HomeMy WebLinkAboutNC0089729_Renewal Application_20171114Water Resources
ENVIRONMENTAL QUALITY
November 14, 2017
Douglas Pierotti, P G.
City of Charlotte
600 E 4th St
Charlotte, NC 28202
Subject: Permit Renewal
Application No. NCO089729
Myrtle/Morehead Storm Drainage Improvement
Mecklenburg County
Dear Applicant:
ROY COOPER
ri -srRor
XhCHAEL S- REGAN
Secretory
LSA. CULPEPPER
hderh" Dkedor
The Water Quality Permitting Section acknowledges receipt of your application for a new NPDES WW permit, including
supporting documentation and your check number 089125 in the amount of $860.00 as payment of the application fee.
These items were received in our offices on November 8, 2017. Your application will be assigned to a permit writer
within the Section's NPDES WW permitting branch. The permit writer will contact you if additional information is
required to complete evaluation of your application. Your timely and direct response to any such request will help to
expedite the review process. Please note that acceptance of the application does not guarantee a NPDES permit will be
issued for the proposed activity. A permit will only be issued following a complete review of the application, concluding
the proposed discharge is allowable per applicable statutes and rules.
Information regarding the status of your renewal application can be found online using the Department of
Environmental Quality's Environmental Application Tracker at:
https://dgg. nc.gov/permits-regulations/perm it -g uida nce/envi ronmental-a ppl ication-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
3f0i
Wren The ford
Administrative Assistant
Water Quality Permitting Section
cc: Central Files w/application
ec: WQPS Laserfiche File w/application
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919-807-6300
ENVIRONMENTAL • GEOTECHNICAL
BUILDING SCIENCES • MATERIALS TESTING
October 16, 2017
North Carolina Department of Environment Quality
Division of Water Quality
NPDES Permit Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
7606 Whitehall Executive Center Drive
Suite 800
Charlotte, NC 28273
Tel 704-529-3200
Fax 704-529-3272
www atcassociates corn
RE: Engineering Alternatives Analysis and NPDES Permit Application
Vicinity of Caldwell Street and South Boulevard
Myrtle/Morehead Storm Drainage Improvement
Charlotte, Mecklenburg County, North Carolina
ATC Project No. 199WO01701
Dear NPDES Permit Unit:
R CE1VED/fl1C,0pQ/DVVR
NOVO 2017
ftltwity
Pe-ffn n,q sectio¢
On behalf of the City of Charlotte, ATC Associates of North Carolina, P.C. (ATC) is
submitting three copies of the National Pollutant Discharge Elimination System (NPDES)
Permit Application for the discharge of treated groundwater at the above referenced project
site. Attached you will find the NPDES permit application short form C — GW and a check
for payment of the NPDES permit application fee, on behalf of the City.
In addition, ATC has evaluated the alternatives to surface water discharge, as required in the
case of any NPDES permit application, in accordance with the Engineering Alternatives
Analysis Guidance Document. If you have any questions or comments, please contact our
office at (704) 529-3200.
Sincerely,
ATC Associates of North Carolina, P.C.
Joseph G. Schold, PE
Principal Engineer
PC: Paul Smith, PE, Woolpert
Doug Pierotti, PG, City of Charlotte
David A. Hunter, PG
Principal Scientist
Charlotte -Mecklenburg
STORM600 E Fourth Street
`�T�T,�JE� Charlotte, NC 28202
��+t�� Fax 704 336 6586
Services
pco,Doq_10�9
October 25, 2017
NC Department of Environmental Quality
Division of Water Resources
Water Quality Permitting Section - NPDES
1617 Mail Sei vice Center
Raleigh, NC 27699-1617
Re: NPDES permit application (Short Form C -GW) - request to discharge into the
City of Charlotte municipal stormwater system from the Myrtle/Morehead Storm
Diainage Improvement Project in Charlotte, NC
Division of Water Resources:
Regarding the City of Charlotte's request in their NPDES permit application C -GW to
discharge treated water from a remediation system at the above -referenced location into
Charlotte's stormwater system, Charlotte Mecklenburg Storm Water Sei vices (CMSWS)
approves the discharge.
CMSWS would like to make the permittee and NC DEQ aware of the following
considerations and information:
CMSWS does not guarantee adequate capacity is available to permitted
dischargers to keep any property or street flee of water or harm as a result of this
discharge.
CMSWS takes no responsibility for backflows fi•om the public drainage system
into the permitted discharger's system.
CMSWS is aware of trichloroethylene (TCE) and perchloroethylene (PCE) levels
above Class C surface water human health standards in Little Sugar Creek (the
proposed receiving water) between E. 36th St. and N. Brevard St. in Charlotte,
NC. The contaminated area is located approximately 3.6 miles upstream from
where the remediation system discharge receiving tributary would enter Little
Sugar Creek. The source of surface water contamination is soil and groundwater
contamination at a vacant industrial property along Cullman Avenue. Kathleen
Lawson with the NC DEQ Hazardous Waste Section is managing the required
remediation in cooperation with the responsible party if you would like more
specific information.
CHARIOTTF.. To report pollution or drainage problems, call 311
http //stormwater charmeck org
NC Department of Environmental Quality
NPDES Permit Unit
October 25, 2017
If you have any questions, please contact Craig Miller at (704) 336-7605.
Sincerely,
c
4
Craig Miller
NPDES Program Supervisor
cc: David Hunter, PG, ATC Group Services LLC
Doug Pierotti, PG, City of Charlotte Environmental Services
2
Engineering Alternatives Analysis
and NPDES Permit Application
Myrtle/Morehead Storm Drainage Improvement
Charlotte, Mecklenburg County, North Carolina
ATC Project Number 199WOO1701
Engineering Alternatives Analysis and NPDES Permit Application
Myrtle/Morehead Storm Drainage Improvement
Charlotte, Mecklenburg County, North Carolina
ATC Project No. 199WOO1701
Prepared by:
David A. Hunter, F
Principal Scientist
.•`o4tN 0 ARU,
VA
4�
Andrew Deppensmith
Project Scientist
seph G. Schold, PE
NC Licensed Engineer6,
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Submitted to:
North Carolina Department of Environment and
Natural Resources
Division of Water Quality
NPDES Permit Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
On Behalf of:
The City of Charlotte
600 East Fourth Street
Charlotte, North Carolma 28202
Phone: (704) 336-3602
Fax: (704) 336-4554
Submitted by:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina 28273
Phone: (704) 529-3200
Fax: (704) 529-3272
October 16, 2017
TABLE OF CONTENTS
1.0 SITE INFORMATION...........................................................................................................1
1.1 Site Description.............................................................................................................1
1.2 Site Background............................................................................................................2
1.3 Dewatering Conditions and Flow Projections..............................................................3
2.0 ENGINEERING ALTERNATIVES ANALYSIS................................................................5
2.1 Connection to an Existing Wastewater Treatment System...........................................5
2.2 Land Application..........................................................................................................5
2.3 Infiltration Galleries......................................................................................................6
2.4 In -Situ Groundwater Remediation Wells......................................................................6
2.5 Closed -Loop Groundwater Remediation Wells............................................................7
3.0 PROPOSED GROUNDWATER TREATMENT SYSTEM...............................................9
4.0 DISCUSSION........................................................................................................................11
ATTACHMENTS
Figure 1 Site Location Map
Figure 2 Environmental Site Map
Figure 3 Treatment System Schematic
Table 1 Maximum Concentrations of Constituents
Appendix A NPDES Permit Application — Short Form C — GW
Appendix B Hart & Hickman Groundwater Monitoring Report — June 2017
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WO01701 October 16, 2017
1.0 SITE INFORMATION
1.1 Site Description
The remaining parts of the Myrtle/Morehead project for the City of Charlotte, Stormwater
Services, will include drainage improvements to the stormwater drain system to relieve flooding
in upper reaches of a tributary of Little Sugar Creek. The area that experiences flooding extends
along South Boulevard between Rensselaer Avenue and Templeton Avenue and extends to areas
east and southeast of that interval of South Boulevard. These areas encompass the proposed
storm drainage improvement construction area, generally between South Boulevard and Euclid
Avenue, and between Rensselaer Avenue and Templeton Avenue. Figure I indicates the project
location on part of a United States Geological Survey, topographic quadrangle map.
The project will entail trenching to depths below the expected water table elevation in
unconsolidated overburden soils beneath the water table along the proposed stormwater drain
alignments. Construction could also encounter bedrock and its included fractures that contain
groundwater. Dewatering will therefore likely be required during project construction. The
groundwater is proposed to be collected, treated, and discharged to stormwater drains which will
convey the flow to a Class C surface water.
Research of environmental conditions in the project vicinity and monitoring of groundwater
monitoring wells were performed by Hart and Hickman. McCorkle's Cleaners, a former
drycleaner, operated at 1437 South Boulevard. According to a Groundwater Monitoring Report
by Hart and Hickman in April 2016, chlorinated solvent impact was identified in the site
monitoring well network. Figure 2 depicts the extent of the chlorinated solvent impact
superimposed on the storm drain system and easements in the affected area. According to the
analytical data presented in the Groundwater Monitoring Report, potential exists for groundwater
to be impacted by drycleaning solvents in this area. Other downstream/downdrain locations with
anticipated improvements are through residential areas with low potential for groundwater
impact.
1 ATC Associates of North Carolina, P C.
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WOO1701 October 16, 2017
The NPDES Permit Application Form is provided as Appendix A, and the other attachments to
include a groundwater analytical table, a USGS topographic map, and a site map with
contaminant plume and discharge locations, and a proposed groundwater treatment system, as
requested by the permit application form.
1.2 Site Background
The former McCorkle's cleaners operation operated at 1437 South Boulevard, Charlotte, North
Carolina. The former drycleaner is monitored and regulated as part of the Dry -Cleaning Solvent
Cleanup Act (DSCA) Program. Figure 2 depicts the site on an aerial photograph, with pertinent
site features. Hart and Hickman conducted a groundwater monitoring event in March 2016.
Chlorinated solvent impact above North Carolina Groundwater and Surface Water Standards was
identified in the monitoring well network for multiple chlorinated solvent constituents. Potential
dewatering associated with the Myrtle/Morehead Storm Drainage Improvement project could
generate groundwater that includes tetrachloroethylene (PCE), trichloroethylene (TCE), and
vinyl chloride (VC) above North Carolina Class C Surface Water Quality Standards (North
Carolina Administrative Code, Title 15A, Subchapter 213; 2B Standards). A summary of
groundwater analytical data and other impact information is provided in the Hart and Hickman
Groundwater Monitoring Report in Appendix B.
Figure 2 in the attached appendix indicates the alignment of the drain construction, and
subsurface impact, principally by chlorinated solvents, which the drain construction is likely to
encounter. Table 1 in the attached appendix provides a summary of maximum concentrations for
groundwater impact based on testing along the proposed construction alignment. Approximately
400 linear feet (STA 3+00 to 8+00) of 48 -inch RCP will be installed with trench depths up to 20
feet deep with anticipated groundwater depth as shallow as 5 feet deep. The project duration
should not exceed six months.
