NCS000315_Nexeo Charlotte Semi-annual Sampling Results_Yr 8 Per 2_Jan 2018_20180108

neAveo�
solutions
January 8, 2018
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Re: Semi -Annual Storm Water Sampling Results for Year 8, Period 2
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 8, Period 2 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on December
5, 2017, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315). Per
the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001 during a
representative storm event that consisted of 0.32 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN -53 at Harding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented below in Table 1.
Table 1
Discharge Characteristic
Inspection Result
Color
Light (milky)
Odor
None observed
Clarity
Medium
Floating Solids
None observed
Suspended Solids
None observed
Foam
Minimal
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Storm water Pollution
No significant change
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
NexeoSolutions.com I Connect,

neAveo�
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value. The results of the storm water sample analyses along with their corresponding benchmark values
as listed in the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
22 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<4.6 mg/L
30 mg/L
Chemical Oxygen Demand
17 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
7
6-9
Total Rainfall
0.32 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 9, Period 1) between January 1 and June 30, 2018, and will submit
the results per the requirements of the permit. Should you have any questions or require additional information,
please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions, LLC
NexeoSolutions.com I Connect,

ENCLOSUREI LABORATORY RESULTS

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-146513-1
Client Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
roi
EHS Support, LLC
100 Georgia Ave
Daphne, Alabama 36526
Attn: Amy Bauer
Authorized for release by. -
1211512017
y.12/15/2017 5:12:18 PM
Jerry Lanier, Project Manager 1
[phone] e.3410
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Table of Contents
TestAmerica Job ID: 680-146513-1
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ..........................................
3 L
Sample Summary .........................................
5
Method Summary ...........................................
6
Definitions/Glossary.......................................
7
Detection Summary ........................................
8
Client Sample Results ......................................
9
Surrogate Summary .......................................
10
QC Sample Results ........................................
11
QC Association Summary ...................................
14
Lab Chronicle ............................................
15
Chain of Custody ..........................................
16
Receipt Checklists .........................................
17
Certification Summary ......................................
18
Page 2 of 18
TestAmerica Savannah
12/15/2017

Case Narrative C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-146513-1
Laboratory: TestAmerica Savannah
Narrative L
CASE NARRATIVE
Client: EHS Support, LLC
Project: Nexeo - Charlotte, N.C. (Outfall 001) C
Report Number: 680-146513-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT I
The samples were received on 12/07/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.8 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples OUTFALL 001 (680-146513-1) and TRIP BLANK (680-146513-2) were analyzed for Volatile Organic Compounds (GC -MS) in
accordance with EPA Method 624. The samples were analyzed on 12/13/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
OIL AND GREASE AND TPH
Sample OUTFALL 001 (680-146513-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples
were prepared and analyzed on 12/12/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample OUTFALL 001 (680-146513-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were
analyzed on 12/11/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample OUTFALL 001 (680-146513-1) was analyzed for chemical oxygen demand in accordance with SM 5220D. The samples were
analyzed on 12/15/2017.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample OUTFALL 001 (680-146513-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed
on 12/13/2017.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
TestAmerica Savannah
Page 3 of 18 12/15/2017

Case Narrative C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-146513-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
TestAmerica Savannah
Page 4 of 18 12/15/2017

Sample Summary
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Lab Sample ID Client Sample ID Matrix Collected Received
680-146513-1 OUTFALL 001 Water 12/05/17 22:20 12/07/17 09:15
680-146513-2 TRIP BLANK Water 12/05/17 00:00 12/07/17 09:15
TestAmerica Savannah
Page 5 of 18 12/15/2017

Method Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
TestAmerica Job ID: 680-146513-1
Method
Method Description
Protocol
Laboratory
624
Volatile Organic Compounds (GC/MS)
40CFR136A
TAL SAV
1664A
HEM and SGT -HEM
1664A
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B
pH
SM
TAL SAV
SM 5220D
COD
SM
TAL SAV
Protocol References:
1664A = EPA -821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 6 of 18 12/15/2017

Definitions/Glossary
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Savannah
Page 7 of 18 12/15/2017

