NC0004685_Renewal (Application)_20180303

liC ROY COOPER
Governor
MICHAEL S.REGAN
Secretary
Water Resources LLNDA CULPEPPER
I:NVfP0NMEi TAL QUALITY Intejjj D1FEclor
March 03, 2018
Todd Douthit, Manager Manufacturing
Electric Glass Fiber America LLC
940 Washburn Switch Rd
Shelby, NC 28150
Subject: Permit Renewal
Application No. NC0004685
Electric Glass Fiber America LLC
Cleveland County
Dear Applicant:
The Water Quality Permitting Section acknowledges the March 2, 2018 receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 1506-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit.
The permit writer will contact you if additional information is required to complete your permit renewal. Please respond
in a timely manner to requests for additional information necessary to allow a complete review of the application and
renewal of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
rr6../ 6).,tv-kil
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Laserfiche File w/application
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh,North Carolina 27699-1617
919-807-6300

GLASS FOR FUTURE
rh Nippon Electric Glass
Renewal of NPDES Permit NCOOO4685
Electric Glass Fiber America, LLC, Shelby, N.C. Facility
February 28, 2018

GLASS FOR FUTUPE
GNippon Electric Glass
Via Certified Mail
Return Receipt Requested
February 28, 2018
Wren Thedford
NC DEQ
Division of Water Resources
WQ Permitting Section — NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Ms. Thedford:
RECEIVEDIDENRIDWR
MAR 0 7 2018
Water Resources
Permitting
940 Washburn Switch Rd
Shelby, North Carolina 28160 USA
T: 7044134-2261 )024
E: [e-mail]
Todd Douthit
Plant Manager
Electnc Glass Fibers America
Nippon Electric Glass
Subject: Renewal of NPDES Permit NC0004685
Electric Glass Fiber America, LLC, Shelby, N.C. Facility
CEC Project 122-243.0017
MAR 0 2 2018
We are pleased to enclose an original, signed NPDES Permit Renewal Application package along
with the two required photocopies. This is for Electric Glass Fiber America, LLC. (EFGA) facility
in Shelby, NC. We are requesting the reissuance of NPDES Permit No. NC0004685. The primary
SIC Code for facility operations is 3229 -Pressed and Blown Glass- not elsewhere classified.
Approximately one percent of the waste load is from the Hanwha sheet laminate facility (SIC
3083). The wastewater outfall, Outfall 001, is located at latitude 35 degrees, 20 minutes, 26
seconds, by longitude 81 degrees, 37 minutes, 0 seconds with the receiving water being Brushy
Creek.
There have not been any changes to the facility since the previous permit renewal. We request
that all NPDES permit issues be directed to Mr. Richard Young, Focus Factory Manager. The
facility Manufacturing Manager, Maintenance Manager, and Enterprise Excellence Manager are
authorized to sign all reports required by the permit.
As part of this permit renewal package, we have included:
1. Cover letter;
2. Introduction;
3. EPA Form 1;
4. EPA Form 2C;
5. Narrative description of the sludge management plan; and
6. Analytical data.

2
The data presented in Form 2C Section V is based on plant operating data for the period December
1, 2016 to November 2017 and special analysis conducted by Pace Analytical Services Inc. Copies
of the Pace reports on the special analysis have been provided in the package (Tab G). The plant
operating data is from monthly DMR submittals.
We are respectfully requesting NCDEQ consider the following changes to our NPDES permit:
1. Eliminate the fluoride monitoring only requirement: The fluoride utilizing processes have
been eliminated from operations at EGFA and formerly, PPG Industries Fiber Glass
Products, Inc. This past year three samples were below 0.5 mg/1, with one sample at 2.2
mg/l.
2. Reduce the oil and grease testing to once per month. Oil and grease has not been detected
above detection levels over the last 52 weekly samples.
3. Test for ammonia October through March only: Ammonia has only been detected during
winter operations because of possible nitrification inhibition during low basin
temperatures. To monitor for this possibility, we request reducing ammonia monitoring
during the winter months only, specifically during October through March.
4. The current permit requires quarterly sampling for copper, lead and zinc. None of these
metals has been detected over the last several years. For this reason, we respectfully
request reducing the metals testing to semi-annually.
5. The EGFA wastewater treatment plant is a biological treatment plant with chemical
addition as shown in the attached application. Chemical addition is commonly ancillary to
biological wastewater treatment, including addition of coagulants, flocculants and pH
adjustment comparable to the activities conducted at this treatment plant. For this reason,
we request a change in the clarification of the treatment plant to biological 3 only,
eliminating the additional PC2 classification. Please note that NCDENR rescinded the PC2
classification in 2015 for the PPG Industries Fiber Glass Products, Inc., Lexington, NC
wastewater treatment plant, which is comparable to this plant.
Please feel free to contact me if you need any additional information or if you have any questions
regarding this submittal.
Sincerely,
Todd Douthit
Plant Manager
Electric Glass Fiber America, LLC.
Attachment
cc: Richard Young
File

Electric Glass Fiber America, LLC
Shelby, North Carolina
NPDES Wastewater Permit Renewal Application for Permit Number NC0004685
TABLE OF CONTENTS
Introduction..........................................................
Sludge Management Plan
EPAForm 1 ............................................
EPA Form 2C — pages 14
Attachments to Form 2C Sections IIA and IIB
EPA Form 2C — Intake and Effluent Characteristics — Outfall 001
EPA Form 2C — Intake and Effluent Characteristics — Outfall 002
Figures
TopographicalMaps................................................................
Laboratory Reports
PaceAnalytical........................................................................
I
Tab A
...............................Tab B
Tab C
Tab D
Tab E
.Tab F
Tab G

INTRODUCTION
Electric Glass Fiber America, LLC (EGFA) operates a Fiber Glass manufacturing facility in
Shelby, North Carolina. This facility operates under the existing NPDES Wastewater Permit
Number NC0004685 which expires on August 31, 2018. This permit allows the facility to
discharge treated wastewater at 1.3 million gallons/day to outfall 001 and to discharge non -
contact cooling water to outfall 002. In addition to EGFA's Fiber Glass Manufacturing
operation, a Hanwha sheet laminate manufacturing facility is located adjacent to the EGFA site
and discharges approximately 10,000 gallons per day to the EGFA Wastewater treatment plant
for treatment. Wastewater from EGFA and Hanwha operations are sent to EFGA's wastewater
plant for treatment and both operations are covered under the existing permit. Additional details
and clarification for several items relevant to this permit application are highlighted below.
1. SIC Codes and Outfall 001 Testing
The SIC code for the Hanwha (sheet laminate facility) is 3083. The Hanwha site
discharges 10,000 gallons wastewater per day to the EGFA wastewater treatment plant
for treatment. This discharge makes up approximately 1/I00t' of EFGA's wastewater
flow. Therefore, as required for the 3083 SIC code, EGFA performed volatile compound
testing on Outfall 001. Results from this testing are incorporated into Form 2C of this
application.
2. Outfall (002) Testing
Outfall 002, the primary stotmwater outfall, is currently permitted for the discharge of
non -contact cooling water. Therefore, EGFA conducted the testing as set forth in Form
2C. This testing also included the required volatile compounds for SIC codes 3083.
3. Wet Weather Only Outfalls
Outfalls 003, 004, 005, 006, 007 and 008 are covered under the General Stormwater
Permit #NCG070000, Certificate of Coverage #NCG070015. These outfalls are wet
weather outfalls only and would contain little, if any, drainage from industrial areas. For
this renewal, testing was not conducted on these wet -weather outfalls.
4. Sample Reporting and Averaging
Sample reporting and averaging was provided in Form 2C as per NCDEQ DWQ's
"Directions for Completing Monthly Monitoring Reports " dated March, 2014. These
instructions provide guidelines with respect to rules for reporting and averaging less than
detectable "<" values. (i.g., a sample result with a value of less than the detectable limit
is considered to equal "zero" when calculating monthly and long-term arithmetic
averages). Also per NC DEQ DMR reporting guidelines, fecal coliform monthly and
long -tern averages were calculated using a geometric mean.
5. Signature Authority
There will be no change requested in signature authority for monthly monitoring report

requirements. Signature authority for monthly reports as a "Duly Authorized
Representative" per 15A NCAC 2B.0506(b)(2)(D), will remain unchanged and is
delegated to the people holding the titles of Manufacturing Manager, Maintenance
Manager and Enterprise Excellence Manager.

SLUDGE MANAGEMENT PLAN
The wastewater treatment plant (W WTP) sludge generated by the Shelby facility is a mixture of
both primary and secondary sludges. The primary sludge is the result of clarification using lime,
aluminum chloride, polymers and coagulants to achieve floc formation and settling. The
secondary sludge is waste activated sludge from the biological treatment system. The secondary
sludge also contains bentonite clay and a small amount of ferric chloride.
Both sludges are combined in a sludge thickener/storage tank prior to dewatering. Polymer
addition and mechanical mixing, along with dilution water, are required to prepare the sludge for
the belt press. The sludge is then pumped to the belt press for dewatering.
The belt press has both a gravity drain section and a pressure section where the water is removed.
Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25-30% solids as
discharged from the belt press. The dewatered sludge is transported via screw conveyors to a
roll -off box. The water is routed back to the head of the W WTP.
Before the roll -off box is picked up for disposal, a paint filter test is conducted on the sludge to
ensure that free liquids are not present. The dewatered sludge is then taken to a permitted, lined
landfill for disposal.

TAB A
EPA FORM 1

Please print or type in the unshaded areas
L11 -in areas ares aced for ei8e type i. e_
FORM
N=�EPA
GENERAL
LABEL ITEMS
I. EPA I.D. NUMBER
III. FACILITY NAME
acteynch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92
U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
GENERAL INFORMATION F 110000349070 T)" o
Consolidated Permits Program
ad the "General Instructions" before starting.) I ' 1 2 13 1+4 15
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE
MAILING LIST
VI. FACILITY
LOCATION
questions, you must submit this form and the supplemental from listed in the
the supplemental form is attached. If you answer "no" to each question, you
excluded from Dermit reouirements: see Section C of the instructions. See at
produced water other quos which arc bmugn[ ro
the surface in connection wnh conventional oil ornatural
MARK "X"
SPECIFIC QUESTIONS
res
No FORM
ATTACHED
A. Is Nis facility a publicly owned treatment works
which results in a discharge to waters of the
❑
® ❑
U.S.? (FORM 2A)
fluids for storage of liquid hydrocereons?
ATTACHED
Does or wi Iia aciity (either axis ng or
16
17 18
C. Is this facility which currently results in
discharges to water of the U.S. other than
®
❑
those described in A or B above FORM 2C
22
23 24
E. Does or will this facility treat, store, or dispose of
the instmctions and which will potentially emittootons
hazardous wastes? (FORM 3)
❑
® ❑
produced water other quos which arc bmugn[ ro
the surface in connection wnh conventional oil ornatural
❑
MARK "X"
gas production, inject fluids used for
containing, within one quarter mile of the well
enhanced recovery of oil or natural gas, or inject
YES
fluids for storage of liquid hydrocereons?
ATTACHED
Does or wi Iia aciity (either axis ng or
FORM4
31
1 32 1
sthis faci iy a proposed ataUonary sourcewhich
❑
L35
is one of the 28 indusmal categories listedin
feeding operation or aquatic animal
special processes such as mining of suiler by the
the instmctions and which will potentially emittootons
production facility which results in a discharge
per year of any air pollutant regulated
❑
M
under the Clean Air Act and may affect or belocated
t9
20
in an attainmentrea? FORM5
s this propose aci iy (of er man those descnbed
NAME OF FACILITY
❑
SKIP I Electric Glass Fiber America,
LLC.
Young, Richard, Focus Factory Manager
the
I any
area
the
nlhesis following the question. Mark "X" in the box in the third column if
I not submit any of these forms. You may answer 'no" if your activity is
action D of the instructions for definitions of bold-faced terms.
uo you or will you inject at this maiay'no usmal or
municipal effluent below the lowermost stratum
❑
MARK "X"
SPECIFIC QUESTIONS
containing, within one quarter mile of the well
FORM
YES
I NO I
ATTACHED
Does or wi Iia aciity (either axis ng or
(FORM 4)
31
1 32 1
proposed) include a concentrated animal
❑
®
❑
feeding operation or aquatic animal
special processes such as mining of suiler by the
production facility which results in a discharge
Frasch process, solution mining of minerals, in
❑
M
to waters of the U.S.? (FORM 2B)
t9
20
2t
s this propose aci iy (of er man those descnbed
❑
®
❑
in A or B above) which will result in a discharge
37
38
uo you or will you inject at this maiay'no usmal or
municipal effluent below the lowermost stratum
❑
®
❑
containing, within one quarter mile of the well
bore, underground sources of drinking water.)
(FORM 4)
31
1 32 1
33
Do you or will you inject at this facility fluids for
special processes such as mining of suiler by the
Frasch process, solution mining of minerals, in
❑
M
❑
situ combustion of fossil fuel, or recovery of
geothermal energy? (FORM 4)
37
38
39
Is this facility a proposed stationary source
which is NOT one of the 28 industrial categories
❑
M
❑
listed in the instructions and which will potentially
emit 250 tons per year of any air pollutant
reoulated under the Clean Air Act and may affect
1940 Washburn Switch Road I
Shelby
940 Washburn
Cleveland
6`[a]
l!I-I i9
C. CITY OR TOWN D. STATE E. ZIP CODE F. COUNTY CODE
Shelbv NC 28150
EPA FORM 3510.1 (&90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII BIOLOGICAL TOXICITY TESTING DATA
v,,,.,e.a,.. ti -nam to behave that env biolooical test for scute or chronic twdedy has been made on any of your discharges or on a receiving water in
relation to your discharge within dM last 3 years?
❑ V111)
© YES (Idrnnfr rAr tnK+) onihir.mbr d.1,l r7vxa Arlon) NO (go ro .14,11.
Chronic toxicity testing (Ceriodaphnia) is conducted quarterly per NPOES permit requirements.
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Rem V pedormed by a contract laboratory or consulting fmn7
® YES (list the name. add.. anal "deplane rasher of an i f-11"mnts araly_ed hy. ❑ NO (ko ra Sailon Al
rack such lahoraory orfin a helox)
C.
D. POLLUTANTSANALYZED
A. NAME
B. ADDRESS
(area code hno.)
i
Pace Analytical Services, Inc.
9800 Xineey Avenue, Suite 100
[phone]
All except PB,
(EPA Lab Code: NC00014) WW Cert.
Huntersville, NC 28078
temperature,lov level
chlorine, conductivity, WET
No. 12
and (MBAs a CTAS)
BNCO Laboratories, Inc. WW Cert.
102 Woodwinds Industrial Ct. Ste. A
[phone]
No. 591
Cary, NC 27511
Research and Analytical
106 Start St.
[phone]
Toxicity, Surfactants (NEW
Laboratories, Inc. WE Cert. No.
PO Box 473
a CTAS)
34, Biological Cart. No. 14
Kernaraville, NC 27284
IX. CERTIFICATION
1 cathfl, under penalty of law that this document
and all attachments were prepared under my direction
or supervision in accordance
with a system designed to assure that
qualified personnel property gather and evaluate
the infonnedon submitted Based on my inquiry
of the person or persons who
manage the system or those persons
directy, responsible for gathering the information.
da information submitted is, to the best of my knowledge
and belief, true, accurate,
and complete. I am aware that there
ere significant penalties ler sub"Ifing Wise
information, including the possibility of fine and imprisonment
forknowing violabona.
A. NAME 6 OFFICIAL TITLE (01. or praQ
B. PHONE NO. ro d, @ no.)
/�
7 C.A �ou�A.T lanr �an. er-
��(//arca
7o (- 4.34-2.?
C. SIGNATURE
D. DATE SIGNED
^
EPA Form 3570-2C (8-00) PAGE 4 of 4

TAB B
EPA FORM 2C
PAGES 1-4

EPA I.D. NUMBER (cap,)m. /rem l rjFann 1) Form Approved.
110000349070 OMB No. 2040-0086.
Please Drint or Noe in the unshaded areas only. I Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
„EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consokdeted Pearl Program
I. OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER B. LATITUDE C. LONGITUDE
(fur) 1. DEG. 2. MIN. 3. SEC. 1. DEG, 2. MIN. 3. SEC.
D. RECEIVING WATER (name)
001 35 20 26 81 37 0
Brushy Creek
002 35 19 23 81 38 12
Unnamed Tributary to Beaverdam Creek
003 35 19 36 81 38 7
Unnamed Tributary to Beaverdam Creek
004 35 19 48 81 37 44
Unnamed Tributary to Beaverdam Creek
005 35 19 42 81 37 38 Unnamed Tributary to Beaverdam Creek
IL FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units. and outfalls. If a water balance cannot be determined (e. g., for certain mining activities), provide a pictonal description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water mrlotf; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT
FALL
NO. (h I)
b. AVERAGE FLOW b. UST CODES FROM
a. OPERATION (list) (include units) a. DESCRIPTION TABLE 2C-1
001
see Attachment 2CII.e. Outfall 001
002
Non -contact Cooling eater 115.000 GPD None
underground spring eater 35,000 GPO None
Stormiater - Peak Plov. i-1hr 74.9 CFS None
003
Stormvater - Peak Plow i -/hr 13.9 CPS None
004
stormvater - Peak Ploy 1'/hr 2.3 CFS Ponx
005
9toonwater - Peak Flow 1"/ht 1.3 CPS
Continued on Nexc Page...
OFFICIAL USE ONLY (e/flnenl ¢uuideGnes slrheoregoner)
EPA Form 3510.2C (8.90) PAGE 1 of 4 CONTINUE ON REVERSE