The currently available groundwater concentrations were derived from analysis of volatile
organic compounds via EPA Method 8260B, which is a standard environmental analysis of
environmental media specified in the EPA SW -846 manual. Testing of groundwater in impacted
2 ATC Associates of North Carolina, P.0
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WO01701 October 16, 2017
areas will be conducted prior to NPDES discharge via EPA Method 8260 to confirm conditions
found by the prior analyses. Testing of NPDES-permitted treatment system conditions will also
be conducted by EPA Method 8260 during discharge treatment.
1.3 Dewatering Conditions and Flow Projections
The source of groundwater from dewatering will likely be primary porosity from residual soils
below the water table. Although rock tunneling is not expected in the project area potential exists
for limited sections of the storm drain system to encounter bedrock and for dewatering to occur
from bedrock fractures. The volume of flow associated with dewatering will likely be variable
based on the materials encountered and other factors; however, the estimated flow volumes are
based on historic flow volumes documented during dewatering along Baxter Street on the
northeastern end of the project, at prior Outfall 3, and flow at the tunnel section, which included
bedrock near the intersection of Morehead Street with Oriole Street, at prior Outfall 1. This
dewatering, treatment and discharge occurred under NPDES Permit NC0089443.
The prior dewatering and treatment was conducted during the period of fall 2014 through the
winter of 2016. Flow was variable based on construction activities and the aquifer materials that
were encountered. The observed flow rates ranged from lows of approximately 0.56 to 1.0
gallons per minute (gpm) up to maximum flows approaching 14 gpm. The lowest flows were
recorded in areas that involved trenching through soil overburden aquifer conditions, and the
highest flows resulted during tunneling through bedrock.
Based on experience with the prior trenching and tunneling at other area's of the project, as well
as bedrock hydraulic testing in the Piedmont Physiographic Province, a rough range of likely
flow volumes for the dewatering if groundwater is encountered could be approximately 1.0 to 50
gpm. ATC estimates an amount for this proposed permit that is less than NPDES Permit No.
0089443, based on the depth and lateral exposure of excavation that are expected to be less than
the downstream parts of the construction. The actual amount of dewatering volume during
construction will depend upon the length of trenching interval that is exposed to aquifer and
whether the excavation occurs within residual soils or in water bearing fractures.
3 ATC Associates of North Carolma, P C
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No. 199WOO1701 October 16, 2017
The area of stormwater improvements proposed for the area approximately 400 to 800 feet to the
east of the intersection of South Boulevard and Rensselaer Avenue encompasses groundwater
impact by chlorinated solvents from the former McCorkle's Cleaners that exceed surface water
standards.
The anticipated dewatering fluids will contain PCE, TCE, and VC impact exceeding 2B
Standards for Class C surface water in the area of the receiving waters. The standard for fish
consumption in Class C waters is 3.3 ug/L for PCE, 30 ug/L for TCE, and 2.4 ug/L for VC.
Collection of groundwater containing impact concentrations of up to 113 ug/L of PCE, 50.7 ug/L
of TCE and approximately 15.2 ug/L of VC could be expected given the most recent
groundwater conditions found during an April 2017 monitoring event of the apparent releases at
McCorkle's Cleaners. Table I contains the maximum concentrations from the April 2017
monitoring event, and Appendix B contains the June 2017 Groundwater Monitoring Report for
the April 2017 sampling data. For the purposes of treatment design, ATC has assumed a flow of
up to 50 gpm, with the three regulated chlorinated solvents' concentrations indicated above, so
that treatment would result in discharge concentrations that are less than the Class C surface
water standards.
4 ATC Associates of North Carolina, P C.
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No. 199WO01701 October 16, 2017
2.0 ENGINEERING ALTERNATIVES ANALYSIS
The North Carolina Division of Water Quality Engineering Alternatives Analysis (EAA)
Guidance Document, dated June 23, 2005, requires an evaluation of wastewater disposal
alternatives in addition to direct discharge. The subject discharge will be from a groundwater
remediation system and the following wastewater disposal alternatives are therefore being
evaluated:
• Connection to an existing wastewater treatment system
• Land application
• Infiltration galleries
• In-situ groundwater remediation wells
• Closed-loop groundwater remediation wells
2.1 Connection to an Existing Wastewater Treatment System
ATC contacted the Charlotte Water to determine if groundwater from the onsite treatment
system could be discharged to the Charlotte Water's Publicly Owned Treatment Works (POTW).
Charlotte Water did not provide permission to discharge pre-treated groundwater to the sewer
system. Thus, POTW discharge for the treated water will not be an acceptable alternative for
discharge of treated dewatering fluids.
2.2 Land Application
Land application of groundwater through drip irrigation or spray irrigation is not a feasible
alternative for disposal of dewatering fluids at the project site. The project is located in an urban
area of Charlotte, and sufficient permeable land is not available in the vicinity for groundwater
application. The land area requirements also entail setbacks of the land application areas from
property boundaries. Additionally, the drainage construction project will be conducted in
municipal roadways, and unpaved private properties would therefore need to be acquired for land
application purposes. According to sales records obtained from Charlotte -Mecklenburg
POLARIS (Property Ownership and Land Records Information System), private properties in the
project vicinity would cost approximately $500,000 to $2,000,000. Groundwater treatment,
5 ATC Associates of North Carolina, P C
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No. 199WOO1701 October 16, 2017
which would be required prior to irrigation, would add to the expense of this alternative. Based
on excessive expenses needed for property purchases, as well as lack of available permeable
area, land application is not a feasible alternative.
2.3 Infiltration Galleries
An infiltration gallery is a horizontal drain constructed of perforated piping and surrounded by
permeable material, such as sand or gravel, which distributes treated water for infiltration to
subsurface soils. An infiltration gallery should be able to store and transmit water to the
subsurface at the same or greater rate that water is being added to prevent flooding. Assuming
the maximum potential discharge rate of 50 gpm, the surficial silt and clay of the Piedmont
would not transmit dewatering fluids at a sufficient rate to prevent flooding. ATC personnel have
extensive experience with past efforts through non -discharge permitting where infiltration, in
Piedmont soils with much lower flow rates were unsuccessful, even with expansion of
infiltration galleries beyond original designs. The galleries would also require extensive land
area for construction, which is not available at the subject site. In addition, because the proposed
project area spans over 1000 feet, a stationary discharge location would not be feasible and
multiple galleries would be necessary. The use of infiltration galleries for discharge of
dewatering fluids is infeasible for the project.
2.4 In -Situ Groundwater Remediation Wells
At least two separate classes of technologies could be interpreted to meet the definition of in-situ
groundwater remediation. In one sense, in-situ groundwater remediation would be conducted by
injection of materials designed to reduce contaminant concentrations in groundwater, so that
water collected during construction dewatering could be directly discharged, without additional
treatment, to surface waters. Such in-situ remediation usually relies upon trenches, galleries, or
injection wells to infiltrate fluids that remediate dissolved contaminants and contaminants that
are sorbed to the soil and aquifer matrix. Such materials either enhance natural biological
processes of aerobic or anaerobic metabolism; act chemically upon the contaminants by
oxidation or reduction; or provide a material, such as activated carbon, to sorb the contaminants.
Combinations of the technologies are also often used.
6 ATC Associates of North Carolina, P C
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATCProiectNo 199WOO1701 October 16. 2017
In-situ groundwater remediation can be effective at reduction of impact to achieve groundwater
regulatory goals; however, full remediation in the limited time before inception of the storm
drain improvement project, especially to concentrations below surface water standards, would be
unlikely. Property access across a much larger footprint than the project currently affects would
also be necessary for effective remediation of materials that might migrate to the dewatering
locations. Reactive barrier walls installed by trenching could be attempted. Again, the project
footprint would be excessively expanded, and potential for impacted groundwater to migrate
beneath the reactive barrier trench would be enhanced due to the dewatering. If wells were used
an underground injection control (UIQ permit would also be required. Full remedial costs to
render the impacted groundwater suitable for discharge would also be prohibitively expensive, if
such a method were even technologically feasible, which is not certain.
Another potential interpretation for in-situ groundwater remediation entails that dewatering
fluids be collected, treated, and re -injected to specifically -installed, subsurface injection wells for
management of the fluid. This process would require sufficient wells for the Piedmont bedrock
aquifer to accept the injection of the dewatering fluid. Approval of the fluid injection would also
require a UIC permit. Installation of piping to carry the fluids to the injection well locations
would be needed, or contaminated water would need to be transported to a separate area for
injection. An extended period of time of likely many years for chlorinated remediation, using
what is essentially a pump -and -treat technology, would also be required and would constitute an
unacceptable time period given the project schedule. As with other alternatives the pump and
treat method with re-injection would be unnecessarily expensive. In-situ groundwater
remediation is judged to be an unacceptable alternative for the project.
2.5 Closed -Loop Groundwater Remediation Wells
A closed-loop groundwater remediation system, typically using recirculation well technology,
collects groundwater from one aquifer interval, treats the groundwater within the well, and
injects the treated water into another aquifer interval. The technology can be set up to operate in
several ways. The water can be collected from a shallow zone, treated, and then inject to a deeper
zone, or the opposite arrangement can be made. Hybrid setups of multiple collection and
7 ATC Associates of North Carolina, P C
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No. 199WOO1701 October 16, 2017
injection zones may also be possible. The hydraulic modeling and design of an inject well system
typically strives to achieve a re -circulation cell in the local groundwater regime, so that impacted
water migrating to the recirculation cell is captured and treated, with the net effect being that the
recirculation cell prevents impacted water from passing the recirculation cell.
As with other remedial options that require groundwater treatment, additional area and property
access would be required for recirculation; pilot testing would be needed to assure that a
sufficient number of wells were placed along the construction alignment; and certainty of
successful cleanup could not be assured, especially because the construction alignment is
through existing groundwater impact. The schedule to provide groundwater cleanup along the
alignment would also be an extended period. The action of dewatering adjacent to the
recirculation wells would also have uncertain consequences and could adversely affect the
technology's ability to assure clean dewatering discharge. Because of the cost of $100,000 or
more per recirculation well, the technology would also be likely to have very high costs. Closed-
loop groundwater remediation wells would be an unacceptable alternative for achieving
groundwater cleanup that would result in clean dewatering fluids collection prior to the project
start.
8 ATC Associates of North Carolina, P C
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WO01701 October 16, 2017
3.0 PROPOSED GROUNDWATER TREATMENT SYSTEM
Appendix A contains the NPDES Permit Application, Short Form C—GW, with supporting
documentation. The proposed groundwater treatment system consists of an air stripper,
Carbonair STAT 80 or equivalent, with four trays and a 350 cubic feet per minute (CFM) blower
with a flow capacity of up to 50 gpm to volatilize the expected chlorinated solvent impact in
groundwater for atmospheric discharge. Groundwater extracted from the trenching project will
be collected into an optional weir/equalization tank to reduce sediment, then into a holding and
settling vessel of approximately 500 to 1,000 gallons each. Flow from the holding tank will be
float switch -controlled and pumped at a maximum rate of 50 gpm through two, parallel filtration
units to remove sediment, and then proceed into the air stripper. The water will then cascade
downward through the ventilated air stripper trays as the air is forced upward through the air
stripper. Once in the holding tank at the base of the air stripper, a set of float switches will
control discharge via a second pump to the NPDES discharge location. Additionally, a second set
of, redundant pumps of 50 gpm maximum capacity will be placed for pumping to the air stripper
from the holding tank and after the air stripper to pump to the discharge. The second, redundant,
set of pumps before and after the stripper will serve as emergency pumps to assure continued
operation in case of filter clogging or other failure of one of the primary pumps. Figure 3 in the
attached appendix is a proposed treatment system schematic.
