is required or available. -
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except In full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report,
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOR; CA: 03217CA; CO; CT:
PH0161; DE; FL; E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS; E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; Rl: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI ONR: 999819810; WY/EPAR8: 8TMS-Q "
TestAmerica Laboratories, Inc. 11i FOccaQ
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, 6A 31404
Tel [phone] Fax [phone] �Yy{w tQstamericainc,.�Qm �Y
ne
Page 1 of 19

, 1
Job Narrative
680-55328-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
i
Page 2 of 19

METHOD SUMMARY
Client: CSX Transportation
Job Number: 680-55328-1
Description
Lab Location Method Preparation Method
Matrix Water
i Metals (ICP)
TAL SAV 40CFR136A 200.7 Rev 4.4
Preparation, Total Metals
TAL SAV EPA 200.7
HEM and SGT-HEM
TAL SAV 1664A 1664A
HEM and SGT-HEM (Aqueous)
TAL SAV 1664A 1664A
Nitrogen, Nitrate -Nitrite
TAL SAV MCAWW 353.2
Solids, Total Dissolved (TDS)
TAL SAV SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendiic A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions,
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 19

J
METHOD / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-55328-1
Method
r
Anal st
-
Analyst ID
40CFR136A 200.7 Rev 4.4
Bland, Brian
BCB
1664A 1664A
Samuel, Sarita
SS
MCAWW 353.2
Ross, Jon
JR
SM SM 2540C
Jackson, Michelle S
MSJ
SM SM 5310E
Blackshear, Kim
KB
TestAmerica Savannah
Page 4 of 19,

SAMPLE SflJflldMARY
Client: CSX Transportation \ Job Number: 680-55328-1
Lab Sample ID Client Sample ID Client Matrix Date/Time Date/Time
Sampled Received _
680-55328-1 Water Sample Water 02/24/2010 1015 02/25/2010 1008
I
TestAmerica Savannah
Page-5 of.19

Analytical Data
Client: CSX Transportation -Job Number: 680-55328-1
Client Sample ID: Water Sample
Lab Sample ID:
680-55328-1
Date Sampled: 02/24/2010 1015
Client Matrix:
Water
Date
Received: 02/25/2010 1008
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-162180
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-161721
Lab File ID:
NIA
Dilution:
1.0
Initial Weight/Volume:
50 mL
Date Analyzed:
03/03/2010 1231
Final Weight/Volume::
50 mL
Date Prepared:
02/25/2010 1701
Analyte
Result m /L
Qualifier
MDL
RL
Arsenic
0.020
U-
0.0046
0.020
Barium
0.618
0.0023
0.010
Cadmium
0.0050
U
-0.0020
0,0050
Chromium
0.010
U
0.0012
0.010
Lead
0.010
U
0.0040
0.010
0
TestAmerica Savannah
Page 6 of 19

Analytical Data
Client: CSX Transportation Job Number: 680-55328-1
General Chemistry
Client Sample ID: Water Sample
Lab Sample ID:' 680-55328-1
Client Matrix: Water
Date Sampled: 02/24/2010 1015
Date Received: 02/25/2010 1008
Analyte Result
Qual Units MDL
RL
Dil
Method
HEM Oil & Grease 1.9
...
J m !L 1.4
5.0
- 1.0
1664A
Analysis Batch: 680-161983
Date Analyzed: 03/02/2010 1421
Prep Batch: 680-161957
Date Prepared: 03/01/2010 1726
Nitrate as N 0.81
mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-162120
Date Analyzed: 02/25/2010 1625
Total Organic Carbon 5.4
mg/L 0.50
1.0
1.0.
SM 53108
Analysis Batch: 680-162348
Date Analyzed: 03/04/2010 1758
Analyte Result
Qual Units RL
RL
Dii
Method
Total Dissolved Solids 140
mg/L 5.0'
5.0
1.0
SM 2540C
Analysis Batch: 680.161708
Date Analyzed: 02/25/2010 1553
TestAmerica Savannah Page 7 of 19

DATA REPORTING QUALIFIERS
Client: CSX Transportation Job Number: 680-55328-1
Lab Section Qualifier Description
Metals
U Indicates the analyte was analyzed for but not detected.
General Chemistry
113
TestAmerica Savannah
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
Page 8 of 19

Client: CSX Transportation
Method Blank -Batch: 680-161721
Lab Sample ID: MB 680-161721/11-A
Client Matrix: Water
Dilution: 1,0
Date Analyzed: 03/03/2010 1117
Date Prepared: 02/25/2010 1701
Analysis Batch: 680-162180
Prep Batch: 680-161721 -
Units: mg/L
Analyte
Result
Qual
Arsenic
..
Barium
0.020
U
0 .010
U
Cadmium
0.0050
U0.010
Chromium
U
Lead -
0.010
U
Lab Control Sample - Batch: 680-161721
Lab Sample ID:
LCS 680-161721112-A
Analysis Batch: 680-162180
Client Matrix:
Water
Prep Batch: 680-161721
Dilution:
1.0
Units: mg/L
Date Analyzed:
03/03/2010 1129
Date Prepared:
02/25/2010 1701
Quality Control Results
Job Number: 680-55328-1
Method: 200.7 Rev 4,4
Preparation: 200.7
Instrument ID: ICPD
Lab File ID: N/A
Initial Wetght/Volume: 50 mL
Final WeighWolume: 50 mL
MDL
RL
0.0046
0.020
0.0023
0.010
0.0020
0.0050
0.0012
0.010
0.0040
0.010
Method: 200.7 Rev 4.4
Preparation: 200;7
Instrument ID: ICPD
Lab File ID: N/A
Initial WeighWolume: 50
mL
Final Weight/Volume: 50
mL
Analyte Spike Amount
Result
i
% Rec.
Limit
Arsenic 2.00
Barium
1.86
.93
85 - 115
2.00
Cadmium
1.91
96
85 - 115
0.0500
Chromium
0.0473
95
85 -115
0.200
Lead
0,190
95
85 - 115
0.500
0.472
94
85 - 115
Calculations are performed before rounding to avoid round -off errors in
calculated results.
TestAmerica Savannah Page
9 of 19
Qual

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-161721
i
Quality Control Results
Job Number: 680-55328-1
Method: 200.7 Rev 4.4
Preparation: 200.7
MS Lab Sample ID:
680-55299-A-4-B MS
Analysis Batch:
680-162180
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-161721
Lab File ID: N/A
Dilution:
1.0
Initial Weight/Volume: 50 mL
Date Analyzed:
03/03/2010 1150
Final Weight/Volume: 50 mL
Date Prepared!
02/25/2010 1701
MSD Lab Sample ID:
680-55299-A-4-C MSD
Analysis Batch:
680-162180
Instrument'ID: ICPD
Client Matrix:
Water
Prep Batch: 680-161721
Lab File ID: N/A
Dilution:
1.0
Initial WeighWolume: 50 mL
Date Analyzed:
03/03/2010 1155
Final We[ghtNolume: 50 mL
Date Prepared:
02/25/2010 1701
% Rec.
Analyte
MS MSD
Limit
RPD
RPD Limit MS Qual MSD Qua[
Arsenic
97 99
75 - 125
2
20
Barium'
99 101
75 -125
3
20
Cadmium
97 98
75 - 125
1
20
Chromium
99 101
75 - 125
.3
20
Lead
97 99
75 - 125
3
20
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 10 of 19

Client: CSX Transportation
.Method Blank - Batch: 680.161957
Quality Control Results
Job Number: 680-55328-1
Method: 1664A
Preparation: 1664A
Lab Sample ID: MB 680-161957/20-A
Client Matrix: Water
Analysis Batch: 680-161983
Instrument ID: No Equipment Assigned
Dilution: 1.0
Prep Batch: 680-161957
.
Lab File ID: N/A
Date Analyzed: 03/02/2010 1421
Units: mg/L
Initial WeighWolume: 500 mL
Date Prepared: 03/01/2010 1726
Final Weight/Volume: 500 mL
Analyte
Result
Qual DL RL
HEM (Oil & Grease)
" "" �� • • ••�
• _ ........
5.0
_.. ..
� 1.4 5.0
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report
- Batch: 680-161957
Method: 1664A
Preparation: 1664A
LCS Lab Sample ID: LCS 680-161967/21-A
Client Matrix:
Analysis Batch: 680-161983
Instrument ID: No Equipment Assigned
Water
Dilution: 1.0
Prep Batch: 680-161957
Lab File ID: N/A
DAte Analyzed: 03/02/2010 1421
Units: mg/L
Initial WeighWolume: 500 mL
Date Prepared: 03/01/2010 1726
Final.WelghWolume: 500 mL
LCSD Lab Sample ID: LCSD 680-161957/22-A
Client Matrix:
Analysis Batch: 680-161983
Instrument ID: No Equipment Assigned
Water
Dilution: 1
Prep Batch: 680-161957
Lab File ID: N/A
Date -Analyzed: 03/3/ 02/2010 1421
Units: mg/L
Initial Weight/Volume: 500 mL
Date Prepared: 03/01/2010 1726
Final Weight/Volume: 500 mL
Rec.-
Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual
HEM (Oil &Grease) -18 -�•- -•�• • ••• •.
85 82 78 - 114 3 __..
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 11 of 19

Quality Control Results
Client: CSX Transportation
Job Number: 680-55328-1
Method Blank - Batch: 680-162120
Method: 353.2
Preparation: NIA
Lab Sample ID: MB 680-162120/1
Analysis Batch: 680-162120
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: NIA
Dilution: 1.0
Units: mg/L
Initial WeighWolume: 2 mL
Date Analyzed: 03/02/2010 1656
Final Weight/Volume: 2 mL
Date Prepared: N/A
Analyte
Result
Qua[ MDL RL
................_.....-......w
Nitrate as N
... ....... _
0,050
._.... ... _ _....._....._............. _._ ...._......._ ..__ _... .__......._. _
U 0.010 0.050
Lab Control Sample - Batch: 680-162120
Method: 353.2
Preparation: NIA
Lab Sample ID: LCS 680-162120/2
Analysis Batch: 680-162120
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: NIA
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 2 mL
Date Analyzed: 03/02/2010 1656
Final Weightolume: 2 mL
Date Prepared: N/A
Analyte
Spike Amount Result
% Rec. Limit Qual
Nitrate as N
0.989 1.02
103 90 - 110
Matrix Spike/
Method: 353.2
Matrix Spike Duplicate Recovery Report -
Batch:.680-162120
Preparation: N/A
MS Lab Sample ID: 680-55082-D-1 MS
Analysis Batch: 680-162120
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Initial Weight/Volume: 10 mL
Date Analyzed: 02/16/2010 1229
Final WeighWolume: 10 mL
Date Prepared: N/A
MSD Lab Sample ID: 680-55082-D-1 MSD
Analysis Batch: 680-162120
Instrument ID: KONELA82
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Initial WeighWolume: 10 mL
Date Analyzed: 02/16/2010 1229
Final Weight/Volume: 10 mL
Date Prepared: N/A
% Rec.
Analyte
MS MSD Limit
RPD RPD Limit MS Qual MSD Qual
Nitrate as N
100 102 90 -110
3 10
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 12 of 19

Client: CSX Transportation
Duplicate -Batch: 680-162120
Lab Sample ID:
680-55184-G-4 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
02/19/2010 1643
Date Prepared:
NIA
Analysis Batch: 680-162120
Prep Batch: N/A
Units: mg/L
Analyte Sample Result/Quai
Nitrate as N 1.5
Quality Control Results
Job Number: 680-55328-1
Method: 353.2
Preparation: N/A
Instrument ID: KONELAB2
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Result RPD Limit Qual
1.50 3 .10'.
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 13 of 19
0

Quality Control Results
Client: CSX Transportation
Job Number: 680-55328-1
Method Blank - Batch: 680-161708
Method: SM 2540C
Preparation: NIA
Lab Sample ID: M8 680-161708/1
Analysis Batch: 680-161708
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: NIA
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial WeightlVolume: 100 mL
Date Analyzed: 02/25/2010 1553
Final Weight/Volume: 100 mL
Date Prepared: N/A
Analyte
Result
Qual RL RL
Total Dissolved Solids
5.0
U 5.0 5.0
Lab Control Sample/
Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680-161708
Preparation: N/A
LCS Lab Sample ID: LCS 680-161708/2
Analysis Batch: 680-161708
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: NIA
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed: 02/25/2010 1553
Final Weight/Volume: 100 mL
Date Prepared: N/A
LCSD Lab Sample ID: LCSD 680-16170813
Analysis Batch: 680-161708
Instrument ID: No Equipment Assigned
Client. Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial WeighWolume: 100 mL
Date Analyzed: 02/25/2010 1553
Final Weight/Volume: 100 mL
Date Prepared: N/A
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qual LCSD Qual
Total Dissolved Solids
88 96 80 - 120
8 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 14 of 19

Client: CSX Transportation
Duplicate -Batch: 680-161708
Lab Sample ID:
680-55253-E-1 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
02/25/2010 1553
Date Prepared:
N/A
Analysis Batch: 680-161708
Prep Batch: N/A
Units: mg/L
I
Quality Control Results
Job Number: 680-55328-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte
Sample Result/Qual
Result
RPD
Limit Qual
Total Dissolved Solids
270
264
1
25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 15 of 19

Quality Control Results
Client: CSX Transportation Job Number: 680-55328-1
Method Blank -Batch: 680-162348
Method: SM 5310B
Preparation: N/A
Lab Sample ID: MB 680-162348/2
Analysis Batch: 680-162348
Instrument ID: TOC3
Client Matrix: Water
Prep Batch: N/A
Lab File ID: NIA
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
25 mL
Date Analyzed: 03/04/2010 1341
Final Weight/Volume:
25 mL
Date Prepared: N/A
J
Analyte
Result Qual
MDL
RL
_.._....._._._.....___._..-•___.___.._....._...
Total Organic Carbon
..._............._._._._......_..___._.._..._....__...--.-.__-_..
1.0 U
__.._.__....._._.._........__._....._...___
0.50
1.0
Lab Control Sample - Batch:.680.162348
Lab Sample ID:
LCS 680-162348/4
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/04/2010 1412
Date Prepared:
N/A
Analysis Batch: 680-162348
Prep Batch: N/A
Units: mg/L
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: N/A
Initial WeighWolume: 25 mL
Final WeighWolume: 25 mL
Analyte
Spike Amount
Result
% Rec. Limit Qual
Total Organic Carbon
20.0
19.2
96 80 - 120
Matrix Spike/
Method: SM 5310B
Matrix Spike Duplicate Recovery Report -
Batch: 680-162348
Preparation: N/A
MS Lab Sample ID:
680-55271-H-1 MS
Analysis Batch:
680-162348
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: 'N/A
Dilution:
1.0
Initial Weight/Volume: 25 mL
Date Analyzed:
03/04/2010 1712
Final Weight/Volume: 25 mL
Date Prepared:
N/A
MSD Lab Sample ID:
680-55271-H-1 MSD
Analysis Batch:
680-162348
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID:. N/A
Dilution:
1.0
Initial WeighWolume: 25 mL
Date Analyzed:
03/04/2010 1725
Final WeightlValume: 25 mL
Date Prepared:
N/A
% Rec.
Analyte
MS MSD
Limit
RPD RPD Limit MS Qual MSD Qual
Total Organic Carbon
106 106
80 - 120
0 25
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 16 of 19

Quality Control Results
` Client: CSX Transportation Job Number: 680-55328-1
Duplicate - Batch: 680-162348 Method: SM 5310B
Preparation: N/A,
Lab Sample ID: 680-55372-C-1 DU Analysis Batch: 680-162348 Instrument ID:. TOC3
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL
Date Analyzed: 03/04/2010 1610 Final Weight/Volume: 25 mL
Date Prepared: NIA
Analyte ' Sample Resuli/Qual Result RPD Limit Qual
Total Organic Carbon 1.0 U 1.0 NC 25 U
r
Calculations are performed before rounding to avoid round -off errors in calculated results.
TestAmerica Savannah Page 17 of 19

