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HomeMy WebLinkAboutNC0005312_Application_20180619 ROY COOPER Governor I IICH EL S. REGAN Secretar Water Resources LINDA CULPEPPER ENVIRONMENTAL OUAl iT V Interim Director June 19, 2018 Scott Taylor Duvaltex US Inc 304 E. Main Street Elkin, NC 28621 Subject: Permit Renewal Application No. NC0005312 Duvaltex RLAP Surry County Dear Applicant: The Water Quality Permitting Section acknowledges the June 15, 2018 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. Sincerely, Ct2i8V5)E.A__ Wren Thedford Administrative Assistant Water Quality Permitting Section ec: WQPS Laserfiche File w/application (WSRO) State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh,North Carolina 27699-1617 919-807-6300 hart „1%. hickman SMARTER ENVIRONMENTAL. SOLUTIONS Via (Email and USPS] June 11,2018 Mr. Joe Corporon NCDEQ-Division of Water Resources RECEIVEDIDENRlDWR Water Quality Permitting Section-NPDES JUN 15 2018 1617 Mail Service Center Raleigh,NC 27699-1617 Water Resources Permitting Section Re: Permit Renewal Application NPDES Permit No.NC0005312 Mr. Corporon, On behalf of Duvaltex (US), Inc. (Duvaltex), Hart and Hickman, PC (H&H) is pleased to provide (1) Original and (1)copy of an application for renewal of NPDES Wastewater Permit No.NC0005312. NPDES permit NC0005312 was reissued on February 5,2018 to reflect the transfer of ownership to Duvaltex(US), Inc. from TrueElkin, Inc. The 2012 permit application describes the downsizing of the facility in 2009, which resulted in the elimination of multiple process operations. In addition,the 2008 application included effluent information from a neighboring manufacturing facility not owned or operated by True Elkin, Inc/Duvaltex(US), Inc. This facility was known as Westpoint Stevens (WPS). WPS remains vacant at the time of writing this letter. This permit application includes completed EPA Forms 3510-1 and 3510-2c as well as all required attachments. The data is supported by permit required periodic test results as well as the 2017 priority pollutant analysis. 2923 South Tryon Street,Suite 100 3921 Sunset Ridge Rd.Suite 301 Charlotte,NC 28203 Raleigh,NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main I _ Mr. Joe Corporon June 11,2018 Should you have any questions or need any additional information,please feel free to call me at your convenience. Sincerely, Hart&Hickman,PC xA, Greg Kanellis Senior Project Engineer Enclosures: (2)Permit Renewal Applications Cc: Glen Gary, Wastewater Treatment Plant Manager ORC, Duvaltex (US), Inc. Scott Taylor, Environmental Coordinator, Duvaltex(US),Inc. 11 hart hickman S'\AAA-Master Protects\DuvalTex(VCP-002)\2018 Submittal\01 Application Cover Letter and Divider Sheets-H&H docx SMARTER ENVIRONMENTAL SOLUTIONS NPDES WASTEWATER APPLICATION PERMIT RENEWAL (PERMIT NO. NC0005312) Duvaltex (US), Inc. Suny County, North Carolina June 2018 Submitted to: Joe Corporon NCDEQ-Division of Water Resources Water Quality Permitting Section-NPDES 610 East Center Ave., Suite 301 Mooresville,NC 28115 Prepared by: Hart&Hickman,P.C. 3921 Sunset Ridge Road, Suite 301 Raleigh,NC 27607 (919)847-4241 Prepared for: Scott Taylor Environmental Coordinator Duvaltex(US),Inc. P.O.Box 179 Guilford,ME 04443 (207)876-1418 TABLE OF CONTENTS Section 1 Form 1 Section 2 Form 2C APPENDICIES Appendix A Production Data Appendix B Whole Effluent Toxicity Tests for 2017 Appendix C .Priority Pollutant Analysis for 2017 Appendix D Discharge Monitoring Reports for 2017 FIGURES Section Figure 1-1 (Facility Location) 1 Figure 1-2 (Facility Drawing) ..1 Figure 1-3 (Production Flow Schematic) 2 Figure 1-4 (Water Use Schematic) 2 Figure 1-5 (Wastewater Treatment Plant Schematic) .2 SECTION 1 EPA Form 3510-1 Figure 1-1 Facility Location Figure 1-2 Facility Site Plan Please print or type in the unshaded areas only (fill-in areas are spaced for elite type,i.e., 12 characters/inch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92 FORM U.S.ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER , GENERAL INFORMATION rA c 1 Rr;'EPA D Consolidated Permits Program F NC005312 GENERAL (Read the"General Instructions"before starting.) 1 2 13 14 15 LABEL ITEMS GENERAL INSTRUCTIONS If a preprinted label has been provided, I. EPA I.D. NUMBER affix it in the designated space.Review the information carefully; if any of it is incorrect cross through it and enter the III. FACILITY NAME correct data in the appropriate fill-in area below.Also,if any of the preprinted data is absent (the area to the left of the label V. FACILITY PLEASE PLACE LABEL IN THIS SPACE space lists the information that should appear), please provide it in the proper fill- MAILING LIST in area(s) below. If the label is complete and correct you need not complete Items 1, Ill,V,andVI(except VI-B which must be VI. FACILITY completed regardless). Complete all items if no label has been proved. Refer to the instructions for detailed item descriptions LOCATION and for the legal authorization under which this data is collected. II. POLLUTANT CHARACTERISTICS INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer"yes"to any questions,you must submit this form and the supplemental from listed in the parenthesis following the question.Mark"X"in the box in the third column if the supplemental form is attached. If you answer"no"to each question,you need not submit any of these forms. You may answer"no"if your activity is excluded from permit requirements;see Section C of the instructions.See also,Section D of the instructions for definitions of bold-faced terms. SPECIFIC QUESTIONS MARK"X" MARK SPECIFIC QUESTIONS MARK11X1FORM YES NO YES NO ATTACHED ATTACHED A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or which results in a discharge to waters of the ❑ ® ❑ proposed) include a concentrated animal ❑ ® ❑ U.S.?(FORM 2A) feeding operation or aquatic animal production facility which results in a discharge 16 17 18 to waters of the U.S.?(FORM 28) 19 20 21 C. Is this facility which currently results in ® ❑ ® D. Is this proposal facility(other than those described ❑ ® ❑ discharges to waters of the U.S. other than in A or B above)which will result in a discharge those described in A or B above?(FORM 2C) 22 23 24 to waters of the U.S.?(FORM 2D) 25 26 27 E. Does or will this facility treat,store,or dispose of F. Do you or will you inject at this facility industrial or hazardous wastes?(FORM 3) ® ❑ ❑ municipal effluent below the lowermost stratum ❑ ® ❑ containing, within one quarter mile of the well bore, underground sources of drinking water'? 28 29 30 (FORM 4) 31 32 33 G. Do you or will you inject at this facility any H. Do you or will you inject at this facility fluids for produced water other fluids which are brought to special processes such as mining of sulfer by the the surface in connection with conventional oil or ❑ ® ❑ Frasch process,solution mining of minerals,in ❑ ® ❑ natural gas production, inject fluids used for situ combustion of fossil fuel,or recovery of enhanced recovery of oil or natural gas,or inject geothermal energy?(FORM 4) fluids for storage of liquid hydrocarbons? _ (FORM 4) 34 35 36 37 38 39 I. Is this facility a proposed stationary source J. Is this facility a proposed stationary source which is one of the 28 industrial categories listed which is NOT one of the 28 industrial categories in the instructions and which will potentially emit ❑ Z CI Z ❑ CI in the instructions and which will potentially 100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant under the Clean Air Act and may affect or be _ regulated under the Clean Air Act and may affect located in an attainment area? FORM 5 40 41 42 or be located in an attainment are? FORM 5 43 44 45 III. NAME OF FACILITY c SKIP Duvaltex (US), Inc. 1 15 16-29 30 69 IV. FACILITY CONTACT A.NAME&TITLE(last,first, &title) B.PHONE(area code&no.) 2 Scott Taylor, Environmental Coordinator 207 876 1418 15 16 45 46 48 49 51 52 55 V. FACILITY MAILING ADDRESS IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIM A.STREET OR P.O.BOX c P.O. Box 530 3 15 16 45 B.CITY OR TOWN C.STATE D.ZIP CODE c Elkin NC 28621 4 15 16 40 41 42 47 51 VI. FACILITY LOCATION A.STREET, ROUTE NO.OR OTHER SPECIFIC IDENTIFIER C 304 East Main Street 5 15 16 45 B.COUNTY NAME Surry 46 70 C.CITY OR TOWN - D.STATE E.ZIP CODE F.COUNTY CODE C Elkin NC 28621 086 6 15 16 40 41 42 47 51 52 54 EPA FORM 3510-1(8-90) CONTINUED ON REVERSE 1 CONTINUED FROM THE FRONT VII. SIC CODES 4-di.it, in order of.riorit A.FIRST B.SECOND C 2262 I (specify) 7 2824 (specify) 7 Finishers of Broadwoven Fabrics of 7 Manmade Organic Fibers,Except Cellulosic 15 16 17 Manmade Fiber and Silk 15 16 19 C.THIRD D.FOURTH C 2221 (specify) 7 (specify) 7 _ Manmade Fiber and Silk 7 15 16 17 15 16 19 VIII. OPERATOR INFORMATION A.NAME B.Is the name listed in Item c Duvaltex (US), Inc. VIII-A also the owner? s 18 19 55 ❑YES ®NO C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other,"specify.) D.PHONE prea code&no.) F=FEDERAL M=PUBLIC(other than federal or state) p (specify) C 336 I 835 0244 S=STATE 0=OTHER(specify) A JI P=PRIVATE 56 15 16 18 19 21 22 25 E.STREET OR PO BOX P.O. Box 530 26 55 F.CITY OR TOWN G.STATE H.ZIP CODE IX. INDIAN LAND -_ Elkin NC 28621facility C Is the located on Indian lands? B ❑YES ® NO 15 16 40 42 42 47 51 X. EXISTING ENVIRONMENTAL PERMITS A.NPDES(Discharges to Surface Water) D.PSD(Air Emissions from Proposed Sources) 9 N ' NC0005312 9 P 8 01315R29 15 16 17 18 30 15 16 17 18 30 B.UIC(Underground Injection of Fluids E.OTHER(specify) (Specify) s T ' N/A s T 6 W00013982 Land Application Permit 15 16 17 18 30 15 16 17 18 30 C.RCRA(Hazardous Wastes) E.OTHER(specif_y) (Specify) 9 ni71 1.6 NCD003219573 s T 8 NCG170000 Stormwater Discharge 15 16 17 18 30 15 16 17 18 30 Permit XI. MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs, rivers and other surface water bodies in the ma. area. See instructions for .recise re.uirements. XII. NATURE OF BUSINESS •rovide a brief descri.tion Duvaltex(US), Inc. leases and operates a textile manufacturing facility and wastewater treatment plant in Elkin, NC.The facility primarily finishes woven upholstery fabric from primarily manmade and some natural fibers. Operations include fabric finishing, yarn extrusion and limited weaving for sample fabrics. The WWTP treats process wastewater from the Duvaltex(US), Inc. The WWTP formerly treated waste from the adjacent former Westpoint Stevens (WPS)facility.The WPS facility is not owned by Duvaltex (US), Inc. and is currently vacant. XIII. CERTIFICATION (see instructions) I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fine..and imprisonment. A.NAME&OFFICIAL TITLE(type or print) B.S ATURE C.DATE SIGNED 2 s-c ,-, IAytr/y - E.Nvi1. C:.'.L1°L , or. —*, L.7)) C,6—C. !y —,,2C.'fi COMMENTS FOR OFFICIAL USE ONLY c C 15 16 55 EPA FORM 3510-1(8-90) .7.. •Elkin •' • • .• ' SITE •• • • ,4,- .' 1 ;•,,,,,,,,,_� 1 A t ♦ v ":1...,:;,:.'•• • .,, k, . • , • ,. .1. :rt 9 1. . ,- a' by '3I . :1 235 -1 1• / j - 1• •rh•t ' �'- '''''� 1 r"0.+' ' .,,,t,f.„ ire r 'f • t'. t ' ,,,; wages "' 4 ,• t4`$ i•,• ` I' ' ,. ! * ,'sal �,",< i . ii. t0 � '' Disposed- .,.-'' • "t * ` s - % " Mf '' ter- ' } •�'` J UTICS V 1 Il E' ° ;ma � agi -.Sta , T . ,----- g9 11.-1� --7.. �•,^€4 __ ; #1 �— • ` 1 * •� _;....._ ^ � / .•• _}mac._,-�•• '�.1� _•k i i i+� • a . "s I • di Y • iV,4. f ▪ %�. i X51,• s,+.. •��•. "may , ! i(t`a t# n 1 —row • pis,•,,,, �� Foe ` .ih•1 •''''' '''•' .,. ^i 1 —" • } '.� . _ _ - _ - __A — , - om --.x,.'.�.r y ..7-.)6,-s ., t. �,�. t.,-_„_-ti •. . • .rig°#• _�.''1 }t H1ch#�1 : r�_� •1• .11 / soh 4 1 .:-. •• `• -t2, g'1 ,r/ .{, ' i• Lt '1-, l • • . • ,,r /ft!" APPROXIMATE TITLE / 0 2000 4000 SITE LOCATION MAP NIIIIIIIIP► SC IN FEET PROJECT DUVALTEX(US), INC.. —ELKIN FACILITY 304 EAST MAIN STREET ELKIN, NORTH CAROLINA 111 U.S.G.S. QUADRANGLE MAP hart hickman 2923 South Tryon Street-Suite100 Charlotte,North Carolina 28203 704586-0007(p)704586-03730 ELKIN SOUTH, NORTH CAROLINA, 1996 SMARTER e-^i Sr#4r,€'sndT'Or-s8iut SOLUTIONS DATE: 5-16-18 REVISION NO: 0 QUADRANGLE 7.5 MINUTE SERIES(TOPOGRAPHIC) JOB NO: VCP-002 FIGURE 1-1 s i,;liwsfi ? s 1 - -- LEGEND 1 i 1. _ I �� , I / 5 SITE PROPERTY BOUNDARY --,., ,,, ST POINT STEVENS cam,, FORMER WE /� �\ _. ) —� aq s .. BUILDINGS /� ``� ) RESERVOIRS a �••_...��� ., DUVALTEX(US),INC BUILDINGS I f hWAR€HOUSE ___,,,,i,,,\ ,,/,, �t • ,� ' n ^w"' SURFACE WATER BODIES,PROCESS J / WATER AND WASTEWATER / r CITY STAND P \ . $5 / / \� ® HAZARDOUS WASTE STORAGE AREA / ? #;, ; { © PAINTS AND SOLVENTS HAZARDOUS WASTE STORAGE AREA r i f •s ,,v _ . �' UNIVERSAL WASTE STORAGE AREA p^IN t1 ' , (D 2 ERS) - , ' i . § , EXTRUSION' g r rFINISHING PLANT 1' IR7I I"IiiI I. �„,',,,r -,\,, ,,,,,/,<,... ,.': \kc_..\,—I i. - 'r: ill. ,,'' I -1 _1,„...„-----_,A -—- ., •III:r .\ Y a <:a i w .fi.,y=,u'_. 4P:' Q ”II*II .�,„ �. X anne ... ;s v..,..x -14 .. t x, -FRE (N.C. NIGNw � �` � AERATION DRYING BEDS �F x .�-.. �n ... . ... A1N ST N RAIL ..BASIN R ,� ,,, 0,.. _< . _•... ,. EAST M SoUTHE .... .,. ......... „.., " ,..„ , MARK �- 3 ��� 4 ..EAST c'v r. t.,,,, _ ,,: I t EQUALIZATION .. �0 _ �. „_ dk /�RAW WATER BASIN .►1F_ ,. APPROXIMATE ' / RESERVOIR t 0 350 700 m � SCALE IN FEET o C N i�` -- -' SITE MAP DUVALTEX (US). INC. ELKIN FACILITY _ 304 EAST MAIN STREET : ELKIN, NORTH CAROLINA S --.—_` y • 2923 South T on Street-Suite 100 hart (C man ry �.,..;' r •"^,„..Sa °_ � '�',„ Charlotte,North Carolina 28203 /i -}j 704-586-0007(p)704586-0373(f) :11 s,.. ,;, >. ..,... ,., :��a a ,a .. ,r, ",'F t r ,rye+ .. 1 / ” -- I 1 �. � � • �� ��� � �� �_... SMARTER"1"dIRONMEfYIAI SOLUTIONS Lxense#C 1269/#C-245(,���I����; �TM '' • t • DATE:5-29-18 REVISION NO. 0 j " �" '' �;t, ; '15 �,, "` JOB NO VCP-002 FIGURE NO. 1-2 i SECTION 2 EPA Form 3510-2c Figure 1-3 Production Flow Schematic Figure 1-4 Water Use Schematic Figure 1-5 Wastewater Treatment Plant Schematic Disclaimer This is an updated PDF document that allows you to type your information directly into the form. This form is the most updated form currently available. Note: You cannot save what you have typed unless you have the full Adobe Professional version. Instructions: 1. Type in your information 2. Print the completed form 3. Sign and date the printed copy 4. Mail the form to the address stated in the instructions United States Office of EPA Form 3510-2C Environmental Protection Enforcement Revised August 1990 Agency Washington,DC 20460 Previous editions are obsolete Permits Division EPA Application Form 2C — Wastewater Discharge Information Consolidated Permits Program This form must be completed by all persons applying for an EPA permit to discharge wastewater (existing manufacturing, commercial, mining, and silvicultural operations). t� Printed on recycled paper r Paperwork Reduction Act Notice The public reporting burden for this collection of information is estimated to average 33 hours per response. This estimate includes time for reviewing instructions, searching existing data sources, gathering and maintaining the needed data, and completing and reviewing the collecttion of information. Send comments regarding the burden estimate or any other aspect of this collection of information to the Chief, Information Policy Branch (PM-223), US Environmental Protection Agency, 1200 Pennsylvania Avenue, NW, Washington, DC 20460, and to the Office of Information and Regulatory Affairs, Office of Management and Budget, Washington, DC 20503, marked Attention: Desk Officer for EPA. t, Printed on recycled paper INSTRUCTIONS—FORM 2c Application for Permit to Discharge Wastewater EXISTING MANUFACTURING,COMMERCIAL, MINING.AND SILVICULTURAL OPERATIONS This form must be completed by all applicants who check "yes" to "Maximum Daily" columns (columns 4-a-2 and 4-b-2). Report the item II-C in Form 1. average of all daily values measured during days when discharge occurred within the last year in the "Long Term Average" columns Public Availability of Submitted Information. (columns 4-a-1 and 4-b-1). Your application will not be considered complete unless you answer every question on this form and on Form 1. If an item does not apply Item III-A to you, enter "NA" (for not applicable) to show that you considered All effluent guidelines promulgated by EPA appear in the Federal the question. Register and are published annually in 40 CFR Subchapter N. A guideline applies to you if you have any operations contributing You may not claim as confidential any information required by this process wastewater in any subcategory covered by a BPT, BCT, or form or Form 1,whether the information is reported on the forms or BAT guideline. If you are unsure whether you are covered by a in an attachment. This information will be made available to the promulgated effluent guideline, check with your EPA Regional office public upon request. (Table 1 in the Form 1 instructions). You must check "yes" if an Any information you submit to EPA which goes beyond that required applicable effluent guideline has been promulgated, even if the by this form or Form 1 you may claim as confidential, but claims for guideline limitations are being contested in court. If you believe that a information which is effluent data will be denied. If you do not assert promulgated effluent guideline has been remanded for a claim of confidentiality at the time of submitting the information, reconsideration by a court and does not apply to your operations, EPA may make the information public without further notice to you. you may check"no." Claims of confidentiality will be handled in accordance with EPA's Item III-B business confidentiality regulations at 40 CFR Part 2. An effluent guideline is expressed in terms of production (or other Definitions measure of operation) if the limitation is expressed as mass of All significant terms used in these instructions and in the form are pollutant per operational parameter; for example, "pounds of BOD defined in the glossary found in the General Instructions which per cubic foot of logs from which bark is removed," or "pounds of accompany Form 1. TSS per megawatt hour of electrical energy consumed by smelting furnace." An example of a guideline not expressed in terms of a EPA ID Number measure of operation is one which limits the concentration of Fill in your EPA Identification Number at the top of each page of pollutants. Form 2c.You may copy this number directly from item I of Form 1. Item III-C Item I This item must be completed only if you checked"yes"to item III-B. You may use the map you provided for item XI of Form 1 to The production information requested here is necessary to apply determine the latitude and longitude of each of your outfalls and the effluent guidelines to your facility and you cannot claim it as name of the receiving water. confidential. However,you do not have to indicate how the reported information was calculated. Report quantities in the units of Item II-A measurement used in the applicable effluent guideline. The The line drawing should show generally the route taken by water in production figures provided must be based on actual daily production your facility from intake to discharge. Show all operations and not on design capacity or on predictions of future operations.To contributing wastewater, including process and production areas, obtain alternate limits under 40 CFR 122.45(b)(2)(ii),you must define sanitary flows, cooling water, and stormwater runoff.You may group your maximum production capability and demonstrate to the Director similar operations into a single unit, labeled to correspond to the that your actual production is substantially below maximum more detailed listing in item II-B. The water balance should show production capability and that there is a reasonable potential for an average flows. Show all significant losses of water to products, increase above actual production during the duration of the permit. atmosphere, and discharge. You should use actual measurements Item IV-A whenever available; otherwise use your best estimate. An example If you check"yes"to this question, complete all parts of the chart, or of an acceptable line drawing appears in Figure 2c-1 to these instructions. attach a copy of any previous submission you have made to EPA containing same information. Item II-B List all sources of wastewater to each outfall. Operations may be Item IV-B described in general terms (for example, "dye-making reactor" or You are not required to submit a description of future pollution "distillation tower'). You may estimate the flow contributed by each control projects if you do not wish to or if none is planned. source if no date are available. For stormwater discharges you may Item V-A,B,C,and D estimate the average flow, but you must indicate the rainfall event upon which the estimate is based and the method of estimation. For The items require you to collect and report data on the pollutants each treatment unit, indicate its size, flow rate, and retention time, discharged for each of your outfalls. Each part of this item addresses and describe the ultimate disposal of any solid or liquid wastes not a different set of pollutants and must be completed in accordance discharged.Treatment units should be listed in order and you should with the specific instructions for that part. The following general select the proper code from Table 2c-1 to fill in column 3-b for each instructions apply to the entire item. treatment unit. Insert"XX"into column 3-b if no code corresponds to General Instructions a treatment unit you list. If you are applying for a permit for a privately owned treatment works, you must also identify all of your Part A requires you to report at least one analysis for each pollutant contributors in an attached listing. listed. Parts B and C require you to report analytical data in two ways. For some pollutants, you may be required to mark "X" in the Item II-C "Testing Required" column (column 2-a, Part C), and test (sample A discharge is intermittent unless it occurs without interruption during and analyze)and report the levels of the pollutants in your discharge the operating hours of the facility, except for infrequent shutdowns whether or not you expect them to be present in your discharge. For for maintenance, process changes, or other similar activities. A all others, you must mark"X" in either the"Believe Present"column discharge is seasonal if it occurs only during certain parts of the or the "Believe Absent" column (columns 2-a or 2-b, Part B, and year. Fill in every applicable column in this item for each source of columns 2-b or 2-c, Part C)based on your best estimate,and test for intermittent or seasonal discharges. Base your answers on actual those which you believe to be present. (See specific instructions on data whenever available; otherwise, provide your best estimate. the form and below for Parts A through D.) Base your determination Report the highest daily value for flow rate and total volume in the that a pollutant is present in or absent from your discharge on your 2C-1 FORM 2c— INSTRUCTIONS (continued) Item V-A,B,C,and D(continued) knowledge of your raw materials, maintenance chemicals, times, the collection of duplicate samples, etc. The time when you intermediate and final products and byproducts, and any previous sample should be representative of your normal operation, to the analyses known to you of your effluent or similar effluent. (For extent feasible, with all processes which contribute wastewater in example, if you manufacture pesticides, you should expect those normal operation,and with your treatment system operating properly pesticides to be present in contaminated stormwater runoff.) If you with no system upsets. Samples should be collected from the center would expect a pollutant to be present solely as a result of its of the flow channel, where turbulence is at a maximum, at a site presence in your intake water, you must mark"Believe Present"but specified in your present permit, or at any site adequate for the you are not required to analyze for that pollutant. Instead, mark an collection of a representative sample. 'X'In the"Intake"column. For pH,temperature,cyanide,total phenols,residual chlorine,oil and A. Reporting. All levels must be reported as concentration grease,and fecal coliform,grab samples must be used. For all other and as total mass. You may report some or all of the pollutants 24-hour composite samples must be used. However, a required data by attaching separate sheets of paper minimum of one grab sample may be taken for effluents from holding instead of filling out pages V-I to V-9 if the separate sheets ponds or other impoundments with a retention period of greater than contain all the required information in a format which is 24 hours. For stormwater discharges a minimum of one to four grab consistent with pages V-I to V-9 in spacing and in samples may be taken, depending on the duration of the discharge. identification of pollutants and columns. (For example, the One grab must be taken in the first hour(or less) of discharge,with data system used in your GC/MS analysis may be able to one additional grab (up to a minimum of four) taken in each print data in the proper format.) Use the following succeeding hour of discharge for discharges lasting four or more abbreviations in the columns headed "Units" (column 3, hours.The Director may waive composite sampling for any outfall for Part A,and column 4,Parts B and C). which you demonstrate that use of an automatic sampler is infeasible and that a minimum of four grab samples will be representative of Concentration Mass your discharge. ppm parts per million lbs pounds Grab and composite samples are defined as follows: mgh...milligrams per liter ton tons(English tons) ppb parts per billion mg milligrams Grab sample: An individual sample of at least 100 milliliters ugh...micrograms per liter g grams collected at a randomly-selected time over a period not exceeding kg kilograms 15 minutes. T tonnes(metric tons) Composite sample: A combination of at least 8 sample aliquots All reporting of values for metals must be in terms of "total of at least 100 milliliters, collected at periodic intervals during the recoverable metal,"unless: operating hours of a facility over a 24 hour period. The composite must be flow proportional; either the time interval between each (1) An applicable, promulgated effluent limitation or standard aliquot or the volume of each aliquot must be proportional to either specifies the limitation for the metal in dissolved,valent, or total the stream flow at the time of sampling or the total stream flow form;or since the collection of the previous aliquot. Aliquots may be collected manually or automatically. For GC/MS Volatile Organic (2) All approved analytical methods for the metal inherently Analysis (VOA), aliquots must be combined in the laboratory measure only its dissolved form(e.g.,hexavalent chromium);or immediately before analysis. Four(4) (rather than eight) aliquots (3) The permitting authority has determined that in establishing or grab samples should be collected for VOA.These four samples case-by-case limitations it is necessary to express the should be collected during actual hours of discharge over a 24- limitations on the metal in dissolved, valent, or total form to hour period and need not be flow proportioned.Only one analysis carry out the provisions of the CWA. is required. If you measure only one daily value, complete only the "Maximum The Agency is currently reviewing sampling requirements in light of Daily Values" columns and insert '1' into the "Number of Analyses" recent research on testing methods. Upon completion of its review, column (columns 2-a and 2-d, Part A, and column 3-a, 3-d, Parts B the Agency plans to propose changes to the sampling requirements. and C). The permitting authority may require you to conduct Data from samples taken in the past may be used,provided that: additional analyses to further characterize your discharges. For composite samples, the daily value is the total mass or average All data requirements are met; concentration found in a composite sample taken over the operating Sampling was done no more than three years before submission; hours of the facility during a 24-hour period; for grab samples, the and daily value is the arithmetic or flow-weighted total mass or average concentration found in a series of at least four grab samples taken All data are representative of the present discharge. over the operating hours of the facility during a 24-hour period. Among the factors which would cause the data to be If you measure more than one daily value for a pollutant and those unrepresentative are significant changes in production level, values are representative of your wastestream, you must report changes in raw materials, processes, or final products, and changes them. You must describe your method of testing and data analysis. in wastewater treatment. When the Agency promulgates new You also must determine the average of all values within the last analytical methods in 40 CFR Part 136, EPA will provide information year and report the concentration and mass under the "Long Term as to when you should use the new methods to generate data on Average Values"columns(column 2-c, Part A,and column 3-c, Parts your discharges. Of course, the Director may request additional B and C), and the total number of daily values under the"Number of information, including current quantitative data, if she or he Analyses" columns (column 2-d, Part A, and columns 3-d, Parts B determines it to be necessary to assess your discharges. and C).Also, determine the average of all daily values taken during each calendar month, and report the highest average under the C. Analysis: You must use test methods promulgated in 40 CFR "Maximum 30-day Values"columns(column 2-c, Part A, and column Part 136; however, if none has been promulgated for a particular 3-b,Parts B and C). pollutant, you may use any suitable method for measuring the level of the pollutant in your discharge provided that you submit a B. Sampling: The collection of the samples for the reported description of the method or a reference to a published method.Your analyses should be supervised by a person experienced in description should include the sample holding time, preservation performing sampling of industrial wastewater. You may contact your techniques, and the quality control measures which you used. If you EPA or State permitting authority for detailed guidance on sampling have two or more substantially identical outfalls, you may request techniques and for answers to specific questions. Any specific permission from your permitting authority to sample and analyse only requirements contained in the applicable analytical methods should one outfall and submit the results of the analysis for other be followed for sample containers, sample preservation, holding substantially identical outfalls. If your request is granted by the 2C-1 FORM 2c— INSTRUCTIONS (continued) Item V-A,B,C,and D(continued) permitting authority, on a separate sheet attached to the application treatment works,determine your testing requirements on the basis of form,identify which outfall you did test,and describe why the outfalls the industry categories of your contributors. When you determine which you did not test are substantially identical to the outfall which which industry category you are in to find your testing requirements, you did test. you are not determining your category for any other purpose and you are not giving up your right to challenge your inclusion in that D. Reporting of Intake Data: You are not required to report data category (for example, for deciding whether an effluent guideline is under the "Intake" columns unless you wish to demonstrate your applicable) before your permit is issued. For all other cases eligibility for a"net"effluent limitation for one or more pollutants,that (secondary industries, nonprocess wastewater outfalls, and is, an effluent limitation adjusted by subtracting