Two stormwater drains have been proposed for potential discharge and are located in an
easement area near the intersection of Cleveland Avenue and Rensselaer Avenue and in an
easement near the bend of South Caldwell Street. The final discharge point of the two storm
drains is Little Sugar Creek and its tributaries. Figure 2 in the attached appendix shows the
proposed discharge locations on a site plan.
A maximum flow rate of 50 gpm and influent concentration maximums from Table I were used
for treatment system design purposes. Table 2 provides model output for treatment by the
specified air stripper or equivalent. The effluent will be sampled initially upon treatment system
startup and again for the system startup after major changes in dewatering locations during the
project. Once certainty regarding dewatering fluid conditions is obtained for each area of
9 ATC Associates of North Carolina, P.0
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WO01701 October 16, 2017
construction, the need for continued NPDES permitted discharge will be evaluated and
communicated to the NPDES Permitting Unit. For each application, the system effluent will be
sampled once per week during the first month of operation and for each month of treatment
system operation thereafter. The laboratory analytical data using EPA Method 8260 for volatile
organic compounds will be utilized to determine that required treatment is being met. The
operator in responsible charge (ORC) will submit monthly discharge monitoring reports
(DMRs).
I
10 ATC Associates of North Carolina, P C.
EAA & NPDES Permit Application Myrtle/Morehead Storm Drainage Improvement
ATC Project No 199WO01701 October 16, 2017
4.0 DISCUSSION
Consideration should be given to the overall storm drainage improvement as a rationale for
requesting NPDES permitting as part of the project construction. That is, the goal of the project
is limit flooding during major storm events, which, especially in urban settings, present
significant contributions to adverse surface water quality conditions. The routing of the drain in
its large diameter, downstream segment as proposed will aid the project schedule and limit the
number of flood events affecting headwaters of the drainage during the planning and
construction phases. Please note that the project design includes methods to seal the drain against
impacted groundwater incursion across intervals affected by groundwater impact. Thus, the
proposed NPDES permit will allow construction of a drainage improvement that will ultimately
serve to increase water quality.
11 ATC Associates of North Carolina, P.C.
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STORMWATER DCHARLOTTE MYRTLE/MOREHEAD STORM DRAINAGE IMPROVEMENTS
OUTFALL TO LITTLE SUGAR CREEK. ENVIRONMENTAL SERVICES—CITY OF CHARLOTTE ASSOCIATES OF NORTH CAROLINA, P.C.
CHARLOTTE, NORTH CAROLINA Charlotte, North Carolina 28273 (704)529-3200 FAX (704)529-3272
PREP. BY REV. BY SCALE DATEPROJECT NO.
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CHARLOTTE, NORTH CAROLINA Charlotte, North Carolina 28273 (704)529-3200 FAX (704)529-3272
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ENVIRONMENTAL SERVICES -CITY OF CHARLOTTE ASSOCIATES OF NORTH CAROLINA, P.C.
CHARLOTTE, NORTH CAROLINA Charlotte, North Carolina 28273 (704)529-3200 FAX (704)529-3272
FB,D Flt "I[. I'RIFP. BY REV. BY SCfV..[:. DATE PROJECT NO.
MMNPDES AD/CS DH NOT TO SCALE 9.22.17 199WO01701
TABLES
Table 1
Maximum Concentrations of Constituents
Myrtle/Morehead Storm Drainage Improvement
Environmental Services - City of Charlotte
Charlotte. North Carolina
Notes:
1. Maximum concentrations obtained from groundwater monitoring analytical data from the most recent Groundwater Monitoring Report completed by Hart & Hickman,
dated June 15, 2017.
2. North Carolina 2B Standards are Class C water quality standards for surface waters (North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters).
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Maximum Concentration
10,300 113 200 50.7 15.2 3.33
20.9 2.44 1,350 43.3 2.70 3.13
NC 2B Standards
NE 3.3 NE 30 2.4 NE
I NE NE NE NE I NE I NE
Notes:
1. Maximum concentrations obtained from groundwater monitoring analytical data from the most recent Groundwater Monitoring Report completed by Hart & Hickman,
dated June 15, 2017.
2. North Carolina 2B Standards are Class C water quality standards for surface waters (North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters).
Table 2
Influent/Effluent Model for Treatment System
fro Ct
ERVICIES (ORPORMIiION ('
Customer:
Date:
Design Basis
ATC Group Services LLC
09/26/2017
Flow rate:
Water temperature
CARkMR
50 Spm
55 OF (assumed)
1140 Conrad Industrial Dr.
Ludington, M149431
office 231.843.2711
fax 231.843.4081
Contaminant
Influent Concentration
(Vg/L)(a)
Effluent Criteria
(µg/Qb)
Cis-1,2-Dichloroethene
10,300
-
Tetrachloroethene (PCE)
113
3.3
Trans-1,2-Dichloroethene (DCE)
200
-
Trichloroethene (TCE)
50.7
30
Vinyl Chloride (VC)
15.2
2.4
Xylene
3.33
-
1,1-Dichloroethene
20.9
-
Chloroform
2.44
-
2-Butanone (MEK)
1,350
-
Tert-Butylbenzene
43.3
-
1,1-Dichloroethane (DCA)
2.7
-
1,2,4-Trimethylbenzene
3.13
-
(a) Based on the given influent concentrations.
(b) Based on the given NC 2B standards.
Bold values indicate contaminants above discharge criteria.
Recommendations: Low Profile Air Stripper
STAT 80 unit with 4 trays, operated at 350 cfm
• PCE is the design contaminant.
• The effluent PCE concentration is predicted to be 1.9 ppb (see the modeling output below). All
contaminants are predicted to be below discharge criteria.
NOTICE
THIS DOCUMENT AND ITS CONTENTS ARE PROPRIETARY TO CARBONAIR ENVIRONMENTAL SYSTEMS, AND MAY NOT
BE COPIED, DISTRIBUTED OR USED BY ANYONE, IN WHOLE OR IN PART, WITHOUT THE EXPRESS AUTHORIZATION OF
CARBONAIR.
THE CONTENT OF THIS DOCUMENT HAS BEEN DEVELOPED BY CARBONAIR TO ADDRESS SPECIFIC FACTUAL
INFORMATION. IT MAY BE BASED ON INFORMATION AND ASSUMPTIONS THAT ARE NOT DISCLOSED WITHIN THIS
DOCUMENT, BUT REFLECT CARBONAIR'S KNOWLEDGE AND EXPERIENCE. THE INFORMATION IN THIS DOCUMENT
SHOULD NOT BE USED OR RELIED UPON BY ANYONE WITHOUT THE COOPERATION OR ASSISTANCE OF CARBONAIR
TO FULLY UNDERSTAND ITS INTENDED APPLICATION AND USE.
Safety - Quality - Teamwork - Professionalism - Positive Attitude
proact-usa.com
carbonair.com
CARBONAIR ENVIRONMENTAL SYSTEMS
1480 County Road C West, Roseville, MN 55113
PHONE: 800-526-4999 FAX: 651-202-2985
STAT MODEL CALCULATIONS
Tue Sep 26 12:22:29 CDT 2017
UNIT MODEL: STAT 80
WATER FLOW RATE (GPM): 50.00
AIR FLOW RATE (ACFM): 350.00
AIR -TO -WATER RATIO: 52:1
WATER TEMPERATURE (F): 55.00
AIR TEMPERATURE (F): 55.00
OPERATING PRESS (ATM): 1.00
SAFETY FACTOR M: 15.00
Influent Conc. for CIS-1,2-DICHLOROETHENE 10300.00000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
54.21330
77.93479
89.11638
94.57150
97.27749
98.63087
EFF CONC
ppb
4716.03037
2272.71688
1121.01241
559.13574
280.41804
141.02010
OFF -GAS CONC
ug/l
107.38403
154.37083
176.5189.9
187.32431
192.68427
195.36500
Influent Conc. for TETRACHLOROETHENE 113.00000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
64.84055
87.39902
95.45327
98.35545
99.40465
99.78441
EFF CONC
ppb
39.73018
14.23911
5.13781
1.85834
0.67275
0.24362
OFF -GAS CONC
ug/l
1.40903
1.89925
2.07427
2.13734
2.16014
2.16839
AIR EMISSION
lb/d
3.35186
4.81849
5.50982
5.84709
6.01440
6.09807
AIR EMISSION
lb/d
0.04398
0.05928
0.06475
0.06671
0.06743
0.06768
Influent Conc. for TRANS-I,2-DICHLOROETHENE 200.00000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
58.34519
81.84956
91.94170
96.39305
98.37966
99.27092
EFF CONC
ppb
83.30961
36.30088
16.11661
7.21390
3.24068
1.45816
OFF -GAS CONC
ug/l
2.24405
3.14806
3.53622
3.70743
3.78383
3.81811
Influent Conc. for TRICHLOROETHENE 50.70000 ppb
NO OF
REMOVAL EFF
EFF CONC
OFF -GAS CONC
TRAY
%
ppb
ug/l
1
63.02637
18.74563
0.61451
2
85.92917
7.13391
0.83781
3
94.58755
2.74411
0.92223
4
97.90956
1.05985
0.95462
AIR EMISSION
lb/d
0.07005
0.09826
0.11038
0.11572
0.11811
0.11918
AIR EMISSION
lb/d
0.01918
0.02615
0.02879
0.02980
5 99.19135 0.40999 0.96712
6 99.68700 0.15869 0.97195
Influent Conc. for VINYL CHLORIDE 15.20000 ppb
NO OF
REMOVAL EFF
EFF CONC
OFF -GAS CONC
TRAY
%
ppb
ug/l
1
73.89606
3.96780
0.21600
2
93.07166
1.05311
0.27206
3
98.15309
0.28073
0.28691
4
99.50709
0.07492
0.29087
5
99.86841
0.02000
0.29192
6
99.96487
0.00534
0.29220
Influent Conc. for XYLENES (TOTAL) 3.33000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
%
57.75230
81.57573
91.85683
96.37981
98.38643
99.27998
EFF CONC
ppb
1.40685
0.61353
0.27117
0.12055
0.05373
0.02398
OFF -GAS CONC
ug/l
0.03698
0.05224
0.05882
0.06172
0.06301
0.06358
Influent Conc. for 1,1-DICHLOROETHENE 20.90000 ppb
NO OF
REMOVAL EFF
EFF CONC
OFF -GAS CONC
TRAY
%
ppb
ug/l
1
72.74583
5.69612
0.29238
2
92.49504
1.56854
0.37176
3
97.92753
0.43315
0.39359
4
99.42725
0.11971
0.39962
5
99.84168
0.03309
0.40129
6
99.95623
0.00915
0.40175
Influent Conc. for CHLOROFORM 2.44000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
%
53.02738
76.79326
88.26236
93.99442
96.90932
98.40470
EFF CONC
ppb
1.14613
0.56624
0.28640
0.14654
0.07541
0.03893
Influent Conc. for MEK 1350.00000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
%
1.90403
3.24246
4.19215
4.87048
5.35730
5.70786
EFF CONC
ppb
1324.29554
1306.22677
1293.40601
1284.24846
1277.67642
1272.94386
OFF -GAS CONC
ug/l
0.02488
0.03603
0.04142
0.04411
0.04547
0.04617
OFF -GAS CONC
ug/l
0.49432
0.84179
1.08835
1.26445
1.39084
1.48185
0.03019
0.03034
AIR EMISSION
lb/d
0.00674
0.00849
0.00896
0.00908
0.00911
0.00912
AIR EMISSION
lb/d
0.00115
0.00163
0.00184
0.00193
0.00197
0.00198
AIR EMISSION
lb/d
0.00913
0.01160
0.01229
0.01247
0.01253
0.01254
AIR EMISSION
lb/d
0.00078
0.00112
0.00129
0.00138
0.00142
0.00144
AIR EMISSION
lb/d
0.01543
0.02628
0.03397
0.03947
0.04341
0.04625
Influent Conc. for tert-BUTYLBENZENE 43.30000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
0
58.57018
82.44624
92.49306
96.77697
98.61389
99.40345
EFF CONC
ppb
17.93911
7.60078
3.25050
1.39557
0.60019
0.25831
OFF -GAS CONC
ug/l
0.48771
0.68652
0.77018
0.80585
0.82115
0.82772
Influent Conc. for 1,1-DICHLOROETHANE 2.70000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
58.17892
81.74715
91.89024
96.36872
98.36841
99.26577
EFF CONC
ppb
1.12917
0.49283
0.21896
0.09804
0.04405
0.01982
OFF -GAS CONC
ug/l
0.03021
0.04245
0.04771
0.05004
0.05108
0.05154
Influent Conc. for 1,2,4-TRIMETHYLBENZENE 3.13000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
43.88496
67.07570
80.20557
87.93073
92.57911
95.41401
EFF CONC
ppb
1.75640
1.03053
0.61957
0.37777
0.23227
0.14354
OFF -GAS CONC
ug/l
0.02642
0.04037
0.04828
0.05293
0.05573
0.05743
Influent Conc. for TOTAL VOCs 12104.70000 ppb
NO OF
TRAY
1
2
3
4
5
6
REMOVAL EFF
0
48.65504
69.85020
79.81133
84.66836
87.08372
88.29939
STAT Modeler Disclaimer
EFF CONC
ppb
6215.15292
3649.54311
2443.77743
1855.84939
1563.47662
1416.32350
OFF -GAS CONC
ug/l
113.26052
162.59917
185.78697
197.09328
202.71583
205.54570
AIR EMISSION
lb/d
0.01522
0.02143
0.02404
0.02515
0.02563
0.02584
AIR EMISSION
lb/d
0.00094
0.00132
0.00149
0.00156
0.00159
0.00161
AIR EMISSION
lb/d
0.00082
0.00126
0.00151
0.00165
0.00174
0.00179
AIR EMISSION
lb/d
3.53528
5.07533
5.79911
6.15202
6.32752
6.41585
Carbonair's STAT Modeler is accurate only when contaminants are completely
dissolved in water in the absence of substances, which may significantly
affect the stripper capabilities of contaminants, such as oil & grease,
surface active and foaming agents, alcohols, ketones, and other potential
Henry's constant altering contaminants. Although the effluent
concentration predictions made by the STAT Modeler are accurate
predictions of field performance, they do not constitute a guarantee that
these concentrations will be met in the field. Please contact your
Carbonair representative for a design review and confirmation.