LABORATORY INFORMATION
Coe #
astAmeriraSavanmh . 5102 LaRoche Aveuue, Savahnah, GA 3Td'04 P: 912-354-7858 F: 9t2-352-0165
CHAIN F
OTestAmedra North Canton - 4101 Shuflel Drive NW, North Caulon. OH 44720 P: 330-497-9396 F:330-497.0772
❑ TestAmerica Tampa - 6712 Benjamin Road. Suite 100. Tampa, FL 33634 P: 813-885-7427 F: 813.885-7049
SHIPMENT INFORMATION
Shipment Method:
CUSTODY
❑TesiAittericaPensarala-3355ticLentoreDtive.Pensacota,FL32514 P:850-474-1001 F:850-478.2671
TRANSPORTATION
❑ TestAmerica Butlalo -10 tiamlrrood DOic, Suite I R Amnelet. NY 14228 P: 716-691-2600 F: 716-961.7991
Shipment Tracking No:
p ToctAmenca Chicago . 2417 Boud Street, University Park. IL 60466 P:908.534.5200 F. 708.534-5211
CSXT PROJECT INFORMATION Proj. State (State of Origin) , "
CONSULTANT INFORMATION Project 4:
CSXT Project Number: Pf0j. City: _
7
Company: PM:
CSXT Project Name:
fr`fF1 �a-o
Address. EmaiL-
CSXT ConlacL LWON: V /�
City, State, Zip: Phone: Fax:
r ` r
Turnaround Time: ❑ Standard 6-13 Days
Preservative Codes: 3 = Sulfuric Acid Note
COMMENTS
LAB USE
METHODS FOR ANALYSIS
❑ 1 Day Rush 3 ify to Days _-
0 = No Preservatives 4 = Sodium Thiosultate Pres.
❑ 2 Day Rush Standard 14 Days
1 = Hydrochloric Acid 6 = Sodium Hydroxide Code
❑ 3 Day Rush ❑ Other
= Nitric Acid 6 = Other
t
V
(�
Dell.vembles: ❑ Other Deliv:
Matrix Codes_ SO = Soil LIQ = Liquid
GW Groundwater SL Sludge
El CSXT Standard (Level II) _
= =
Q
Lovei Iii u cuv required, Foromi_
u-v'ri='vvasia'vvaier' Oi = Oil
'�rn
Level IV _
SW = Surface Water SOL = Other Solid
v,
0
tv
SAMPLE INFORMATION
Containers
Sam le Collection
Filtered
Type
Matrix
Number &
Date
Time
Sampler
Y or N
Comp
Grab
.Code
Sample identification
-
V
Type
or
ff� 1
^C;
S 'f
II
�7 d
o,I
v1�
NLv
WD
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spL
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n e� " v v ,4,a -_C
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2
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. I
2-112411,8
r'l
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;?24/1 b
t
3
1.
DP IS
C( C
ReiinquishedBy:
Dalelrme:
Receiv
Dalemme:
Comments Analytical Requirements:
1 q
26 '
^&�Special
�C1 t� yJ - �0
1
,
RoWu4wshodBy:
Datemme:
ecaived lir
DaWTimm
Rrdinquisrted By:
Detect-ime:
Received By:
DalerTime:
rR coved By Laktaelary:
DalalTime:
r `
Lab Remarks:
LAB USE: Custody Intact
❑Yes ❑No
Custody Seat a
LAB Lo Number _
r7r7 �7
' 1 in I, 1 t 1
<�• rQ I ) )
11
IY
ORIGINAL - RETURN TO LABORATORY Wt(N SAMPLES INVUlUe Mus I uta SU1JM1 I I to I V C iX I YY1 I t-1 VK[UtNAL tic: TAL-6005 (0509)

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYMAL REPORT
Job Number: 680-56297-1
Job Description: CSX Hamlet, NC WWTP Monthly
For:
CSX Transportation
500 Water Street
Jacksonville, FL 32202
Attention: Mr. Mike Gregory
r�j'p)` Approved for release.
4 Kathryn Smith
Project Manager I
4/16/2010 7:29 PM
. Kathryn Smith
Project Manager I
[e-mail]
04/16/2010
cc: * Mr. Jerry Cato
Mr. Alan Pinnix
LWON-ENV0000027258//Project-R000011790
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY•EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 20.08022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DER 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc. �tk A001.0 y
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericainc.com
� �=z
Page 1 of 18

Job Narrative
680-56297-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
Method(s) 353.2: The following sample(s) was analyzed outside of analytical holding time: March Outfall 2010 (680-56297-1).
No other analytical or quality issues were noted
Page 2 of 18

METHOD SUMMARY
Client: CSX Transportation Job Number: 680-56297-1
Description Lab Location Method Preparation Method
Matrix: Water
Metals (ICP)
TAL SAV 40CFR136A 200.7 Rev 4.4
Preparation, Total Metals
TAL SAV EPA 200.7
HEM and SGT-HEM
TAL SAV 1664A 1664A
HEM and SGT-HEM (Aqueous)
TAL SAV 1664A 1664A
Nitrogen, Nitrate -Nitrite
TAL SAV MCAWW 353.2
Solids, Total Dissolved (TDS)
TAL SAV SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal
Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
ER, = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes",
EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 18

METH®® / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-56297-1
Method
Analyst
Analyst ID
40CFR136A 200.7 Rev 4.4
Bland, Brian
BCB
1664A 1664A
Samuel, Sarita
SS
MCAWW 353.2
Ross, Jon
JR
SM SM 2540C
Jackson, Michelle S
MSJ
SM SM 53108
Blackshear, Kim
KB
6
TestAmerica Savannah
Page 4 of 18

SAMPLE SUMMAIIY
Client: CSX Transportation
Job Number: 680-56297-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-56297-1 March Outfall 2010 Water 03/36/2010 0920 03/31/2010 0945
TestAmerica Savannah
Page 5 of 18

Analytical Data
Client: CSX Transportation Job Number: 680-56297-1
Client Sample ID:
March Outfall 2010
Lab Sample ID:
680-56297-1
Date
Sampled: 03/30/2010 0920
Client Matrix:
Water
Date
Received: 03/31/2610 0945
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-164781
Instrument ID:
ICPD
Preparation:
200.7
Prep Batch: 680-164572
Lab File ID:
N/A -
Dilution:
1.0
Initial Weight/Volume:
50 mL
Date Analyzed:
04/02/2010 1330
Final Weight/Volume:
50 mL
Date Prepared:
03/31/2010 1445
Analyte
Result (mg/L)
Qualifier
MDL
RL
rse Anic
0.020
U
0.0046
0.020
Barium
0.017
0.0023
0.010
Cadmium
0.0050
U
0.0020
0.0050
Chromium
0.010
U
0.0012
0.010
Lead
0.010
U
0.0040
0.010
TestAmerica Savannah Page 6 of 18

Analytical Data
Client: CSX Transportation Job Number: 680-56297-1
General Chemistry
Client Sample ID:
Lab Sample ID
Client Matrix:
March Outfall 2010
680-56297-1
Water
Date Sampled: 03/30/2010 0920
Date Received: 03/31/2010 0945
Analyte Result
Qual Units MDL
RL
Dil
Method
HEM (Oil & Grease) 2.8
J mg/L 1.4
&0
1.0
1664A
Analysis Batch: 680-165001
Date Analyzed: 04/06/2010 2132
Prep Batch: 680-164987
Date Prepared: 04/06/2010 1735
Nitrate as N 0.025
J H mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-165215
Date Analyzed: 04/01%2010 1333
Total Organic Carbon , 10
mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-165297
Date Analyzed: 04/08/2010 2118
Analyte Result
Qua] - 'Units RL
RL
Dil
Method
Total Dissolved Solids 120
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 680-164576
Date Analyzed: 03/31/2010 1500
TestAmerica Savannah Page 7 of 18

DATA REP®RTNG QUALIFIERS
Client: CSX Transportation Job Number: 680-56297-1
Lab Section Qualifier Description
Metals
U Indicates the analyte was analyzed for but not detected.
General Chemistry
U Indicates the analyte was analyzed for but not detected. '
J Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
H Sample was prepped or analyzed beyond the specified holding
time
TestAmerica Savannah
Page 8 of 18

Quality Control Results
Client: CSX Transportation Job Number: 680-56297-1
Method Blank -Batch: 680-164572
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
MB 680-164572/7-A
Analysis Batch: 680-164781
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-164572
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeighWolume: 50
mL
Date Analyzed:
04/02/20.10 1220
Final Weight/Volume: 50
mL
Date Prepared:
03/31/2010 1445
Analyte
'Result
Qua[
MDL
RL
Arsenic
0.020
U
0.0046
0.020
Barium
0.010
U
0.0023
0.010
Cadmium
0.0050
U
0.0020
0.0050
Chromium
0.010
U
0.0012
0.010
Lead
0.010
U
0.0040
0.010
Lab Control Sample - Batch: 680-164572
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
LCS 680-164572/8-A
Analysis Batch: 680-164781
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-164572
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 50'
mL
Date Analyzed:
04/02/2010 1226
Final Weight/Volume: 50
mL
Date Prepared:
03/31/2010 1445'
Analyte
Spike Amount Result
% Rec. Limit
Qual
Arsenic
2.00 1.95
98
85 - 115
Barium
2.00 2.04
102
85 - 115
Cadmium
0.0500 0.0498
100
85 - 115
Chromium
0.200 0.202
101
85 - 115
Lead
0.500 0.495
99
85 - 115
TestAmerica Savannah Page 9 of 18

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-164572
MS Lab Sample ID:
680-56270-A-1-B MS
Analysis Batch: 680-164781
Client Matrix:
Water
Prep Batch: 680-164572
Dilution:
1.0
Date Analyzed:
04/02/2010 1303
Date Prepared:
03/31/2010 1445
MSD Lab Sample ID:
680-56270-A-1-C MSD
Analysis Batch: 680-164781
Client Matrix:
Water
Prep Batch: 680-164572
Dilution:
1.0
Date Analyzed:
04/02/2010 1309
Date Prepared:
03/31/2010 1445
Quality'Control Results
Job Number: 680-56297-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICPD
Lab File ID: N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Instrument ID: ICPD
Lab File ID: N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
MS
% Rec.
MSD
Limit
RPD
RPD Limit MS Qual MSD Qual
Arsenic
95
90
75 - 125
5
20
Barium
99
93
75 - 125
6
20
Cadmium
97
91
75 - 125
6
20
Chromium
98
92.
75 - 125
6
20
Lead
95
90
75 - 125
6
20
r
TestAmerica Savannah Page 10 of 18
J

Quality Control Results
Client: CSX Transportation Job Number: 680-56297-1
Method. Blank - Batch: 680-164987
Method: 1664A
Preparation: 1664A
Lab Sample ID: MB 680-164987/18-A
Analysis Batch: 680-165001
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-164987
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 500 mL
Date Analyzed: 04/06/2010 2132
Final Weight/Volume: 500 mL
Date Prepared: 04/06/2010 1735
Analyte
Result
Qual MDL RL
HEM (Oil & Grease)
5.0
U 1.4 5.0
Lab Control Sample/
Method: 1664A
Lab Control Sample Duplicate Recovery Report - Batch: 680-164987
Preparation: 1664A
LCS Lab Sample ID: LCS 680-164987/19-A
Analysis Batch: 680-165001
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-164987
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 500 mL
Datp Analyzed: 04/06/2010 2132
Final WeighWolume: 500 mL
Date Prepared: 04/06/2010 1735
LCSD Lab Sample ID: LCSD 680-164987/20-A
Analysis Batch: 680-165001
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-164987
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 500 mL
Date Analyzed: 04/06/2010 2132
Final WeighttVolume: 500 mL
Date Prepared: 04/06/2010 1735
}
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qual LCSD Qua]
HEM (Oil & Grease) M�
92 84 78 - 114
8 18
TestAmerica Savannah Page 11 of 18

Quaflty Control Results
Client: CSX Transportation P Job Number. 680-56297-1
Method Blank - Batch: 680-165215
-
Method: 353.2
Preparation: NIA
Lab Sample ID: MB 680-16521511
Analysis Batch: 680-165215
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: NIA
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 2 mL
Date Analyzed: 04/08/2010 1205
Final Weight/Volume: . 2, mL
Date Prepared: N/A
Analyte
Result
Qual MDL RL
Nitrate as N
0.050
U 0.010 0.050
Lab Control Sample - Batch: 680-165215
Method: 353.2
Preparation: N/A
Lab Sample ID: LCS 680-165215/2
Analysis Batch: 680-165215
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: NIA
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 2 mL
Date Analyzed: 04/08/2010 1205
Final Weight/Volume: 2 mL
Date Prepared: N/A
Analyte
Spike Amount Result
r
% Rec. Limit Qua]
Nitrate as N
1.00 0.994
99 90 - 110
Matrix Spike/
Method: 353.2
Matrix Spike Duplicate Recovery Report - Batch:
680-165215
Preparation: NIA
MS Lab Sample ID: 680-56258-D-1 MS
Analysis Batch: 680-165215
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Initial Weight/Volume: 10 mL
Date Analyzed: 03/30/2010 4923
FinalWeight/Volume: 10 mL
Date Prepared: N/A
MSD Lab Sample ID: 680-56258-D-1 MSD
Analysis Batch: 680-165215
Instrument ID: KONELAB2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Initial Weight/Volume: 10 mL
Date Analyzed: 03/30/2010 1923
Final Weight/Volume: 10 mL
Date Prepared: N/A
% Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qua[ MSD Qual
Nitrate as N 105 102 90 - 110 3 10
TestAmerica Savannah Page 12 of 18

Client: CSX Transportation
Duplicate -Batch: 680-165215
Lab Sample ID: 680-56297-1
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/01/2010 1333
Date Prepared: N/A
Analyte
Analysis Batch: 680-165215
Prep Batch: N/A
Units: mg/L
Sample Result/Qua] Result
Quality Cont.roO Results
Job Number: 680-56297-1
Method: 353.2
Preparation: NIA
Instrument ID: KONELAB2
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
RPD Limit Qual
Nitrate as N 0.025 1 0.0159 45 10 J
TestAmerica Savannah
Page 13 of 18

Quality Control Results
Client: CSX Transportation
Job Number: 680-56297-1
Method Blank - Batch: 680-164576
Method: SM 2540C
Preparation: N/A
Lab Sample ID: MB 680-164576/1
Analysis Batch: 680-164576
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed: 03/31/2010 1500
Final Weight[Volume: 100 mL
Date Prepared: N/A
Analyte
Result
Qual RL RL
Total Dissolved Solids
5.0
U 5.0 5.0
Lab Control Sample - Batch: 680-164576
Method: SM 2540C
Preparation: N/A
Lab Sample ID: LCS 680-164576/2
Analysis Batch: 680-164576
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed: 03/31/2010 1500
Final WeightlVolume: 100 mL
Date Prepared: N/A
' Analyte
Spike Amount Result
% Rec. Limit Qual
Total Dissolved Solids
475 385
81 80 - 120�
Duplicate - Batch: 680-164576 -
Method: SM 2540C
Preparation: N/A
Lab Sample ID: 680-56267-B-1 DU
Analysis Batch: 680-164576
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed: 03/31/2010 1500
Final WeightlVolume: 100 mL
Date Prepared: N/A
Analyte
Sample ResuIt/Qual
Result RPD Limit Qua[
Total Dissolved Solids
250
204 20 25
TestAmerica Savannah Page 14 of 18

Client: CSX Transportation
Method Blank - Batch: 680-165297
Lab Sample ID:
MB 680-165297/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
04/08/2010 1040
Date Prepared:
N/A
Analysis Batch: 680-165297
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-56297-1
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Analyte
Result Qua]
MDL
RL
Total Organic Carbon
1.0 U
0.50
1.0
Lab Control Sample - Batch: 680-165297
Method: SM 5310B
Preparation: N/A
Lab Sample ID: LCS 680-165297/4
Analysis Batch: 680-165297
Instrument ID: TOC3
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
25 mL
Date Analyzed: 04/08/2010 1111
Final WeightlVolume:
25 mL
Date Prepared: N/A
Analyte Spike Amount Result
Total Organic Carbon 20.0 19.5
Matrix Spike/'
Matrix Spike Duplicate Recovery Report -'Batch: 680-165297
MS Lab Sample ID:
680-56255-C-2 MS
Analysis Batch: 680-165297
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
04/08/2010 2020
Date Prepared:
N/A
MSD Lab Sample ID:
680-56255-C-2 MSD
Analysis Batch: 680-165297
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
04/08/2010 2033
Date Prepared:
N/A
% Rec. Limit
98 80 - 120
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Instrument ID: TOC3
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Qual
% Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qua]
Total Organic Carbon 102 103 80 - 120 0 25
TestAmerica Savannah Page 15 of 18