the average level of nonrequired GC/MS fractions), you must mark "X" in either the the pollutant(s) present in your intake water, NPDES regulations "Believed Present" column (column 2-b) or the "Believed Absent" allow net limitations only in certain circumstances. To demonstrate column(column 2-c)for each pollutant.For every pollutant you know your eligibility, under the "Intake"columns report the average of the or have reason to believe is present in your discharge in results of analyses on your intake water (if your water is treated concentrations of 10 ppb or greater, you must report quantitative before use, test the water after it is treated), and discuss the data. For acrolein, acrylonitrile, 2,4 dinitrophenol, and 2-methyl-4, 6 requirements for a net limitation with your permitting authority. dinitrophenol, where you expect these four pollutants to be Part V-A discharged in concentrations of 100 ppb or greater, you must report quantitative data. For every pollutant expected to be discharged in Part V-A must be completed by all applicants for all outfalls,including concentrations less than the thresholds specified above, you must outfalls containing only noncontact cooling water or storm runoff. either submit quantitative data or briefly describe the reasons the However,at your request,the Director may waive the requirement to pollutant is expected to be discharged. At your request the Director, test for one or more of these pollutants, upon a determination that Office of Water Enforcement and Permits, may waive the available information is adequate to support issuance of the permit requirement to test for pollutants for an industrial category or with less stringent reporting requirements for these pollutants. You subcategory. Your request must be supported by data also may request a waiver for one or more of these pollutants for representatives of the industrial category or subcategory in question. your category or subcategory from the Director, Office of Water The data must demonstrate that individual testing for each applicant Enforcement and Permits. See discussion in General Instructions to is unnecessary, because the facilities in question discharge item V for definitions of the columns in Part A. The "Long Term substantially identical levels of the pollutant, or discharge the Average Values" column (column 2-c) and "Maximum 30-day pollutant uniformly at sufficiently low levels. If you qualify as a small Values"column(column 2-b)are not compulsory but should be filled business (see below) you are exempt from testing for the organic out if data are available. toxic pollutants,listed on pages V-4 to V-9 in Part C.For pollutants in Use composite samples for all pollutants in this Part,except use grab intake water,see discussion in General Instructions to this item.The samples for pH and temperature. See discussion in General "Long Term Average Values" column (column 3-c) and "Maximum Instructions to Item V for definitions of the columns in Part A. The 30-day Values"column(column 3-b) are not compulsory but should "Long Term Average Values" column (column 2-c) and "Maximum be filled out if data are available. You are required to mark"Testing 30-Day Values"column (column 2-b) are not compulsory but should Required" for dioxin if you use or manufacture one of the following be filled out if data are available. compounds: Part V-B (a) 2,4,5-trichlorophenoxy acetic acid,(2,4,5-T); Part V-B must be completed by all applicants for all outfalls,including (b) 2-(2,4,5-trichlorophenoxy)propanoic acid,(Silvex,2,4,5-TP) outfalls containing only noncontact cooling water or storm runoff.You must report quantitative data if the pollutant(s) in question is limited (c) 2-(2,4,5-trichlorophenoxy)ethyl 2,2-dichloropropionate,(Erbon); in an effluent limitations guideline either directly, or indirectly but (d) 0,0-dimethyl 0-(2,4,5-trichlorophenyl)phosphorothioate,(Ronnel); expressly through limitation on an indicator (e.g., use of TSS as an indicator to control the discharge of iron and aluminum). For other (e) 2,4,5,-trichlorophenol,(TCP);or discharged pollutants you must provide quantitative data or explain (f) hexachlorophene,(HCP). their presence in your discharge. EPA will consider requests to the Director of the Office of Water Enforcement and Permits to eliminate If you mark "Testing Required" or "Believed Present," you must the requirement to test for pollutants for an industrial category or perform a screening analysis for dioxins, using gas chromotography subcategory.Your request must be supported by data representative with an electron capture detector. A TCDD standard for quantitation of the industrial category or subcategory in question. The data must is not required. Describe the results of this analysis in the space demonstrate that individual testing for each applicant is unnecessary, provided; for example, "no measurable baseline deflection at the because the facilities in the category or subcategory discharge retention time of TCDD"or"a measurable peak within the tolerances substantially identical levels of the pollutant or discharge the of the retention time of TODD."The permitting authority may require pollutant uniformly at sufficiently low levels. Use composite samples you to perform a quantitative analysis if you report a positive result. for all pollutants you analyze for in this part, except use grab The Effluent Guidelines Division of EPA has collected and analyzed samples for residual chlorine,oil and grease, and fecal coliform.The samples from some plants for the pollutants listed in Part C in the "Long Term Average Values" column (column 3-c) and "Maximum course of its BAT guidelines development program. If your effluents 30-day Values" column (column 3-b) are not compulsory but should are sampled and analyzed as part of this program in the last three be filled out if data are available. years, you may use these data to answer Part C provided that the permitting authority approves, and provided that no process change Part V-C or change in raw materials or operating practices has occurred since Table 2c-2 lists the 34 "primary" industry categories in the lefthand the samples were taken that would make the analyses column. For each outfall, if any of your processes which contribute unrepresentative of your current discharge. wastewater falls into one of those categories, you must mark"X" in "Testing Required"column(column 2-a)and test for(I)all of the toxic Small Business Exemption: If you qualify as a "small business", metals, cyanide, and total phenols, and (2)the organic toxic you are exempt from the reporting requirements for the organic toxic pollutants contained in Table 2c-2 as applicable to your category, pollutants, listed on pages V-4 to V-9 in Part C.There are two ways unless you qualify as a small business(see below).The organic toxic in which you can qualify as a"small business."If your facility is a coal pollutants are listed by GC/MS fractions on pages V-4 to V-9 in Part mine, and if your probable total annual production is less than V-C. For example,the Organic Chemicals Industry has an asterisk in 100,000 tons per year, you may submit past production data or all four fractions; therefore, applicants in this category must test for estimated future production (such as a schedule of estimated total all organic toxic pollutants in Part V-C. The inclusion of total phenols production under 30 CFR § 795.14(c)) instead of conducting in Part V-C is not intended to classify total phenols as a toxic analyses for the organic toxic pollutants. If your facility is not a coal pollutant. If you are applying for a permit for a privately owned mine, and if your gross total annual sales for the most recent three years average less than$100,000 per year(in second quarter 1980 2C-1 FORM 2c— INSTRUCTIONS (continued) Item V-A,B,C,and D(continued) dollars), you may submit sales data for those years instead of 40 CFR Part 122.22 requires the certification to be signed as follows: conducting analyses for the organic toxic pollutants. The production or sales data must be for the facility which is the source of the (A) For a corporation: by a responsible corporate official. For purposes of this section, a responsible corporate discharge. The data should not be limited to production or sales for official means (i) a the process or processes which contribute to the discharge, unless president,secretary,treasurer,or vice-president of the corporation in those are the only processes at your facility. For sales data, in charge of a principal business function, or any other person who situations involving intracorporate transfer of goods and services,the performs similar policy- or decision-making functions for the transfer price per unit should approximate market prices for those corporation, or (ii) the manager of one or more manufacturing, goods and services as closely as possible. Sales figures for years production, or operating facilities employing more than 250 persons after 1980 should be indexed to the second quarter of 1980 by using or having gross annual sales or expenditures exceeding$25,000,000 the gross national product price deflator (second quarter of (in second-quarter 1980 dollars), if authority to sign documents has 1980=100). This index is available in National Income and Product been assigned or delegated to the manager in accordance with Accounts of the United States(Department of Commerce, Bureau of corporate procedures. Economic Analysis). Note: EPA does not require specific assignments or delegation of Part V-D authority to responsible corporate officers identified in §122.22(a)(1)(i). The Agency will presume that these responsible List any pollutants in Table 2c-3 that you believe to be present and corporate officers have the requisite authority to sign permit explain why you believe them to be present. No analysis is required, applications unless the corporation has notified the director to the but if you have analytical data,you must report it. contrary. Corporate procedures governing authority to sign permit Note: Under 40 CFR 117.12(a)(2), certain discharges of hazardous applications may provide for assignment or delegation to applicable substances (listed in Table 2c-4 of these instructions) may be corporate position under §122.22(a)(1)(ii) rather than to specific exempted from the requirements of section 311 of CWA, which individuals. establishes reporting requirements, civil penalties and liability for (B) For a partnership or sole proprietorship: by a general partner or cleanup costs for spills of oil and hazardous substances.A discharge the proprietor,respectively;or of a particular substance may be exempted if the origin, source, and amount of the discharged substances are identified in the NDPES (C) For a municipality, State, Federal, or other public agency: by permit application or in the permit, if the permit contains a either a principal executive officer or ranking elected official. For requirement for treatment of the discharge, and if the treatment is in purposes of this section, a principal executive officer of a Federal place. To apply for an exclusion of the discharge of any hazardous Agency includes(i)the chief executive officer of the Agency,or(ii)a substance from the requirements of section 311, attach additional senior executive officer having responsibility for the overall sheets of paper to your form,setting forth the following information: operations of a principal geographic unit of the Agency (e.g., Regional Administrators of EPA). Applications for Group II 1. The substance and the amount of each substance which may stormwater dischargers may be signed by a duly authorized be discharged. representative (as defined in 40 CFR 122.22(b)) of the individuals 2. The origin and source of the discharge of the substance. identified above. 3. The treatment which is to be provided for the discharge by: a. An onsite treatment system separate from any treatment system treating your normal discharge; b. A treatment system designed to treat your normal discharge and which is additionally capable of treating the amount of the substance identified under paragraph 1 above;or c. Any combination of the above. See 40 CFR§117.12(a)(2)and (c)published on August 29, 1979, in 44 FR 50766, or contact your Regional Office (Table 1 on Form 1, Instructions),for further information on exclusions from section 311. Item VI This requirement applies to current use or manufacture of a toxic pollutant as an intermediate or final product or byproduct. The Director may waive or modify the requirement if you demonstrate that it would be unduly burdensome to identify each toxic pollutant and the Director has adequate information to issue your permit. You may not claim this information as confidential; however, you do not have to distinguish between use or production of the pollutants or list the amounts. Item VII Self explanatory. The permitting authority may ask you to provide additional details after your application is received. Item IX The Clean Water Act provides for severe penalties for submitting false information on this application form. Section 309(c)(2) of the Clean Water Act provides that"Any person who knowingly makes any false statement, representation, or certification in any application,... shall upon conviction, be punished by a fine of not more than$10,000 or by imprisonment for not more than six months,or by both." 2C-2 1 CODES FOR TREATMENT UNITS PHYSICAL TREATMENT PROCESSES 1—A Ammonia Stripping 1—M Grit Removal 1—B Dialysis 1—N Microstraining 1—C Diatomaceous Earth Filtration 1-0 Mixing 1—D Distillation 1—P Moving Bed Filters 1—E Electrodialysis 1—Q Multimedia Filtration 1—F Evaporation 1—R Rapid n Sand Filtration 1—G Flocculation 1—S Reverse Osmosis(Hyperfiltration) 1—H Flotation 1—T Screening 1—I Foam Fractionation 1—U Sedimentation(Settling) 1—J Freezing 1—V Slow Sand Filtration 1—K Gas—Phase Separation 1—W Solvent Extraction 1—L Grinding(Comminutors) 1—X Sorption CHEMICAL TREATMENT PROCESSES 2—A Carbon Adsorption 2—G Disinfection(Ozone) 2—B Chemical Oxidation 2—H Disinfection(Other) 2—C Chemical Precipitation 2—I Electrochemical Treatment 2—D Coagulation 2—J Ion Exchange 2—E Dechlorination 2—K Neutralization 2—F Disinfection(Chlorine) 2—L Reduction BIOLOGICAL TREATMENT PROCESSES 3—A Activated Sludge 3—E Pre-Aeration 3—B Aerated Lagoons 3—F Spray Irrigation/Land Application 3—C Anaerobic Treatment 3—G Stabilization Ponds 3—D Nitrification—Denitrification 3—H Trickling Filtration OTHER PROCESSES 4—A Discharge to Surface Water 4—C Reuse/Recycle of Treated Effluent 4—B Ocean Discharge Through Outfall 4-D Underground Injection SLUDGE TREATMENT AND DISPOSAL PROCESSES 5—A Aerobic Digestion 5—M Heat Drying 5—B Anaerobic Digestion 5—N Heat Treatment 5—C Belt Filtration 5-0 Incineration 5—D Centrifugation 5—P Land Application 5—E Chemical Conditioning 5—Q Landfill 5—F Chlorine Treatment 5—R Pressure Filtration 5—G Composting 5—S Pyrolysis 5—H Drying Beds 5—T Sludge Lagoons 5—I Elutriation 5—U Vacuum Filtration 5—J Flotation Thickening 5—V Vibration 5—K Freezing 5—W Wet Oxidation 5—L Gravity Thickening Table 2C-1 TESTING REQUIREMENTS FOR ORGANIC TOXIC POLLUTANTS INDUSTRY CATEGORY* INDUSTRY CATEGORY GC/MS FRACTION' Volatile Acid Base/Neutral Pesticide Adhesives and sealants X X X — Aluminum forming X X X — Auto and other laundries X X X X Battery manufacturing X — X — Coal mining X X X X Coil coating X X X — Copper forming X X X — Electric and electronic compounds X X X X Electroplating X X X — Explosives manufacturing — X X — Foundries X X X — Gum and wood chemicals X X X X Inorganic chemicals manufacturing X X X — Iron and steel manufacturing X X X — Leather tanning and finishing X X X X Mechanical products manufacturing X X X — Nonferrous metals manufacturing X X X X Ore mining X X X X Organic chemicals manufacturing X X X X Paint and ink formulation X X X X Pesticides X X X X Petroleum refining X X X X Pharmaceutical preparations X X X — Photographic equipment and supplies X X X X Plastic and synthetic materials manufacturing X X X X Plastic processing X — — — Porcelain enameling X — X X Printing and publishing X X X X Pulp and paperboard mills X X X X Rubber processing X X X — Soap and detergent manufacturing X X X — Steam electric power plants X X X — Textile mills X X X X Timber products processing X X X X *See note at conclusion of 40 CFR Part 122,Appendix D(1983)for explanation of effect of suspensions on testing requirements for primary industry categories. 'The pollutants in each fraction are listed in Item V-C. X=Testing required. —=Testing not required. Tabe 2C-2 1t TOXIC POLLUTANTS AND HAZARDOUS SUBSTANCES REQUIRED TO BE IDENTIFIED BY APPLICANTS IF EXPECTED TO BE PRESENT TOXIC POLLUTANT HAZARDOUS SUBSTANCES HAZARDOUS SUBSTANCES Asbestos Dichlorvos Naled Diethyl amine Napthenic acid HAZARDOUS SUBSTANCES Dimethyl amine Nitrotoluene Dintrobenzene Parathion Acetaldehyde Diquat Phenolsulfonate Allyl alcohol Disulfoton Phosgene Allyl chloride Diuron Propargite Amyl acetate Epichlorohydrin Propylene oxide Aniline Ethion Pyrethrins Benzonitrile Ethylene diamine Quinoline Benzyl chloride Ethylene dibromide Resorcinol Butyl acetate Formaldehyde Strontium Butylamine Furfural Strychnine Captan Guthion Styrene Carbaryl Isoprene 2,4,5-T(2,4,5-Trichlorophenoxyacetic acid) Carbofuran Isopropanolamine TDE(Tetrachlorodiphenyl ethane) Carbon disulfide Kelthane 2,4,5-TP[2-(2,4,5-Trichlorophenoxy)propanoic acid] Chlorpyrifos Kepone Trichlorofon Coumaphos Malathion Triethanolamine Cresol Mercaptodimethur Triethylamine Crotonaldehyde Methoxychlor Trimethylamine Cyclohexane Methyl mercaptan Uranium 2,4-D(2,4-Dichlorophenoxyacetic acid) Methyl methacrylate Vanadium Diazinon Methyl parathion Vinyl acetate Dicamba Mevinphos Xylene Dichlobenil Mexacarbate Xylenol Dichlone Monoethyl amine Zirconium 2,2-Dichloropropionic acid Monomethyl amine Table 2C-3 HAZARDOUS SUBSTANCES 1.Acetaldehyde 74.Carbaryl 145.Formaldehyde 2.Acetic acid 75.Carbofuran 146.Formic acid 3.Acetic anhydride 76.Carbon disulfide 147.Fumaric acid 4.Acetone cyanohydrin 77.Carbon tetrachloride 148.Furfural 5.Acetyl bromide 78.Chlordane 149.Guthion 6.Acetyl chloride 79.Chlorine 150.Heptachlor 7.Acrolein 80.Chlorobenzene 151.Hexachlorocyclopentadiene 8.Acrylonitrile 81.Chloroform 152.Hydrochloric acid 9.Adipic acid 82.Chloropyrifos 153.Hydrofluoric acid 10.Aldrin 83.Chlorosulfonic acid 154.Hydrogen cyanide 11.Allyl alcohol 84.Chromic acetate 155.Hydrogen sulfide 12.Allyl chloride 85.Chromic acid 156.Isoprene 13.Aluminum sulfate 86.Chromic sulfate 157. Isopropanolamine 14.Ammonia 87.Chromous chloride dodecylbenzenesulfonate 15.Ammonium acetate 88.Cobaltous bromide 158.Kelthane 16.Ammonium benzoate 89.Cobaltous formate 159.Kepone 17.Ammonium bicarbonate 90.Cobaltous sulfamate 160.Lead acetate 18.Ammonium bichromate 91.Coumaphos 161.Lead arsenate 19.Ammonium bifluoride 92.Cresol 162.Lead chloride 20.Ammonium bisulfite 93.Crotonaldehyde 163.Lead fluoborate 21.Ammonium carbamate 94.Cupric acetate 164.Lead flourite 22.Ammonium carbonate 95.Cupric acetoarsenite 165.Lead iodide 23.Ammonium chloride 96.Cupric chloride 166.Lead nitrate 24.Ammonium chromate 97.Cupric nitrate 167.Lead stearate 25.Ammonium citrate 98.Cupric oxalate 168.Lead sulfate 26.Ammonium fluoroborate 99.Cupric sulfate 169.Lead sulfide 27.Ammonium fluoride 100.Cupric sulfate ammoniated 170.Lead thiocyanate 28.Ammonium hydroxide 101.Cupric tartrate 171.Lindane 29.Ammonium oxalate 102.Cyanogen chloride 172.Lithium chromate 30.Ammonium silicofluoride 103.Cyclohexane 173.Malathion 31.Ammonium sulfamate 104.2,4-D acid(2,4-Dichlorophenoxyacetic 174.Maleic acid 32.Ammonium sulfide acid) 175.Maleic anhydride 33.Ammonium sulfite 105.2,4-D esters(2,4-Dichlorophenoxyacetic 176.Mercaptodimethur 34.Ammonium tartrate acid esters) 177.Mercuric cyanide 35.Ammonium thiocyanate 106.DDT 178. Mercuric nitrate 36.Ammonium thiosulfate 107.Diazinon 179.Mercuric sulfate 37.Amyl acetate 108.Dicamba 180.Mercuric thiocyanate 38.Aniline 109.Dichlobenil 181.Mercurous nitrate 39.Antimony pentachloricle 110.Dichlone 182.Methoxychlor 40.Antimony potassium tartrate 111.Dichlorobenzene 183.Methyl mercaptan 41.Antimony tribromide 112.Dichloropropane 184.Methyl methacrylate 42.Antimony trichloride 113.Dichloropropene 185.Methyl parathion 43.Antimony trifluoride 114.Dichloropropene-dichloproropane mix 186.Mevinphos 44.Antimony trioxide 115.2,2-Dichloropropionic acid 187.Mexacarbate 45.Arsenic disulfide 116.Dichlorvos 188.Monoethylamine 46.Arsenic pentoxide 117.Dieldrin 189.Monomethylamine 47.Arsenic trichloride 118. Diethylamine 190.Naled 48.Arsenic trioxide 119.Dimethylamine 191.Naphthalene 49.Arsenic trisulfide 120.Dinitrobenzene 192.Naphthenic acid 50.Barium cyanide 121. Dinitrophenol 193.Nickel ammonium sulfate 51.Benzene 122.Dinitrotoluene 194.Nickel chloride 52.Benzoic acid 123.Diquat 195.Nickel hydroxide 53. Benzonitrile 124.Disulfoton 196.Nickel nitrate 54. Benzoyl chloride 125.Diuron 197.Nickel sulfate 55. Benzyl chloride 126.Dodecylbenzesulfonic acid 198.Nitric acid I 56. Beryllium chloride 127.Endosulfan 199.Nitrobenzene 57. Beryllium fluoride 128.Endrin 200.Nitrogen dioxide 58.Beryllium nitrate 129.Epichlorohydrin 201.Nitrophenol 59.Butylacetate 130. Ethion 202.Nitrotoluene 60.n-Butylphthalate 131.Ethylbenzene 203.Paraformaldehyde 61. Butylamine 132.Ethylenediamine 204.Parathion 62. Butyric acid 133. Ethylene dibromide 205.Pentachlorophenol 63.Cadmium acetate 134. Ethylene dichloride 206.Phenol 64.Cadmium bromide 135. Ethylene diaminetetracetic acid(EDTA) 207.Phosgene 65.Cadmium chloride 136. Ferric ammonium citrate 208.Phosphoric acid 66.Calcium arsenate 137.Ferric ammonium oxalate 209.Phosphorus 67.Calcium arsenite 138. Ferric chloride 210.Phosphorus oxychloride 69.Calcium carbide 139.Ferric fluoride 211.Phosphorus pentasulfide 69.Calcium chromate 140.Ferric nitrate 212.Phosphorus trichloride 70.Calcium cyanide 141.Ferric sulfate 213.Polychlorinated biphenyls(PCB) 71.Calcium dodecylbenzenesulfonate 142.Ferrous ammonium sulfate 214.Potassium arsenate 72.Calcium hypochlorite 143.Ferrous chloride 215.Potassium arsenite 73.Captan 144.Ferrous sulfate 216.Potassium bichromate Table 2C-4 HAZARDOUS SUBSTANCES 217.Potassium chromate 247.Sodium selenite 270.Trimethylamine 218.Potassium cyanide • 248.Strontium chromate 271.Uranyl acetate 219.Potassium hydroxide 249.Strychnine 272.Uranyl nitrate 220.Potassium permanganate 250.Styrene 273.Vanadium penoxide 221.Propargite 251.Sulfuric acid 274.Vanadyl sulfate 222.Propionic acid 252.Sulfur monochloride 275.Vinyl acetate 223.Propionic anhydride 253.2,4,5-T acid(2,4,5- 276.Vinylidene chloride 224.Propylene oxide Trichlorophenoxyacetic acid) 277.Xylene 225.Pyrethrins 254.2,4,5-T amines(2,4,5-Trichlorophenoxy 278.Xylenol 226.Quinoline acetic acid amines) 279.Zinc acetate 227.Resorcinol 255.2,4,5-T esters(2,4,5 Trichlorophenoxy 280.Zinc ammonium chloride 228.Selenium oxide acetic acid esters) 281.Zinc borate 229.Silver nitrate 256.2,4,5-T salts(2,4,5-Trichlorophenoxy 282.Zinc bromide 230.Sodium acetic acid salts) 283.Zinc carbonate 231.Sodium arsenate 257.2,4,5-TP acid(2,4,5-Trichlorophenoxy 284.Zinc chloride 232.Sodium arsenite propanoic acid) 285.Zinc cyanide 233.Sodium bichromate 258.2,4,5-TP acid esters(2,4,5- 286.Zinc fluoride 234.Sodium bifluoride Trichlorophenoxy propanoic acid esters) 287.Zinc formate 235.Sodium bisulfite 259.TDE(Tetrachlorodiphenyl ethane) 288.Zinc hydrosulfite 236.Sodium chromate 260.Tetraethyl lead 289.Zinc nitrate 237.Sodium cyanide 261.Tetraethyl pyrophosphate 290.Zinc phenolsulfonate 238.Sodium dodecylbenzenesulfonate 262.Thallium sulfate 291.Zinc phosphide 239.Sodium fluoride 263.Toluene 292.Zinc silicofluoride 240.Sodium hydrosulfide 264.Toxaphene 293.Zinc sulfate 241.Sodium hydroxide 265.Trichlorofon 294.Zirconium nitrate 242.Sodium hypochlorite 266.Trichloroethylene 295.Zirconium potassium flouride 243.Sodium methylate 267.Trichlorophenol 296.Zirconium sulfate 244.Sodium nitrite 268.Triethanolamine 297.Zirconium tetrachloride 245.Sodium phosphate(dibasic) dodecylbenzenesulfonate 246.Sodium phosphate(tribasic) 269.Triethylamine Table 2C-4(continued) 1 LINE DRAWING Blue River Municipal GPD Water Supply Blue River 190,000 10,000 GPD 45,000 GPD 45,000 GPD 30,000 GPD Cooling Water Raw Materials Fiber 15yT Dyeing 20,000 Washing 10,000 Drying 5,000 GPD 10,000 GPD Preparation GPD GPD GPD To Atmosphere 40,000 GPD 40,000 GPD 40,000 10,000 To Product GPD GPD 5,000 GPD Solid Waste Grit Neutralization Loss Waste Separator Tank 6,000 GPD ► Treatment � • — 4,000GPD Plant#2 36,000 GPD 34,000 GPD Outfall 002 50,000 GPD Waste t Treatment Outfall 001 Stormwater 70,000 GPD+Stormwa er Max:20,000 GPD Plant#1 Schematic of Water Flow Brown Mills,Inc. City,County,State Figure 2C-1 EPA I.D.NUMBER(copy'from Item I of Form l) Form Approved. OMB No.2040-0086. Please print or type in the unshaded areas only. Approval expires 3-31-98. FORMU.S.U.S.ENVIRONMENTAL PROTECTION AGENCY 2C �"iEPA EXISTING MANUFACTURING,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS CATION FOR PERMIT TO DISCHARGE WASTEWATER NPDES Consolidated Permits Program I.OUTFALL LOCATION For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE (lr''t) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name) 001 36 14 40 80 50 22 Yadkin River II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations, treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT FALL b.AVERAGE FLOW b.LIST CODES FROM NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1 See Figure 1-4 See Figure 1-5 OFFICIAL USE ONLY(effluent guidelines sub-categories) EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal? ❑YES(complete the/allowing table) NO(go to Section III) 3.FREQUENCY 4.FLOW a DAYS PER B.TOTAL VOLUME 2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mg.) (speoilp with unity) 1.OUTFALL CONTRIBUTING FLOW (,yx-gly PER YEAR 1.LONG TERM' 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION NUMBER(list) (hst) average) (spect.$'average) AVERAGE DAILY AVERAGE DAILY (in days) III.PRODUCTION A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? IZI YES(complete Item 111-B) El NO(go to Section IV) B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)? ©YES(complete Item Ill-(') El NO(go to Section II) C. If you answered"yes"to Item Ill-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the applicable effluent guideline,and indicate the affected outfalls. 1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS a.QUANTITY PER DAY b.UNITS OF MEASURE C.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers) (spect6) 752 Lbs/day Subpart C- Low Water Use Processing 001 14,687 Lbs/day Subpart D- Woven Fabric Finishing 001 Details provided in Appendix A. Production numbers represent the highest operating level values from years 2015, 2016, and 2017 IV.IMPROVEMENTS A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to. permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions. E lYES(complete the following table) ❑NO(go to Item IV-B) 1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE AGREEMENT,ETC. a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for construction. E l MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3 EPA I.D.NUMBER(copy from Item I of Form 1) CONTINUED FROM PAGE 2 V.INTAKE AND EFFLUENT CHARACTERISTICS A,B,8 C: See instructions before proceeding-Complete one set of tables for each outfall-Annotate the outfall number in the space provided. NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE Acetaldehyde These pollutants are found at Formaldehyde trace levels in some process Propylene oxide chemicals used in the Styrene manufacturing of textiles at Vinyl Acetate Duvaltex (US), Inc. VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct? YES(list all such pollutants below) ❑NO(go to Item V!-B) The following detectable pollutants are components of the fibers, dyes, and auxillary chemicals currently used at Duvaltex (US) , Inc. to manufacture textiles: METALS, CYANIDE, & TOTAL PHENOL- Total Antimony, Total Arsenic, Total Chromium, Total Zinc, Total Cyanide, Total Phenols, and Total Copper GC/MS FRACTION- VOLATILE COMPOUNDS- Acrylonitrile The following detectable pesticide pollutants have not definitively been determined to be components of materials used to manufacture textiles: GC/MS FRACTION-PESTICIDES- 4,4-DDD, Dieldrin, Endrin, Endrin aldehyde Though non-detect in the 2017 Priority Pollutant Analysis, the following pollutants are believed present as components of the fibers, dyes, and auxilary chemicals currently used at Duvaltex (US) , Inc. to manufacture textiles: METALS,CYANIDE, & TOTAL PHENOL- Total Cadmium, Total Lead, Total Mercury (Prop65 threshold only) , Total Nickel, Total Silver GS/MS FRACTION- VOLATILE COMPOUNDS- 1,1-Dichloroethylene, Ethylbenzene, Vinyl Chloride GC/MS FRACTION- BASE/NEUTRAL COMPOUNDS- 1,2-Dichlorobenzene, Di-N-Butyl Phthalate, Hexachlorobenzene EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT VII.BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? ©YES(idenn(v the test(s)and describe their purposes below) ❑NO(go to Section VIII) As a condition of NPDES Permit N0005312, Duvaltex (US) , Inc. is required to perform quarterly monitoring of toxicity using test procedures outlined in the permit (Ceriodaphnia Effluent Bioassay) . Effluent sampling fol this testing is performed at the NPDES permitted final discharge. The permit specified effluent concentration at which there may be no observable inhibition of reproduction or significant mortality is 1.9%. A summary table of chronic toxicity testing and attached reports for the 2017 calendar year are included in Appendix B. VIII.CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? YES(list the name,address,and telephone number of and pollutants analyzed by, ❑NO(go to Section IX) each such laboratory or firm below) A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED (area code&no.) (list) Pace Analytical 9800 Kincey Avenue, Suite 100 (704) 875-9092 1) Priority pollutant Guntersville, NC 28078 analysis; 21Other sampling for renewal: TOC, Color, Ammonia (as N), Nitrate-Nitrite, Oil & Grease; 3)Permit requirements: BOD, COD, TSS, Sulfides, Phenols, Chromium, Fecal Coliform, Total Nitrogen, Total Phosphorous, Chronic Toxicity, Total Lead, Total Arsenic, Benzene, Ethylbenzene, Chloroform (See Appendicies C & D) IX.CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations. A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.) Scott Taylor- Environmental Coordinator (207) 876-1418 C.SIGNATURE D.DATE SIGNED EPA Form 3510-2C(8-90) PAGE 4 of 4 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I D.NUMBER(cope from Nem/of Form I) on separate sheets(use the same format)instead of completing these pages. SEE INSTRUCTIONS. OUTFALL NO. V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C) PART A—You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details. 3.UNITS 4.INTAKE 2.EFFLUENT (specify if blank) (optional) b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF 1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES a.Biochemical Oxygen SEE ATTACHED DATA SHEET IN Demand(HOD) b.Chemical Oxygen SECTION 2 & APPENDIX C Demand(('OD) c.Total Organic Carbon (TO(') d.Total Suspended Solids(TS'S) e.Ammonia(a.s A VALUE VALUE VALUE VALUE f.Flow g Temperature VALUE VALUE VALUE VALUE (winter) h.Temperature VALUE VALUE VALUE VALUE (.summer) pH MINIMUM MAXIMUM MINIMUM MAXIMUMi. STANDARD UNITSg,roy 4 c`t PART B— Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements. 