APPENDIX A
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
NPDES Permit Number INCOO
If you are completing this form in computer use the TAB key or the up - down arrows to move from one
field to the next. To check the boxes, click your mouse on top of the box. Otherwise, please print or type.
1. Contact Information:
Owner Name
City of Charlotte, Attn. Douglas Pierotti, P.G.
Facility Name
Myrtle/Morehead Storm Drainage Improvement
Mailing Address
600 East Fourth St.
City
Charlotte
State / Zip Code
North Carolina / 28202
Telephone Number
(704)651-4366
Fax Number
(704)336-4554
e-mail Address
dpierotti@charlottenc.gov
2. Location of facility producing discharge:
Check here if same as
above ❑
South Boulevard; South Caldwell Street; Templeton
Street Address or State Road Avenue; Euclid Avenue; Rensselaer Avenue, and Cleveland
Avenue
City
Charlotte
State / Zip Code
North Carolina / 28202
County
Mecklenburg
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the
Operator in Responsible Charge or ORC)
Name
City of Charlotte Attn. Douglas Pierotti, P.G.
Mailing Address
600 East Fourth St.
City
Charlotte
State / Zip Code
North Carolina / 28202
Telephone Number
(704)651-4366
Fax Number
(704)336-4554
4. Ownership Status:
Page 1 of 3 C -GW 03/05
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
Federal ❑ State ❑ Private ❑ Public
5. Products recovered:
Gasoline ❑ Diesel fuel ❑ Solvents ® Other
6. Number of separate discharge points: 3
Outfall Identification number(s) #1 and #2 (Little Sugar Creek)
7. Frequency of discharge: Continuous ® Intermittent ❑
If intermittent:
Days per week discharge occurs: Duration:
8. Treatment System Design flow 0.050 MGD
9. Name of receiving stream(s) (Provide a map showcng the exact location of each outfall, including
latitude and longitude):
Little Sugar Creek "Class C"
10. Please list all additives to the treatment system, including chemicals or nutrients, that have
the potential to be discharged.
No Additives
11. Is this facility located on Indian country? (check one)
Yes ❑ No
12. Additional Information
All applicants (including renewals):
A USGS topographical map (or copy of the relevant portion) which shows all outfalls
A summary of the most recent analytical results (effluent data, if available) containing the
maximum values for each chemical detected
NEW Applicants only:
Engineering Alternative Analysis
Description of remediation treatment system components, capacities, and removal efficiency
for detected compounds.
If the treatment system will discharge to a storm sewer, written approval from the
municipality responsible for the sewer.
A list of any chemicals found in detectable amounts at the site, with the maximum observed
concentration reported for each chemical (the most recent sample must be collected less
than one year prior to the date of this application)
For petroleum -contaminated sites - Analyses for Volatile Organic Compounds (VOC) should
be performed. Analyses for any fuel additives likely to be present at the site and for phenol
and lead should also be performed.
For sites contaminated with solvents or other contaminants - EPA Method 624/625
analysis should be performed.
Page 2 of 3 C -GW 03/05
NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities
13. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
Douglas Pierotti, P.G. Senior Project Manager
Printed name of Persop Signing Title
Da
North Ciro a General Statute 143-215 6 (b)(2) provides that Any person who knowingly makes any false
statein t r presentation, or certification in any application, record, report, plan, or other document files or
required o be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or
monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable
by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both (18 U S C. Section
1001 provides a punishment by a fine of not more than $25,000 or imprisonment not more than 5 years, or both,
for a similar offense.)
Page 3 of 3 C -GW 03/05
APPENDIX B
Groundwater Monitoring Report
McCorkle's Cleaners
DSCA ID: DC600077
1437 South Boulevard
Charlotte, Mecklenburg County
North Carolina Dry -Cleaning
Solvent Cleanup Act Program
H&H Job No. DSO -80G
June 15, 2017
nuoihq
.Q
Ste- _
OV221 !
•, j NGINE�G.
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
#C-1269 Engineering
#245 Geology
2923 South Tryon Street, Suite 100 3334 Hillsborough Street
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586 0007 main 1 919.847.4241 main
Groundwater Monitoring Report Forms
for
North Carolina Dry -Cleaning Solvent Cleanup Act Program
Facility Name:
McCorkle's Cleaners
1437 South Blvd, Charlotte, Mecklenburg County, North Carolina
DSCA ID No.:
DC600077
Submittal Date:
June 15, 2017
Prepared By:
Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC 28203
Reporting Period: April 2017 to
Type of Report: One -Time Event RI
Semi -Annual 0
Quaterly ❑
Annual 0
Table of Contents
LVA I "Nall
DSCA ID No.:
DC600077
Form/Att
. No.
Description
Check box
if included
Groundwater Monitoring Report Forms
Form 1
Report Summary
0
Form 2
Quality Assurance/Quality Control Procedures
0
Form 3
Results Conclusions and Recommendations
Groundwater Monitoring Report Attachments
Aft. 1
Disposal of IDW receipts from receiving facilities, or any required harzardous
p
Aft. 2
Site Location Map
p
Att. 3
Site Map
p
Att. 4
Groundwater Gradient Map
p
Att. 5
Groundwater Isoconcentration Maps
0
Att. 6
Groundwater Concentration Trend Graphs
0
Att. 7
Laboratory Analytical Report
p
CA ID No.: DC600077
Dates samples were collected 4/24/2017
Number of existing monitoring wells 9
List the sampled monitoring wells MW -1, MW -2S, MW -2D, MW -3, MW -4, MW -5, MW -6, MW -7, and
MW -8
List the sampled water supply wells No water supply wells sampled
List surface water samples collected No surface water samples collected
Date analyses were performed 4/27/2017 & 4/28/2017
Were any holding times exceeded? O Yes O No
Dates monitoring/supply wells were gauged 4/24/2017
Does investigation derived waste (IDW) generated during these activities still remain at the site pending
disposal9 F77 OO No
Average depth to groundwater 9 07 ft - shallow wells
Groundwater flow direction southeast
Was the static groundwater level above the top of the well screen in any wells? OO Yes O No
If Yes, indicate which wells MW -1, MW -2D, MW -4, and MW -6
Is the aquifer I O Confined (9 Unconfined O Perched
Were any existing monitoring wells damaged O Yes O No
If Yes, indicate which wells
Has the groundwater plume been defined? O Yes O No
Any ongoing assessment activities? O Yes O No
If Yes. provide details in the space below
Any ongoing remediation activates? I O Yes O No
If Yes, provide details in the space below
Any significant changes in the subsurface conditions9
If Yes, provide details in the space below-
O Yes) No
Quality Assurance/Quality Control Procedures
DSCA ID No.: DC600077
Describe the standard quality assurance/quality control (QA/QC) procedures which are practiced in order to
ensure that the samples are representative of actual conditions and that analytical results are valid
The water level and water quality meters were decontaminated using Alconox detergent and distilled water
after each well was gauged, measured, and/or pumped to avoid cross -contamination New nitrile gloves and
purge/sample tubing (both polyethylene and silicone) were used at each well Samples were collected
directly into laboratory -prepared sample containers, labeled with the site and sample identifications, time,
date, sampler's initials, and analysis method Samples were secured in protective wrap or bags before being
covered with ice and cooled to 4 degrees Celsius in a laboratory -supplied sample cooler A sample chain -of -
custody was completed and placed in the sample cooler The cooler was picked up by a courier for delivery
to TestAmerica Laboratories, Inc in Nashville, Tennessee The laboratory ran standard Type Il QC
measures.
Describe the specific sampling technic ue employed during the collection of all ground water samples.