Client: CSX Transportation
Duplicate - Batch: 680-165297
Lab Sample ID: 680-56400-A-6 DU
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/08/2010 2214
Date Prepared: N/A
Analyte
Total Organic Carbon
Analysis Batch: , 680-165297
Prep Batch: N/A
Units: mg/L
Sample ResulUQual . Result
2.8 2.85
(duality Control Results
Job Number: 680-56297-1
Method: SM 5310B
Preparation: N/A
'r
Instrument ID: TOC3
Lab File ID: N/A
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
RPD Limit Qual
0 25
TestAmerica Savannah
Page 16 of 18

ro
w
to
0)
/� t� t
CHAIN V OF
TRANSPORTATION CUSTODY
LABORATORY INFORMATION
COC # ,
❑ TestAmerica Savannah - 5102 LaRoche Avenue, Savannah, GA 31404 P: 912.354-7858 F. 912.352-0165
OTestAmerica North Canton - 4101 Shuffel Drive NW. North Canton, OH 44720 P: 330.497-9396 F: 330.497-0772
OTestAmerica Tampa - 6712'Benjamin Road, Suite 100. Tampa, FL 33634 P. 813.885-7427 F. 813-885-7049
❑ TestAmerica Pensacola - 3355 McLemore Drive, Pensacola, FL 32514 P: 850.474-1001 F: 850.478.2671
O TestAmerica Buffalo -10 Hazelwood Drive, Suite 106. Amherst, NY 14228 P: 716-691-2600 F: 716-961-7991
o TestAmerica Chicago - 2417 Bond Street, University Park, IL 60466 P. 708-534-5200 F: 708-534.5211
SHIPMENT INFORMATION
Shipment Method:
Shipment Tracking No:
CSXT PROJECT INFORMATION Pro]. State (State of Origin)
CONSULTANT INFORMATION Project 4:
CSXT Project Number: Proj. City:—
Company: PM:
CSXT Project Name: / / " U n
Address: Email:
CSXT Contact: /C LWON: — 6, 11Z
City, State, ZIP: Phone: Fax:
Turnaround Time: ❑ Standard 6-13 Days
❑ 1 Day flush SpQcify # Days
El Day flush tandard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: 3 = Sulfuric Acid' 0 . N042 m►
0 = No Preservatives 4 = Sodium Thiosuifpte Pres.
i = Hydrochloric Acid 5 = Sodium Hyc(roxi(te Code
2 = Nitric Acid 6 = Other
COMMENTS
LAB USE
METHODS FOR ANALYSIS
>�
t n
-
N
I
M
Deliverables:- ❑ Other Deliv:
❑ CSXT Standard (Level II)
❑ Level III ❑ EDD Required, Format:
❑ Level IV
Matrix Codes: SO = Soil LIQ = Liquid
GW = Groundwater SL = Sludge
WW = Waste Water OI = Oil
SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION
Sample Identification
Containers
Sample Collection
Filtered
Tvpe
Matrix
Number &
Type
Date
Time
Sampler
Y or N
Comp
or Grab
Code -
$ i C
26
D: ?FSF)
.:. aoss
.: - 4- p
24
2
1.
t > f✓�.
Sao 1
ID
'i?!i
C
v
_ s
as
_
f/
C,
► w
3
Relinquished By:
Date/Time:
Recei y:
DateTme:
—p
f
Comments & Special Analytical Requirements:
i��t�.
t
l
Relinquished By:
Daterrime:
eceived By:
atemme:
Relinquished By:
Dale/Time.
Received By:
Datemme.
eived B Laborator :
DateTme:
t c-
Lab Remarks:
LAB USE: Custody Intact
❑Yes ❑No
Custody Seal q
#
LAB Lo Number
# G
ORIGINAL - RETURN TO LABORATORY WITH'SAMPLES ""v"t`•�'"'u" 0� o"p""' ' "" 1v vOA 1 11"" """"'"^` """" `""""'

Login Samp8e receipt Check Lust
Client: CSX Transportation
Login Number: 56297
Creator: Daughtry, Beth
List Number: 1
Question T / F/ NA
Radioactivity either was not measured or, if measured, is at or below
N/A
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True'
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
There are no discrepancies between the sample IDs on the containers and
True
the COC.
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
N/A
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
N/A
Samples do not require splitting or compositing.,
N/A
Is the Field Sampler's name present on COC?
False
Sample Preservation Verified
True
Job Number: 680-56297-1
List Source: TestAmerica Savannah
TestAmerica Savannah Page 18 of 18

WQ0000601® CSXT HAMLET, NC
APRIL 2010

ATTACHMENT A — LIMITATIONS AND MONITORING REQUIREMEENTS
PPI 001— WWTF Effluent
EFFLUENT CHARACTERISTICS
Parameter Description — parameter Code
Flow, in conduit or thru treatment plant — 50050
Solids. Total Dissolved— 180 Deg.C— 70300
pH — 00400
Carbon, Total Organic (TOC) — 00680
Nitrogen, Nitrate Total (as N) — 00620
Barium, 'Total (as Ba)— 01007
Cadmium, Total (as Cd) — 01027
Chromium, Total (as Cr) — 01034
Lead, Total (as Pb) — 01051
Arsenic, Total (as As) —01002
EFFLUENT LIMITS
Monthly Average Weekly Average
------------------
1.0 mgd
3 X year monitoring shall be conducted in March, July and November.
Additional monitoring performed April 2010
W00000601 Version 3.6
Attachment A
]hermit Number: WQ0000601 Version: 3.0
oDailyLmg/L
0.046
0.016
< 0, 0 0
<0 .01
<0. 01
<0. 02
mg / L
mg/L
mg/L
mg/L
mg/L
mg/L
MONITORING REQUIREMENTS
Monitoring Frequency
Continuous
3 X yearGrob
3 X year
3 X year
3 X year
3 X year
3 X year
3 Xyear
3 Xyear
3 Xyear
Sample Type
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Page 1 of 1

�estAmeir'ica
THE LEADER IN ENVIRONMENTAL TESTING
Job Number: 680-57105-1
Job Description: CSX Hamlet, NC WWTP April 2010
For:
CSX Transportation
500 Water Street
Jacksonville, FL 32202
Attention: Mr. Mike Gregory
11
VLOJ�q-& .&�t4
Kathryn Smith
Project Manager I
[e-mail]
05/19/2010
cc: Mr. Jerry Cato
Mr. Alan Pinnix
LWON-ENV0000027258HProject-R000011790
Approved fw relaase.
Kathryn Smith
P-1-t Manager I
5/19/2010 3:02 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A21-A: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001: TN: TN0296; TX: T104704185; US EPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc
1R3 AGCp
TestArnerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericainc.com �`� ``''1 ` c`
�r
Page 1 of 17

Job Narrative
680-57105-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
Method(s) 353.2: The matrix spike? matrix spike duplicate (MS/MSD) recoveries for batch 167428 were outside control limits. The
associated laboratory control sample (LCS) recovery met acceptance criteria.
No other analytical or quality issues were noted.
Page 2 of 17

METHOD SUMMARY
Client: CSX Transportation
Job Number: 680-57105-1
Description Lab Location Method Preparation Method
Matrix Water
Metals (ICP) TAL SAV 40CFR136A 200.7 Rev 4.4
Preparation, Total Metals TAL SAV
EPA 200.7
HEM and SGT-HEM TAL SAV -1664A 1664A
HEM and SGT-HEM (Aqueous) TAL SAV 1664A 1664A
Nitrogen, Nitrate -Nitrite TAL SAV MCAWW 353.2
Solids, Total Dissolved (TDS) TAL SAV SM SM 2540C
Organic Carbon, Total (TOC) TAL SAV SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1664A= EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
r
Page 3 of 17

METHOD / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-57105-1
Method Analyst
Anal st ID
40CFR136A 200.7 Rev 4.4 Bland, Brian
BCB
1664A 1664A Samuel, Sarita
SS
MCAWW 353.2 Ross, Jon
JR
SM SM 2540C Jackson, Michelle S
MSJ
SM SM 5310E Blackshear, Kim
KB
TestAmerica Savannah
Page 4 of 17

SAMPLE SUMMARY
Client: CSX Transportation
Job Number: 680-57105-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sam led
P Received
680-57105-1 Effluent Water 04/27/2010 0925 04/28/2010 1010
TestAmerica Savannah
Page 5 of 17

Client: CSX Transportation
Analytical Data
Job Number: 680-57105-1
Client Sample ID:
Effluent
Lab Sample ID:
680-57105-1
Client Matrix:
Water
Date Sampled: 04/27/2010 0925
Date Received: 04/28/2010 1010
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-167268
Instrument ID;
Preparation:
200.7
Prep Batch: 680-167027
Lab File ID:
ICPD
Dilution:
1.0
N/A
Date Analyzed:
04/29/2010 1923
Initial Weight/Volume:
50 mL
Date Prepared:
04/28/2010 1426
Final Weight/Volume: 50 mL
Analyte
Arsenic
Result m !L)
( 9
Qualifier
fier
MDL
RL
Barium
0.020
U
0.0046
6.
Cadmium
0.W6
0.0023
.020
0.010
Chromium
0.0050
U
.
00020
0.0050
Lead
0.010
U
0.0012
0.010
0.010
U
0.0040
0.010
TestAmerica Savannah Page 6 of 17

Client: CSX Transportation
General chemistry
Client Sample ID:
Effluent
Lab Sample ID:
680-57105-1
Client Matrix:
Water
Analytical Data
Job Number: 680-57105-1
Date Sampled: 04/27/2010 0925
Date Received: 04/28/2010 1010
Analyte Result
HEM (Oil & Grease)
Qual Units MDL
_.._ .... _........... ......-._._.__....._....__. _
_...._ . RL
Dil
Method
5 0
Analysis Batch: 680-167326
U mg/L 1.4
Date Analyzed: 05/03/2010 1330
5.0..... _
1.0
1664A
Prep Batch: 680-167318
Date Prepared: 05/02/2010 0935
Nitrate as N 0.046
J mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-167428
Date Analyzed: 04/29/2010 0907
Total Organic Carbon 8.7
mg/L 0.50
1.0
Analysis Batch: 680-167632
Date Analyzed: 05/04/2010 1302
1.0
SM 5310E
Analyte Result
_ ...... . ...........
Total Dissolved Solids -'
Qual Units RL
'" � ........ • .. __........
RL
Dil
Method
95
Analysis Batch: 680-167386
m/L.5.0
g
Date Analyzed: 05/03/2010 1259
_ .. _._ . _ ...._ ._.._ ..
5.0
1,0
5M 2540C
TestAmerica Savannah Page 7 of 17

DATA REPORTING QUALIFIERS
Client: CSX'Transportation
Lab Section Qualifier Description
Metals
General Chemistry
I
TestAmerica Savannah
Job Number: 680-57105-1
U Indicates the analyte was analyzed for but not detected.
U Indicates the analyte was analyzed for but not detected.
F MS or MSD exceeds the control limits
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
Page 8 of 17

Client: CSX Transportation
Method Blank -Batch: 680-167027
Lab Sample ID:
MB 680-167027/7-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
04/29/2010 1816 ,
Date Prepared:
04/28/2010 1426
Analysis Batch: 680-167268
Prep Batch: 680-167027
Units: mg/L
Quality Control Results
Job Number: 680-57105-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICPD
Lab File ID: N/A
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte
Result
Qual
MDL
RL
mumBarium
0.020
U
0.0046
0.020^
Cadmium
0.010
U
0.0023
0.010
Chromium
0.0050
U
0.0020
0.0050
Lead
0.010
U
0.0012
0.010
0.010
U
0.0040
0.010
Lab Control Sample
- Batch: 680-167027
Method: 200.7 Rev 4.4
-
Preparation: 200.7
Lab Sample ID:
LCS 680-167027/8-A
Analysis Batch: 680-167268
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-167027
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeightfVolume: 50
mL
Date Analyzed:
04/29/2010 1821
Date Prepared:
04/28/2010 1426
Final Weight/Volume: 50
mL
Analyte
Spike Amount
Result
% Rec.
Limit
Qual
Arsenic
2.00
1.94
97
.._.. 1. ................
85 -11115
_.._.....__...... .
Barium
2.00
2.05
103
85 - 115
Cadmium
0.0500
0.0502
100
85 -115
Chromium
0.200
0.204
102
85 - 115
Lead
0.500
0.500
100
85 - 115
TestAmerica Savannah Page 9 of 17

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-167027
Quality Control Results
Job Number: 680-57105-1
Method:.200.7 Rev 4.4
Preparation: 200.7
MS Lab Sample ID:
680-57056-B-1-B MS
Analysis Batch:
680-167268
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-167027
Lab File ID: N/A
Dilution:
1.0
Date Analyzed:
04/29/2010 1842
Initial Weight/Volume: 50 mL
Date Prepared:
04/28/2010 1426
Final Weight/Volume: 50 mL
MSD Lab Sample ID:
680-57056-B-1-C MSD
Analysis Batch:
680-167268
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-167027
Lab File ID: NIA
Dilution:
1.0
Initial WeightlVolume: 50 mL
Date Analyzed:
04/29/2010 1847
Date Prepared:
04/28/2010 1426
Final Weight/Volume: 50 mL
% Rec.
Analyte
MS MSD
Limit
RPD
RPD Limit MS Qual MSD Qual
A1senic
98 97
75 - 125
1
20
Barium
103 102
75 - 125
1
20
Cadmium
102 100
75 - 125
2
20
Chromium
102 101
75 - 125
1
20
Lead
101 99
75-125
1
20
,r
TestAmerica Savannah Page 10 of 17

Client: CSX Transportation
Method Blank -Batch: 680-167318
Quality Control Results
Job Number: 680-57105-1
Method: 1664A
Preparation: 1664A
Lab Sample ID:
MB 680-167318/19-A
Analysis Batch: 680-167326
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: 680-167318
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 500 mL
Date Analyzed:
05/03/2010 1330
Final WeighWolume: 500 mL
Date Prepared:
05/02/2010 0935
Analyte
Result Qua[
MDL RL
EM (Oil &Grease)
5.0 U
_...._..._............ _.._ ........._._.
1.4 ...1._._. 5.0
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-167318
Method: 1664A
Preparation: 1664A
LCS Lab Sample ID:
LCS 680-167318120-A
Analysis Batch: 680-167326
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: 680-167318
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeighWolume: 500 mL
Date Analyzed:
05/03/2010 1330
Final WeighWolume: 500 mL
Date Prepared:
05/02/2010 0935
LCSD Lab Sample ID:
LCSD 680-167318/21-A
Analysis Batch: 680-167326
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: 680-167318
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial WeighWolume: 500 mL
Date Analyzed:
05/03/2010 1330
Final Weight/Volume: 500 mL
Date Prepared:
05/02/2010 0935
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qua[ LCSD Qual
HEM (Oil & Grease)
90 93 78 - 114
4 18
TestAmerica Savannah Page 11 of 17

Client: CSX Transportation
Method Blank -Batch: 680-167428
Quality Control Results
Job Number: 680-57105-1
Method: 353.2
Preparation: N/A
Lab Sample ID:
MB 680-167428/1
Analysis Batch: 680-167428
Instrument ID: KONELAB2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
Date Analyzed:
1.0
05/03/2010 1601
Units: mg/L
Initial Weight/Volume: 2 mL
Date Prepared:
N/A
Final Weight/Volume: 2 mL
Analyte
Result Qual
MDL RL
Nitrate as N
_. _... ._. _. _......__........... _. ......-. U --. __......._
0.050
.._..._
0.010 0.050
Lab Control Sample - Batch: 680-167428
Lab Sample ID: LCS 680-167428/2
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 05/03/2010 1601
Date Prepared: N/A
Analysis Batch: 680-167428
Prep Batch: N/A
Units: mg/L
Method: 353.2
Preparation: N/A
Instrument ID: KONELA82
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final WeighWolume: 2 mL
Analyte Spike Amount Result % Rec. Limit
Qual
Nitrate as N •
.00 0.995 1.00 ........ .
90 - 110
Matrix Spike/ Method: 353.2
Matrix Spike Duplicate Recovery Report - Batch: 680467428 Preparation: N/A
MS Lab Sample ID: 680-57044-G-1 MS Analysis Batch: 680-167428
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 04/24/2010 1419
Date Prepared: N/A
MSD Lab Sample ID: 680-57044-G-1 MSD Analysis Batch: 680-167428
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 04/24/2010 1419
Date Prepared: N/A
% Rec.
Analyte MS MSD Limit
Nitrate as N 17 17 90 - 110
TestAmerica Savannah Page 12 of 17
Instrument ID: KONELAB2
Lab File ID: N/A
Initial WeighWolume: 2 mL
Final Weight/Volume: 2 mL
Instrument ID: KONELA62
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Welght/Volume: 2 mL
RPD
RPD Limit
MS Qual
MSD Qual
1
10
..........
F
......... ......
F

Client: CSX Transportation
Method Blank - Batch: 680-167386
Lab Sample ID: MB 680-167386/1 Analysis Batch: 680-167386
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 05/03/2010 1259
Date Prepared: N/A
Quality Control Results
Job Number: 680-57105-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weightolume: 100 mL
Analyte Result Qual RL RL
Total Dissolved Solids 5.0 U 5.0 5.0
Lab Control Sample/ Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680.167386 Preparation: NIA
LCS Lab Sample ID: LCS 680-167386/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
05/03/2010 1259
Date Prepared:
N/A
LCSD Lab Sample ID: LCSD 680-167386/3
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
05/03/2010 1259
Date Prepared:
N/A
Analysis Batch: 680-167386
Prep Batch: N/A
Units: mg/L
Analysis Batch: 680-167386
Prep Batch: N/A
Units: mg/L
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Instrument ID: No Equipment Assigned
Lab File ID:. NIA
Initial Weight/Volume: 100 mL
Final WeighWolume: 100 mL
% Rec.
Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual
Total Dissolved Solids 85 86 80 - 120 1 25
Duplicate - Batch: 680-167386
Method: SM 2540C
Preparation: NIA
Lab Sample ID:
680-57144-B-2 DU
Analysis Batch: 680-167386
Instrument ID: No Equipment Assigned
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 100 mL
Date Analyzed:
05/03/2010 1259
Final Weight/Volume: 100 mL
Date Prepared:
N/A
Analyte
Sample Result/Qual Result
RPD Limit Qual
Total Dissolved Solids
__._.._ ............. _ _ .. _.. .....
810 802
_....... _..._......... ..... ... _........_
0 25
TestAmerica Savannah Page 13 of 17