EPA I.D. NUMBER (copyfrom lnnr l JPan„ 1) Form Approved.
110000349070 OMB No. 2040-0086.
Please print or type in the unshaded areas only. I I Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLIFOR PERMIT TO DISCHARGE WASTEWATER
.=CEPA EXISTING MANUF CTURING,4COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
I. OUTFALL LOCATION
For each outfall, list the latitude and longitude of Its locaflon to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER B. LATITUDE C. LONGITUDE
(l-) 1. DEG. 2. MIN. 3. SEC. 1. DEG. 2. MIN. 3. SEC.
I D. RECEIVING WATER (.a,,)
006 35
19
23 81
37
18
Unnamed Tributary to Beaverdam Creek
007 35
19
25 81
37
29
Unnamed Tributary to Beaverdam Creek
008 35
19
24 81
37
48
Unnamed Tributary to Beaverdam Creek
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water. operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more debuted descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and oudalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of. (1) All operations contributing wastewater to the effluent, including process wastewater. sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets K
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT
FALL
NO. (Gori)
b. AVERAGE FLOW b. LIST CODES FROM
a. OPERATION (list) (melude umrs) a. DESCRIPTION TABLE 2C-1
006
stoxmwacer - Peak Plow 1" Er 2,a CFS Nene
007
stormvater - Peak Plov 1^/Er 12.2 CPS None
OOB
9torewater - Peak Flow 1^/hr 12.9 CFS None
OFFICIAL USE ONLY (e{puen, gurd h.,,r sub-cmrgones)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (¢ampler, rhe /ollowmg table) m NO (go w Semon lll)
3. FREQUENCY
4. FLOW
a. DAYS PER
WEEK
I rwfe
awmgr)
b. MONTHS
PER YEAR1.
(avr''h"r"ergr)
a. FLOW RATE (,n mgd)
B. TOTAL VOLUME
Ir( -A 1. 11h note)
1. OUTFALL
NUMBER (141)
2. OPERATION(s)
CONTRIBUTING FLOW
(ImJ
LONG TERM
AVERAGE
2. MAXIMUM
DAILY
1. LONG TERM
AVERAGE
2. MAXIMUM
DAILY
G DURATION
(in Jmx)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑ YES (comp/ere Ire. 111-13) ® NO W, m Sorunn AV)
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure ofoperaXon)?
❑ YES (complete ire. 1110 ® NO (lw m Srauon 11)
C. If you answered 'yes' to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(G.rr anyali rmmberr)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
e. OPERATION, PRODUCT, MATERIAL. ETC.
AP -h')
IV. IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may effect the discharges described in this application? This includes, but is not limited to,
permit conditions. administrative or enforcement orders, enforcement compliance schedule letters, stipulations. court orders, and grant or loan conditions.
❑ YES (complete the (ollowmg roble) NO (go ro Gem 11'-B)
1. IDENTIFICATION OF CONDITION,
AGREEMENT, ETC.
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
a NO.
D. SOURCE OF DISCHARGE
a REQUIRED
b. PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK W IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8.90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA Fofm 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reeaon to believe that any biological Lest for acute or chronic toxloity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
© YES (,dery Jwhe rare) ore/ drsmbe rhea purpurer hrlow) ❑ NO (Su lir S'ern. Vlll)
Chronic toxicity testing (Ceriodaphnia) is conducted quarterly per NPDES permit requirements.
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(her the name. ddm.. anal Weplrone.,.ber o%am/palhaanh onoly-edhy. ❑ NO (g. to S'ation/d)
each ,h lahumrury orinn hdl )
C. TELEPHONE
D. POLLUTANTS ANALYZED
A. NAME
& ADDRESS
(ore. axle Ann.)
(fist)
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
(704) 1175-9092
All except pH,
temlerature.low level
(SPA Lab Code: NC00014) ww Cert.
Hunteraville, NC 28078
chlorine, conductivity, war
No. 12
and (tABAB a CTAS)
ENCO Laboratories, Inc. wN Cert.
102 woodwinds Industrial Ct. Ste. A
[phone]
No. 591
Cary, NC 27511
Research and Analytical
106 Short St.
1336) 996-2841
Toxicity, Surfactants IFAS
Laboratories, Inc. ww Cert. No.
PO Box 473
a CTAS)
34, Biological Cert. No. 19
%<rnezaville, NC 27284
IX. CERTIFICATION
1 cedify under penally of low that this document and all attachments vers prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel property gather and evaluate the inhumation submitted. Based on my inquiry of the person or persons who manage Me system or Mose persons
directly responsible for gathering the information, the Information subrra(fed is, to the best of my knowledge and belief, We, accurate, and complete. I am aware that them
are significant penalties for submitting false information. inducting the possibility of fine and imprisonment Mr knowing violations.
A. NAME a OFFICIAL TITLE (npe uryrrer)
B. PHONE NO. (ams cods Ano)
/
odd J'.4.1 Plant /'law. er"
Ios4 t�34F-z2G�
C. SIGNATURE
C1AT UR1/�+/�^/'Illi, - [
D. DATE SIGNED
z - ZS- ( 8
EPA Forth 351 D -2C (8-90) PAGE 4 of 4

TAB C
ATTACHMENTS TO FORM 2C
SECTIONS IIA AND IIB

EPA FORM 2C SECTION ILA
OUTFALL 001 SCHEMATIC
Electric Glass Fiber America, I.I.C.
City Water Supply
1,500,000 gpd
Research Misc.
Sanitary
Boiler Misc Process
Filtration Forming
1,000 gpd 3,000
60,000
43,000 Water
15,000 850,000
Bpd
Bpd
gpd 75.000 gpd
gpd gpd
poration
Stormwater Garage/ PadsL—C33
(185,000 gpd)
W WTP
,000BPd
1" rainfall
(See W WTP Schematic)
Product
1,300 gpd
HANWA SIC CODE 83083
-10,000 gpd
�\
Sludge
OUTFALL
DewateringP MGD
33,250 gpd up [0 1.3 MGD

EPA FORM 2C SECTION ILA
OUTFALL 002 SCHEMATIC
Electric Glass Fiber America, LLC.
City Water
Supply
Stormwater
98.6 acres
Non -Contact
peak flow =
Cooling up to
74.9 cfs
115,000 gpd
Underground
Spring est.
35,000 gpd
Outfall
#002
Up to 150,000 gpd
+ stormwater
Notes:
Outfall #002 is the primary stormwater outfall for the Industrial portions of the property.
Cooling water discharges from the outfall are permitted under #NC0004685.
Stormwater Discharges are covered under the General Stormwater Discharge Permit #NC070000,
COC #NCG070015
Stormwater Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q = peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1 = Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flow for stormwater was calculated using an intensity of 1"/hr.
The runoff coefficient (C) used was 0.76 based on the following estimate: 80% Industrial, (0.9).
10% wooded (0.1)

EPA FORM 2C SECTION ILA
OUTFALL 003, 004, 005, 006, 007 & 008 SCHEMATIC
Electric Glass Fiber America, LLC.
Stormwater Stormwater Stormwater Stormwater Stormwater Stormwater
30.8 acres 3.1 acres 2.7 acres 9.0 acres 33.8 acres 2.6 acres
Outfall Outfall Outfall Outfall Outfall Outfall
#003 #004 #005 #006 #007 #008
Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow
12.9 cfs 2.3 cfs 1.3 cfs 2.8 cfs 12.2 cfs 0.9 cfs
Discharges from Outfalls #003, #004, #005, #006, #007 & #008 are covered under the General
Stormwater Discharge Permit #NC070000, COC #: NCG070015.
These areas contain limited drainage from industrial areas of the property. Outfall 002 is the primary
stormwater discharge point of the Industrial portions of the property.
Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q = peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1= Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flows were calculated using an intensity of 1"/hr. See below for runoff coefficient
calculations.
RUNOFF COEFFICIENT CALCULATIONS
OUTFALL
C
003
0.42
20% Industrial (.9), 80% grassed (.3)
004
0.75
90% paved parking lot (.9) and 10% grassed (.3)
005
0.48
30% paved parking lot (.9) and 70% grassed (.3)
006
0.31
95% lawn (.3), 2.5% wooded (.1), 2.5% graveled (.8)
007
0.36
10% Industrial (.9) and 90% grassed (.3)
008
0.36
10% Industrial (.9) and 90% grassed (.3)

EPA FORM 2C SECTION 11.11
W WTP Treatment / OUTFALL 001 SCHEMATIC
Electric Glass Fiber America, I.I.C.
NPDES Permit NCOOD4685 Renewal Application
Process Water — (0.8 MGD)
Eary—(0.06 MGD)Screenater—(0.12 MGD) IT
HANWA—(0018MGD)
OUTFALL 0001
14
1 Flocculation
yA
Grinding IComminutors
1-0
I -T
xreenin
1-U
S .nrerl.non tsenlln I
Recycle /
I
2{
Coding water
1-0
al
3A
SLUDGE PROCESS SCHEMATIC
a.s
Gravely Thickener
3{
Bann
5-L
MWO.11
3-L
5-Q
Polymer
Belt Press
5-E.1-0.5{
Dilution
Water
Wast.H.W Sludge.
. &WVTPa-C .neB113-0
Grmcmg Flow toad Flash Mla Primary
li equalisation Equalization Tank CliinfZ
(;
1-O 2-D 1-0, Ili, 2l 1-U
time AICI Anionic Polymer
Slue to
Cationic Coaeulan[ Thickener
Secondary
Clarifiers (3)
2-C, 1-U 1-V
Anionic
Polymer
Sludge to
Thickener
Aeration
Tanks(!)
2-U
Lime
H1P0.
Defoamer
RAS to
Alratl0h
Bentonite
Clay
Treatment Codes Used From
Table 2C-1
14
1 Flocculation
1-L
Grinding IComminutors
1-0
Mi,ine
I -T
xreenin
1-U
S .nrerl.non tsenlln I
1-V
Ane Rltneon
2{
chem'.] P,.clphat..
1-0
ulat'on
3A
Ao...d Slud e
a.s
3{
Bann
MWO.11
3-L
5-Q

TAB D
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 001

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. Youmry report wma or M Mtlas Yrlormaborr EPA I.D. NUMBER (r., tn. Rem 1w Farm I)
n separate Mots (use fame •ama Rama" kal M Cwnpe lllp that papas. 110000349070
SEE INSTRUCTIONS.
EPA Form 3510.2C (690) PAGE V-1 CONTINUE ON REVERSE
ou FUL No.
V. INTAKE AND EFFLUENT CHMUCTERISTICS (mMnuadlpn pope S a✓Fpm 2{J
PART A -You mule poNde the revels of le Meet ave anaNMs W every POYand In Ws IaMe, C.4,14%. MDIs IYr each MIM, Sea W Wglon9 br 9WNbrW MM W.
8. UNITS
4. INTAKE
2. EFFLUENT
r r/Dark)
(n rana9
to. MAXIMUM W MY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a MAXIMUM DAILY VALUE
p/mrulaSle)
P/mnilaelr)
AVERAGE VALUE
If NO. OF
a. OONCEM
D. NO. OF
INiRAl10N
1. POLLUTANT
CONCE
121 MAIM
CONCENTIUTON
121 W35
111 CONCEMRATCN
121 MISS
ANALYSES
TgATION
D.MA86CpNCFNt{RAnca,
12)tM99
ANKYSEG
. BMFMmlcal OXYpw
7.2
31.2
2.33
9.95
1.71
7.22
52
mg/L
lbs
Demand (81111)
to ChemlWOgym
<25
0
1
h /L
lbs
Demand (I
c Total Oman. C.
4.5
24.4
N/A
N/A
N/A
N/A
1
mg/L
lbs
Dent )
Total
Soad. IDSDeoded
4.0
21.7
1.0
i
52
mg/L
lbs
c. Arn.la(iuM
c0.1
0
52
Tg/L
lbs
VALUE
VALUE
VALUE
VALUE
L Fax
0.65
0.57
0.50
365
MGD
9. Temperleure
VALUE
VALUE
VALUE
VALUE
p.rmw)
25
23.3
19.6
258
'c
In. TemPoroture
VALUE
VALUE
VALUE
VALUE
(rnm•v.)
28
27.5
24.1
258
'C
MINIMUM
NUM
MINIMUM
MAAMUM
rPH
6.2
.4
258
STANDARD UNITS
PARTB- MaM'X'tncobmn24MrtRhpM Youknowor Mvemesonto DMew Iapms Ma 'X'nwlumn2.EWawhpq MyoubWieve IoeaeawM.BpumaMWumn2aMranyp aMR iUMfimdedeew
detwN. or inor" but exannall In an emMM MrstMms pWaYra, you mule praiw Na Marls of N bast oM anaMlsW Me Poluleni Fp other polulaMa M anaw You mark colo m 2s, you must anoM9a
Uan4MM 4N p N e rytipl dlMa porlearral n alcr thicintep, CoMpeta oM MDM M Ycl1 MMa1. Gee the nstnIobons for notational Meals aM nalmaMt.
2. MARK -X' 3. EFFLUENT
4. UNITS
5. IN (, -W))
L POLLUTANT
D. MAXIMUM M DAY VALUE c LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a b a. MAXIMUM DAILY VALUE (rl m�uluM1lrJ (rlmrnlnnlo)
VALUE
CAB NO.
O. W. OF a CONCENY
II)
b. NO. OF
ffi.E ED OFU'V O 1y M Ile
N-4dk)
PRESENT AHSEM C XT'aonI (21.6 COrICENTRATON 121MV9 CONCEN ,,A 121M0.49
ANALYSES TRATION b.MAIS CpNCEMMiIIXi IIIMA59
AIULYBEB
a womdo
�/
(2495"7-9)
x
E. ClAonne Toad
xRandUN
Calor
X
d.F«N Caklmm
20.0 3.38 1.96
52
M/100 ml
�X
04994tH)
/� 2.2 11.9 2.2 10.5 0.85 3.5
4
mg/L lbs
L NtrnwNmM
X 17.4 94.3 17.4 82.7 14.63 61.0
4
mg/L I lbs
P• M
EPA Form 3510.2C (690) PAGE V-1 CONTINUE ON REVERSE

ITEM V -B CONTINUED FROM FRONT
EPA Fa m 0515W (690) PAGE V-2 CONTINUE ON PAGE V-3
2, MARK
W 3. EFFLUENT
4, UNITS
5. INTAKE ( mall
1. POLLUTANT
b. MAXIMUM 50OAY VALUE
c. LONG TERM AVRG. VALUE
E. LONG TERM
AND
b a. MAXIMUM DAILY VALUE
4f—fik/r)
(ilmwluAlol
AVERAGE VALUE
CAS NO,
BEUEVED
BEUEVEO III
4. NO. OF
E. CONCE
III b. NO. OF
GI
III
l�/mnilunl•1
VRESENL
4BSEN! CONCENTPAI RIk4bB
CONC ,AnON
121 MARS
CONUNTRAIIDN
121 MAW
AWILYSES
TR
E. MASE
CATION ENTWITION (21MA99 ANALYSES
W
TOW 0,'.0,'.(u.
1)
/)(\
b'apa"n
<5
52
mg/L
lbs
o.Z.X
L P"o.pnome
\ '
Ma Pl, T./X\
3.6
19.5
3.6
:7.1
1.32
5.5
4
mg/L
lbs
(222}1401
1. Radosc
(1)PWM1a. To1W
X
(2) Beta. Telal
X
Ta1N
HI Ra4wm )2S.
TOW
SU MY
(u•.ar�
32.1
174.0
1
mg/L
lb.
(1H06TSd1
SJAE
v
(m 1)
n. SUIMa
v
1AMsiSJ)
I. . Sunaclanb
X
u0.4
O
1
mg/L
lbs
a. AN—
TOW
X X0.1
0
1
mg/L
'.b.0A2&965)
p. Baum0 . T"W
(2N -2i2)
X
(7 24)
X
0.36'
1.9
1
mg/L
lbs
r. C.w Tei
�/
(7""")
x
X
<.05
o
1
mg/L
lb.
('43"M)
I. M.'.0 .
Tow
X
2.]B
12.9
1
mg/L
The
(74310,9")
u. Mo114Meum,
Total
X
(74WW7)
v Manpan —
T..l
X
(743
.. T. Taal
V«aysl
x�/
TiUm..
TOW
XH
324)
EPA Fa m 0515W (690) PAGE V-2 CONTINUE ON PAGE V-3