Standard USEPA-approved low-flow/low-stress purge techniques were employed during the collection of the
groundwater samples Polyethylene tubing was installed to the middle of the well screen, secured at the top
of the well, and connected to a short piece of silicone tubing at the peristaltic pump rotor A second piece of
polyethylene tubing was connected to the outflow side of the silicone tubing Depth -to -water was then
measured with a decontaminated water level probe, and the probe was set at the top of the water column
Groundwater was drawn through the tubing by the peristaltic pump at a rate that prevented drawdown of the
water column in the well (approximately 100-250 mUmm at this site) Field measurements of temperature,
pH, conductivity, dissolved oxygen (DO), and oxidation-reduction potential (ORP) were collected during low
flow purging Readings of each parameter were collected at 5 minute intervals After field readings stabilized,
samples were collected using the EPA -approved "soda -straw method".
Describe the EPA approved methods used to extract and analyze the samples submitted the laboratory.
Reference the maximum holding time for each type of analysis performed
Groundwater samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260B The
maximum holding time for VOC analysis is 14 days from the sample collection date (when the sample is
preserved in HCL). All samples were preserved with HCL and were analyzed within 14 days of collection
There were no discrepancies noted on the laboratory analytical reports for the analytes detected in the
samples
Results, Conclusions and Recommendations
DSCA ID hlo.: DC606056
Results
Maximum Concentration Detected in Groundwater
Most Recent Event Detected at Site To -date
Chemical Sampling Concentration Sampling Concentration
Date Sample ID 1mg/L1 Date Sample ID [mg/L1
Tetrachloroethylene 04/24/17 MW -3 0.113 03/09/16 MW -2S 0.622
Trichloroethylene 04/24/17 MW -3 00507 03/09/16 MW -2S 0 754
Vinyl Chloride 04/24/17 MW -2S 00152 10/20/15 MW -2S 0.097
cis-1,2-Dichloroethene 04/24/17 MW -2S 10.3 01/28/15 MW -2S 13
trans-l,2-Dichloroethene 04/24/17 MW -2S 0.200 03/09/16 MW -2S 0.348
Note Other constituents have been detected in groundwater. See Table 8 for a complete list
Conclusions
Instructions Discuss any trends or changes noted in analytical results
Hart & Hickman, PC (H&H) conducted a groundwater sampling event on April 24, 2017, which included gauging water levels
and collecting samples from all site monitoring wells The primary constituents of concern at the site are tetrachloroethene
(PCE) and it's degradation products trichloroethene (TCE), cis-l,2-dichloroethene (cis-1,2-DCE), trans-l,2-dichloroethylene
(trans-1,2-DCE), and vinyl chloride (VC) Other petroleum -related compounds are present in site monitoring wells (see Table
8)
Graphs of concentration versus time are provided in Attachment 6 Based on review of the graphs, PCE and TCE
concentrations in source area shallow monitoring well MW -2S have fluctuated dramatically over time and were not detected
during the April 2017 event Concentrations of cis-1,2-DCE, trans-1,2-DCE, and VC have been more consistent in MW -2S
over time Concentrations of PCE and its degradation products in deeper source area monitoring well MW -21), nearby
downgradient well MW -3, and the remaining upgradient and downgradient wells (except MW -6) appear to be generally stable
or decreasing However, concentrations in MW -6 (located approximately 360 ft downgradient of the source property to the
southeast) appear to be increasing overtime Additional sampling is needed to further evaluate concentration trends a the site
Recommendations
H&H conducted a groundwater sampling event at the McCorkle's Cleaners site on April 24, 2017 to evaluate
current concentrations in the site monitoring wells. The analytical results indicate a potential decreasing
concentration trend for dry-cleaning related constituents in source area monitoring well MW -2S and an
increasing trend in downgradient well MW -6 (located in a residential area). Concentrations in the remaining
site monitoring wells appear to be stable or decreasing. H&H recommends additonal groundwater sampling to
further evaluate groundwater concentration trends at the site
TABLES
Analytical Data Tables
for
North Carolina Dry -Cleaning Solvent Cleanup Act Program
McCorkle's Cleaners
Facility Name:
1437 South Blvd, Charlotte, Mecklenburg County, North Carolina
DSCA ID No.:
DC600077
Submittal Date:
June 15, 2017
Hart & Hickman, PC
11 Prepared By:
2923 S. Tryon Street, Suite 100, Charlotte, NC 28203
Table of Contents
•
DSCA ID No.: DC600077
Table/
Att. No.
Description
Check box
if included
Tables
Table 1
Site Chronology
D
Table 2
Analytical Data for Soil
❑
Table 3
Analytical Data for Sub -slab Gas
❑
Table 4
Analytical Data for Soil Gas
❑
Table 5
Analytical Data for Indoor and Outdoor Air
❑
Table 6
Monitoring Well Construction Data
0
Table 7
Groundwater Elevation Data
O
Table 8
Analytical Data for Groundwater
El
Table 9
Analytical Data for Surface Water
❑
Table 10
Water Well(s) Survey Data
❑
Table 11
Analytical Data for Water Supply Well(s)
❑
Table 12
Analytical Data for Natural Attenuation Parameters
O
Attachments
Att 1
Site map showing location(s) of soil boring(s)
❑
Att 2
Soil contaminant concentration maps showing the concentration at each sampling
point
❑
Att 3
Soil isoconcentration maps.
❑
Att 4
Site map showing location(s) of monitoring well(s)
❑
Att 5
Well completion diagrams and records of construction submitted to state
❑
Att 6
Groundwater gradient map for each sampling event
❑
Att 7
PCE concentration map showing the concentration at each sampling point and
isoconcentration map However, if there are significant plumes for other dry-
cleaning contaminants, contaminant concentration maps for each chemical of
concern should be included.
❑
Att. 8
Groundwater concentration trend plots
❑
Att. 9
Map showing location(s) of surface water sample(s) (if applicable)
❑
Att 10
Surface water concentration map showing the concentration at each sampling
point (if applicable)
El
Att 11
USGS Quad map with plotted water well location(s) within the 1,500 foot and 0 5
mile radii of the site (if applicable)
11
Att 12
Site map showing location(s) of monitoring well(s) for natural attenuation paramet
❑
Att 13
Site map showing location(s) of indoor air, outdoor air, or soil gas samples
❑
Att 14
Air and soil gas concentration map showing the concentration at each sampling point ❑
Att 15
Signed laboratory analytical reports including chain -of custody and quality
assurance/quality control (QA/QC) documentation (only if not previously
submitted)
❑
Att 16
❑
Att 17
❑
Att 18
❑
Att 19
❑
Att 20
❑
Att. 21
❑
Note.
1 All maps must include a bar scale, north arrow, site name, DSCA ID No., and date
Table 1: Site Chronology
DSCA ID No.: DC600077
Chronology of Events
Instructions Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility Commence with the first date a problem was suspected and continue
through the most recent activity described In the current report
Terracon Consultants, Inc conducted a Phase I Limited Site Assessment (LSA) of the site property The LSA revealed
September 2012
that the source property building operated as an active dry-cleaner from at least the 1920s to the 1960s Remnants of the
former dry-cleaning operations were found during the assessment including an old dryer located inside the back of the
building and an empty, 55 -gallon drum of Perchloroethylene located outside in a cmder-block storage area
Terracon Consultants, Inc conducted a Phase 11 LSA of the site property which included collecting soil and groundwater
October 2012
samples from two downgradient borings and collecting one, upgradient groundwater sample The results of the
assessment indicated a dry-cleaning release had occurred at the site Both petroleum (Stoddard Solvent) and
tetrachloroethene (PCE) based constituents were detected in soil and groundwater samples
March 8, 2013
The site is certified into the DSCA Program
H&H conducted Pnontization Assessment (PA) activities at the site The PA activities included the installation and
sampling of seventeen soil borings (SB -1 through SB -17), ten temporary monitoring wells (TW -1 through TW -10), four
Type -II monitoring wells (MW -1, MW -3, MW -4 and MW -5) and one nested well pair (MW-2S/D) As partof the PA
activities, H&H conducted vapor intrusion (VI) assessment activities which included collection of two sub -slab soil gas
samples (VMP-1 and VMP-2), two indoor air samples (IAS -1 and IAS -2), and one outdoor background air sample (BAS
June - August 2013
1) Both indoor air samples (IAS -1 and IAS -2) collected in June 2013 (with no HVAC system operating) had Hazard
Index (HI) values above 1 H&H re -sampled indoor air in the same locations (IAS -1 and IAS -2) in August 2013 after the
HVAC system had been operating for a few days The indoor air samples collected in August 2013 had HI values less
than1 On September 11, 2013, H&H submitted a Vapor Intrusion Assessment letter report to the DSCA Program On
September 20, 2013, H&H submitted a Priontization Assessment Report and associated attachments to the DSCA
Program documenting the results of the PA activities
H&H conducted additional assessment activities at the site to further delineate the extents of soil and groundwater
impacts, including the collection of samples from two soil borings (SB -18 and SB -17) and twelve temporary
January 2015
groundwater sampling locations (TW -11 through TW -22) H&H also collected groundwater samples from the existing
site monitoring wells (MW -1, MW-2S/D, MW -3, MW -4 and MW -5) On April 30, 2015, H&H submitted a report to
the DSCA Program documenting the results of the additional assessment activities
H&H conducted additional vapor intrusion assessment activities at the site Initially, H&H collected near -slab,
January - March
subsurface soil gas samples (SGP -1 through SGP -5) on the source property and adjacent properties to the east and south
2015
Based on the results, H&H subsequently collected an indoor air sample from the adjacent Elizabeth House Flowers
building located at 1431 South Blvd On April 30, 2015, H&H submitted a letter report to the DSCA Program
documenting the additional vapor intrusion assessment activities
H&H conducted additional groundwater assessment activities at the site to further delineate the extent of groundwater
impacts downgradient of the source property The additional assessment activities included the installation of three
October 2015
permanent monitoring wells (MW -6, MW -7, and MW -8) Following installation, the newly installed monitoring wells
were sampled along with the existing site monitoring wells (MW -1, MW -2, MW -3, MW -4 and MW -5) On January7,
2016, H&H submitted a Monitoring Well Installation Report to the DSCA Program documenting the results of the
additional groundwater assessment activities
H&H conducted soil gas and groundwater sampling activities at the at the site The soil gas sampling was conducted at
the Charlotte Housing Authority property located to the southeast and downgradient of the site and included the
March 2016
collection of six sub -surface soil gas samples (VMP-1 through VN/IP-6) The groundwater sampling activies included the
collection of groundwater samples from monitoring wells MW -2S, MW -21), MW -3, MW -6, MW -7, and MW -8 On
April 7, 2016, H&H submitted a Groundwater Monitoring Report to the DSCA Program documenting the results of the
groundwater sampling activities
H&H conducted additional soil gas sampling activities on the Charlotte Housing Authority property located southeast
(downgradient) of the McCorkles Clenaers source property Three subsurface soil gas samples (VMP-7 through VMP-9)
May 2016
were collected to adjacent to the apartment tower evaluate the potential vapor intrusion risk On May 20, 2016, H&H
submitted a brief letter report to the DSCA Program documenting the sampling activities and results
Page 1 of 2
Table 1: Site ChronoIogy 1101
DSCA ID No.: DC600077
Chronology of Events
Instructions Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the most recent activity described in the current report.