Detection Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
TestAmerica Job ID: 680-146513-1
Client Sample ID: OUTFALL 001
Lab Sample ID: 680-146513-1
Analyte Result
Qualifier
NONE
NONE Unit
Dil Fac D Method Prep Type
pH 7.0
HF
SU
1 SM 4500 H+ B Total/NA
Analyte Result
Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
Chemical Oxygen Demand 17
10
mg/L
1 SM 5220D Total/NA
Analyte Result
Qualifier
RL
RL Unit
Dil Fac D Method Prep Type
a
Total Suspended Solids 22
2.2
mg/L
—
1 SM 2540D Total/NA
Client Sample ID: TRIP BLANK
Lab Sample ID: 680-146513-2
LNo Detections
This Detection Summary does not include radiochemical test results.
Page 8 of 18
TestAmerica Savannah
12/15/2017

Client Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
TestAmerica Job ID: 680-146513-1
Client Sample ID: OUTFALL 001 Lab Sample ID: 680-146513-1
Date Collected: 12/05/17 22:20 Matrix: Water
Date Received: 12/07/17 09:15
Method: 624 - Volatile Organic Compounds (GC/MS
Analyte
Result
Qualifier
Toluene
<1.0
ug/L
Xylenes, Total
<2.0
2.0
Surrogate
%Recovery
Qualifier
Toluene -d8 (Surr)
100
Prepared Analyzed
1,2-Dichloroethane-d4 (Surr)
113
12/12/17 11:18
4-Bromofluorobenzene (Surr)
105
70-130
Dibromofluoromethane (Surr)
106
1
General Chemistry
RL Unit
12/13/17 20:52
Analyte
Result
Qualifier
pH
7.0
HF
Analyte
Result
Qualifier
HEM (Oil & Grease)
<4.6
Chemical Oxygen Demand
17
Analyte
Result
Qualifier
Total Suspended Solids
22
Client Sample ID: TRIP BLANK
Date Collected: 12/05/17 00:00
Date Received: 12/07/17 09:15
RL
MDL Unit
D Prepared Analyzed
Dil Fac
C
1.0
ug/L
12/13/17 20:52
1
2.0
ug/L
12/13/17 20:52
1
Limits
105
Prepared Analyzed
Dil Fac
79-119
12/12/17 11:18
12/13/17 20:52
1
70-130
12/13/17 17:34
12/13/17 20:52
1
71-121
RL Unit
12/13/17 20:52
1
77-129
2.2
12/13/17 20:52
1
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
Toluene
<1.0
Xylenes, Total
<2.0
Surrogate
%Recovery Qualifier
Toluene -d8 (Surr)
100
1,2-Dichloroethane-d4 (Surr)
111
4-Bromofluorobenzene (Surr)
105
Dibromofluoromethane (Surr)
105
NONE
NONE Unit
D Prepared
Analyzed
Dil Fac
ug/L
SU
1
12/13/17 07:29
1
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
4.6
mg/L
12/12/17 0800
12/12/17 11:18
1
10
mg/L
12/13/17 17:34
12/15/1712:01
1
RL
RL Unit
D Prepared
Analyzed
Dil Fac
2.2
mg/L
12/11/1713:51
1
Lab Sample ID: 680-146513-2
Matrix: Water
RL
MDL Unit
D Prepared Analyzed
Dil Fac
1.0
ug/L
12/13/1717:34
1
2.0
ug/L
12/13/1717:34
1
Limits
Prepared Analyzed
Dil Fac
79-119
12/13/17 17:34
1
70-130
12/13/17 17:34
1
71-121
12/13/17 17:34
1
77-129
12/13/17 17:34
1
Page 9 of 18
TestAmerica Savannah
12/15/2017

Surrogate Summary C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: 624 - Volatile Organic Compounds (GC/MS)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TOL
DCA
BFB
DBFM
Lab Sample ID
Client Sample ID
(79-119)
(70-130)
(71-121)
(77-129)
680-146513-1
OUTFALL 001
100
113
105
106
680-146513-2
TRIP BLANK
100
111
105
105
LCS 680-506252/3
Lab Control Sample
89
103
95
97
LCSD 680-506252/6
Lab Control Sample Dup
90
103
95
96
MB 680-506252/9
Method Blank
101
112
106
105
Surrogate Legend
TOL = Toluene -d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TestAmerica Savannah
Page 10 of 18 12/15/2017
0

