NCS000315_Nexeo Charlotte Semi-annual Sampling Results_Yr 9 Per 1_20180327

nexeo�
solutions
March 27, 2018
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Re: Semi -Annual Storm Water Sampling Results for Year 9, Period 1
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 9, Period 1 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on March 6,
2018, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315). Per
the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001 during a
representative storm event that consisted of 0.49 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN -53 at Harding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table 1.
Table 1
Discharge Characteristic
Inspection Result
Color
Slight brown
Odor
None observed
Clarity
Slightly cloudy
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Stormwater Pollution
No significant change
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
NexeoSolutions.com I Connect.

nexeo�
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value with the exception of pH of 3.62 detected in the field, which is unusual compared to previous
monitoring events from the past three years. Records indicate that the field meter used to analyze pH was properly
calibrated. The lab reported pH as 7.2, and although outside of 15 minute hold time, this result is more consistent
with previous monitoring events. No spills or significant change in operations was identified and all other
parameters were within benchmark values. Thus, the low field pH detected on March 6, 2018, appears to be an
anomalous pH reading. However, in accordance with Tier One benchmark protocol, the facility will conduct a
stormwater inspection to identify possible causes of the pH exceedance and follow the corrective action procedure
accordingly.
All of the results of the storm water sample analyses along with their corresponding benchmark values as listed in
the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
43 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<2.6 mg/L
30 mg/L
Chemical Oxygen Demand
31 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
3.62 (field reported) / 7.2 (lab reported)
6 - 9
Total Rainfall
0.49 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 9, Period 2) between July 1 and December 31, 2018, and will
submit the results per the requirements of the permit. Should you have any questions or require additional
information, please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions, LLC
NexeoSolutions.com I Connect.

ENCLOSUREI LABORATORY RESULTS

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-149643-1
Client Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
roi
EHS Support, LLC
100 Georgia Ave
Daphne, Alabama 36526
Attn: Amy Bauer
Authorized for release by. -
311512018
y.3/15/2018 4:05:19 PM
Jerry Lanier, Project Manager 1
[phone] e.3410
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Table of Contents
TestAmerica Job ID: 680-149643-1
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ..........................................
3 L
Sample Summary .........................................
5
Method Summary ...........................................
6
Definitions/Glossary.......................................
7
Detection Summary ........................................
8
Client Sample Results ......................................
9
Surrogate Summary .......................................
10
QC Sample Results ........................................
11
QC Association Summary ...................................
14
Lab Chronicle ............................................
15
Chain of Custody ..........................................
16
Receipt Checklists .........................................
17
Certification Summary ......................................
18
Page 2 of 18
TestAmerica Savannah
3/15/2018

Case Narrative C
Client: EHS Support, LLC TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-149643-1
Laboratory: TestAmerica Savannah
Narrative
� f -'M =1 \
Client: EHS Support, LLC
Project: Nexeo - Charlotte, N.C. (Outfall 001) F
Report Number: 680-149643-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 03/07/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.5 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples Outfall 001 (680-149643-1) and Trip Blank (680-149643-2) were analyzed for Volatile Organic Compounds (GC -MS) in
accordance with EPA Method 624. The samples were analyzed on 03/11/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
680-515382.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
OIL AND GREASE AND TPH
Sample Outfall 001 (680-149643-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples were
prepared and analyzed on 03/13/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with preparation batch 680-515578.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Outfall 001 (680-149643-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were analyzed
on 03/13/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample Outfall 001 (680-149643-1) was analyzed for chemical oxygen demand in accordance with SM 5220D. The samples were
analyzed on 03/13/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Outfall 001 (680-149643-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed on
TestAmerica Savannah
Page 3 of 18 3/15/2018

Case Narrative C
Client: EHS Support, LLC TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-149643-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
03/14/2018.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 4 of 18 3/15/2018

Sample Summary
Client: EHS Support, LLC TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Lab Sample ID Client Sample ID Matrix Collected Received
680-149643-1 Outfall 001 Water 03/06/18 13:46 03/07/18 09:20
680-149643-2 Trip Blank Water 03/06/18 13:46 03/07/18 09:20
TestAmerica Savannah
Page 5 of 18 3/15/2018
0