H&H conducted additional soil gas sampling activities on four residentially -zoned properties located southeast
(downgradient) of the McCorkles Clenaers source property Subsurface soil gas samples were collected adjacent to each
September and
of the downgradient buildings to evaluate the potential vapor intrusion risk The samples were collected at 401
December 2016
Rensselaer Ave (VMP-10 and VMP-11), 323 Rensselaer Ave (VMP-12 and VMP-13), 325 Rensselaer Ave (VMP-14
and VMP-15), and 405 Rensselaer Ave (VMP-16 VMP-17, and VMP-18) On January 26, 2017, H&H submitted a
brief letter report to the DSCA Program documenting the sampling activities and results
H&H conducted groundwater sampling activities at the at the site The groundwater monitoring achvies included gauging
April 2017
Fater levels and collecting groundwater samples from each of the site monitoring wells (MW -1, MW -2S, MW -21), and
MW -3 through MW -8 On June 15, 2017, H&H submitted a Groundwater Monitoring Report to the DSCA Program
documenting the sampling activities and results
Page 2 of 2
Table 6:Monitoring
Well Construction Data
�61 11319-3
DSCA ID No.: DC600077
Well ID
Date Installed
(mm/dd/yy)
Number of Samples
Well Depth
[feet]
Well Diameter
[inch]
Screen Interval
[feet]
Status
(Active/Inactive)
MW -1
06/28/13
4
30
2
15-30
Active
MW -2S
08/05/13
5
23
1
8-23
Active
MW -2D
08/05/13
5
67
1
62-67
Active
MW -3
08/05/13
5
25
2
10-25
Active
MW -4
08/05/13
4
20
2
5-20
Active
MW -5
08/06/13
4
20
2
5-20
Active
MW -6
10/14/15
3
20
2
5-20
Active
MW -7
10/14/15
3
25
2
10-25
Active
MW -8
10/14/15
3
20
2 1
5-20
Active
Page 1 of I
Table 7: Groundwater Elevation Data
MIWA
DSCA ID No.:
DC600077
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevation
[feet]
Depth to NAPL NAPL Thickness Corrected*
[feet bgs] [feet] Groundwater
Elevation [feet]
MW-1
08/07/13
73198
13 72
71826
-- - -
01/28/15
15 52 71646
- -
10/20/15
1411 71787
- -- --
03/09/16
12 15 71983
04/24/17
13 17 718 81
MW-2S
08/07/13
72675
1252
71423
- -- --
01/28/15
1097 715 78
-- --
10/20/15
1190 71485
-- - --
03/09/16
10 16 71659
-- - --
04/24/17
1150 71525
- --
MW-2D
08/07/13
72663
1265
713 98
-- -- -
01/28/15
1172 71491
-- - --
10/20/15
1250 714 13
-- -
03/09/16
1052 716 11
-- -
04/24/17
1203 71460
-- -
MW-3
08/07/13
72797
15 14
71283
-- - -
01/28/15
1413 713 84
-- --
10/20/15
1495 71302
-- -
03/09/16
1275 71522
-- -- --
04/24/17
1465 71332
-- -- --
MW-4
08/07/13
723 14
497
718 17
- --
01/28/15
3 88 71926
-- --
10/20/15
549 71765
--
03/09/16
3 54 71960
-- -- --
04/24/17
301 720 13
-- -- --
MW-5
08/07/13
71847
809
71038
- -- --
01/28/15
656 71191
- -- --
10/20/15
766 710 81
-- -- --
03/09/16
535 713 12
-- - --
04/24/17
722 71125
-- -- --
MW-6
10/20/15
70872
641
70231
-- -
03/09/16
452 70420
-- - --
04/24/17
479 703 93
-- - --
Page 1 of 2
Table 7: Groundwater Elevation Data
DSCA ID No.: DC600077
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevation
[feet]
Depth to NAPL NAPL Thickness
[feet bgs] [feet]
Corrected*
Groundwater
Elevation [feet]
MW-7
10/20/15
716 17
1456
70161
-- --
03/09/16
1156
70461
--
04/24/17
1269
70348
--
MW-8
10/20/15
70397
7 11
69686
-- --
03/09/16
457
69940
04/24/17
5 53
69844
--
Note
TOC elevations for MW -1 through MW -5 were professionally surveyed by the Isaacs Group on 8/7/2013
TOC elevations for MW -6 through MW -8 were professionally surveyed by the Isaacs Group on 12/7/2015
Page 2 of 2
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DSCA ID No.: DC600077
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Page 3of4
Table 8(1): Anal tical Data for Groundwater ser Specified Chemicals
DSCA ID No.: DC600077
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Page 4 of 4
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ATTACHMENT I
IDW DISPOSAL RECEIPTS
Please onnt or Noe (Form designed for use on elite (12 -aitch) tvoewnter )
Form Approved OMB No 2050-0039
EPA Form 8700-22 (Rev 3-05) Previous editions are obsolete O V1rs1 Bc�9 i ED F,/ CC 9T4: TO S'TAME-E (IF REQU9RED)
UNIFORM HAZARDOUS
1. Generator ID Number
2 Page 1 of
3 Emergency Response Phone
4. Manifest Tracking Number
015460105 JJ K
WASTE MANIFEST
NGFO IS3459
1
800-266-3924-M1 37951
5 Generator's Name and Mailing Address Generators Site Address (if different than mailing address)
Petitioner for RSCA ate DCSM77, Slaw #007 McCorkles Cleaners 1437 Soffih Blvd,
DWNI-DSCA 1546 Niall Sefvtoe Center
Charlotte, NC26=3Slav�0ii7
R3121gh, NG 276-99-16M USA
Generator's Phone d.,c
6 Transporter 1 Company Name U S EPA ID Number
A&D Environmental SeriloeS (SC), LLC SC09575-%ni
7 Transporter 2 Company Name U.S. EPA ID Number
8. Designated Facility Name and Site Address U S EPA ID Number
Clean Harbors Deerpark, LP. TkD055141376
2027 Independence Parkway South
La Pone, TX 77671 USA
Facility's Phone. 261-930-23M
9a
9b U S. DOT Description (including Proper Shipping Name, Hazard Class, ID Number,
10. Containers
11. Total
12 Unlit
13 Waste Codes
No.
Type
HM
and Packing Group (If any))
Quantity
WtNGI
X
1
UNMM. w4a to Environmentally hazardous substance. Ilquid, n.o.s.,—
P
---
(teitaah}eraethplene), 9, PG Ill, ERG# 171, W101LU
i
Z
2
LU
3
I
t
4
r
14 Special Handling Instructions and Additional Information
9b.1) CHO-M11 (liquids) P x 55�a1
A&D Job No. %1479 Pw -7b Transponer V i Phone. 8M-434-7750
15. GENERATOR'SIOFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged,
marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable international and national govemmental regulations If export shipment and I am the Primary
Exporter, I certify that the contents of this consignment conform to the terms of the attached EPAAcknowledgment of Consent.
I certify that the waste minimization statement identified in 40 CFR 262 27 ) (if I am a large quantity generator) or (b) (if I am a small quan generator) is true
I r 024A,5 Signature •0.1 Month Day Year
C7n behalf of Petitioner OC, 6 0000 % 7
-j
f—
16 International Shipments
❑ Import to U S. ❑ Export from U S Port of entrylexit.
Transporter signature (for exports only), Date leaving U S
w
17 TransporterAcknowledgment of Receipt of Materials
Transporter 1 Printedrryped Name f Month Day
(Year
/ d
U411-1
M
ISignature
ZTransporter2
PnntedlTyped Name Signature Month Day Year
r-
18 Discrepancy
18a Discrepancy Indication Space ❑ Quantity ❑TypeElFull Rejection
❑ Residue ❑Partial Rejection
Manifest Reference Number
E�.
18b Alternate Facility (or Generator) U S. EPA ID Number
V
Facility's Phone
W
18c. Signature of Alternate Facility (or Generator)
Month Day Year
19. Hazardous Waste Report Management Method Codes ( e, codes for hazardous waste treatment, disposal, and recycling systems)
W
1
2
1
3
4
20 Designated Facility Owner or Operator Certification of receipt of hazardous materials covered by the manifest except as noted In Item 1 B
lTd-ntedfFyped
Name Signature Month Day Year
EPA Form 8700-22 (Rev 3-05) Previous editions are obsolete O V1rs1 Bc�9 i ED F,/ CC 9T4: TO S'TAME-E (IF REQU9RED)
CLEAN HARBORS ENVIRONMENTAL SERVICES, INC
LAND DISPOSAL RESTRICTION FORM LDR-1
MANIFEST NO a��� ':Z_ -V
THE HAZARDOUS WASTES IDENTIFIED ON THE HAZARDOUS WASTE MANIFEST IDENTIFIED ABOVE AND BEARING THE EPA
HAZARDOUS WASTE CODES LISTED BELOW ARE RESTRICTED WASTES WHICH ARE PROHIBITED FROM LAND DISPOSAL
WITHOUT FURTHER TREATMENT UNDER THE LAND DISPOSAL RESTRICTIONS, 40 CFR PART 268.7 (3)(2), AND RCRA SECTION
3004(D). IN ACCORDANCE WITH 40 CFR 268.7(a), THE EPA WASTE CODE, WASTE SUBCATEGORY, AND TREATABILITY
GROUPS, AS APPLICABLE, ARE INCLUDED BELOW
INSTRUCTIONS — COMPLETE ALL SECTIONS. REFER TO PAGE 3 OF THIS FORM FOR KEY TERMS/DEFINITIONS.
Column 1 - Line Item Enter the manifest line item number (e g , 11 a) that corresponds to the waste code(s).
Column 2 - Waste Codes/Subcategory Check off all applicable waste codes For D001 through D043, also check applicable
subcategory, for F001 through F005, check applicable constituents
Column 3 - Wastewater/Non-wastewater Check off "WW" for wastewater and "Non -WW" for non -wastewaters.
Column 4 - LDR Handling Code Circle the appropriate handling code, as follows
1 = The waste is a characteristic hazardous waste D001, D002, D003, D004 -D011, or D018-43 which is intended for
treatment/disposal in a CWA system, CWA-equivalent system, or Class I SDWA system. Underlying Hazardous Constituents
(UHC's) are NOT required to be identified.
1A= The waste is a characteristic hazardous waste D001 High TOC Ignitable Liquids Subcategory (i e , greater than
or equal to 10% TOC). Pursuant to 40 CFR 268 40, the waste must be treated using organic recovery (RORGS) or combustion
(CMBST) technology UHC's are NOT required to be Identified.
2 = The waste is a characteristic hazardous waste D001 (other than High TOC Ignitable Liquids), D002, D003 Explosive, Water
Reactive or Other Reactive subcategory, D004 -D011, D012-17 non -wastewater, or D018-43 which is intended for
treatment/disposal in a non-CWA system, non-CWA-equivalent system, or non -Class I SDWA system located in the United States
All UHC's which are reasonably expected to be present must be identified, except for D001 waste that is intended to be treated
using organic recovery (RORGS) or combustion (CMBST) technologies Identify UHC's by completing Sections I and IV of CHI
Form LDR-1 Addendum and attach completed Addendum to this form.