Client: CSX Transportation
Method Blank -Batch, 680-167632
Quality Control Results
Job Number: 680-57105-1
Method: SM 5310B
Preparation: NIA
Lab Sample ID:
MB 680-167632/2
Analysis Batch: 680-167632
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: T00050410.txt
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 25 mL
Date Analyzed:
05/04/2010 1101
Date Prepared:
N/A
Final Weight/Volume: 25 mL
Analyte
..........g. _ni.....
.. ....
._... ........
Result Qua[
MDL RL
Total Oranic Carbon.. ._......._ ...:.........
..._.._ .._..._. _..............__.
1.0
-•_ _.
U
0.50 1.0
Lab Control Sample - Batch: 680-167632
Method: SM 5310B
Preparation: N/A
Lab Sample ID:
LCS 680-167632/4
Analysis Batch: 680-167632
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: T00050410.txt
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 25 mL
Date Analyzed:
05/04/2010 1132
Final WeightfVolume: 25 mL
Date Prepared:
N/A
Analyte
Spike Amount Result
% Rec. Limit Qual
Total Organic Carbon
20.0 19.0
95 80 - 120
Matrix Spike/ Method: SM 53108
Matrix Spike Duplicate Recovery Report - Batch: 680-167632 Preparation: N/A
MS Lab Sample ID: 680-57105-1
Client Matrix:
Water
Dilution: -
1.0
Date Analyzed:
05/04/2010 1319
Date Prepared:
N/A
MSD Lab Sample ID: 680-57105-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
05/04/2010 1332
Date Prepared:
N/A
Analyte
Total Organic Carbon
Analysis Batch: 680-167632
Prep Batch: NIA
Analysis Batch: 680-167632
Prep Batch: N/A
% Rec.
MS MSD Limit
99 97 80 -120
Instrument ID: TOC3
Lab File ID: T00050410.txt
Initial Weight/Volume: 25 mL
Final WeightfVolume: 25 mL
Instrument ID: TOC3
Lab File ID: T00050410.txt
Initial Weight/Volume: 25 mL
Final WeightfVolume: 25 mL
RPD RPD Limit MS Qual MSD Qual
1 25
TestAmerica Savannah Page 14 of 17

Client: CSX Transportation
Duplicate - Batch: 680-167632
Lab Sample ID:
680-57237-8-5 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
05/04/2010 1815
Date Prepared:
NIA
Analysis Batch: 680-167632
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-57105-1
Method: 5M 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00050410.txt
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Analyte Sample Result/Qual Result
RPD Limit Qual
Total Organic Carbon-•••�•••�•••�••.-....•......._..
0.76 _........................� _ ..-....... _.
0.772 1 25
TestAmerica Savannah Page 15 of 17

O TestAmerica Savannah .5102 LaRoche Avenue, Savannalr, GA 31404 P: 912.354-7B58 F: 912-352.0165 coc #
O TeslAmerica North Canton -4101 Shuftel Drive iVW. Nortlr Canton, 017 44720 P: 330-497.9J96 F: �30.497.0T72 SHIPMENT INFORMATION
CSX CHAIN OF --
O TestAmerica Tampa- 6712 Benjamin Road, Suite 100. Tampa, FL 33634 P: 813.885.7427 F. 813-885-7049
TRANSPORTATION CUSTODY O TeSlAmerica Pensacola - 3355 Mclemore Drive, Pensacola. FL 32514 P:850-474-1001 F: 850.478.2671 Shipment Method:
O TestAmerica Buffalo • 101lazehvood Drive, Suite 106, Amherst, NY 14228 P: 716-691-2600 F: 716-961-799t
O TeslAmarica Chicago . 2417 Bond Street. University Park. IL 60468 P: 708-534.5200 F: 708-534.5211 Shipment Tracking No:
CSXT PROJECT INFORMATION �SS.Ialle(State of Origin) CONSULTANT INFORMATION Project A:
CSXT Projecl Number: ? Company. P nY= PM:
CSXT Project Name:
Address: Email:
CSXT Contact r LWON: City, State, Zip: Phone: Fax:
t c.
Turnaround Time: ❑ Standard 6.13 Days
❑ 1 Day Rush r�---�� �Specify # Days
❑ 2 Day Rush 0-Standard 14 Daysloric
❑ 3 Day Rush ❑ Other
TPreservative Codes: 3 = Sulfuric Acid Note
ervatives 4 = Sodium Thlosulfate . Pres.
Acid 5 = Sodium Hydroxide Code
d 6 =Other
a
l
COMMENTS LAB USE
METHODS
FOR
ANALYSIS
V
n
' v
1 4
n7
Deliverables: ❑ Other Deliv:
❑ CSXT Standard (Level II)
❑ Level M ❑ EDD Required, Format:
❑ Level IV
SAMPLE INFORMATION
Matrix Codes: SO = Soil LIO = Liquid
GW = Groundwater SL = Sludge
WW = Waste Water OI = Oil
SVV = Surface'Nater SOL = Other Solid
N
F' Sample Identification
rn
0
Containers
Sam le Collectio n
Filtered T e
Matrix
Number &
Type
Date
Time
Sampler
Y or N Cep
or Grab
Code
rn .�
o OM I
iZ —/b
Z5
j2- n
d
oG a IA
fzr,�t
►� 7-16
CZ5
-
p
6. 2F
oontl
Z -16
G'2S
I}
-2
' 5
cd ca
_fo
zs
G2
Relinquished By:
DateTma:
Rec 6v y:
Received By: I
Receivetl By:
Da ime:
Comments & Special Analytical RegVirements:
Relinquished By:
DatelTime:
Date/Time:
Relinquished By;
DalelTme:
Date/Time:
Received By Labor a ry. Date/Time: Lab Remarks:
r� I /�
` I C
ORIGINAL —RETURN TO 1A8O TORY W H SAMPLES INVOICE
LAB USE: Custody Intact
❑Yes ❑ No
Custody Seal #
#
LAB Lo ju/�ber r
N (J VT f OS
MUST eE SUBMITTED TO
CSXT WITH ORIGINAL CDC TAL•6005 (0509)

Login Sample receipt Check mist
Client: CSX Transportation
Login Number: 57105
Creator. Daughtry, Beth
List Number:.1
Question
T / F/ NA Comment
Radioactivity either was not measured or, if measured, is at or - below
N/A
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not,appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
There are no discrepancies between the sample IDs on the containers and
True
the COC.
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample cpllection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
There is sufficient vol. for all requested analyses, Incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
NIA
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
N/A
Samples do not require splitting or compositing.
N/A
Is the Field Sampler's name present on COC?
False
Sample Preservation Verified
True
TestAmerica Savannah
Page 17 of 17
.Job Number:
List Source: TestAmerica
105-1

Q0000601 o CSXT HAMLET9 IBC
MAY 2010

ATTACHMENT A — LIMITATIONS AND MONITORING REQUIREMENTS
PPI 001— WWTF Effluent
Permit Number; WQ0000601 Version. 3.0
EFFLUENT CHARACTERISTICS
EFFLUENT LIMITS
Parameter Description -Parameter Code
MONITORING REQUIREMENTS
Weekly Average
Daily Maximum
Monitoring Frequency
Sample Type
Flow, in conduit or thru treatment
Monthly
Average
6-CoLk
fha l
Continuous
plant - 50050
Solids, Tots( Dissolved- 180 Deg.C- 70300
1.0
mgd
Recorder
95
mg/L
3 X year
Grab
pH - 00400
3 X year
Grab
Carbon, Total Organic (TOC) - 00680
Nitrogen, Nitrate Total (as N) •- 00620
12
mg/L
3 X year
Grab
Grab
Barium, Total (as Ba) - 01007
----
0.13
mg/L
3 X year
Grab
Cadmium, Total (as Cd) - 01027
0. 023
mg/L
3 X year
Chromium, Total (as Cr) - 01034
<0 . 00
mg/L
3 X year
Grab
Lead, Total (as Pb) - 01051
< 0 . 01
mg / L
3 X year
Grab
Arsenic, Total (as As) - 01002
< 0 . 01
mg/ L
3 X year
Grab
<0 . 02
mg/L
3 X year
Grab
.. yc4r monitoring stiall be conducted in March, July and November.
Additional monitoring performed May 2010
WQ0000601 Version 3.0
Attachment A Page l of l

TestAmer'ica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-58078-1
Job Description: CSX Hamlet, NC WWTP Monthly
For:
CSX Transportation
500 Water Street
Jacksonville, FL 32202
Attention: Mr. Mike Gregory
of • _
4
1 jr• 1
APitrelease.
Kathryn thrynS Smile
PrujeG Manager I
6/22/2010 3:45 PM
Kathryn Smith
Project Manager I
[e-mail]
06/22/2010
cc: Mr. Jerry Cato
Mr. Alan Pinnix
LW ON-E NV0000027258//Project-R000011790
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and. ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPARB: 8TMS-Q
TestAmerica Laboratories, Inc. n `R aocogv TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404 ��` y �'
Tel [phone] Fax [phone] www.testamericainc.coLn
�-
Page 1 of 18

Job Narrative
680-58078-9
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Page 2 of 18

METHOD SUMMARY
Client: CSX Transportation
Job Number: 680-58078-1
Description Lab Location Method Preparation Method
Matrix: Water
Metals (ICP) TAL SAV 40CFR136A 200.7 Rev 4.4
Preparation, Total Metals TAL SAV EPA 200.7
HEM and SGT-HEM TAL SAV 1664A 1664A
HEM and SGT-HEM (Aqueous) TAL SAV 1664A 1664A
Nitrogen, Nitrate -Nitrite TAL SAV MCAWW 353.2
Solids, Total Dissolved (TDS) TAL SAV SM SM 2540C
Organic Carbon, Total (TOC) TAL SAV SM SM 5310E
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1.664A = EPA-821-98,002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 18

METHOD / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-58078-1
Method
Anal st
Anal st ID
40CFR136A 200.7 Rev 4.4
Bland, Brian
BCB
1664A 1664A
Samuel, Sarita
SS
MCAWW 353.2
Ross, Jon
JR
SM SM 2540C
Robinson, Tiffany
TR
SM SM 5310E
Blackshear, Kim
KB
TestAmerica Savannah
Page 4 of 18

SAMPLE SUMMARY
Client: -CSX Transportation
Job Number: 680-58078-1
_Lab Sample ID Client SamDate/Time Date/Timeple ID Client Matrix Sampled P Received
680-58078-1 Water Sample Water 05/27/2010 0930 05/28/2010 1010
TestAmerica Savannah
Page 5 of, 18

Client: CSX Transportation
Client Sample ID: Water Sample
Anall ocal Data
Job Number: 680-58078-1
Lab Sample ID:
680-58078-1
Client Matrix:
Water
Date Sampled: 05/27/2010 0930
Date Received: 05/28/2010 1010
200.7 Rev 4.4 Metals. (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-170814
Instrument ID: ICPD
Preparation:
200.7
Prep Batch: 680-170556
Lab File ID: 170556.chr
Dilution:
1
Date Analyzed:
06/08/2010 0018
Initial Weight/Volume:. 50 mL
Date Prepared:
06/04/2010 0850
Final WeightNolume: 50 mL
Analyte
Result (mg1L)
Qualifier
MDL RL
Arsenic........
Barium
0.020
.. _ ....._....._...
U
.
0.0046 _......_.... _..._..... ..... _..0.020 _ —.. ... ......
Cadmium
0.023
0.0023 0.010
Chromium
0.0050
U
0.0020 0.0050
Lead
0.010
U
0.0012 0.010
0.010
U
0.0040 0.010
n
TestAmerica Savannah Page 6 of 18

Client: CSX Transportation
General Chemistry
Client Sample ID: Water Sample
Lab Sample ID: 680-58078-1
Client Matrix: Water
Analytical Data
Job Number: 680-58078-1
Date Sampled: 05/27/2010 0930
Date Received: 05/28/2010 1010
Analyte Result Qual Units MDL
_.._...( .........._ _._. j..---.....__ ._._.._.._._. 5.0 RL Dil Method
HEM OII & Grease _... _... _...__... __.. __.__...___ _._ .......__.___.._._ _._.. _. _..__
U mg/L 1.4 5.0 1.0 �1664A`
Analysis Batch: 680-170282 Date Analyzed: 06/02/2010 0000
Prep Batch: 680-170250 Date Prepared: 06/01/2010 1705
Nitrate as N 0.13 mg/L 0.010
Analysis Batch: 680-170222 Date Analyzed: 05/28/2010 1612 0.050 1.0 353.2
Total Organic Carbon 12 mg/L 0.50
Analysis Batch: 680-171156 Date Analyzed: 06/09/2010 1339 1 0 1.0 SM 53108
Analyte Result Qual Units .
.._.._.... _ ..... RL RL
Total Dissolved Solids ""' • •• • •-•
mglL 5.0
Analysis Batch: 680-170253 Date Analyzed: 06/01/2010 1453
TestAmerica Savannah Page 7 of 18
Dil Method
1.0 SM 2540C

DATA REPORTING QUALIFIERS
Client: CSX Transportation
Lab Section Qualifier Description
Metals
General Chemistry
TestAmerica Savannah
Job Number: 680-58078-1
Indicates the analyte was analyzed for but not detected.
U Indicates the analyte was analyzed for but not detected.
4 MS, MSD: The analyte present in the original sample is 4 times
greater than the matrix spike concentration; therefore, control
limits are not applicable.
J Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
Page 8 of 18

Client: CSX Transportation
Method Blank -Batch: 680-170556
Quality Control Results
Job Number: 680-58078-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
MB 680-170556/21-A
Analysis Batch: 680-170814
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-170556
Lab File ID: 170556.chr
Dilution:
Date Analyzed:
1.0
06/07/2010 2318
Units: mg/L
Initial WeightNolume:
50 mL
Date Prepared:
06/04/2010 0850
Final WeightNolume:
50 mL
Analyte
Result
Qual
MDL
RL
Arsenic
0. .• • ••-•-• _... __..-__.....__.
20
U
Barium
0.0046
0.020
Cadmium
0.010
U
0.0023
0.010
Chromium
0.0050
U
0.0020
0.0050
Lead
0.010
U
0.0012
0.010
0.010
U
0.0040
0.010
Lab Control Sample - Batch: 680-170556
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
LCS 680-170556/22-A
Analysis Batch:
680-170814
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-170556
Lab File ID: 170556.chr
Dilution:
Date Analyzed:
1.0
06/07/2010 2323
Units: mg/L
Initial Weight/Volume: 50 mL
Date Prepared:
06/04/2010 0850
Final WeighWolume: 50 mL
Analyte
Spike Amount
Result
% Rec.
Limit Qual
Arsenic
Barium
2.06
103
._ . _. .
85 - 115
Cadmium
2.00
2.08
104
85 - 115
Chromium
0.0500
0.0499
100
85 - 115
Lead
0.200
0.206
103
85 - 115
0.500
0.518
104
85 - 115
TestAmerica Savannah Page ' 9 of 18

Client: CSX Transportation
Quality Control Results
Job Number: 680-58078-1
Matrix Spike/
Matrix Spike Duplicate
Recovery Report
- Batch: 680-170556
Method: 200.7 Rev 4.4
Preparation: 200.7
MS Lab Sample ID:
Client Matrix:
680-58078-1
Analysis Batch: 680-170814
Instrument ID: ICPD
Dilution:
Water
1.0
Prep Batch: 680-170556
Lab File ID: 170556.chr
Date Analyzed:
06/08/2010 0034
Initial Weight/Volume: •50 mL
Date Prepared:
06/04/2010 0850
Final Weight/Volume: 50 mL
MSD Lab Sample ID:
Client Matrix:
680-58078-1
Analysis Batch: 680-170814
Instrument ID: ICPD
Dilution:
Water
1.0
Prep Batch: 680-170556
Lab File ID: 170556.chr
Date Analyzed:
06/08/2010 0039
Initial Weight/Volume: 50 mL
Date Prepared:
06/04/2010 0850
Final Weight/Volume: 50 mL
Analyte
% Rec.
MS MSD Limit
RPD
RPD Limit MS Ctual MSD Qual
Arsenic_......_
_................_.�.:.............._..
105 106 75 - 125
,._....... ...................._....._ .
Barium
Cadmium
106 105 75 - 125
0
20
Chromium
102 101 75 - 125
� 0
20
Lead
105 105 75 - 125
0
20
105 106 75-125
1
20
TestAmerica Savannah Page 10 of 18