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) 1 POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE AND a b a.MAXIMUM DAILY VALUE (I/available) (if available) VALUE CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF Of available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES a.Bromide (24959-67-9) b.Chlorine,Total Residual c.Color d.Fecal Coliform e Fluoride (16984-48-8) f.Nitrate-Nitrite (as M EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(upuonal) 1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AND a. b a.MAXIMUM DAILY VALUE (Uavadahle) (+i/available) AVERAGE VALUE CAS NO. BELIEVED BELIEVED (1) d.NO.OF a.CONCEN- b. NO.OF (+(avaduCONCENTRATION (2)MASS CONCENTRATION hle) PRESENT ABSENT (1) (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2)MASS ANALYSES g.Nitrogen, Total Organic(as N) h.Oil and Grease i.Phosphorus (as P),Total (7723-14-0) j.Radioactivity (1)Alpha.Total (2)Beta,Total (3)Radium, Total (4)Radium 226. Total k.Sulfate (us SU,) (14808-79-8) I.Sulfide m.Sulfite (a,SO.) (14265-45-3) n.Surfactants o.Aluminum, Total (7429-90-5) p.Barium,Total (7440-39-3) q.Boron.Total (7440-42-8) r Cobalt,Total (7440-48-4) s.Iron,Total (7439-89-6) t.Magnesium. Total (7439-95-4) u.Molybdenum. Total (7439-98-7) v.Manganese, Total (7439-96-5) w.Tin,Total (7440-31-5) x.Titanium. Total (7440-32-6) EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3 EPA I.D.NUMBER(copy from hem I of Form I) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C PART C- If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark"X"in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a(secondary industries, nonprocess wastewater outfalls. and nonrequired GC/MS fractions), mark"X"in column 2-b for each pollutant you know or have reason to believe is present. Mark"X"in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant,you must provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table(all 7 pages)for each outfall. See instructions for additional details and requirements. 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(uprrunul) 1.POLLUTANT b. MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM ANDa b. c a.MAXIMUM DAILY VALUE (daro+lable) VALUE(+f arodahlr) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1)NO.OF a.CONCEN- b.NO.OF (ifaradoh (2)MASS CONCENTRATION (2)MASS /e) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (1) CONCENTRATION (2)MASS ANALYSES TRATION b.MASS (1) ANALYSES METALS,CYANIDE,AND TOTAL PHENOLS 1M.Antimony,Total (7440-36-0) 2M Arsenic,Total (7440-38-2) 3M.Beryllium,Total (7440-41-7) 4M.Cadmium,Total (7440-43-9) 5M.Chromium, Total(7440-47-3) 6M.Copper,Total (7440-50-8) 7M.Lead,Total (7439-92-1) 8M Mercury,Total (7439-97-6) 9M.Nickel,Total (7440-02-0) 10M.Selenium, Total(7782-49-2) 11M Silver,Total (7440-22-4) 12M.Thallium, Total(7440-28-0) 13M Zinc,Total (7440-66-6) 14M.Cyanide, Total(57-12-5) 15M.Phenols, Total DIOXIN 2,3,7,8-Tetra- DESCRIBE RESULTS chlorodibenzo-P- Dioxin(1764-01-6) EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 2.MARK"X" 3.EFFLUENT 4. UNITS 5.INTAKE(upn ,u/) 1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM AND a b c a.MAXIMUM DAILY VALUE (rJnrud,rh/e) VALUE(!/available) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED ((1) (1) (1) d.NO.OF a CONCEN- (1) b NO.OF (r/rn available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS r CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES GC/MS FRACTION—VOLATILE COMPOUNDS Accrolein 1V ccr lean (107-02-8) • 2V.Acrylonitrile • (107-13-1) 3V.Benzene (71-43-2) 4V.Bis(I'hloru- urcdnl)Ether (542-88-1) 5V.Bromoform (75-25-2) 6V.Carbon Tetrachloride (56-23-5) 7V.Chlorobenzene (108-90-7) 8V.Chlorodi- bromomethane (124-48-1) 9V.Chloroethane (75-00-3) 10V.2-Chloro- ethylvinyl Ether (110-75-8) 11V.Chloroform (67-66-3) 12V.Dichloro- bromomethane (75-27-4) 13V.Dichloro- difluoromethane (75-71-8) 14V.1,1-Dichloro- ethane(75-34-3) 15V.1,2-Dichloro- ethane(107-06-2) 16V.1.1-Dichloro- ethylene(75-35-4) 17V.1,2-Dichloro- propane(78-87-5) 18V.1,3-Dichloro- propylene (542-75-6) 19V.Ethylbenzene (100-41-4) 20V.Methyl Bromide(74-83-9) 21V.Methyl Chloride(74-87-3) EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5 CONTINUED FROM PAGE V-4 2 MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(uprmnr(l) 1. POLLUTANT b MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM ANDa b e. a.MAXIMUM DAILY VALUE ((/ararl�rhle) VALUE(?/available) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- b.NO.OF (!Ianurlrrhlr) REQUIRED PRESENT ABSENT CONCENTRATION ANALYSES TRATION b.MASS (1) (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASSCONCENTRATION (2)MASS ANALYSES GC/MS FRACTION—VOLATILE COMPOUNDS(c m!,nu /) 22V.Methylene Chloride(75-09-2) 23V.1,1,2,2- Tetrachloroethane (79-34-5) 24V.Tetrachloro- ethylene(127-18-4) 25V.Toluene (108-88-3) 26V.1.2-Trans- Dichloroethylene (156-60-5) 27V.1,1,1-Trichloro- ethane(71-55-6) 28V.1,1,2-Trichloro- ethane(79-00-5) 29V Trichloro- ethylene(79-01-6) 30V,Trichloro- fluoromethane (75-69-4) 31V.Vinyl Chloride (75-01-4) GC/MS FRACTION—ACID COMPOUNDS 1A.2-Chlorophenol (95-57-8) 2A.2,4-Dichloro- phenol(120-83-2) 3A.2,4-Dimethyl- phenol(105-67-9) 4A.4,6-Dinitro-O- Cresol(534-52-1) 5A.2,4-Dinitro- phenol(51-28-5) 6A.2-Nitrophenol (88-75-5) 7A.4-Nitrophenol (100-02-7) 8A.P-Chloro-M- Cresol(59-50-7) 9A.Pentachloro- phenol(87-86-5) 10A.Phenol (108-95-2) 11A.2,4,6-Trichloro- phenol(88-05-2) EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(opnnn,d) 1. POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG a.LONG TERM ANDa b c a.MAXIMUM DAILY VALUE (//arud,rhlr) VALUE(furoduhl))) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (11 d NO.OF a.CONCEN- (1) b. NO.OF (,{ar,al),h/ ) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2)MASS ANALYSES GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS 18.Acenaphthene (83-32-9) 28.Acenaphtylene (208-96-8) • 3B.Anthracene (120-12-7) 4B.Benzidine (92-87-5) 58.Benzo(a) Anthracene (56-55-3) 6B.Benzo(„) Pyrene(50-32-8) 7B.3.4-Benzo- fluoranthene (205-99-2) 8B.Benzo(A/e) Perylene(191-24-2) 9B.Benzo(A) Fluoranthene (207-08-9) 108.Bis(2-(111oro- ethoxy)Methane (111-91-1) 11B.Bis(2-(7duro- 1rh,ii Ether (111-44-4) • 12B.Bis(2- ('hlarn,sopraprn Ether(102-80-1) • 13B.Bis(2-Erinl- hes3l)Phthalate (117-81-7) 14B.4-Bromophenyl Phenyl Ether (101-55-3) • 158.Butyl Benzyl Phthalate(85-68-7) • 16B.2-Chloro- naphthalene (91-58-7) 17B.4-Chloro- phenyl Phenyl Ether (7005-72-3) 188 Chrysene (218-01-9) • 19B.Dibenzo(a.h) Anthracene (53-70-3) 208.1,2-Dichloro- benzene(95-50-1) 21B.1,3-Di-chloro- benzene(541-73-1) ,3-Di-chloro- benzene(541-73-1) '•• EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7 CONTINUED FROM PAGE V-6 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(n/ni,nul) 1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM ANDa b c a.MAXIMUM DAILY VALUE (,/or (/,h/e) VALUE(,J,nv,/ahl(e) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF (,/urmlohl(,) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (21 MASS ANALYSES GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(un,nnurd) 228.1,4-Dichloro- benzene(106-46-7) 238.3,3-Dichloro- benzidine(91-94-1) 24B.Diethyl Phthalate(84-66-2) • 25B.Dimethyl Phthalate (131-11-3) 26B.Di-N-Butyl Phthalate(84-74-2) 278.2,4-Dinitro- toluene(121-14-2) 28B.2.6-Dinitro- toluene(606-20-2) • 29B.Di-N-Octyl Phthalate(117-84-0) 30B.1,2-Diphenyl- hydrazine(as Azo- benzene)(122-66-7) 31B.Fluoranthene (206-44-0) 328.Fluorene (86-73-7) 338 Hexachloro- benzene(118-74-1) 348.Hexachloro- butadiene(87-68-3) 35B.Hexachloro- cyclopentadiene (77-47-4) 36B Hexachloro- ethane(67-72-1) 37B.Indeno (1,2,3-cd)Pyrene (193-39-5) 38B.Isophorone (78-59-1) 39B.Naphthalene (91-20-3) 40B.Nitrobenzene (98-95-3) 41B.N-Nitro- sodimethylamine (62-75-9) 428.N-Nitrosodi- N-Propylamine (621-64-7) EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) 1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM ANDa- b. c. a.MAXIMUM DAILY VALUE (II available) VALUE(!t available) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF ((/uradahlr) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continue(/) 43B.N-Nitro- sodiphenylamine (86-30-6) 44B.Phenanthrene (85-01-8) 45B.Pyrene (129-00-0) 46B.1,2,4-Tri- chlorobenzene (120-82-1) GC/MS FRACTION—PESTICIDES 1 P.Aldrin (309-00-2) 2P.a-BHC (319-84-6) 3P.)3-BHC (319-85-7) 4P.y-BHC (58-89-9) 5P.8-BHC (319-86-8) 6P.Chlordane (57-74-9) 7P.4,4'-DDT (50-29-3) 8P.4,4'-DDE (72-55-9) 9P.4,4'-DDD (72-54-8) 10P.Dieldrin (60-57-1) 11P.a-Enosulfan (115-29-7) 12P.)3-Endosulfan (115-29-7) 13P.Endosulfan Sulfate (1031-07-8) 14P.Endrin (72-20-8) 15P.Endrin Aldehyde (7421-93-4) 16P.Heptachlor (76-44-8) EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9 EPA I.D.NUMBER(copyfrom Item l of Form I) OUTFALL NUMBER CONTINUED FROM PAGE V-8 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) 1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM AND a. b. c. a.MAXIMUM DAILY VALUE (iJavailable) VALUE(!l available) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF (if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES GC/MS FRACTION—PESTICIDES(continued) 17P.Heptachlor Epoxide (1024-57-3) 18P.PCB-1242 (53469-21-9) 19P.PCB-1254 (11097-69-1) 20P.PCB-1221 (11104-28-2) 21P.PCB-1232 (11141-16-5) 22P.PCB-1248 (12672-29-6) 23P.PCB-1260 (11096-82-5) 24P.PCB-1016 (12674-11-2) 25P.Toxaphene (8001-35-2) EPA Form 3510-2C(8-90) PAGE V-9 EPA ID#NC0005312 OUTFALL# 001 ITEM V 2. EFFLUENT 3. UNITS 4. INTAKE(optional) PART A a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE(4 available) c. LONG TERM AVERAGE VALUE(if available) a. LONG TERM AVERAGE VALUE CONCENIRATION CONCENIRAIION d. No.of d. No.of 1. POLLUTANT (mg/L) MASS(Ib/day) (mg/L) MASS(lb/day) CONCENTRATION(mg/L) MASS(Ib/day) Analyses CONCENTRATION MASS CONCENTRATION(mg/L) MASS(Ib/dayl) Analyses BOD 16.8 36.219 16.8 36.219 6.368 4.303 249 mg/L lbs NA NA NA COD 137 340.940 137 340.940 101.5 68.704 49 mg/L lbs NA NA NA TOC 33.7 15.011 33.7 15.011 33.7 15.011 1 mg/L lbs NA NA NA TSS 243 431.873 243 431.873 38.537 26.041 249 mg/L lbs NA NA NA Ammonia(as N) ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Flow 0.47535 0.47535 0.080408476 365 NA MGD NA NA NA Temperature(winter) 22.5 22.5 _ 16.6 122 1C NA NA NA � Temperature(summer) 26.3 26.3 24.6 126 "C NA NA NA H 7.02(Minimum) 7.59 (Maximum) 7.02(Minimum) 7.59 (Maximum) 248 Standard Units NA NA NA ITEM V 2. MARK"X" 3. EFFLUENT 4. UNITS 5. INTAKE(optional) PART B a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE(if available) c. LONG TERM AVERAGE VALUE(if available) a. LONG TERM AVERAGE VALUE 1. POLLU IAN f AND CAS NUMBER Of b. BELIEVED CONCEN I RATION CONCEM RATION d. No.of d. No.of available) a. BELIEVED PRESENT ABSENT (mg/L) MASS(Ib/day) (mg/L) MASS(Ib/day) CONCENTRATION(mg/L) MASS(lb/day) Analyses CONCENTRATION MASS CONCENTRATION(mg/L) MASS(Ib/dayl) Analyses Bromide(24959-67-9) X NA NA NA NA NA NA 0 NA NA NA NA NA Chlorine,Total Residual X <25 pg/L 0 <25 pg/L 0 <25 pg/L 0 248 pg/L lbs NA NA NA Color X ND ADMI Units 0 ND ADMI Units 0 _ ND ADMI Units 0 1 ADMI Units NC NA NA NA Fecal Coliform X 23 #/100mL NC 23 #/100mL NC 12.5 #/100mL NC 24 #/100mL NC NA NA NA Fluoride(16984-48-8) X 0.14 0.129 0.14 0.129 0.14 0.129 1 mg/L lbs NA NA NA Nitrate-Nitrite(as N) X 0.92 0.849 0.92 0.849 0.92 0.849 1 mg/L lbs NA NA NA Nitrogen,Total Organic(as N) X 3.2 6.746 3.2 6.746 3.2 2.437 15 mg/L lbs NA NA NA Oil and Grease X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Phosphorus(as P)(7723-14-0) X 2.8 8.095 2.8 8.095 2.8 2.153 12 mg/L lbs NA NA NA Radioactivity Alpha.Total - X NA NA NA NA NA NA 0 NA NA NA NA NA Beta,Total X NA NA NA NA NA NA 0 NA NA NA NA NA Radium,Total X NA NA NA NA NA NA 0 NA NA NA NA NA Radium 226,Total X NA NA NA NA NA NA _ 0 NA NA NA NA NA Sulfate(as SO4)(14808-79-8) X 27.1 25.022 28.8 26.592 28.8 26.592 1 mg/L Lbs NA NA NA Sulfide(as S) X 0.11 0.254 0.11 0.254 0.08 0.170 24 mg/L lbs NA NA NA Sulfite(as SO3)(14265-45-3) X NA NA NA NA NA NA 0 NA NA NA NA NA Surfactants X 0.18 0.081 0.18 0.081 0.18 0.081 1 NA NA NA NA NA Aluminum,Total(7429-90-56) X 0.116 0.107 0.116 0.107 0.116 0.107 1 mg/L lbs NA NA NA Barium,Total(7440-39-3) X 0.0106 0.010 0.0106 0.010 0.0106 0.010 1 mg/L lbs NA NA NA Boron,Total(7440-42-8) X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Cobalt,Total(7440-48-4) X ND 0 ND 0 ND 0 1 NA NA NA NA NA Iron,Total(7439-89-6) X 0.0904 0.083 0.45 0.415 0.45 0.415 1 mg/L lbs NA NA NA Magnesium,Total(7439-95-4) X 2.61 2.410 2.23 2.059 2.23 2.059 1 mg/L NA NA NA NA Molybdenum,Total(7439-98-7) X NA NA NA NA NA NA 0 NA NA NA NA NA Manganese,Total(7439-96-5) X 0.0056 0.005 0.0143 0.013 0.0143 0.013 1 mg/L lbs NA NA NA Tin,Total(7440-31-5) X NA NA NA NA NA NA 0 NA NA NA NA _ _ NA Titanium,Total(7440-32-6) X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA ITEM V 2. MARK"X" 3. EFFLUENT 4. UNITS 5. INTAKE(optional) PART C a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE(if available) c. LONG TERM AVERAGE VALUE(if available) a. LONG TERM AVERAGE VALUE 1. POLLUTANT AND CAS NUMBER Of a.TESTING b. BELIEVED c. BELIEVED CONCENTRATION CONCENTRATION d. No.of d. No.of available) REQUIRED PRESENT ABSENT (mg/L) MASS(Ib/day) (mg/L) MASS(lb/day) CONCENTRATION(mg/L) MASS(Ib/day) Analyses CONCENTRATION MASS CONCENTRATION(mg/L) MASS(Ib/dayl) Analyses METALS,CYANIDE,AND TOTAL PHENOLS Antimony,Total(7440-36-0) X X 0.496 0.224 0.496 0.224 0.496 0.224 1 mg/L lbs NA NA NA Arsenic,Total(7440-38-2) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Beryllium,Total(7440-41-7) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Cadmium,Total(7440-43-9) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Chromium,Total(7440-47-3) X X 0.026 0.069 0.026 0.069 0.0253 0.016 25 mg/L lbs NA NA NA Copper,Total(7440-50-8) X X 0.014 0.013 0.014 0.013 0.014 0.013 1 mg/L lbs NA NA NA Lead.Total(7439-92-1) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Mercury,Total(7439-97-6) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Nickel,Total(740-02-0) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA - Selenium,Total(7782-49-2) X X ND 0 ND 0 _ ND 0 1 mg/L lbs NA NA NA Silver,Total(7440-28-0) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Thallium,Total(7440-28-0) X X ND 0 ND 0 - ND 0 1 mg/L lbs NA NA NA Zinc,Total(7440-66-6) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Cyanide.Total(57-12-5) X X ND 0 ND 0 ND 0 1 mg/L lbs NA NA NA Phenols,Total X X 0.024 0.044 0.024 0.044 _ 0.016 0.013 25 mg/L lbs NA _ NA NA DIOXIN 2,3,7,8-Tetra-chlorodbenzo-PDioxin (1764-01-6) NA X DESCRIBE RESULTS (testing requirements waived) GC/MS FRACTION-VOLATILE COMPOUNDS Accrolein(107-02-8) X X ND 0 ND 0 ND 0 1 �g/L lbs NA NA NA Acrylonitrile(107-13-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzene(71-43-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Bis(Ch/oro-methyl)Ether(542-88-1) X X NA NA NA NA NA NA I' 0 pg/L lbs NA NA NA Bromoform(75-25-2) X X ND 0 ND 0 ND _ 0 1 pg/L lbs NA NA NA Carbon Tetrachloride(56-23-5) X X ND 0 ND 0 ND _ 0 1 pg/L lbs NA NA NA Chlorobenzene(108-90-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Chlorodibromomethane(124-48-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Chloroethane(75-00-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2-Chloro-ethylvinyl Ether(110-75-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Chloroform(67-66-3) _ X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Dichlorobromomethane(75-27-4) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Dichlorodifluoromethane(75-71-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,1-Dichloroethane(75-34-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,2-Dichloroethane(107-06-2) X X ND 0 ND 0 ND _ 0 1 pg/L lbs NA NA NA 1,1-Dichloroethylene(75-35-4) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,2-Dichloropropane(78-87-5) X X ND0 ND _ 0 ND 0 1 pg/L lbs NA NA NA 1.3-Dichloropropylene(542-75-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Ethylbenzene(100-41-4) X _ X ND 0 - ND 0 ND 0 1 pg/L lbs NA NA NA Methyl Bromide(74-83-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Methyl Chloride(74-87-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Methylene Chloride(75-09-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,1,2,2-Tetrachloroethane(79-34-5) X X ND _ 0 ND 0 ND 0 1 pg/L lbs NA NA NA Tetrachloroethylene(127-18-4) X X ND _ 0 ND 0 ND 0 1 pg/L lbs NA NA NA Toluene(108-88-3) X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1.2-Trans-Dichloroethylene(156-60-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,1.1-Trichloroethane(71-55-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,1,2-Trichloroethane(79-00-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Trichloroethylene(79-01-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Trichlorofluoromethane(75-69-4) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Vinyl Chloride(75-01-4) X X ND _ 0 ND 0 ND 0 1 pg/L lbs NA NA NA GC/MS FRACTION-ACID COMPOUNDS 2-Chlorophenol(95-57-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA -. 2,4-Dichlorophenol(120-83-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2,4-Dimethylphenol(105-67-9) X X ND 0 ND _ 0 ND 0 1 pg/L lbs NA NA NA 4,6-Dinitro-O-Cresol(534-52-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2,4-Dinitrophenol(51-28-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2-Nitrophenol(88-75-5) X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4-Nitrophenol(100-02-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA P-Chloro-M-Cresol(59-50-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Pentachlorophenol(87-86-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Phenol(108-95-2) X X ND 0 _ ND 0 ND 0 1 pg/L lbs NA NA NA 2,4.6-Trichlorophenol(88-05-2) X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA _ NA NA GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS Acenaphthene(83-32-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA _ Acenaphtylene(208-96-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Anthracene(120-12-7) X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzidine(92-87-5) X _ X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzo(a)Anthracene(56-55-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzo(a)Pyrene(50-32-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 3,4-Benzofluoranthene(205-99-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzo(ghi)Perylene(191-24-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Benzo(k)Fluoranthene(207-08-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Bis(2-Chloro-ethoxy)Methane(111-91-1) X X ND 0 ND 0 ND 0 1 pg/L lbs Bis(2-Chloro-ethyl)Ether(111-44-4) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Bis(2-Chloroisopropyl)Ether(102-80-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Bis(2-Ethyl-hexyl)Phthalate(117-81-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4-Bromophenyl Phenyl Ether(101-55-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA _ Butyl Benzyl Phthalate(85-68-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2-Chloro-naphthalene(91-58-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4-Chlorophenyl Phenyl Ether(7005-72-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Chrysene(218-01-9) X X ND 0 ND 0 ND 0 _ 1 pg/L lbs NA NA NA Dibenzo(ah)Anthracene(53-7T3) X X ND 0 ND 0 ND 0 _ 1 pg/L lbs NA NA NA 1,2-Dichlorobenzene(95-50-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,3-Dichlorobenzene(541-73-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,4-Dichlorobenzene(106-46-7) X X ND 0 ND 0 _ ND 0 1 pg/L lbs NA NA NA 3,3-Dichlorobenzidine(91-94-1) X X ND 0 ND 0 _ ND 0 1 pg/L lbs NA NA NA Diethyl Phthalate(84-66-2) X X ND 0 ND 0 ND 0 1 pg/L - lbs NA NA NA Dimethyl Phthalate(131-11-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Di-N-Butyl Phthalate(84-74-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2,4-Dinitrotoluene(121-14-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 2,6-Dinitrotoluene(606-20-2) X X ND 0 ND 0 ND 0 1 _ pg/L lbs NA NA _ NA Di-N-Octyl Phthalate(117-84-0) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,2-Diphenylhydrazine(as Azobenzene)(122-66-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Fluoranthene(206-44-0) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Fluorene(86-73-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Hexachlorobenzene(118-74-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Hexachlorobutadiene(87-68-3) X X ND 0 ND 0 - ND 0 1 pg/L lbs NA NA NA Hexachlorocyclopentadiene(77-47-4) X X ND 0 ND 0 _ ND 0 1 _ pg/L lbs NA NA "" NA Hexachloroethane(67-72-1) X X ND 0 ND 0 __ ND 0 1 pg/L lbs NA NA NA • • Indeno(1,2,3-cd)Pyrene(133-39-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Isophorone(78-59-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA • Naphthalene(91-20-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA • Nitrobenzene(98-95-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA • N-Nitro-sodimethylamine(62-75-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA N-Nitrosodi-N-Propylamine(621-64-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA N-Nitro-sodiphenylamine(86-30-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Phenanthrene(85-01-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Pyrene(129-00-0) X X ND _ 0 ND 0 ND 0 1 pg/L lbs NA NA NA 1,2,4-Trichlorobenzene(120-82-1) X X ND _ 0 ND - 0 ND 0 - 1 pg/L lbs NA NA NA GC/MS FRACTION-PESTICIDES Aldrin(309-00-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA a-BHC(319-84-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA (i-BHC(319-85-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA y-BHC(58-89-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 6-BHC(319-86-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Chlordane(57-74-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4.-4'-DDT(50-29-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4,-4'-DDE((2-55-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA 4,-4-DDD(72-54-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Dieldrin(60-57-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA a-Enosulfan(115-29-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA (3-Endosulfan(115-29-7) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Endosulfan Sulfate(1031-07-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Endrin(72-20-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Endrin Aldehyde(7421-93-4) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Heptachlor(76-44-8) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Heptachlor epoxide(1024-57-3) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Toxaphene(8001-35-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA GC/MS FRACTION-PCBs PCB-1242(53469-21-9) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1254(11097-69-1) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1221(11104-28-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1232(11141-16-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1248(12672-29-6) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1260(11096-82-5) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA PCB-1016(12674-11-2) X X ND 0 ND 0 ND 0 1 pg/L lbs NA NA NA Duvaltex (US), Inc. WWTP Totals 2017 Average Maximum #of BOD Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan 2.20049 0.07027 3.75500 15.98380 0.30421 6.30000 20 Feb 2.26583 0.06154 4.41500 14.86069 0.23141 7.70000 20 Mar 2.38188 0.06927 4.12273 19.64946 0.31414 7.50000 22 Apr 3.43093 0.10008 4.11053 20.56580 0.27707 8.90000 19 May 3.75157 0.10699 4.20455 27.75093 0.47535 7.00000 22 Jun 1.80802 0.05305 4.08636 7.57644 0.11798 7.70000 22 Jul 1.66079 0.06671 2.98500 7.12463 0.18176 4.70000 20 Aug 1.37323 0.08607 1.91304 10.61649 0.28288 4.50000 23 Sep 1.86472 0.09126 2.45000 13.27316 0.25262 6.30000 20 Oct 1.65118 0.09922 1.99545 14.93554 0.37309 4.80000 22 Nov 3.00420 0.07738 4.65500 36.21895 0.25850 16.80000 20 Dec 4.30336 0.08102 6.36842 26.65881 0.21310 15.00000 19 MAX 4.30336 6.36842 36.21895 16.80000 249 2017 Average Maximum #of COD Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) 1 mg/L Analysis Jan 45.41630 0.07027 77.50000 253.71114 0.30421 100.00000 4 Feb 52.09090 0.06154 101.50000 264.40444 0.23141 137.00000 4 Mar 46.21957 0.06927 80.00000 238.41341 0.31414 91.00000 4 Apr 61.97425 0.10008 74.25000 205.65798 0.27707 89.00000 4 May 68.70448 0.10699 77.00000 340.94003 0.47535 86.00000 5 Jun 41.81161 0.05305 94.50000 124.96206 0.11798 127.00000 4 Jul 53.55134 0.06671 96.25000 168.26250 0.18176 111.00000 4 Aug 60.15386 0.08607 83.80000 219.40739 0.28288 93.00000 5 Sep 57.65417 0.09126 75.75000 233.86044 0.25262 111.00000 4 Oct 55.27504 0.09922 66.80000 304.93392 0.37309 98.00000 5 Nov 50.66166 0.07738 78.50000 204.80955 0.25850 95.00000 4 Dec 0.06757 0.08102 0.10000 0.26659 0.21310 0.15000 2 MAX 68.70448 101.50000 340.94003 137.00000 49 2017 Average Maximum #of TSS Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan 15.45180 0.07027 26.36750 253.71114 0.30421 100.00000 20 Feb 10.79026 0.06154 21.02500 94.56801 0.23141 49.00000 20 Mar 7.75491 0.06927 13.42273 68.11812 0.31414 26.00000 22 Apr 10.06876 0.10008 12.06316 64.70139 0.27707 28.00000 19 May 15.18069 0.10699 17.01364 172.05578 0.47535 43.40000 22 Jun 4.96752 0.05305 11.22727 25.18920 0.11798 25.60000 22 Jul 4.84927 0.06671 8.71579 24.25405 0.18176 16.00000 20 Aug 4.66275 0.08607 6.49565 30.19801 0.28288 12.80000 23 Sep 9.21325 0.09126 12.10500 84.27403 0.25262 40.00000 20 Oct 13.20192 0.09922 15.95455 133.79754 0.37309 43.00000 22 Nov 14.64670 0.07738 22.69500 134.74313 0.25850 62.50000 20 Dec 26.04064 0.08102 38.53684 431.87272 _ 0.21310 243.00000 19 MAX 26.04064 38.53684 431.87272 243.00000 249 True Elkin, Inc. WWTP Totals 2017 Average Maximum #of Sulfides Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan NA 0.07027 <0.100 NA 0.30421 <0.100 2 Feb NA 0.06154 <0.100 NA 0.23141 <0.100 2 Mar NA 0.06927 <0.100 NA 0.31414 <0.100 2 Apr 0.16981 0.10008 0.08000 0.25435 0.27707 0.11000 2 May NA 0.10699 <0.100 NA 0.47535 <0.100 2 Jun NA 0.05305 <0.100 NA 0.11798 <0.100 2 Jul NA 0.06671 <0.100 NA 0.18176 <0.100 2 Aug NA 0.08607 <0.100 NA 0.28288 <0.100 2 Sep NA 0.09126 <0.100 NA 0.25262 <0.100 2 Cct NA 0.09922 <0.100 NA 0.37309 <0.100 2 Nov 0.04843 0.07738 0.07500 0.21573 0.25850 0.10000 2 Dec 0.00642 _ 0.08102 0.00950 0.02490 0.21310 0.01400 2 MAX 0.16981 0.08000 0.25435 0.11000 24 2017 Average Maximum #of Phenols Lb/Day _ Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan 0.00762 0.07027 0.01300 0.03300 0.30421 0.01300 2 Feb 0.00385 0.06154 0.00750 0.01931 0.23141 0.01000 2 Mar NA 0.06927 <0.0100 0.00000 0.31414 0.00000 2 Apr 0.01336 0.10008 0.01600 0.04393 0.27707 0.01900 2 May 0.00714 0.10699 0.00800 0.04364 0.47535 0.01100 2 Jun 0.00553 0.05305 0.01250 0.01378 0.11798 0.01400 2 Jul 0.00807 0.06671 0.01450 0.03640 0.18176 0.02400 2 Aug 0.00790 0.08607 0.01100 0.02597 0.28288 0.01100 2 Sep NA 0.09126 <0.0100 0.00000 0.25262 0.00000 2 Oct NA 0.09922 <0.0100 0.00000 0.37309 0.00000 2 Nov NA 0.07738 <0.0100 0.00000 0.25850 0.00000 2 Dec 0.00646 0.08102 0.00955 0.02027 0.21310 0.01140 2 7/25/17 ppa 0.01016 0.11071 0.011 0.01016 0.11071 0.011 1 MAX 0.01336 0.01600 0.04393 0.02400 25 2017 Average Maximum #of Chromium Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan 0.00956 0.07027 0.01630 0.05433 0.30421 0.02140 2 Feb 0.00786 0.06154 0.01530 0.02955 0.23141 0.01530 2 Ma- 0.00373 0.06927 0.00645 0.01992 0.31414 0.00760 2 Apr 0.00864 0.10008 0.01035 0.03145 0.27707 0.01360 2 May 0.01424 0.10699 0.01595 0.06863 0.47535 0.01730 2 Jun 0.00503 0.05305 0.01135 _ 0.01526 0.11798 0.01550 2 Jul 0.00404 0.06671 0.00725 0.01138 0.18176 0.00750 2 Aug 0.00316 0.08607 0.00440 0.01487 0.28288 0.00630 2 Sep 0.00762 0.09126 0.01000 0.02446 0.25262 0.01160 2 Oct 0.00468 0.09922 0.00565 0.02740 0.37309 0.00880 2 Nov 0.01634 0.07738 0.02530 0.05609 0.25850 0.02600 2 Dec 0.00270 0.08102 0.00400 0.00889 0.21310 0.00500 2 7/25/17 ppa 0.00508 0.11071 0.00550 0.00508 0.11071 0.00550 1 MA) 0.01634 0.02530 0.06863 0.02600 25 True Elkin, Inc. WWTP Totals 2017 Average Maximum #of Fecal Coliform col/100mL Flow(MGD) 1, col/100mL Flow(MGD) Analysis Jan <2.5 0.07027 <3 0.30421 2 Feb <1 0.06154 <1 0.23141 2 Mar <1 0.06927 <1 0.31414 2 Apr <1 0.10008 <1 0.27707 2 May 0.75 0.10699 1 0.47535 2 Jun <1 0.05305 <1 0.11798 2 Jul <1 0.06671 <1 0.18176 2 Aug 12.5 0.08607 _ 23 0.28288 2 Sep 3.25 0.09126 6 0.25262 2 Oct <1 0.09922 <1 0.37309 2 Nov <1.5 0.07738 <2 0.25850 2 Dec 6.25 0.08102 12 0.21310 2 MAX 12.50000 23.00000 24 2017 Average Maximum #of Chlorine Residual pg/L Flow(MGD) Lbs pg/L Flow(MGD) Lbs Analysis Jan <25 0.07027 <25 0.30421 20 Feb <25 0.06154 <25 0.23141 20 Mar <25 0.06927 <25 0.31414 21 Apr <25 0.10008 <25 0.27707 19 May <25 0.10699 <25 0.47535 22 Jun <25 0.05305 <25 0.11798 22 Jul <25 0.06671 <25 0.18176 20 Aug <25 0.08607 <25 0.28288 23 ' Sep <25 0.09126 <25 0.25262 20 Oct <25 0.09922 <25 0.37309 22 Nov <25 0.07738 <25 0.25850 20 1 Dec <25 0.08102 <25 0.21310 19 MAX <25 0.00000 <25 0.00000 248 2017 Average Maximum it of Total Nitrogen Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Jan 0.32838 0.07027 0.56 1.42170 0.30421 0.56 1 Feb 0.58030 0.06154 1.13 2.18227 0.23141 1.13 1 Mar 0.41046 0.06927 0.71 1.86135 0.31414 0.71 1 Apr 0.43431 0.10008 0.52 1.20238 0.27707 0.52 1 May 0.60713 0.10699 0.68 2.69755 0.47535 0.68 1 Jun 1.07143 0.05305 2.42 2.38271 0.11798 2.42 1 Jul 0.50106 0.06671 0.9 1.36517 0.18176 0.9 1 Aug 1.27138 0.08607 1.77 4.17852 0.28288 1.77 1 Sep 2.43713 0.09126 3.2 6.74629 0.25262 3.2 1 Oct 0.94393 0.09922 1.14 3.54949 0.37309 1.14 1 Nov 0.55538 0.07738 0.86 1.85527 0.25850 0.86 1 Dec 0.43951 0.08102 0.65 1.15596 0.21310 0.65 4 MAX 2.43713 3.20000 6.74629 3.20000 15 1 True Elkin, Inc. WWTP Totals 2017 Average I Maximum #of Total Lb/Day Flow(MGD) mg/L Lb/Day Flow(MGD) mg/L Analysis Phosphorous Jan 1.34871 0.07027 2.3 5.83914 0.30421 2.3 1 Feb 1.38657 0.06154 2.7 5.21427 0.23141 2.7 1 Mar 1.50311 0.06927 2.6 6.81623 0.31414 2.6 1 Apr 1.92098 0.10008 2.3 5.31820 0.27707 2.3 1 May 1.69640 0.10699 1.9 7.53728 0.47535 1.9 1 Jun 1.06257 0.05305 2.4 2.36302 0.11798 2.4 1 Jul 1.55887 0.06671 2.8 4.24721 0.18176 2.8 1 Aug 1.65207 0.08607 2.3 _ 5.42972 0.28288 2.3 1 Sep 1.67553 0.09126 2.2 4.63808 0.25262 2.2 1 Oct 2.15282 0.09922 2.6 8.09533 0.37309 2.6 1 Nov NA 0.07738 <0.010 NA 0.25850 <0.010 1 Dec 1.14949 _ 0.08102 1.7 3.02329 0.21310 1.7 1 MAX 2.15282 2.80000 8.09533 2.80000 12 2017 Average Maximum #of Temp °C Flow(MGD) °C Flow(MGD) Analysis Jan 6.1 0.07027 10.2 0.30421 _ 20 Feb 7.5 0.06154 11.3 0.23141 20 Mar 9.3 0.06927 14.6 0.31414 21 Apr 15.4 0.10008 17.7 0.27707 19 May 18.7 0.10699 21.5 0.47535 22 Jun 21.9 0.05305 24.4 0.11798 22 Jul 24.6 0.06671 25.9 0.18176 20 Aug 23.9 0.08607 26.3 0.28288 23 Sep 20.4 0.09126 22.2 0.25262 _ 20 Oct 16.6 0.09922 22.5 0.37309 22 Nov 9.7 0.07738 15.0 0.25850 20 Dec 4.9 0.08102 8.3 _ 0.21310 i 19 MAX 16.6 22.5 122 (Jan-Mar/Oct-Dec) MAX 24.6 26.3 126 (April-Sept.) 2017 Minimum Maximum #of pH pH Flow(MGD) pH ' Flow(MGD) Analysis Jan 7.3 0.02964 7.4 0.30421 20 Feb 7.1 0.06752 7.4 0.23141 20 _ Mar 7.1 0.13732 7.3 0.31414 21 Apr 7.2 0.17579 7.6 0.27707 19 May 7.3 0.02766 7.5 0.47535 22 Jun 7.3 0.03991 7.6 0.11798 22 Jul 7.4 0.08023 7.5 0.18176 20 Aug 7.2 0.12271 7.4 0.28288 23 Sep 7.2 0.01407 7.4 0.25262 20 Oct 7.1 0.09969 7.3 0.37309 22 Nov 7.2 0.04375 7.3 0.25850 20 I Dec 7.0 0.03459 7.2 0.21310 19 MAX 7.0 7.6 248 Notes: Prior to calculating average values,non-detect values were changed to 1/2 of the laboratory reporting limit. Highlighted cell =Maximum value for analyte. YARN MANUFACTURING RAW MATERIALS RECEIVING -EXTRUSION ► SAMPLE WARPING WEAVING OFFSITE FACILITIES/VENDORS -TEXTURIZING FINISHING -FLAME RETARDANT -SOIL REPELLENCY -LATEX COATING -NEEDLING -DRYING V INSPECTION WAREHOUSE `o a DISTRIBUTION NPDES WASTEWATER APPLICATION LL PRODUCTION FLOW SCHEMATIC DUVALTEX (US), INC. - ELKIN FACILITY 3 304 EAST MAIN STREET ELKIN, NORTH CAROLINA •g2923 South Tryon Street-Suite 100 hart hickman Charlotte,North Carolina 28203 704586-u007(p)704-586-0373(f) SMARTER ENVIRONMENTAL SOWTIONS License#C-1269/#C-245 Geology g DATE: 5-23-18 REVISION NO.0 JOB NO.VCP-002 FIGURE NO. 1-3 f DUVALTEX(US),INC.TRUE ELKIN,INC. BIG ELKIN CREEK PUMP ELKIN FACILITY WATER USAGE(GPD) MAY 16,2018 152,000 A ' 18,0008 NOTE: WEAVE II SETTLING POND EVAPORATION VALUES ROUNDED TO NEAREST 100 133,200 C 2017 USAGE DATA 111 W ATER FILTRATION PLANT USAGE BASED ON 365 DAYS ANNUALLY 133,200 C ' I TOWN OF ELKIN POTABLE WATER ICLEARWELL I 8,200 E 1 8,200 E 200 F FACILITY DOMESTIC WATER USAGE MUNICIPAL WWT 133,200 C 0 FIRE PROTECTION ONLY USED IN EMERGENCY I V 1,000 D LARGE RESERVOIR -- EVAPORATION ELKIN FACILITY NPDES WASTEWATER APPLICATION r 2017 SURFACE NC LOCATION ON FLOW WATER SOURCEAREA(FTr) EVAPORATION DIAGRAM (GALIDAY) COMMENT RATE(IN/DAY) ELKIN CREEK A 151,654 2017-ANNUAL WATER USE REPORT WEAVE II RESERVOIR EVAPORATION 207,258 0.1425 B 18,410 WATER FILTRATION PLANT PRODUCTION C 133,244 LARGE RESERVOIR EVAPORATION 11,310 0.1425 D 1,005 CITY WATER E 8.189 AVERAGE AS INVOICED 132,200 C 8,000 CITY WATER F 187 AVERAGE AS INVOICED FILTER WATER CONSUMED-BOILER G 36,794 FROM MONTHLY REPORT-ASSUME 50%BOILER RETURN CONDENSATE FLASH EVAPORATION H 15,085 ASSUME 8%NORMAL FLASH LOSSES+33%VENT FOR OVERSIZD BOLIER BOILER ROOM ANCILLARY EQUIPMENT I 2,880 ASSUME 2 GPM BOILER TOTAL 54,759 WWiP EVAPORATION/LOSS J 28,150 INFLUENT/EFFLUENT METERING DISCHARGE TO YADKIN RIVER K 80,238 2017-ANNUAL WATER USE REPORT ENTERING FABRIC MOISTURE(%BY WEIGHT) 60% ENTERING FABRIC COATING(%BY WEIGHT) 23% EXITING FABRIC MOISTURE(%BY WEIGHT) 3% EXITING FABRIC COATING(%BY WEIGHT) 12% ANNUAL FABRIC PRODUCTION(YARDS)-COATED 584.790 21 ANNUAL FABRIC PRODUCTION(YARDS)-POLYBINDER 692,827 130 ANNUAL FABRIC PRODUCTION(YARDS)-SCOUR&DRY 2,644,992 497 37,000 G 15,100 H TOTAL ANNUAL PRODUCTION 3,922,609 L 648 STEAM PLANT OPERATIONS EVAPORATION 21,900 0 BLOW DOWN 2,9001 95.200ii v 19,000 11.900 FINISHING OPERATIONS ; TENTERS 65�►EXHAUST NPDES WASTEWATER APPLICATION LL 95,200 WATER USE SCHEMATIC I 113,550 DUVALTEX (US), INC. - ELKIN FACILITY 3 125,450 304 EAST MAIN STREET 45,200 ELKIN, NORTH CAROLINA .m WASTEWATER TREATMENT PLANT EVAPORATION/LOSS . 