EPA FOm 351620 (600) PAGE V-3 CONTINUE ON REVERSE
EPA I.D. NUMBERI 1— Ixw 1,0— — I)
OUTFALL NUMBER
130000349070
001
CONTINUED FROM PAGE 3 OF FORM 2-C
PART C - B you aro • primary eMumM 0M Ws ou11Y caMYM promas ymmtvM ar. most to Table 202 in nM Immruch na to Memnle which of Me GCIMS harlcns you Mum Ier for Me* X- In column 2+ for Y such GCrWS
f... Inal apply to your neumry ant for A.l logo me1W. ayame.s. W halal pMnob. B your are rid I Wre4 to mark column 2-a (aemWvy whir mrs nWpowss wuMw Vat oullYk. a+0 mnapuia0 GUMS
/a lou). me* 'X' in column 240 for each ptlla6tl you know or Im. ruwn t0 bIIMW Is owes nl. Mah'X' In COWmn 24 for /NN pollution you ONls" Is abs/n1. M you Want column 2a M " pdYXam, you mug
prouf4alhe mMs Of at Mug A. m IFw m that poWlala. B you mark column Tb for any polulamyou must prou4e the mWhs of at ben one analysis for that po1Mn0 M you kn.w or haw rump to N"n 0 MI M
discharged In co sommea lam of 10 ppb or pnatx. B you mi Column 21, for aGoMn. acryon tri La binllrophand, or 2-mMh*4. B Mnt rophanol, you mum prowft the stab of M Mar OM mMy ns for each of them
pokilem. WhKh you halon a hew me. 1. Nam. MM you OiaCMrya M CpKemm.ne.1100 opo or greater. 01Mm10e, W polN/ma for Which you mark column 2b, you mum either submit r Mar an Nei or
brieRy, 0eacme this MOWS the poeueu is ingsi 10 W 4iWhargeo, We Met Mime ant 2 pees to Ibis pm. plea4 1aMaW each camugy, CompMa .m takes (as ) Fear) M each ouCY, Sea iMMC1Mm for
a40MoM MOM and mememenb.
2 YARN'X'
3. EFFLUENT
4, UNITS
5. INTAKE (aryi�Ml
1. POLLUTPNT
p. MAVMl1N b DAY VALUE c. LONG TERM AVRG.
a. LONG TERM
ANO
• n.
a
a. MAXIMUM DNLY VMUE
p/mru,Ae) VALUE(a—d.AW)
AVERAGE VALUE
CASNNMBER
TESnNG BFIIEVEO
BEpE'E.
IL NO. OF
aLONCEN-
ar
ly
Ill Ip
(11
Of—for")
gEOVIRED Pg. T
ABSENT
LONLENIIUnW 121 MP64
CONCENTMTON 12I AUS$ CONLENigAl10N I$I MP 33
ANALYSES
TRATION b. MASS
LgyLENTRAWN 121NP33
NIOLYSF
YSE
METALS, CYANIDE, AND TOTAL PHENOLS
I M. MMnmy, Tobi x(]eW26U)
2WAr•arm, Tpbl
X c0.01 0 1 mg/L lb.
pee0.J62)
3M. BwyWm, TWA x(]4641-T)
4M_Ca mu JoW xIT
-191
SWImT440-42-3 X c.05 0 l mg/L lbs
0
IM.Cappw, TOW
x c0. 005 0 4 mg/L lbs
74654a)
X <0.005 0 4 mg/L lbs
QM4C9-931) 1
BM. M.—q TOW X
OU497-g
9M. Nickel, TOW X
n4WA2n1
I OM. Smamum, X
TOW In32O3-2)
IM, Sh
I1ect.22 X c0.005 0 1 mg/L lbs
-e) )TOM
12M. Thallom.
TWA (7440-2M) X
13M, Zinc. Tonal
(Tee6 ) X
14M, CyaWOe,
TOM (57.12-5) X
Tar
DIOXIN
2.)754.m-/
DESCRIBE RESULTS
chbmWMn
x
Oenn 11940(t -01
EPA FOm 351620 (600) PAGE V-3 CONTINUE ON REVERSE

EPA Form 061&2C (&so) PAGE VJ CONTINUE ON PAGE V-5
L MARN'N'
S. EFFLUENT
(UNITS 6. WTARE (,,-A
1. POLLUT,WT
p. YNOYUY 50 WY VALUE c. LONG TERM AVRG,
a LONG TERM
AND
e.
c
p. YAEIMUM DAILY VALUE r/mrulr2lel VALUE 41m .....b q
AVENGE VALUE
GAS NUMBER
tEaiING 19FilEVED
I)EUEVEO
p. NO. OF
aCONCEW Itl
NO OF
Itl Itl Itl
...R/nT
(r/rnrnlW(r)
PEOUMED PPESENi
IBSEM
CONCENiMnm III. cO 121. CONCENTRATION
121 MRaa
ANALY$EB
TRATION p.MA55 CCNCEMMiNIN 121 MA55
YSE
GC MS FRACTION- VOLATILE COMPOUNDS
IV.xm
X
<.005
0
1
1Pg/L
lbs
,01L221
ZV. M1e
X
0
11g/L
lbs
pox --11p')
<.05
(71412) e
X
0
1
mg/L
lbs
<.002
lnilow-
` V
—,M&
X
(U2M 1)
(N2d&II
SV. &omobm
X
c.002
0
1
mg/L
lbs
(7}2&2)
eV. Cemw
TerveUlro00e
X
x.002
0
1
mg/L
lb.
eruenexc.002
0
1
mg/L
lbs
/�
W(7M�3);
\ ,ene
X002
0
1
m3/L
lbs
enww
xc,002
0
1
mg/L
lbs
/�
w. 2CNwu
nyNinyl Ener
X
<. 005
0
1
Pg/L
lbs
'M")
IVC( .r �/
x
002
0
1
mg/L
lbs
(6xd&])
<.
tN. O"<Nwa
p,omemen.ne
X
c. 002
0
1
mg/L
lbs
(7&Ix�l
I IV.OvlAero-
tiluwomeuene
X
<. 002
0
1
Irg/L
lbs
Ix&2t-0
14v. 1.
X
<. 002
0
1
11g/L
lbs
..117=3)
Isv. 1.2-O ,N
X
c.002
0
1
mg/L
lbs
em.o (0)-06-x1
Iw.tYOCNoro-
X
c.002
0
1
11g/L
lbs
enslwN OS]Se)
IN. LDI?eNwo-
x
c.002
0
1
I1g/L
lbs
FreP.napuxal
/�
IeV., }ptlYoro-
prp ne
X
c.002
0
1
mg/L
lbs
Isea>sil
Iw. Enseeniem
V
x
c, 002
0
1
mg/L
The
tl00M1-el
2w. MenM
X
< 002
0
1
mg/L
lba
9romlEe (4(191
xtV. M.
<.002
0
1
mg/L
169
CRMee (7"7.3)
EPA Form 061&2C (&so) PAGE VJ CONTINUE ON PAGE V-5

EPA Fwm 35162C (690) PAGE V-5 CONTINUE ON REVERSE
2 MARK'%'
3. EFFLUENT
A. UNITS
5. INTAKE ( 1wn,0
1. POLLUTANT
N W IDA
p. MAXIMUM b MY VALUE
p. LONG TERN AVRG.
Anse)
A LONG TEPM
AND
p
c
.- MAXIMUM DAILY
VALUE
O
VALUE TERM
AVENGE VALUE
GAS NUMBED
iEstlnG BELIEVED
O. NO. OF
e. CONGER
III
p. NO.Of
BELIEVED P) III DI
(r/rnvrlurtle)
REWMED MEWND
/rBSEM
CCNCEMMIIOx
13)NI
CONCENTMTICN 121M.9S
C.4')RA11ON
-"'AS
ANALYSES
TPATION
p. MASS
CONCENTRATRIR 131MA55
YSE
GCNS FRACTION- VOLATILE COMPOUNDS Kwmw,..p
2N. M."In.�/
x
<. 002
0
mg/L
lbs
Cw.(75aa2)
-
3]V. 1.1.3 L
T.tr.vNo�wm.n.
X
<.002
0
1
mg/L
lbs
0.345
24V. T.p.dA..
�/
c.002
0
1
mg/L
lbs
Mllene(t2i-1H)
/�
25V. TuA—�/
x
<.002
0
1
mg/L
lbs
000.90.3)
28V. laTrem-
umMrwmA.ne
X
<.002
0
1
ng/L
lbs
156da5
2N, IJ 1 -TA
X
<. 002
0
1
mg/L
lbs
.mem (7tasal
/�
2ev.t �,3-Trwewo
V
<.002
0
1
mg/L
lbs
39v inWwo-
�/
c.002
0
1
mg/L
lbs
empme psora)
/�
]pv. Tnrlba
W— .m.n.X
<.002
0
1
mg/L
lbs
S"
nV'wnA CNI
V
<.002
0
1
mg/L
lb.
75010
3CIM5 FRACTION -ACID COMPOUNDS
IA. 2LMmopMnd
x(9S53a)
IA1.6pWwo-
x
ppwwl (1200.0.21
/�
e9ry4
X
0-
ppenN O05-07-9)
000
sA. souvveo-
�/
x
Cre.a lsNa2-t)
5A2.-pMb
xOw
(51.10.5)
9A 2—W,"
(W7] 5)
]A 4Npop .
1100-92- )
SA. Pcnlwow
�/
x
C'..,, (511-W)
9A. P.nla
X
Men.l (eland)
pAPn M
tloa9sx)
11A 2. aTrh:JN o-
xAh.d(eapen)
EPA Fwm 35162C (690) PAGE V-5 CONTINUE ON REVERSE

EPA F01m 351120 (6%) PAGE VE CONTINUE ON PAGE V4
2. MARK'%'
I
3. EFFLUENT
t UNRS
5. INTAKE (, ,—A
1. POLLUTANT
b. MAXIMUM M DAY VALUE c. LONG TERM AVRG.
•. LONG TERM
XND
• e
r
a. MAXIMUM DAILY VALUE (✓m.uLA,I.) VALUE yLnvJWrle)
AVERAGE VALUE
CAS NUMBER
TEsnNO BFilEvBG
BEUEYEO
O.NO.OF
aCONCEK
O. NO. OF
III tlI 1D
I+1
REOUIREO PRESENT
A85EM
CONLEMMTION 12)MAM CONCENTIUTC I21MA55 CONCE("MMN 12)N>99
ANALYSES
T TION E.M s
CCNCENTFATION 121 NA95
YSE
GCMS FRACTION- BASEMEUTRAL COMPOUNDS
1B. A..., .n
xjo:LM4)
28.hmyNeNM
Ro6M-01
x
/�
38. MNr.wn.
�/
(12112-7)
x
.B.e«Imn.
�/
(92-02.5)
x
5& e.rix•(•)
AMN•c•n.
v
x
(5655]1
88.Bmxo lul
x
Pyram (.2132-7)
/�
28. 3.-0•nxo-
Marne,m•
X
(205843)
ee. e•nm LN,p
x
PNyNm (191342)
/�
9B. Bmza (i)
Flum•nNme
x
1202L69)
/�
11;11;
v
Bl)
.9b-1)
118. BY Q, N,,—
E
V
111 )
/�
B.BNG
20,
(M.,m(t024p]
X
0@-0PI
'3& ltlM.
;]8.81.1:
"17
..005
0
1
mg/L
lb.
1-71
(112x141
+48. A N.nf1
E6 r
EB,er
x
ool-P.
(101-56]1
/�
158. BNM B.N]31
V
x
PBMM•N 185594)
168.zLNao-
x
p+-5aq
ne.acnolP
Bbn,M 2-3ENw
x
)
/�
IM
C"
x
(218-01-9)
ne. Dea,:.1x(11
(52-79
x
(5NP0
/�
208.1.2-PtlWro-
�/
X
b.rmm• 1BSso-+I
2+8. 1.]LMIbu
b.ru•n. I5.u511
x
EPA F01m 351120 (6%) PAGE VE CONTINUE ON PAGE V4

CONTINUED FROM PAGE VA
EPAFa 661M1X(690) PAGE V-7 CONTINUE ON REVERSE
]. MARR'1C 8. EFFLUENT
.. UNRS
5. WARE( imwQ
1. POLLUTANT
b. MAMMOM W DAY VALUE c. LONG TERM AVRG.
.. LONG TERM
AND
p
•. MA%MUM DNLY VALUE (�I m.ulw�lel VALUE 1
AVERAGE VALUE
CAB NUMBER
TESIINO BELEVEO
tl. NO. OF.
b. NO. OF
BELIEVED tli 111 111
111
(�/mutlulAel
REOUREO PRESENT
A W coNCENTPAT1di 121MA55 CCNCENiMi1CN 121M65 CONCENTRAT1oN 121M0.55
ANALYSES
TRATION b. MASS
CIX FNTMTK 121MAss
YSE
GC/MS FRACTION –B NEUTRAL COMPOUNDS (—,-0
228.tFpmiors
x
22B. 3,1A —
(91-W )
xb....
NB. D .N
Nb m.4(.#2)
258. N .Mo
PM1N9M.
�/
(131-11-3)x
MB_p WW
<. 005
0
mg/i :bs
Ph,M.t. (S 7] 21
219.2,.-09.bo-
�/
WIN. (121-1.-31
x
2e8.36-0.Ao-
�/
1pwme ISoe-2a31
/�
298. DN2-0uM
x
2OB. 11-Dp
hyd,.. (.v Am-
Lenzene 1122E 4)
11 B. M—nN.n.
v
20f )
12B. FW—n.
v
0o-727
228.....Wpro-
�/
b.m.n.0W4-11
x
NB. N...Worn
x..0on.lmaa»
558. N.uWoro-
(77474)
(17�1�)
MBINO.Waa
.mM. l(67-72-1)xz-t)
/�
37B. lmm.
11.22WPn.n.
�/
Ii W5)
/�
me l.apliwm.
x
(7 SWl)
29B. N.PIM.In.
ISI -2021
08. NM.bmmm
�/
(969}2)
x
.IB. N Ypu
..,Z,l.m1n.
162-7s9)
420. KNromo&
NAapyMMn.
X
031#
EPAFa 661M1X(690) PAGE V-7 CONTINUE ON REVERSE

CONTINUED
EPA Form 351aX (690) PAGE Vd CONTINUE ON PAGE V-9
3. MARK X'
3. EFFLUENT
A. UNRS
5. INTAKE (......p
1. POLLUTANT
0. MAXIMUM 30 MY VALUE
a LONG TERM AVRG.
•. LONG TERM
AND
9. MAXIMUM ONLY VALUE
0/mndAle)
VALUE phm.n4Al.1
AVERAGE VALUE
CAS NUMBER
TE6TNG BHIEVFD
BELIEVED
E. NO. OF •CONGER
III
E. NO.OF
pl
ly III
(�lmvllu5l<)
REOLWED %iESEHT
ABSEM
CONCENTRRTION 1$I MA$$
CONLENTRATIpI DI MA55
CONCENTRATION 131 MA55
AILALVSES TMTION U. MASS
CONCENTRATION I$I MA55
LYSE
GEMS FRACTION-BASEMEUTRAL COMPOUNDS 1-1--))
RtMb
4338.
9w6.ewme,.
l(8&3M)X
u5. PnmMlwe••
g5-0I.el
x�/
458. P5,«I•
D$?9a9)
X
b8. I $.4TM1
X
02 1
140.6b4q
OCMS FRACTION - PESTICIDES
1p.N \/
13699o-$) x
2P—AHC �/
x
Otswd)
JP. �/
(3t"&7) x
AP. AHC
(56da9) X
OF n.B11C
94661 X
IP. CM * �/
57-749) x
:P. A•'.DOT X
156$631
9P. 4.4 -DDE
p3-5Sq X
9P.•A''ODD
3SHr X
maszp
IIP.�.-E�e.JM1n �/
n1636n x
11P. 9 -End• w
nlb 9n X
IJP. Eb.&AOP
X
IIOJI-0741
" 03,
14P. Entrin
p$-$691 X
15P. EnJn
N6e6Y6
X
(H31 -9]J)
16P. Hepd< X
(76N6)
EPA Form 351aX (690) PAGE Vd CONTINUE ON PAGE V-9

EPA I.D. NUMBER (.,y/ Ire.l w— ii OUTFALL NUMBER
CONTINUED FROM PAGE V4 110000349070 001
.PA PAM 351030 (6 W) PAGE V -B
3 EFFLUENT
4, UNRB�mmm�
5. INTAKE
1. PoLLUTANi
0. MAXIMUM 50 DAY VALUE
.. LONG TERM AVAG.
A. LONG TERM
AND
p
•. MA%IMUM DAILY VALUE
p/aalollr)
VALUE yl.nrmhlr)
AVERAGE VALUE
CAG NUMBER
TE NO BELIEVED
BEUEYEO
O. NO. OF
6. CONGER-
O, NO. OF
III nl PI
111
(11.1 O
REWIRED PREMW
ABSENT
[DNCENTRATION 131 M466
GONCEN1MTdi 131 M455
CCNCENTNAPON 1]I MFSG
ANALYSEG
]RATION E. M/SG
CCNLENTM1. 131...
ZNALYGES
OCMG FRACT)ON- PEGTICIOES (rw11n1�r10
ITP. R.pr
` '
x
1102"1-3)
I fiP. PCB.1343
x
IBP.PCB-1154
I IOW -0&11
201. PCB -1331
x
S P. PCB.12u
v
-1")
(11141-1")x
33P. PC6t20
v
p3mz-za61
x
3IP. KS -1360
v
ItID%6351
/�
uv. vcB•tm6
836]411-31
Z1-]S3)T1=11 1
v
600
.PA PAM 351030 (6 W) PAGE V -B