Client: CSX Transportation
Method Blank -Batch. 680-170250
Quality Control Results
Job Number: 680-58078-1
Method: 1664A
Preparation: 1664A
Lab Sample ID: MB 680-170250/21-A
Client Matrix: Water
Analysis Batch: 680-170282
Instrument ID: No Equipment Assigned
Dilution: 1.0
Prep Batch: 680-170250
Lab File ID: N/A
Date Analyzed: 06/02/2010 0000
Units: mg/L
Initial Weight/Volume: 500 mL
Date Prepared: 06/01/2010 1705
Final Weight/Volume: 500 mL
Analyte
Result Qual
MDL RL
HEM (Oil & Grease)
5.
5.0
U'
1.4 5.0
Lab Control Sample/
Lab Control Sample Duplicate Recovery
Report -Batch: 680-170250
Method: 1664A
Preparation: 1664A
LCS Lab Sample ID:, LCS 680-170256/22-A Analysis Batch: .680-170282
Client Matrix: Water Prep Batch: 680-170250
Dilution; 1.0 Units: mg/L
Date Analyzed: 06/02/2010 0000
D13te Prepared: 06/01/2010 1705
LCSD Lab Sample ID: LCSD 680-170250/23-A Analysis Batch: .680-170282
Client Matrix: Water Prep Batch: 680-170250
Dilution: 1.0 Units: mg/L
Date Analyzed: 06/02/2010 0000
Date Prepared: 06/01/2010 1705
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 500 mL
Final Weight/Volume: 500 mL
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 500 mL
Final Weight/Volume: 500 mL
% Rec.
Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qua[
__ ...
EM (Oil & Grease) 100 99 78 - 114 1 '18" '- _..._.._..-..
TestAmerica Savannah Page 11 of 18

Client: CSX Transportation
Method Blank -Batch: 680-170222
Lab Sample ID:
MB 680-17022211
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
05/28/2010 1612
Date Prepared:
N/A
Analyte
Nitrate as N
Lab Control Sample - Batch: 680-170222
Analysis Batch: 680-170222
Prep Batch: NIA
Units: mg/L
Quality Control Results
Job Number: 680-58078-1
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weightolume: 7 mL
Final WeighWolume: 7 mL
Result Qual MDL RL
0.010 0.050
Method: 353.2
Preparation: N/A
Lab Sample ID:
LCS 680-170222/2
Analysis Batch: 680-170222
Instrument ID: Latchat 2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
Date Analyzed:
1.0
05/28/2010 1612
Units: mg/L
Initial Weight/Volume: 7 mL
Date Prepared:
N/A
Final WeighWolume: 7 mL
Analyte
Spike Amount Result
% Rec. Limit Qual
Nitrate as N --
0.501 100 90 - 110
Matrix Spike/ Method: 353:2
Matrix Spike Duplicate Recovery Report - Batch: 680-170222 Preparation: NIA
MS Lab Sample ID: 680-58064-E-1 MS Analysis Batch: 680-170222 Instrument ID: Latchat 2
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 5.0
5/ Initial WeighWolume: 25 mL
Date Analyzed: 005/28/2010 1612 Final WeightNolume: 25 mL
Date Prepared: N/A
MSD Lab Sample ID: •680-58064-E-1 MSD Analysis Batch: 680-170222 Instrument ID: Latchat 2
Client Matrix: Water Prep Batch: N/A Lab File ID: N/A
Dilution: 5.0 Initial WeighWolume: 25 mL
Date Analyzed: 05/28/2010 1612 Final Weight/Volume: 25 mL
Date Prepared: N/A
% Rec.
Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual
Nitrate as N •
10 4 4
TestAmerica Savannah Page 12 of 18

Client: CSX Transportation
Duplicate - Batch: 680-170222
Lab Sample ID:
680-58072-G-3 DU
Client Matrix:
Water
Dilution:
4.0
Date Analyzed:
05/28/2010 1612
Date Prepared:
N/A
Analysis Batch: 680-170222
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number. 680-58078-1
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 7 mL
Final We[ghtA/olume: 7 mL
Analyte Sample Result/Qual
Result RPD Limit Qua[
Nitrateas N—._.__..._............... ....__ .�... __..._.. _.. _ .._..._......_._... 0.20 U 0.20 NC 10 ...._......_._.._.....
U
u
TestAmerica Savannah Page 13 of 18

Client: CSX Transportation
Method Blank Batch: 680-170253
Lab Sample ID:
MB 680-170253/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/01/2010 1453
Date Prepared:
N/A
Analysis Batch: 680-170253
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-58078-1
Method: SM 2540C
Preparation: H/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte
_ ._...._.... .. _..__. _.
Result
Qual RL
Total Dissolved Solids
5.0 "' -
- -
U 5.0 5.0
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-170253
Method: SM 2540C
Preparation: N/A
LCS Lab Sample ID: LCS 680-170253/2
Client Matrix:
Analysis Batch: 680-170253
Instrument ID: No Equipment Assigned
Water
Dilution: 1.0
Prep Batch: N/A
Lab File ID: N/A
Date Analyzed: 06/01/2010 1453
Units: mg/L
Initial Weight/Volume: 100 mL
Date Prepared: N/A
Final WeighWolume: 100 mL
LCSD Lab Sample ID: LCSD 680-17025313
Client Matrix:
Analysis Batch: 680-170253
Instrument ID: No Equipment Assigned
Water
Dilution: 1.0
Prep Batch: N/A
Lab File ID: N/A
Date Analyzed: 06/01/2010 1453
Units: mg/L
Initial Weight/Volume: 100 mL
Date Prepared: N/A
-
Final WeightlVolume: 100 mL
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qual LCSD Qual
Total Dissolved Solids
101 99 80 -120
--• •-•••-
2 25 .
D.uplicate - Batch: 680-170253
-
Method: SM 2540C
Preparation: N/A
Lab Sample ID: 680-58081-F-1 DU
Client Matrix: Water
Analysis Batch: 680-170253
Instrument ID: No Equipment Assigned
Dilution: 1
Prep Batch: N/A
Lab File ID: N/A
Date Analyzed: 06/6/ 01/2010 1453
Units: mg/L
Initial Weight/Volume: 100 mL
Date Prepared: N/A
Final Weight/Volume: 100 mL
Analyte Sample Result/Qual Result
RPD Limit Qual
Total Dissolved Solids 100 107 3 25
TestAmerica Savannah Page 14 of 18

Client: CSX Transportation
Method Blank - Batch: 680-171156
Lab Sample ID:
MB 680-171156/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/09/2010 1056
Date Prepared:
NIA
Analysis Batch: 680-171156
Prep Batch: N/A
Units: mg/L
Analyte Result
Qual
Total Organic Carbon 1:0"'
Lab Control Sample - Batch: 680-171156
Lab Sample ID: LCS 680-171156/4 Analysis Batch: 680-171156
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 06/09/2010 1129
Date Prepared: N/A
Quahty Control Results
Job Number: 680-58078-1
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00060910.txt
Initial WeighWolume: 25 .mL
Final WeighWolume: 25 mL
MDL
RL
0.50 1.0
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00060910.txt
Initial Weight[Volume: 25 mL
Final WeighWolume: 25 mL
Analyte Spike Amount Result
% Rec. Limit
Total Organic Carbon 97 -•
20.0 .......• 19.4 ... 80•- 120
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-171156 Method: 5310E
Preparation
: N/A
MS Lab Sample ID: 680-58093-1-4 MS
Client Matrix:
Water
Dilution:
1•0
Date Analyzed:
06/09/2010 1628
Date Prepared:
NIA
MSD Lab Sample ID:
680-58093-1-4 MSD
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/09/2010 1641
Date Prepared:
N/A
Analysis Batch: 680-171156
Prep Batch: N/A -
Analysis Batch:, 680-171156
Prep Batch: N/A
Instrument ID: TOC3
Lab File ID: T00060910.txt
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Instrument ID: TOC3
Lab File ID: T00060910.txt
Initial Weight/Volume: 25 mL
Final WeighWolume: 25 mL
Qua]
% Rec.
Analyte MS MSD Limit
RPD RPD Limit MS Qual MSD Qual
o t al Organic Carbon 97 80 - 120 25 .. ... ... ........ .
1
TestAmerica Savannah Page 15 of 18

Client: CSX Transportation
Quality Control Results
Job Number: 680-58078-1
Duplicate -Batch: 680-171156
Method: SM 5310B
Preparation: N/A
Lab Sample ID: 680-58091-A-2 DU Analysis Batch: 680-171156
Client Matrix: Water Instrument ID: TOC3
Prep Batch: N/A Dilution: 1.0 Units: mg/L Lab File ID: T00060910.txt
Date Analyzed: 06/09/2010 1451 Initial Weight/Volume: 25 mL
Date Prepared: N/A
Final WeightNolume: 25 mL
Analyte Sample Result/Qual Result
RPD Limit
-.___....---ni_c__a_rb,'._.... __ .. ___...._�._...__. ._.......___..._ .__ ..__... ..__. _...._.__._...__. _.__.. _..
Total Organic Carbon 0.86 J . 0.868
1 25
TestAmerica Savannah Page 16 of 18
Qual

q t�
CM! 1I 1 Y 'O F
TRANSPORTATION CUSTODY
LABORATORY INFORMATION
COC #
QTestAmerira Savannah - 5'162 LaRoche Avenue, Savannah. G 131404 P: 912.354-7858 F. 912-352-0165
it TestAmerica North Canton - 4101 Shuffel Drive NW, North Canton, OH 44720 P: 330.497-9396 F: 330-497-0772
❑ TestAmerica Tampa -.6712 Benjamin Road, Suite 100. Tampa, FL 33634 . P: 813-885-7427 F. 813-885.7049
❑T6stAmericaPensacola-3355McLemoreDrive,Pensacola,FL32514 P:850-474.1001 F:850-47B-2671
❑ TestAmerica Buffalo- 10 Hazelwood Drive, Suite 106, Amherst, NY 14228' P:716-691-2600 ' F: 716-961-7991
❑ TestAmerica Chicago- 2417 Bond Street, Univf8aity Park, IL 60466 P:-i08.534-5200 F: 708-534-5211
SHIPMENT INFORMATION
Shipment Method:
Shipment Tracking No:
Proj, State (State of Origin
CSXT PROJECT INFORMATION G
Project g:
CONSULTANT 1NFQFiMATIOid
CSXT Project Number- ^ Proj. City:
(C �.
Company: PM:
CSXT Project Name: O t7
Address: Email:
CSXT Contact: LWON: —
City, State, Zip: .. Phone: Fa)c
TumarounclTime: ❑ Standard 6-13 Days
❑ 1 Day Rush Specify # Days
❑ 2 Day Rush E Standard 14 Days
❑ 3 Day Rush ❑ Other
Preservative Codes: . 3 = Sulfuric Acid' Note a*
O = No Preservatives 4 - Sodium Thlosulfate Ares.
1 = Hydrochloric Acid 5'= Sodium Hydroxide Code
2 = Nitric Acid 6 = Other
COMMENTS
LAB USE
METHODS FOR ANALYSIS
If
v
d
L?
f�
^ 1
.
-
Deliverablos: ❑ Other Deliv:
❑ CSXT Standard (Level Il)
❑ Level III ❑ EDD Required, Format:
❑ Level IV
Matrix Codes: SO = Soil LIQ = Liquid
GW = Groundwater SL = Sludge
W W = Waste Water 01= Oil
SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION
Sample Identification
Containers
Sam le Collection
Filtered
Type
Matrix
Number &
Type
gate
Time
Sampler
Y or N
Comp
or Grab
Code
ss d
� °°
�� a.
.
o
6c, %J'. :c a
tzs st
2 —to.
G
�-
G
E
o: I e S�
50o M
27--10
3 0
,3
27:1
6
2.
WIWI
zs°�"°
-2W0b
2
,c
t 27-1t1
" 31S
eYL
Relinquished By:
Date7irme:
Reco' ey
Datefrime:
Comments & Special Analytical Requirements:
Ce mc— k 1 e 1
f p
Relinquished By:
Date/rme:
F4ceived By:
Data(Tfine:
Relinquishad By:
DateTme:
Received By:
DateTme:
ceived y bo
DateTme:
�}' e 01 D
Lab Remarks:
LAB.USE: Custody Intact
Dyes ❑Na
Custody Seat #
#
LAB L umber Q
# l T
UHIt3iNAL—RETURN TO LA8013pTORY 1(11ITH SAMPLES INVOICE MUST BE SUBMITTED TO CSXT'WITH ORIGINAL COP TAL-6006 (0509)

Login Sample Receipt Check List
Client: CSX Transportation
Login Number: 58078
Creator: Daughtry, Beth
List Number: 1
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sampl2 collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Muitiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
T / F/ NA Comment
N/A
True
True
False
N/A 15.2
True
True
True
True
Tru e
True
True
True
True
True
True
True
N/A
True
N/A
N/A
False
True
TestAmerica Savannah
Page 18 of 18
Job Number: 680-58078-1
List Source: TestAmerica Savannah

®l®z amar
s

THE LEADER IN ENVIRONMENTAL TESTING
Job Number: 680-58997-1
Job Description: CSX Hamlet, NC WWTP
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Alan Pinnix
*
Approved for release.
Kathryn Smith
t*j4�
Project Manager I
7/9/2010 1:37 PM
Kathryn Smith
Project Manager I
[e-mail]
07/09/2010
cc: Mr. Jerry Cato
Mr. Mike Gregory
LWON-ENV0000038652//Project-9522202
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions 'should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A21-A: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI:,LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc. o VA AOcOgO
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericainc.com�
Page 1 of-18

Job Narrative
680-58997-1
Comments
No additional comments
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
Method(s) 353.2: The following sample(s) was analyzed outside of analytical holding time due to analyst oversight: June Outfall 2010
(680-58997-1).
No other analytical or quality issues were noted.
Page 2 of 18

METHOD SUMMARY
Client: ARCADIS U.S., Inc. Job Number: 680-58997-1
Description
Lab Location
Method Preparation Method
Matrix Water
Metals (ICP)
TAL SAV
40CFR136A 200.7 Rev 4.4
Preparation, Total Metals
TAL SAV
EPA 200.7
HEM and SGT-HEM
TAL SAV
1664A 1664A
HEM and SGT-HEM (Aqueous)
TAL SAV
1664A 1664A
Nitrogen, Nitrate -Nitrite
TAL SAV
MCAWW 353.2
Solids, Total Dissolved (TDS)
TAL SAV
SM SM 2540C
Organic Carbon, Total (TOC)
TAL SAV
SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal
Industrial Wastewater",
40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes",
EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 18

v
METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-58997-1
Method
Analyst
Analyst ID
40CFR136A 200.7 Rev 4.4
Robertson, Bryn
BR
1664A 1664A
Samuel, Sarita
SS
MCAWW 353.2
Ross, Jon
JR
SM SM 2540C
Robinson, Tiffany
TR
SM SM 5310B
Blackshear, Kim
KB
n
TestAmerica Savannah
Page 4 of 18 \

- SAMPLE SUMMARY
Client: ARCADIS U.S., Inc.
Job Number: 680-58997-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-58997-1 June Outfall 2010 Water 06/29/2010 0915 06/30/2010 1017
K
TestAmerica Savannah
Page 5 of 18

Client: ARCADIS U.S., Inc.
Client Sample ID: June Outfall 2010
Analytical Data
Job Number: 680-58997-1
Lab Sample ID:
680-58997-1
Date Sampled: 06/29/2010 0915
Client Matrix:
Water
Date Received: 06/30/2010 1017
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-173554
Instrument ID: ICPD
Preparation:
200.7
Prep Batch: 680-173457
Lab File ID: 070710.chr
Dilution:
1.0
Initial Weight/Volume: 50 mL
Date Analyzed:
07/07/2010 2144
Final WeightNolume: 50 mL
Date Prepared:
07/07/2010 1213
Analyte
Result (ug/L)
Qualifier MDL RL
Arsenic
20
U 4.6 20
Barium
30
2.3 10
Cadmium
5.0
U 2.0 5.0
Chromium
10
U 1.2, 10
Lead
10
U 4.0 10
TestAmerica Savannah Page 6 of 18

Client: ARCADIS U.S., Inc.
Analytical Data
Job Number: 680-58997-1
General Chemistry
Client Sample ID: June Outfall 2010
Lab Sample ID: 680-58997-1 Date Sampled: 06/29/2010 0915
Client Matrix:. Water Date Received: 06/30/2010 1017
Analyte
Result
Qua] Units MDL
RL
Dil
Method
Oil & Grease
5.0
U mg/L 1.4
5.0
1.0
1664A
Analysis Batch: 680-173066
Date Analyzed: 07/01/2010 1405
Prep Batch: 680-173054
Date Prepared: 06/30/2010 1830
TPH
5.0
U mg/L 1.4
5.0
1.0
1664A
Analysis Batch: 680-173066
Date Analyzed: 07/01/2010 1405
Prep Batch: 680-173054
Date Prepared: 06/30/2010 1830
Nitrate as N
1.7
H mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-173324
Date Analyzed: 07/01/2010 1657
Total Organic Carbon 12
mg/L : 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-173440
Date Analyzed: 07/06/2010 1617
Analyte
_ Result
Qual Units RL
RL
Di]
Method
Total Dissolved Solids 110
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 680-173063
Date Analyzed: 06/30/2010 1820
TestAmerica Savannah Page 7 of 18

DATA REP®RTNG QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section 'Qualifier Description
Metals
General Chemistry
Job Number: 680-58997-1
U Indicates the analyte was analyzed for but not detected.
U Indicates the analyte was analyzed for but not detected.
J Result is less than the RL but greater than or equal to the
MDL and the concentration is an approximate value.
H Sample was prepped or analyzed beyond the specified
holding time
TestAmerica Savannah
Page 8 of 18