82923 South Tryon Street-Suite 100 u 80,200 K hart ► hIC man Charlotte,North Carolina 28203 , 704-586-0007(p)704-586-9373(1) YADKIN RIVER SMARTER ENVIRONMENTAL SOLUTIONS License#C-1269/#C-245 Geolog c DATE: 5-25-18 REVISION NO.0 li JOB NO.VCP-002 FIGURE NO. 1-4 r 4 g 3 PROCESS 1-T 3-E 3-B 1-U INFLUENT SCREENING PRE-AERATION = AERATION SETTLING (EQ BASIN) BASIN (2 SECONDARY CLARIFIERS) A I V V 5-A 2-F AERATION DISINFECTION DIGESTION (CHLORINE) V 5-H DRYING 2-E BEDS DECHLORINATION TREATMENT UNIT CODE SIZE RETENTION TIME FLOW(MGD) V V 1-T SCREENING 8 SCREENS RATED CAPACITY=3.1 NA 0.0804 MGD EACH 5-P 4-A 3-E PRE-AERATION 2.9 MG 36 DAYS 0.0804 LAND DISCHARGE TO 3-B AERATION BASIN 2.1 MG 72 HR 0.07034 APPLICATION SURFACE WATERS 1-U SETTING/AEROBIC 0.376 MG EACH 13 HR 0.7034 DIGESTION 5-A AEROBIC DIGESTION 0.040 MG 10 DAYS 0.004 5-H DRYING BEDS 6 BEDS 35'X 82'X 2'EACH 12-36 WKS 0.003 5-P LAND APPLICATION 80.6 ACRES NA 0 OUTFALL 001 2-F DISINFECTION 0.086 MG 26 HR 0.0804 2-E DECHLORINATION 4.0 MG NA 0.0804 4-A DISCHARGE TO SURFACE WATERS 20 INCH BANK OUTFALL PIPE NA 0.0804 2 NPDES WASTEWATER APPLICATION LL WASTEWATER TREATMENT PLANT SCHEMATIC 3 PROJECT DUVALTEX (US), INC. - ELKIN FACILITY 5 304 EAST MAIN STREET 0 ELKIN, NORTH CAROLINA • 2923 South Tryon Street-Swte till I g hart hickman Charlotte,North Carolina 28203 Z 704-586-011117(p)704-586-0373(0 SMARTER ENViRONMENTAI.SOWTIONS License#C-1269/#C-245 Geolog DATE: 5-23-18 REVISION NO. 0 JOB NO.VCP-002 FIGURE NO. 1-5 i Duvaltex (US) , Inc . EPA ID# NC0005312 Appendix A Production Data Production Data for NPDES Effluent Permit Calculations Subpart C -Low Water Use Processing Subcategory Total Operating Level Year Average pounds/day Max. pounds/day _ Pounds/day 2015 _ 1,037 3,399 752 2016 1,123 3,843 _ 612 2017 1,251 3,739 735 Subpart D-Woven Fabric Finishing Subcategory Total Operating Level Year Average pounds/day Max. pounds/day Pounds/day 2015 22,846 37,057 14,687 2016 22,670 36,100 13,664 2017 21,798 37,052 13,594 Average pounds/day is the annual average for actual production days. Max. pounds/day is the actual maximum production day for the year. Operating Level pounds/day is the calendar year average. Duvaltex (US), Inc . EPA ID# NC0005312 Appendix B Wet Tests North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test LC50/Acute Toxicity Test Effluent Concentration: 1.9% Date Passed Failed % Reduction 2/15/2017 X 3.0 5/17/2017 X 1.8 8/9/2017 X 2.6 11/15/2017 X 8.3 <m .Fria. (664)07T-6542.1AX(884)877-8938 P.O.Box 16414.Creenvlle SC 29606 4 Craftsman Court,Greet,SC 29650 Ceriodaphnia dubia Survival and Reproduction Test EPA-821-R-02-013 Method 1002 Client: TRUE TEXTILES Facility:ELKIN NPDES#:NC0005312 Test Date: 15-Feb-17 Laboratory ID#:T48617 Test Reviewed and Approved By: Robcrt W.Kelley,Ph.D. Farhad Rostamp/our QA/QC Officer Laboratory Director Certification#E87814 SCDHEC Certification#23104 Test results presented in this mat conbrm to all requirements of NELAC,conducted tinder NELAC Certification Number E87819 Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# #22 Page 1 of 6 Effluent Toxicity Report Form-Chronic Pass/Fall and Acute LC50 Date 24-Feb-17 Facility: TRUE TEXTILES WWTP NPDES#NC0005312 Pipe# 001 County Surry J Laboratory Perform ing est: ETT Environmental,Inc. Comments Signature of Ope ' Respo /rm Signature of Laboratory Supervisor MAIL ORIGINAL TO Environmental Sciences Branch Div.of Water Quality N.C.DENR 1621 Mail Service Center Raleigh,North Carolina 27699-1621 North Carolina Cerlodaphnla Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t= -0.8015 Critical Value= 2.508 CONTROL ORGANISMS1 2 3 4 5 6 7 8 9 10 11 12 %Reduction= -3.0% A Young Produced 18 19 19 18 18 19 17 20 22 21 21 18 %Mortality Avg.Repral. Adult (L)Ive (D)ead L L L L L L L _L L L L L 0% 19.2 Control Control Effluent% 1.9% 0% 19.8 Treatment 2 Treatment 2 Control CV TREATMENT 2 ORGANISMS1 2 3 4 5 8 7 6 9 10 11 12 8.0% #Young Produced 23 17 19 19 17 20 23 21 21 20 19 18 %3r0 Stood PASS FAIL Adult (L)Ive (D)ead L L L L L L L L L L L L 100% I X I 1 Complete This for Either Test Test Start Date Collection(Starti Dale 15-Feb-17 pH 1st serrate 1st earn a 2nd sample Sample 1 13-Feb-17 serape 2 15-Feb-17 Control 7.5 7.9 7.7 7.6 7.7 7.9 ,Sande Text(Duration) Treatment 2 6.9 7.9 7.7 7.7 7.6 8.0 Grab Comp Duration 1st 2nd Sample 1 X 24hrs. lox Too Sample 2 X 24hrs. Dilution Sample Sample start end sari end stall end 0.0. 1st sarpte 1st earn in 2nd a= to Hardness(mg/L) 45 1 Control 7.6 7.5 7.4 8.4 NE Spec.Cord (pmhos) 184 187 181 Treatment 2 7.7 7.9 7.7 8.4 PP Chlorine(rn9lL) <.05 <.05 Sample Temp.at receipt CC) 0.0 0.4 not frozen LC50/Acute Toxicity Test (Mortality expressed as%,combining replicates) Concentration 1. Mortality / start/end etarVend LC50= % Method of Determination IIIcontra 95%Confidence Unfits Moving Average Probit High Conc. % F17 Spearman Kerber Other pH D.O. Organism Tested Ceriodaphnia dubia I DEM Form AT-1 Page 2 of 6 STATISTICAL ANALYSIS RESULTS Facility: TRUE TEXTILES NPDESM NC0005312 Sample ID: WWTP Erna T45617 Date: 15-Feb-17 Laborato2: I I 1 F:nairunmen131.Fni. Certification#:NCO22 Exp.Date: 11/1/2017 Survival Data 7 Day Survival Test Used: FISHERS TEST Control 100% Test Statistic: P= 1.000 Effluent 100% Critical Value. P 0.01 PASS:The effluent does not reduce survival of the test organisms. Reproduction Data Raw Data Test for Normality Mean young/female Std.Dev. Test Used: Shapiro-Wilks Test: Control 19.2 1.53 Effluent 19.8 2.01 W: 0.953 Critical Value: 0.884 Analysts for Differences in Reproduction Test for Homogeneity of Variance Test Used: Equal Variance t Test. Test Used: F Test Calculated t -0.80 F= 1.72 Critical Value 2.51 Critical Value= 5.32 The data are homogeneous in variance PASS:The effluent is not chronically toxic. Page 3 of 6 Co wJ 3 N w 0 la ffig v 7 L) _ O m 00 ' u m R H o4n e C 0 0 S u V u = EE 0wo .N rz � N :-' Q U .1 .° z � yt - 8rmA0d, 0EiE " Et c :4 w o 1 : oxa o • w o. E 8 . Eo ; kK ?.g t dE Ewo o fS OW $ :/ �6OCCr • a 0 > Ea3.Z • E ] oeC '" i waVKi . z ° )- 154 % siiagel r334nWn " ^ • liNl WO ni N 40U 2 _2oemo ; C N C CO CO 0 CO of a) rr 0 0 0 0 0 0 n O Nx 0 0 0 0 0 0 0 0 0 n CA Of n o n O Of CO 0 0 0 0 0 0 0 0 N N N r r r r N N N N N r r rs. M 7 ‹ r - r m LL _ m (NV --f ys C m n .- O) 0 Of O O. 0 .- 0 CO ^ CO CO 0 n W " 0 0 Q) 0 n n n (-4 N a o • II a T i F•- `o 0 to U o t l c 3 n 2 '.... '- '4. o N n f n 0 0 0 0 0 b n 0 O N 0 in CO 0 0 n COIn n 0 n 0 ti, et * • ♦ ♦ ♦ i + ♦ n < < e N N N 0 ,t0) a v) e a in at n n e n e v n • r ♦ i i i v o K Q v o 1 o C V o Z 2 a n g o < Fa U a e Cr' N CD I N Q Q o N N N N w l aa o m a z • Z z z z Z Z z ZZZZZZZZ c r Nr , 0 O N0 Is CO 0 0 r N f7 V N 0 n CO Or 0 r N OS V 0 0 n CO m 0 r N n V 0 0n 0 0 0 r r r r r r r N N U O. U o— Q U P )'+ N M N n n n N t;t n (') 17m N Com)N c,M (h N N N 0 0 0 0 0 0 0 0 F Z H N r ri (c�V N ry c� N N N N N N N N N (V N N N N N a ..i o a et et 4 VI K 0 S to 1 ��. n 0 b R - C') Ol N- CD v I- U)n C (y O 3 b cto > >� xa>af- m> cco> v , z o ET,I' CHAIN OF CUSTODY RECORD tea:::s::r.;t:,qi? -.k .{s+!~2r+ci- _E IPage of PO Box 1 641 4,8866NvcLi.t,SC 29606.74 t 4 (864)077-6942, 18001 891-2335 f4n:18641 877 6938 91-1I1.ptoa Ao08636,4 CBAR•.eSN CT, 986(8,SC 20650 W W W.ttTENVIR0.elt NTAL.Caw Client: ' f " Program Containers Preservative Parameters Facility: 1 ELICk'l•-' whole Emuent T°nicily State: it.- _ NPDES a: NG GOO_c 3/ 2 Acute Chronic Tett Ore*atsms p tt o29C2,vCM 23 2 (Composite only) (Grab or Composite) Q a' .- U (-) ° e . LU o u [ r m u " c '-t1250J ! a E =_ a _, t V 3 ' e -HCL m 3 — `L i0 i' s u e ' 3 " U y 4 3-tut03 a .P _g :a Ti `a a s 5 "n 612' . € E c w . g 4•i.Ote = 2 o o E eR ,- °) o `v ? ¢ SAMPLE ID �? CompmleStutDuia Time 0 ° tL o o o ` s-zee u chi v a ,E j,> .w w ul ��Mt�+}} Sate* Time °Wetted by V Tin vi z a F. V_> a.ow, ¢ ¢ v U Ci o u; 7 x U P 3 M Chemical Analysis&Other u 0.11-to j"C �2-13•-/7 071.4.4,t-17 :571-5- 14A-"(717/ i IX ''-i- V.434 1 /- 5'`lo t/r la f-t c•nJ t,_,../\ 9$67 1?R w to _ . 0, Special Instructions Sample Custody Transfer Record Secure 1 Receipt Sample I Date Time ` i' quished y/Organization Received By/Organization Area Temp°C Preserved? g.-IN�7o72 , ,u( zr 2 i15-11e1 C855 Fedx_ V L .4 • - OODria+�-t7 ` COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional: I sample each hour for 24 how-s.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum I sample every4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit ___ , Eimaims CHAIN OF CUSTODY RECORD Po 9411 MfiMMLLk.a0 11960e-741.1 Of I ea.1N 977-I94II. (ICO!091-3320',AX:ta641!IT.?6989 1141144411 A94414.1 4 CNMr9N4.4 U.°wRIA•a 29690 WWW.CPrOM414444+TA1-40M 71u C Program c6ltals.rs 1P.......stirs Parameters I___. ____________, paedlity: Ci 45 \ _ i anima xell .cT.eaq FState:tV C, NPDltB fl: —0047,,,5-3 ---"IIm, � Tat. A I S I E V ( wy) (OnborCmposite) .i g' c $ : o AZ CG7 .5 t�HL7. o & t-Xsos 0 SAMPLE IR v r��rssrsc.I met g �t oZ ° w 8 zw E E w $ ,� Gear Dr. rim Gelded V en a, 1 > U R - y i Chemical Mal Ia&Other I •••-11 .r:r1 24647 74741firearalllinieSaMillinir 1111111111111EMEMM 7 13, 4. 111111.=111111 IIN MINN 0 111,1111 I 111111 — . re*Custody Transfer Record Secure Date nine e',. ...ti- ,. ; '/ls �. .. ' .tics Ares I rarm.mis dr, Thum°C coed? irdimilIV . _ 24 a O4a f,A 2IR FIT' 0.4 COMPOSITESAWING PROCEDURES TEMPERTUREMONT1)RINGPROCEDURES HOLD liMEPROCEDURES Caine tanples mast be collected over a 24 boar period. Sample temperature during collection and transport mutt be between For LD7aC[t38 the sample must first be used within 36 horns Time Proportional:(sample each boar Sar 24 hours.Equal voila 0.0 end 6.0'C.Samples must not be froom Use water ice in waled her of 1. or at minimum 1 sample every 4 bolus over 24 boors, collection bm sed aftetloo noes sample). Sample may not be used after 72 hams from sample collection. Plow RamorsiaoaL N err raetrnGioen 1 NPDES permit EI0. (664)077-6942 .rAJ((884)6776938 PO Box 16414,Greenville SC 29606 4 Craftsman Caurt,Greer,SC T80:>D Ceriodaphnia dubia Survival and Reproduction Test EPA-821-R-02-013 Method 1002 Client: True Textiles Facility:ELKIN NPDES#:NC0005312 Test Date: 17-May-17 Laboratory ID#:T49328 Test Reviewed and Approved By: Robert W.Kelley,Ph.D. Farhad Rostampour QA/QC Officer Laboratory Director nelac Certification#E87819 SCDHEC certification#23104 Test results presented in this report conform to all requirements of NELAC,conducted under NELAC Certification Number E87819 Florida Dept of Health.Included results pertain only to provided samples. NCDENR Certification# 022 Page 1 of 6 Effluent Toxicity Report Form-Chronic Pass/Fail and Acute LC50 Date 24-May-17 Facility: True Textiles WWTP NPDES#NC0005312 Pipe# 001 County: Sorry Laboratory Performing Test: ETT Environmental,Inc. Comments X Signature of Operator• R p. : .le .e Signature of Laboratory Supervisor MAIL ORIGINAL TO Environmental Sciences Branch Div.of Water Quality N.C.DENR 1621 Mail Service Center Raleigh,North Carolina 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Teat Chronic Test Results Calculated t= 0.4674 Critical Value= 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 %Reduction= 1.8% I Young Produced 24 23 20 21 26 26 25 26 24 23 24 19 %Mortality Avg.vg Reprod Adult (Leve (D)ead L L L L L L L L L L L L 0% 23.4 Control Control Effluent% 1.9% 0% 23.0 Treatment 2 Treatment 2 Control CV TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 10.0% r #Young Produced 25 26 22 19 21 22 24 21 24 24 24 24 %3rd Brood PASS FAIL Adult (L)ive (D)ead L L L L L L L L L •L L L 100% , X I Complete This for Either Test Test Start Date aoulectcn tStartl Date 17-May-17 pH 1st sample 1st sample 2nd sample Sample 1 15-May-17 Sample 2 17-May-17 Control 7.5 7.7 7.4 7.6 7.6 7.6 Same Twee lDuradonl Treatment 2 7.5 7.7 7.7 7.5 7.6 7.4 Grab Duration 1st 2nd Sample 1 X 24hrs. Tox Tox Sample 2 X 24hrs. Dilution Sample Sample r start end star end start end D.O. 151 sample 1st sample 2nd sample HAM/Wss(mg/L) 48.0 Control 7.6 8.5 8.1 8.4 8.3 8.0 Spec.Coad (pmhos) 184 178 182 Treatment 2 7.8 7.8 8.2 8.9 8.7 8.2 chionne lrng&L) <.05 <.05 Sample Terryat receipt(-C) 0.6 0.8 LC50/Acute Toxicity Test (Mortality expressed as%.corntanmg repficales) Concert-aeon Mortality start/end start/end LC50= % Method of Determination Control 95%Confidence Lmts Moving Average Probit ME III III High Conc. Spearman Kerber Other pH D.O. Organism Tested Ceriodaphnia dubia I DEM Form AT-1 Page 2 of 6 STATISTICAL ANALYSIS RESULTS Facility: True Textiles NPDESM NC0005312 Sample ID: WWTP erre T45328 1Date 17-May-17 Laboratory: I I 4 I nia1/nn.,ut:,I.Inc. _Certification k:NCO22 Exp.Date: II/12017 1 s urvival Data 7 Day Survival Test Used: FISHERS TEST Control 100% Test Statistic: P= 1.000 Effluent 100% Critical Value: P= 0.01 PASS:The effluent does not reduce survival of the test organisms. Reproduction Data Raw Data Test for Normality Mean young/femak Std Dev Test Used: Shapiro-Wilks Test: Control 23.4 2.35 Effluent 23 0 2.00 W 0.937 Critical Value: 0.884 Analysis for Differences in Reproduction Test for Homogeneity of Variance Test Used Equal Variance t Test. Test Used: F Test Calculated t- 0.47 F 1 38 Critical Value= 2.51 Critical Value— 5 32 The data are homogeneous in variance PASS:The effluent is not chronically toxic. Page 3 of 6 S N • o �o f O ¢ --=.'"'''' ' '153; M 8 ; A L f a U LL E E C) N N - O 251.:::- ' ' O C) U U7 O N b V O O r r T 51. o U zln a sI - N o d i g `o q; E g E ._ s 0 U E t 1. e . O O w • . q 2 E O d v w U O w E E Yi t t r E E a K w 3 o Z : c 4I" y.4 f: i0 b t ° n n r• e mii> > a 7. e E D ` E o 5 , C Y ■ m a w 6 0 0 .9 S .� i2 $ e � e U ^ c c � t g o 4 0 �. a sn_z v m H ar w r.z z r A rG iR r r = a as > r o C < G O (0 N (1:3 M N NOO co r N T 0 0 0 0 0 0 0 0N N N N N N NN .- N g N m N N NQ .N- N N N V o 0 n d c C To To O3 I-- 171 . . -r a) 0 m v v co m 0 N N cn ti a M N C) O M N N O < V C) N O O D N .- a N M N N to n n N m a m a Y•- Io CI )o U c N n V If) N Y w n n m m 0, F2 m m n n n n 4 N .- m m � n Ip CO n m m 00 ¢ ¢ *0. N N N CC C M O YI Cr, h ' .g : N O ± : M 0 0 0. • a a • a CC F▪ o LL d D d m o -' e o " E a O r N w N 3 S -- ..- N N a d O U , v r d d d d d d d d d 4 Q d d d d d Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z 0.101 .0 0) CO n C) O. O .- N M < V) CO n CO Ci O .- N M V m m N. N A O .- N M Q I[) CO n C) T O N N V O E e U U P. `� q. y� ,� 000000C>0 `� n n s5 ,m Y u) N r r5 v) n n . N „ Ifj Il) ,Aj th 4) lA ui tt) h m V 2 l T O °n = O? 1- 2 Y it �i < n M R Cr, f7 il N • g 4 c rJO-)H2 W XZ $ CJ a ,2 a z O u l ETriii CHAIN Crr, CUSTODY RECORD .�a, 'Page - of C PO BOx 16414, ORCNVllt.t. BC 29606.7414 15641 B77-6942. (90011191-2325 F4x:1854)577 6936 8HipP.N0 AODRta4: 4 CRAFTSMAN CT,OR[(R,SC 29650 W W W.tTT[Nv,RD NMCNTAI.cc M Client: -- Th _., 1 / �Y�l 110 i` :NC_ Program Containers Preservative Parameters Facility: Pi tk} State: -PVC. NPDES it: [l_ l� Whole Toxicity Acute Chronic Tat Ovictetims 0 CI RU 0 < u E U (Composite only) (Crab or Composite) Q ,1 u .e o o D C 3 :ij j .q a °' _ ; c _ _ DIZ 3 01-41 `z' ' m E• u o 2-3:11C a ° m _ £ sui tj F E CL U .c� 03 .� L b �„ y ° L� = . c ,,_ m I 4.N°OFF g o t E S o lE ix o ¢ SAMPLE ID c? cee :e�s/,.,l>.,[ Time s c c v o o i2 b o ^ s- n. u u s s v c W : 'c w .mpk c°aezo°e Dalt Time Collected by Li rn In 2 a —a v > 6.o ¢ ¢ U U U C] u. M z U t= 3 2 Chemical Analysis&Other t� f ffJ -C 2,7c7-5:Se o2/r-0s'-l4-17 47is' 4/A44y I of I L a/' 0:-i `fi93a$R co en E I Special[nstrilctions: A '_ `- , T Sample Custody Transfer Record Secure Receipt Sample Date f Time Relinquished By/Organization ��Received By/Organization Area Temp°C Preserved? S=1G i71 0-7410_ ( / J ' / nu& Y''l ..�.; s—iGit �53� — 511.71r) 11th edE.x °t ,,_- ;err' o.co COMPOSIT4 SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Compositespies must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Prop° oriel: 1 sample each hour for 24 hours.Equal'Arius 0.0 and 6.0°C.Samples must not be frozen.Use water ice in seated bags. of sample collection(completion of composite sample). or at minim 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit- 1 I ET1, CHAIN uF CUSTODY RECORD Pb Box 164 4, Ogccnvt,LC.SC 29606,7414 Page Of (864/1377-742. 19001 891-232B P'47,:03641 1377 6928 9HIPPI746 AO`O`RCBe:4 CRARBM..H Cr, ORCCR�SC 29880 W. WWCTT.I.V flpnMCMT..1..COM Client: J - i[V E' TeX-A/ -r 2vt Program Containers Preservative Parameters Facility: 1,i--.k__c___ 1-,CAP-,-e— rca N...../ State: f C NPDES S#: /✓�Q C sr-y1 Whale Efficient Toxicity 11 11 7J Acute Chronic.) Test Oreniaw 2 al J U (Composite Only) (Grab a Composite) O —, O ti C� o e _ _ .m U y o p- .0 u 0 .v.. t _ g t•H2504 lu • o a A ,E v_i Z ° u C u k HCL $ a °- m c > O L tx.� /1 /� c y 3 0.' ,v J 7�F9Jnl °.. .Y .'-' `° .n 'fl 9 0 ° -L� y'l2 r, r7) G Q E e n F hNaOH 0 3 o Q v z .6-. C u 8 1._ P 04.J SAMPLE QD C? C.nmuh.Stan D.0 Ttme sample Condon rime Time Canectee by C] y c7 ,Z� ox " C7 > p,Qu.„ s a ' ' m '-' r ri- c-quQ ¢ ¢ u v v j Tis yr s� 1= 3 Chemical Analysis&Oder u, co cm 1r o4 - . Special lnsIru dons: .^.,1, Sample Cstody Transfer Record Secure Receipt Sample Date 1 Time Reli uished /Organization Received By/Organization Area Temp°C Preserved? 5:6-17-17 C571/,' dr ,-.......7 iii .4--'`' ice®fit- S J 17 C2 !2 C, )l S--j CYO) 1-fat cc.- 4 inti A t F o. COMPOSITF1S 4MPL[NG PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Composite sapies must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional: t sample each hour for 24 hours.Equal volui 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit. 1 084)8774942.FAX(864)6774838 P.O.Box 16414,GnawHe.6C 296O6 4 Craftsman Own,Gnaw,SC 29680 Ceriodaphnia dubia Survival and Reproduction Test EPA-821-R-02-013 Method 1002 Client: True Textiles Facility:Elkin NPDES#:NC0005312 Test Date: 09-Aug-17 Laboratory ID#:T49798 Test Reviewed and Approved By: 4 Robert W Kelley,Ph.D. Farhad Rostampour QA/QC Officer Laboratory Director Certification#E87819 SCDHEC Certification#23104 Test results presented in this report conform to all requirements of NELAC,conducted under NELAC Certification Number E87819 Florida Dept.of Health Included results pertain only to provided samples. NCDENR Certification# 022 Page 1 of 6 Effluent Toxicity Report Form-Chronic Pass/Fail and Acute LC50 Date 17-Aug-17 Facility: True Textiles WWTP NPDES#NC0005312 Pipe 8 001 County: Surry Laboratory Performi . Test: ETT Environrrantat,Inc. Comments X r . /_ Signature g ator in repo . e C Py X Signature of Laboratory Supervisor MAIL ORIGINAL TO Environmental Sclencea Branch Div.of Water Quality N.C.DENR 1621 Mall Service Center Raleigh,North Carolina 27699-1621 North Carolina Coriodaohnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t= -0.467 Critical Value= 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 %Reduction= -2.6% Or Young Produced 23 23 15 24 21 20 24 23 24 23 25 21 %Mortality Avg.Reprod Adult (L)ive (D)ead L L L L L L L L L L L L 0% 22.2 Contra Control Effluent% 1.9% 0% 22.8 Treatment 2 Treatment 2 Control CV TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 12.1% 4 Young Produced 26 19 19 19 18 27 23 23 25 23 23 28 %3rd Brood PASS FAIL Adult (L)ive (D)ead L L L L L L L L L L L L 100% [ X I Complete This for Either Teat Test Start Date Collection(Slam Cate 09-Aug-17 pH 1st sample 1st sample 2nd sa .e sample 1 07-Aug-17 Sample 2 O-Au9-17 Control 7.6 7.5 7.5 7.8 ®® sanyeLia tourer ort Treatment 2 7.6 7.5 7.5 7.6 NM Grab Comp Curator 1st 2nd Sample 1 X 24hrs Tox Tox Sample X 24hrs Dilution Sample Sample start end start end start end D.O. 1st sam a (st sample 2nd sariPle Hardness(mg/L) 46.0 1 Control 8.0 8.1 7.6 8.2 8.4 8.6 Spec.Coed (t.nhos) 185 145 192 Treatment 2 7.9 7.9 7.7 8.4 8.7 8.5 Chlonne(rryti) <.05 <.05 Sample Temp at receipt('C) 0.5 0.9 LCSOfAcute Toxicity Test (Mortality expressed as%,combining replicates) i Concentration Monatty start/end starvend LC50= % Method of Determination Control 95%Confidence Limits Moving Average Probit 111. 111 II High Conc % % Spearman Kerber I Other pH D.O. Organism Tested Ceriodaphnia dubia I DEM Form AT-1 Page 2 of 6 STATISTICAL ANALYSIS RESULTS Facility: True Textiles NPDEse NC0005312 Sample ID: WWTP me T49798 IDate: 09-Aug-17 Laboratory. FII I mirnnuicniai.Jnr. Certification#:NCO22 Exp.Date: 11/1/2017 Survival Data 7 Day Survival Test Used: FISHERS TEST Control 100% Test Statistic: P= 1.000 Effluent 100% Critical Value: P= 0.01 PASS:The effluent does not reduce survival of the test organisms. Reproduction Data Raw Data Test for Normality Mean young/femak Std.Dev Test Used: Shapiro-Wilks Test: Control 22.2 2.69 Effluent 22.8 3.39 W: 0.962 Critical Value: 0.884 Analysis for Differences in Reproduction Test for Homogeneity of Variance Test Used: Equal Variance t Test. Test Used: F Test Calculated t= -0.47 F= 1.58 Critical Value= 2.51 Critical Value= 5.32 The data are homogeneous in variance PASS:The effluent is not chronically toxic. Page 3 of 6 r� N IR m A r m L 0 W r G- p o $ a ry a m E ¢ �. rn 4 z{ S ] Q m ¢ o V N . E m o o 1- r S z u) m a U o z u) f g t2i :2 `D n o 4 .` g o' o ° ° o O F $ C a q ... o Q ° a '� E 8 m Q A .�• °. .e ' o o ° o K = 7. `o m 2 z II o E G 3 c aa o ° D O 3 a °' ; Y ¢ o o 11 V 07 X V M w 77 w 1- x z h P P G X t !- « 2 co T t-, p 40111/ C N = m� Cy N ccd F L 441 0 0 . V 4- O 0 05 O M V0 0 0 0 0 0 0 0 '40 03 0, 0, In n 0, 0, ,0 ry o m 0 Cl p In 0 0 0 0N N 1- N N N N N N N N N .- N N N r Q o N Q1 0 15'F.. _ r . I - 0 • 4- O N 0 N N N 0 0 011, .n m m m m n m m � m n rn .o2O n mm m n Io n n m 0) m '4' / C0 f` • z 2 t 4) ul R Q Q N N N a ° ¢ v y c 4.T3 2 Q t. 3 r-T ° co M Ca. Clw N < f° V' C' V. < <^, N N N m s < < g g g g g < Q < < < < < Q Z z z Z z ; z 2 `z z` 2 2 2 z z i •' N r) V u) m n m O+ O 4- N 02 Y h 40 n co O1 o •- N m Q N m n m Q• 0 4- 0. en Q N m n m 01 O ' N u 0. n " n m m m n n m m n N,; N 0. (v N NNN N co oc 0 0 0 0 0 0 0 d e a i ° N n cI N N A H " N " c. X2 t o a r- n n n r- o r r n r l'- n r= r� n r or, - ,... 0) m (h N N V 0 a0 07 N O)0)(p E I s 'e n o C9 ,J N v COm m cooso X o z m z o o z (.7(..9J p X D Z M Z (D D Z E $ a,_ z O u' ET, '1 CHAIN OF CUSTODY RECORD r+.%i`,,EF_,,.e..•J,..i_,i L't,;{tom'["-i:, 'Page of PO Cox 16414, ORECMVILLE. SC 29606-7414 16841 677.6942. 1e00)891-2329 F4x11864)677 6996 9NIPPIN6 AOopaaa: 4 CRArTSMAN CT.ORttn,30 29660 W W W.1TI-CP V W ONMCNTAL.COM Client: -7-/-T,.._ __ Pragram Containers Preservative Parameters Facility: ' 't...) Windt Effluent Toxicity _ State: /li NPDES#: / Acute Chronic Test Organisms O 1 - m E ' _ o o V (Catnposite only) (Grab or Composite) < E Ti;,.. U m !'tl p d a p 3 F K U .L•1 3-1$403 cL .. .c .n X, 10 q '� u Q = .Q h t' ' y S 4-NaOH 2 7 o e e`F .1 2 F C Q SAMPLE ID �3 c..owwsllAow Tama $ ,a 0 0 41 4 o 8 3.LIM u z v E >.? a L t3 cu Q s..µeaeau;..Due Tim* Collected by U in 1n Z 4t 0.40 > ¢,o,k, ¢ < U 0 U q� h x U` 3 2 Chemical Analysis&Other w - C T-7-17 oar-93_g--17 a74r gT 1� vIoA V !-q o biJJ+ta ' 7 A 1v N y w ciL' Special Instructions: - - Sample Custody Transfer Record Secure Receipt Sample Date Time Relinquished By/OrganizationR-. "ved By/Organization Area Temp°C Preserved? (fi c+17 07)0 �, �% �0 1�I 1,- f" ..� ' r '" / L ( _ . tatti, -:.... cit,,vy E-rr D.5 6D COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional: I sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:Asper instructions in NPDES permit ET' ' CHAIN OF CUSTODY RECORD u,_ '••$:.--(,,ePy-,....-,-,-fi '...-E -, iT Page of PO 9OX 18414. OwCe NVIILL,ac 39608-7414 1e641 977.6942, 19001 891-2226 F44:(5641 977 6986 SNIPPING ADORe86: 4 CAAFT•NAN CT.GRLLR,SC 19850 W W W.CM.LNVIRONM[NTAL.6OM _Client: TruE Program Containers Preservative Parameters FacilityPreservative- -- Whole State: k/c. NPDES#: n/�-- ai em°eLc remToxici ' JIB >z Acute �Chroaic Tc.t Or�.aium Q Y. S < c c 4.1 6 (Compoine only) {Grab orCompasoe) < �" - a V o u O C' I 3 -E 1-+2804 TT- r g G 5 v C g y 2_,„ . a. 2 „ m.4 •c 9y+ ee tr t > y L' _ 5 •y1t 0.' U t 1.104'03 2 .0 .G i, a -g a., ., g ' -€ v1 SAMPLE ID c ,2 8 0 0 o $ r-z H o' P .= .e"U o , >,_: ':c w �p.:lesl.e act rime s..Iplcc.o.d..o.,. Time Carried by u 1n z a a o > 6.06,0, < < U 0 0 Ci u.. v, z U i-- 3 2 Chemical Analysis&Other 1' T '7 c, r, , . r Special Instructions: • Sample Custody Transfer Record Secure Receipt Sample Date Time Relinquished By I Organization :y/Organization Area Temp°C Preserved? 41,c- iiip el-16-4 7 °7Z-rj . A i t, 4,,_ •. .1 ea .16 6 ar •ear (13, k0, [ip 9)03.11 _ - . r bl g l!r7 fham �y, gvp) ` f' iv -;7, _T 0 q COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HDL a IME PROC ; RES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional:I sample each hour for 24 hours.Equal voles 0.0 and 6.0'C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit. _ ars .Ins, (684)9776942.l•AJ(884)8776938 P0.Box 16414,Creenvlle SC 29606 4 Craftsman Cowl,Greer,SC 29650 Ceriodaphnia dubia Survival and Reproduction Test EPA-821-R-02-013 Method 1002 Client:TRUE TEXTILES Facility: Elkin NPDES#:NC0005312 Test Date: 15-Nov-17 Laboratory ID#:T50430 Test Reviewed and ApppQroo,vyyed By: Robert W.Kelley,Ph.D. // Farbad Rostampour QA/QC Officer Laboratory Director n e I a c Certification BK87819 SCDHEC Certification 023104 Test results presented in this report conform to all requveme tt of NELAC,cooducted under NELAC Certification Number E87819 Florida Dept.of Health.Included results pertain only to provided satrapies NCDENR Certificatian 4 022 Page 1 of 6 Effluent Toxicity Report Form-Chronic Pass/Fail and Acute LC50 Facili : True Textiles WWTP Date 27-Nov-17 Laboratory PerformingTeS: NPDES#NC0005312 Pipe# 001 Court . Su ETT Environmental,Inc. - ��I' _Cormrente ���itWX ott saw ', Signature of Operate_spo -Ibl= ate' x Si.nature of Laborato Su.:rvisor MAIL ORIGINAL TO Environmental Sciences Branch Div.of Water Quality N.C.DENR 1621 Mall Service Center Raleigh,North Carolina 27899-1621 North Carolina Cerlodaphnia Chronic PassiFall Reproduction Toxicity Teat Chronic Test Results Calculated t= 1.3822 CONTROL ORGANISMS Critical Value= 2.508 1 2 3 4 5 6 7 8 9 10 11 12 %Reduction= 8.3% #Young Producetl126121 / 25 / 20 j221 16 20 22 19 27 19 122 1 %Mortallty Avg.Reprod. Adult (L)lve (plead LL LL L LL L L L L L 0% 211 Effluent% f 1.9% I Con Control 0% 19.3 Treatment 2 Treatment 2 Control CV TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 12.7% 0 Young Produced 17 18 24 21 20 17 11 22 21 18 23 20 %3rd Brood PASS FAIL Adult (L)Ive (D)ead L L L L IL L IL IL L L L L 1 100% J X , Complete Thta for Either Test Test Start Date Collection(Start)Data 15-Nov-17 pH 1st sample 1st sample 2nd same Sample 1 13-Nov-17 Sample 2 15-Nov-17pl Control 1 7.7 8.0 1 7.6 7.9 1 7.6 I 8.0 Sample Two IDurado0) Treatment 2 7.8 7.9 7.6 7.9 7.6 8.0 freb JCotnp Duration 1st 2nd Sample 1 X [oration Tox Tox Sample 2 X 24hrs. Dilution Sample Sample D.O. start end start end start end tat aemwlle 1st sem le 204 sample Hardness(ms/1.) 46.0 Control 1 7.6 8.0 7.9 8.3 7.9 8.2 Spec Gond.(ymhos( 183 182 185 Treatment 2 7.7 8.2 7.9 8.3 7.7 8.3 Chlorine(mg/1) <.05 <.05 Sample Tempal receipt CC) 0.0 0.2 no{ LC50/Acute Toxicity Test frozen (Mortality expressed as%,combining replicates) r Concentration Mortality start/end star-Vend LC50= % Method of Determination ^ Control ConAdence Limits Moving Average Probit I I High Conc. °/s % Spearman Herter �ther pH D.O. Organism Tested Cenodaphnia dubia DEM Form AT-1 Page 2 of 6 STATISTICAL ANALYSIS RESULTS acility: True Textiles xroesa NC0005312 ple ID: WWTP Errs rsoaso Date: 15-Nov-17 boratory: F:'! I l;iisirilnnlcntai.Inc. Certificationti:NCO22 Exp.Date: 11/1/2018 Survival Data 7 Day Survival Test Used: FISHERS TEST Control 100% Test Statistic: P= 1.000 Effluent 100% Critical Value: P= 0.01 PASS:The effluent does not reduce survival of the test organisms. Reproduction Data Raw Data Test for Normality Mean young/female Std.Dev. Test Used. Shapiro-Wilks Test: Control 21.1 2.68 Effluent 19.3 3.47 W: 0.949 Critical Value: 0.884 Analysis for Differences in Reproduction Test for Homogeneity of Variance Test Used: Equal Variance I Test Test Used: F Test Calculated t 1.38 F 1.68 Critical Value 2.51 Critical Value= 5.32 The data are homogeneous in variance PASS:The effluent is not chronically toxic. Page 3oi_. Control Mortality and Reproduction by Test Day source rep 1 2 3 4 5 6 7 8 Total Lab* T50430 E4 11-3 1 .3.7 16 26 Client True Textiles R5 11-2 2 4 +8.9 21 Sample ID WWTP X2 11-3 3 3 .10.12 25 NPDES$ NC0005312 I, IIMMIIIIIMINM•111111•1 J6 11.2 4 +4+7 9 20 County Story 88 11-3 5 +3.8 11 22 Month 11 P2 11-2 6 .3.5 8 16 Start&fed Date 15-Nov-17 1 W8 11.3 7 +3+7 10 20 Start&fed Time 0110 PM 05 11.2 6 .3*8 11 22 Started&fed By JC M4 11-2 9 +3*8 8 19 Test Organism Cedodaphnla dubia S8 11-3 10 .4.7 10 21 Neo.born date 14-Nov-17 13 11-2 11 .3.7 9 19 Neo.born time 1705-2200 05 11-2 12 5 *8.9 22 Test Typo NCCPF 13 N/A 0 bllutlon Water SSF 11/3/15 14 N/A ,,,w0 Units for Cone. % 15 N/A 0 ,IWC 1.9 16 N/A 0 %Srd BROOD 17 N/A 0 Test visaed* 30 mi 16 N/A _ 0� Test volume 16 ml 19 N/A 0 can I lncubetor* 1 20 N/A 0 211 light 161//846 1.9 % Effluent Mortality and Reproduction by Test Day Initial Temp'V 24.8 1 2 3 4 5 6 7 8 Totes Salsnastrum 0.05 rni E4 11-3 1 +4+7 6 17 YAT 0.05 mi 8511-2 2 4 +6.8 18 Test method CPAe21.s-02.0's 1002 X2 11-3 3 4 *9.11 24 J6 11-2 4 .3.5 13 21 8811-3 5 .3.7 10 20 P2 11-2 6 •4.6 7 17 W8 11 7 3 8 11 Comments G5 11-2 8 *4*7 11 22 P M4 11-2 9 +3+8 10 21 S8 11-3 10 .3*7 8 18 _ 13 11-2 11 +3.9 11 23 ontrd rl terrp _ 24 7 0511-2 12 5 +8*9 20 0 13 N/A _ 0 0, 14 N/A 0 0 15 N/A 0 0 16 N/A 0 , 0 17 N/A 0 0 18 N/A 0 0 19 N/A o(MearlI 0 20 N/A 0 19.3 renew JC JC 1 End Da e fed JC JC JC AM JC JC 1 22-Nov-17 lime fad&renew 00.V AM 03 35 PM 05 LAM 10 55 AM 91 H PM DO 50 AM 0/Am PM I FJ •_ New temp.'C 24.7 24.5 Old temp.'c 24.5 24.3 25.3 censor New temp.'c 24.4 24.2 ,D',Dead N/A-Lost or nol used Page 4 of d i ETri CHAIN OF CUSTODY RECORD `Pave of PO Box 16414,Greenvale,SC 29808-7414 (884)877-8942, (800)891-2325 Farc(884)877 8938 ShlppYlg Address:4 Craftsman Ct,Greer,SC 29850 www. TTCNvl n OHM ENTAL-COM Client: � - - - - Program Containers Presert•afive Parameters Facility: / e_kve‘_; State: )t/ NPD ES#: AIC-000S-3 C2-.