3 = The waste is a characteristic (i e , D -code) or listed (i e , F-, K-, U-, or P -code) hazardous waste which is intended for export and
treatment/disposal at a facility located outside the United States. LDR treatment standards do not apply to hazardous waste
treated/disposed in a foreign country, and per USEPA guidance, the identification of UHC's (if applicable) is not required for
hazardous waste that is intended to be exported. Note however that if the exported waste is subsequently returned for
treatment/disposal in the United States, all applicable LDR regulations would apply and a revised LDR notification would be
required
4 = The waste meets the definition of hazardous debris pursuant to 40 CFR 268.2(h) and is intended for treatment/ disposal in
compliance with the alternate debris treatment technologies of 40 CFR 26845 In accordance with the requirements of 40 CFR
2687(a)(2) the contaminants subject to treatment (CSTT's) must be identified as part of this notification. Identify CSTT's by
completing Section III and IV of the CHI Form LDR-1 Addendum and attach completed Addendum to this form These constituents
are being treated to comply with 40 CFR 268 45
5 = The waste is a characteristic waste D003 Reactive Sulfide, Reactive Cyanide, or Unexploded Ordnance subcategory, a
characteristic waste D012- 17 wastewater, or a listed (i e, F-, K-, U-, or P -code) hazardous waste. UHC's are NOT required to be
identified
6 = The waste is a lab pack that is intended for incineration using the alternative lab pack treatment standard under 40 CFR 268 42(c).
UHC's are NOT required to be identified, however, the generator must complete and attach the lab pack certification statement
on CHI Form LDR-LP Note that In accordance with 40 CFR Part 268 Appendix IV, lab packs which contain waste codes D009,
F019, K003, K004, K005, K006, K062, K071, K100, K106, P010, P011, P012, P076, P078, U134, and U151 are not eligible for
alternative lab pack treatment standard
`** NOTE: IF THE WASTE IS A SOIL CONTAMINATED WITH A LISTED OR CHARACTERISTIC WASTE AND THE GENERATOR
WANTS TO USE THE ALTERNATE TREATMENT STANDARD FOR SOILS, CONTACT CORPORATE COMPLIANCE FOR THE
APPROPRIATE LDR NOTIFICATION FORM.
SECTION I. CHARACTERISTIC WASTES D001 THROUGH D043
COLUMN 1 COLUMN 2.
COLUMN 3
LINE ITEM WASTE CODE / SUBCATEGORY
WASTEWATER/
SEE MANIFEST
NON -WASTEWATER
[ ] D001 Ignitables, except High TOC subcategory
[ ] WW [ ] Non -WW
[ ] D001 High TOC Ignitable Liquids Subcategory
[ ] Non -WW only
(Greater than or equal to 10% TOC)
[ ] D002 Corrosives
[ ] WW [ 1 Non -WW
[ ] D003
[ ] Reactive Sulfide, per 26123 (a)(5)
[ ] WW [ ] Non -WW
[ ] Reactive Cyanide, per 261.23(a)(5)
[ ] WW [ ] Non -WW
[ J Explosive, per 261 23(a)(6), (7) & (8)
[ ] WW [ ] Non -WW
[ ] Water Reactive, per 261 23(a)(2), (3) & (4)
[ ] Non -WW only
[ ] Other Reactive, per 261.23(a)(1)
[ ] WW [ ] Non -WW
[ ] Unexploded Ordnance, Emergency Response
[ ] WW [ ] Non -WW
[ ] D004 Arsenic
[ ] WW [ ] Non -WW
[ ] D005 Barium
[ ] D006
[ ] Cadmium
[ ] Cadmium Containing Batteries
[ ] D007 Chromium
(] D008
[ ] Lead
[ ] Lead Acid Batteries
[ ] WW [ ] Non -WW
[ ] WW [ ] Non -WW
[ ] Non -WW only
[ J WW [ ] Non -WW
[ 1 WW [ ] Non -WW
[ ] Non -WW only
CHI Form LDR-1, Page 1 of 3
COLUMN 4
HANDLING CODE
1 2 3 4 6
1A 3 6
1 2 3 4 6
1 3 4 5 6
1 3 4 5 6
1 2 3 4 6
1 2 3 4 6
1 2 3 4 6
1 3 4 5 6
1 3 4 5 6
1 3 4 5 6
1 2 3 4 6
2 3 6
1 2 3 4 6
1 2 3 4 6
2 3 6
[Effective 2/281001
CLEAN HARBORS ENVIRONMENTAL SERVICES, INC
LAND DISPOSAL RESTRICTION FORM LDR-1
MANIFEST NO
SECTION I. CHARACTERISTIC WASTES D001-43 (CONTINUED)
COLUMN 1 COLUMN 2 COLUMN 3 COLUMN 4
LINE ITEM WASTE CODE / SUBCATEGORY WASTEWATER/ HANDLING CODE
SEE MANIFEST NON -WASTEWATER
[ ] D009
[ ] Low Mercury, less than 260 mg/kg Mercury [ ] WW
[ ] Non -WW
1 2
3 4
[ ] High Mercury Organic
Subcategory [ ] Non -WW only
2 3
4
(] High Mercury Inorganic Subcategory [ ] Non -WW only
2 3
4
[) D010 Selenium
[ J WW
[ ] Non -WW
1 2
3 4 6
[ ] D011 Silver
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D012 Endnn
[ ] WW
[ ] Non -WW
2 3
4 5 6
[ J D013 Lindane
[ ] WW
[ ] Non -WW
2 3
4 5 6
[ ] D014 Methoxychlor
[ ] WW
[ ] Non -WW
2 3
4 5 6
[ ] D015 Toxaphene
[ ] WW
[ ] Non -WW
2 3
4 5 6
[ ] D016 2,4-D
[ J WW
[ ] Non -WW
2 3
4 5 6
[ ] D017 2,4,5 -TP (Silvex)
[ ] WW
[ ] Non -WW
2 3
4 5 6
[ J D018 Benzene
[] WW
[ j Non -WW
1 2
3 4 6
[ ] D019 Carbon tetrachloride
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D020 Chlordane
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D021 Chlorobenzene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ J D022 Chloroform
[] WW
[ J Non -WW
1 2
3 4 6
[ ] D023 o -Cresol
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D024 m -Cresol
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ j D025 p -Cresol
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D026 Cresol
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D027 1,4 -Dichlorobenzene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D028 1,2-Dichloroethane
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D029 1,1-Dichloroethylene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ J D030 2,4-Dinitrotoluene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D031 Heptachlor (and its epoxide) [ ] WW
(] Non -WW
1 2
3 4 6
[ ] D032 Hexachlorobenzene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D033 Hexachlorobutadiene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ J D034 Hexachloroethane
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D035 Methyl ethyl ketone
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D036 Nitrobenzene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ J D037 Pentachlorophenol
[ ] WW
[ ] Non -WW
1 2
3 4 6
(] D038 Pyridine
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D039 Tetrachloroethylene
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D040 Trichloroethylene
[ ] WW
[ j Non -WW
1 2
3 4 6
[ ] D041 2,4,5 -Trichlorophenol
[ ] WW
[ ] Non -WW
1 2
3 4 6
[ ] D042 2,4,6-Tnchlorophenol
[ ] WW
[ ] Non -WW
1 2
3 4 6
(] D043 Vinyl Chloride
[ ] WW
[ J Non -WW
1 2
3 4 6
SECTION II SPENT SOLVENT WASTES F001 THROUGH F005
COLUMN V COLUMN 2
COLUMN 3
COLUMN 4
LINE ITEM WASTE CODE / SUBCATEGORY WASTEWATER/
HANDLING CODE
SEE MANIFEST
NON -WASTEWATER
[ J F001 [F002 [ ] F003
[ ] F004 [ ] F005 [ ] WW
[Non -WW
3
4 (5 6
[ ] 1. ALL F001 -F005
[ ] 12 Cyclohexanone
[ ] 25
Pyndine
[ J 2. Acetone
[ ] 13 o -Dichlorobenzene
i`
[ ] 26
Tetrachloroethylene
[ ] 3. Benzene
[ ] 14 2-Ethoxyethanol (F005)
[ j 27
Toluene
[ ] 4 n -Butyl alcohol
only)
[ ] 28.
1,1,1-Trichloro-
[ ] 5 Carbon disulfide
[ ] 15 Ethyl acetate
ethane
[ ] 6 Carbon tetrachloride
[ ] 16 Ethyl benzene
[ ] 29
1,1,2-Trichloro-
[ ] 7 Chlorobenzene
[ ] 17. Ethyl ether
ethane
[ ] 8 o -Cresol
[ ] 18 Isobutyl alcohol
[ ] 30. Trichloroethylene
[ ] 9 m -Cresol (difficult to
[ ] 19 Methanol
[ ] 31
1,1,2-Tnchloro-
distinguish from
[ ] 20. Methylene chloride
1,2,2-trifluoroethane
p -cresol)
[ ] 21 Methyl ethyl ketone
(] 32.Tnchloromonofluorc-
[ ] 10 p -Cresol (difficult to
[ j 22 Methyl isobutyl ketone
methane
distinguish from
[ ] 23 Nitrobenzene
[ ] 33
Xylene - mixed isomers
m -cresol)
[ ] 24 2-Nitropropane (F005
(sum of o-, m-, and
[ ] 11 Cresol - mixed isomers
only)
p -xylene)
(sum of o-, m- and
p -cresol)
CHI Form LDR-1, Page 2 of 3 [Effective 2/28/00]
CLEAN HARBORS ENVIRONMENTAL SERVICES, INC
LAND DISPOSAL RESTRICTION FORM LDR-1
SECTION III CALIFORNIA LIST WASTES
COLUMN 1 COLUMN 2
LINE ITEM WASTE CODE / SUBCATEGORY
SEE MANIFEST
MANIFEST NO el -5-y6 a-,0-5-
COLUMN
-05
COLUMN 3
WASTEWATER/
NON -WASTEWATER
Hazardous waste containing one or more of the following [ ] WW [ ] Non -WW
California List constituents
[ ] ALL CALIFORNIA LIST CONSTITUENTS
[ J Liquids with nickel greater than or equal to 134 mgfl
[ J Liquids with thallium greater than or equal to 130 mg/I
[ ] Liquids with PCB's > or= 50 ppm
[ ] Waste containing HOC's > or = 1,000 mg/kg
COLUMN 4
HANDLING CODE
1 2 3 4 6
SECTION IV OTHER LISTED WASTES (F006-12. F019 -F028. F037-38, F039 K- U- AND P -CODES)
COLUMN 1 COLUMN 2 COLUMN 3' COLUMN 4
LINE ITEM WASTE CODE / SUBCATEGORY WASTEWATER/ HANDLING CODE
SEE MANIFEST NON -WASTEWATER
[ ] WW [ ] Non -WW 3 4 5 6
[ ] WW [ ] Non -WW 3 4 5 6
[ ] WW [ ] Non -WW 3 4 5 6
[ ] WW [ ] Non -WW 3 4 5 6
[ ] WW [ ] Non -WW 3 4 5 6
[ ] CHECK HERE IF ADDITIONAL LISTED WASTE CODES ARE PRESENT. COMPLETE AND ATTACH LDR-1 CONTINUATION
SHEET
[ ] CHECK HERE IF WASTE CODE F039 (MULTISOURCE LEACHATE) IS PRESENT IDENTIFY F039 CONSTITUENTS BY
COMPLETING SECTIONS II AND IV OF CHI FORM LDR-1 ADDENDUM AND ATTACH COMPLETED ADDENDUM TO THIS FORM.