TAB E
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 002

PLEASE PRINT OR TYPE IN THE UNSHADED MEAS ONLY. Youmay rpon some mal of eEarllub0n EPA ID. NUMBER (nryn Ir� free I of r,mn 1)
on•enere.afraid, lac. herr same kA+nM.Yeas d comple" these pepea 110000349070
SEE INSTRUCTIONS.
W fAI NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (CmlNurEAOTn pq ] of "i" 2 -C7
PART A-Ydu mol mom.In. ..I. d d Med mN anayeu for. very poYnFll in mill able. Complete oner vi W sell aullsl. Sas huwcuone Mr e5E5bnal ddaM.
3, UNITS
4. INTAKE
2. EFFLUENT
b M-Jelmkl
(e hmv0
b. MA%IMUNI 30 MY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
if. MAXIMUM DAILY VALUE
(r2mnlMN)
(rymmlNAlr)
AVERAGE VALUE
J. NO. OF
e. CONCEAL
b. NO. Of
I. POLLUTANT
CONCENRUTON
Or MASS
CONCENTRATION
121 MASS
IIICCNCENRATION
(2).
ANALYSES
TRATION
b. MAGS
CONCENTRATON
121 MA53
ANALYSES
e. B1.Mmael O'Non
<0.02
0
1
mg/L
lbs
Demand (6110)
b. Chemical OMen
.25
0
1
mg/L
lbs
Demand (IOP)
c. Total Organa Carom
2.1
0.53
1
mg/L
lbs
Irn1)
of TOW Suspended
Sold. (MI
Q 5
0
1
mg/L
lbs
e. AmmmM lm£)
0.27
0.07
1
mg/L
lbs
VALUE
VALUE
VALUE
I. Floe,
03
.03
01
.02
2
MGD
p. Twgrah a
VALUE
VALUE
VALUE
'C
VALUE
(.mire)
14
1
h. Temperature
VALUE
VALUE
VALUE
'C
VALUE
(mmmrr)
19
1
MINIMUM
MAXIMUM
MINIMUM
MAAMUM
i, PH
6.7
7.1
2
STANDARD UNITS
PARTS- Md 'X' in c.unn 2i for Oa pc M You k m un nasm to M w m pawn. Mark 'X' in column 2-b for each pdgnant You believe to be abl a at 6 ed. redk column 2. M Mly palulxp rhiclr is MNMO eller
dindly, m melent DN epreMlyin an eIMMM Inei atims pui.M.. you mull moved Ins neaps of At bast on. emesis lar that popuUmt. For What Miriam. lar which you mark cold. L. you must pri
yuaMpative Ens Dr en a .neigh ollMir 00011 n W CiMNr Complete one table for each oWal. See the lnslrudions ler addtional details and requirements.
2. MaRK'X].EFFLUENT 4. UNITS
S. INTNtEI nn+o0
t. POLLUTANT
b, MAXIMUM 00 MY VALUE c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
• e •. MAXIMIMI DAILY VALUE lr
VALUE
CAS NO.
d. NO. OF a. CONCETL
b. NO. OF
EEUEV O BFUEYED tll Ili Ip
111
b/✓rnJnblr)
PRESENT ABSENT CONCENTigN 121MA95 CCNCEN.. RI MASS CONCENTRATION 121 MASS
M
ANALYSES TRATION b.MASS
CONOENBATON L1 M435
ANALYSES
•.BeMd
(2495&
x52-91 I�
b.CNanne. TOW
�/ 1910 0098 19.0 10.5 .0018
2 ug/L lbs
Ruud M
.0098
/�
c C.I.
X
d. Feed CoM m
X
e. roan.
�/
('$a$ ")
x
I. Nbde-Nell•
X
be M
EPA Form 35100.2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V -S CONTINUED FROM FRONT
EPA FOml351PX (&W) PAGE V-2 CONTINUE ON PAGE V-3
2. MARK
'X' 3. EFFLUENT
4. UNRS
5. INTAKE tr w.rOO
L POILIRANT
9. M MkAM M DAY VALUE
O. LONG TERM AVRG. VALUE
B. LONG TERM
AND
n n. MAXIMUM DAILY VALUE
4/mrulullrl
4/.n.ulWlcl
AVERAGE VALUE
CAS NO.
BEIIEVEG
BEIIEVEO Itl
6. NO. OF
LCONCEK
U'NO'OF
111
Itl
(r/•nrrrlWle)
PFESEM
R05EM COrM:ENTRATIW I]ILWS
COruCENTRATKJN
I11 W95
Cd+[ENinAnON
(2)MASS
ANALYSES
]RATION
O.MA55 CONCEMRATON IIIMa95
W
ANALYSES
TOWIXen
pxxo lO,
x
1)
09On4
Ga"
x
(7T23 1w)
1. R6ON4ptlMN
(1)Abnp. tOW
X
(2)6ea, TmM
X
(3) R6vlum,
�/
x
Ta
R
14) Retlum 226,
v
k. SW ea
V
(ulO6-T9d1
S 9M
Ia•A
/�
x
n. SUMb
X14MS�w1
s mm�n
X
o. AMmnum,
T.
c0.1
0
1
Tg/L
lbs
(7429-965)
p. Bknum, TeW
v
(74 3P3)
'Boron. T"�/
(7""241
/�
33.7
8.4
1
mg/L
lbs
r. C" TOW
puwal
x
(P,I— T6W
X
1.37
0.34
1
mg/L
lba
IT
i)
TOaI
X
6.68
1.67
1
mg/L
lbs
4,3'
u. Md ...
Toal
�/
x
(T4]9-96)1
v. Manpeneu,
W
X
puo-vo-sl
a.T., TOW
�/
(]440.]13)
x
v. TNnlum,
Ta
X
R44"I$)
EPA FOml351PX (&W) PAGE V-2 CONTINUE ON PAGE V-3

EPA LD. NUMBER µsyn aim /um l o/Hem 11 OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C 1100003490J0 002
PART C - HIP rte • ppmcry mdugry and lags ousbl mmcmt peoceu wagawefar, nbr m Tebb 2u2In ms 1nglugbne to dgnmina wNO of the GCRAS iragbn. you mug nM for. Made Win column 2a lar N heck GCWS
hN1wrLL test apply to roar molugry eM for ALL bob therms Wedges. and nW Pllenok. If you sm MI didar e l to sees cdomn 2-e (Paoamd y lndognea nOnp9cism eggs. oWNk, clod mrvpueN Gcows
eegbn d meM -X' in column 2-b M mch pobmm you lama ce esn neon to bNbm is prompt. Me* 'X' In column 2-c for each pollultnt Wu Mason is absent. If you meM column 29 for airy poludid! you mug
mV the pea} a al beg om andabas M Mug poW Xg..passed, 2b bus goy pWYMfII, yW mug pnwUe 1M pasateoIst Mm10us market{ or test polaMmnYW sees G NN fisher, ba}N awi be
dlKMfpol In <oMsmnlbns 0110 ppb or yngef. If di mark Column 2b lar }rvb}, ecr i nus , 2.4 dlnNophenN, of 2 -methyl-<, 6 dInIINpNnol, you mug pfoNde IM neule of g beg one an.yxe lar each .1 than
pddaane which rou Mcw or Nag neem 10 stages beet you gedu ri n heedpnbgbne M too ppb w pnalef, gnerene, for popNSMe far whbh YW mete column 2b. YW mug mow euMns Is beg one order of
prefer mecnbe me reasons IM Pi M le e " to be g shad ed, Not that Nen to ) Payee to Nb pees. Flame reabw eah carefully, Complete one table mol 2 pcptg for each ruses. See Inclmdmne for
tddabMl dMa} ark maps
2. MAFtEX
3, EFFLUENT
t. UNDS
5, p TAXE Lnwma0
1. POLLI/TN9T
b. MAXIMUM 00 DAY VALUE c, LONG TERM AVRG.
a. LONG TERM
AND
p
a. MAXBAUM DAILY VALUE plmrnlmlr2 VALUE pluwnl�dlrl
AVERAGE VALUE
CAB NUMBER
TES,NO BELIEVED
gELIEVEO
d. NO. OF
a, CONCEAL
b. NO.OF
IO p1 III
"'RASION
III
"l—inter)
REOIIIREO PRESENT
ABSENr
C.,C 121 W65 CCNCEx(') TION 121 MA65 CONCENIRATON 121 eM65
ANALYSER
TRAT ON s. MA55
CONCENTRATION i21MA56
YBE
METALS, CYANIDE, AND TOTAL PHENOLS
I M. Ammon, Total
x
(7441 8L1
2M,Ari Tool
X <0.01 0 1 Ing/L lbs
0440.30.3)
-38-2)
3M. Beryllium, Tot x044011-01
SM. Cummum, Tot x(7a
3-91
SM. Chu mium,
<.05 0 1 mg/L lbs
ret(Taa0AT31
SM. Copper. Tot
x]NO-50d)
M. Lead, Tet
x(7439-2-1)
We. Mew, Tot x(7439
-974S)
9M. Will, Total
(7440-02-0)
ISM. Selenium,
Tot (T28N9-2)
��440Toral
.22-4) X <0.005 0 1 mg/L lbs
12M, Thabum,
Tot (7440.28-0)
13M. 21no Tolg v
(7440383)
1'M. Cysn", v
TMA (57-123)
15M. Phenols.
Tom
DIOXIN
1371 -TSA
\ /
DEBCRIBE RESULTS
deem (176 18)
EPA Form 3516X 18-01 PAGE V-3 CONTINUE ON REVERSE

THE FROM
2. MAR77
0. EFFLUENT
♦. UNITS S. INTAKE ( umuQ
1. POLLMANT
p. MA%IMUM JO MY VALUE
c. LONG TERM AVRG.
s. LONG TERM
AND N
�RIEIIIRIPRESENT
a. MA%IMUM DAILY VA UE pfM1!! e)
VALUE Q/mvJoDle
AVERAGE VALUE
CAS NUMBER 9FLEVED
BELIEVED
6NO.OF
aCONCEK IE
D. NO.OF
III 0,
IT
(il�nv�IMle)
ABSENT
COm.-r-ON RI Me88 CONCENIMTION 121M5s6
CONLENTRATON 121MFSa
AHALYaES
TRATION p. MA63 CCNCENIRATION RI MA55
LYSE
GCIMS FRACTION-VOI TILE COMPOUNDS
1V. in
V
c 005
0
1
mg/L
lbs
42'4)
N. AvAe
x
05
0
1
Ilg/L
lbs
(IDT -1y1)
9V. 314Un
B e
x
002
0
1
ng /L
lbs
2)
/�
<.
AV. Bb (01—
—*4 Eft
1L
0
1
mg/L
lbs
(%24 1)
SV. Brame .
x
002
0
1
mg/L
lbs
(S2"2)
w.cen
TroaNbIN
c.002
0
1
Ilg/L
lbs
@62151
N. CNm°pemru
x
<.002
0
3
mg/L
lbs
(1 7)
/�
ev. cw.m
N°m°mMMN
X
<. 002
0
1
^t3/L
lbs
12H41
X<.
002
0
1
mg/L
lbs
(S�JI
w.1LNws
IIM754d'r
X
<.005
0
1
Ilg/L
lbs
110.]5-0)
IIV.CNoff
X
002
0
1
lbs
(874�31IM
<.
m9/L
DOW.
I:Io..nie0..
<. 002
0
1
^Ig/L
lbs
(7"270
13V. PU
aMwemeuene
<, 002
0
1
mg/L
lbs
("714)
14V.I
uV. U75
X/
<.002
0
I
ag/L
lbs
-U -m-
O5->.-21
/�
15V. 1,2-DCMmo
x
002
0
1
mg/L
lbs
.—(107-06-2)
1�
X
<. 002
0
1
mg/L
lbs
ty��-0'y2,ylO"e
17V. 1.2-0iwpo-
�/
x
<.002
0
1
L
lbs
propene(S-0T4)
�/1
1
Iw. LlUtllbo-
`/
proppene
X
<. 002
0
1
rtg/L
lbe
(5/2-75b)
Iev. ENMeIRxN
V
<.002
0
1
mg/L
lbs
<. 002
0
1
IIg/L
lba
B—IM pHiy)
21V. LM"
<. 002
0
1
Dg/L
iba
cxwnae (uT4)
EPA Fpm 3510.20 (690) PAGE V4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE VJ
EPA Fpm 551&2C (&90) PAGE V.6 CONTINUE ON REVERSE
3. MARR-A-
0. EFFLUENT
�. UNITS
5. WTME
1, POLLUTANT
b. MA M, JO WY VALUE
e. LONG TERM AVRG.
.. LONG TERM
AND
b
rEWFE]
., MAA►IUM OAILY
VALUE
4/aml,.uel
VALUE (4 a+nlaele)
AVERAGE VALUE
CAS NUMBER
NSEUEYED
E. NO. OF
.. CONCEP&
b. NO.OF
BELIEVED 111 Iq Itl
tll
lr/wurlydla)
PRESENT
ABSENt
CONCEMMTON
(134
CONCENT TION 131 MA66
CONCENTRAl10N 131 MP66
ANALYSES
TRATION
b. MASS
LONLENTMTBN 2)MASS
YBE
GC/MS FRACTION– VOLATILE COMPOUNDS (•.wrnued)
2V, M.".�/
x
<, 002
0
mg/L
IDS
CM n& (7"0.2)
'
23V. 1112.
T... .
X
<.002
0
1
mg/L
lbs
VW
0.x&5
24V. Teb.a9«o-
V(127-1
<.002
0
1
mg/L
lba
25V.Tau.rn
25V. TE
x
<.002
0
1
mg/L
lbs
/�
Z6V.1]-Trem-
DicSN.eemylene
X
<.002
0
1
mg/L
lb.
156403
2N. 11.1-Tn
X
<.002
0
1
mg/L
lb.
emw. 171-5541
/�
28P¢neL1I-Trbi1]"651wo-
�/
<.002
0
1
mg/L
lb.
eme
/�
26v TRm«o-
X
<.002
0
1
my/L
Ins
Mllene p0.0181
/�
xM. Tria
Auemmemme
X
<.002
0
1
mg/L
lbs
540.
nv.wnP cm«le.
�/
x
<.002
0
1
mg/L
lbs
]w1;1
3CWS FRACTION—AC
IO COMPOUNDS
1A2CNwwmnm
x(9&5]-8)
3A.2 FQC
x0b.na
U2Me )
2A 26-0im *
�/
x
phend(105-0]-9)
U.6-0mNo O-
Creea (53444)
wz4 .
x0..1(51-2")
60.2.NbW-a
x(e&]&5)
7A.84.bapberM
�/
x
(I0 -02a)
BA. PCNwPK
�/
x
Cr..a 150-50.7)
9A PenMaiwa-
V
x
,h.na(8]-8&5)
1oA Pb.na
x/
11A.z10-Trw,we.
�/
ph.n, (ewsxl
x
EPA Fpm 551&2C (&90) PAGE V.6 CONTINUE ON REVERSE

EPA F Wm 351M36 (&90) PAGE V5 CONTINUE ON PAGE V-7
3. MARK'X'
J. EFFLUENT
6. UNRB
5. INTAKE (npumop
1. PoLLUTANT
p, MAXIMUM BO DAY VALUE c LONG TERM AVRG.
a. LONG TERM
AND
a b
c
a. MAXIMUM DAILY VALUE (�Im.wLdlq VALUE pLe+u✓W/z)
AVERAGE VP1UE
CAS NUMBER
1E911NG BEIJEVED
eEUEVED
O. No. OF
t CONCEK
b. NO, OF
III DI. III
111
/Mle)
PEST D PgESENT
ABSENT
CONCEN"' nON 131 MASS CONCE MAATION 131 MASS CONCE")FATON 131 MA55
ANPLYSES
TRNTION
b. MA
CONCENigA"LN I31 MA55
YSE
GCIMS FRACTION— BASE/NEUTRAL COMPOUNDS
1B.Acenaphth—
�/
x
(B1-33-9)
3B.Acen,hWne
�/
x
(3069641
38.M raun
�/
(130.1241
x
e8. B .-.
(9347-5)
se. Benzo (u)
Annnc.n.
X
(wss4)
BB. Beniu(o)
�/
x
P„.n. (5LLJ34,
7B. ].48enxu
&—r en.
(205A9-3)
ee. e.n:. peJ
x
Peplene 1191-N3)
/�
9B.Benz w
F0142.2ene
X
hM,.eo.
,M n)
X
M
11191-1)-')
110. Im
NInO Ether
x
/�
2B.
IB.
X
Ether (unpm0{1
03--1)
80
138, &
(117-014)
Nmyl
fAfl,I
PnmM mel
Em'
x
(101-sSJ)
/�
1 SB. wtM Ben4
�/
x
PMlliele(85 &7)
668.3-Chloro-
pl .N "
(91-567)
178, 4CM
0-0 Phenyl M.
V
x
(7 9 7za7
1318-01-9)
198.04enm (nh)
MPrew a
x
(5Y76J
I�
308.11-oicAbro-
X
benzene (9650.1)
r B.I to -NW.
�/
bmleene(5a1-7J1)
x
EPA F Wm 351M36 (&90) PAGE V5 CONTINUE ON PAGE V-7