Client: ARCADIS U.S., Inc.
Method Blank - Batch: 680-173457
Lab Sample ID: MB 680-173457/18-A Analysis Batch: 680-173554
Client Matrix: Water Prep Batch: 680-173457
Dilution: 1.0 Units: ug/L
Date Analyzed: 07/07/2010 2030
Date Prepared: 07/07/2010 1213
Quality Control Results
Job Number: 680-58997-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICPD
Lab File ID: 070710.chr
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
Analyte Result Qual MDL RL
Arsenic
20
U
4.6
20
Barium
10
U
2.3
10
Cadmium
5.0
U
2.0
5.0
Chromium
10
U
1.2
10
Lead
10
U
4.0
10
Lab Control Sample - Batch: 680-173457
Method: 200.7 Rev 4.4
Preparation: 200.7
L
Lab Sample ID:
LCS 680-173457/19-A
Analysis Batch: 680-173554
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-173457
Lab File ID: 070710.chr
Dilution:
1.0
Units: ug/L
Initial WeighWolume: 50
mL
Date Analyzed:
07/08/2010 1001
Final Weight/Volume: 50
mL
Date Prepared: 07/07/2010 1213
s
Analyte Spike Amount Result % Rec. Limit Qua[
Arsenic
2000
2190
109
85 - 115
Barium
2000
2250
113
85 - 115
Cadmium
50.0
55.5
111
85 - 115
Chromium
200
224
112
85 - 115
Lead
500
r
553
•
111
85 - 115
TestAmerica Savannah Page 9 of 18

. Qual*y ControUResulte
Client: ARCAD|GU.G,Inc. Job Number: 080-58897'1
Matrix Spike/ '
Method: %0UJRev 4.4
Matrix Spike Duplicate Recovery Report 'Batch:
680473457
`
Preparation: 30VJ
M8Lab Sample ID:
'B MS
Analysis Batch:
688-17355*
Instrument |o: |CPo
Client Matrix:
Water
Pmp,Bomh 080-173457
Lab File ID: 0707 O.ch
Dilution:
1.0
|nitiaVVoghtfVo|umo no mL
Date Analyzed:
07107/2010 uiOU
FimdVVoighUwoumo: 50 mL
Date Prepared:
0707/2010 1213
mooLab Sample ID:
680-58855-A,~CMno
Analysis Batch:
680173554
Instrument ID: |CPo '
Client matrix
vVote,
Prep Batch: 680�73*57
Lab File ID: 070710.mx
Dilution:
1.0
|mUa|weight/m|umo: 50 mL
Date Analyzed:
0707/2010-2105
Fimywm|yxVvo|umo: 50 mL
Date Prepared:
07/07/2010 1213
% Rec.
^nalyto
--
me mao
Limit
Rpo
nPoLimm meQua MSoQva
Arsepic
105 105
75'125
1
20
Barium
107 107
75'125
O
20
Cadmium
104 105
7e'125
1
zu
Chromium
105 106
75'125 �
o
oU
Lead
104 103
75'125
O
�
20
'
�
Teou*nenvauuvannu» Page 10 of IS
�

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-173054
Lab Sample ID:
MB 680-173054117-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/01/2010 1405
Date Prepared:
06/30/2010 -1830
Analysis Batch:.680-173066
Prep Batch: 680-173054
Units: mg/L
Quality Control Results
Job Number: 680-58997-1
Method: 1664A
Preparation: 1664A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight[Volume: 500 mL
Final Weight/Volume: 500 mL
Analyte Result Qual MDL RL
Oil & Grease 5.0 U 1.4 5.0
TPH 5.0 U 1.4 5.0
Lab Control Sample/ Method: 1664A
Lab Control Sample Duplicate Recovery Report - Batch: 680-173054 Preparation: 1664A
LCS Lab Sample ID: LCS 680-173054/18-A Analysis Batch: 680-173066 Instrument ID: No Equipment Assigned
Client Matrix: Water Prep Batch: 680-173054 Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 500 mL
Date Analyzed: 07/01/2010 1405 Final Weight/Volume: 500 mL
Date Prepared: 06/30/2010 1830
LCSD Lab Sample ID: LCSD 680-173054/19-A Analysis Batch: 680-173066 Instrument ID: No Equipment Assigned
Client Matrix: Water -Prep Batch: 680-173054 Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 500 mL
Date Analyzed: 07/01/2010 1405 Final WeightlVolume: 500 mL
Date Prepared: 06/30/2010 1830
% Rec.
Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual
Oil & Grease 99. 96 78 - 114 3 18
TPH 99 96 64 - 132 3 34
\1
TestAmerica Savannah Page 11 of . 18

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-58997-1
Method Blank - Batch: 680-173324
Method: 353.2
Preparation: N/A
Lab Sample ID: MB 680-173324/1
Analysis Batch:
680-173324
Instrument ID: Latchat 2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 7 mL
Date Analyzed: 07/01/2010 1637
Final Weight/Volume: 7 mL
Date Prepared: N/A
Analyte
Result
Qual MDL RL
Nitrate as N
0:050
U 0.010 0.050
Lab Control Sample - Batch: 680-173324
Method: 353.2
Preparation: N/A
Lab Sample ID: LCS 680-173324/2
Analysis Batch:
680-173324
Instrument ID: Latchat 2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 7 mL
Date Analyzed: 07/01/2010 1638
Final Weight/Volume: 7 mL
Date Prepared: N/A
Analyte
Spike Amount
Result
% Rec. Limit Qua[
Nitrate as N
0.500
0.506
101
Matrix Spike/
Method: 353.2
Matrix Spike Duplicate Recovery Report - Batch: 680-173324
Preparation: N/A '
MS Lab Sample ID: 680-59022-R-3 MS
Analysis Batch:
680-173324
Instrument ID: Latchat 2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0 -
Initial Weight/Volume: 25 mL
Date Analyzed: 07/01/2010 1641
Final Weight/Volume: 25 mL
Date Prepared: N/A
MSD Lab Sample ID: 680-59022-R-3 MSD
Analysis Batch:
680-173324
Instrument ID: Latchat 2
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Initial Weight/Volume: 25 mL
Date Analyzed: 07101/2010, 1642
Final Weight/Volume: 25 mL
Date Prepared: N/A
% Rec.
Analyte
MS MSD
Limit
RPD RPD Limit MS Qual MSD Qua[
Nitrate as N
100 100
0
TestAmerica Savannah
Page
12 of 18

Client: ARCADIS U.S., Inc.
Duplicate -Batch: 680-173324
Lab Sample ID:
680-58997-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/01/2010 1658
Date Prepared:
N/A
Analyte
Analysis Batch: 680-173324
Prep Batch: N/A
Units: mg/L
Sample Result/Qual Result
Quality Control Results
Job Number: 680-58997-1
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 7 mL
Final Weight/Volume: 7 mL
RPD Limit Qual
Nitrate as N 1.7 1.65 0
TestAmerica Savannah Page 13 of 18

Client: ARCADIS U.S., Inc.
Method Blank - Batch: 680-173063
Lab Sample ID:
MB 680-173063/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/30/2010 1820
Date Prepared:
N/A
Quality C®ntlroB Results
Job Number: 680-58997-1
Method: SM 2540C
Preparation: N/A
Analysis Batch: 680-173063 Instrument ID: No Equipment Assigned
Prep Batch: N/A Lab File ID: N/A
Units: mg/L Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Analyte Result Qual RL RL
Total Dissolved Solids - 5:0 U
Lab Control Sample/ Method: SM 2540C
Lab Control Sample Duplicate Recovery Report - Batch: 680-173063 Preparation: N/A
LCS Lab Sample ID: LCS 680-173063/2 Analysis Batch: 680-173063 Instrument ID: No Equipment Assigned
Client Matrix: Water v Prep Batch: N/A Lab File ID: N/A
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 100 mL
Date Analyzed: 06/30/2010 1820 Final Weight/Volume: 100 mL
Date Prepared: N/A
LCSD Lab Sample ID: LCSD 680-173063/3
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/30/2010 1820
Date Prepared:
N/A
Analyte
Total Dissolved Solids
Duplicate - Batch: 680-173063
Lab Sample ID:
680-59022-1-3 DU.
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
06/30/2010 1820
Date Prepared:
N/A
Analyte -
Total Dissolved Solids
TestAmerica Savannah
Analysis Batch: 680-173063
Prep Batch: N/A
Units: mg/L
% Rec.
LCS LCSD
93 97
Limit RPD
80 - 1204�
Analysis Batch: 680-173063
Prep Batch: N/A
Units: mg/L
Sample Result/Qual
81
Page 14 of 18
Result
78.0 '
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeightlVolume: 100 mL
Final Weight/Volume: 100 mL
RPD Limit LCS Qual LCSD Qual
25
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
RPD Limit Qual
4 25

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-58997-1
Method Blank - Batch: 680-173440
Method: SM 5310E
Preparation: N/A
Lab Sample ID: MB 680-173440/2
Analysis Batch: 680-173440
Instrument ID: TOC3
Client Matrix: Water -
Prep Batch: N/A
Lab File ID: T00070610.txt
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
25 mL
Date Analyzed: 07/06/2010 1019
Final WeightfVolume:
25 mL
Date Prepared: N/A
Analyte
Result Qual
MDL
RL
Total Organic Carbon
1.0 U
0.50
1.0
Lab Control Sample - Batch: 680-173440
Method: SM 5310B
Preparation: N/A
Lab Sample ID: LCS 680-173440/4
Analysis Batch: 680-173440
Instrument ID: TOC3
Client Matrix: Water
Prep Batch: N/A
Lab File ID: T00070610.txt
Dilution: 1.0
Units: mg/L
Initial WeightlVolume:
25 mL
Date Analyzed: 07/06/2010 1050
Final Weight/Volume:
25 mL
Date Prepared: N/A
Analyte
Spike Amount
Result
% Rec. Limit Qual
Total Organic Carbon
20.0
19.4 .
97 80 - 1'20
Matrix Spike/
Method: SM 5310B
Matrix Spike Duplicate Recovery Report - Batch: 680-173440
Preparation: N/A
MS Lab Sample ID:
680-58997-1
Analysis Batch:
680-173440
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: T00070610.txt
Dilution:
1.0
Initial Weight/Volume: 25 mL
Date Analyzed:
07/06/2010 1633
Final WeightlVolume: 25 mL
Date Prepared:
N/A
MSD Lab Sample ID:
680-58997-1
Analysis Batch:
680-173440
Instrument ID: TOC3
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: T00070610.txt
Dilution:
1.0
Initial Weight/Volume: 25 mL
Date Analyzed:
07/06/2010 1646
Final Weight/Volume: 25 mL
Date Prepared:
N/A
% Rec.
Analyte
MS MSD
Limit
RPD RPD Limit MS Qual MSD Qual
Total. Organic Carbon
99 98
80 - 120
1 25
TestAmerica Savannah Page 15 of 18

Client: ARCADIS U.S., Inc.
Duplicate -Batch: 680-173440
Lab Sample ID: 680-58923-H-1 DU Analysis Batch: 680-173440
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 07/06/2010 1528
Date Prepared: N/A
Analyte Sample Result/Qual
Total Organic Carbon 0.57 1
Quality Control Results
Job Number: 680-58997-1
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00070610.txt
Initial Weight[Volume: 25 mL
Final Weight/Volume: 25 mL
Result RPD Limit Qual
0.512 10 25 J
TestAmerica Savannah Page 16 of 18

LABORATORY INFORMATION
COC #
O TestAmerica Savannah - 5102 LaRoche Avenue, Savannah, GA 31404 Pi 912-354-7858 F; 912-352.0165
SHIPMENT INFORMATION
CHAIN OF ❑
TestAmerica North Canton - 4101 Shuffet Drive NW, North Canton, OH 44720 P: 330-497-9396 F: 330-497-0772
CUSTODY
OTestAmenca Tampa - 6712 Benjamin Road, Suite 100. Tampa, FL 33634 P: 813-885-7427 F: 813.885-7049
Shipment Method
TRANSPORTATION
OTestAmefica Pensacola -3355 McLemore Drive, Pensacola, FL 32514 P: B50-474-1001 F:850.478-2671
t
❑ TestAmerica Buffalo • 10 Hazelwood Drive, Suite 106. Amherst, NY 14228 P: 716-691-2600 F 716-961-7991
Shipment tracking No: 11
O TestAmerica Chicago - 2417 Bond Street, University Park, IL 60466 P: 708.534-5200 F: 708-534-5211
CSXT PROJECT INFORMATION Proj. State (State of Origin) CG
CONSULTANT INFORMATION Project d:
CSXT Project Number: Proj. City:
♦'L
Company:. PM:
CSXT Project Name:
Address: Email:
CSXT Contact: C - LWON:
l tl.no
City, State, ZIP: Phone: Fax:
Turnaround Time: ❑ Standard 6-13 Days Preservative Codes: 3 = Sulfuric Acid Note trap
COMMENTS
LAB USE
Cl 1 Day Rush S ecify #Days 0 = No Preservatives 4 = Sodium Thiosulfate Pres. METHODS FOR ANALYSIS
❑ 2 Day Rush gStandard 14 Days 1 = Hydrochloric Acid 5 =Sodium Hydroxide Code
l
❑ 3 Day Rush ❑ Other 2 = Nitric Acid 6 = Other
Deliverables: ❑ Other Deliv: Matrix Codes: SO = Soil LIQ = Liquid
}
❑ CSXT Standard (Level 11) GW = Groundwater SL = Sludge 3
❑ Level III ❑ EDD Required, Format: WW = Waste Water ' OI = Oil
❑ Level IV SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION' Q
Containers Sam le Collection' Filtered Type Matrix
Sample Identification Number & ` Date Time Sampler Y or Ni; Comp Code
I
Type or Grab
5`to A4
:
R.
b f1 CA-IA
Soo.vt. (-
..2 � 1b
q'12
0—;
-
F s�
Sa o.�r t1
-Z - i t7
C1
- !} cd Go ft
z o.wL
-Z� io
(Z
Z
,A
_
C C)
-
�H
=
Relinquished By:
Date/Time:
Rec v ,By
D to imp:
n
Comments & Special Analytical Requirements:
P T
Relinquished By:
Datemme:
eceived By:
Date/-tiMme:me:
t
Relinquished By:
Date/Time:
Received By:
oatemme:
Receiv ' ey ab atory:
k
Da "Rt
La Rem/��rks:
`as,
LAB USE Custody Intact
Custody Seal #
LAB Log Number
Im
Y
Y�'V G/
❑Yes ❑No
#
#
ORIGINAL — tit t UHN fU LABUHATUHY WITH SAMPLES INVOICE MUST BE SUBMITTED TO CSXT WITH ORIGINAL CDC TAL-6006 (0509)

Login Sample Receipt Check Last
Client: ARCADIS U.S., Inc.
Login Number: 58997
Creator: Kicklighter, Marilyn
List Plumber: 1
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled,
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Is the Field Sampler's name present on COC?
Sample Preservation Verified
T / F/ NA Comment
N/A
True
True
False no
False 17.2
True
True
True
True
True
True
True
True
True
True
True
True
N/A
True
N/A
N/A
N/A
True
Job Number: 680-58997-1
List Source: TestAmerica Savannah
TestAmerica Savannah
Page 18 of 18

WQ0000601 o CSXT HAMLET, NC
JULY 2010

TestAmerica
THE LEADER IN ENVIRONMENTAI.. TESTING
Job Number: 680-59918-1
Job Description: CSX Hamlet, NC WWTP Monthly
For:
CSX Transportation
173 CSX Drive
Hamlet, NC 28345
Attention: Mr. Mike Gregory
Y
Kathryn Smith
Project Manager I
[e-mail]
08/11 /2010
cc: Mr. Jerry Cato
Mr. Alan Pinnix
LWON-ENV0000052320; Project No.: R000011790
Approved for release.
Kathryn Smith
Project Manager I
af11/2010 9:24 AM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only -to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022;"IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc. eo `A°°oqo
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericaino.com
Page 1 of 18

Job Narrative
680-59918-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
Metals
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
L.
Page 2 of 18

METHOD SUMMARY
Client: CSX Transportation Job Number: 680-59918-1
Description Lab Location Method Preparation Method
Matrix Water
Metals_ (ICP) TAL SAV 40CFR136A 200.7 Rev 4.4
Preparation, Total Metals TAL SAV EPA 200.7
HEM and SGT-HEM TAL SAV 1664A 1664A
HEM and SGT-HEM (Aqueous) TAL SAV 1664A 1664A
Nitrogen, Nitrate -Nitrite TAL SAV MCAWW 353.2
Solids, Total Dissolved (TDS) TAL SAV SM SM 2540C
Organic Carbon, Total (TOC) TAL SAV SM SM 5310B
Lab References:
TAL SAV = TestAmerica Savannah
- Method References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
TestAmerica Savannah
Page 3 of 18