- Whole Effluent Toxicity n Acute Chronic Tout Organisms _ 21 9 CJ (Composite only) (Grab or Composite) 75 P _ CJ .Q U g a i7 l ? e. `v - g z--tH04 — 2 a j Sign,and Print below u - o :4 r4nos -'_ -Y ¢ a :=":the dotted line e E U — 4-N-,OH o — — o —, .6 c ' o S a c o 0 5-7,,,,,,„ - v O t r > ^ `,2SAMPLE ID U Composite Sun Due Time s.npte Coileatne nue Time Collected by U oto2aaU > 6-Ohe0: Lc� rn = U _ Chemical Analysis SOther 1-17 lIi1 a761 � - ( ,7qv N4S�3 0A rx>tO CO CD tr cr • �_� , r--> , , - - . Special Instructions: Sample Custody Transfer Record Secure Receipt Sample Date Time *el' ,uish •.t /Organization R_ ived By/Organization Area Temp°C Preserved? JI-M-)7 O7z�✓. r ,trAr ♦ _ two/ d it-(q.(-7 ( •! I l �� �. / it 11.1 ) 7;/ ',�` t)t I opo •- - � � ., � `� , CO� 7 � 411 1/ I COMPOSITE SAMPLING PROCEDURES TEAIPERATURE MONITORING PROCEDURES I HOLD TIME PROCEDURES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional: 1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit. ET": CHAIN Of CUSTODY RECORD4„ __ r• 'Page of I Po Box 16414, QRCCM VILI(, 9C 29606.7414 1864)877-6942, (900)091-2225 F4x:(964)877 9938 BHiP.IN9 ADORCCC:4 C6411-TSM4M Cr.GR[CR.50 29650 WWW.CTTCM V IR ONMC MTAL.COM Client: Tccir Program Containers Preservative Parameters Facility: / � I c 1N Whole Emaeot Toxicity Ai State: r NPDES#: A/t^_oc o 3i'Z Acute C�'61 oaie Test Orprisau O n m 4. c _ a ?r U (Composite only) (Grab or Composite) Q p c •ri (5 S zi U c a d z ct. N _ vt P ? W m ° K CJ : HCG R oa zL E 3-te+o) n. a ,y a 16 n H c .E wfrL/ t7 u o ,Qoam a aV4 '°Fi 1 3 L •Ei m > T.g W5 < SAMPLE D 02 t°mpwieeSuno.c Tima SCgkcasxT;eR9,c Time Collected by U 'Co-:,rn z R i 5r > 6,paa u ¢VR c.) tisi[ �;ns —. = ± Chemical Analysis BOther 1 ft( .f" C lr-,s-17 oars' ii-1G-r7 0NY(4/e..-.11 �' . ) %// 1/2,S ✓ r- ✓ V -Q 7c. h�t v+i c —' 50430(3 N . a cn 0 . co Special Instructions: Sample Custody Transfer Record Secure Receipt Sample Date Time •crag,uish ./:y/Organization -cc?ved By/Organization Area Temp°C Preserved? ,l-1t;1; 72 ' I`k tI-16- I7 c. . Or . OF .....-- . Jlff7/L0330 Fed x Er r 0.Q- COMPOSITE •Q-COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours Time Proportional: I sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flow Proportional:As per instructions in NPDES permit. Duvaltex (US), Inc . EPA ID # NC0005312 Appendix C Priority Pollutant Analysis Results Pace Analytical Services,LLC aceAnalytical 9800 KinceyAve. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 August 04, 2017 Mr. Glen Gary TRUE, Inc. 304 E. Main St. Elkin, NC 28621 RE: Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Dear Mr. Gary: Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Scott Taylor,True Textiles REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 41 @• Pace Analytical Services,LLC aceAnalytical100 9800 Kincey Ave. C 2 078 Huntersville,NC 28078 ./. ° wwwpacelabs.com (704)875-9092 CERTIFICATIONS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Charlotte Certification IDs 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Certification#:99006001 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 VirginiaNELAP Certification#:460221 Asheville Certification IDs 2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 Massachusetts Certification#: M-NC030 VirginiaNELAP Certification#:460222 North Carolina Drinking Water Certification#:37712 Eden Certification IDs 205 East Meadow Road Suite A,Eden,NC 27288 North Carolina Wastewater Certification#:633 North Carolina Drinking Water Certification#:37738 VirginiaNELAP Certification#:460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 41 Pace Analytical Services,LLC 79800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92348913001 Effluent Comp EPA 6010 SH1 20 PASI-A EPA 7470 KAL 1 PASI-A EPA 300.0 CDC 2 PASI-A EPA 350.1 1993 Rev 2.0 AES2 1 PASI-A EPA353.2 CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A EPA7196 CJH1 1 PASI-A 92348913002 Effluent Grab SM 2120E Color ADMI CTB 4 PASI-E EPA 1664B JMS 1 PASI-C EPA 8081 PKS 22 PASI-C EPA 8082 HSK 8 PASI-C EPA 8270 BPJ 74 PASI-C EPA 8260 ZDO 34 PASI-C SM 4500-S2D NAL 1 PASI-A EPA420.4 DMN 1 PASI-A SM 4500-CN-E BRJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 41 Pace Analytical Services,LLC e aceAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Sample: Effluent Comp Lab ID: 92348913001 Collected: 07/25/17 07:15 Received: 07/25/17 07:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method:EPA 6010 Preparation Method:EPA 3010A Aluminum 116 ug/L 100 1 07/31/17 15:40 08/02/17 05:12 7429-90-5 Antimony 496 ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-36-0 Arsenic ND ug/L 10.0 1 07/31/17 15:40 08/02/17 05:12 7440-38-2 Barium 10.6 ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-39-3 Beryllium ND ug/L 1.0 1 07/31/17 15:40 08/02/17 05:12 7440-41-7 Boron ND ug/L 50.0 1 07/31/17 15:40 08/03/17 18:21 7440-42-8 Cadmium ND ug/L 1.0 1 07/31/17 15:40 08/02/17 05:12 7440-43-9 Chromium 5.5 ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-47-3 Cobalt ND ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-48-4 Copper 14.0 ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-50-8 Iron 90.4 ug/L 50.0 1 07/31/17 15:40 08/02/17 05:12 7439-89-6 Lead ND ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7439-92-1 Magnesium 2610 ug/L 100 1 07/31/17 15:40 08/02/17 05:12 7439-95-4 Manganese 5.6 ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7439-96-5 Nickel ND ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-02-0 Selenium ND ug/L 10.0 1 07/31/17 15:40 08/02/17 05:12 7782-49-2 Silver ND ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-22-4 Thallium ND ug/L 10.0 1 07/31/17 15:40 08/02/17 05:12 7440-28-0 Titanium ND ug/L 5.0 1 07/31/17 15:40 08/02/17 05:12 7440-32-6 Zinc ND ug/L 10.0 1 07/31/17 15:40 08/02/17 05:12 7440-66-6 7470 Mercury Analytical Method:EPA 7470 Preparation Method:EPA 7470 Mercury ND ug/L 0.20 1 07/26/17 11:18 07/27/17 00:24 7439-97-6 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Fluoride 0.14 mg/L 0.10 1 07/30/17 20:20 16984-48-8 Sulfate 27.1 mg/L 1.0 1 07/30/17 20:20 14808-79-8 350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0 Nitrogen,Ammonia ND mg/L 0.10 1 08/01/17 15:08 7664-41-7 353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA 353.2 Nitrogen,NO2 plus NO3 0.92 mg/L 0.020 1 08/01/17 04:18 5310B TOC Analytical Method:SM 5310B Total Organic Carbon 33.7 mg/L 1.0 1 08/02/17 21:31 7440-44-0 7196 Chromium,Hexavalent Analytical Method:EPA 7196 Chromium,Hexavalent ND mg/L 0.010 1 07/26/17 05:41 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 41 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received: 07/25/17 07:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2120E Color ADMI Analytical Method:SM 2120E Color ADMI Color,ADMI ND units 25.0 1 07/26/17 13:08 Adjusted Color,ADMI ND units 25.0 1 07/26/17 13:08 pH 7.4 units 1.0 1 07/26/17 13:08 Adjusted pH,ADMI 7.6 units 1.0 1 07/26/17 13:08 HEM,Oil and Grease Analytical Method:EPA 1664B Oil and Grease ND mg/L 5.0 1 08/02/17 06:28 8081 Organochlorine Pesticides Analytical Method:EPA 8081 Preparation Method:EPA 3510 Aldrin ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 309-00-2 alpha-BHC ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 319-84-6 beta-BHC ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 319-85-7 delta-BHC ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 319-86-8 gamma-BHC(Lindane) ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 58-89-9 Chlordane(Technical) ND ug/L 0.20 1 07/26/17 15:30 07/26/17 19:18 57-74-9 4,4'-DDD ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 72-54-8 4,4'-DDE ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 72-55-9 4,4'-DDT ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 50-29-3 Dieldrin ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 60-57-1 Endosulfan I ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 959-98-8 Endosulfan II ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 1031-07-8 Endrin ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 72-20-8 Endrin aldehyde ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 7421-93-4 Endrin ketone ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 53494-70-5 Heptachlor ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 07/26/17 15:30 07/26/17 19:18 1024-57-3 Methoxychlor ND ug/L 0.15 1 07/26/17 15:30 07/26/17 19:18 72-43-5 Toxaphene ND ug/L 0.20 1 07/26/17 15:30 07/26/17 19:18 8001-35-2 Surrogates Tetrachloro-m-xylene(S) 55 % 20-130 1 07/26/17 15:30 07/26/17 19:18 877-09-8 Decachlorobiphenyl(S) 31 % 20-130 1 07/26/17 15:30 07/26/17 19:18 2051-24-3 8082 GCS PCB Analytical Method:EPA 8082 Preparation Method:EPA 3510 PCB-1016(Aroclor 1016) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 11104-28-2 PCB-1232(Aroclor 1232) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 11141-16-5 PCB-1242(Aroclor 1242) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 53469-21-9 PCB-1248(Aroclor 1248) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 12672-29-6 PCB-1254(Aroclor 1254) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 11097-69-1 PCB-1260(Aroclor 1260) ND ug/L 0.50 1 07/26/17 09:01 07/26/17 20:10 11096-82-5 Surrogates Decachlorobiphenyl(S) 37 % 10-132 1 07/26/17 09:01 07/26/17 20:10 2051-24-3 8270 MSSV Semivolatile Organic Analytical Method:EPA 8270 Preparation Method:EPA 3510 Acenaphthene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 83-32-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 41 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 .71v wwwpacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received: 07/25/17 07:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method:EPA 3510 Acenaphthylene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 208-96-8 Aniline ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 62-53-3 Anthracene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 207-08-9 Benzoic Acid ND ug/L 50.0 1 07/27/17 14:30 07/28/17 12:22 65-85-0 Benzyl alcohol ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 100-51-6 4-Bromophenylphenyl ether ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 101-55-3 Butylbenzylphthalate ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 85-68-7 4-Chloro-3-methylphenol ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 59-50-7 4-Chloroaniline ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 106-47-8 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 111-91-1 bis(2-Chloroethyl)ether ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 111-44-4 2-Chloronaphthalene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 91-58-7 2-Chlorophenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 95-57-8 4-Chlorophenylphenyl ether ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 7005-72-3 Chrysene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 53-70-3 Dibenzofuran ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 132-64-9 1,2-Dichlorobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 106-46-7 3,3'-Dichlorobenzidine ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 120-83-2 Diethylphthalate ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 84-66-2 2,4-Dimethylphenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 105-67-9 Dimethylphthalate ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 131-11-3 Di-n-butylphthalate ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 84-74-2 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 534-52-1 2,4-Dinitrophenol ND ug/L 50.0 1 07/27/17 14:30 07/28/17 12:22 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 117-84-0 bis(2-Ethylhexyl)phthalate ND ug/L 6.0 1 07/27/17 14:30 07/28/17 12:22 117-81-7 Fluoranthene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 206-44-0 Fluorene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 86-73-7 Hexachloro-1,3-butadiene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 87-68-3 Hexachlorobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 77-47-4 Hexachloroethane ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 193-39-5 Isophorone ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 78-59-1 1-Methylnaphthalene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 90-12-0 2-Methylnaphthalene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 91-57-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 41 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received: 07/25/17 07:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method:EPA 3510 2-Methylphenol(o-Cresol) ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 15831-10-4 Naphthalene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 91-20-3 2-Nitroaniline ND ug/L 50.0 1 07/27/17 14:30 07/28/17 12:22 88-74-4 3-Nitroaniline ND ug/L 50.0 1 07/27/17 14:30 07/28/17 12:22 99-09-2 4-Nitroaniline ND ug/L 20.0 1 07/27/17 14:30 07/28/17 12:22 100-01-6 Nitrobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 98-95-3 2-Nitrophenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 88-75-5 4-Nitrophenol ND ug/L 50.0 1 07/27/17 14:30 07/28/17 12:22 100-02-7 N-Nitrosodimethylamine ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 62-75-9 N-Nitroso-di-n- ro lamine ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 621-64-7 P PY 9 N-Nitrosodiphenylamine ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 108-60-1 Pentachlorophenol ND ug/L 25.0 1 07/27/17 14:30 07/28/17 12:22 87-86-5 Phenanthrene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 85-01-8 Phenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 108-95-2 Pyrene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 129-00-0 1,2,4-Trichlorobenzene ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 120-82-1 2,4,5-Trichlorophenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1 07/27/17 14:30 07/28/17 12:22 88-06-2 Surrogates Nitrobenzene-d5(S) 33 % 21-110 1 07/27/17 14:30 07/28/17 12:22 4165-60-0 2-Fluorobiphenyl(S) 41 % 27-110 1 07/27/17 14:30 07/28/17 12:22 321-60-8 Terphenyl-d14(S) 54 % 31-107 1 07/27/17 14:30 07/28/17 12:22 1718-51-0 Phenol-d6(S) 13 % 10-110 1 07/27/17 14:30 07/28/17 12:22 13127-88-3 2-Fluorophenol(S) 17 % 12-110 1 07/27/17 14:30 07/28/17 12:22 367-12-4 2,4,6-Tribromophenol(S) 57 % 27-110 1 07/27/17 14:30 07/28/17 12:22 118-79-6 8260 MSV Analytical Method: EPA 8260 Acrolein ND ug/L 100 1 07/30/17 01:48 107-02-8 Acrylonitrile ND ug/L 100 1 07/30/17 01:48 107-13-1 Benzene ND ug/L 5.0 1 07/30/17 01:48 71-43-2 Bromodichloromethane ND ug/L 5.0 1 07/30/17 01:48 75-27-4 Bromoform ND ug/L 5.0 1 07/30/17 01:48 75-25-2 Bromomethane ND ug/L 10.0 1 07/30/17 01:48 74-83-9 Carbon tetrachloride ND ug/L 5.0 1 07/30/17 01:48 56-23-5 Chlorobenzene ND ug/L 5.0 1 07/30/17 01:48 108-90-7 Chloroethane ND ug/L 10.0 1 07/30/17 01:48 75-00-3 2-Chloroethylvinyl ether ND ug/L 10.0 1 07/30/17 01:48 110-75-8 c2 Chloroform ND ug/L 5.0 1 07/30/17 01:48 67-66-3 Chloromethane ND ug/L 5.0 1 07/30/17 01:48 74-87-3 2-Chlorotoluene ND ug/L 5.0 1 07/30/17 01:48 95-49-8 4-Chlorotoluene ND ug/L 5.0 1 07/30/17 01:48 106-43-4 Dibromochloromethane ND ug/L 5.0 1 07/30/17 01:48 124-48-1 1,1-Dichloroethane ND ug/L 5.0 1 07/30/17 01:48 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1 07/30/17 01:48 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1 07/30/17 01:48 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 41 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 7112eAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received: 07/25/17 07:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 trans-1,2-Dichloroethene ND ug/L 5.0 1 07/30/17 01:48 156-60-5 1,2-Dichloropropane ND ug/L 5.0 1 07/30/17 01:48 78-87-5 cis-1,3-Dichloropropene ND ug/L 5.0 1 07/30/17 01:48 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 1 07/30/17 01:48 10061-02-6 1 ug /L(benzene ND u /L 5.0 1 07/30/17 01:48 100-41-4 Y Methylene Chloride ND ug/L 5.0 1 07/30/17 01:48 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 5.0 1 07/30/17 01:48 79-34-5 Tetrachloroethene ND ug/L 5.0 1 07/30/17 01:48 127-18-4 Toluene ND ug/L 5.0 1 07/30/17 01:48 108-88-3 1,1,1-Trichloroethane ND ug/L 5.0 1 07/30/17 01:48 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1 07/30/17 01:48 79-00-5 Trichloroethene ND ug/L 5.0 1 07/30/17 01:48 79-01-6 Vinyl chloride ND ug/L 5.0 1 07/30/17 01:48 75-01-4 Surrogates I 4-Bromofluorobenzene(S) 99 % 70-130 1 07/30/17 01:48 460-00-4 1 1,2-Dichloroethane-d4(S) 94 % 70-130 1 07/30/17 01:48 17060-07-0 Toluene-d8(S) 100 % 70-130 1 07/30/17 01:48 2037-26-5 4500S2D Sulfide Water Analytical Method:SM 4500-S2D Sulfide ND mg/L 0.10 1 07/31/17 17:42 18496-25-8 420.4 Phenolics,Total Analytical Method: EPA 420.4 Phenol 0.011 mg/L 0.010 1 07/31/17 14:33 108-95-2 4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E Cyanide ND mg/L 0.0080 1 08/02/17 05:40 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 41 11 Pace Analytical Services,LLC aceAnalytical® 9800 KineyAveSuite 100 � Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370563 Analysis Method: SM 2120E Color ADMI QC Batch Method: SM 2120E Color ADMI Analysis Description: 2120E Color ADMI Associated Lab Samples: 92348913002 METHOD BLANK: 2053311 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Color,ADMI units ND 25.0 07/26/17 12:56 LABORATORY CONTROL SAMPLE: 2053312 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Color,ADMI units 125 122 98 90-110 SAMPLE DUPLICATE: 2053313 92348816001 Dup Parameter Units Result Result RPD Qualifiers Color,ADMI units ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 41 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite 100 7Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371460 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease Associated Lab Samples: 92348913002 METHOD BLANK: 2058032 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 08/02/17 06:26 LABORATORY CONTROL SAMPLE: 2058033 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 37.8 94 78-114 MATRIX SPIKE SAMPLE: 2058034 92348970002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 40 40.0 97 78-114 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 41 Pace Analytical Services,LLC /�q/�n /� 9800 Kincey Ave. Suite 100 /f1 !�iceAnalytiicCT Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370574 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92348913001 METHOD BLANK: 2053343 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 07/26/17 22:17 LABORATORY CONTROL SAMPLE: 2053344 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Mercury ug/L 2.5 2.7 108 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2053345 2053346 MS MSD 92348930001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.3 2.3 90 90 75-125 0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 41 Pace Analytical Services,LLC t 9800 KinceyAve. Suite 100 7n2eAnalytical Huntersville,NC 28078 wrov.pace/abs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371135 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92348913001 METHOD BLANK: 2056354 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aluminum ug/L ND 100 08/01/17 14:28 Antimony ug/L ND 5.0 08/01/17 14:28 Arsenic ug/L ND 10.0 08/01/17 14:28 Barium ug/L ND 5.0 08/01/17 14:28 Beryllium ug/L ND 1.0 08/01/17 14:28 Boron ug/L ND 50.0 08/01/17 16:14 Cadmium ug/L ND 1.0 08/01/17 14:28 Chromium ug/L ND 5.0 08/01/17 14:28 Cobalt ug/L ND 5.0 08/01/17 14:28 Copper ug/L ND 5.0 08/01/17 14:28 Iron ug/L ND 50.0 08/01/17 14:28 Lead ug/L ND 5.0 08/01/17 14:28 Magnesium ug/L ND 100 08/01/17 14:28 Manganese ug/L ND 5.0 08/01/17 14:28 Nickel ug/L ND 5.0 08/01/17 14:28 Selenium ug/L ND 10.0 08/01/17 16:14 Silver ug/L ND 5.0 08/01/17 14:28 Thallium ug/L ND 10.0 08/01/17 16:14 Titanium ug/L ND 5.0 08/01/17 16:14 Zinc ug/L ND 10.0 08/01/17 14:28 LABORATORY CONTROL SAMPLE: 2056355 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Aluminum ug/L 5000 4710 94 80-120 Antimony ug/L 500 489 98 80-120 Arsenic ug/L 500 542 108 80-120 Barium ug/L 500 550 110 80-120 Beryllium ug/L 500 544 109 80-120 Boron ug/L 500 491 98 80-120 Cadmium ug/L 500 547 109 80-120 Chromium ug/L 500 542 108 80-120 Cobalt ug/L 500 558 112 80-120 Copper ug/L 500 558 112 80-120 Iron ug/L 5000 4630 93 80-120 Lead ug/L 500 550 110 80-120 Magnesium ug/L 5000 4530 91 80-120 Manganese ug/L 500 543 109 80-120 Nickel ug/L 500 539 108 80-120 Selenium ug/L 500 579 116 80-120 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 41 1 Pace Analytical Services,LLC aceAnalyticale 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 wwwpacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 LABORATORY CONTROL SAMPLE: 2056355 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Silver ug/L 250 242 97 80-120 Thallium ug/L 500 555 111 80-120 Titanium ug/L 500 492 98 80-120 Zinc ug/L 500 552 110 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2056356 2056357 MS MSD 92349027001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Aluminum ug/L ND 5000 5000 4750 4870 94 96 75-125 2 Antimony ug/L ND 500 500 483 499 97 100 75-125 3 Arsenic ug/L ND 500 500 542 564 108 113 75-125 4 Barium ug/L ND 500 500 546 559 109 112 75-125 2 Beryllium ug/L ND 500 500 547 560 109 112 75-125 2 Boron ug/L ND 500 500 495 507 95 98 75-125 2 Cadmium ug/L ND 500 500 538 555 108 111 75-125 3 Chromium ug/L ND 500 500 536 549 107 110 75-125 2 Cobalt ug/L ND 500 500 539 557 108 111 75-125 3 Copper ug/L ND 500 500 558 572 111 114 75-125 2 Iron ug/L 52.5 5000 5000 4620 4740 91 94 75-125 2 Lead ug/L ND 500 500 527 545 105 109 75-125 3 Magnesium ug/L 1700 5000 5000 6130 6270 89 91 75-125 2 Manganese ug/L ND 500 500 535 549 107 109 75-125 3 Nickel ug/L ND 500 500 523 540 104 108 75-125 3 Selenium ug/L ND 500 500 549 577 109 115 75-125 5 Silver ug/L ND 250 250 240 245 96 98 75-125 2 Thallium ug/L ND 500 500 586 495 117 99 75-125 17 Titanium ug/L ND 500 500 483 610 96 122 75-125 23 R1 Zinc ug/L ND 500 500 546 562 108 111 75-125 3 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 41 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 /6.23ceAnalytical® Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371101 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Associated Lab Samples: 92348913002 METHOD BLANK: 2056233 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1-Trichloroethane ug/L ND 5.0 07/30/17 00:11 1,1,2,2-Tetrachloroethane ug/L ND 5.0 07/30/17 00:11 1,1,2-Trichloroethane ug/L ND 5.0 07/30/17 00:11 1,1-Dichloroethane ug/L ND 5.0 07/30/17 00:11 1,1-Dichloroethene ug/L ND 5.0 07/30/17 00:11 1,2-Dichloroethane ug/L ND 5.0 07/30/17 00:11 1,2-Dichloropropane ug/L ND 5.0 07/30/17 00:11 2-Chloroethylvinyl ether ug/L ND 10.0 07/30/17 00:11 2-Chlorotoluene ug/L ND 5.0 07/30/17 00:11 4-Chlorotoluene ug/L ND 5.0 07/30/17 00:11 Acrolein ug/L ND 100 07/30/17 00:11 Acrylonitrile ug/L ND 100 07/30/17 00:11 Benzene ug/L ND 5.0 07/30/17 00:11 Bromodichloromethane ug/L ND 5.0 07/30/17 00:11 Bromoform ug/L ND 5.0 07/30/17 00:11 Bromomethane ug/L ND 10.0 07/30/17 00:11 Carbon tetrachloride ug/L ND 5.0 07/30/17 00:11 Chlorobenzene ug/L ND 5.0 07/30/17 00:11 Chloroethane ug/L ND 10.0 07/30/17 00:11 Chloroform ug/L ND 5.0 07/30/17 00:11 Chloromethane ug/L ND 5.0 07/30/17 00:11 cis-1,3-Dichloropropene ug/L ND 5.0 07/30/17 00:11 Dibromochloromethane ug/L ND 5.0 07/30/17 00:11 Ethylbenzene ug/L ND 5.0 07/30/17 00:11 Methylene Chloride ug/L ND 5.0 07/30/17 00:11 Tetrachloroethene ug/L ND 5.0 07/30/17 00:11 Toluene ug/L ND 5.0 07/30/17 00:11 trans-1,2-Dichloroethene ug/L ND 5.0 07/30/17 00:11 trans-1,3-Dichloropropene ug/L ND 5.0 07/30/17 00:11 Trichloroethene ug/L ND 5.0 07/30/17 00:11 Vinyl chloride ug/L ND 5.0 07/30/17 00:11 1,2-Dichloroethane-d4(S) % 89 70-130 07/30/17 00:11 4-Bromofluorobenzene(S) % 101 70-130 07/30/17 00:11 Toluene-d8(S) % 97 70-130 07/30/17 00:11 LABORATORY CONTROL SAMPLE: 2056234 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 50 47.2 94 71-129 1,1,2,2-Tetrachloroethane ug/L 50 44.1 88 79-124 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 41 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 9aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 LABORATORY CONTROL SAMPLE: 2056234 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,2-Trichloroethane ug/L 50 43.4 87 85-125 1,1-Dichloroethane ug/L 50 44.4 89 73-126 1,1-Dichloroethene ug/L 50 50.0 100 66-135 1,2-Dichloroethane ug/L 50 43.9 88 67-128 1,2-Dichloropropane ug/L 50 46.7 93 75-132 2-Chloroethylvinyl ether ug/L 100 96.6 97 40-160 2-Chlorotoluene ug/L 50 45.9 92 74-132 4-Chlorotoluene ug/L 50 45.1 90 76-133 Acrolein ug/L 250 325 130 24-160 Acrylonitrile ug/L 250 232 93 40-160 Benzene ug/L 50 49.0 98 80-125 Bromodichloromethane ug/L 50 46.9 94 78-124 Bromoform ug/L 50 40.9 82 71-128 Bromomethane ug/L 50 34.7 69 40-160 Carbon tetrachloride ug/L 50 48.6 97 69-131 Chlorobenzene ug/L 50 46.9 94 81-122 Chloroethane ug/L 50 46.2 92 39-148 Chloroform ug/L 50 44.4 89 73-127 Chloromethane ug/L 50 51.7 103 44-146 cis-1,3-Dichloropropene ug/L 50 45.6 91 72-132 Dibromochloromethane ug/L 50 44.1 88 78-125 Ethylbenzene ug/L 50 46.6 93 79-121 Methylene Chloride ug/L 50 53.4 107 64-133 Tetrachloroethene ug/L 50 43.5 87 78-122 Toluene ug/L 50 48.4 97 80-121 trans-1,2-Dichloroethene ug/L 50 48.7 97 71-127 trans-1,3-Dichloropropene ug/L 50 44.2 88 69-141 Trichloroethene ug/L 50 45.3 91 78-122 Vinyl chloride ug/L 50 51.2 102 58-137 1,2-Dichloroethane-d4(S) % 92 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 100 70-130 MATRIX SPIKE SAMPLE: 2056235 92348343003 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L ND 400 415 104 70-130 1,1,2,2-Tetrachloroethane ug/L ND 400 395 99 70-130 1,1,2-Trichloroethane ug/L ND 400 402 101 70-130 1,1-Dichloroethane ug/L ND 400 423 106 70-130 1,1-Dichloroethene ug/L ND 400 451 113 65-160 1,2-Dichloroethane ug/L ND 400 406 101 70-130 1,2-Dichloropropane ug/L ND 400 441 110 70-130 2-Chloroethylvinyl ether ug/L ND 800 ND 0 70-130 P5 2-Chlorotoluene ug/L ND 400 403 101 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 41 Pace Analytical Services,LLC QD9800 Kincey Ave. Suite 100 7.2eAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 MATRIX SPIKE SAMPLE: 2056235 92348343003 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 4-Chlorotoluene ug/L ND 400 398 100 70-130 Acrolein ug/L ND 2000 3520 176 70-130 M1 Acrylonitrile ug/L ND 2000 2180 109 70-130 Benzene ug/L ND 400 431 108 58-162 Bromodichloromethane ug/L ND 400 431 108 70-130 Bromoform ug/L ND 400 355 89 70-130 Bromomethane ug/L ND 400 307 77 70-130 Carbon tetrachloride ug/L ND 400 453 113 70-130 Chlorobenzene ug/L ND 400 417 104 70-138 Chloroethane ug/L ND 400 432 108 70-130 Chloroform ug/L ND 400 443 111 70-130 Chloromethane ug/L ND 400 440 110 70-130 cis-1,3-Dichloropropene ug/L ND 400 418 105 70-130 Dibromochloromethane ug/L ND 400 390 97 70-130 Ethylbenzene ug/L ND 400 409 102 22-189 Methylene Chloride ug/L ND 400 495 124 70-130 Tetrachloroethene ug/L ND 400 385 96 70-130 Toluene ug/L ND 400 491 110 65-152 trans-1,2-Dichloroethene ug/L ND 400 450 112 70-130 trans-1,3-Dichloropropene ug/L ND 400 383 96 70-130 Trichloroethene ug/L ND 400 386 96 70-142 Vinyl chloride ug/L ND 400 437 109 70-130 1,2-Dichloroethane-d4(S) % 98 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 100 70-130 SAMPLE DUPLICATE: 2056236 92348343002 Dup Parameter Units Result Result RPD Qualifiers 1,1,1-Trichloroethane ug/L ND ND 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 2-Chloroethylvinyl ether ug/L ND ND 2-Chlorotoluene ug/L ND ND 4-Chlorotoluene ug/L ND ND Acrolein ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 41 1 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 /12e Analytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 SAMPLE DUPLICATE: 2056236 92348343002 Dup Parameter Units Result Result RPD Qualifiers Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane u9/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Ethylbenzene ug/L ND ND Methylene Chloride ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L 3590 3670 2 trans-1,2-Dichloroethene ug/L ND ND trans-1,3-Dichloropropene ug/L ND ND Trichloroethene ug/L ND ND Vinyl chloride ug/L ND ND 1,2-Dichloroethane-d4(S) % 99 101 2 4-Bromofluorobenzene(S) % 106 99 7 Toluene-d8(S) % 98 99 1 Results presented on this page are in the units Indicated by the"units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 41 Pace Analytical Services,LLC at 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370645 Analysis Method: EPA 8081 QC Batch Method: EPA 3510 Analysis Description: 8081A GCS Pesticides Associated Lab Samples: 92348913002 1 METHOD BLANK: 2053818 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 07/26/17 20:12 4,4'-DDE ug/L ND 0.050 07/26/17 20:12 4,4'-DDT ug/L ND 0.050 07/26/17 20:12 Aldrin ug/L ND 0.050 07/26/17 20:12 alpha-BHC ug/L ND 0.050 07/26/17 20:12 beta-BHC ug/L ND 0.050 07/26/17 20:12 Chlordane(Technical) ug/L ND 0.20 07/26/17 20:12 delta-BHC ug/L ND 0.050 07/26/17 20:12 ' Dieldrin ug/L ND 0.050 07/26/17 20:12 Endosulfan I ug/L ND 0.050 07/26/17 20:12 Endosulfan II ug/L ND 0.050 07/26/17 20:12 Endosulfan sulfate ug/L ND 0.050 07/26/17 20:12 Endrin ug/L ND 0.050 07/26/17 20:12 Endrin aldehyde ug/L ND 0.050 07/26/17 20:12 Endrin ketone ug/L ND 0.050 07/26/17 20:12 gamma-BHC(Lindane) ug/L ND 0.050 07/26/17 20:12 Heptachlor ug/L ND 0.050 07/26/17 20:12 Heptachlor epoxide ug/L ND 0.050 07/26/17 20:12 Methoxychlor ug/L ND 0.15 07/26/17 20:12 Toxaphene ug/L ND 0.20 07/26/17 20:12 Decachlorobiphenyl(S) % 64 20-130 07/26/17 20:12 Tetrachloro-m-xylene(S) % 84 20-130 07/26/17 20:12 LABORATORY CONTROL SAMPLE&LCSD: 2053819 2053820 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers 4,4'-DDD ug/L .25 0.20 0.23 80 92 20-150 13 30 4,4'-DDE ug/L .25 0.19 0.22 75 87 20-150 15 30 4,4'-DDT ug/L .25 0.19 0.23 78 94 20-150 19 30 Aldrin ug/L .25 0.15 0.17 61 69 20-150 13 30 alpha-BHC ug/L .25 0.17 0.20 70 82 20-150 16 30 beta-BHC ug/L .25 0.16 0.18 64 74 20-150 16 30 delta-BHC ug/L .25 0.17 0.21 70 84 20-150 18 30 Dieldrin ug/L .25 0.19 0.21 78 85 20-150 9 30 Endosulfan I ug/L .25 0.19 0.22 78 87 20-150 12 30 Endosulfan II ug/L .25 0.20 0.22 80 89 20-150 11 30 Endosulfan sulfate ug/L .25 0.20 0.23 80 91 20-150 13 30 Endrin ug/L .25 0.20 0.23 82 92 20-150 11 30 Endrin aldehyde ug/L .25 0.18 0.21 71 83 20-150 15 30 Endrin ketone ug/L .25 0.19 0.21 78 87 20-150 11 30 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 41 Pace Analytical Services,LLC 2ceAnalyticar 9800 KineyAveSuite 100 Huntersville,NC 28078 www.paceiabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 LABORATORY CONTROL SAMPLE&LCSD: 2053819 2053820 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers gamma-BHC(Lindane) ug/L .25 0.18 0.21 72 84 20-150 16 30 Heptachlor ug/L .25 0.15 0.19 62 76 20-150 20 30 Heptachlor epoxide ug/L .25 0.17 0.21 70 84 20-150 19 30 Methoxychlor ug/L .74 0.64 0.70 86 94 20-150 9 30 Decachlorobiphenyl(S) % 69 80 20-130 Tetrachloro-m-xylene(S) % 85 96 20-130 Results presented on this page are in the units indicated by the"units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 41 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 ,') eAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370359 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Associated Lab Samples: 92348913002 METHOD BLANK: 2052153 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016(Aroclor 1016) ug/L ND 0.50 07/26/17 20:30 PCB-1221 (Aroclor 1221) ug/L ND 0.50 07/26/17 20:30 PCB-1232(Aroclor 1232) ug/L ND 0.50 07/26/17 20:30 PCB-1242(Aroclor 1242) ug/L ND 0.50 07/26/17 20:30 PCB-1248(Aroclor 1248) ug/L ND 0.50 07/26/17 20:30 PCB-1254(Aroclor 1254) ug/L ND 0.50 07/26/17 20:30 PCB-1260(Aroclor 1260) ug/L ND 0.50 07/26/17 20:30 Decachlorobiphenyl(S) % 72 10-132 07/26/17 20:30 LABORATORY CONTROL SAMPLE&LCSD: 2052154 2052155 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers PCB-1016(Aroclor 1016) ug/L 5 4.1 4.5 81 90 50-150 10 30 PCB-1260(Aroclor 1260) ug/L 5 3.2 3.3 65 67 50-150 3 30 Decachlorobiphenyl(S) % 83 84 10-132 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 41 Pace Analytical Services,LLC to 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370788 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 92348913002 METHOD BLANK: 2054651 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,2,4-Trichlorobenzene ug/L ND 10.0 07/28/17 11:01 1,2-Dichlorobenzene ug/L ND 10.0 07/28/17 11:01 1,3-Dichlorobenzene ug/L ND 10.0 07/28/17 11:01 1,4-Dichlorobenzene ug/L ND 10.0 07/28/17 11:01 1-Methylnaphthalene ug/L ND 10.0 07/28/17 11:01 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 07/28/17 11:01 2,4,5-Trichlorophenol ug/L ND 10.0 07/28/17 11:01 2,4,6-Trichlorophenol ug/L ND 10.0 07/28/17 11:01 2,4-Dichlorophenol ug/L ND 10.0 07/28/17 11:01 2,4-Dimethylphenol ug/L ND 10.0 07/28/17 11:01 2,4-Dinitrophenol ug/L ND 50.0 07/28/17 11:01 2,4-Dinitrotoluene ug/L ND 10.0 07/28/17 11:01 2,6-Dinitrotoluene ug/L ND 10.0 07/28/17 11:01 2-Chloronaphthalene ug/L ND 10.0 07/28/17 11:01 2-Chlorophenol ug/L ND 10.0 07/28/17 11:01 2-Methylnaphthalene ug/L ND 10.0 07/28/17 11:01 2-Methylphenol(o-Cresol) ug/L ND 10.0 07/28/17 11:01 2-Nitroaniline ug/L ND 50.0 07/28/17 11:01 2-Nitrophenol ug/L ND 10.0 07/28/17 11:01 3&4-Methylphenol(m&p Cresol) ug/L ND 10.0 07/28/17 11:01 3,3'-Dichlorobenzidine ug/L ND 20.0 07/28/17 11:01 3-Nitroaniline ug/L ND 50.0 07/28/17 11:01 4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/28/17 11:01 1 4-Bromophenylphenyl ether ug/L ND 10.0 07/28/17 11:01 4-Chloro-3-methylphenol ug/L ND 20.0 07/28/17 11:01 4-Chloroaniline ug/L ND 20.0 07/28/17 11:01 4-Chlorophenylphenyl ether ug/L ND 10.0 07/28/17 11:01 4-Nitroaniline ug/L ND 20.0 07/28/17 11:01 4-Nitrophenol ug/L ND 50.0 07/28/17 11:01 Acenaphthene ug/L ND 10.0 07/28/17 11:01 Acenaphthylene ug/L ND 10.0 07/28/17 11:01 Aniline ug/L ND 10.0 07/28/17 11:01 Anthracene ug/L ND 10.0 07/28/17 11:01 Benzo(a)anthracene ug/L ND 10.0 07/28/17 11:01 Benzo(a)pyrene ug/L ND 10.0 07/28/17 11:01 Benzo(b)fluoranthene ug/L ND 10.0 07/28/17 11:01 Benzo(g,h,i)perylene ug/L ND 10.0 07/28/17 11:01 Benzo(k)fluoranthene ug/L ND 10.0 07/28/17 11:01 Benzoic Acid ug/L ND 50.0 07/28/17 11:01 Benzyl alcohol ug/L ND 20.0 07/28/17 11:01 bis(2-Chloroethoxy)methane ug/L ND 10.0 07/28/17 11:01 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 41 Pace Analytical Services,LLC ® 9800 KinceyAve. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 METHOD BLANK: 2054651 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers bis(2-Chloroethyl)ether ug/L ND 10.0 07/28/17 11:01 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/28/17 11:01 Butylbenzylphthalate ug/L ND 10.0 07/28/17 11:01 Chrysene ug/L ND 10.0 07/28/17 11:01 Di-n-butylphthalate ug/L ND 10.0 07/28/17 11:01 Di-n-octylphthalate ug/L ND 10.0 07/28/17 11:01 Dibenz(a,h)anthracene ug/L ND 10.0 07/28/17 11:01 Dibenzofuran ug/L ND 10.0 07/28/17 11:01 Diethylphthalate ug/L ND 10.0 07/28/17 11:01 Dimethylphthalate ug/L ND 10.0 07/28/17 11:01 Fluoranthene ug/L ND 10.0 07/28/17 11:01 Fluorene ug/L ND 10.0 07/28/17 11:01 Hexachloro-1,3-butadiene ug/L ND 10.0 07/28/17 11:01 Hexachlorobenzene ug/L ND 10.0 07/28/17 11:01 Hexachlorocyclopentadiene ug/L ND 10.0 07/28/17 11:01 Hexachloroethane ug/L ND 10.0 07/28/17 11:01 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/28/17 11:01 Isophorone ug/L ND 10.0 07/28/17 11:01 N-Nitroso-di-n-propylamine ug/L ND 10.0 07/28/17 11:01 N-Nitrosodimethylamine ug/L ND 10.0 07/28/17 11:01 N-Nitrosodiphenylamine ug/L ND 10.0 07/28/17 11:01 Naphthalene ug/L ND 10.0 07/28/17 11:01 Nitrobenzene ug/L ND 10.0 07/28/17 11:01 Pentachlorophenol ug/L ND 25.0 07/28/17 11:01 Phenanthrene ug/L ND 10.0 07/28/17 11:01 Phenol ug/L ND 10.0 07/28/17 11:01 Pyrene ug/L ND 10.0 07/28/17 11:01 2,4,6-Tribromophenol(S) % 41 27-110 07/28/17 11:01 2-Fluorobiphenyl(S) % 90 27-110 07/28/17 11:01 2-Fluorophenol(S) % 44 12-110 07/28/17 11:01 Nitrobenzene-d5(S) % 83 21-110 07/28/17 11:01 Phenol-d6(S) % 33 10-110 07/28/17 11:01 Terphenyl-d14(S) % 99 31-107 07/28/17 11:01 LABORATORY CONTROL SAMPLE&LCSD: 2054652 2054653 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers 1,2,4-Trichlorobenzene ug/L 50 33.1 31.3 66 63 31-120 6 30 1,2-Dichlorobenzene ug/L 50 30.4 32.9 61 66 38-120 8 30 1,3-Dichlorobenzene ug/L 50 28.1 28.2 56 56 30-122 0 30 1,4-Dichlorobenzene ug/L 50 30.9 30.6 62 61 37-120 1 30 1-Methylnaphthalene ug/L 50 42.6 39.2 85 78 34-113 8 30 2,2'-Oxybis(1-chloropropane) ug/L 50 30.5 32.1 61 64 18-120 5 30 2,4,5-Trichlorophenol ug/L 50 45.1 41.2 90 82 43-113 9 30 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 22 of 41 Pace Analytical Services,LLC aceAnalytical® 9800 KinceyAve. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 LABORATORY CONTROL SAMPLE&LCSD: 2054652 2054653 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers 2,4,6-Trichlorophenol ug/L 50 49.0 46.7 98 93 42-120 5 30 2,4-Dichlorophenol ug/L 50 41.9 39.8 84 80 30-120 5 30 2,4-Dimethylphenol ug/L 50 42.4 43.3 85 87 29-111 2 30 2,4-Dinitrophenol ug/L 250 234 227 94 91 19-132 3 30 2,4-Dinitrotoluene ug/L 50 49.1 49.1 98 98 58-128 0 30 2,6-Dinitrotoluene ug/L 50 51.1 50.6 102 101 54-129 1 30 2-Chloronaphthalene ug/L 50 47.3 47.7 95 95 43-117 1 30 2-Chlorophenol ug/L 50 37.0 40.7 74 81 37-120 9 30 2-Methylnaphthalene ug/L 50 41.3 38.7 83 77 33-120 6 30 2-Methylphenol(o-Cresol) ug/L 50 31.2 35.9 62 72 31-120 14 30 2-Nitroaniline ug/L 100 80.9 77.0 81 77 48-121 5 30 2-Nitrophenol ug/L 50 40.9 41.1 82 82 25-116 0 30 3&4-Methylphenol(m&p Cresol) ug/L 50 52.9 59.9 106 120 23-120 12 30 3,3'-Dichlorobenzidine ug/L 100 77.2 75.3 77 75 10-154 3 30 3-Nitroaniline ug/L 100 88.8 85.8 89 86 43-115 3 30 4,6-Dinitro-2-methylphenol ug/L 100 92.6 92.2 93 92 44-124 0 30 4-Bromophenylphenyl ether ug/L 50 38.1 37.2 76 74 34-113 2 30 4-Chloro-3-methylphenol ug/L 100 84.1 83.4 84 83 31-110 1 30 4-Chloroaniline ug/L 100 61.8 60.2 62 60 20-120 3 30 4-Chlorophenylphenyl ether ug/L 50 42.8 41.4 86 83 34-116 3 30 4-Nitroaniline ug/L 100 96.5 97.7 96 98 46-128 1 30 4-Nitrophenol ug/L 250 111 102 44 41 11-120 8 30 Acenaphthene ug/L 50 46.3 45.2 93 90 48-114 2 30 Acenaphthylene ug/L 50 43.8 42.7 88 85 48-112 2 30 Aniline ug/L 50 21.4 20.6 43 41 26-120 4 30 Anthracene ug/L 50 42.9 42.7 86 85 57-118 1 30 Benzo(a)anthracene ug/L 50 41.8 41.8 84 84 56-121 0 30 Benzo(a)pyrene ug/L 50 42.9 42.8 86 86 55-127 0 30 Benzo(b)fluoranthene ug/L 50 44.7 43.5 89 87 53-128 3 30 Benzo(g,h,i)perylene ug/L 50 43.9 52.5 88 105 54-125 18 30 Benzo(k)fluoranthene ug/L 50 42.4 42.2 85 84 51-123 0 30 Benzoic Acid ug/L 250 95.4 84.7 38 34 10-120 12 30 Benzyl alcohol ug/L 100 64.4 72.4 64 72 27-120 12 30 bis(2-Chloroethoxy)methane ug/L 50 37.7 35.1 75 70 32-120 7 30 bis(2-Chloroethyl)ether ug/L 50 38.1 41.2 76 82 33-111 8 30 bis(2-Ethylhexyl)phthalate ug/L 50 45.1 44.2 90 88 50-145 2 30 Butylbenzylphthalate ug/L 50 45.5 44.0 91 88 54-138 3 30 Chrysene ug/L 50 42.3 41.8 85 84 58-127 1 30 Di-n-butylphthalate ug/L 50 46.6 46.5 93 93 56-125 0 30 Di-n-octylphthalate ug/L 50 45.7 44.6 91 89 50-134 2 30 Dibenz(a,h)anthracene ug/L 50 45.0 52.3 90 105 53-129 15 30 Dibenzofuran ug/L 50 45.8 45.1 92 90 45-120 2 30 Diethylphthalate ug/L 50 48.7 48.1 97 96 53-120 1 30 Dimethylphthalate ug/L 50 49.7 49.0 99 98 55-116 1 30 Fluoranthene ug/L 50 45.1 45.4 90 91 57-125 1 30 Fluorene ug/L 50 46.2 44.9 92 90 53-118 3 30 Hexachloro-1,3-butadiene ug/L 50 29.3 28.9 59 58 23-120 1 30 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 41 Pace Analytical Services,LLC aceAnalytical a 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 LABORATORY CONTROL SAMPLE&LCSD: 2054652 2054653 Spike LCS LCSD LCS LCSD %Rec Max Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers Hexachlorobenzene ug/L 50 44.4 43.4 89 87 49-116 2 30 Hexachlorocyclopentadiene ug/L 50 34.5 31.4 69 63 26-158 9 30 Hexachloroethane ug/L 50 27.5 28.8 55 58 30-114 5 30 Indeno(1,2,3-cd)pyrene ug/L 50 47.4 54.7 95 109 55-128 14 30 Isophorone ug/L 50 40.9 39.2 82 78 31-118 4 30 N-Nitroso-di-n-propylamine ug/L 50 42.5 46.2 85 92 32-119 8 30 N-Nitrosodimethylamine ug/L 50 26.8 28.0 54 56 13-120 4 30 N-Nitrosodiphenylamine ug/L 50 42.3 41.4 85 83 43-120 2 30 Naphthalene ug/L 50 37.8 37.0 76 74 32-120 2 30 Nitrobenzene ug/L 50 40.0 36.9 80 74 33-110 8 30 Pentachlorophenol ug/L 100 91.7 92.0 92 92 10-137 0 30 Phenanthrene ug/L 50 42.2 42.0 84 84 57-117 0 30 Phenol ug/L 50 20.8 23.0 42 46 10-120 10 30 Pyrene ug/L 50 39.2 39.7 78 79 55-122 1 30 2,4,6-Tribromophenol(S) % 96 90 27-110 2-Fluorobiphenyl(S) % 91 86 27-110 2-Fluorophenol(S) % 50 49 12-110 Nitrobenzene-d5(S) % 85 77 21-110 Phenol-d6(S) % 33 36 10-110 Terphenyl-d14(S) % 97 91 31-107 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 24 of 41 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 CONTROL ONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370915 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92348913002 METHOD BLANK: 2055361 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide mg/L ND 0.10 07/31/17 17:42 LABORATORY CONTROL SAMPLE: 2055362 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Sulfide mg/L .5 0.53 105 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2055363 2055364 MS MSD 92348902005 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Sulfide mg/L ND .5 .5 0.44 0.44 80 80 80-120 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2055365 2055366 MS MSD 92349104001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Sulfide mg/L ND .5 .5 0.48 0.48 96 96 80-120 0 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 41 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 1 QC Batch: 370558 Analysis Method: EPA 300.0 l QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92348913001 METHOD BLANK: 2053285 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fluoride mg/L ND 0.10 07/30/17 13:26 Sulfate mg/L ND 1.0 07/30/17 13:26 LABORATORY CONTROL SAMPLE: 2053286 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Fluoride mg/L 2.5 2.7 108 90-110 Sulfate mg/L 50 54.4 109 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2053287 2053288 MS MSD 92348833001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Fluoride mg/L 10.9 2.5 2.5 14.5 13.9 146 120 90-110 5 M6 Sulfate mg/L 5760 50 50 5770 5740 33 -32 90-110 1 M6 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2053289 2053290 MS MSD 92348730008 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Fluoride mg/L ND 2.5 2.5 3.4 3.4 134 135 90-110 0 M1 Sulfate mg/L 5.2 50 50 75.1 75.1 140 140 90-110 0 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 26 of 41 i Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371344 Analysis Method: EPA 350.1 1993 Rev 2.0 QC Batch Method: EPA 350.1 1993 Rev 2.0 Analysis Description: 350.1 Ammonia Associated Lab Samples: 92348913001 METHOD BLANK: 2057310 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,Ammonia mg/L ND 0.10 08/01/17 14:42 LABORATORY CONTROL SAMPLE: 2057311 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,Ammonia mg/L 5 4.9 98 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057312 2057313 MS MSD 92348842027 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Ammonia mg/L 1.7 5 5 6.4 6.4 94 94 90-110 0 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057314 2057315 MS MSD 92348913001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,Ammonia mg/L ND 5 5 4.9 4.9 98 98 90-110 0 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 41 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 _ aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371277 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate+Nitrite,preserved Associated Lab Samples: 92348913001 METHOD BLANK: 2057068 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen,NO2 plus NO3 mg/L ND 0.020 08/01/17 03:54 LABORATORY CONTROL SAMPLE: 2057069 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen,NO2 plus NO3 mg/L 2.5 2.5 98 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057070 2057071 MS MSD 92349334008 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,NO2 plus NO3 mg/L ND 2.5 2.5 2.6 2.6 103 102 75-125 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057072 2057073 MS MSD 92349326001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Nitrogen,NO2 plus NO3 mg/L 8.3 2.5 2.5 10.9 11.0 104 109 75-125 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 28 of 41 Pace Analytical Services,LLC /+Q/fin /+ ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370723 Analysis Method: EPA 420.4 QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics Associated Lab Samples: 92348913002 METHOD BLANK: 2054277 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phenol mg/L ND 0.010 07/31/17 13:32 LABORATORY CONTROL SAMPLE: 2054278 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Phenol mg/L .05 0.049 98 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2054279 2054280 MS MSD 92347765002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phenol mg/L 43.7 .05 .05 0.16 0.16 235 240 90-110 2 M1 ug/L MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2054281 2054282 MS MSD 92348521002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phenol mg/L 1.5 .05 .05 1.5 1.5 2 -44 90-110 2 M6 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 29 of 41 Pace Analytical Services,LLC QD 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371302 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 4500CNE Cyanide,Total Associated Lab Samples: 92348913002 METHOD BLANK: 2057187 Matrix: Water Associated Lab Samples: 92348913002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide mg/L ND 0.0080 08/02/17 05:26 LABORATORY CONTROL SAMPLE: 2057188 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Cyanide mg/L .1 0.099 99 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057189 2057190 MS MSD 92349156001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Cyanide mg/L ND .1 .1 0.099 0.096 94 90 80-120 3 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057191 2057192 MS MSD 92348937001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Cyanide mg/L ND .1 .1 0.11 0.10 104 94 80-120 10 ResultsP resented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 30 of 41 Pace Analytical Services,LLC ace9800 Kincey Ave. Suite 100 Analytical Huntersville,NC 28078 wwwpacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 371309 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310B TOC Associated Lab Samples: 92348913001 METHOD BLANK: 2057215 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 08/02/17 18:51 LABORATORY CONTROL SAMPLE: 2057216 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.4 94 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057217 2057218 MS MSD 92349334006 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Total Organic Carbon mg/L 4.0 25 25 26.4 26.1 90 88 90-110 1 M1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2057219 2057220 MS MSD 92348968003 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Total Organic Carbon mg/L 1.4 25 25 23.6 23.7 89 89 90-110 0 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 31 of 41 Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 aaceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 QC Batch: 370541 Analysis Method: EPA 7196 QC Batch Method: EPA 7196 Analysis Description: 7196 Chromium,Hexavalent Associated Lab Samples: 92348913001 METHOD BLANK: 2053247 Matrix: Water Associated Lab Samples: 92348913001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chromium,Hexavalent mg/L ND 0.010 07/26/17 05:41 LABORATORY CONTROL SAMPLE: 2053248 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chromium,Hexavalent mg/L .25 0.27 107 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2053249 2053250 MS MSD 92348913001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chromium,Hexavalent mg/L ND .25 .25 0.20 0.20 79 80 75-125 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 32 of 41 Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 /112aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services-Asheville PASI-C Pace Analytical Services-Charlotte PASI-E Pace Analytical Services-Eden ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. P5 The EPA or method required sample preservation degrades this compound,therefore acceptable recoveries may not be achieved in sample matrix spikes. R1 RPD value was outside control limits. c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 33 of 41 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Annual Sampling 07/25/17 Pace Project No.: 92348913 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92348913002 Effluent Grab SM 2120E Color ADMI 370563 92348913002 Effluent Grab EPA 1664B 371460 92348913002 Effluent Grab EPA 3510 370645 EPA 8081 370726 92348913002 Effluent Grab EPA 3510 370359 EPA 8082 370550 92348913001 Effluent Comp EPA 3010A 371135 EPA 6010 371329 92348913001 Effluent Comp EPA 7470 370574 EPA 7470 370636 92348913002 Effluent Grab EPA 3510 370788 EPA 8270 370919 92348913002 Effluent Grab EPA 8260 371101 92348913002 Effluent Grab SM 4500-52D 370915 92348913001 Effluent Comp EPA 300.0 370558 92348913001 Effluent Comp EPA 350.1 1993 Rev 2.0 371344 92348913001 Effluent Comp EPA 353.2 371277 92348913002 Effluent Grab EPA 420.4 370723 92348913002 Effluent Grab SM 4500-CN-E 371302 92348913001 Effluent Comp SM 5310B 371309 92348913001 Effluent Comp EPA 7196 370541 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, I Date:08/04/2017 05:20 PM without the written consent of Pace Analytical Services,LLC. Page 34 of 41 uocument Name: uocument Kevisea:Sept.11,201b �aceAnalytical a Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Laboratory receiving samples: Asheville❑ Edens I Greenwood❑ Huntersville h Raleigh Mechanicsville❑ Sample Condition Upon Client Name: W 0# : 92348913 Receipt ---' t� Project p � 1 �' , II 1111111111111111111 Courier: Fed Ex Dips ❑USPS ❑Client 0 Commercial (L!:l0ace ['Other: 92348913 I 1 Custody Seal Present? Dyes t ❑No Seals Intact? Oyes (❑No 1, �A I I Date/Initials Person Examining Contends: 2- .A.\ Packing Material: ❑Bubble Wrap ❑Bubble Bags [}None ❑Other: _ Thermometer: n ' ^ s-� 4\A/et ❑Blue None t (T„}-�amples on ice,cooling process has begun [i IR Gun ID: \lyO J Type of Ice: // Correction Factor: Cooler Temp Corrected(°C): l•°�, Biological Tissue Frozen? Dyes riip EIN/A Temp should be above freezing to 6'C USDA Regulated Soil(D N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally, Oyes ON). including Hawaii and Puerto Rico)?['Yes .ONo Comments/Discrepancy: Chain of Custody Present? 'OYes ❑No ON/A 1. Samples Arrived within Hold Time? 0t4e's ❑No ON/A 2. Short Hold Time Analysis(<72 hr.)? (❑Yes ❑No ON/A 3. Rush Turn Around Time Requested? Oyes k_QNo ON/A 4. Sufficient Volume? TPes ❑No ❑N/A 5. Correct Containers Used? pies ❑No ON/A 6. -Pace Containers Used? ,Clies ❑No ON/A Containers Intact? `Q1es ❑No ON/A 7. Samples Field Filtered? Oyes ❑No t-.1:14/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? `� 1 _ tQ1>es ❑No ON/A 9. 1`tmcC no (om. cAk cop.ik 4vZ� -Includes Date/Time/ID/Analysis Matrix: `��'/� Headspace in VOA Vials(>5-6mm)? ❑Yes ❑No .Efi1+)/A 10. Trip Blank Present? Oyes Duo ON/A 11. Trip Blank Custody Seals Present? I Des ❑No _QN/A CLIENT NOTIFICATION/RESOLUTION Field Data Required? Des ❑No Person Contacted: Date/Time: Comments/Sample Discrepancy: Project Manager SCURF Review: , i k. L •l Date: I), z 11'! Project Manager SRF Review: ✓/ t,-1.:-- Date: II?-U I I Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(i.e. Out of hold,incorrect preservative,out of temp,incorrect containers) Page 35 of 41 N N N W CO -J 01 V. A W N N * * m N o Item* t* m _ m //7///////// BP4U-125 mL Plastic Unpreserved(N/A)(Cl-) K rD t n O O BP3U-250 mL Plastic UnpreservedN/A) Q- ( O 13.) y y 7 Z jr J BP2U-500 mL Plastic Unpreserved(N/A) -.. rtr fl- C m13 0 3 2. BP1U-1 liter Plastic Unpreserved(N/A) is �_ - W x N of St -w Cb� ""� is� BP3S-250 ml Plastic H2504(pH<2)(CI-) H . p ::fD 0_. al Fi- r) T BP3N-250 mL plastic HNO3(pH<2) O vri x O l . BP32-250 mL Plastic ZN Acetate &NaOH(>9) 3 -- x J C y = 30 / BP3C-250 mL Plastic NaOH (pH>12)(Cl-) s ( 7 -I - \ CD.rg 'C WGFU-Wide-mouthed Glass jar Unpreserved 0 Di O _ 00 G D -- AG1U-1 liter Amber Unpreserved(N/A)(Cl-) m. n an d Q S O iir co C / /� / / / / // 1� / AG1H-1 liter Amber HCI(pH<2) ril 13 ID. 3 /// / / / 7 r' m al AG3U-250 mL Amber Unpreserved(N/A)(Cl-) Di = 0 m .-•• O z o �' o mI- AG1S-1 liter Amber H2SO4(pH<2) O m c 3 . O Ui 3 g I� w m v a -9, Ar AG3S-250 mL Amber H2504(pH<2) W O Z Aeir E, z Z 0 au 3 a AG3A(DG3A)-250 mL Amber NH4CI(N/A)(CI-) C 0 IV m I- — .. A) �� DG9H-40 mL VOA HCI (N/A) v, 3• O VG9T-40 mL VOA Na2S203(N/A) n A D., D 0- ,- a St N N N VG9U-40 ml VOA Unp(N/A) rir m 0. to , o DG9P-40 ml VOA H3PO4(N/A) N 3 3 Z 3 O o VOAK(6 vials per kit)-5035 kit(N/A) -I = n 2 . .- 03 '�F 3 D V/GK(3 vials per kit)-VPH/Gas kit(N/A) N d N O 1 m , -0 P3 !D SPST-125 ml Sterile Plastic(N/A-lab) j N A ao r°Oo N. e« n SP2T-250 mLSterilePlastic (N/A-lab) 0 < o CL 0w N n m / N• Z. A ...g.: W r, m Z. BP3A-250 mL Plastic(NH2)2504(9.3-9.7) A No m Cubitainer (4Oo c3 co o VSGU-20 mL Scintillation vials (N/A) oho m a _ CO 0) GN v o_ A CHAIN-OF-CUSTODY I Analytical Request Document paceAnalytical The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. /� www.pacelabs.com Page: ! of Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: CompanyEReport To: y ,.....7 Attention: Address: �� To: 7 ���1•/ (ICU 1 __ -._. _ _ i‹.10%) _ L j�Lf�} Copy ! Company Name: REGULATORY AGENCY f I i‹. tiT ri J�l-"z- ,2-1 Address: NPDES GROUND WATER DRINKING WATER Email To. / f Purchase Order No.: Pace Quote UST RCRA OTHER Reference: Phone: Fax: Project Name: Paco Prefect - Site Location Manager: Requested Due Date/TAT: Project Number: Pace Profile U. STATE: Requested Analysis Filtered(YIN) ..► Section D Matrix Codes 11.- _ Required Client Information MATRIX/CODE - o COLLECTED Preservatives i Drinking Water DW . O z -', -. Water WT ',u 3 O j v Waste Water WW m COMPOSITE COMPOSITE U Ir_� `] Product P - START END/GRAB w Vi .t -•� •}f5 - Z SodJSolid SL 0 O y V ', -tee J 1° } SAMPLE ID oil oL _ ,° c- =t'1 �, Wipe WP N w N -. .� 4 .� ?- (A-Z.0.91.-) AirAR O w a Z h '�� 1y�7 `: G J o Sample IDs MUST BE UNIQUE Tissue TS O a r dpi y "P •a �' v c ( O e f•-:::.,, r Other OT 0 'rw- Z a 'y S.,ti G ? 0 Lt' J _ll '� U CO o J 6 1 # X w w O N O C a J See �+ J U E F- a a tui d O O = u5 .c m c0 -,-L .1 -3 r f 7-32 r;. 't.l 9-9 l ia ¢ a ¢ O c• Z U O ca m = C OJ L� 4 G om•'� !`! c i +' ...,., 2 + 44 rn DATE TIME DATE TIME rn a D _ I I Z Z 2 O y 1!'� G�`�"- -GG. `J cc Pace Project No./Lab I.D. 1 F�c. `H UE A..,t . C-c%;,� ) c 7-3M 17 C 1s.�.7 =i 7 c r.;'i 7 �( i 2 T F'�! t1 s•ti.•r C rt_V1 ti,. q. — 7:2517 �!t'� �� �� X'A. 'f'f L)es[ i/1 ,-.' 3 4 5 6 8 9 10 11 i 12 ADDITIONAL COMMENTS " RELINQUISHED V I AFFILIATION DATE TIME AC5EPTED BY!AFFILIATION DATE TIME SAMPLE CONDITIONS .re(i , f`�nti 7_ =j�V/�J �--- � 22S'. ' QJ�_r _'`� �G�- 7.11-��, flys (15 SAMPLER NAME AND SIGNATURE o^ 1 Zi C.3 PRINT Name of SAMPLER: / I J(0 `- 75 ?> o ci} Is- n a m DATE Signed m v E c i" ` E SIGNATURE of SAMPLER: --77 t- cc a c '..,,,:z.42:/// (MWDD(YY): c 7- :X.('^� 7 v: N important Nolo:By signing fres form you am accepting Pace's NET 30 day payment terns and agroomg fe late charges of 1.5%per month for Try Invoices not paid within 30 days./ j F-ALL-0-02Orev.07.15-May-2007 o� CHAIN-OF-CUSTODY / Analytical Request Document PaceAnalytical The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. www.pacelabs.cont Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company. Report To 1 I Attention: _ (7 lt2fL.,I 7C;_ty -- — Address !•7 --/-- j ` Copypto: Company Name REGULATORY AGENCY r t IBJ-ltv f'j I(�t yLIC- Address: < -2.1.„,5/4,-,,, NPDES GROUNDWATER DRINKING WATER Email To: '7✓t-'i i Purchase Order No' Roto error UST RCRA OTHER J Reference Phone: Fax- Protect Name PiiBO['lei,: Site Location Mariam, Requested Due Date/TAT: Project Number: Pace Prolde a STATE' Requested Analysis Filtered(YIN) Section D Matrix Codes - z RequiredChent Information MATRIX r CS/QF - COLLECTED Preservatives i _ Drinking Water DW T, O0 z _ Water WT o U Waste Water WW m coMnos.rt cnslvc rant" w J ‘7'. _Z Product P a START END'GRnB _ Soil.'Solid SL r SAMPLE ID w e S W 2 p 4 d � 1J o (A-Z.0-91,-) Air W AR O w a a F- n Sample IDs MUST BE UNIQUE Tissue TS 0 a- `w 2j- a) H ,::I U Other OT X tu u1 O N O c a U 3 Lu ¢ `¢ a O a O, ZZ U O m m E.m Q 2% '' d .j.. / t /N" DATE TIME DATE %� TIME 0% D I I I Z Z 2 O y CC�/C/�:, • 25 Pace Project No.!Lab I.D. 1 ( f—`'/t i.1:. 1 - l 7 j�-- �l y t '' — 7-Z)=//jL: — ?Y ',X x .- 2 [ f 3 4 5 6 7 8 9 10 r 11 1 12 ADDITIONAL COMMENTS RELINQUISHED-BV I AFFILIATION _ DATE V TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS </1. � a.y l 251 2 1 3 %• � �!7� ! l r �� -O m M SAMPLER NAME AND SIGNATURE ,� o 5 5 o, ORIGINAL �f o T o C PRINT Name of SAMPLER ( y / a ( 0 / „ > a} a -t 7DATE Signed __ =�_ A SIGNATURE of SAMPLER: / '- ce v U / / (MIWDD/YY): ci 7�._ I N N -important Note:By signing this lorm you are accepting Pace's NET 30 day payment terms and agremen to late chary,of 1 5'1 per month It :py vel ens not 0:111 within:10 iI:lys ' / F-ALL-O-020rev.07,15-May-2007 1 1 I Analytical Results Pace Analytical ®� 9800 Kincey Suite 100 Huntersville, NC 28078 Receive Date: 07/26/2017 STATESVILLE Reported: 07/27/2017 ANALYTICAL For: 92348913 � 1 Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 170726-10-01 MBAS Eff 0.18 mg/L SM5540C-2000 07/27/2017 CL ,Rlespectfully submitted, 0 Dena Myers NC Cert#440, NCDW Cert#37755, EPA#NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 rage 39 of 41 Condition of Receipt Sample Number 170726-10-01 Temp on Arrival: 2 Parameter Schedule: MBAS Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 rage 40 of 41 N 0 rn ',:r- LO rN cEL t\ co W Chain of Custody `° a o^ a. aceAnalytical , / ww�..pxeleb1 corn t\ 1 CO W Workorder:92348913 Workorder Name: Effluent 07125/1 1 Results Requested By: 8/8/2017 cc cv --�—^--^ n k f J6C!P>iaj'Subogntraat'[t�" lilt iv..v . ifi?.i�4ir inEsr: = fe::f id; iReq-i ested:Analystsso ti4t ca d U Ri3�ort�IovoioeTo` = , f z Matthew Brainard P rv`1' (�� Pace Analytical Charlotte 9800 Kincey Ave. Suite 100 .-tcoleS.i41t C A H4l r_`1' vl Huntersville,NC 28078 oo v Phone(704)875-9092 Email:matthew.brainard@pacelabs.com `n 2 • 2 co ?P e5 iMid ofltalnterei.t"�. ;, co State of Sample Origin: NC 20x y{�v ��r ?$r+i. ,- 6 FAY '� a p tom e jam_� , •„ 4of1 :z , !Vie' LAB USE ONLY Effluent � x �r1O"t Q-1� 1 Etf uent Grao 7/252017 07:40 92348913002 Water 2 --f✓•- 3 _ - — . 4 4 - 5grol;'�' + ' `QT c "`-m"__:s„ r..;r D '41' "-r i . 24..xF. rumen's -.a .F��Fr'liMa. s c x ;x s Y Transfers Released By Date/Time Received �4 { ate/Time 1 NI{Zls 7/7 ki'3d LWJ?SGC 7iZ417 x:0-00,m 2 3 LCooler Temperature on Receipt 91 °C I Custody Seal Y or N _ Received on Ice/Y for N I Samples Intact I r/or N IAC I FMT-ALL-C-002rev-00 24March2009 Page 1 of I Tuesday,July 25,2017 3:19'39 PM Duvaltex (US) , Inc . EPA ID # NC0005312 Appendix D DMRs NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:959696 GRADE:WW-4. ORC HAS CHANGED:Na eDMR PERIOD:01-2017{January 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO • aMaso 009141 04400 50064 Q0310 00034 31014 00004 C0645 e S a e e g Continuous 5 X<ask 5 X week S X week 5 X week 5 X wsk 2 X month Monthly sfanchl o < F h E Y Y Z . U Recorder Grab Grab Grab Composite Composite Grab Composite Compr rite Z 6 ss s F J q C i FLOWTT:ANC pll (l4[PA114F, boa-Qrr 0.07 TSS.Qry D.n3 FCOLI Mt TOTAL N• TOTAL P•f..ar J 14046.16 lir. 3404 r1uck On MIN mgd doge su ug/1 Ibs7Say lbs/lay 40100m1 me/1 mei 1 0700 _ y 0.03351 1 0700 2 y 0.03423 3 0715 24 0700 9 0.07158 7 7.2S <2$ 2 8 <3 0.56 2.3 4 0115 24 0700 9 y 0.04/88 7.7 7.41 <25 <I <6 3 0715 24 0700 9 y 0,04097 5.6 7.39 <25 1 34 6 0715 24 07009 y 0.0485 5.2 7.33 <25 I 5 T 1000 2 a 0.0485 4 1 a 0945 2 n 0.03686 0713 24 0100 9 y 0.05664 0.5 7.34 <32 3 26 , 1a 0315 ,24 0100 9 y 0.05332 _0.3 7.39 <25 I 22 11 0715 24 0700 9 y 0.04919 1.2 73 <25 2 11 12 0715 34 0700 9 y 0.047 2.4 7.32 <25 I 4 13 0715 24 0700 9 y 0.03859 4.4 732 <25 1 6 14 0700 y i 0.04559 i13 1 0700 2 Y 0.05543 16 0700 9 y 0.05961 12 071$ 24 0700 9 ,y 0.05364 7-6 7.08 <25 2 1$ <2 14 071$ 24 0700 9 y 0.03851 0.4 7.13 <25 2 15 r 17 0715 24 0700 9 y 0.07624 7.6 7,35 <25 4 10 30 0715 24 0700 9 y 0.11923 95 7.37 <25 6 14 71 0630 2 n 0.14219 11 0630 1 n 0.01761 J 0715 24 0700 9 y 0.10152 10.2 7.33 <25 4 _22 u 0745 24 ,0700 9 y 0,30421 101 7.35 <25 10 43 ( rs 0713 24 0700 9 y 0.00844 9.1 7.29 <25 3 24 16 0715 24 0700 9 y 0.08282 9.5 7.39 <25 2 9 1T 0715 24 0700 9 y 0.10993 3.1 7.29 <25 4 21 1a_ 070U r 0.88381 10 0700 2 Y 0.07974 34 071$ 24 0700 9 y 0.06471 5.3 7.41 <23 2 6 31 0715 24 0700 9 Y 0.05396 4 7.4 <25 1 9 mn Ar. hly A. .ye GIME4 1111.! r171.3 104 Afmraty Aron.: , 0.070266 6.14 0 2.6 15.3 1 0.56 23 o.0y A7..1nn4m: 0.30421 10.2 7R1 0 10 45 0 0.56 2.3 0.00 31/of marl: 0.01701 0.3 7.08 0 0 0 0 0.56 2.3 ••••Na Reporting Reason:ENFRUSE=No FIosv-Reuse/Recycic; ENVW7HR=No VLsitatiun-Adverse Wcadloe;NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday I NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4, COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eD1MR PERIOD:01-2017(January 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:NO (Continue) 01014 00.10 17710 00745 F F C 8 ' e t 2 X mond, Wokl 2 X month 2X month r. < F • I g s O` € Composite Com.oak Grab Grab 1 at 2 2 P- 7 .3 O Cr-TOTAU COO P1tER11l SULFIDE 1400 cwrl< .4000«t lbsJday Ibslday lbs/day Ibiday 0700 0700 0715 0700 0,013 38 0.008 <0.06 4 0715 I 0700 II 4 0715 0700 4 0715 0700 1 1000 0 0945 9 0715 0700 10 0715 0700 26 1:::: 10700 0700 II MI0715 ®0700 MIMI I__I: ®I® ®0700 ME 0.005 !0.004 <0.04 NI 0715 ®0700 MEE._�_ -- 1:_1:0MO 0 I " 07 ©M_ 1071$_1700 ®®®0700 IIIIINIIII_ 754 ®0719 ®0700 11111111111 76 0715 ll 0700 111111 v 0715 0700 5a n700 2 y �9 0700 2 y 10 0715 24 0700 9 31 0715 24 0700 9 y 34 01•0Nly,irarav tlmn: [.5 15745 IS 1 MenlIly Average: 0.009 78.2 0,004 0 Daly Naef,nvm: 0,013 254 0.008 0 Daily Mlatmom: 0.005 26 0 0 •••eNoReporting Reason[ENFRUSE=No Flow•Rcuse/Recyetc;ENVWTHRn.NoVisitation—AdverseWeather;NOFLOW=No Flow;HOLIDAY=NoVisitation—Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:01-2017(January 20172 VERSION:1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE#:3368351083 SUBMISSION DATE:02/16/2017 -.- f& dot,..---k--.. 02-- 1 7—) 02/16/2017 ORC/Certifier Signature: Ole E Gary E-Maitl:glen.gary@truetextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any infomtation shalt be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II,E.6 of the NPDESermit. �.�/ Gel�fl(r Z.:-- 0.L.— i7 II 02/16/2017 Permittee/Submitter Signature:** Scott Taylor E-Mail:scott.taylor@truetextiles,com Phone #:207-876-3331 x641& Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date:12131/2018 I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB#:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting Iittp://ponal.nedenr.org/web/wq/swp/ps/npdes/forms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there arc no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204. ***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No cDMR PERIOD:01-2017(January 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: Contract Laboratory Qualified Lab Data: In observance of the state holidays no samples were taken on January 2 and 16. AeALAe..January 03,Effluent TSS The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/1. WLAE January 09,Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples may be biased low. NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4, COUNTY:Sum OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:984696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.:001 NO DISCHARGE*:NO ` '" y 39659 90111 66406 OM 947119 00531 33109C«« 10461 a F 6. TJ I i I i r Coatings 5 X week 5 X pock $X week 5 X week 5 X week 2 X month Monthly Monthly E _ E E F a f Recorder _Gob Grab Grab Composite Composite Gast' Composite Composite o -c O I z FLOW TLMF•C 90 CKtbR1NI 800•Qty Palk 105 Qty D411y 1007.316 TOTAL X• TOTAL r-Ccsc 249444 nth 201 cW6 MI 94849 mOd dcyc u 41 11M/day lbs/day 41100m1 mtfl mei 1 0715 24 0700 9 y 0.05413 4,9 736 <25 1 7 2 0715 24 0700 9 -Y 0.0337 5.4 7.24 <20 I _2 _ a 0715 24 0700 9 y 0.23141 _6.7 7.14 <25 6 26 4 0650 2 n 0.077 5 0630 2 .n 00203 , - 4 0715 24 0700 9 y 0.04575 4,2 7.10 <23 2 13 7 -0715 24 0700 9 y 0.07077 5,9 6.67 <25 5 _29 <1 1.13 2.7 4 07)5 24 0700 9 y 0.04379 7.6 7.11 <25 3 15 0715 24 0700 9 y 0.03878 8,5 7.24 <25 2 13 , 71 0715 24 0700 9 y 00471 5.4 7.2 <25 3 11 0700 2 7 0,06546 . 