EPA Form 3510.20 (8-90) PAGE V-7 CONTINUE ON REVERSE
x. MAR
3. EFFLUENT
<. UNITS S. INTAKE (n f—ul
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE c LONG TERM AVRG.
a. LONG TERM
AND
e.
r
c
a. MAXIMUM DAILY VALUE
IrlmnJnel.) VALUE y/mm4d/.)
AVERAGE VALUE
LAS NUMBER
STING eEuBVED
6EUEVE
a. NO. OF
a. CONCExt Ib.NO.
OF
D1
01 111
OI11RE0 PRESENT
PBSEM
CONCENTRATION O)MASS
CONCENTRATION ($1 MASS CONCENTRATION IxI MA55
ANALYSES
TRATION b. MASS CONCENTRATION I$I MASS
ANALYSES
GOATS FRACTION-BAS EUTRAL COMPOUNDS 1.•rmm,...0
22B.l/-D61om-
X
bemMe (101,x6'7)
235.3 HA~'
,M—d.na(91.941)
24B.0 MO
v
Nifialte(U,ML2)
25B.0meNyl
MNe11-
(131-11-3)
m. DI-N-Bum
P.M. 1x47421
27B.24-Dn.
taMenx (121-142)
28B. 26U
xtduens(606-30.x)
29B. CFN-0 M
PMheMP (I 17246)
enyt
311,.etl1,$-Dghne
hybrlee Azm
X
benzene111 x228-
EYrorannnna
21M 4o1
xOw
X
128. FMwem
xMMT)
338. Hesadloro-
benzene (1161411
.B. Heee.W.—
bubbene (87243)
35B. Hev.Mwo-
rydo7en
(71474)(71474))
]6B NeaaWw
�/
x
M.ne (67-72-1)
311,.1
11.13M1 Pyrem
PI
(193-39-51
39B. leophomne
nds9 p
31 B. NephNYene
91-20.3)
eOB. Ntrabenzsie
19695])
I�
X
B. liNltro-
it
oB�metrrylemim
X
(62459)
x2B. &Nitrosob-
N-%aONamine
X
16x121-71
EPA Form 3510.20 (8-90) PAGE V-7 CONTINUE ON REVERSE

ft1MIN11Ff1
3. MARX'X'
3. EFFLUENT
l UNITS
5. INTAKE (rr"_I
L POLLUTMIT
p. MAXIMUM 30 DAY VALUE
c. LONG TERM AWG.
A. LONG TERM
AND p,
c
e. MAXIMUM DAILY VALUE
(I/nrndnala)
VALUE [/wntlrAlo)
AVERAGE VALUE
CAB NUMBER iEsilNa BELIEVED
BELIEVED
d NO. OF L CONCEN-
E. NO. OF
(p
III p(
III
(rlwvJrrAle) REOVIRED PRESENT
ABSEM
CM'C ENTRRTION 121MA55
CONCENTMTIDN NIMASS
CONCENTRATIDN 131M496
ANALYSES TMTION p.MASS
CONLEMRRTI IN 121 MF5E
YSE
GCMS FRACTION– BASEMEUTRAL COMPOUNDS (n 1-1)
438 NN.o
alvOenyM1mma
�/
x
(B 3M)
.B. PnenurMana
�/
(am")
x
458. Pyrene
v
(130.00A)
468. 1.24Try
(120-02-1)
GCMS FRACTION – PESTICIDES
IP.NJin
N04Oo 21
2P. , BHC �/
x
(319-844)
MC v
4)
P
FP�HC
-9)
HC �/
x
1141641
53-048)
IP. 4A' -DOT
(5b2?3)
SP.4 f -DDE
(72 -SSB)
9P.4/' -DDD \/
(12-wx
)
IOP. peMrn v
(W5]-1)
11 P. u-EnamXm \/
(115-24n x
IIP. hEnauMen
1115.24(1 /�
x
I3P. EnaoWM1n
WIN,
(1031-012)
14P. En.n
(72-2")
uv.E e,m
M&h, e
(7421-9 1
16P.Hropc W
(7642)
EPA Fo m 3510.2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

SPA Form 35132C (390) PAGE V-9
EPA G. NUMBER(,, from Lam lu//u.m l)OU
NUMBER
110000349070
002TFALL
CONTINUED FROM PAGE V-0
. MARK 'X
]. EFFLUENT
4, UNITS
S. INTAKE ppumnQ
1. POLLUTANT
0. MAXIMUM ]0 DAY VALUE
c. LONG TERM AVRG,
a. LONG TERM
AND
nE
e.
a
e. MAXIMUM DAILY VALUE p/mmbM1le)
VALUE 01mmlMle)
AVERAGE VALUE
CAS NUMBER
6EUEVE0
0. NO. OF
6. CONCEN-
0_NO.OF
SEUEVE Ut Ol rn
III
I!Im IWe)
PRESEM
ABSEM
OgyCFMMnON 1$I MA55 GONCFNTRTTION 121 MA56
CONCENTRAPON 121 MA56
ANPLYSES
]RATION O. MA55
CONCENTgpTION 121 MA55
YSE
DONS FRACTION- PESTICIDES (r. ... . .Q
17P. HepncM1lw
1 e
X
(102to245]-])
16P. PCB -1242
(5]464219)
19P. PCS -1291
x(1108]631)
29P. PC0-1221 �/
(11104-2631 x
21P.PC0-1232 �/
(11141-163) x
22P. PCB -1248 v
(126]2-246)
23P.P061260 v
(1109F616)
24P. PCB -1016($62411'2)
15P. T...h.- \�
6001-052)
SPA Form 35132C (390) PAGE V-9

TAB F
TOPOGRAPHIC MAP
FORM 1
SECTION XI

Kingston )
9821
- _1,
OUTFALL 001 TO BRUSHY CREEK
LATITUDE: 35'20'25"
`�l J��-/ I LONGITUDE: 81'36'58de
"
W�wjI b o
/-77
Wiliam
3• - ' f� 'P
su6riNtyn hil.
•i• - 'f'�Ill:\ YY L •'
sae
OUTFALL 002 TO OVERFLOW
o r LATITUDE: 3519'27"
..
LONGITUDE: 81'37'50" + 1
1 REFERENCE SCALE IN FEET
y 1. U.S.G.S. 7.5' TOPOGRAPHIC MAP, BOILING SPRINGS NORTH NEEMMEEM
AND SHELBY QUADRANGLE, NORTH CAROLINA DATED: 2002. 0 2000 4000
,:,=,= ELE940 W S BTRIC S RN SWITCH ROAD S FIBER AMERICA, LLC
Civil & Environmental Consultants, Inc. SHELBY, NORTH CAROLINA
R 1900 Center Park Drive - Sufte A - Charlotte, NC 28217
Ph: 980.237.0373 - Fall: 980.237.0372 SITE LOCATION MAP
w .cecinc.com
ZDRAWN BY: JK$ I CHECKED BY: GPT APPROVED BY: - FIGURE NO.:
DATE: JANUARY 2018 DWG SCALE: V = 2000'1 PROJECT NO: 122-243.015

TAB G
LABORATORY REPORTS

zacAna4 al'
,,, pamws.mn
November 14, 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: Permit Renewal 001
Pace Project No.: 92361385
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Muntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
Ab, REPORT OF LABORATORY ANALYSIS
This report shall not be %produced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

-Pace Analytical"
•ww.pxe w o=
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9900 Kincey Ave. Suite 100
Huntersville. NC 28079
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

�PaceAnalytical"
xuwpxebba.ovn
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Sufte 100
Huntersville, NC 28078
[phone]
Project.
Pace Project No
Permit Renewal 001
92361385
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92361385001
001
EPA200.7
DS, SH1
7
PASI-A
EPA 625
Bpi
5
PASI-C
EPA 624
GAW
35
PASI-C
EPA 300.0
CDC
1
PASI-A
SM 5220D
SLB
1
PASI-A
SM 53108
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrl0en consent of Pace Analytical Services, LLC. Page 3 of 23

,162ceAnaocal'
ANALYTICAL RESULTS
Pau Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Permit Renewal 001
Pace Project No.: 92361385
Sample: 001
Lab ID: 92361385001
Collected: 11/01/1708:00
Received: 11/01/1709:00 Matrix:Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
Aluminum
NO
ug/L
100
1
11/07/17 01:15
11/13/17 14:49
7429-90-5
Arsenic
NO
ug/L
10.0
1
11/07/1701:15
11/14/1701:26
7440-38-2
Boron
367
ug/L
50.0
1
11/07/1701:15
11/13/1714:49
7440-42-8
Chromium
NO
ug/L
5.0
1
11/07/1701:15
11/13/1714:49
744047-3 P8
Iron
NO
ug/L
50.0
1
11/07/1701:15
11/13/1714:49
7439-89-6 PB
Magnesium
2380
ug/L
100
1
11/07/17 01:15
11/13/17 14:49
7439-95-4
Silver
ND
ug/L
5.0
1
11/07/1701:15
11/13/1714:49
7440-22-4
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA 625
Di-n-butylphthalate
NO
ug/L
5.0
1
11/0711710:06
11/08/1723:43
84-74-2
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
11/07/1710:06
11/08/1723:43
117-81-7
Surrogates
Nitrobenzene-d5(S)
53
q
10-120
1
11/07/1710:06
11/08/1723:43
4165-60-0
2-Fluorobiphenyl(S)
49
%
15-120
1
11/07/17 10:06
11/08/17 23:43
321-60-8
Terphenyl-014 (S)
58
%
11-131
1
11/07/17 10:06
11/08/17 23:43
1718-51-0
624 Volatile Organics
Analytical Method:
EPA 624
%crolein
NO
ug/L
5.0
1
11/03/1702:27
107-02-8
lcrylonilrile
NO
uglL
50.0
1
11/03/1702:27
107-13-1
3enzene
NO
uglL
2.0
1
11/03/1702:27
7143-2
Bromodichloromethane
NO
uglL
2.0
1
11/03/17 02:27
75-274
Bromoform
NO
uglL
2.0
1
11/03/17 02:27
75-25-2
Bromomethane
NO
ug/L
2.0
1
11/03/1702:27
74-83-9
Carbon tetrachloride
NO
uglL
2.0
1
11/03/17 02:27
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
11/03/17 02:27
108-90-7
Chloroethane
NO
ug/L
2.0
1
11103/1702:27
75-00-3
2-Chlorcelhylvinyl ether
NO
ug/L
5.0
1
11/03/1702:27
110-75-8 c2
Chloroform
NO
ug/L
2.0
1
11/03/1702:27
67-66-3
Chloromethane
NO
ug/L
2.0
1
11/03/1702:27
74-87-3
Dibromochloromelhane
NO
ug/L
2.0
1
11/03/1702:27
12448-1
Dichlorodifluoromethane
NO
ug/L
2.0
1
11/03/1702:27
75-71-8
1,1-Dichloroethane
NO
ug/L
2.0
1
11/03/17 02:27
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
11/03/17 02:27
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
11/03/17 02:27
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
11/03/17 02:27
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
11/03/17 02:27
156-60-5
1,2-Dichloropropane
NO
uglL
2.0
1
11/03/17 02:27
78-87-5
cis-1,3-Dichloropropene
NO
uglL
2.0
1
11/03/1702:27
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
11/03/1702:27
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
11/03/1702:27
10041-4
Methylene Chloride
ND
ug/L
2.0
1
11/03/1702:27
75-09-2
1,1,2,2 -Tetrachloroethane
ND
ug/L
2.0
1
11/03/1702:27
79-34-5
Tetrachloroethane
ND
ug/L
2.0
1
11/03/17 02:27
127-18-4
Toluene
ND
ug/L
2.0
1
11/03/1702:27
108-88-3
1,1,1 -Trichloroethane
ND
ug/L
2.0
1
11/03/1702:27
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
2.0
1
11/03/17 02:27
79-00-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

Pats Analytical Services, LLC
aceAmlytical 9500 ncey Ave. Sude
Huntersville, NC 28078078
..areslsbs.owi [phone]
ANALYTICAL RESULTS
Project: Permit Renewal 001
Pace Project No.: 92361385
Sample: 001
Lab ID: 92361385001 Collected:
11/01/1708:00
Received: 11/01/1709:00 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared Analyzed
CAS No. Oual
624 Volatile Organics
Analytical Method: EPA 624
Trichloroethene
ND ug/L
2.0
1
11/03/17 02:27
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1
11/03/1702:27
75-69-4
Vinyl chloride
ND ug/L
2.0
1
11/03/1702:27
75-01-4
Surrogates
4-Bromofluorobenzene(S)
98 %
70-130
1
11/03/1702:27
460-00-4
Toluene-d8(S)
104 %
70-130
1
11/03/1702:27
2037-26-5
1,2-Dichloroethane-d4(S)
103 %
70-130
1
11/03/1702:27
17060-07-0
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
32.1 mg/L
1.0
1
11/06/1717:48
14808-79-8
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L
25.0
1
11/13/17 19:02
L2
53108 TOC
Analytical Method: SM 53108
Total Organic Carbon
4.5 mg/L
1.0
1
11/02/1719:15
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 23

/ !2C6Ana0cal e
weeyzelsbe.txvn
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
OC Batch: 385479
QC Batch Method: EPA 200.7
Associated Lab Samples: 92361385001
MSD
Spike
Conc.
Analysis Method:
Analysis Description:
EPA 200.7
200.7 MET
METHOD BLANK: 2137810
% Rec
Matrix: Water
Units
Conc.
Associated Lab Samples: 92361385001
%Rec
Limits Qualifiers
Aluminum
ug/L
5000
4640
Blank Reporting
85-115
Parameter
Units
Result Limit
467
Analyzed
Aluminum
ug/L
ND
100
11/13/1716:30
Arsenic
ug/L
ND
10.0
11/14/17 01:20
Boron
ug/L
NO
50.0
11/13/1716:30
Chromium
ug/L
200
5.0
11/13/1714:34
Iron
ug/L
188
50.0
11/13/1714:34
Magnesium
ug/L
ND
100
11/13/1716:30
Silver
ug/L
ND
5.0
11/13/1716:30
LABORATORY CONTROL SAMPLE: 2137811
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2137812
MS
92361368001 Spike
Parameter Units Result Conic.
MSD
Spike
Conc.
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
Aluminum
ug/L
5000
4640
93
85-115
Arsenic
ug/L
500
467
93
85-115
Boron
ug/L
500
456
91
85-115
Chromium
ug/L
500
446
89
85-115
Iron
ug/L
5000
4460
89
85-115
Magnesium
ug/L
5000
4470
89
85-115
Silver
ug/L
250
229
91
85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2137812
MS
92361368001 Spike
Parameter Units Result Conic.
MSD
Spike
Conc.
2137813
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Ret
Limits
RPD Qual
Aluminum
ug/L
ND
5000
5000
4760
4750
94
94
70-130
0
Arsenic
ug/L
NO
500
500
478
478
96
96
70-130
0
Boron
ug/L
0.090
500
500
557
560
93
94
70-130
1
mg/L
Chromium
ug/L
NO
500
500
444
442
88
88
70-130
1
Iron
ug/L
0.23
5000
5000
3450
3450
64
64
70-130
0 M1
ri
Magnesium
ug/L
1.6
5000
5000
6070
6090
90
90
70-130
0
mg/L
Silver
ug/L
NO
250
250
232
232
93
93
70-130
0
Results presented on this page ere In the units indicated by the'Unbs' column except where an alternate unit Is presentee to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 23

CeAnaytical e
eawrpaaltle.00+n
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Nuntersville. NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137814
2137815
MS
MSD
92361488001 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Conc.
Conic.
Result
Result % Rec
% Roo Limits RPD Qual
Aluminum ug/L
4650
4660
0
Arsenic ug/L
468
469
0
Boron ug/L
485
483
0
Chromium ug/L
626
625
0
Iron ug/L
4430
4490
1
Magnesium ug/L
4710
4750
1
Silver ug/L
229
229
0
Results presented on this page are in the units indicated by the 'UmW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

i �PaceAnaVical"
wewpacwaoacnm
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385093
Analysis Method: EPA 624
QC Batch Method: EPA 624
Analysis Description: 624 MSV
Associated Lab Samples: 92361385001
METHOD BLANK: 2134818
Matrix:
Water
Associated Lab Samples: 92361385001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1,1 -Trichloroethane
ug/L
ND
2.0
11/02/1717:58
1,1,2,2 -Tetrachloroethane
ug/L
ND
2.0
11/02/17 17:58
1,1,2 -Trichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,1-Dichloroethane
ug/L
ND
2.0
11/02/1717:58
11-Dichloroethene
ug/L
NO
2.0
11/02/17 17:58
1,2-Dichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,2-Dichloropropane
ug/L
NO
2.0
11/02/17 17:58
2-Chloroethylvinyl ether
ug/L
NO
5.0
11/02/17 17:58
Acrolein
ug/L
NO
5.0
11/02/1717:58
Acrylonitrile
ug/L
NO
50.0
11/02/1717:58
Benzene
ug/L
NO
2.0
11/02/1717:58
Bromodichloromethane
ug/L
NO
2.0
11/02/1717:58
Bromofonn
ug/L
NO
2.0
11/02/1717:58
Bromomethane
ug/L
NO
2.0
11/02/1717:58
Carbon tetrachloride
ug/L
NO
2.0
11/02/17 17:58
Chlorobenzene
ug/L
NO
2.0
11/02/17 17:58
Chloroethane
ug/L
ND
2.0
11/02/1717:58
Chloroform
ug/L
NO
2.0
11/02/1717:58
Chloromethane
ug/L
NO
2.0
11/02/1717:58
cis-1,2-Dichlcroethene
ug/L
ND
2.0
11/02/1717:58
cis- 1, 3-Dichloropropene
ug/L
ND
2.0
11/02/1717:58
Dibromochloromethane
ug/L
NO
2.0
11/02/1717:58
Dichlorodifluoromethane
ug/L
NO
2.0
11/02/1717:58
Ethylbenzene
ug/L
ND
2.0
11/02/1717:58
Methylene Chloride
ug/L
NO
2.0
11/02/1717:58
Tetrachloroethene
ug/L
NO
2.0
11/02/1717:58
Toluene
ug/L
NO
2.0
11/02/17 17:58
trans-1,2-Dichloroethene
ug/L
NO
2.0
11/02/1717:58
trans-1,3-Dichloropropene
ug/L
NO
2.0
11/02/17 17:58
Trichloroethene
ug/L
NO
2.0
11/02/17 17:58
Trichlorofluoromethane
ug/L
NO
2.0
11/02/1717:58
Vinyl chloride
ug/L
NO
2.0
11/02/1717:58
1,2-Dichloroethane-d4 (S)
%
97
70-130
11/02/17 17:58
4-Bromofluorobenzene (S)
%
100
70-130
11/02/1717:58
Toluene -d8 (S)
%
104
70-130
11/02/1717:58
LABORATORY CONTROL SAMPLE: 2134819
Qualifiers
Pap Analytical Semloee, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS %Res
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1 -Trichloroethane ug/L 20 18.2 91 52-162
fthh b presented on this page are in the unit. Indicated by the "Unit." column e ... pt where en Nterri unit la peMnted to tM right of ate neua.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Anal0t;al Services, LLC. Page 8 of 23