METHOD / ANALYST SUMMARY
Client: CSX Transportation
Job Number: 680-59918-1
Method
Analyst
Analyst ID
40CFR136A 200.7 Rev 4.4
Bland, Brian
BCB
1664A 1664A
Samuel, Sarita
SS
MCAWW 353.2
Ross, Jon
JR
SM SM 2540C
Robinson, Tiffany
TR
SM SM 5310B
Blackshear, Kim
KB
TestAmerica Savannah
Page 4 of 18

SAMPLE SUMMARY
Client: CSX Transportation
Job Number: 680-59918-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-59918-1 Outfall001 Water 07/29/2010 0910 07/30/2010 1002
e
TestAmerica Savannah
1
Page 5 of 18

Analytical Data
Client: CSX Transportation Job Number: 680-59918-1
Client Sample ID: Outfall 001
Lab Sample ID:
680-59918-1
Date Sampled: 07/29/2010 0910
Client Matrix:
Water
Date Received: 07/30/2010 1002
200.7 Rev 4.4 Metals (ICP)
Method:
200.7 Rev 4.4
Analysis Batch: 680-176766
Instrument ID: ICPD
Preparation:
200.7
Prep Batch: 680-176408
Lab File ID: • 080910.chr
Dilution:
1.0
Initial Weight/Volume: 50 mL
Date Analyzed:
08/09/2010 2114
Final Weight/Volume: 50 mL
Date Prepared: 08/05/2010 1457
Analyte
Result (mg/L)
Qualifier
MDL
RL
Arsenic
0.020
U
0.0046
. 0.020
Barium
0.020
0.0023
0.010
Cadmium
0.0050
U
0.0020
0.0050
Chromium
0.010
U
0.0012
0.010
Lead
0.010
U
0.0040
0.010
TestAmerica Savannah Page 6 of 18

Client: CSX Transportation
General Chemistry
Analytical Data
Job Number: 680-59918-1
Client Sample ID: Outfall 001
Lab Sample ID: 680-59918-1
Date Sampled: 07/29/2010 0910
Client Matrix: Water
Date Received: 07/30/2010 1002
Analyte Result
Qual Units MDL
RL-
Dil
Method
HEM (Oil & Grease) 5.0
U mg/L 1.4
5.0
1.0
1664A
Analysis Batch: 680-176044
Date Analyzed: 08/03/2010 1321
Prep Batch: 680-175994
Date Prepared: 08/02/2010 1515
Nitrate as N 0.38
mg/L 0.010
0.050
1.0
353.2
Analysis Batch: 680-176360
Date Analyzed: 07/30/2010 1703
Total Organic Carbon 9.7
mg/L 0.50
1.0
1.0
SM 5310B
Analysis Batch: 680-176704
Date Analyzed: 08/06/2010 1644
Analyte Result
Qual Units RL
RL
Dil
Method
Total Dissolved Solids 74
mg/L 5.0
5.0
1.0
SM 2540C
Analysis Batch: 680-176040
Date Analyzed: 08/02/2010 2050
9
TestAmerica Savannah Page 7 of 18

DATA DEPORTING QUALIFIERS
Client: CSX Transportation
Lab Section Qualifier Description
Metals
General Chemistry
TestAmerica Savannah
Job Number: 680-59918-1
U Indicates the analyte was analyzed for but not detected.
U Indicates the analyte was analyzed for but not detected.
Page 8 of 18

Quality Control Results
Client: CSX Transportation Job Number: 680-59918-1
Method Blank -Batch: 680-176408
Method: 200.7 Rev 4.4
Preparation: 200.7
Lab Sample ID:
MB 680-176408/15-A
Analysis Batch: 680-176766
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-176408
Lab File ID: 080910.chr
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 50 mL
Date Analyzed:
08/09/2010 2033
Final Weight[Volume: 50 mL
Date Prepared:
08/05/2010 1457
Analyte Result Qual MDL RL
Arsenic
0.020
U
0.0046
0.020
Barium
0.010
U
0.0023
0.010
Cadmium
0.0050
U
0.0020
0.0050
Chromium
0.010
U
0.0012
0.010
Lead
0.010
U
0.0040
0.010
Lab Control Sample - Batch: 680-176408
Method: 200.7 Rev 4.4
Preparation: 200.7 -
Lab Sample ID:
LCS 680-176408/16-A
Analysis Batch: 680-176766
Instrument ID: ICPD
Client Matrix:
Water
Prep Batch: 680-1764.08
Lab File ID: 080910.chr
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 50
mL
Date Analyzed:
08/09/2010 2038
Final WeightlVolume: 50
mL
Date Prepared: 08/05/2010 1457
Analyte
Spike Amount
Result
% Rec.
Limit Qual
Arsenic
2.00
2.00
100
85 - 115
Barium
2.00
2.06
103
85 - 115
Cadmium
0.0500
0.0505
101
85 - 115
Chromium
0.200
0.202
101
85 - 115
Lead
0.500
0.508
102
85 - 115
TestAmerica Savannah Page 9 of 18

Client: CSX Transportation
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-176408
MS Lab Sample ID: 680-59918-1 Analysis Batch: 680-176766
Client Matrix: Water Prep Batch: 680-176408
Dilution: 1.0
Date Analyzed: 08/09/2010 2119
Date Prepared: 08/05/2010 1457
MSD Lab Sample ID:
680-59918-1
Analysis Batch:
680-176766
Client Matrix:
Water
Prep Batch: 680-176408
Dilution:
1.0
Date Analyzed:
08/10/2010 1103
Date Prepared:
08/05/2010 1457
% Rec.
Analyte
MS MSD
Limit
Arsenic
105 113
75 - 125
Barium
109 118
75 - 125
Cadmium
104 111
75-125
Chromium
107 116
75 - 125
Lead
106 113
75 - 125
Quality Control Results
Job Number: 680-59918-1
Method: 200.7 Rev 4.4
Preparation: 200.7
Instrument ID: ICPD
Lab File ID: 080910.chr
Initial Weight/Volume: 50 mL
Final WeightlVolume: 50 mL
Instrument ID: ICPD
Lab File ID: 080910.chr
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
RPD RPD Limit MS Qual MSD Qual
7 20
8 20
6 20
9 20
6 20
TestAmerica Savannah Page 10 of 18

QuaNty Contro9 Results
Client: CSX Transportation Job Number: - 680-59918-1
Method Blank - Batch: 680-175994
Method: 1664A
Preparation: 1664A
Lab Sample ID: MB 680-175994/13-A
Analysis Batch: 680-176044
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-175994
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial WeighWolume:
500 mL
Date Analyzed: 08/03/2010 1321
Final Weight/Volume:
500 mL
Date Prepared: 08/02/2010 1515
Analyte
Result Qua[
MDL
RL
HEM (Oil & Grease)
5.0 U
1.4
5.0
Lab Control Sample/
Method: 1664A
Lab Control Sample Duplicate Recovery Report - Batch: 680-175994
Preparation: 1664A
LCS Lab Sample ID: LCS 680-175994/14-A
Analysis Batch: 680-176044
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-175994
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
500 mL
Datd Analyzed: 08/03/2010 1321
Final Weight/Volume:
500 mL
Date Prepared: 08/02/2010 1515
LCSD Lab Sample ID: LCSD 680-175994/15-A Analysis Batch: 680-176044
Client Matrix:
Water
Prep Batch: 680-175994
Dilution:
1.0
Units: mg/L
Date Analyzed:
08/03/2010 1321
Date Prepared:
08/02/2010 1515
% Rec.
Analyte
LCS LCSD Limit
HEM (Oil & Grease)
97 96 78 - 114
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 500 mL
Final Weight/Volume: 500 mL
RPD RPD Limit LCS Qual LCSD Qua[
2 - � 18 .�.w.
TestAmerica Savannah Page. 11 of 18

Client: CSX Transportation
Method Blank - Batch: 680-176360
Lab Sample ID:
MB 680-176360/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/30/2010 1640
Date Prepared:
N/A
Analysis Batch: 680-176360
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-59918-1
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Analyte
Result Qual
MDL
RL
Nitrate as N
0.050 U
0.010
0.050
Lab Control Sample - Batch: 680-176360
Method: 353.2
Preparation: N/A
Lab Sample ID:
LCS 680-176360/2
Analysis Batch: 680-176360
Instrument ID: Latchat 2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2
mL
Date Analyzed:
07/30/2010 1641
Final Weight/Volume: 2
mL
Date Prepared: N/A
Analyte Spike Amount
Nitrate as N 0.500
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-176360
Result % Rec. Limit Qual
0.497 99
MS Lab Sample ID: 680-59899-E-1 MS Analysis Batch: 680-176360
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 07/30/2010 1644
Date Prepared: N/A
MSD Lab Sample ID: 680-59899-E-1 MSD Analysis Batch: 680-176360
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0
Date Analyzed: 07/30/2010 1645
Date Prepared: N/A
Analyte
Nitrate as N
% Rec.
MS MSD
101 98
Limit
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 10 mL
Final Weight/Volume: 10 mL
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 10 mL
Final Weight/Volume: 10 mL
RPD RPD Limit MS Qual MSD Qual
1
TestAmerica Savannah - Page 12 of 18

Client: CSX Transportation
Duplicate -Batch: 680-176360
Lab Sample ID:
680-59910-E-23 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
07/30/2010 1701
Date Prepared:
N/A
Analyte
Analysis Batch: 680-176360
Prep Batch: N/A
Units: mg/L
Sample Result/Qua[ Result
Nitrate as N 0.050 U
Quality ContrPoB Results
Job Number: 680-59918-1
Method: 353.2
Preparation: N/A
Instrument ID: Latchat 2
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
RPD Limit Qual
0.05Q NC U
TestAmerica Savannah Page 13 of 18

Client: CSX Transportation
Method Blank -Batch: 680-176040
Lab Sample ID: MB 680-176040/1 Analysis Batch: 680-176040
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: mg/L
Date Analyzed: 08/02/2010 2050
Date Prepared: N/A
Analyte
Result
Total Dissolved Solids
5.0
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-176040
LCS Lab Sample ID:
LCS 680`176040/2
Analysis Batch: 680-176040
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Datp Analyzed:
08/02/2010 2050
Date Prepared:
N/A
LCSD Lab Sample ID:
LCSD 680-176040/3
Analysis Batch: 680-176040
Client Matrix:
Water -
Prep Batch: N/A
Dilution:
1.0
Units: mg/L
Date Analyzed:
08/02/2010 2050
Date Prepared:
N/A
Analyte
Total Dissolved Solids
Duplicate - Batch: 680-176040
Lab Sample ID:
680-59905-13-1 DU
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
08/02/2010 2050
Date Prepared:
N/A
Analyte
Total Dissolved Solids
Quality Control Results
Job Number: 680-59918-1
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final WeightlVolume: 100 mL
Qual RL RL
U 5.0 5.0
Method: SM 2540C
Preparation: N/A
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
% Rec.
LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual
89 93 80 - 120 5 25 µ
Method: SM 2540C
Preparation: N/A
Analysis Batch: 680-176040 Instrument ID: No Equipment Assigned
Prep Batch: N/A Lab File ID: N/A
Units: mg/L Initial Weight/Volume: 100 mL
Final Weight/Volume: 100 mL
Sample Result/Qual Result RPD Limit
76 77.0 1 25
Qual
TestAmerica Savannah Page 14 of 18

Client: CSX Transportation
Method Blank -Batch: 680-176704
Lab Sample ID:
MB 680-176704/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
08/06/2010 1313
Date Prepared:
N/A
Analyte
Quality Control Results
Job Number: 680-59918-1
Method: SM 5310B
Preparation: N/A
Analysis Batch: 680-176704 Instrument ID: TOC3
Prep Batch: N/A Lab File ID: T00080610.txt
Units: mg/L Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Result Qual MDL RL
Total Organic Carbon 1.0 U 0.50 1.0_
Lab Control Sample - Batch: 680-176704 Method: SM 5310B
Preparation: N/A
Lab Sample ID: LCS 680-176704/4 Analysis Batch: 680-176704 Instrument ID: TOC3
Client Matrix: Water Prep Batch: N/A Lab File ID: T00080610.txt
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL
Dat6 Analyzed: 08/06/2010 1344 Final Weight/Volume: 25 mL
Date Prepared: N/A
Analyte Spike Amount Result % Rec. Limit Qual
Total Organic Carbon
20.0 19.2
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-176704
MS Lab Sample ID:
680-60044-B-2 MS
Analysis Batch: 680-176704
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
08/06/2010 2002
Date Prepared:
N/A
MSD Lab Sample ID:
680-60044-B-2 MSD
Analysis Batch: 680-176704
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Date Analyzed:
08/06/2010 2015
Date Prepared:
N/A
% Rec.
Analyte MS MSD Limit
Total Organic Carbon
96 80 - 120
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00080610.txt
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
__.........._....:_.._..........................._....... _.......... ................... ............ .....
.......
Instrument ID: TOC3
Lab File ID: T00080610.txt
Initial Weight/Volume: 25 mL
Final WeighUVolume: 25 mL
RPD RPD Limit MS Qual MSD Qual
94 93 80 - 120 1 25
TestAmerica Savannah Page 15 of 18

Client: CSX Transportation
Duplicate - Batch: 680-176704
Lab Sample ID:
680-59918-1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
08/06/2010 1655
Date Prepared:
N/A
Analyte
Total Organic Carbon
Analysis Batch: 680-176704
Prep Batch: N/A
Units: mg/L
Sample ResulUQual
9.7
Quality Control Results
Job Number: 680-59918-1
Method: SM 5310B
Preparation: N/A
Instrument ID: TOC3
Lab File ID: T00080610.txt
Initial Weight/Volume: 25 mL
Final Weight/Volume: 25 mL
Result RPD Limit
9.82 1 25
Qua]
TestAmerica Savannah Page 16 of 18

LABORATORY INFORMATION
CCC ##
O TestAmerica Savannah - 5102 LaRoche Avenue, Savannah,13A 314U4 P: 912.354-7858 'r: 912-352-0165
'
CHAIN O F
Q TestAmerica North Canton - 4f Canton. 01 Shuffel Drive NW. North Caon. OH 44720 P: 330-497.9396 F: 330-497.0772
SH.i PMENT INFORMATION
Shipment Method:
Q TestAmerica Tampa - 6712 Beniamin Road. Suite 100. Tampa, FL 33634 P: 813-885.7427 F: 813-885-7049
CUSTODY
O TestAmerica Pensacola - 3355 t�lcLelnore Drive. Prllsacola. FL 32574 P:-850.474.1001 F: 850.478-2671
Shipment Tracking No:
TR,ANSPORTATiON
Q TestAmerica Buffalo - 10 Hazelwood Drive, Suite 106, Amherst. NY 14228 P: 716.691-2600 F: 716-961.7991
Q TestAmerica Chicago - 2417 Bond Street. University Park, IL 60466 P: 700-534-5200 F: 708-534-5211
Prof. State (State of Origin) /
CSXT PROJECT INFORMATION
CONSULTANT INFORMATION Projects:
CSXT Project Number: Proj. City: t Company: PM:
Address: Email;
CSXT Project Name:
J LA I t CA� y—� C�
_\ �r�t
LWON: /J City, Slate. Zip: Phone; Fax:
CSXT Contact: / r _ ,c
l
Turnaround Time: ❑ Standard 6-1 Days Preservative Codes: 3 = Sulfuric Acid Note COMMENTS LAB USE
❑ 1 Day Rush Specify # Days 0 = No Preservatives 4 = Sodium Thiosulfate Pres. METHODS FOR ANALYSIS
❑ 2 Day Rush Standard 14 Days 1 = Hydrochloric Acid 5 = Sodium Hydroxide Code
❑ 3 Day Rush ❑ Other 2 = Nitric Acid 6 = Other
Deliverables: ❑ Other De0v: Matrix Codes: SO = Soil LIQ = Liquid
❑ CSXT Standard (Level 11) v_ ___ GIN = Groundwater SL = Sludge V �tr �
❑ Level III ❑ EDO Required, Format: WIN = Waste Water OI = Oil
❑ Level IV SW = Surface Water SOL = Other Solid
SAMPLE INFORMATION
Containers Sam le Collection Filtered Type Matrix
o Sample Identification Number & Date Time Sampler Y or N or Grab Code �.
Type
F
IV
01
Soo tM j
Z`=/D
L�
J. C---
�^ A )L
Z`=
217-10
Lei()
� d
r
E.r r iC
Oate�me:
Comments & Speclat Analytical Requirements:
Relinquished By:
Dalefrime:
/
b n
��I Y )U 1( ^
1 t j l..i
Relinquished By:
Datefrirne:
Received By:
Oate7Time:
Relinquished By.
Uatelrime:
Received By:
Oa[e�me:
cerved By Lgbor3ory:
( �+ `\ (�c -1t
!r �' ` `•
OatelTrjne:
I �\ C • ^ '
Lab Homarks:
LAB USE: Custody Intact
❑Yes ONO
IMVnICF KAI 1CT AP SI IRMITTFf)
Custody Seal s
#
Tr) CSXT WITH ORIGINAL
LAB Log Number ( C
# v y
CDC TAL-6006 (05091
ORIONAt• - RE TURN TO LAIB&Arom1 WITH SAMPLES