Method Summary
Client: EHS Support, LLC
TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method Method Description
Protocol
Laboratory
624 Volatile Organic Compounds (GC/MS)
40CFR136A
TAIL SAV
1664A HEM and SGT -HEM
1664A
TAIL SAV
SM 2540D Solids, Total Suspended (TSS)
SM
TAIL SAV
SM 4500 H+ g pH
SM
TAIL SAV
SM 5220D COD
SM
TAIL SAV
Protocol References:
1664A = EPA -821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References: F
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 6 of 18 3/15/2018

Definitions/Glossary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
G
Abbreviation These commonly used abbreviations may or may not be present in this report.
XX Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 680-149643-1
TestAmerica Savannah
Page 7 of 18 3/15/2018

Detection Summary
Client: EHS Support, LLC
TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: Outfall 001
Lab Sample ID: 680-149643-1
Analyte Result Qualifier
NONE
NONE Unit
Dil Fac D Method Prep Type
pH 7.2 HF
SU
1 SM 4500 H+ B Total/NA
Analyte Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
Chemical Oxygen Demand 31
10
mg/L
1 SM 5220D Total/NA
Analyte Result Qualifier
RL
RL Unit
Dil Fac D Method Prep Type
a
Total Suspended Solids 43
5.0
mg/L
—
1 SM 2540D Total/NA
Client Sample ID: Trip Blank
Lab Sample ID: 680-149643-2
[ No Detections.
F
F
This Detection Summary does not include radiochemical test results.
TestAmerica Savannah
Page 8 of 18
3/15/2018

Client Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: Outfall 001
Date Collected: 03/06/18 13:46
Date Received: 03/07/18 09:20
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Toluene
<1.0
Toluene
<1.0
Xylenes, Total
<2.0
Xylenes, Total
<2.0
Surrogate
%Recovery Qualifier
Toluene -0 (Surr)
98
Toluene -0 (Surr)
101
1,2-Dichloroethane-d4 (Surr)
104
1,2-Dichloroethane-d4 (Surr)
103
4-Bromofluorobenzene (Surr)
100
4-Bromofluorobenzene (Surr)
97
Dibromofluoromethane (Surr)
96
Dibromofluoromethane (Surr)
99
General Chemistry
70-130
Analyte
Result Qualifier
pH
7.2 HF
Analyte
Result Qualifier
HEM (Oil & Grease)
<2.6
Chemical Oxygen Demand
31
Analyte
Result Qualifier
Total Suspended Solids
43
Client Sample ID: Trip Blank
Date Collected: 03/06/18 13:46
Date Received: 03/07/18 09:20
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Toluene
<1.0
Xylenes, Total
<2.0
Surrogate
%Recovery Qualifier
Toluene -d8 (Surr)
99
1,2-Dichloroethane-d4 (Surr)
103
4-Bromofluorobenzene (Surr)
97
Dibromofluoromethane (Surr)
96
C
TestAmerica Job ID: 680-149643-1
NONE
NONE Unit
Lab Sample ID: 680-149643-1
Matrix: Water
RL
MDL Unit
D Prepared Analyzed Dil Fac C
1.0
ug/L
03/11/1816:37 1
1.0
ug/L
03/11/1817:00 1
2.0
ug/L
03/11/1816:37 1
2.0
ug/L
03/11/1817:00 1
Limits
1
Prepared Analyzed Dfl Fac
79-119
03/11118 13:56
03/11118 16:37 1
79-119
RL
03/11118 17:00 1
70-130
Analyzed
03/11118 16:37 1
70-130
mg/L
03/11118 17:00 1
71-121
1
03/11118 16:37 1
71-121
03/11118 17:00 1
77-129
03/11/18 16:37 1
77-129
03/11/18 17:00 1
NONE
NONE Unit
D Prepared
Analyzed
Dil Fac
ug/L
SU
1
03/14/18 17:14
1
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
2.6
mg/L
03/13/18 08:21
03/13/18 11:07
1
10
mg/L
03/11118 13:56
03/13/1815:26
1
RL
RL Unit
D Prepared
Analyzed
Dil Fac
5.0
mg/L
03/13/1813:15
1
Lab Sample ID: 680-149643-2
Matrix: Water
RL
MDL Unit
D Prepared Analyzed
oil Fac
1.0
ug/L
03/11/1813:56
1
2.0
ug/L
03/11/1813:56
1
Limits
Prepared Analyzed
Dil Fac
79-119
03/11118 13:56
1
70-130
03/11118 13:56
1
71-121
03/11118 13:56
1
77-129
03111118 13:56 _
1
Page 9 of 18
TestAmerica Savannah
3/15/2018