1 12 0700 2 y 0.02446 { '7 0725 24 0700 9 y ,0.0697E 8.7 7,18 <25 3 5 14 6715 24 0700 9 y 004152 7.1 722 <25 1 14 15 0715 24 0700 9 y 0.07728 7.9 7.14 <2.5 3 _a to 0715 24 0700 9 y 0.07713 6.5 7.2 <25 2 19 17 0715 24 0700 9 y 0,04513 6 6.68 <25 J 2 5 to 0630 2 n 0,0747 _ _ + 19 0630 2 n 0.0199 V 74 0713 24 0700 9 y 0.03863 7.9 7.22 <25 1 3 _ . 21 071$ 24 0700 9 ,y 0,04652 8.5 6,46 <25 2 6 <I 21 0715 24 0700 9 y 0.07322 9.4 7,14 <25 2 12 73 0715 24 0700 9 y 0.07772 10,4 7.14 <25 3 13 34 0715 24 0706 9 y 0.07766 11.3 1.1 <25 3 9 25 0700 2 y 007395 24 0700 2 Y 0.0273$ • 27 0715 24 0700 9 .y 0.066E9 PYA 7.27 <25 3 Ii 2E 0715 24 0700 9 y 0.01107 8.9 7.19 <25 6 7 9444,40y4oMact UAW:4 a r 1014 2713 200 McOtklyAwara:0.061536 7.49 0 2.7 II I 1.13 2.7 1).17y141u4a m 0.23141 113 1,35 0 r6 29 0 .1.13 2.7 runy511aaae'0.0199 14.2 6.46 t0 1 2 0 _1.13 ,2.7 "r"NO Repelling Reason;ENFRUSIi-NoFlow•Reuse/Recycic; ENVWTHR=NoVisitation-Advent Weather,3.00FL0W=NoFlow;HOG[DAY=NoVisilntior.-Holiday H NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 List Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:984696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) t 91334 0001* TOP3a 32730 .1711 I n 3 ,� ) s E 2 X meads Wcs1ly Qcanerly 2 X month 2 X month p < v y g a Composite Compmitc C•.•.•rite Gmb Gnb a s C V - k O T. Cm70141, COD CTR17044, 3171370E 1*adot 9 R.r •.00300«4 Rn WI" &Idly lbt114y .. '1 ibrld* i 1 0715 .24 0700 4 y i 2 0715 24 0700 9 y 1 0715 24 0700 .9 y 4 0630 2 n 5 0630 2 a * 0715 24 0700 9 Y 7 0715 24 0700 9 y 0.009 81 1 <0.01 <0.05 4 0715 24 0709 9 9 0 0715 24 _0700 9 y 10 0715 24 0700 9 y i1 0700 2 y 12 0100 2 Y )3 0715 24 0700 9 y H 0715 24 0700 9 y 40 05 0715 24 0700 9 y i _ K 971$ 24 0700 9 2 . 17 0715 24 ,0700 4 9 y II 0630 2 n 19 0630 7 n 2* 0715 24 0700 9 y 31 0715 24 6700 9 y 0.036 43 0.004 <0.04 27 0715 24 0700 9 y 21 0715 24 0700 9 y 24 0715 24 0700 9 y r 0700 2 ..y 29 0700 2 y 17 0713 24 07009 y 30 0715 24 .0700 }9 y 29 Mml*.y A.mp lies: 17 15215 23 3 13t3at►ry"map: 0.0075 0.25 i 0.002 0 Dos M=dmes: 0.009 Et 1 0004 0 047 Mtulde... 0.006 29 1 0 0 '•'•No Reporting itemon7 ENFRUSE=No F10w.Rsuse/Recycle;ENVWFHR=140 Visitation-Adver*e Weathcr, NOFLOW-No Flow; HOLIDAY=No Visittlinc—Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW.4, COUNTY:Scary OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE#:3368351083 SUBMISSION DATE:03/15(2017 f 7 03/14/2017 ORC/Certifier Signature: GI E Gary E-Mail:glen.gary@truetextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. Regional Office anynoncompliance that potentially threatens public health or the environment. The permittee shall report to the Director or the appropriategt Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. lithe facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDES permit, 03/15/2017 Permittee/Submitter Signature:*** / cott Taylor E-Mail:scott.taylar@truetextiles.com Phone 4:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date:12/31/2018 1 certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the infomtation submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, .accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB K:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/fortns. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. ••ORC on Site?:ORC must visit facility and document visitation of facility as required per I5A NCAC 80_0204. •••Signature of Permittee:If signed by other than the perrttittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surly OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: Contract Laboratory Qualified Lab Data: la February 02,07,13 and 27 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples may be biased low. 840 February 24,Effluent TSS The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/I. NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW.4. COUNTY:Surry OWNER NAME:True Textiles lac ORC:Glen Edward Gary ORC CERT NUMBER:939696 GRADE:MW-4. ORC HAS CHANGED:No eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:NO k46 awn 09401 54040 00511 90539 51111 C0400 C04044s 9 1 ' 8 . a E 4 : Continuous 5 X work 5 X week $X week 5 X wed 5 X week 2 X month Monthly Monthly it It < y I V ST♦ e S Fte:order Grab Grab Gnb COtwposile Composite � Composite Composite I 6 4 E C r o 0 3. PLOW 7ar4rC pM cMeoxtxc GOD•gyoe0y 'MS-QryDaly scoltaa Torun- TOTAL r.a.4 Us4.Ak Nes 3400 41•4 Mn 914.74 MO 4e8e c us/1 lbdd4y 164A16y ,0110061 m91 4n0 1 0713 24 0700 9 y 0.05972 10.7 7.08 <25 1 11 2 0715 24 0700 9 y 0.04655 1 10 3 0 0700 4 y 54001-040 4 0630 2 0 NOFLOW 5 0630 2 n 0.01492 4 0755 24 0700 9 y 096878 7.7 7 <251 12 7 0715 24 0.700 9 y 0.07495 ,9.4 7.16 <25 2 14 <1 0.71 2.6 t 0713 14 0700 9 y 0.18589 10.7 7.32 <25 7 34 t 0715 24 0700 9 y 0.31414 103 6.94 <75 9 16 , 11 0715 24 ,0700 9 y )0.04543 9.9 7.22 <25 2 2 s 0700 3 ,y 0.03241 12 9700 2 ,y 0 , 15 0715 24 0700 9 .y 0,03564 4 93 6,4 ,<25 2 3 t1 0715 24 0700 .9 y 0.01422 69 7.96 <25 0.3 3 . \ 11 0715 24 0700 9 y 0.04475 4.6 714 <23 1 5 u. 0715 24 0700 9 ,y 0.05231 3.4 7.24 <25 2 2 17 0715 24 0700 9 y 0.02556 31 7.07 <29 1 1 It 0630 2 n 0.02152 1t 0630 2 n 0.02031 1. S0 0715 24 0700 9 y 0.03699 5.9 7.27 <25 1 11 23 0715 24 0700 9 y 0.0158 J 7.7 6.78 <25 1 3 1<.1 32 0715 24 ,0700 9 y 0.05055 10 7.2 <25 2 8 1 13 0715 24 0700 9 y 0.04002 0 7.34 <2S 2 1 U 0715 24 0700 9 y 0.114 9 7.22 <25 4 6 15 0700 2 y 0.0443 u ,0700 2 y 0.02509 27 0735 24 0700 9 y 003859 12.6 7.17 ..425 1 2 14 0715 24 0700 - 4 y 0.04644 13.7 7.15 <25 2 9 19 0715 24 0700 9 y 0.10039 13,6 7.26 <25 4 $ 38 0715 24 0700 9 y 0.06223 14.6 7.15 <28 4 9 _ 51 0715 24 0700 9 y 0.2021 143 7.04 <2.0 3 35 /442414 Avotore llmin 4 141.6 5721 101 M.e111y Awrett: 0.066883 9,27619 0 2.413636 4.707273 1 0.71 2.6 0017a1.v..~. 0.31414 14.6 7.34 0 t 33 0 0.71 2.6 Daily a1O1"" 0 3.2 6,4 0 0.5 1 0 0.71 2.6 .""No Reyorling Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-,Advuse Weather, NOFLOW-No Flow: HOLIDAY=No Visitation-Holiday NPDES PERMIT NO.:NC00053 12 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:NO (Continue) 1 01704 44540 172714 04745 r = d n o 1F i i 2Xmon01 Weddy 2Xmoat 2X month Iu ag I Composite Commit: Onb Ore, a C+ FS• C O O T. Cr.707AL COD rim,TR SULFIDE lam elate nn 2440 Oesk An VILLA :y1do mkslynldoy tte/0oy ., *0715 24 0700 =I _ 0715 0700 9 III 0710 9 NOFLOW 0630 2 NOFLOW MI0630 ©M 111 0715 ®0700 MEM 1 In0715 24 0700 =P—0.005 41 <0.01 (<0.06 0715 I 0700 NO 0715 0700 0715 0700 IN 0790 0700 22 11111� 0715I24 0700 0725 11 24 0700 9 0715 24 0700 0715 24 0700 I 0700 1111 0630 0630 I::: 24 0700 9 y 27 0715 24 0700 9 y 0.902 250.003 <0.03 51 0715 24 0700 9 y =7 0715 21 0700 9 y u 0715 24 0700 9 0700 ill 0700 24 0700 24 0715 24 0700 9 y 35 2> 0715 24 0700 9 y 59 0715 24 0700 9 y II 0715 24 _0700 9 Y Met Ary Anrep 1411*:4 IS 1020.5 IS 3 Maattly Asmec 00070 27.5 0 0 Day Mahon.: 0.007 41 0 0 OkayNfvaaa, 0.002 9 0 0 ••••No Reporting Reoso=:ENFRUSE=No Flow-Reose/Rocycie; ENVWFHR-No Visitation-Adverse Weather; NOFLOW-No Flow; HOLIDAY—No V isitation—Hot oily NPDES PERMIT NO.:NC000S312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sun), OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE#:3368351083 SUBMISSION DATE:04/18/2017 uhC 01/- f 9- / 04/18/2017 ORC/Certifier Signature: en E�Gary E-Mail:glen.gary@trtfctextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part Il.E,6 of the NPDES� it. , „.,x_: erm 'e--5 :7( ` , cOj D,/ (g'-of 7 04/18/2017 Permittee/Submitter SignatuTaylor E-Mail:scott.taylor@truetextilcs.com Phone #:207-876.3331 x64I8 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/20I8 i certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB#:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there arc no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204. ***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY;Surry OWNER NAME:True Textiles Inc ORC;Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed Outtait 00]-Effluent Comments: A transformer blew on March 1,2017 power outage to site from 16:00 3/1 iG4 12:00 3/4 no flow during this lime Contract Laboratory Qualified Lab Data: f March 7,Effluent Phosphorus Matric spike recovery exceeded QC limits.Batch accepted based on laboratory control sample(LCS)recovery. l March 14,Effluent BOD The precision between the sample and sample duplicate exceeded laboratorQcontrol limits. af,0 March 15,Effluent TSS The precision between the sample and sample duplicate exceeded laboratory control limits. ii„0 March 20,Effluent BOD The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/l. ite March 28,30 and 31 Effluent HOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples may be biased low. • • NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No I eDMR PERIOD:04-2017(April 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:NO 50400 46619 1444 54440 00110 00510 35415 C0641 C0445 d i ConSrua. 5 X week 5 X week 5 X week I X week 5 X week 2 Xa.ona Monthly Monthly ls+ F S Recorder IGrab Grab Grab Ccmpeale Compen0: l Grab Coiopaailc C0e9136o P a � a r mow fI TBMlC ellCA.0RII41. 100-Q.y 75407 755-44u 0a09 PCOW*4t 702AI.11. TOTAL?•Coe. 1 1416.A nn 2464 WO, }tin 10/111 Ind JI deg C N u93l 1b5/day 'Ibl/dly *100e1 me 391/1 1 D530 I2 n 0.17282 I 1 1 J 0630 2 n 0.01303 3 0715 24 0700 9 y 0.03715 13.4 7.12 <23 1 1 4 5715 24 0700 9 y 013913 143 6,45 <25 17 54 <1 0.52 2.3 $ 0715 24 0700 9 y 0.16816 14.8 63 <25 7 9 a 0715 24 0700 9 y 0.09606 15 6.82 <23 4 5 7 0715 24 0700 9 y 9133471 ILS 7.13 <25 6 13 4 0700 I Y 10.04199 10.05651 2 0700 2 y . 19 9715 24 0700 ,9 y 0.05436 11.9 7.22 <25 1 S 11 0715 24 0700 9 y 0.03055 13.2 7.24 <25 1 3 12 0715 24 0700 9 y 0.0509 14.9 73 <25 2 7 13 0715 24 0700 9 y 0,03405 14.0 7.4 <25 2 7 14 0630 2 n 0.11519 i5 0630 2 n 0.02 _ 14 0630 2 n 0.02539 1 u 0715 24 0700 9 y 0.0307 16.6 732 c25 1 4 14 0715 24 0700 9 y 0.07278 17.4 6.99 <25 3 13 <5 17 0715 24 0700 9 y 0.00222 16.6 737 <25 2 3 21 0715 24 0700 9 y 0,13097 16,4 7,28 <23 3 15 21 0715 0700 9 y 0.2483 17.7 7.22 <2S 7 30 51 0700 2 y 9.0934 22 0700 2 y 0,00429 n 0715 24 0700 9 y 0.14892 16.4 7.59 <25 4 7 5 0713 124 0700 9 v 0.17624 115.6 6.96 _<23 3 10 14 0715 )24 0700 9 y 0.27707 1 15.2 7.31 <27 6 19 • 77 0715 24 0700 9 y 0.52103 17.2 735 <25 4 3 74 0715 24 0700 9 y 0.10201 57,4 7.27 <25 3 6 77 0630 2 n 0.45405 34 0610 I n 0.02 MoondyAnmaget.:.16 4 CCC 111.1 2723 sec MamWy A.era(r: 0.10008 15.784211 C 4.052632 11,694737 II 0.52 2.3 Oa07 M.atnnr 0.27757 17.7 739 0 17 54 10 0.52 2.3 11'97Mnt.a.L/ 001103 11.9 6.48 0 1 1 10 032 2.3 •'••NoReponingReason:ENT-RUSE-No Flow•RcuScRccycle;ENVWTHR-NoVisilation-AdverseWeattler,NOFLOW=No Flow; HOLM AY-NoVisitalion-Holiday' r — NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4,0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:04-2017(April 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION:EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) • 11634 10341 02770 KM S KK S I F Z 2 X month Weekly 2 X month 2 X month I u I I S I Composite Composite Grab Gad, I; 44 a R V il t i O z C.-T07AL COD MIEN,711 S11I.TIDE 2444 chit (Ir4 246041.4k lin Y51174 ilasklay tbNday 165/64y Iteiday , 1 0630 2 n 2 0639 2 a 2 0715 24 0700 9 y 4 0715 24 0700 9 y 0.0I6 171 0.036 <0.19 3 0715 24 0700 9 y - I 3715 24 0700 9 y 7 0715 24 0700 9 y a ,0700 2 7 5 0700 2 y 1a 0715 124 0700 9 y 21 0715 24 0700 ,9 y 21 12 07(5 124 0700 9 y LI 0715 124 0700 9 y , 14 0630 2 a 15 0630 2 a 140630 2 n r 17 0715 24 0700 9 Y , 16 0715 24 0700 9 y 0.004 41 !3.0113 0.067 1$ y 0713 24 0700 9 _y 20 0715 24 0100 9 y 21 ,0715 ,0700 9 y tt 22 0700 2 y I 21 0700 2 y ` 14 0715 24 0700 9 y ff 00 0735 24 0709 9 y 85 21 0715 24 0700 9 y 27 0715 24 0700 9 y 1 24 0715 24 0700 9 y 2$ 0630 2 JA 0630 2 a MN1ny Ar4nae Vim' 1f 45245 13 7 Mw1117 Aran., 0.015 79.5 0.022 0.0333 o.orMali MOM: 0.076 171 0.036 0.067 a12r sllalc.r 0.004 21 6,000 0 •'44 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recyelg ENVWTITR-No Visitation Adverse Weather;NOFLOW No Row; HOLIDAY•No Visitation—Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:9.0 PERMIT STATUS:Active . FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Suny OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4, ORC HAS CHANGED:No eDMR PERIOD:04-20I7(April 2017) VERSION:L0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE k:3368351083 SUBMISSION DATE:OS/10/2017 � r7, {c�<., - ,'%'_`.r- 05/10/2017 ORC/Certifier Signature:� Glen Gary E-Mail:glen.gary®truetextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NP rmit. ���,�` \— vl , ) 05/10/2017 Permittee/Submitter Signature:*** colt Taylor E-Mail:scott.taylor@truetextiles.eom Phone #:207-876-3331 x641 S Date • Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date:12/31/2018 I certify,under penalty of law,that this document and all attachments were.prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB 4:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Cade assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.orgiweb/wglswp/ps/npdes/fotms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. *•ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 80.0204. ***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per ISA NCAC 2B .0506(b)(2)(D). - I NPDES PERMIT NO.:NC00053 t2 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:04-2017(April 2017) VERSION:1.0 STATUS;Processed Outfall 001-Effluent Comments: No samples on 04.14.2017 in observance of the state holiday, Contract Laboratory Qualified Lab Data: la April 17,21,24 and 28 Effluent ROD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples may be biased low. r ' NPDES PERMIT NO.:NC00053 12 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Swry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:05-2017(May 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.:001 NO DISCHARGE*: NO 18000 0002$ 00196 34040 (103111 00330 31414 00400 C0445 F v a „aZ s COntinuaa9 5Xweek 5Xwort 5Xwrt0 _5 Xseck 5Xweek 2Xmonth Monthly Monthly i $ t S 1 Rocooder Grab Grab Grab Coa a,3e Carpal-4 Grob Comporilt Conlwolllo ♦ t I £ R o U H O Q z FLOW TV4P.{ el CHLORINS TOO-12/1 Day TSS•Qt75011 1/00LI IR TOTAL N- TOTAL Y-Cee9 24a deet Ha 240 0.11 lin Y76171 mgd deg t u ugll Ila'day ,lbse ay 61100m1 mgk al 1 0715 24 0630 8 a 0.03872 20.9 7.22 <25 1 2 2 0715 24 0630 6 a 007469 12.9 7.24 <25 2 3 <I 0.68 1.9 III0715 24 0530 . 0.14056 18.1 7.28 <25 _ 15 6 3 0715 24 0630 8 n 0.19906 10.6 7.29 <25 6 23 4 0630 2 a 005564 , 7 0630 2 a 0.01897 1 0735 24 0700 9 y 0.03537 14.3 7,35 <25 I 5 I7 0715 24 0700 9 y ,0.05166 14.4 742 <25 I 4 14 0715 24 0700 9 y 0.05745 15.9 731 <25 1 2 _ 11 0715 24 0700 9 y 0.08433 17.8 732 <75 1 5 12 0713 24 0700 9 y 0.14494 183 737 <29 S 13 13 0700 2 y 0.00006 V 0700 2 y 0.07767 ! y 11 0715 24 0700 9 y 0.00364 17.4 7.45 <25 2 12 _ 14 0715 24 0700 0 y 0.03789 184 732 <23 I 9 1 77 0715 24 0700 9 0.05222 183 7,42 <25 3 10 14 0715 24 0704 9 y 0.0469 20 7.36 <75 2 12 19 0735 24 0700 9 y 0.17662 214 735 <25 7 29 to 0630 2 p 0.07909 21 0630 0 n 0. I02053 7 0715 24 0700 9 0.09213 20 7.35 <25 5 120 ✓ 0715 24 0700 9 n 0.47535 213 7.12 <25 19 132 - ' 2A 0715 24 0700 9 n 0318 19.8 707 <25 8 40 _ u 0715 24 0700 9 n 0.26943 19.9 7.36 <25 10 24 Z4 0715 24 0300 15 n 0.18563 19.2 7.29 <25 7 67 27 0700 4 y 0 L 0700 2 y 0,12174 27 0700 2 y 0.06626 34 0715 24 0700 9 y 006192 21,2 731 <25 2 6 31 0715 24 0700 9 0.04298 21.1 738 <25 2 Ar 1 6441.6 7 raie u.x: 4 101.6 272.3 214 aleetvyA.,rete' 0.103535 18.740909 0 4.227273 19.838112 1 9.60 1.9 Dep73y4nenl 0.41535 21.5 7.45 D 19 132 1 0.60 1.9 0143 641daeen10 143 7.07 0 _I .,2 0 0.68 1.9 44"4 No Reporting Rs Lien:ENFRVSE No Flow-Reuse/Recycle;ENVWCHR-No Visitation-Adverse Weather; NOFLOW i.No Flow; HOLIDAY=No Visitation-Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4,0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:05-2017(May 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION:EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) R • 414. 1,11/44 TCP28 327,4 4440 F a 0 r 4 f 7 Fr 2 X ma1Ut W[41119 Quarterly 2 X month I X mms:h COmpo�te C1 •�2c Composite Cosi* G a U i 1= 0 i it O T. Cr-TOTAL COD C611170PF 1191114,711 aVUTDt 2440 el4ek Rn 2+ooa.rt R. YI8N 1bi16av Ibyday pazazil tbfldry I13/day 1 0715 24 0630 8 n J 3 0715 24 0630E a 0.007 S2 I 1007 <0.06 3 0715 24 0630 0 _ ..0715 24 4630 8 In 5 0715 24 0630 8 4 0630 2 n 7 0630 2 n a 0715 24 0700 9 y f 0715 24 0700 9 y 28 10 0715 74 0700 9 y 71 0715 24 0700 9 y II 0715 24 0740 9 Y _ 11 0700 2 y 14 0104 2 y IS 0715 24 0700 9 .y 14 0715 24 0700 9 y 0.065 271 <0.001 <0.052 17 0715 24 0700 9 y II 0715 24 0700 9 y II 0715 24 0700 9 y 24 0630 2 n 11 7630 2 a 31 0715 24 0700 9 y 23 0715 24 0700 9 ■ 131 21 0715 24 0700 9 a 04 0715 24 0700 9 n 24 0715 24 0300 1S n I1 0700 4 y Ia 0700 2 y 11 0700 2 y 3f 0715 24 C1700 9 y 35 31 0715 24 0700 9 y N44111.7 Awra■<rJal, 73 102[3 1.5 f "°°"'404"": 0.006 95 1 0.0030 0 DD)111:914D)111:914D)111:914.0•1904. 0.007 }1333 1 0.007 0 Day Sne1aaa: 0,005 27 _1 0 0 ""No Reporting Reason:ENFRUSE=No Flow-Rene Recycle; ENVWIHR=NO Visitation—AdverseWeather. NOFLOW=No Flaw;HOLIDAY a No Visitation—Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Story OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:05-2017(May 2017) VERSION: 1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE*:3368351083 SUBMISSION DATE:06115/2017 aO/ 06/15/2017 ORC/Certifier Signature: len E Gary E-Mail:glen.gary@truetextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of the NPDES permit. \ �C r o (o — 1 (o ZO 1 7 06/15/2017 Permittee/Submitter Signature: ** Scott Taylor E-Mail:scott.taylor®iruetextiles,com Phone #:207-876-3331 x6418 Date Pemtittee Address:304E Main St Elkin NC 28621 Permit Expiration Date:12/31/2018 I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB*:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/fotms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 80.0204. ••*Signature of Pennittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). I , NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS;Active FACILITY NAME:304 East Main Streetlam P CLASS:WW-4. COUNTY:Em OWNER NAME;True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No OMR PERIOD:05-2017(May 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: No samples on 05-29-2017 in observance of the state holiday. Contract Laboratory Qualified Lab Data: ilLe May 4,11 and 22 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples may be biased low. May 1 and 25 Effluent SOD The dissolved oxygen depletion of the water blank exceeded 0.2 mg/I. NPLES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD;06-2017()une 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION:EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:NO • 40096 *0030 Ow* 2OO10 130210 Q0572 31110 COdm C0i43 : 8 4 a t e 4 N Continuous S X week 5 X w«k S X vrak S X week 5 X aYek Z X month t+Feaihiy Monthly C, Y o Z Reeadtr Grab Grsb Grab a` CORf(f03LC Corvosito Gab ,Ctmpalitc COO/pi/Site a l 0 1'. FLOW TEMP.0 p14 COLORLY6 a0O•Qq Da0y TSS-Qts Rdly FCOL1 OR TOTAL74- TOTALle•C.0 2400 cock Hn 5401roca nn YR.'N - mgfl desc u ugO Ib0/dty 11,46141., ro 9/100mt 5 my/1 1 0715 24 0700 9 y 0.07578 21.1 7.29 <25 2 S 3 0715 24 0700 9 y 0.05476 21 7.3 <25 2 4 1 0630 2 n 0.93723 4 0630 2 n 0.01902 3 0715 24 0700 9 y 004206 213 7,33 <25 2 1 "` 4 0715 24 0700 9 y 0.95769 21.6 7.01 <25 2 S <I 2.42 2.4 7 0715 24 0700 9 y 0.05551 20.2 7.57 <25 3 4 1 a 0713 24 0700 9 ,y 4067 19.9 7.31 <25 2 5 0715 24 0700 9 y 0.05264 16.6 734 <25 2 5 10 0700 2 n 0.0676 V 11 0700 2 n 0.06251 11 0715 24 0700 9 y 0.03961 21.7 73 <25 1 3 13 0715 24 0700 9 y 0.065E6 22.6 7.15 <23 2 8 14 0713 24 0700 9 y 0.01311 22.5 7.30 <25 1 . 4 - 10 07(5 24 0700 9 y 0.04469 23.2 7.2 <25 <1 5 10 0715 24 0700 9 Y 0.07473 23.7 7.22 <25 2 7 17 0630 2 n 0.11796 It 0670 2 n 0.02012 I4 0115 24 0700 9 y 0.0434 24.4 7.42 <25 2 6 30 0713 24 0707 9 y 0.04672 24 7.38 <25 Z 10 <I 11 0725 24 0700 9 y 0.04056 23 7,37 <25 2 7 - 7.4 0715 24 0700 9 y 002404 23.5 7,23 <25 2 3 , u 0715 24 0700 9 y 0.01367 23.7 7.36 <25 3 3 , 34 0700 2 n 003614 _ 15 0700 2 n 0.02963 y 24 0715 24 0700 9 y 0,07954 21,8 3.32 <25 2 4 27 0715 24 0700 9 y 0.04789 21.4 7.41 <25 2 5 c 21 0715 24 0700 9 y 0.04621 20 7,4 <25 I 5 29 0715 24 0700 9 y 00372 120.1 1735 <25 I 3 39 0715 74 0100 _ 9 y 0.04907 1220 73 <15 2 5 M.aalyAwns<tlwkl 4 161.6 1723 1 me , 1.1.1.1,,0,1.11.: 0.053052 21459091 0 1.610182 4.954545 1 2.42 . 2.4 13.3yMa'3"`' 0.11706 24.4 7.57 0 3 19 0 2.42 2.4 T1aCy Mlalrau: 0.01002 16.8 7.01 0 ,0 3 0 2.42 2,4 •.•'NoReporting Reason:ENFRUSE*No Flow-Reuse/Recycle;ENVWTHR=NoVisitatiion-AdverseWeathei NOFLOW 74o Flow: FIOLI1MY..NoVisitation-Holiday r NPDES PERMIT Na:NC000SI12 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Scary OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:909695 GRADE:WW-4. ORC HAS CHANGED:No eDti4 PERIOD:06.2017(June 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) 11434 4034 315)1 04740 y < = 2Xmanib Weekly 2X month 2Xmenet C F H E y, b t Cmnpainc Composite Oris Grsb : 3 n U H C z Cr7oTAr. COO PM.TR MAT= 2000 rbr>< 1tn, 240441.41 fin WAN Ibsld3y Ibif0Jy II/Idly Ibliday 7 0715 24 0700 9 y 2 0715 24 0700 9 y 5 0630 2 n a 06}0 2 n 3 0711 24 0700 9 i 4 0715 24 0700 9 y 0.003 30 10.007 <0.041 7 0715 24 0700 9 y 4 0715 24 0700 9 - 0715 24 0703 y 0700 n 0700 n 0715 24 0700 - 0715 24 0700 y 50 0715 24 0700 y 0715 24 0700 y 0715 24 0700 y 0632 n 0633 n 0715 24 0700 y 0715 24 0709 0.006 49 0004 <0-039 IWits0700 9 y 2 0715 0700 9 y 0715 0700 9 0700 a 0700 2 a 24 0715 74 0700 9 27 0715 24 0700 9 y 39 24 0715 24 0700 9 v 77 0715 24 0700 9 y 1 34 0713 24 0700 9 y Ii a4anah A,resp 12w3a 73 15243 LS 3 M.u►y Amato:0.0445 42 0.0055 0 64=y M.atk.a.:0.006 so 0.007 0 Dalry MWsso: 0.003 30 0004 0 'aa•NaReporting Reason:ENFRUSE No Flow-Reuse/Recycle; ENVWTHR-NoVisitation—AdverseWeather;NOFLOW.NoFlow;HOLIDAY.No Visitation—Holiday I I NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:06-2017(June 2017) VERSION:L0 STATUS:Processed COMPLIAN CE STATUS:Compliant CONTACT PHONE#':3368351083 SUBMISSION DATE:07/112017 ,x. — - C �A2 ! / ?--/ 07118!2417 ORC/Certifier Signature: Glen Gary E-Mail:glen.gary©truetextiles.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of the NPDAIE serrnit. 9/ '-y ilIFF - /.`t/` ��t (�— 7^ (� / 07/18/2017 Permittee/Submitter Signature:* * Scott Taylor E-Mail:scott.taylor@atruetextiles.com Phone #:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date:12/31/2018 I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB#:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http:l/portal.ncdenr.org/web/wq/swplps/npdes/forms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204. ***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per I5A NCAC 2B .0506(b)(2)(D). NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-0. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:06-2017(June 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: Contract Laboratory Qualified Lab Data: al{June 6 and 7 Effluent BOD The dissolved oxYgen depletion of the water blank exceeded 0.2 mg/I. of t June 8 and 9 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples June be biased low. T - i r • • NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surly • OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:969696 GRADE:WW.4. ORC HAS CHANGED:No OMR PERIOD:07-2017(July 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: OOI NO DISCHARGE*: NO • 11459 41411 W414 52444 00314 00179 71420 (OW (044.5 e Z r a J , i E i i Ccntiraoous 5 X wrek 5 742ek 5 X week 5 X week 5 x week 2 X rriotth Momhly Momhly v s 'D [� Retarder Ceib Oral, Orb Composite Camped-4k Grab Composite Conralsite C v e • o V , O 0 0 P . 77.MFC 7H ' CHtoaist =OD-QQO.D, 751•Illy Orty rCOL1ae 10TALla. TOTAL r.Coax 1410 clock tin 2449 chid lin Mild •m9d dcte w nil rov'riay Ibn4ay 4110021 m901 mel. 1 0630 3 n 0.05315 2 19630 2 n • 0,02476 2 0715 24 0700 9 y 0.64121 23,9 73 <25 2 2 • • 6 0700 2 y 0.05427 5 0715 240700 9 y 0.67136 24.3 739 <25 2 7 <1 0.9 2.8 6 0715 124 0700 9 y 0.06462 24,3 7.42 <25 1 5 7 0715 24 0700 9 2 0.0603 25 7.29 <25 2 3 1 0700 2 0 0.13455 I 1 0700 2 a 0.03773 • 11 0715 24 0700 9 y ,0.06534 236 7.46 I<25 1 4 - If '9715 24 !0700 9 y • 0.03041 243 7.44 l<25 1 3 12 0715 24 0700 9 y 0.0529 24.7 7.02 <25 2 7 Is 10713 24 0700 9 y 0.0475 25.2 7.41 225 7 4 14 I D715 24 0700 17 y 008296 25.1 735 <25 3 4 15 0630 2 n 60755 • Ii 0630 • 2 n 0.01976 17 0715 240700 9 y 0.05422 23.9 734 .<25 2 6 14 0715 24 0700 9 063101 24.4 7.25 <15 1 3 . <1 1 ' i1 0715 24 0700 9 y 0.0622 23.4 7.46 <25 2 4 • 7• 0715 24 0700 9 y 0.16176 25 737 <25 5 11 21 0713 24 0700 9 •,y' 0.13171 27.6 7.4 425 4 5 I 2t 0720 2 y 9.99266 03 0700 2 2 0.04467 I • 24 0715 24 0700 9 y 0.05341 25.4 7.49 <25 1 <5 15 0715 24 0700 9 y _0.11071 25.9 735 <23 2 5 , 74 0715 24 0700 9 y 0.07112 23> 7.5 <25 ,2 7 27 0I)5 24 0700 9 y 0.07764 241 7.43 1<25 <2 3 34 071.5 24 0700 9 y 0.06294 24.7 7.4 I<25 <1 3 2f 0630 2 y 0.06515 _ • 50 - 0630 2 n 0.03365 ' 51 0715 24 0700 9 n 005203 22.5 7.29 <25 <I '2 .4 74.6aalrAre.dy 2.6.30 4 101.1 lnJ 200 :1lpf1117 A`.nt„ 0.066712 24.575 0 1.7 4.4 1 0.9 2.8 ei07 141`2414'' 0.12176 25.9 7.52 0 5 _I t _0 _0.9 2.1 oaar 3416/6au. 0.91976 223 7.25 0 D 0 D 0.9 231 ••••NoReporting Reason:ENFRUSE=NoFlow-Reuse/Recyelet ENVWTHR..NoVisloslioa-Adverse Weetbcr, NOFLOW No Flow)HOLIDAY NoVisitation-Holiday r NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Gkn Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANCED:No eltrrill PERIOD:07-2017(July 2017) VERSION;1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) 01511 44340 11715 00731 FG0. 3 i. ic 2 x mond, woods Y 2 X .ob 2 X sno tb I d C,mpasi:e Llxn�ezitc NGc� Craba o z ctimrst, con PNav,71' SULFIDE 1440.1w1 sin uxd..1 tin 1'mn 1piday 1113May Ib3rday lbid3y I 0630 2 r 7 ( 0630 2 n 3 0715 24 0700 9 y I 0700 2 Y 4 0715 24 0700 9 y 0.004 10 I<0.04 <0.06 4 0713 24 s 0700t 9 y _, 0715 2.4 0700 9 y 1 _0700 2 n 9 0700 2 0 14 0715 24 0700 9 y ti 0715 24 0700 9 ly 20 1, 0715 24 0700 9 Y 11 0715 24 0700 9 y 14 0175 24 0700 9 r .. 1s 0630 2 n 11 0650 2 n I7 0715 24 0700 9 Y sa 0711 24 0700 9 Y 0.002 25 0.006 50.026 ti 0715 24 0700 9 ly _ 34 0715 24 0703 9 r 33 0715 24 0700 9 ,y 3: y 0700 y 23 0700 2 u 0713 24 0700 9 y 33 0715 24 0700 9 y 27 34 0715 24 0700 9 y 27 0715 24 0700 9 Y 1 2+ 071$ 24 0700 9 y 27 0630 2 Y 11 0610 2 a ,, 10715 24 0700 9 n M.•nty•nnri ua.s:: 15 1(315 13 3 ai.alvy Maarr. 0.001 47 0.003 0 Daily Kinnear 0.004 77 0.006 0 AsPy Malan= 0.003 25 10 0 •'•"No Reporting Reason-ENFRUSE>.No Flow-ReuserRecycle;ENVWTHR No Visitation Adverse Weather,NOFLOW=No Flow; HOLIDAY a No Visitation—Holiday I NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4,0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:07-2017(July 2017) VERSION:1.0 STATUS:Processed COMPLLANCE STATUS:Compliant CONTACT PH NE R:3368351083 SUBMISSION DATE:08/21(2017 21-aq -/7 08/16/2017 ORC/Certifier Signature: Glen E ary E-Mail:glen.gary@tructextilcs.com Phone #:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDES permit. � �I co— 22- 17 08/21/2017 Permittee/Submitter Signature:*** ott Taylor E-Mail:scott.taylor®a truetextiles.com Phone #:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date:12/31/2018 I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief true, accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB th 5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web(wq/swp/ps/npdes/forms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:-ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204, ***Signature of Permittee:If signed by other than the permitted,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). 1 NPDES PERMIT NO.:NC000S312 PERMIT VERSION:4.0 PERMIT STATUS;Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Suny OWNER NAME:True Textiles Int ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:07-2017(July 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: Contract Laboratory Qualified Lab Data: No samples on July 4 in observance of the state holiday. aze July 3 Effluent TSS The precision between the sample and sample duplicate exceeded laboratory control limits, ALE July 6,11,13,14,21 and 24 Effluent BOD The dissolved oxygen depletion of the water blank exceeded 0.2 mg/1. Ai,E July 10 and 18 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples July be biased low. r NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Starry OWNER NAME:True Textiles Inc ORC:G1er:Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANCED:No cDMR PERIOD:08-2017(August 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO 54 659 KMIo 0000 6.6.0 OM* 00520 31414 C0409 COKS ° •9 F m Continuous S X week 5 X week $X w<d1 I5 X work S X Auk 2 X math 4 onlh� Monthly < I C i Recorder Grab Grab Grab Composite Composite Gob Composite Composite e Y rc C V F O O O x PLOW TEMP{ 1H CRLORC/L BOO•QT oa11y T55•1719 97.171 SCOUR TVTAL eI• TOTAL.t-C..c uos Oak Hr. 1444 rkrf 11 r YN24 laad 049 ru 43/1 Ibsf4y l tbs'd.y ,61100m) me no 1 0715 24 0700 9 y 0.0497 22.3 7,4 <23 1 3 2 1.77 2.3 7 0715 `24 0700 9 y 0.13651 24 7.39 <25 3 14 1 0715 24 0700 9 y 0.05911 332 7.14 <25 <1 2 4 0715 24 0700 9 y 0.17372 23.2 {{7.37 <25 6 19 5 0700 2 y 003727 1 • 0700 3 y 0,05323 17 .2S 5 0715 24 0700 9 y 0,04216 23.3 <25 1 - 4 a 0711 24 0100 9 !y 0.10791 24.1 7.25 <25 <2 6 0715 24 0700 9 y 0.11634 24.3 72 <29 <2 4 ` n 0715 24 0700 9 1Y 0.1053 22.7 7.12 <25 5 1 11 0715 24 0700 9 y 0.03953 21.3 7.26 <25 I 1 I 18 1 0630 - n 0.05294 I II 0630 _ n 0,01795 14 0715 24 0700 9 y 0.09526 24,1 7,32 <2S <1 3 1S 0715 24 0700 9 y 0.15096 24.5 6.90 <25 3 5 23 14 0715 24 0700 19 y 011351 24.6 7,26 <25 _ 5 )1 7 0715 24 0700 9 y 0.23238 252 734 <25 6 20 - 4 [0715 24 0700 9 y 0.17402 25.6 7,4 <25 A 7 19 0100 II y 0.1065 09 0700 2 r 0.06535 21 0715 24 0700 9 y 0,01694 24.9 732 <25 <1 7 u 0715 24 0700 9 y 0.05733 25.1 7.35 <25 <I 6 15 0715 24 0700 9 y 0.04709 ,23.4 7.25 <25 I 5 24 0115 24 0700 9 y 0,10312 263 6.34 <2.5 4 5 15 0715 24 0700 9 y 0.03209 250 6.65 425 <I I [04 0630 2 0 005934 11 ,0610 2 n 0,02217 D 0715 24 0700 9 y 0.04815 20,3 7,29 <25 <1 3 44 0715 24 0700 9 y 0.02784 233 7.25 <25 <1 1 A 10715 24 0700 9 a 0.03341 20.3 7.19 <25 <I 2 _ 71 k 0715 24 0700 9 y ( ,0.03305 213 7.24 <23 <I 5 5194.51/AbW +eC L1: 4 1415 155.1 NO ' e/.aa1y 4999.2. 008607 23.93913 0 1.608696 5.603696 6.73233 1,77 2.3 D.O.14a4sss: 0.2328E 263 7.4 0 6 20 23 1,77 23 0•15 540Jsss`0,01795 2513 6.65 0 0 I 2 1,77 23 ••••No Repotting Reason:ENFRUSE-No Flow•Rei efRecycle; ENVWTI{R=No Visitation-Adverse Weather,NOFLOW=No Flow;HOLIDAY-No Visilstion-Holiday 1 1 1 T NPDES PERMIT NO.:NC00053 t2 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4, COUNTY;Surly OWNER NAME:True Textiles Inc ORC;Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANCED:Nu eDMR PERIOD:OS-2017(August 2017) VERSION:1.0 STATUS;Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) • II 554 10520 I TetSR 32720 00745 f 2 s !4 FKK o ; 1 6 K 1 a s Y 2 X month Weekly 1 Querterly 2 X mcndi 2 X month + r! g . 3 d it Corn a Colnpnsim 'Composite GM Grab 2s� pyo V o V 1=. es i 113141y i Cr-T0?At. Cbl) ICRAITOP4 PHEN,TR SLLFTn6 I1410dark 9. Mtrl«t 51n V15.44 Ibs'dty Ipitt7all Ibslday 1b5,'day 1 10715 • 24 0700 9 y 0,004 19 11 <0.004 <0.941 1 0715 24 0700 9 y 1 1 3 0715 24 0700 9 y f 4 0715 24 0700 9 y 1 5 0700 -2 y . 4 0700 2 Y 7 0715 24 0700 9 ,y t 0715 24 0700 9 y E1 t 0715 14 _0700 9 y 19 0715 24 0700 9 y " 10715 24 0790 9 v 1 t1 1 0630 2 n 13 0610 2 n f t4 0715 24 0700 9 y 15 0715 24 0700 9 y 0006 112 0.014 <0.126 16 0715 24 0700 9 y . 