Login Sample Receipt Check List
Client: CSX Transportation
Login Number: 59918
Creator: Daughtry, Beth
List Number: 1
Question T / F/ NA Comment
Radioactivity either was not measured or, if measured, is at or below
True
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the sample IDs on the containers and
True
the COC.
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
N/A
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Job Number: 680-59918-1
List Source: TestAmerica Savannah
TestAmerica Savannah
Page 18 of 18

TR�1I�TSPQ1tTA�'ION'
Carl A. Gerhardstein, P.E.
AVP Environmental Systems and Sustainability
[phone]
Mr. Joel Shields
North Carolina Department of
Environment, and Natural Resources
Division of Water Quality
225 Green Street — Suite 714
Fayetteville, NC 28301
RECEIVED
OCT 18 2010
DENR-FAYEfTEMLLE REGIONAL OFFICE
Permit No. W00000601; Richmond County
CSX Transportation; Inc. (CSXT); Hamlet; NC
Public Safety & Environment _
500 Water Street, J275
Jacksonville, FL 32202
October 15, 2010
File. 9613703
Mr. Shields,
We are in receipt of yourletter, dated October 11, 2010 regarding the Compliance Evaluation
Inspection conducted on October 4 2010 at our Hamlet, NC. facility.
CSX Transportation is committed to maintaining the. highest standards of environmental compliance
and we are pleased thatyou found the facility to be in compliance.
If you have any questions or comments, please do not hesitate to contact me at [phone]
Sincerely,
arA.ar stem,
AVP Environmental Systems and Sustainability
Enclosures

North Carolina
2 4j Department of Environment & Natural Resources
Division of Water Quality
Aquifer Protection Section
MONITORING WELL INSPECTION REPORT
sw ,f�gm��'eQi`« � Date �." „.
Well Location: C f�/�do
� �
Owner: WELL VYPE 3,Y"40ai.;l�
Address:X66 tjA- e/1 5-i .�Rgkte V;11,e lA, 32 a -OIL County R-,Cz. E>,V s
Road/StreetK[ w 77 r.54Lr. j. n
Quad No.
MW #-
b wl SerialNo.CDdf/oDY97S
M I? �) Lath . ! Long. �r41' 3
We1T' onstruetion .
Well Contractor
'Name Address .
Contractor Certification# Check Items Meets Min. Standards Remarks
Measured Yes No
Permit Required ?(YIN) I.....
Location -]Distance From:.......... .
Water Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
Other Poll. Source( )
Other•Poll. Source( )
Casino
Type.......................
Depth ...........
Weight/thickness ............... .
Height(A.L.S.).................
Other ( )
Grout J 6
Type.......................
Thickness ..... :..............
Depth ...pp .......... ......... .
Other( dd 2 d4,j,
Screens
Screened interval... . . .....
Other( )
Well Contractor ............
Abandonment
t
(Permit No.WQ ®dO o
1
{y
f
Plastic Carbon Cialy. St. Other
a i
y
1
•d
5 g
C
s
�•
✓
t
t
1
;
Temporary, ........ .......
. i
Permanent .................
I

Cuttings
Reports
Construction (GW-1) ...... .
Abandonment (GW-30) .....
Well Head Completion'.".:. .
Access port ...............
Water tight pipe entry ... ,
Well entry .
Date Well Constructed q' / 6 `" l M6
INSPECTOR t�Q�
Name
Witness(es)
(If Available) Name
Name
I
Check Items Meets Min. Standards 1. Remarks I
t� 1
i Measured Yes No
ii
r
4
Office
Address
Address
Type
Type

ec l /e-"1 fro krd do R (, North Carolina .
Department of Environment & Natural Resources
d// ,v Division of Water Quality
Aquifer Protection Section
`� v w ►� MONITORING WELL INSPECTION REPORT
Well Location:_(,
Owner: C
Address: _S"o o lOA4e-..,2
Well Contractor
Name
Contractor Certification#
]Permit Required ? (Y/N) I.
Location - Distance From:.......... .
Waiver Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
Other Poll. Source( )
Other Poll. Source( )
Casino
Type............F� 20
Depth..:...................
We.ight/thickness ............. :. .
Height(A.L.S.).................
Other ( )
Grout
Type ......... �.? .... YY
Thickness .....:............. .
Depth ........... P.
Other(,6r-df 04i'Pe ) ��
Screens
Screened interval Jg
Other( )
Well Contractor ............
Abandonment
Temporary ..................
Permanent .................
4 .
�ldC� Date -T /AVD107 D l0
4. WELL YPE 4 a Y1e40f?,f, S
e 1a9, J2 �Zo2 County�c�.�p
Road/StreeWC,0AjV i7
Quad No.
MW #= - .7.
Serial No. CiD e po !/Zj
Address
Check Items Meets Min. Standards
Remarks R
(Permit NoW Q dO 1
Plastic Carbon Ga1V. St.
f -a
V Y
}
si
k
- $
r¢F 9-
✓ � rtr

Cuttings
Re orts
Construction (GW-1) ..... .
Abandonment (GW-3 0), .
Well Head Completion.'..'. }.. .
Access port ...............
Water tight pipe entry. .
Well entry .... ......... .
Date Well Constructed ' l L, - /q S)L
INSPECTOR
Check Items Meets Min. Standards;, Remarks j
Measured Yes No j
i;
tl,
3,
.B;
Name Office
(If Available) Name Address Type
Name Address Type
'M

bo cv-) G(A e �North Carolina
R ex I e— W ',�epartment of Environment & Natural Resources
+ Division of Water Quality
/e �ng12�Ler41 Aquifer Protection Section
MONITORING WELL INSPECTION REPORT
Well Location:_ ��� t/�Z'" ��i! �/� Date 3 .3 10
Owner'. C �� %d2�s>t�c�aia$.a.�r ire. ° WELL YPE /'J%�oatvJS <'
Address. -Son tj,44ee 5-h 32 County lk.,J of -0A
Road/Streowc&jV 77
Quad No.
MW #= 3
Serial No. Cyrtl 1406,60954
La ? Long. f
Wellnsiraaction
Well Contractor
Narne
Contractor Certification#
)Permit Required ? (Y/N) I.....
Location - Distance From:.......... .
Water Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
Other Poll. Source( )
Other Poll. Source( )
)1
Casino (.-t
Type......................
Depth.................• ..... .
Weight/thickness ................
Height (A.L.S.) ...........o..•.
Other ( )
Grout
Type ............. ov� .
Thickness .....................
Depth.......................
Other( 1131
Screens
Screened interval ...3. . 43
Other( )
Well Contractor ............ .
Abandonment
Temporary .................
Permanent .................
Address '
Check Items Meets Min. Standards Remarks
Measured Yes No
(Permit No.&J Q pc, 0
r
Plastic Carbon (galy. St. Other
j i y V i� I,e b CSxS Y,
I

Cuttings
Reports
Construction (GW-1) .......�
Abandonment (GW-3 0)
Well I3ead Completion .... t.l
Access port ..........
Water tight pipe entry ...
Well entry .... ; . . ... ±, .:... .
leckItems Meets Min. Standards,. Remarks j
V
Measured Yes No j.
I it
i 9 a
y" Y.
Date Well Constructed
INSPECTQR '�� Z V
Name Off] ce
Witness(es) •
(If Available) Name Address Type
Name Address Type

4rvm �l p%fie Lou e4da,e-'L' North Carolina
4- Department of Environment & Natural kesources
Q Division of Water Quality
Aquifer Protection Section
MONITORING WELL INSPECTION REPORT
Well Location: C����d�2" ��i! �/� f
4 Owner` (2
j2- �102 t.
1`
•
WeII �onstructlo�a �
Well Contractor
'
�
Date -' 1
WELL E W?,)*01 ofzev,rs5
County
Road/StreeWC ¢1r,�a/ ' -77
Quad No.
MW #=
Serial No.Cpvr / 1/6n &,?3
Lat,f. Ttgjzo Lorig.7q, GSG (. G
- - ..
Name
Address
Contractor Certification#
Check Items
Meets Min. Standards
Remarks
&
Permit Required ? (YIN) 1.....
Measured
Yes
(
No
(permit No.&)t90
d
]Location - Distance From:...........
Water Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
F
Other Poll. Source(
F
r /
Other Poll. Source( )
Casing �/�
,,
f
;
Plastic Carbon Galy. St. Other
:?
Type........ ...............
I
Depth ......................
r/
WeighVthickness ..............
r
Height (A-L.S.) ........... r .4
It4
Other
t
Grout
Thickness .....:.............
Depth.......................
Y
/
1
Other( a +J t �) 3%` ��
s
E
6
4
pp
Screens
Screened interval
r
4
t}}[
rA
R.
j
.. a? .......
F.
Other(
t
Well Contractor ............
r ��
Abandonment
x
Temporary .................
!
E
j
Permanent .................
t"

Cuttinjzs
Rel orts
Construction (OW-1) ...... .
Abandonment (GW-3 0) s... _. .
Well Head Completion-.-. .
Access port.
Water tight pipe entry ...:.
" Well entry } ... .
t,necx xMMS
Meets Min. Sta11 rds L Remat.ks
Measured
"Yes
t
No
4
s
R
0.
F
t
p
r.
---�
A.

14e. ab'Iri � ilk e.e 'kiz)4rfQ/gr'Zou Carolina
I Department.o f Environment & Natural Resources
�Qd i'J Division of Water Quality
Aquifer Protection Section
MONITORING WFLL INSPECTION REPORT
We11 Location: e �� ,�t'ig,l�2'" /�� ! ¢� Date n B ©f a
Owner` C 5X /�is�s>fg�Di�ia� moire.. �. WELL typLf6'yl c� �llo�dev+l�
Address: Sc) 6; tj' ,i4e e 5_47 County C4;� e,
Y Road/StreeWC&jV -7
Quad No.
MW # S-
Serial No. CDn/fi 0x&
at.3� 9 G9� ong•7 6
Well.constraactioaa �,. .... .
Well Contractor
Name.
Contractor Certification#
Permit Required ? (YIN) I......
]Location - Distmice )From:...'........ .
Wager Tight Sewage/waste collection
Waste Disposal (septic tank.drain field)
Other Poll. Source(. )
Other Poll. Source( )
Casino
Type,.......,v... ....,
Depth.: ...................
Weight/thickness .........C' ..� . .
Height (A.L.S.) ....... ��. J... .
Other ( )
Grout
Type............... �. We ke/Y6'tr111�
Thickness ...... ..............
Depth.......................
Other( �,3 —d
Screens
Screened interval ............
Other( )
Well Contractor .............
Abandonment
Tempoiary ..................
Permanent ................
Address
Check Items Meets Min. Standards
t
Remarks t
(PerU)jtNo.&JQ d C0 104 1
]ast)i Carbon Galy. St. Other
a
c
F k
s
F �
�
�
t
r
E . .
_
'
lJA
}

cuttings
Reports
Construction (GW-1) ...... .
Abandonment (GW-30)
Well Head Completion..... .
Access port ...............
Water tight pipe entry,
Well entry ............. .
Date Well Constructed �—
INSPICCT®R (�Y�
Name
Witness(es)
(If Available) Name
iCy ?f
Check Items
Meets Min. Standards`, Remarks j
Measured
Ales
t.
No }:
r
(/
l:
I;
Off] cc
Address
Name Address
Type
Type

1 "North Carolina
� 2A_d rler� Department of Environment & Natural Resources Division of Water Quality
Aquifer Protection Section
MONITORING WELL INSPECTION REPORT
Well Location:_ SK 2 AM ZA1- . 1/2 Date � D �(
Owner' e:Sg 7—ghzfs'pa sa-14,�,,r ��• WELL YPE 10o•,!,'o1g.,
Addxess:.�o® La��/� Eli//,e �.o J2�2 County
Road/StreeWC N&jV ry-7
Quad No.
MW
Serial.No. iW, Cori!=41
Lat,3f.9,xo�3 Lon
Well Contractor
Name
Contractor Certification#
Permit Required ? (Y[N) I.....
Location - Distance From:.......... .
Water Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
Other Poll. Source( )
Other Poll. Source( )
Casino
Type ........... �.�.L ......
Depth .. ......... _ x'
Weight/thickness ....... �..
Height (A.L.S.) .........©� r.. v. .
Other ( )
Grout
Type...........' .............
Thickness .....................
Depth........................
Other( )
Screens
Screened interval ......
Other( )
X:D Plate -
Well Contractor ............
Abandonment
Temporary ..... .......... .
Permanent ..................
Address • .
Check Items Meets Min. Standards
r
v
Remarks
(Permit No.&) d db IDA
1 1
f -i tiAarbon GaIv. St. Other 's
J I,

Cuttings
Reports
Construction (GW-1) ....... .
Abandonment (GW-30)_t .
Well Head Completion
Access port., ..............
Watertight pipe entry. , . ,
Well enti-y
Check Items
Meets,Min. Standards;♦' `R6iarlcs .;
Measured'
Yes No j
r.
r r_
.n
Date Well Constructed
INSPECTOR... (�
Name Office
Witness(es)
(If Available) Name Address Type
Name Address Type

t t Dow.�C y
�.�(j lCol� Re Sll e W North Carolina
Department of Environment & Natural Resources
Up �PA-d t �'`��' Division of Water Quality
Aquifer Protection Section
MONITORING WELL INSPECTION REPORT
Well Location: C ZIX — Am le-e" I&i ` Date Z
l e .9 ° WELL 7PE
Owner: 194ogg,PD A-�iae.r fie. �iv,PS
Address: X6 ® t+),g 4e/z V; Ae P.41 32 �102 County R.'r-4,v14E
Road/StreeWC¢/w`/ 77
Well Contractor
Name
Contractor Certification#
)Permit Required,? (YID I.....
Location - Distance From:.......... .
Water Tight Sewage/waste collection
Waste Disposal (septic tank drain field)
Other Poll. Source( )
Other Poll. Source( )
Casing
Type ....... ..... ;
Depth.. t ...................
Weight/thickness ................
Height(A.L.S.).................
Other ( )
Grout JJ
Type..........�.`.`7.�...
Thickness .....:. JAI .
Depth.......................
Other(
Screens
Screened iinterval ... -. '��✓
Other( )
TD
Well Contractor ............
Abandonment
Temporary ...................
Permanent .................
Checkltems Meets Min. Standards
Quad No.
MW #_
Serial Ne o :`�
La ong.� d
I

CuttinLys
Reports
Construction (OW-1) ....... .
Abandonment (GW-30) .. ' .
Well Head Completion
Access port ...............
Water tight pipe entry, ... .
Well entry ..................
Date Well Constructed
Check Items Meets Mio.Stand ards`, Remarks
Measured Yes No
3 r
s
r:
'r
INSPECTOR
Name Office
(If Available) Name Address Type
Name Address Type

4 to
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
,everly Eaves Perdue Coleen H. Sullins
Governor Director
February 22, 2010
Mr. Carl A. Gerhardstein, Director of Environmental Systems
CSX Transportation, Inc.
500 Water Street — J275
Jacksonville, Florida 32202
RECEIVED 1 DENR 1 DVVQ
Aquifer Protection Section
MAR 0 4 2010
Subject: Permit Extension
Permit No. WQ0000601
CSX Transportation, Inc.
Infiltration Lagoon System
Richmond County
Dee Freeman
Secretary
Dear Mr. Gerhardstein:
On August 5, 2009, Session Law 2009-406, entitled "An Act to Extend Certain Government
Approvals Affecting the Development of Real Property Within the State," was enacted by the General
Assembly and signed into law. The Act, known as the Permit Extension Act of 2009, extends the
expiration date of certain government approvals and permits. For additional information, the following
website ( http:/portal.nedenr.org/web/wqlaps/lau#extension ) can be viewed to address this statute and
affected DWQ permits.
Non -discharge permit, WQ0000601, issued by the Division of Water Quality falls within the
scope of this Act and is therefore being extended until 31 July 2017. Please note per your permit, a
renewal application must still be submitted six months in advance of the extended expiration date. If CSX
Transportation needs to modify, upgrade, retrofit infrastructure at this facility which would require
modification of the permit; a permit application can be submitted for review and the necessary modified
permit issued.
If you have any questions regarding this letter, please contact Division staff in the Fayetteville
Regional Office at [phone] or Central Office at [phone]. Thank you in advance for your
cooperation.
Sincerely,
.
�AWW�2'1
Jim Barber
Aquifer Protection Section
cc: Fayetteville Regional Office, Aquifer Protection Section
WQ0000601 Permit File
WQ0000601 Notebook File
Richmond County Health Department
Technical Assistance and Certification Unit
DWQ Budget Office —Fran McPherson
AQU[FER PROTECTION SECTION
1636 Mail Service Center. Raleigh, North Carolina 27699-1636
Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604 One
Phone: [phone] FAX 1; 919-71M588; FAX 2: 919-715-60481 Customer Service: 1-877-623-6748 NorthCa.rohna
Internet: www.ncwaterguality.org �
An Equal Opportunity 4 Affirmative Action Em�ati�rQ'�ly
ployer