QC Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Spike
TestAmerica Job ID: 680-146513-1
Method: 624 - Volatile Organic Compounds (GC/MS)
%Rec.
Lab Sample ID: MB 680-506252/9
Analyte
Client Sample ID: Method Blank
Matrix: Water
Unit
Prep Type: Total/NA
Analysis Batch: 506252
Toluene
20.0
MB MB
ug/L
100 47-150
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Toluene <1.0
1.0
ug/L 12/13/1716:50 1
Xylenes, Total <2.0
2.0
ug/L 12/13/17 16:50 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Toluene -d8 (Surr) 101
79-119
12/13/17 16:50 1
1,2-Dichloroethane-d4 (Surr) 112
70-130
12/13/17 16:50 1
4-Bromofluorobenzene (Surr) 106
71-121
12/13/17 16:50 1
Dibromofluoromethane (Surr) 105
77-129
12/13/17 16:50 1
Lab Sample ID: LCS 680-506252/3
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 506252
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Toluene
20.0
19.6 ug/L 98 47-150
Xylenes, Total
40.0
38.9 ug/L 97 78-119
LCS LCS
Surrogate %Recovery Qualifier
Toluene -d8 (Surr) 89
1,2-Dichloroethane-d4 (Surr) 103
4-Bromofluorobenzene (Surr) 95
Dibromofluoromethane (Surr) 97
Lab Sample ID: LCSD 680-506252/6
Matrix: Water
Analysis Batch: 506252
Limits
79-119
70-130
71-121
77-129
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene -d8 (Surr) 90 79-119
1,2-Dichloroethane-d4 (Surr) 103 70-130
4-Bromofluorobenzene (Surr) 95 71-121
Dibromofluoromethane (Surr) 96 77-129
Method: 1664A - HEM and SGT -HEM
Lab Sample ID: MB 680-506010/1-A
Matrix: Water
Analysis Batch: 506059
MB MB
Analyte Result Qualifier RL
HEM (Oil & Grease) <5.0 5.0
Page 11 of 18
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 506010
MDL Unit D Prepared Analyzed Dil Fac
mg/L 12/12/17 08:20 12/12/17 11:18 1
TestAmerica Savannah
12/15/2017
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
RPD Limit
Toluene
20.0
20.1
ug/L
100 47-150
2 30
Xylenes, Total
40.0
39.3
ug/L
98 78-119
1 30
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene -d8 (Surr) 90 79-119
1,2-Dichloroethane-d4 (Surr) 103 70-130
4-Bromofluorobenzene (Surr) 95 71-121
Dibromofluoromethane (Surr) 96 77-129
Method: 1664A - HEM and SGT -HEM
Lab Sample ID: MB 680-506010/1-A
Matrix: Water
Analysis Batch: 506059
MB MB
Analyte Result Qualifier RL
HEM (Oil & Grease) <5.0 5.0
Page 11 of 18
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 506010
MDL Unit D Prepared Analyzed Dil Fac
mg/L 12/12/17 08:20 12/12/17 11:18 1
TestAmerica Savannah
12/15/2017

QC Sample Results C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: 1664A - HEM and SGT -HEM (Continued)
Lab Sample ID: LCS 680-506010/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 506059 Prep Batch: 506010
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
HEM (Oil & Grease) 40.0 38.80 mg/L 97 78-114
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-505933/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 505933 0
TestAmerica Savannah
Page 12 of 18 12/15/2017
MB MB
Analyte
Result Qualifier
RL RL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids
<1.0
1.0 mg/L 12/11/17 13:51 1
Lab Sample ID: LCS 680-505933/2
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 505933
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Total Suspended Solids
20.0
20.5 mg/L 103 80-120
Lab Sample ID: LCSD 680-505933/3
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 505933
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Total Suspended Solids
20.0
21.5 mg/L 108 80-120 5 25
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-506236/7
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 506236
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
pH
7.00
7.1 SU 101 63 - 158
Method: SM 5220D - COD
[Lab Sample ID: MB 680-506630/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 506630
MB MB
Analyte
Result Qualifier
RL MDL Unit D Prepared Analyzed Dil Fac
Chemical Oxygen Demand
<10
10 mg/L 12/15/17 12:01 1
TestAmerica Savannah
Page 12 of 18 12/15/2017

QC Sample Results C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method: SM 5220D - COD (Continued)
Lab Sample ID: LCS 680-506630/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 506630
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Chemical Oxygen Demand 50.0 48.1 mg/L 96 -90-110
0
TestAmerica Savannah
Page 13 of 18 12/15/2017