17 0715 24 0700 9 v 1t 9715 24 0700 9 v 14 0700 2 y 1• 0700 2 ,y 77 0715 24 0700 9 ,y 1 23 0715 74 0700 9 y so 27 0715 24 0700 9 y 14 0715 24 0700 9 ,y r �5 0713 24 0700 9 y I 25 0430 2 n 17 0620 2 n is 0715 24 0750 9 Y 71 0715 24 0700 9 y 17 I 1 Ii 0715 24 0700 9 ly 71 0713 24 0700 I9 Y 1 `` Maa9}!own..1.1.4; 1.5 1014.5 f 1.0 1 SEousy Average 0.003 56.E II 0.007 0 1271.9 Mninnn:0406 112 11 0.014 0 Daly Mkk•vu' O.OM 17 11 0 0 ••••No Reporting Reason:ENFRUSE a No Flow-Reuse/Recycle; ENVWTHR-No Visitation-Adverse Weather,NOFLOW^•No Row;HOLIDAY®No Visitation-Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Sum/ OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-0, ORC HAS CHANGED:No eDMR PERIOD:08.2017(August 2017) VERSION:1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE#:3368351083 SUBMISSION DATE:09/i 8/2017 _ G tr Q 9'1 1" �/ 09/15/2017 ORC/Certifier Signature: Gle E Gary E-Mail:glen.gary®truetextiles.com Phone P:(336)835-1083 Date By this signature,I certify that this report is accurate and complete to the best of my knowledge. The perminee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. if the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of the NPDE emit. Cee-%/C70. o r— 9—c,20(7 09/18/2017 Permittee/Submitter Signature:* Scott Taylor E-Mailscott.taylor@truetextiles.com Phone #:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018 I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete.l am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB 0:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http:/lportal.ncdenr.org/web/wq/swp/pslnpdes/forrns. FOOTNOTES_ Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 8G.0204. "•Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per ISA NCAC 2B 0506(bX2)(D) l NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:959696 GRADE:WW-4, ORC HAS CHANGED:No tDNA PERIOD:08-2017(August 2017) VERSION:1.0 STATUS:Processed Outfall 001•Effluent Comments: Contract Laboratory Qualified Lab Data: lye.August 3 Effluent TSS The precision between the sample and sample duplicate exceeded laboratory control limits. axe August 7 Effluent BOD The seed blank was outside acceptance criteria.Results were accepted based on remaining quality control indicators lid August 18 Effluent TSS The precision between the sample and sample duplicate exceeded laboratory control limits. ILLS August II,17,18,24 and 31 Effluent BOD The dissolved oxygen depletion of the water blank exceeded 0.2 mall. zj,f August 21 Effluent SOD Oxygen usage is less than 2.0 for all dilutions set.The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. dial August 29 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this enalyle in associated samples August be biased low. NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4,0 PERMIT STATUS:Active FACILITY NAME:304 East Moot Street plant CLASS:WW-4. COUNTY:Sun OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:939696 GRADE:WW-4 ORC HAS CHANGED:No cDMRPERIOD:09-2017(September 2017) VERSION:1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO 56e9 :M1a 9609 9919 0[1)10 01930 11416 C0<e4 CO60F is 1 jisCnminulxu s X neck S X 1v;ci: 5 X week 5 x week S N week 2 X month nlund113 Monthly a r 01 o 3`1 40 1 C e` 1 Recom rder Crab Grob Grab Co00ute Composite Grab Composite C094.010: 7. 5 Q p :J -� x , O C Z FLOW TCMP.0 1X14 011,0911.E BOO-QAns0. T5S-Q904IW FC01-196 TOTAL.rl- TOTALP-Case i+m rl.k Iln 1mucln'1, 11r. .9467( nry;d de>;c 60 140 tbsldnY Ib3!d41 6/100n0 171k1 nn;A 1 `0715 24 0630 8 n 10.11238 122.2 7.22 <25 6 4 I 0650 2 n -�- j43.04178 3 0630 2 n 10 02348 - , 1 0630 2 n 10.01124 ' . 5 mis 24 0610 8 n {005451 20.4 7.15 <75 <I 3 6 32 _2 + 0715 24 0630 0 n 0.07023 20.9 706 <25 2 6 07(5 24 10630 e n 0.1803 20.7 7.1 <25 4 21 Y 0715 14 0830 117 n 0.15793 19 9 7.09 <25 3 10 7 0030 2 n 013957 00 0630 2 n 0.02075 _ 11 10715 24 0700 0 - 0.05151 17 5 7 25 <25 1 6 12 0713 24 0700 0 Y 0 10065 16 B 714 <25 <2 5 1 11 0715 24 10700 91 0.26292 174 73 <I3 5 84 I, 0715 24 10100 0 y I 0 10149 18 7 7 19 <25 2 12 i•' 0715 14 10700 9 y 0.24157 193 714 <21 7 64 I• 0700 2 v 0.07379 17 0700 2 y 0.04(0) • 16 041I 5 24 0700 0 . 00665 20 7 7.3 .,25 2 7 19 0715 23 0700 9 Y 0.03007 120 9 7 2.1 <25 I 10 <i 18 0715 24 0700 9 y- 0.29901 21 2 7 22 <25 3 6 71 0715 24 7700 9 y 009072 215 72 <25 2 -- 0715 34 0700 9 5' 0.17979 219 7.26 <25 4 4 23 0630 2 n 0.06918 1) 0630 2 n 0.02104 25 0715 14 0700 9 c 0.05699 20.0 7 32 <25 I _ _ 26 0715 24 0700 19 v 0.03105 221 1 7 22 <25 1 2 25 0713 24 0700 f 9 p 10 05939 21 5 lit '<25 <I 3 =n 0715 _24 0700 0 v 017219 222 713 <25 4 8 n 0715 24 0700 9 v 048955 24.4 7.3 <23 1 1 - w 0700 - v 0 05353 a - . 043.k15 4,c.1n'L1n.16 I 103.6 272.1 59 2t..M.A..r.pr: 1209126 20375 0 245 13.5 244449 3_ 73 D<60 11•11twer 0.25232 22 2 738 0 7 _84 0 3 3 2 2 0.11.435)o6* .10.02095 168 706 0 0 2 0 .i2 52 •••No Reporting Reason:ESFRUSE"No Flow-RC115CIRRcc c5e: ENV'WTHR,No Visitation Adverse Weather: NOFLOW•,,,No flow: HOLIDAY-No Visitation Iiol•day I I NPD ES PERMIT 19O.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Ac11ve FACILITY NAME:304 East Maio Street plant CLASS:WW.4. COUNTY;Sorry OWNER NAME:True Testlies Inc ORC:Glen Edward Gary ORC CERT NUMBER:989695 GRADE:WW-4_ ORC HAS CHANGED:No eDlMR PERIOD:09-2017(September 20171 VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) r • 01,14 .1)40 31736 011749 1 # G : X . y _ 2 X amid: Y4, cd.ly 2 X mond, 3 X month I 1 c", I 3 C9rroolur Comxanc Crab Grab n7. .. .., .! C K f. Cr-TOTAL COD %10.9,10 5VLT0E Uw.1A6 H.. 24r7h,r4 nn 916:9 0l !day. Ito.'day Ibsfday ItrJfay 1 0715 24 0630 >♦ n 2 0610 2 ,n __J 1 0530 2 a 4 0630 La n 5 0715 24 0630 8 a 0 004 52 40005 70047 4 0715 24 0630 0 7 0715 24 11430 Y a t 0715 I24 0630 A n • 0630 2 n 10 0630 _ n 11 0715 24 0700 9 1. - . 12 0715 24 0700 9 6 40 Il 0715 24 0700 9 14 0715 24 0700 c 45 0715 :4 10701 9 V I le 10700 - 17 10700 2 y 1" 0715 ,24 0100 9 Y 1'1 0715 24 10700 9 v 0001 23 <000) 40.933 15 0715 24 10700 9 v I I 11 0715 24 10700 9 Y I 21 0715 I24 0100 9 y 24 0630 2 24 0039 2 n 15 0715 24 0700 9 28 0715 24 0700 9 y i V 33 0715 24 0700 9 . I 26 0715 24 0700 9 t I 27 0715 24 0700 9 y I Yo I 0100 2 y I - 5talnir A1•wry.1.166 11.2 16265 1.53 66.6407"cr6K- o oco 139 0 ,0 061004 ,,..., 0004 c o0406 510140+40: 0004 162 '_) 0 O •6t•No Reposing R1:1160 ENFRUSE=No I'Icw.RvtoaofReeyd_: ENVWTHR-No 1'isiation Ad,crse We:oher. NOFLOW: Na Flow,HOLIDAY-No Vi&itati0o-holiday I f ' NPDES PERMIT NO.:NC000S312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 Fast Main Street plant CLASS:WW-4. COUNTY:Sony OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No OMR PERIOD:09.2017(September 2017) VERSION:1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE#:3368351083 SUBMISSION DATE:10/18/2017 10/18/201 7 ORC/Certifier Signature: Cite E Gary E-Ivtail:glen.garyi,duvaltex.com Phone #:(336)835-1083 Date By this signature.I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours front the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permitice becomes aware of the circumstances. If the facility is noncompliant.please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDE / -/9^ / 10/1 8/20 17 Permittee/Submitter Signature:*** Vott Taylor E-Mail:scott.tayior4;truetextiles.com Phone #:207-876-3331 x6418 Date Permittee Address:304E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018 I certify.under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system.or those persons directly responsible for gathering the information,the information submitted is.to the hest of my knowledge and belief:true. accurate.and complete.I am aware that there are significant penalties for submitting false information.including the possibility of tines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME: CERTIFIED LAB k:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary.Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.nedenr.ora/web/wq/s++p(ps/npdesifotms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. '`No Flow/Discharge From Site:Check this box if no discharge occurs and.as a result.there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 80.0204. ***Signature of Permittee:if signed by other than the permittee.then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). 1 NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active • FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD:09-201?(September 2017) VERSION:1.0 STATUS:Processed Outfall 001-Effluent Comments: No samples taken on September 4 in observance of the State holiday Contract Laboratory Qualified Lab Data: ajj September 1.7.12.13.I8.22.27 and 28 Effluent BOD The dissolved oxygen depletion of the water blank exceeded 0.2 mg/I kg September I I,12,19.21.22.27.and 29 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyse in associated samples September be biased low NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4 0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4, COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No eDMRPERIOD: 10-2017(Octoher2017) VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO 0004 00010 wu.o noun Q5110 Q1A10 11416 C0450 Cass i= S t a 12 - o° a` a Condnuout 5 X week 5 X week 5 X week 5 X week S X week 2 X monde Mon161y Monthly ii., i 2 i" Recorder Coob Gab Gab Compooinr Conrposne Crab Composite Composite C a O j = FLOW TE0I0-e p6 CHLORINE BOD-Or5 Ore. TSS•Qrc0.03 FCOLI BR 707/41.31• TOTAL P.C... C 10.1,..1. 2l6Or4 Hr. 5itvrt mi y4 dee +so 0. nn 4 opt lbrtday Ibsrdar tin00651 ns t mig1 I 0700 2 y 003024 2 0715 24 0700 9 0.04768 16.1 7,14 <25 <t 6 3 0715 24 0700 9 5 005541 16 665 <25 <1 5 <I 114 2.6 2 0715 24 0700 9 Y 004156 16 7.2 <75 I - S 0715 24 0700 9 y 0(765 16.4 727 <25 <3 12 _ 6 0715 24 0700 9 y 0.19105 17 7.19 <25 6 113 S 0630 2 n 0.06476 " 0610 2 n 0.01{63 • 9 0715 24 0700 9 y 0.17309 20.9 6.93 <25 <6 (34 u 0715 24 0700 9 y 0.19065 219 713 <23 3 54 II 0715 24 0700 9 y 0.12496 225 7.07 <25 3 20 12 0715 24 0700 9 y _0.15333 22.4 714 <25 3 30 _ 13 0715 24 0700 9 jr 0.14312 2(7 715 <25 6 36 14 0700 2 y 0.05800 1S 0700 1 y 0.05799 16 0715 24 0700 9 Y 0,07554 I0) 7.22 <25 <I 6 1 0 0715 24 0700 9 y 0.03712 16.7 6.61 <25 <I <1 IR 0715 24 0705 9 y 0.04961 151 717 <23 I 5 _ ` t' 0715 24 07013 9 y 0.05549 N 5 7,25 <25 <1 <2 10 0715 24 0700 9 y 0.06423 14.5 7 14 <25 <I 3 11 0630 2 n 0,06325 14 0630 2 n 0 02002 _ V :3 0715 24 0700 9 y 004425 139 7,27 <25 <1 24 0715 24 0700 9 y 0.13058 15.3 72 <25 3 17 L< 0715 24 0700 9 Y 0.16918 148 7.(5 <25 4 26 l6 0715 24 0700 9 y 0 10344 13 2 7.19 <25 2 12 2' 0715 24 0700 9 y 0.13428 12.6 7.25 <25 3 17 1a 0700 2 y 0,13168 49 0700 2 y 0.08508 3° 0715 24 0700 9 y 0.06925 II 7.00 <25 1 13 41 0715 24 0700 _9 y 006405 10,3 7.25 <25 <1 , 81.ann A,...ze Limit a 101.4 , 271.3 Seo sm011,1r Montle: D 049217 16 604545 0 1.727273 19.636364 1 I N 2 6 0.0.11.o11.1000 0.07309 22.5 727 0 6 131 0 114 2.6 006.111a11nunr 002002 110.3 6.61 0 0 0 0 117 26 •"`No Reporting Reason,ENFRUSE-No Flow-RcoseRecycle: ENVWTHR a No Visitation-Adtrorse Weather, NOFLOW=No Flow: HOLIDAY"No Visilaoon Holiday 1 I r 1 NPDES PERMIIT NO.:NC0005312 PERMIT VERSION:4 0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD: 10-2017(October 2017) VERSION: LO STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) 61034 06340 32736 0740 Y 2,I 7 R. R `e ar 2 X month Ws.1:ly 2 X month 2 X momh g c o g Compasiic Composle Grab Grab x E x 0 e a a v r O t- o i CrTOTAL COD PFIEN,TR SULFIDE 240 4.404 Hr. 2460 cb<k 11n 170/5 lbs/day 1bs/day lbs/day lbs/day I 0700 2 y 1 0715 24 0700 9 y 1 0715 24 0700 9 Y 0 004 28 <0.005 <0.004 4 0715 24 0700 9 y 5 0715 24 0700 9 y 6 0715 24 0700 9 v 7 0630 2 n M 0630 _ n Y 0715 24 0700 9 v Ia 0715 24 0700 9 y 156 II 0715 24 0700 9 v 12 0715 03 0700 9 y 13 0715 24 0700 9 v 14 0700 2 y 15 0700 2 tC 0715 24 0700 9 y 17 0715 24 0700 9 v <0 WI I! <0003 <0031 10 0715 24 0700 9 v 0 0715 24 0700 9 < 7' 0715 2,4 0700 9 v 21 0630 2 n 22 0630 2 n — 13 0715 24 0700 9 y 24 0715 24 0700 9 y 71 25 071$ 23 0700 9 y 26 0715 24 0700 9 y 11 0715 24 0700 9 y IR 0700 2 y 20 0700 2 Y 44 0715 24 0700 9 y 11 0715 24 0700 9 y 40 51.o1hl}Awnac Lido 13 1524,-< 1.5 3 51440Ik1 A.cD,o, 0 002 61..2 0 0 NU;66,1/..< 0001 156 o 0 Day Jtd ire 0 I I 0 0 6 t6•No Reporting Reason:ENFRUSE=No Flow-ReusclRccycic; ENVWTHR=No Visitation Ads erre Weather, NOFLOW=No Flow: HOLIDAY-No Visiladon Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATES:Active FACILITY NAME:304 East Main Street plant CLASS;WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW4 ORC HAS CHANGED:No eDMR PERIOD: 10.2017(October 2017) VERSION: 1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTAC/'PHONE#:3368351083 SUBMISSION DATE: 11/17/2017 11,16'2017 ORC/Certifier Signature: Glen - Gary E-Mail:glen.gary,aduvaltex.com Phone #:(336)835- 1083 Date By this signature,I certify that this report is accurate and complete to the hest of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. lithe facility is noncompliant.please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDES permit. a156/� �, I— Zc�— Zd �1 r t 7 11.1712017 Permittee/Submitter Signatur :*** Scott Taylor E-Mail:scott.taylorn?truetextiles.com Phone #:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date: 11'311201S I certify.under penalty of law.that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system.or those persons directly responsible for gathering the information.the information submitted is.to the best of my knowledge and belief.true. accurate.and complete.I am aware that there are significant penalties for submitting false information.including the possibility of lines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles.Inc CER'rIFIED LAB#:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary.Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.orglweb/wq/swp/ps/npdes/fonns. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and.as a result.there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 8G.0204. ***Signature of Permittee:If signed by other than the permittee.then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). NPOES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANCED:No eDMR PERIOD: 10-2017(October 2017) VERSION: 1 0 STATUS:Processed Outfall 001-Effluent Comments: Contract Laboratory Qualified Lab Data: a�f October 2,3,5,6.and 13 Effluent ROD The dissolved oxygen depletion of the water blank exceeded 0.2 mg/l. $i,4 October 2,3,5,10, 16,17,20,23,24 and 25 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples October be biased low I 1 r- NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4 9 PERMIT STATUS:Active FACILITY NAME:304 East Main Sweet plant CLASS:WW-4. COUNTY:Sorry OWNER NAME:True Textiles lac ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No eDM1R PERIOD: 10-2017(October 2017) VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO 59450 PICOa a0460 00440 Q0710 Q0530 31616 CO6n4 COW Y ~ _ O t. :: C s - s` Condnoaao S X weak S X trek S X week S X wao6 5 X ween 2.X mon h Mthly onJ. r - 7 I t i Record< Grob Grab Gab Composite Composite Crab Compocile Composite 23 C L 1- .. o j z' FLOW TEMP-C 105 CHLORINC SO0-Oct De26 TM,Qty 0.0. FCOU BR TOTAL:5. TOTAL P-C.ac 23445..k Hr. 2706 4444 Ito. 5.79734 m11d deg c su o 5l Ibsrdey Ibsldev 1111000 m1;tl x42611 i 0700 _ y 0.03024 2 0715 24 0700 9 v 0.047E8 16.3 7.14 <25 <I 6 ) 0715 24 0700 9 y 0.05541 16 6.65 <25 <1 5 <I 1 15 2.6 3 0715 24 0700 9 y 0.04156 16 7.2 <25 1 ' 5 0715 24 0700 9 y 0.1758 164 7.27 <25 <3 12 6 0715 24 0700 9 y0.19105 17 7.19 <25 6 18 7 0630 2 n '0,05476 11 0630 2 a 0.07063 • S' 0715 24 0700 9 1' 0.37309 30.9 6.95 <25 <6 134 14 0715 24 0700 19 p 0.19085 219 713 <25 5 54 II 0715 24 0700 19 y 0.12496 22,5 7.07 <25 13 20 12 0715 24 0700 9 v 0.15333 224 714 <25 3 30 73 0715 24 0700 9 y 0.14312 21 7 715 ,<2$ 6 36 11 0700 _2 y 0.05008 15 0700 2 y 0.05799 - 16 0715 24 10700 9 y 0.07554 203 7.22 <25 <I 6 77 0715 124 0700 S y 0,03712 16.7 661 <25 <1 2 <I 11 0715 24 0700 9 y 10.04961 15 t 717 <25 1 5 15 0715 24 0700 9 v 0.05549 145 7.25 <25 <I <2 24 0715 2-1 0700 9 y • 0.06423 14.0 7 14 <25 <I 3 21 0630 2 n 0.06323 • 22 0630 2 Fn 0.02802 D 0715 24 0700 9 y 00442E 159 7.27 <25 <1 _ 24 0715 24 0700 0 y 0.13058 15.3 7.2 <25 3 17 '-4 0715 24 0700 9 y 0.16978 14.3 7.15 <2$ 4 25 16 0715 24 0700 9 y 0.10334 13 2 7.19 <25 2 12 27 0715 24 4 0700 9 y 0.15488 126 7,25 <25 3 17 211 0700 2 y 0.13168 19 0700 2 y 0.08508 39 071$ 24 0700 9 v • 0.06925 II 7.0E <25 13+1 Jt 0715 24 0700 9 y 0,06305 10.3 7.25 <25 !<l 12 SI.mrMy A.rnae Limit ., 1461.4 2723 704 1144411,1 A.cnr>K; 0099217 16.603545 0 1 1.72727) 19.636364 1 114 2 6 Daily 01301140.0 037309 22,5 727 0 6 ESS 0 114 2.6 052.511eImoo, 0.02002 10 6.61 0 0 0 0 114 2 6 e"'No Reporting Reason:ENFRUSE-No Flow-Reuse:Recycle; ENVWTHR No Visitation-Adverse Weather; NOFLOW=No Flow: HOLIDAY_No Visiinuon Holiday NPDES PERMIT NO.:N00005312 PERMIT VERSION:4 0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Suny OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD: 10-2017(October 2017) VERSION: 1,0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) 11034 0934* 7225* 00745 22 e" v q 3 r -4 ,7 1 ,i b _E` 2 X month Weekly 2 X month 2 X month 7. '2• 4 f 5t. 4 Composite Compovle Grab Grab ,', t- 0 L- j Z CnTOTAL COD 91MEN,TR SULFIDE 2401 sick li.. 24.04. 3. Iin vIsry lbs/day abslday lbsrday lbs/day 1 0700 2 y 2 071$ '14 0700 9 v 3 0715 24 0700 9 v 10.004 28 <0.005 <0.004 , 4 0715 124 0700 9 y c _0715 .124 0700 9 y 0 0710 24 0700 9 v 7 0630 2 n 1 '< 0530 2 n ' 9 0715 24 0700 9 y 1* 0715 24 0700 9 y ISO ,I D715 24 0700 9 y I2 0715 24 070D 9 y 13 0715 24 0700 9 v t4 0700 2 y 15 0700 2 y I is 0715 24 0700 9 y t7 0715 24 0700 9 y <0.002 11 <0.003 <0 051 II 0715 24 0700 9 y 17 0715 24 0700 9 v 00 0715 24 0700 9 y 21 0630 2 n 02 0030 12 n 23 0715 24 0700 9 24 0715 24 0700 9 y 71 Tt 0795 24 0700 9 y 26 0715 24 0700 9 27 0715 24 0700 9 Y 28 0700 2 y 29 0700 2 v 3* 0725 24 0700 9 y 31 0715 24 0700 9 y 40 510161$A.*nv 1340$ 15 It314, ly 3 11.111,'A vourn 0.002 61.2 0 0 0.03 al.dmmn: 0.004 156 0 0 D.My Minimum 0 I I 0 0 '•'.No Reporting Reason:ENFRUSE=No Floe-•Reose/Rccycle: ENVWTHR=No Visitation Adlcrse Weather, NOFLOW=No Flow: HOL@AY No Visitation-Holiday • 1 NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY;Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No eDMR PERIOD: f0-20I7(October 2017) VERSION: 1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTAC PHONE#:3368351083 SUBMISSION DATE: 11/17/2017 -�-'� !�-it�'t 1 Q U' t 11,1612017 ORC/Certifier Signature: Glen Gary E-Mail:glen.garyirduvaltex.com Phone #:(336)835-1083 Date By this signature,1 certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant.please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDES permit. ( I— 2c Z� h' c i 7 11/17;2017 PermitteetSubmitter Signatur :*** Scott Taylor E-Mailscott.taylor;_ truetextites.corn Phone f1:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date: 12;31/2018 I certify.under penalty of law.that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system.or those persons directly responsible for gathering the information.the information submitted is.to the best of my knowledge and belief.true. accurate.and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles.Inc. CERTIFIED LAB 4:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdeslfonns. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and as a result.there are no data to be entered for all of the parameters on the DMR for entire monitoring period. **ORC on Site?:ORC must visit facility and document visitation o1'facility as required per I5A NCAC 8G.0204. ***Signature of Permittee:If signed by other than the permittee.then delegation of'the signatory authority'must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). 1 NPDES PERMIT NO,:N00005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:W W-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No eDMR PERIOD: 10-2017(October 2017) VERSION: 1 0 STATUS:Processed OutfiII 001-Effluent Comments: Contract Laboratory Qualified Lab Data: Sfy October 2,3,5,6,and 13 Effluent BOD The dissolved oxygen depletion oldie water blank exceeded 0.2 mg/I. 51,E October 2,3,5.10,16,17,20.23,24 and 25 Effluent BOD Analyte recovery in the laboratory control sample(LCS)was below QC limits.Results for this analyte in associated samples October be biased low- NPDESPERMIT NO.:NC000S3I2 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Mann Street plant CLASS:W W-4. COUNTY:Story OWNER NAME:True Texlilts Inc ORC:Glen Edward Gary ORC CERT NUMBER:939646 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD: 11-2017(November 2017) VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO moon 0*41a WM= 9111it, QD71* 00f)8 31416 <040 00443 r a X .9 E • C C e p Cantsnlaous 5 X week 5 a week 5 X week 5 X trxk 5 X week 2 X mar% SfaluhIy 1.10111117 it7 E 1 V 7 C R Recorder Gab Grab Gab Composite CO45,105 45 Crab Composite Composite F. E c y r j j 0 2 FLOW TEalP,C PH CHLOBIKE DOD-Qn O.fh TSS-Q.•.All. FOOL!00 , M. TOTALF•Cow 4cu.iwi 14311.11.0.11.. _ ...I. 130 1lira 65 troyd3 076 sat .x,.1 Ibsrd45• rbstday 06( 0 n10001 `o o ! 0715 24 8638 0 n 0,05514 11.1 7.12 <15 1 5 2 0715 24 0700 .9 y 009632 12.6 7.12 <25 5 17 4fI 1 3 10715 74 0700 1,9 y 0.05803 136 7.26 <25 I 3 1 I 0630 i2 n 0.08368 1 1 , 0630IjI 7 n 0.00127 L 0715 34 0700 +9 Y 0.05178 144 7.24 <25 2 15 7 0715 24 0700 9 y 0.06773 15 17.04 <25 5 12.7 - <I 086 <001 1 9 0715 24 0700 9 y 008141 34.1 17.21 <25 <1 17 _ t. 7 0710 24 0700 19 y 0.09831 027 IJf 726 <25 6 17 14 0715 24 0700 9 y 005437 11.3 17.I7 <25 2 +I6 i I 0700 12 y 000 Si • 0700 2 y 004959 j 23 0715 24 0700 9 0.08502 91 7.23 <25 <I I9 r 14 0715 24 0700 9 y 0.06657 00 1 7 24 <25 1 127 15 0715 24 0703 9 Y 0.07957 8.6 17.22 <25 1 115 14 0715 24 0700 9 y 0.10122 8.6 7 2 <15 2 -I 9 4 17 0715 24 0700 9 Y 025E5 8.9 727 <25 36 1135 at 0630 2 I n 0.10505 _ 19 0630 2 , 003116 I 21, 0715 24 0700 9 p 0.05757 7,3 7.16 <25 2 7 =1 0715 24 0700 9 v 007047 7 708 <25 3 23 T 12 071$ 24 0700 J9 0.13768 S 1 7,17 <20 3 13 :1 0700 12 y 0.0:831 - !3 0700 2 y 0.04827 2,4 0700 3 Y 0.0910 14 0700 2 }. 905702 27 0711 24 0700 9 - 0,07954 79 7.1 <25 2 11 - 2n 0715 24 0700 9 y 0.0670; 5.6 7.15 <21 7 30 1 29 0715 24 0700 9 9 00667E 5 3 7.22 <25 2 14 1 3' 0715 24 0700 9 y 0.05373 5.8 7 O <21 7 9 Sto<.432 AlcnmL1 440% 114.4 1723 SW %Uad931sna"' 0077363 960 0 4.15 11.25 1 0.86 0 Dell,34.1man 0.2505 13 727 0 36 135 0 086 0 ` D*O.atA.inm.< 0 031 16 5 3 1701 0 0 0 0 056 0 °°°°No Reporting Reason:ENFRUSE-No flow-RensdRooycic: ENVWTHR-No Vis onon-Adsrne Wc:1111<i- NOF LOW=No Flow: 110410 9Y*No Visitation-Holiday r I 1 1 1 NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Sorry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER;939696 GRADE:WW-4. ORC HAS CHANGED:No cDltIR PERIOD; 11.-2017(November 2017) VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue) 01424 00744 70030 77730 02140 t • z g E Y = 2 C mamaW':.t:ly Q�v1.2;1v 2 X morth 2 X month i K 7 i vil C '- CORTOilte ComOosi1C Cumpositc 6141, Grob e 3 L v a" 3 7 0` 0 . i C1•TO7A1.. COD CTRIlOPr PIC\,Ill SL2rm6 140 rl.ch lb, 7414:.4..1. H.. Y70.11 lbSA13v IbS/d;,V nos/int Ibsldey 164'day 1 10715 24 ,0630 8 n 2 10715 24 0700 9 3 10715 424 0705 9 r 4 0000 2 n a 06)0 : n 6 0755 24 070 9 r l 1 7 0715 27 0700 9 y 10.014 N 1 <0.006 0.056 • 71 0715 24 0700 4 v I 0715 24 0700 9 y y . I. V1 0719 24 07047 0 y II 070 I7 5 110 1 12 0706 2 r I 13 J0715 12+ 10700 9 s 17 0715 24 0700 526 I3 0715 24 0700 9 y 1' 0715 24 0700 9 y 17 0715 24 0700 9 p II 0650 2 19 0030 2 n 70 0715 24 0700 9 y E7 0715 74 0730 9 1-Y', 6015 35 <0 006r 0.055 72 0715 24 0100 9 1I, 14 0700 2 I y 1 76 0700 2 20 < 0100 2 Iy It 10700 �2 1Y I �.. 27 0710 7A 0700 9 161 0715 24 0700 9 y 42 12r 0715 24 0700 9 y 40 0715 74 0700 9 y t , 3I.n1u,A1rr.cc Limit 1< rsza.< 1.9 3 s!-.my A....e: 00145 4775 II 0 0.028 0.97 a6,1,,./o.,< 0.015 55 I 0 0 056 D.ii15tI.1m4.s 0 9(4 28 II 0 0 "••No Reporting Reason:L3NFRUSE No FIOAc•ReuulRecyele: I NV WTIIR n No Visitation-At'erse Weather. NOFLOW=No Flo,.HOLIDAY-No Visitation-Holid : NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Surty OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD: 11-2017(November 2017) VERSION: 1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE 11:3368351083 SUBMISSION DATE:12/18/2017 9-AcI 12/18/2017 ORC/Certifier Signature: Glen E ary E-Mail:glen.garynduvaltex.com Phone #:(336)835-1083 Date By this signature.I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the perminee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. lithe facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of the NPDE ermit. / - /9- 02017 12/18/2017 Permittee/Submitter Signature:#** S out Taylor E-Mail:scott.taylotruetextiles.com Phone 4:207-876-3331 x6418 Date Permittee Address:304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018 I certily.under penalty of law.that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons IA ho managed the system.or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief.true, accurate,and complete.1 ant aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB#:5010 PERSON(s)COLLECTING SAMPLES:Glen Gary,Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http llportal.nelenr.ore/webhvq/swp/ps/npdes/forn:s. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. *No Flow/Discharge From Site:Check this box if no discharge occurs and.as a result-there are no data to be entered for all of the parameters on the DMR for entire monitoring period. •*ORC on Site?:ORC must visit facility and document visitation of facility as required per I5A NCAC 8G.0204. ***Signature of'Permittee:If signed by other than the permittee.then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). NPDES PERM/T.NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:W W-4 COUNTY:Surly OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW 4. ORC IIAS CHANGED:No eDMR PERIOD: I1-2017(November 2017) VERSION: 1.0 STATUS:Processed Outran 001-Elituent Comments: No samples taken on November 23 and 24 in observance of the State holiday. Contract Laboratory Qualified Lab Data: ur,Q November I,6 and 8 Effluent ROD Analyte recovery in the laboratory control sample(ICS)was below QC limits,Results for this analyte in associated samples November be biased low 40 November 2 and 7 Effluent ROD The precision between the sample and sample duplicate exceeded laboratory control limits, 5,,e November 1,9, 10 and 13 Effluent ROD The dissolved oxygen depletion of the water blank exceeded 0.2 mgil NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4. COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:W W4 ORC HAS CHANGED:No eDMR PERIOD: 12-2017(December 2017) VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO N.K. aaala MUM Mlii QOM. QBV• $1646 COfa• CONS _' con....., 5 X welt X wesk 5 X wok 5 X weak 5 X week 2 X mono. Monti* Monthly 1... ,,, � 3 � Recorder Gob Gab Gap Composite Compote Gab Composite Compostog. u a t 1 3O 1 LOW __TEMP.Z FII CHLO10K[ 600.0.Doily 7241.Pry 0.85 FCOLI IM TOTAL N. TOTAL P.Ow 1412 Awl.. xn I4Md..6 M. 519<9 mgd dega so WO lb.iday tbs)day 0/100n4 m8.9 m.4 1 0715 24 0700 9 y 005935 X69 716 <25 1 7 2 0630 2 • 0065% ' 3 0630 2 a 0.01972 4 0715 24 0700 9 y 0.03693 65 7.15 <25 1 3 5 0715 24 0700 9 y 005016 69 659 <25 1 7 <1 0.65 1.7 4 0715 24 0700 9 y 0.06979 1,1 7,14 <23 2 2 7 0715 24 0700 9 y 0.05014 6.5 7.17 <25 I 1 a 0715 24 0700 9 Y 0 20867 7.2 7.09 <25 <5 59 11 9 06)0 2 a 0,02371 11 0630 2 a 0,15259 II 0715 24 0630 1 a 005168 3,6 706 <25 2 21 12 0715 24 0630 8 • 0,08013 3.7 703 <25 3 39 13 0745 24 0630 a a 00106* 3 721 <25 3 4 14 0715 24 0630 31 a 0.14906 2,3 7.07 <25 6 27 15 0715 24 0630 8 • 0.14565 3.3 7.06. <23 7 II 16 0610 2 a 0,15563 , 47 0630 _2 n 0 02502 18 0715 24 0700 9 a 0.06505 3 7.1 <25 4 432 1f 0715 24 0700 9 y 004866 5.7 6.57 <25 5 51 12 • 0745 24 0700 4, 9 y 0.14335 5.0 704 <23 17 61 71 0715 24 0790 9 y 02131 65 7 <25 Il 59 22 0713 24 0700 9 y 0.1103* 67 697 <25 4 5 24 0700 2 y 0 07027 24 0700 2 y 0.03022 35 0700 2 y 0 0569E n 0700 2 y 004799 rt 0715 24 0700 9 y 0 06376 4.5 7 06 <25 4 3 ix 0715 24 5700 9 y 0 07077 2.9 099 <25 4 11 25 0715 24 0700 9 y 005305 11 7,02 <2! 6 7 2a 0630 2 a 010235 21 0630 2 n 00299 51..445•,/ate Liao.. 4 1.1.4 272,1 36. 51..9•''A'mM. 0081023 4 165421 0 4 684211 27 210526 3 464102 063 1 7 0.06 AL.iw.oc 02431 83 724 0 i1 132 12 0.65 17 OA2 a1ww.. 001972 1 1 657 _0 0 I 0 0.65 17 ••••NoRepetnlll Reason.ENFRUSE. ,N'oFloss•RruuRecyck; ENVWTHR No Visitation-Adsclsc Weather. NOFLOW n No Flow; HOLfDAY-No Visitation Holiday NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:W W-1. COUNTY:Surly OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:939696 GRADE:WW-4. ORC HAS CHANGED:No eDMR PERIOD: 12-2017(December 20171 VERSION: 1.0 STATUS:Processed SAMPLING LOCATION: EFFLUENT DISCHARGE NO.:001 NO DISCHARGE*: NO (Continue) n,w 100 WM 16746 • x t • 2 X mond, wR+ly 2 x mont0 z x 1866583i d cwl asoo c«nvo.r GrabGrab 3 I • � � � c.rorwL COO MEM,TR slx.noc 44164.I.0. Nn 1416 r1..l• N•. Inn Ibi'doy ib/day IbYday Ibs'day I 0715 24 0700 9 r • 1 0630 2 n 3 0630 2 n 4 0715 24 0700 9 y 7 0715 24 0700 9 y 0.301 2) <0 004 <0 042 4 0715 24 0700 9 y 7 0715 24 0700 9 y a 0715 I4 0700 9 y 4 0630 2 n 16 0630 2 a 11 0715 24 0610 8 12 0715 24 0610 8 n 106 Ii 0711 24 0630 0 n ,1 0715 24 0630 I n 11 0715 24 0630 8 n 11 0630 2 17 0610 2 n 10 0715 14 0700 9 y I/ 0715 24 0700 9 y 0.005 25 0006 0061 15 0715 24 0700 9 Y 11 0710 24 0700 9 y 17 0713 24 0700 9 ry 21 0700 2 Y - 34 0700 2 y 15 0700 5 y 1 0700 2 2 27 0715 24 0700 9 y 72 Y 0715 24 0700 9 y „ 0715 24 0700 9 y 36 0610 2 n Al 0630 2 n 4, Nt...1.1.,w..ns Limit 1 (556.1 1.1 3 "."6""-e' 0.004 54 5 0 001 0.0105 Mil,1Ld.•w 0 005 106 0000 0.061 0•81,1(wn.m 0003 13 ,0 0 "••No Reporting Reason:ENFRUSE No F1ow•RcuseRec)dc; ENVWTHR No Visiranon Adverse Weather. NOFLOW No Flom. HOLIDAY ,No Violation-Holiday 1 NPDES PERMIT NO.:NC0005312 PERMIT VERSION:4.0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plant CLASS:WW-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4, ORC IIAS CHANGED:No eDMR PERIOD: 12-2017(December 2017) VERSION: 1.0 STATUS:Processed COMPLIANCE STATUS:Compliant CONTACT PHONE k:3368351083 SUBMISSION DATE:01122/2018 ( ---L-2 -. n/ 01/18/2018 ORC/Certifier Signature/len E Gary E-Mail:glen.gary@duvaltex.com Phone #:(336)835- 1083 Date By this signature.I certify that this report is accurate and complete to the best of my knowledge. The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. lithe facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of the NP permit. �Z v cSi„J /-023- I 01/22/2018 Permittee/Submitter Signature:** Cott Taylor E-Mail:scott.taylor@truetextites.com Phone 8:207-876-3331 x6418 Date Permittee Address:304E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018 I certify.under penalty of law.that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the system.or those persons directly responsible for gathering the information the information submitted is,to the best of my knowledge and belief,true. accurate.and complete.I am aware that there are significant penalties for submitting false information.including the possibility of fines and imprisonment for knowing violations. CERTIFIED LABORATORIES LAB NAME:True Textiles,Inc. CERTIFIED LAB 8:5010 PERSON(st COI.LECTING SAMPLES:Glen Gary.Billy Stone PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit(919)807.6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms. FOOTNOTES Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. 'No Flow/Discharge From Site:Check this box if no discharge occurs and as a result,there are no data to be entered for all of the parameters on the DMR for entire monitoring period. •'ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 8G.0204. •*•Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2XD). NPDE,S PERMIT NO.:NC000532 PERMIT VERSION:4 0 PERMIT STATUS:Active FACILITY NAME:304 East Main Street plantCLASS:W W-4 COUNTY:Surry OWNER NAME:True Textiles Inc ORC:Glen Edward Gary ORC CERT NUMBER:989696 GRADE:WW-4 ORC HAS CHANGED:No eDMR PERIOD: 12-2017(December 2017) VERSION: 1.0 STATUS:Processed Ostia!!00I-Effluent Cornmeal,: No samples taken on December 25 and 26 in observance of the State holiday. Contract Laboratory Qualified Lab Data �s¢December 4,5,6, 11,12,20,21,22.28Emuent BOD Analyte recovery in the laboratory control sampk(LCS)was below QC limits.Results for this analyte in associated samples December be biased low 5�¢December 4 Effluent TSS The precision between the sample and sample duplicate exceeded laboratory control limits. rt;¢December 7. 11,12,15,19,20 Effluent BOD The dissolved oxygen depletion of the water blank exceeded 0.2 mglL