-PaceAna/ytical e
awwpxNebawm
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9800 Kincey Ave. Sufte 100
Huntersville, NC 28078
(704)8759092
LABORATORY CONTROL SAMPLE:
2134819
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
%Rec
Limits
Qualifiers
1,1,2,2 -Tetrachloroethane
ug/L
20
17.1
86
46.157
1,12 -Trichloroethane
ug/L
20
18.6
93
52-150
1,1-Dichloroethane
ug/L
20
17.5
87
59-155
1,1-Dichloroethene
ug/L
20
19.2
96
1-234
1,2-Dichloroethane
ug/L
20
18.2
91
49-155
1,2-Dichloropropane
ug/L
20
19.3
97
1-210
2-Chloroethylvinyl ether
ug/L
40
29.8
75
1-305
Acrolein
ug/L
100
130
130
15-152
Acrylonitrile
ug/L
100
89.0
89
75-132
Benzene
ug/L
20
18.5
93
37-151
Bromodichloromethane
ug/L
20
18.4
92
35-155
Bromoform
ug/L
20
16.3
81
45-169
Bromomethane
ug/L
20
20.1
100
1-242
Carbon tetrachloride
ug/L
20
18.5
93
70-140
Chlorobenzene
ug/L
20
18.1
91
37-160
Chloroethane
ug/L
20
18.9
94
14-230
Chloroform
ug/L
20
17.8
89
51-138
Chloromethane
ug/L
20
17.3
87
1-273
cis-1,2-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
19.2
96
1-227
Dibromochloromethane
ug/L
20
16.8
84
53-149
Dichlorodifluoromethane
ug/L
20
16.2
81
70.130
Ethylbenzene
ug/L
20
17.5
88
37-162
Methylene Chloride
ug/L
20
21.6
108
1-221
Tetrachloroethene
ug/L
20
18.8
94
64148
Toluene
ug/L
20
18.5
92
47-150
trans-1,2-Dichloroethene
ug/L
20
18.3
92
54156
trans-l,3-Dichloropropene
ug/L
20
18.9
94
17-183
Trichloroethene
ug/L
20
19.6
98
71-157
Trichlorofluoromethane
ug/L
20
17.9
90
17-181
Vinyl chloride
ug/L
20
18.2
91
1-251
1,2-Dichlorcethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene -08(5)
%
104
70-130
MATRIX SPIKE SAMPLE:
2134821
92361205001
Spike
MS
MS
%Rec
Parameter
Units
Result
Cone.
Result
% Roe
Limits
1,1,1 -Trichloroethane
ug/L
NO
20
20.9
105
46-171
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
18.2
91
73-159
1,1,2 -Trichloroethane
ug/L
NO
20
20.0
100
64152
1,1-Dichlormthane
ug/L
NO
20
20.1
100
43-172
1,1-Dichloroethene
ug/L
NO
20
22.1
111
48-189
1,2-Dichlormthane
ug/L
NO
20
20.4
102
42-171
1,2-Dichloropropane
ug/L
NO
20
21.6
108
55157
Results presented on this page are in the units indicated by Me -Unlu- column except where an alternate unit is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 23

,162ceft ytical e
wlrwystwkGe.mm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Sufte 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
ug/L
ND
ND
1,1,2,2 -Tetrachloroethane
ug/L
ND
Pace Project No.: 92361385
1,1,2 -Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
MATRIX SPIKE SAMPLE: 2134821
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
92361205001
Spike
MS
Ms
% Red
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Chloroethylvinyl ether
ug/L
ND
40
ND
0
70-130 M1,c2
Acrolein
ug/L
ND
100
138
138
70-130 M1
Acrylonitrile
ug/L
ND
100
101
101
70-130
Benzene
ug/L
ND
20
20.3
101
54-163
Bromodichloromethane
ug/L
ND
20
19.8
99
56-152
Bromoform
ug/L
ND
20
17.1
85
53-151
Bromomethane
ug/L
ND
20
16.8
84
10-200
Carbon tetrachloride
ug/L
ND
20
20.1
101
41-175
Chlorobenzene
ug/L
ND
20
20.7
103
67-152
Chloroethane
ugll-
ND
20
22.8
114
23-200
Chloroform
uglL
ND
20
18.4
92
51-166
Chloromethane
uglL
ND
20
17.0
85
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
21.2
106
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
19.9
100
38-146
Dibromochloromethane
ug/L
ND
20
18.8
94
65-144
Dichlorodifluoromethane
ug/L
ND
20
18.5
92
70-130
Ethylbenzene
ug/L
ND
20
19.8
99
57-152
Methylene Chloride
ug/L
ND
20
20.0
100
40-167
Tetrachloroethene
ug/L
ND
20
21.0
105
59-155
Toluene
ug/L
ND
20
20.6
103
47-162
trans-12-Dichlorcethene
ug/L
ND
20
21.1
106
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
19.4
97
39-148
Trichloroethene
ug/L
ND
20
21.7
109
60-153
Trichlorofluoromethane
ug/L
ND
20
21.3
107
42-199
Vinyl chloride
ug/L
ND
20
21.2
106
46-176
12-Dichlorcethane-d4 (S)
%
101
70-130
4-13romofluorobenzene (S)
%
96
70-130
7oluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1 -Trichloroethane
ug/L
ND
ND
1,1,2,2 -Tetrachloroethane
ug/L
ND
ND
1,1,2 -Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
2-Chloroethylvinyl ether
ug/L
ND
ND
Acrolein
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Results preaantetl an We pace an In the unea Inc2ote4 by the "Units" column excW where an altamab writ Is praaai b are right a/ the rnult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

2ceAnaVical a
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
NO
ND
Chlorobenzene
ug/L
ND
NO
Chloroethane
ug/L
ND
NO
Chloroform
ug/L
ND
NO
Chloromethane
ug/L
ND
NO
cis-1,2-Dichloroethene
ug/L
NO
ND
cis-1,3-Dichloropropene
ug/L
NO
ND
Dibromochloromethane
ug/L
NO
ND
Dichlorodifluoromethane
ug/L
NO
ND
Ethylbenzene
ug/L
NO
ND
Methylene Chloride
ug/L
ND
ND
Tetrachlorcethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
NO
NO
trans-1,3-Dichloropropene
ug/L
ND
NO
Trichloroethene
ug/L
NO
NO
Trichlorofluoromethane
ug/L
ND
NO
Vinyl chloride
ug/L
ND
NO
1,2-Dichloroethane-d4 (S)
%
100
102
4-Bromofluorobenzene (S)
%
100
97
Toluene -d8 IS)
%
106
102
RPD Qualifiers
2
3
4
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Muntersville, NC 28078
[phone]
Resulb pnwrlW on this page an in the ones IrMlute! by the'UnW column except where an Ntemate unit Is presel to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

PaceAnaVical e
www.pocabbs can
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385556 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92361385001
METHOD BLANK: 2138167
2138168
Matrix:
Water
Associated Lab Samples: 92361385001
Spike LCS LCS
% Ret
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Blank
Reporting
50 41.6 83
Parameter
Units
Result
Limit
Analyzed Qualifiers
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
11/08/17 11:48
Di-n-butylphthalate
ug/L
ND
5.0
11/08/17 11:48
2,4,6-Tdbromophetol(S)
%
88
10-137
11/08/17 11:48
2-Fluorobiphenyl(S)
%
73
15-120
11/08/17 11:48
2-Fluorophenol(S)
%
38
10-120
11/08/17 11:48
Nitrobenzene -d5 (S)
%
81
10-120
11/08/1711:48
Phenol -d6 (S)
%
25
10-120
11/08/17 11:48
Terphenyl-d14 (S)
%
74
11-131
11/08/17 11:48
Pace Anaytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
LABORATORY CONTROL SAMPLE:
2138168
2138170
Spike LCS LCS
% Ret
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
bis(2-Ethylhexypphthalate
ug/L
50 41.6 83
8-158
Di-n-butylphthalate
ug/L
50 40.9 82
1-118
2,4,6-Tribromophenol (S)
%
91
10-137
2-Fluorobiphenyl (S)
%
74
15-120
2-Fluorophenol (S)
%
39
10-120
Nitrobenzene -d5 (S)
%
78
10-120
Phenol -d6 (S)
%
29
10-120
Terphenyl-014 (S)
%
70
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2138169
2138170
MS
MSD
92361660001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Ret
Limits RPD Dust
bis(2-Ethylhexyl)phthalate
ug/L
NO
100
100
88.1
85.2
88
85
8-158 3
Di-n-butylphthalate
ug/L
NO
100
100
87.7
83.4
Be
83
1-118 5
2,4,6-Tribromophenol (S)
%
100
98
10-137
2-Fluorobiphenyl (S)
%
73
77
15-120
2-Fluorophenol(S)
%
53
52
10-120
Nitrobenzene-d5(S)
%
80
81
10-120
Phenol-d6(S)
%
45
43
10-120
Terphenyl-d14(S)
%
48
39
11-131
Results presented on this page are In the units indicated by Me -Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

PaceAnaVical e
arw-0rraleD<.mrr�
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385402
QC Batch Method: EPA 300.0
Associated Lab Samples: 92361385001
METHOD BLANK: 2136998
Associated Lab Samples: 92361385001
Parameter Units
Sulfate mglL
LABORATORY CONTROL SAMPLE: 2136999
Parameter Units
Sulfate m91L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8769092
QUALITY CONTROL DATA
Analysis Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 11/06/1713:48
Spike LCS LCS % Rec
Com. Result % Rec Limits Qualifiers
50 49.7 99 9x110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137000 2137001
MS MSD
92361863002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L NO 50 50 52.4 52.9 104 105 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137002 2137003
MS MSD
92361823001 Spike Spike MS MSD MS MSD e/ Rec
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 53.0 53.1 106 106 90-110 0
Result. presented on MIs page em In the units indicated Ey me "UnlW column except where an alternate unit Is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

2ceAnayicalo
sarwPacablet com
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Hunters,ndle. NC 28078
(704)8759092
Project:
Permit Renewal 001
Pace Project No.:
92361385
OC Batch:
386547 Analysis Method: SM 5220D
QC Batch Method:
SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92361385001
METHOD BLANK: 2143913
Associated Lab Samples: 92361385001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2143914
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 11/13/1719:02
Spike LCS LCS % Rao
Conc. Result % Roo Limits Qualifiers
1120 751 67 90-110 L2
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143915
2143916
MS
MSD
92360409001 Spike
Spike
MS
MSD
MS MSD %Rec
Parameter Units Result Conc.
Conic.
Result
Result
% Rao % Rao Limits RPD Qual
Chemical Oxygen Demand mg/L 803 150
150
900
907
65 69 90-110 1 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143917
2143918
MS
MSD
92361431002 Spike
Spike
MS
MSD
MS MSD % Rao
Parameter Units Result Conic.
Conic.
Result
Result
% Rec % Rao Limits RPD Qual
Chemical Oxygen Demand mg/L 27.0 150
150
145
141
79 76 90-110 3 MO
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services. LLC.
Page 14 of 23

/ ZeAnaVical*
auw.psosltla.ayn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kmcey Ave. SuHe 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 384971
Analysis Method: SM 53108
QC Batch Method: SM 5310B
Analysis Description. 5310B TOC
Associated Lab Samples: 92361385001
METHOD BLANK: 2133960
Matrix: Water
Associated Lab Samples: 92361385001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
11/02/17 16:28
LABORATORY CONTROL SAMPLE: 2133961
Spike LCS
LCS % Rec
Parameter Units
Conic. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.6
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2133962 2133963
MS MSD
92361364001
Spike Spike MS
MSD MS MSD %Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Dust
Total Organic Carbon mg/L 9.5
25 25 32.4
32.3 91 91 90110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/1412017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

PaceAnalytical
Kincey Ave. Suite 100
aceAnalytical a Huntersvllle, INC 28078
m. w.pacelabs. caro (704)0769092
QUALIFIERS
Project: Permit Renewal 001
Pace Project No.: 92361385
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below OC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
This repo" shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23

/ ZcAnapical e
e Pecsieba.mn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Permit Renewal 001
Pace Project No.: 92361385
Pap Analytical Services, LLC
98001(incey Ave. SuRe100
Huntersville, NC 28078
(704)8759092
Date: 11/14/2017 05:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 23
Analytical
Lab ID
Sample ID
OC Batch Method
OC Batch
Analytical Method
Batch
92361385001
001
EPA 200.7
385479
EPA 200.7
385555
92361385001
001
EPA625
385556
EPA625
385759
92361385001
001
EPA 624
385093
92361385001
001
EPA 300.0
385402
92361385001
001
SM 5220D
386547
92361385001
001
SM 5310B
384971
Date: 11/14/2017 05:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Ralelgh❑ Mechanicsville[]
• `lien` Name:
me: ^` i�G�� Projecta:I WN 92361385
L C TV1 U �bfi Q� �:JILh II'III IIIII�I'IIIIIIII
Courier: ❑Fed Ea ❑UPS ❑USPS ❑Client
❑ Commercial [')Pace []Other:_ 92361386
t
Custody Seal Present? ❑Yes NO Seals Intact?
rryX/
Packing Material: ❑Bubble Wrap LJBubble Bags
Thermomet `
IR Gun ID: �tqU1 Ty7f
Correction Factor: Cooler Temp Corrected PC):.
Dyes Oo
Date/Initial; Person Examining Contents: 1
❑None❑ Other Biological Tissue Fr ran?
[]Yes ❑No N/A
wet ❑Blue ❑none
Temp should be above freezing to 6'C
❑Samples out of temp criteria Samples on ice. coding process
has begun
USDA Regulated Still (a N/A, water samplel
Did samples onglyyAte In a quarantine tone within the United States'. CA, NY, or X Icheck maps)]
ny.. Title
Did samples originate from a foreign source i nternationa0y,
nrludine Hawaii and Puerto Riml? 17IYes I "{Na
Document Name: Document Revised August 4, 7017
Simple Condition Up.Recel tiSCURI Pae 1 of 7
Document No.: Issuing Authority:
t CBAnaiyUCdl
. es
F-CAR-CS-033-Rev.04 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Ralelgh❑ Mechanicsville[]
• `lien` Name:
me: ^` i�G�� Projecta:I WN 92361385
L C TV1 U �bfi Q� �:JILh II'III IIIII�I'IIIIIIII
Courier: ❑Fed Ea ❑UPS ❑USPS ❑Client
❑ Commercial [')Pace []Other:_ 92361386
t
Custody Seal Present? ❑Yes NO Seals Intact?
rryX/
Packing Material: ❑Bubble Wrap LJBubble Bags
Thermomet `
IR Gun ID: �tqU1 Ty7f
Correction Factor: Cooler Temp Corrected PC):.
Dyes Oo
Date/Initial; Person Examining Contents: 1
❑None❑ Other Biological Tissue Fr ran?
[]Yes ❑No N/A
wet ❑Blue ❑none
Temp should be above freezing to 6'C
❑Samples out of temp criteria Samples on ice. coding process
has begun
USDA Regulated Still (a N/A, water samplel
Did samples onglyyAte In a quarantine tone within the United States'. CA, NY, or X Icheck maps)]
ny.. Title
Did samples originate from a foreign source i nternationa0y,
nrludine Hawaii and Puerto Riml? 17IYes I "{Na
CLIENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
Lot IO of split containers'
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? IJYes LJNO
Date/Time:
Date:
Date:
Note: Whenever there Is a discrepancy affecting North Caruana compliance samples, a copy or this form will be sent to the North Carolina OEHNR Certification Office (i e
Out of hold, mcorrect preservative, out of temp, Incorrect conialnersl
Page 18 of 23
Comments/Discrepancy:
Chain of Custody Present?
. es
ONO
N/A
1.
Samples Arrived within Hold Time?res
ONO
N/A
7.
Short Hold Time Analysis 1<72 hr.j?
Dyes
N
N/A
3.
Rush Tum Around Time Requested?
]ym
Na
N/A
4.
Sufficient Volume?
-( /Y
ONO
❑N/A
5
Correct Containers Used?
-Pace Containers Used?
61
Yes
ONO
ONO
❑N/A
ON/A
6.
Containers intact?
Yes
NoN
A
7.
Dissolved analysis: Samples Field Filtered?
Yes
No
N/A
a.
Sample Labels Match COC?
Includes Date/Time/ID/Analysis Matrix:
es
ONO
❑N/A
9.
Heads ace in VOA Vials b5 6mm17
Dyes
dNQ
ONJA
10.
Trip Blank Present?
Trip Blank Custody Seals Present]
Dyes
yrs
o
No
❑N/
n/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
Lot IO of split containers'
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? IJYes LJNO
Date/Time:
Date:
Date:
Note: Whenever there Is a discrepancy affecting North Caruana compliance samples, a copy or this form will be sent to the North Carolina OEHNR Certification Office (i e
Out of hold, mcorrect preservative, out of temp, Incorrect conialnersl
Page 18 of 23

m
O
0
3
r
0
0
as
O
N
3
Cr
Cr
O
n
N
O
3
P
O
ncme
a
O
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9►4U-125 mL Plastic Unpresemed (N/A) (Cl.)
r
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SPZU-500 mL Plastic Unpreserved (N/A)
A
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BP4S-12S mL Plastic H2SO4 IpH <2) (Cl
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O
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O
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T�
A
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AG1U-1 liter Amber UAPresemed IN/A) (CI-)
zzzzAGIN-]
iR
n
+
N
c
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AG3U-2SO ml Amber Unptesemed (N/A) ICH
L
N
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AG3S-1 liter Amber H2SO4 (pH < 2)
p
c
AUS -250 ml Amber H2SW (pH < 21
n =
^o 'n
v
c
AG3AIMMI.250 mL Amber NHACI (N/A)(Cf)
e
m
O
0
3
r
0
0
as
O
N
3
Cr
Cr
O
n
N
O
P
ncme
9►4U-125 mL Plastic Unpresemed (N/A) (Cl.)
BP3U-2SO mL Plastic Unpresemeci (N/A)
SPZU-500 mL Plastic Unpreserved (N/A)
9PIU I iter Plastic Unpreterved (N/A)
BP4S-12S mL Plastic H2SO4 IpH <2) (Cl
)IM -250 mL plastic HNO3 (pH <2)
BP4Z-125 ml. Plastic 2N Acelate & NaOH 1>91
BPeC-12S mi. Plastic NaOH (pH > 12) (0-1
WGPU-Wide-mouthed Glass far Unpresened
T�
AG1U-1 liter Amber UAPresemed IN/A) (CI-)
zzzzAGIN-]
liter Amber HCI IPH < 21
AG3U-2SO ml Amber Unptesemed (N/A) ICH
AG3S-1 liter Amber H2SO4 (pH < 2)
AUS -250 ml Amber H2SW (pH < 21
AG3AIMMI.250 mL Amber NHACI (N/A)(Cf)
DG9H40 mt VOA I ICI (N/A1
VG9T40 mL VOA Na2S2O3 (N/A)
VG9U<O mL VOA Unp IN/A)
(�
OG910-a0 mL VOA 143PO4 IN/A)
VOAK (9 vols per k 1)5035 kit IN/A)
V/GK 13 vials per ki*VPH/W s kA (N/A)
SPST-12S mL Stenle Plastic (N/A - lab)
SP23.250 mL Sterne Plastic (N/A -lab)
BPM -250 mL Plastic (NH2)25D4 (9.3-9 71
Cubdainer
USGU-20 ml Scintillation vials (N/A)
GN
m
O
0
3
r
0
0
as
O
N
3
Cr
Cr
O
n
N