Surrogate Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: 624 - Volatile Organic Compounds (GC/MS)
Matrix: Water
TOL
DCA
Lab Sample ID
Client Sample ID
(79-119)
(70-130)
680-149643-1
Outfall 001
98
104
680-149643-1
Outfall 001
101
103
680-149643-2
Trip Blank
99
103
LCS 680-515382/3
Lab Control Sample
95
95
LCSD 680-515382/4
Lab Control Sample Dup
98
99
MB 680-515382/8
Method Blank
100
103
Surrogate Legend
TOL = Toluene -d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
C
TestAmerica Job ID: 680-149643-1
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM
(71-121) (77-129)
100 96
97 99
97 96
97 91
101 95
97 97
TestAmerica Savannah
Page 10 of 18 3/15/2018

QC Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: 624 - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-515382/8
Matrix: Water
Analysis Batch: 515382
MB MB
Analyte Result Qualifier
Toluene <1.0
Xylenes, Total <2.0
MB MB
Surrogate %Recovery Qualifier
Toluene -d8 (Surr) 100
1,2-Dichloroethane-d4 (Surr) 103
4-Bromofluorobenzene (Surr) 97
Dibromofluoromethane (Surr) 97
Lab Sample ID: LCS 680-515382/3
Matrix: Water
Analysis Batch: 515382
Analyte
Toluene
Xylenes, Total
RL
1.0
2.0
Limits
79-119
70-130
71-121
77-129
MDL Unit
ug/L
ug/L
Spike
LCS LCS
Limits
Added
Result Qualifier
Unit
20.0
19.2
ug/L
40.0
39.9
ug/L
Lab Sample ID: LCSD 680-515382/4
Matrix: Water
Analysis Batch: 515382
Analyte
Toluene
Xylenes, Total
Spike
LCS LCS
Limits
Surrogate
%Recovery Qualifier
Limits
Toluene -d8 (Surr)
95
79-119
1,2-Dichloroethane-d4 (Surr)
95
70-130
4-Bromofluorobenzene (Surr)
97
71-121
Dibromofluoromethane (Surr)
91
77-129
Lab Sample ID: LCSD 680-515382/4
Matrix: Water
Analysis Batch: 515382
Analyte
Toluene
Xylenes, Total
Spike
LCSD LCSD
Limits
Added
Result Qualifier
Unit
20.0
19.9
ug/L
40.0
41.7
ug/L
Surrogate
LCSD LCSD
%Recovery Qualifier
Limits
Toluene -d8 (Surr)
98
79-119
1,2-Dichloroethane-d4 (Surr)
99
70-130
4-Bromofluorobenzene (Surr)
101
71-121
Dibromofluoromethane (Surr)
95
77-129
Method: 1664A - HEM and SGT -HEM
C
TestAmerica Job ID: 680-149643-1
Client Sample ID: Method Blank
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
%Rec. RPD
D %Rec Limits RPD Limit
100 47-150 4 30
104 78-119 4 30
Lab Sample ID: MB 680-515578/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 515643 Prep Batch: 515578
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM (Oil & Grease) <5.0 5.0 mg/L 03/13/18 08:21 03/13/18 11:07 1
Page 11 of 18
TestAmerica Savannah
3/15/2018
Prep Type: Total/NA
D Prepared
Analyzed Dil Fac
03/11/18 13:10 1
03/11/18 13:10 1
Prepared
Analyzed Dil Fac
03/11/18 13:10 1
03/11/1813:10 1
03/11/18 13:10 1
03/11/18 13:10 1
Client Sample
ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
D %Rec
Limits
9647-150
100
78-119
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
%Rec. RPD
D %Rec Limits RPD Limit
100 47-150 4 30
104 78-119 4 30
Lab Sample ID: MB 680-515578/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 515643 Prep Batch: 515578
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM (Oil & Grease) <5.0 5.0 mg/L 03/13/18 08:21 03/13/18 11:07 1
Page 11 of 18
TestAmerica Savannah
3/15/2018