QC Association Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
GC/MS VOA
Analysis Batch: 506252
TestAmerica Job ID: 680-146513-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-146513-1
OUTFALL 001
Total/NA
Water
624
680-146513-2
TRIP BLANK
Total/NA
Water
624
MB 680-506252/9
Method Blank
Total/NA
Water
624
LCS 680-506252/3
Lab Control Sample
Total/NA
Water
624
LCSD 680-506252/6
Lab Control Sample Dup
Total/NA
Water
624
General Chemistry
Analysis Batch: 505933
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-146513-1
OUTFALL 001
Total/NA
Water
SM 2540D
MB 680-505933/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-505933/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-505933/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Prep Batch: 506010
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-146513-1
OUTFALL 001
Total/NA
Water
1664A
MB 680-506010/1-A
Method Blank
Total/NA
Water
1664A
LCS 680-506010/2-A
Lab Control Sample
Total/NA
Water
1664A
Analysis Batch: 506059
Prep Batch
Prep Batch
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-146513-1
OUTFALL 001
Total/NA
Water
1664A
506010
MB 680-506010/1-A
Method Blank
Total/NA
Water
1664A
506010
LCS 680-506010/2-A
Lab Control Sample
Total/NA
Water
1664A
506010
Analysis Batch: 506236
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-146513-1
OUTFALL 001
Total/NA
Water
SM 4500 H+ B
LCS 680-506236/7
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
Analysis Batch: 506630
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-146513-1
OUTFALL 001
Total/NA
Water
SM 5220D
MB 680-506630/3
Method Blank
Total/NA
Water
SM 5220D
LCS 680-506630/4
Lab Control Sample
Total/NA
Water
SM 5220D
TestAmerica Savannah
Page 14 of 18 12/15/2017

Lab Chronicle
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: OUTFALL 001
Date Collected: 12/05/17 22:20
Date Received: 12/07/17 09:15
C
TestAmerica Job ID: 680-146513-1
Lab Sample ID: 680-146513-1
Matrix: Water
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D 1 445 mL 1000 mL 505933 12/11/17 13:51 JEC TAL SAV
Instrument ID: NOEQUIP F
Total/NA Analysis SM 4500 H+ B 1 506236 12/13/17 07:29 JEC TAL SAV
Instrument ID: MANTECH
Total/NA Analysis SM 5220D 1 2 mL 2 mL 506630 12/15/17 12:01 JER TAL SAV
Instrument ID: SPC7
Client Sample ID: TRIP BLANK
Date Collected: 12/05/17 00:00
Date Received: 12/07/17 09:15
Lab Sample ID: 680-146513-2
Matrix: Water
Batch
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
12/13/17 17:34 JLK TAL SAV
Total/NA
Analysis
624
1
5 mL
5 mL
506252
12/13/17 20:52
JLK
TAL SAV
Instrument ID: CMSB
Total/NA
Prep
1664A
540 mL
500 mL
506010
12/12/17 08:20
JAS
TAL SAV
Total/NA
Analysis
1664A
1
506059
12/12/17 11:18
JAS
TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D 1 445 mL 1000 mL 505933 12/11/17 13:51 JEC TAL SAV
Instrument ID: NOEQUIP F
Total/NA Analysis SM 4500 H+ B 1 506236 12/13/17 07:29 JEC TAL SAV
Instrument ID: MANTECH
Total/NA Analysis SM 5220D 1 2 mL 2 mL 506630 12/15/17 12:01 JER TAL SAV
Instrument ID: SPC7
Client Sample ID: TRIP BLANK
Date Collected: 12/05/17 00:00
Date Received: 12/07/17 09:15
Lab Sample ID: 680-146513-2
Matrix: Water
Batch
Batch
Dil
Initial
Final
Batch
Prepared io
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis
624
1
5 mL
5 mL
506252
12/13/17 17:34 JLK TAL SAV
Instrument ID: CMSB
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 15 of 18
TestAmerica Savannah
12/15/2017

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Page 16 of 18
12/15/2017

Login Sample Receipt Checklist
Client: EHS Support, LLC
Job Number: 680-146513-1
Login Number: 146513
List Number: 1
Creator: Edwards, Jessica R
Question
List Source: TestAmerica Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Savannah
Page 17 of 18 12/15/2017

Accreditation/Certification Summary C
Client: EHS Support, LLC TestAmerica Job ID: 680-146513-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Laboratory: TestAmerica Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 269 12-31-17 L
7
m
TestAmerica Savannah
Page 18 of 18 12/15/2017