G CHAIN -OF -CUSTODY I Analytical Request Document
PaeeAnalytieal TIIe Chain- CuVady Is a LEGAL DOCUMENT All relevant fieltls must be enmpleled accurately
..patrol. Wm
Section A Section ISSedbeC pa / W / m
Required Clmnl htlwr�wm Required Pr,.t i�.,m.enai �" a
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DATE
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SAMPLE CONDITIONS
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Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 11/02/2017
Reported: 11/08/2017
For: 92361385
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
171102-17-01 MBAS 001 <0.1 mg/L sMSWC-2000 11/03/2017 MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/34697
Page 1 gage 21 of 23

Condition of Receipt
Sample Number 171102-17-01 Temp on Arrival: 3
Parameter Schedule: MBAS
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 Q, 22 of 23

Chain of Custody
Wo. hurdor 9235'395
W rrhnrcler N,mic Pei^ut Renewal 001
Wcti ull� R,apn�s Lrtl By 'r1 S �„
Pace Analytical•
Row I toys e• To {ubeplYaCI TO _
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A�gi,1a Baur.
Pace Analytical Cha0one J"{LA-4tSUIt IL_E PO
9800 'St Ave 8OIL
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Munnr5v4le Nf..B07B OlS
078Soth, 100 �l
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phone 170418 %59092 -1 /' 1
Email ar 3eW Deroni@pacelabs com 122- Z 1. r'uV --
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State or Sample On In NC Fel j •r••wwa C&IMM •
Militia!LAS
USE ONLY
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11ceAnaly &O
ssw.psalebauonl
November 15. 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: Permit Renewal 002
Pace Project No.: 92361389
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a,qq.
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

1 -Pace Analytical
www paterabs. tom
Project: Permit Renewal 002
Pace Project No.: 92361389
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)8769092
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

Pace Analytical Services, LLC
aca mlytical 9800 ncey Ave. Suite100
Hunlersville, NC 28078
'✓�"^ [phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.
Permit Renewal 002
92361389
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92361389001
002
EPA 200.7
SHi
7
PASI-A
EPA 624
GAW
35
PASI-C
SM 2540D
SLB
1
PASI-A
SM 52108
KMM
1
PASI-A
EPA 350.1 1993 Rev 2.0
BRJ
1
PASI-A
SM 5220D
SLB
1
PASI-A
SM 53108
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not oe reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

1 !f'dceAn Vital o
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
ND
ug/L
5.0
1
11/03/17 02:45
107-02-8
Acrylonitrile
Sample: 002
Lab ID: 92361389001
Collected: 11/01/1707:55
Received: 11/01/1709:00 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND
ug/L
Aluminum
NO
ug/L
100
1
11/14/1712:35
11/15/1712:26
7429-90-5
Arsenic
NO
ug/L
10.0
1
11/14/17 12:35
11/15/17 12:26
7440-38-2
Boron
33700
ug/L
500
10
11/14/17 12:35
11/15/17 14:10
7440-42-8 M6
Chromium
NO
ug/L
5.0
1
11/14/1712:35
11/15/1712:26
7440-47-3
Iron
1370
ug/L
50.0
1
11/14/17 12:35
11/15/17 12:26
7439-89-6
Magnesium
6680
ug/L
100
1
11114/1712:35
11/15/1712:26
7439-95-4
Silver
NO
ug/L
5.0
1
11/14/1712:35
11/15/1712:26
7440-22-4
624 Volatile Organics Analytical Method: EPA 624
Acrolein
ND
ug/L
5.0
1
11/03/17 02:45
107-02-8
Acrylonitrile
NO
ug/L
50.0
1
11/03/1702:45
107-13-1
Benzene
ND
ug/L
2.0
1
11/03/17 02:45
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
11/03/1702:45
75-27-0
Bromoform
ND
ug/L
2.0
1
11/03/1702:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/03/1702:45
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
11/03/17 02:45
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
11/03/1702:45
108-90-7
:hloroethane
ND
ug/L
2.0
1
11/03/1702:45
75-00-3
t-Chloroethylvinyl ether
ND
ug/L
5.0
1
11/03/17 02:45
110-75-8 c2
;hlomform
ND
ug/L
2.0
1
11/03/1702:45
67-66-3
Chloromethane
ND
ug/L
2.0
1
11/03/1702:45
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
11/0311702:45
124-48-1
Dichlorodifluoromethane
NO
ug/L
2.0
1
11/03/17 02:45
75-71-8
1,1-Dichloroethane
NO
ug/L
2.0
1
11/03/1702:45
75-34-3
1,2-Dichlorcethane
NO
ug/L
2.0
1
11/03/1702:45
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
11/03/17 02:45
75-35-0
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
11/03/1702:45
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
11/03/17 02:45
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
11/03/17 02:45
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:45
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:45
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
11/03/17 02:45
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
11/03/17 02:45
75-09-2
1,1,2,2 -Tetrachloroethane
ND
ug/L
2.0
1
11/03/1702:45
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
11/03/17 02:45
127-18-4
Toluene
NO
ug/L
2.0
1
11/03/1702:45
108-88-3
1,1,1 -Trichloroethane
ND
ug/L
2.0
1
11/03/1702:45
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
2.0
1
11/03/17 02:45
79-00-5
Trichloroethene
ND
ug/L
2.0
1
11/03117 02:45
7901-6
Trichlorofluoromethane
NO
ug/L
2.0
1
11/0311702:45
75-69-0
Vinyl chloride
NO
ug/L
2.0
1
11/03/1702:45
75-01-4
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
11/03/17 02:45
460-00-4
Toluene-d8(S)
101
%
70-130
1
11/03/1702:45
2037-26-5
1,2-Dichlorcethane-d4(S)
101
%
70-130
1
11/03/1702:45
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20

162ceAnaVical e
wewPW#18W cmn
ANALYTICAL RESULTS
Pau Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Permit Renewal 002
Pace Project No.: 92361389
Sample: 002
Lab ID: 92361389001 Collected: 11/01/1707:55
Received: 11/01/1709:00 Matrlx:Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
2.5
1
11/02/17 08:29
52108 BOD, 5 day
Analytical Method: SM 5210B
BOD, 5day
ND mg/L
2.0
1
11/02/1702:41 11/06/1721:19 B2,1_2
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
0.27 mg/L
0.10
1
11/09/17 01:16 7664-41-7
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L
25.0
1
11/13117 19:02 L2
53108 TOC
Analytical Method: SM 53108
Total Organic Carbon
2.1 mg/L
1.0
1
11/02/17 19:25 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

1 !2ceAnaViC8l e
wewpaMtlaoom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 386674
Analysis Method:
EPA200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92361389001
METHOD BLANK: 2144442
Matrix: Water
Associated Lab Samples: 92361389001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aluminum
ug/L
NO
100
11/15/17 12:20
Arsenic
ug/L
NO
10.0
11/15/1712:20
Boron
ug/L
NO
50.0
11/15/17 14:04
Chromium
ug/L
NO
5.0
11/15/1712:20
Iron
ug/L
NO
50.0
11/15/1712:20
Magnesium
ug/L
NO
100
11/15/1712:20
Silver
ug/L
NO
5.0
11/15/1712:20
LABORATORY CONTROL SAMPLE:
2144443
Spike
LCS
LCS e/ Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Aluminum
uglL
5000
4830
97
85-115
Arsenic
ug/L
500
485
97
85-115
Boron
ug/L
500
486
97
85115
Chromium
ug/L
500
480
96
85-115
Iron
ug/L
5000
4750
95
85-115
Magnesium
ug/L
5000
4790
96
85-115
Silver
ug/L
250
245
98
85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2144444
2144445
MS
MSD
92361389001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Aluminum
ug/L
NO
5000
5000
4920
4970
98 99
70-130
1
Arsenic
ug/L
NO
500
500
493
492
99 98
70-130
0
Boron
ug/L
33700
500
500
36700
36600
608 584
70-130
0 M6
Chromium
ug/L
NO
500
500
490
495
98 99
70.130
1
Iron
ug/L
1370
5000
5000
6240
6250
97 98
70-130
0
Magnesium
ug/L
6680
5000
5000
11800
11800
103 103
70-130
0
Silver
ug/L
NO
250
250
247
252
99 100
70-130
2
Results presented on this page are in the unite Indicated by the'UrW column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

aceAnalytical
awwpecial com
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 385093 Analysis Method: EPA624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92361389001
METHOD BLANK: 2134818
Associated Lab Samples: 92361389001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1 -Trichloroethane
ug/L
NO
2.0
11/02/1717:58
1,1,2,2 -Tetrachloroethane
ug/L
NO
2.0
11/02/1717:58
1,1,2 -Trichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,1-Dichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,1-Dichlorcethene
ug/L
NO
2.0
11/02/1717:58
1,2-Dichloroethane
ug/L
NO
2.0
11/02/1717:58
1,2-Dichloropropane
ug/L
NO
2.0
11/02/1717:58
2-Chloroethylvinyl ether
ug/L
NO
5.0
11/02/1717:58
Acrolein
ug/L
NO
5.0
11/02/1717:58
Acrylonitrile
ug/L
NO
50.0
11/02/1717:58
Benzene
ug/L
NO
2.0
11/02/1717:58
Bromodichloromethane
ug/L
NO
2.0
11/02/1717:58
Bromoform
ug/L
NO
2.0
11/02/1717:58
Bromomethane
ug/L
NO
2.0
11/02/1717:58
Carbon tetrachloride
ug/L
NO
2.0
11/02/17 17:58
Chlorobenzene
ug/L
ND
2.0
11/02/1717:58
Chloroethane
ug/L
NO
2.0
11/02/17 17:58
Chloroform
ug/L
NO
2.0
11/02/1717:58
Chloromethane
ug/L
NO
2.0
11/02/1717:58
cis-1,2-Dichloroethene
ug/L
NO
2.0
11/02/1717:58
cis-1,3-Dichloropropene
ug/L
NO
2.0
11/02/1717:58
Dibromochloromethane
ug/L
NO
2.0
11/02/1717:58
Dichlorodifluoromethane
ug/L
NO
2.0
11/02/1717:58
Ethylbenzene
ug/L
NO
2.0
11/02/17 17:58
Methylene Chloride
ug/L
NO
2.0
11/02/1717:58
Tetrachloroethene
ug/L
NO
2.0
11/02/17 17:58
Toluene
ug/L
NO
2.0
11/02/17 17:58
trans-1,2-Dichloroethene
ug/L
NO
2.0
11/02/17 17:58
trans-1,3-Dichloropropene
ug/L
NO
2.0
11/02/1717:58
Trichloroethene
ug/L
ND
2.0
11/02/17 17:58
Trichlorofluoromethane
ug/L
NO
2.0
11/02/1717:58
Vinyl chloride
ug/L
ND
2.0
11/02/1717:58
1,2-Dichloroethane-d4 (S)
%
97
70-130
11/02/17 17:58
4-Bromofluorobenzene (S)
%
100
70-130
11/02/17 17:58
Toluene -d8 (S)
%
104
70-130
11/02/1717:58
Qualifiers
Pace Anatyllcal Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2134819
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rae Limits Qualifiers
11,1 -Trichloroethane ug/L 20 18.2 91 52-162
Results presentee on M4 pope an in Me units Indicated by the "Units" column except where an alternate unit is presented to the right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20

ceAnaVical e
aaa Psestabemn
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
LABORATORY CONTROL SAMPLE:
Parameter
2134819
Units
Spike
Conc.
1 -CS
Result
LCS
%Rec
%Rec
Limits
1,1,2,2 -Tetrachloroethane
ug/L
20
17.1
86
46.157
1,1,2 -Trichloroethane
ug/L
20
18.6
93
52-150
1,1-Dichloroethane
ug/L
20
17.5
87
59.155
1,1-Dichloroethene
ug/L
20
19.2
96
1-234
1,2-Dichloroethane
ug/L
20
18.2
91
49-155
1,2-Dichloropropane
ug/L
20
19.3
97
1-210
2-Chloroethylvinyl ether
ug/L
40
29.8
75
1-305
Acrolein
ug/L
100
130
130
15-152
Acrylonitrile
ug/L
100
89.0
89
75-132
Benzene
ug/L
20
18.5
93
37-151
Bromodichloromethane
ug/L
20
18.4
92
35-155
Bromoform
ug/L
20
16.3
81
45-169
Bromomethane
ug/L
20
20.1
100
1-242
Carbon tetrachloride
ug/L
20
18.5
93
70-140
Chlorobenzene
ug/L
20
18.1
91
37-160
Chloroethane
ug/L
20
18.9
94
14-230
Chloroform
ug/L
20
17.8
89
51-138
Chloromethane
ug/L
20
17.3
87
1-273
cis-12-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
19.2
96
1-227
Dibromochloromethane
ug/L
20
16.8
84
53-149
Dichlorodifluoromethane
ug/L
20
16.2
81
70-130
Ethylbenzene
ug/L
20
17.5
88
37-162
Methylene Chloride
ug/L
20
21.6
108
1-221
Tetrachloroethene
ug/L
20
18.8
94
64148
Toluene
ug/L
20
18.5
92
47-150
trans-1,2-Dichloroethene
ug/L
20
18.3
92
54-156
trans-1,3-Dichloropropene
ug/L
20
18.9
94
17-183
Trichloroethene
ug/L
20
19.6
98
71-157
Trichlorofluoromethane
ug/L
20
17.9
90
17-181
Vinyl chloride
ug/L
20
18.2
91
1-251
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8(S)
%
104
70-130
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
Parameter
2134821
Units
92361205001
Result
Spike
Colic.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1 -Trichloroethane
ug/L
NO
20
20.9
105
46-171
1,1,2,2 -Tetrachloroethane
ug/L
NO
20
18.2
91
73-159
1,1,2 -Trichloroethane
ug/L
NO
20
20.0
100
64152
1,1-Dichloroethane
ug/L
NO
20
20.1
100
43-172
1,1-Dichloroethene
ug/L
NO
20
22.1
111
48-189
1,2-Dichloroethane
uglL
NO
20
20.4
102
42-171
1,2-Dichloropropane
ug/L
NO
20
21.6
108
55-157
Results presented on this page are in the units indicated by the'Units' column except where an alternate unit is presented to an right of re.ua.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20

/ f ZeAnalyfical*
xww.Wroleba.00m
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kinsey Ave. Suge 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
MATRIX SPIKE SAMPLE:
2134821
92361205001
Spike
MS
MS
% Ree
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
2-Chloroethylvinyl ether
ug/L
NO
40
NO
0
70-130 M1,c2
Acrolein
ug/L
NO
100
138
138
70-130 M1
Acrylonitrile
ug/L
NO
100
101
101
70-130
Benzene
ug/L
NO
20
20.3
101
54163
Bromodichloromethane
ug/L
NO
20
19.8
99
56-152
Bromofonn
ug/L
NO
20
17.1
85
53-151
Bromomethane
ug/L
NO
20
16.8
84
10-200
Carbon tetrachloride
ug/L
NO
20
20.1
101
41-175
Chlorobenzene
ug/L
NO
20
20.7
103
67-152
Chloroethane
ug/L
NO
20
22.8
114
23-200
Chloroform
ug/L
NO
20
18.4
92
51-166
Chloromethane
ug/L
NO
20
17.0
85
40-175
cis-1,2-Dichloroethene
ug/L
NO
20
21.2
106
45-174
cis-1,3-Dichloropropene
ug/L
NO
20
19.9
100
38-146
Dibromochloromethane
ug/L
NO
20
18.8
94
65-144
Dichlorodifluoromethane
ug/L
NO
20
18.5
92
70-130
Ethylbenzene
ug/L
NO
20
19.8
99
57-152
Methylene Chloride
ug/L
NO
20
20.0
100
40-167
Tetrachloroethene
ug/L
NO
20
21.0
105
59-155
Toluene
ug/L
NO
20
20.6
103
47-162
trans-1,2-Dichloroethene
ug/L
NO
20
21.1
106
47-178
trans-1,3-Dichloropropene
ug/L
NO
20
19.4
97
39-148
Trichloroethene
ug/L
NO
20
21.7
109
60-153
Trichlorofluoromethane
ug/L
NO
20
21.3
107
42-199
Vinyl chloride
ug/L
NO
20
21.2
106
46-176
1,2-Dichloroethaned4 (S)
e/
101
70-130
4-Bromofluorobenzene (S)
a/
96
70-130
Toluene -d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1 -Trichloroethane
uglL
NO
NO
1,1,2,2 -Tetrachloroethane
ug/L
NO
NO
1,1,2 -Trichloroethane
ug/L
NO
NO
1,1-Dichloroethane
ug/L
NO
NO
1,1-Dichloroethene
uglL
NO
NO
1,2-Dichloroethane
uglL
NO
NO
1,2-Dichloropropane
ug/L
NO
NO
2-Chloroethylvinyl ether
ug/L
NO
NO
Acrolem
ug/L
NO
NO
Acrylonitrile
ug/L
NO
NO
Benzene
ug/L
NO
NO
Bromodichloromethane
ug/L
NO
NO
Bromoform
ug/L
NO
NO
Results Presented on this page are In Me units indicated by the'Unitc' column except when an altemate unit is presented to In. right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20