QC Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: 1664A - HEM and SGT -HEM (Continued)
Lab Sample ID: LCS 680-515578/2-A
Matrix: Water
Analysis Batch: 515643
Analyte
HEM (Oil & Grease)
Lab Sample ID: LCSD 680-515578/3-A
Matrix: Water
Analysis Batch: 515643
Analyte
HEM (Oil & Grease)
C
TestAmerica Job ID: 680-149643-1
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-515689/1
Client Sample ID: Lab Control Sample
C
Analysis Batch: 515689
mg/L
Prep Type: Total/NA
MB MB
Analyte
Result Qualifier
Prep Batch: 515578
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier
Unit D %Rec Limits
40.0
34.60
Added
mg/L 86 78-114
20.0
Lab Sample ID: LCSD 680-515689/3
Client Sample ID: Lab Control Sample Dup
120 80-120
Analysis Batch: 515689
Prep Type: Total/NA
Spike
Analyte
Added
Prep Batch: 515578
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit •
40.0
33.20
Result Qualifier
mg183 78.114 4 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-515689/1
Matrix: Water
C
Analysis Batch: 515689
mg/L
MB MB
Analyte
Result Qualifier
Total Suspended Solids
<1.0
Lab Sample ID: LCS 680-515689/2
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 515689
LCS
Spike
Analyte
Added
Total Suspended Solids
20.0
Lab Sample ID: LCSD 680-515689/3
Matrix: Water
120 80-120
Analysis Batch: 515689
Client Sample ID: Lab Control Sample Dup
Spike
Analyte
Added
Total Suspended Solids
20.0
Lab Sample ID: 680-149643-1 DU
Matrix: Water
Result
Analysis Batch: 515689
Unit
D %Rec Limits RPD Limit
Sample Sample
Analyte
Result Qualifier
Total Suspended Solids
43
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
RL Unit
D Prepared Analyzed Dil Fac
C
1.0
mg/L
03/13/1813:15 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS
LCS
%Rec.
Result
Qualifier
Unit
D %Rec Limits
24.0
mg/L
120 80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD
LCSD
%Rec. RPD
Result
Qualifier
Unit
D %Rec Limits RPD Limit
24.0
mg/L
120 --8-0--120 0 25
Client Sample ID: Outfall 001
Prep Type: Total/NA
DU
DU
RPD
Result
Qualifier
Unit
D RPD Limit
42.5
mg/L
1 5
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-515940/6 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 515940
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7.00 7.1 Su 101 63-158
Page 12 of 18
TestAmerica Savannah
3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: SM 5220D - COD
Lab Sample ID: MB 680-515724/3
Matrix: Water
Analysis Batch: 515724
Analyte
Chemical Oxygen Demand
Lab Sample ID: LCS 680-515724/4
Matrix: Water
Analysis Batch: 515724
Analyte
Chemical Oxygen Demand
QC Sample Results
MB MB
Result Qualifier RL MDL Unit
<10 10 mg/L
Spike LCS LCS
Added Result Qualifier Unit
50.0 51.3 mg/L
Page 13 of 18
C
TestAmerica Job ID: 680-149643-1
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
03/13/18 15:26 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LiRec.
D %Rec Limits •
103-9--0.110
TestAmerica Savannah
3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
GC/MS VOA
Analysis Batch: 515382
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
680-149643-1
Outfall 001
680-149643-2
Trip Blank
MB 680-515382/8
Method Blank
LCS 680-515382/3
Lab Control Sample
LCSD 680-515382/4
Lab Control Sample Dup
General Chemistry
Client Sample ID
Prep Batch: 515578
Matrix
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
MB 680-515578/1-A
Method Blank
LCS 680-515578/2-A
Lab Control Sample
LCSD 680-515578/3-A
Lab Control Sample Dup
Analysis Batch: 515643
Water
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
MB 680-515578/1-A
Method Blank
LCS 680-515578/2-A
Lab Control Sample