25ceAnayicale
wswpecelabs.com
QUALITY CONTROL DATA
Project. Permit Renewal 002
Pace Project No.: 92361389
SAMPLE DUPLICATE: 2134820
Parameter
Units
92361204001
Result
Dup
Result
Bromomethane
ug/L
NO
NO
Carbon tetrachloride
ug/L
NO
NO
Chlorobenzene
ug/L
NO
NO
Chloroethane
ug/L
NO
NO
Chloroform
ug/L
NO
NO
Chloromethane
ug/L
NO
NO
cis-1,2-Dichloroethene
ug/L
NO
NO
cis-1,3-Dichloropropene
ug/L
NO
NO
Dibromochloromethane
ug/L
NO
NO
Dichlorodifluoromethane
ug/L
NO
NO
Ethylbenzene
ug/L
NO
NO
Methylene Chloride
ug/L
NO
NO
Tetrachloroethene
ug/L
NO
NO
Toluene
ug/L
NO
NO
trans-1,2-Dichloroethene
ug/L
NO
NO
trans-1,3-Dichloropropene
ug/L
NO
NO
Trichloroethene
ug/L
NO
NO
Trichlorofluoromethane
ug/L
ND
NO
Vinyl chloride
ug/L
NO
ND
1,2-Dichloroethane-d4 (S)
%
100
102
4-Bromofluorobenzene (S)
%
100
97
Toluene -d8 (S)
%
106
102
RPD Qualifiers
2
3
4
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presenteci on this page are in Me unite Indicated by Me "Unita" column except where an altemate unit Is presentee to the right of Me meet.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20

/ 2ace Analytical a
saew7arelNN,.
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 384949 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92361389001
METHOD BLANK 2133904 Matdx: Water
Associated Lab Samples: 92361389001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 11/02/1708:25
Pace Analytical Servicas, LLC
9800 Kincey Ave. Suds,100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2133905
Spike LCS LCS % Rec
Parameter Units Corl Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 228 91 90-110
SAMPLE DUPLICATE: 2133906
92361383001 Cup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND NO
SAMPLE DUPLICATE: 2133907
92361391003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND NO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Face Analytical Services, LLC. Page 11 of 20

// /-PaceftVica/a
aww.panabt.com
Project: Permit Renewal 002
Pace Project No.: 92361389
OC Batch: 384933
OC Batch Method: SM 52108
Associated Lab Samples: 92361389001
METHOD BLANK: 2133872
Associated Lab Samples: 92361389001
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 52108
Analysis Description: 52108 BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 2.0 11/06/1720:53
Pace Analytical Services, LLC
9800 Kincey Ave. Sults 100
Hunlersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2133873
Spike LCS LCS % Red;
Parameter Units Conic. Result % Roo Limits Qualifiers
BOD, 5 day mg/L 198 154 78 84.6-115.4 L2
SAMPLE DUPLICATE: 2133874
92361437001 Dup
Parameter Units Result Result RPD Qualifiers
HOD, 5 day mg/L ND ND D6
Results presented on this page are In the units Indicated by the 'UMW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 20

1!2ceAnaoical a
0 N pacelabs com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 385507
Analysis Method: EPA 350.1 1993 Rev 2.0
QC Batch Method: EPA 350.1 1993 Rev 2.0
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92361389001
METHOD BLANK: 2137940
Matrix: Water
Associated Lab Samples: 92361389001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/L
ND 0.10
11/09/17 00:36
LABORATORY CONTROL SAMPLE: 2137941
Spike
LCS
LCS %Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Nitrogen, Ammonia mg/L
5
5.1
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137942
2137943
MS
MSD
92361633002
Spike
Spike MS
MSD MS
MSD
°% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Ammonia mg/L 4.8
5
5 9.6
9.6 97
97
90-110
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137944
2137945
MS
MSD
92362056001
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Ammonia mg/L NO
5
5 4.9
4.9 98
98
90-110
0
Results presented on this page are in the units indicated by the -Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, I.I.C.
Page 13 of 20

/ 21!eAnalytical a
srwpacelaes.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntemville, NC 28078
[phone]
Project:
Permit Renewal 002
Pace Project No.:
92361389
QC Batch:
386547 Analysis Method: SM 5220D
QC Batch Method:
SM 5220D Analysis Descripfiow 5220D COD
Associated Lab Samples: 92361389001
METHOD BLANK: 2143913
Associated Lab Samples: 92361389001
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 11/13/1719:02
LABORATORY CONTROL SAMPLE: 2143914
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 1120 751 67 90-110 L2
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143915 2143916
MS MSD
92360409001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 803 150 150 900 907 65 69 90-110 1 MO
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2143917 2143918
MS MSD
92361431002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 27.0 150 150 145 141 79 76 90-110 3 MO
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 20

ZeAnapical'
swww.penlabscom
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 384971
QC Batch Method: SM 53108
Associated Lab Samples: 92361389001
METHOD BLANK: 2133960
Associated Lab Samples: 92361389001
Parameter Units
Total Organic Carbon mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5310B
Analysis Description: 53108 TOC
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 1.0 11/02/1716:28
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
LABORATORY CONTROL SAMPLE: 2133961
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carlon mg/L 25 23.6 94 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2133962
2133963
MS
MSD
92361364001 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec
% Rec Limits RPD Qual
Total Organic Carbon mg/L 9.5 25
25
32.4
32.3 91
91 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 20

2IA-PaceAnalytical e
www0acelabtoam
QUALIFIERS
Project: Permit Renewal 002
Pace Project No. 92361389
DEFINITIONS
Pace Analytical Services, LLC
9800 Kinoey Ave. Suke 100
Huntereville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
82 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20

2cekwcalo
~Paoall
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pau Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Permit Renewal 002
92361389
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92361389001
002
EPA 200.7
386674
EPA 200.7
386787
92361389001
002
EPA624
385093
92361389001
002
SM 2540D
384949
92361389001
002
SM 5210B
384933
SM 52108
384937
92361389001
002
EPA 350.1 1993 Rev 2.0
385507
92361389001
002
SM 5220D
386547
92361389001
002
SM 53108
384971
Date: 11/15/2017 07:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 20

Laboratory receiving samples:
Asheville L] Eden Greenwood 0 Huntersville Raleigli Mechanicsville[;
Courier
❑ Commercial
Client Name: WO# • 92361389
L—:1for, (,,tics, %1n yF P+�Y�,.r Project #: III IIIIIIIIvlllllllllll
L]Eod Ea ❑UPS ❑USPS []Client
Pace ❑Other
92381389
i L
Custody Seal Present?
Document Name. Document Revised August d, 7017
❑Nio
Sample Condluon Upon Recei t(SCUR) Page 1 of 2
No Issuing Authority
' c7Ce AnNyftealDocument
Lf Other Biological Tissue Fr all
G-CARS-033-Rev.OA Pace Quality Office
—
Laboratory receiving samples:
Asheville L] Eden Greenwood 0 Huntersville Raleigli Mechanicsville[;
Courier
❑ Commercial
Client Name: WO# • 92361389
L—:1for, (,,tics, %1n yF P+�Y�,.r Project #: III IIIIIIIIvlllllllllll
L]Eod Ea ❑UPS ❑USPS []Client
Pace ❑Other
92381389
i L
Custody Seal Present?
❑Yes []NO Seals Intact? []yes
❑Nio
Date/Initials Person Examining Contents '. I)3 ILIL
Packing Material:
❑bubble Wrap []Bubble Bags ❑None
Lf Other Biological Tissue Fr all
Thermometer
RGun 1O
wit
Type
Cave
❑Sone ❑yes LINO N/A
Short Hold Time Analysis c72 hr.7
o�lS1[e:
2.
L9No
❑N/A
Correction Factor:
Cooler Temp Corrected j'C):
r/es
Temp should be above freezing to 6'C
N/A
A.
Sufficient Volume?
❑Sampler out of remp,ter., Samples ar qe, Cooling process
ONO
❑N/A
5.
has betun
USDA Regulated Soils ❑ N/A, water samples
ONO
ONO
ON/A
N/A
Did samples originate in a quarantine tone within the United States CA, NY, or SC (cmeck
maps)?
Did samples Originate from a foreign source (internationally,
❑Yes ❑No
N/
7.
includine Hawaii and Puerto Rica Pny'es nNo
CLIENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
tot iD of split containers
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes ❑No
Date/Time:
Date
Date: is �
NoteWhenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form ii be sem to the North Carolina Df HNR Certification Office (i e
Out of hold, incorrect preservative, out of temp, mco[rect contalners)
Page 18 of 20
Commanta/Dhaepancy:
1.
Chain of Custody Present/ MYeI, ONO N/A
Samples Arrived within Hold Time?
res
O�-,�No
N/A
2,
Short Hold Time Analysis c72 hr.7
res
L9No
❑N/A
3.
Rush Turn Around Time Requested?
r/es
No
N/A
A.
Sufficient Volume?
k
L2y t
ONO
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Y
res
ONO
ONO
ON/A
N/A
6.
Containers Intact?ret
No
N/
7.
Dissolved analysis: Samples Field Filtered?
r
Nn
N/A
a.
Sample labels Match COO
Includes Date/Time/10/Analysis Matrix:
Yes
w
ON.
❑N/A
9.
Head space in VOA Vials(>5-6mmj?
El yes
EJNPI
ON/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
res
NO
ho
❑N/
N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
tot iD of split containers
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes ❑No
Date/Time:
Date
Date: is �
NoteWhenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form ii be sem to the North Carolina Df HNR Certification Office (i e
Out of hold, incorrect preservative, out of temp, mco[rect contalners)
Page 18 of 20

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9P2U-SOO mL Plastic Unpresened (N/AI
a►tU-1 icier Plkstc Unprese iced (Il
V6 -12S ml Plastic I,l ION. 21 (CO
SP3111a-250 ml plastic HNO3 (PH c 2)
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AGIU-1 liter Amber Unpreferved IN/A) (CI-)
AGIN-1 bier Amber HCI (pH. 2)
AG341-250 ml Amber Unprese,"d INN (a)
AGISI liter Amber H25O4 lost <2)
AGJS-250 mL Amber HISOA (pH <2)
AG3AIOG3A)-250 mL Amber NIMCI (N/A)(Clk)
V_
DG9H-a0 mL VOA IICI(N/Al
VGITA0 ml VOA MZS203 (N/A)
VGW40 mL VOA Uro IN/AI
tt ``
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DGIP-40 mL VOA 143PO4 IN/A)
VOM (e trial, per kill -5035 kit (N/AI
V/Ga 13 trials No Wd VPH/Gas kit IN/A)
3PST V5 mL Slarve Platt. (N/A -bb)
SPIT -250 mL Sterile Pil lK (N/A -lob)
N3A-750 ml Plastic INH2)2500 (9 3-9 7)
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Cubit kw
VSGU 20 ml Scintillation V wls 1N/A)
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CHAIN -OF -CUSTODY I Analytical Request Document
PaeeAnalytical Tile CNalnof-Cusbdy Is a LEGAL DOCUMENT All nPevant Gents must De mmpleted accuralcly
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Section A Section B Section C
RRCyyOuhayd C111!Inlpmalion RMINrad Pm,11 In:ornu!. Inv,. Intmnal,M
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SIGNATURE W SgYPLFA: /y G!
DATE Si —
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'Y^1xarL�1 .'rnl Rn X.myes.v,'.6.yMIP.xv'. NL11p 61y P'rPrmm kYnrs Yd agex/gm Nm cR Te:d 15`: pn mmNln.H•y Nrm.wnx, )n M1r.s F -ALL -0-020r LT. 15-M2

,2ceAna0ca1a
awwpKaltlta0m
November 22, 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: CTAS Resample - Permit Renewal
Pace Project No.: 92362439
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvills, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
axq£Q, 4Y1- `$cuam
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seroces, LLC.
Page 1 of 6

Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville[]' Raleigh❑ Mechanicsville❑
Client Name: WO# : 92362439
_
Projects
ps 111111IIIIIIII
Courier: ❑fed Ex UPS USPSSPS ❑Client
❑ Commercial �e ❑OtnerIIIIIIII
— 92362439
Custody Seal Present? ❑Yes Jam° Seals intact? []Yes ..❑No
Date/InnlaK Person Examining Contents:
Packing Material: []Bubble Wrap ❑Bubble Bags IDNdne ❑ Other Biological Tissue Frozen?
Thermometer: I ❑Yes_-qN0 []N/A
❑ lit Gun ID: I I l o I Type of lea: Wet ❑91ue []None
Correction Factor: Cooler Temp Corrected ('Cj: Temp should be above freezing to 6Y
❑Samples out of temp Cniena Samples on ice, cooling process
hasbelun
USDA Regulated Soil N/A, water sample)
Did samples origin a in a quarantine zone within the United States U, NY, or SC (check mapsi7 Did samples originate from a foreign source (internationally,
MYes n. � mtludlne Hawaii and Puerto RICOI? ayes Died
Document Name:
Document Revised: August a, 2017
comments/Oisne anry:
Chain of Custody Present?
V
Sample Condition Upon Recei t(SCUR)
Pae 1 or 2
1.
Document No.:
Issuing Authority:
Dive
' aCeAnalybcal
2,
Short Hold Time Analysis 1<72 hr.)?
Yes
f-CAR-CS-033-Rev.04
Pace Quality Office
3.
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville[]' Raleigh❑ Mechanicsville❑
Client Name: WO# : 92362439
_
Projects
ps 111111IIIIIIII
Courier: ❑fed Ex UPS USPSSPS ❑Client
❑ Commercial �e ❑OtnerIIIIIIII
— 92362439
Custody Seal Present? ❑Yes Jam° Seals intact? []Yes ..❑No
Date/InnlaK Person Examining Contents:
Packing Material: []Bubble Wrap ❑Bubble Bags IDNdne ❑ Other Biological Tissue Frozen?
Thermometer: I ❑Yes_-qN0 []N/A
❑ lit Gun ID: I I l o I Type of lea: Wet ❑91ue []None
Correction Factor: Cooler Temp Corrected ('Cj: Temp should be above freezing to 6Y
❑Samples out of temp Cniena Samples on ice, cooling process
hasbelun
USDA Regulated Soil N/A, water sample)
Did samples origin a in a quarantine zone within the United States U, NY, or SC (check mapsi7 Did samples originate from a foreign source (internationally,
MYes n. � mtludlne Hawaii and Puerto RICOI? ayes Died
CUENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
Los 10 of split containers.
Project Manager SCURF Review:
Date/time:
Date:
Field Data Requlred? Utes UND
Project Manager SRF Review: Date:
Note whenever then is a discrepancy affecting North Carolina compliance Sampks, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (,.e.
Out of hold, riconect pn1ervattse, out or temp. mcorrect containers(
Page 2 of 6
comments/Oisne anry:
Chain of Custody Present?
V
rINO
nNJA
1.
Samples Arrived within Hold Time?Yes
Dive
N/A
2,
Short Hold Time Analysis 1<72 hr.)?
Yes
o
ON/A
3.
Rush Tum Around Time Requested?
res
o
N/A
4.
Sufficient Volume?
es
i]Np
N/A
5.
Correct Containers Used?
-Pace Containers Used?
es
es
❑NO
NO
❑N/A
ON/A
6.
Containers Intact?es
no
N A
7.
Dissolved analysis: Samples Field Filtered?
M A
B.
Sample Libels Match COC?
Includes Date/Tlme/ID/Anal is Matrix:
Elyes
❑No
❑N/A
9.
Heads ace In VOA Vials (a5-6mm)?
yes
No
lYl< 1
10.
Trip Blank Present?
Trip Blank Custody Seals Presents
[]Yes
r1yes
rImo
❑N/A
/A
Il.
CUENT NOTIFICATION/RESOLUTION
Person Contacted.
Comments/Sample Discrepancy:
Los 10 of split containers.
Project Manager SCURF Review:
Date/time:
Date:
Field Data Requlred? Utes UND
Project Manager SRF Review: Date:
Note whenever then is a discrepancy affecting North Carolina compliance Sampks, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (,.e.
Out of hold, riconect pn1ervattse, out or temp. mcorrect containers(
Page 2 of 6

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RESEARCh & /ANAlyTICAI
LAbORATORIES, INC@
For: Pace Analytical-Huntersville
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
Attn: Angela Baioni
Report of Analysis
11/21/2017
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Site: Pace -Huntersville Collection Date: 11/8/2017 8:00
Parameter Method Result Units Rep Limit Analyst Analysis Date/Tlme
CTAS SM5540D <0.4 mg/L 0.4 DW 11/9/2017 1530
NA = not onolyzeo
P.O. Boz 473 106 Short Street Kemersville, North Carolina 27264 Tel: [phone] Fax [phone] www randalabs corn Page t
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C....n of Custody
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