LCSD 680-515578/3-A
Lab Control Sample Dup
Analysis Batch: 515689
Total/NA
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
MB 680-515689/1
Method Blank
LCS 680-515689/2
Lab Control Sample
LCSD 680-515689/3
Lab Control Sample Dup
680-149643-1 DU
Outfall 001
Analysis Batch: 515724
SM 2540D
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
MB 680-515724/3
Method Blank
LCS 680-515724/4
Lab Control Sample
Analysis Batch: 515940
Total/NA
Lab Sample ID
Client Sample ID
680-149643-1
Outfall 001
LCS 680-515940/6
Lab Control Sample
QC Association Summary
C
TestAmerica Job ID: 680-149643-1
Prep Type
Matrix
Method
Total/NA
Water
624
Total/NA
Water
624
Total/NA
Water
624
Total/NA
Water
624
Total/NA
Water
624
Total/NA
Water
624
Prep Type
Matrix
Method
Total/NA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A
Prep Batch
Prep Batch m
Prep Type
Matrix
Method
Prep Batch
C
Total/NA
Water
1664A
515578
Total/NA
Water
1664A
515578
Total/NA
Water
1664A
515578
Total/NA
Water
1664A
515578
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
SM 2540D
Total/NA
Water
SM 2540D
Total/NA
Water
SM 2540D
Total/NA
Water
SM 2540D
Total/NA
Water
SM 2540D
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
SM 5220D
Total/NA
Water
SM 5220D
Total/NA
Water
SM 5220D
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
SM 4500 H+ B
Total/NA
Water
SM 4500 H+ B
Page 14 of 18
TestAmerica Savannah
3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: Outfall 001
Date Collected: 03/06/18 13:46
Date Received: 03/07/18 09:20
Batch Batch
Prep Type Type Method
Total/NA Analysis 624
Instrument ID: CMSC
Total/NA Analysis 624
Instrument ID: CMSC
Total/NA Prep 1664A
Total/NA Analysis 1664A
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D
Instrument ID: NOEQUIP
Total/NA Analysis SM 4500 H+ B
Instrument ID: MANTECH
Total/NA Analysis SM 5220D
Instrument ID: SPC7
Client Sample ID: Trip Blank
Date Collected: 03/06/18 13:46
Date Received: 03/07/18 09:20
Lab Chronicle
C
TestAmerica Job ID: 680-149643-1
Dil
Run Factor
Initial
Amount
Final
Amount
Batch
Number
Lab Sample ID: 680-149643-1
Matrix: Water
Prepared
or Analyzed Analyst Lab
1
5 mL
5 mL
515382
03/11/18 16:37 WAS TAIL SAV
1
5 mL
5 mL
515382
03/11/18 17:00 WAS TAIL SAV
965 mL
500 mL
515578
03/13/18 08:21 JAS TAIL SAV
1
515643
03/13/18 11:07 JAS TAIL SAV
1
200 mL
1000 mL
515689
03/13/18 13:15 JEC TAIL SAV
1
515940
03/14/18 17:14 JEC TAIL SAV
1
2 mL
2 mL
515724
03/13/18 15:26 JER TAIL SAV
Lab Sample ID: 680-149643-2
Matrix: Water
Batch Batch Dil Initial
Prep Type Type Method Run Factor Amount
Total/NA Analysis 624 1 5 mL
Instrument ID: CMSC
Laboratory References:
TAIL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 15 of 18
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst Lab
5 mL
515382
03/11/18 13:56
WAS TAIL SAV
TestAmerica Savannah
3/15/2018

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3/15/2018
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Page 16 of 18
3/15/2018

Login Sample Receipt Checklist
Client: EHS Support, LLC
Job Number: 680-149643-1
Login Number: 149643
List Number: 1
Creator: Anderson, Jordan K
Question
List Source: TestAmerica Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Savannah
Page 17 of 18 3/15/2018

Accreditation/Certification Summary
Client: EHS Support, LLC TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Laboratory: TestAmerica Savannah
The accreditations/certifications listed below are applicable to this report.
F -
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 269 12-31-18
7
m
TestAmerica Savannah
Page 18 of 18 3/15/2018