SECTION V. CONTACT NAME AND DATE
On behalf of DSCA Petitioner S'te 000 7-7 /}
Pint Name z�� Date 2-67
7
KEY TERMS/DEFINITIONS
CLASS I SDWA SYSTEM means a Class I deep well facility regulated under the Safe Drinking Water Act (SDWA)
CWA SYSTEM means a centralized wastewater treatment facility discharging under a Clean Water Act (CWA) permit For example, a CWA
facility would treat organic or inorganic aqueous wastes and discharge the treated effluent to the local sewer system. Examples of CWA
treatment systems owned and operated by Clean Harbors include the wastewater treatment operations at Baltimore (including the CES
system), Bristol, Chicago, Cincinnati and Cleveland.
CWA-EQUIVALENT SYSTEM means a "zero discharge system" that engages in "CWA-equivalent" treatment before land disposal Zero -
discharge facilities treat hazardous wastes using "CWA-equivalent" treatment methods, but do not discharge the treatment effluent to a
sewer or water body (e g., spray irrigation land farm). "CWA-equivalent" treatment methods means biological treatment for organics, alkaline
chlorination, or ferrous sulfate precipitation for cyanide, precipitation/ sedimentation for metals, reduction of hexavalent chromium, or other
treatment technology that can be demonstrated to perform equally or greater than these technologies.
HIGH TOC IGNITABLE LIQUIDS SUBCATEGORY means an ignitable liquid hazardous waste (waste code D001) which contains
greater than or equal to 10% total organic carbon (TOC) Pursuant to 40 CFR 268 40, such wastes must be treated using organic recovery
(RORGS) or combustion (CMBST) technology. Examples of RORGS technologies include the CES unit at Clean Harbors of Baltimore
Examples of CMBST technologies include hazardous waste fuel blending and subsequent reuse at a cement kiln, or destruction at a RCRA
incinerator
WASTEWATERS are wastes that contain less than 1% by weight total organic carbon (TOC) and less than 1% by weight total suspended
solids (TSS). [See 40 CFR 268.2(f)]
CHI Form LDR-1, Page 3 of 3 [Effective 2128/00]
ATTACHMENT 2
SITE LOCATION MAP
IT A l r ,h Wil• .�¢/ .^
71
Bryan.
N �I( M, `—_�+f — Oc i1 l l•4 ~� O� YVl ,.A
01
Air—
fij Q� S 1 i E
t �►St 1' �y_c
n
4 1�N
Th P�on
1., J s •:�� i £;� o :Ori anage 9
r
B ` 741 '_•� bilMo/ ', f - �\o� � �1'�'.
W, X10 `�\�1 •1 Q �'� z�
thleh
S
P
sx'
Par
9
a • 3 / Park
efk
f v, .`:i,
AVI
APPROXIMATE
N 0 2000 4000
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA (1991)
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
- E
SITE LOCATION MAP
PROJECT
McCORKLE'S CLEANERS
DSCA ID: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE MECKLENBURG COUNTY
hart
2923 TryonSroina2re100
� hiekman
Chazlotte, North Carolina 28211
Charlotte,
704-586-0007 (p) 704-586-0373 .r
SMARTER ENVIRONMENTAL SOLUTIONS
DATE:
6-15-2017
REVISION NO: 0
JOB NO:
DSO -80
ATTACHMENT: 2
ATTACHMENT 3
SITE MAP
LEGEND
\ i / \ ♦ !\• ��' SOURCE PROPERTY BOUNDARY
♦`\ PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
BUILDING
APARTMENTS TYPE II MONITORING WELL
RESIDENCE
RESIDENCE
RESIDENCE
RESIDENCE
RESIDENCE
RESIDENCE
AWA
RESIDENCE
RESIDENCE
*1WA
RESIDENCE
ex\
O
RESIDENCE
RES
NOTES:
1. MONITORING WELLS SURVEYED IN AUGUST 2013,
AND DECEMBER 2015 BY THE ISAACS GROUP.
8
APPROXIMATE
\ 0 80 160
SCALE IN FEET
SITE MAP
♦� PSE" McCORKLE'S CLEANERS
`\ \ DSCA SITE: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
hart''` hickman 2923 South Tryon Street -Suite loo
\ Charlotte, North Carolina 28203
\'\ �` i • 704586-0007(p) 704586-03730
SMARTER ENVIRONMENTAL SOLUT10N5 License # C-1269 / #C-245 Geolc
y�
iFDATE: 6-15-17 REVISION NO. 0
�'�JJOB N0. DSO -80 ATTACHMENT NO. 3
ATTACHMENT 4
GROUNDWATER GRADIENT MAP
APARTMENTS
✓y
:'FORMER MCCOI-ILE'S I i i \
f
i'CLEANERS
v�
0�J I ELIZABETH HOU
MW -1 FLOWERS
60 A MBE E\
2tPs '•♦ OFFICE
W-4
♦ ♦(720.13)
ET NAIL
\\.A
B
TOUE Q
WESTPORT B
& TAL
MW 2
t/(715.25/
*
2tPs '•♦ OFFICE
W-4
♦ ♦(720.13)
/ 'MW -7
(703.48) ^
'�0
RESIDENCE
e
CE
I
or
RESIDENCE O
I• 'AO
RESIDENCE ` RES
RESIDENCE
RESIDENCE
WA
(698.44)
RESIDENCE
RESIDENCE
RESIDENCE '
\ \ \
LEGEND
SOURCE PROPERTY BOUNDARY
------- PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
BUILDING
TYPE II MONITORING WELL
(711.15) GROUNDWATER ELEVATION (FT
MSL)
700 �� GROUNDWATER ELEVATION
CONTOUR (FT MSL)
INFERRED GROUNDWATER FLOW
DIRECTION
NOTES
1. PERMANENT MONITORING WELLS GAUGED ON
4/24/17.
2. MONITORING WELLS SURVEYED IN AUGUST 2013
AND.DECEMBER 2015 BY THE ISAACS GROUP.
a
APPROXIMATE
0 80 160
SCALE IN FEET
GROUNDWATER GRADIENT MAP
SER McCORKLE'S CLEANERS
DSCA SITE: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
hart 2121 South'l'ryon Street -Suite loll
hiekman Charlotte, North Carolina 28203
704-586-0007(p) 704586-03730
SMAUER ENVIf00MAENTAL SOLUi1p05 License # C-1369 / #C-245 Geolc
DATE: 6-15-17 REVISION NO. 0
JOB NO. DSO -80 ATTACHMENT NO. 4
V IOUS RETAIL
r'
r
MW -3 t
(713.32)'.v•
r
/ 'MW -7
(703.48) ^
'�0
RESIDENCE
e
CE
I
or
RESIDENCE O
I• 'AO
RESIDENCE ` RES
RESIDENCE
RESIDENCE
WA
(698.44)
RESIDENCE
RESIDENCE
RESIDENCE '
\ \ \
LEGEND
SOURCE PROPERTY BOUNDARY
------- PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
BUILDING
TYPE II MONITORING WELL
(711.15) GROUNDWATER ELEVATION (FT
MSL)
700 �� GROUNDWATER ELEVATION
CONTOUR (FT MSL)
INFERRED GROUNDWATER FLOW
DIRECTION
NOTES
1. PERMANENT MONITORING WELLS GAUGED ON
4/24/17.
2. MONITORING WELLS SURVEYED IN AUGUST 2013
AND.DECEMBER 2015 BY THE ISAACS GROUP.
a
APPROXIMATE
0 80 160
SCALE IN FEET
GROUNDWATER GRADIENT MAP
SER McCORKLE'S CLEANERS
DSCA SITE: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
hart 2121 South'l'ryon Street -Suite loll
hiekman Charlotte, North Carolina 28203
704-586-0007(p) 704586-03730
SMAUER ENVIf00MAENTAL SOLUi1p05 License # C-1369 / #C-245 Geolc
DATE: 6-15-17 REVISION NO. 0
JOB NO. DSO -80 ATTACHMENT NO. 4
ATTACHMENT 5
GROUNDWATER ISOCONCENTRATION MAPS
APARTMENTS
RMER MCCORKLE'S
EANERS
,ELIZABETH HC
FLOWERS
8 EVE`
`CACHET NAIL
BOUTIQUE
,\ WESTPORT BIG 8 TALL
BENJAMIN MOORE
(BASEMENT)
ss
2
.001
OFFICE
VARIOUS RETAIL
1
\ \ RESIDE
'MWb
0.0409
\x, \
RESIDENCE
RESIDENCE
RESIDENCE
7MW-7
0.00211
RESIDENCE
RESIDENCE \
RESIDENCE
/ RESIDENCE
RESIDENCE /
/
C
.\ r'\ Z ✓ G� /f\� \ \
j i
\ \ \
N'
�' •' \ \ \ \
RES
LEGEND
SOURCE PROPERTY BOUNDARY
------- PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
' BUILDING
TYPE II MONITORING WELL
0.00211 PCE CONCENTRATION IN mg/L
PCE ISOCONTOUR LINE IN mg/L
—0.0007— (DASHED WHERE INFERRED)
NOTES:
1. MONITORING WELLS SAMPLED ON 4/24/17.
2. MW -2D NOT USED IN CONTOURING
a
APPROXIMATE
0 80 160
immimmi
SCALE IN FEET
GROUNDWATER PCE
ISOCONCENTRATION MAP
R° `T McCORKLE'S CLEANERS
DSCA SITE: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
• 7.92.3 South Tryon Street -Suite 100
hart � hickman Charlotte, North Carolina 28203
704-586-0007(p) 70+586-0373(0
SMARTER ENVIRONMENTAL SOLUTIONS license # C-1269 / #C-245 Geok
DATE: 6-15-17 REVISION NO. 0
JOB NO. DSO -80 ATTACHMENT NO. 5A
APARTMENTS
:R MCCORKLE'S
ERS
VARIOUS RETAIL /r
00J I $ ELIZABETH HOUSE
.�� MW -1 FLOWERS
10, -♦ / 10.,W-7
-\
ADAM &EVE`
�e % \
`CACHET NAI
BOUTIQUE
WESTPORT BIG & TALL
r BENJAMIN MOOR
` (BASEMENT)
\`*W4
Q�
w
DO
�G
y�04'
Z' �G
j poi
qv /
RESIDENCE
RESIOEtIFE
RESIDENCE
RESIDENCE
RESIDENCE \
RESIDENCE
RESIDENCE
RESIDENCE
RESIDENCE
®RESIDENCE
O
LEGEND
SOURCE PROPERTY BOUNDARY
------- PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
BUILDING
TYPE II MONITORING WELL
TCE CONCENTRATION IN mg/L
TCE ISOCONTOUR LINE IN mg/L
(DASHED WHERE INFERRED)
NOTES:
1. MONITORING WELLS SAMPLED ON 4/24/17.
2. MW -2D NOT USED IN CONTOURING
8
APPROXIMATE
0 80 160
SCALE IN FEET
i \ GROUNDWATER TICE
ISOCONCENTRATION MAP
PFOJECT
` McCORKLE'S CLEANERS
DSCA SITE: DC600077
O'� \ 1437 SOUTH BOULEVARD
�� `•� CHARLOTTE, MECKLENBURG COUNTY
�. \ ��� • 2923 South Tryon Street -Suite 100
hart hickman Chadotre, North Carolina 28203
\ / 704586-0007(p) 704586-0373(0
\,\ ••,� \\ SNWrtflt ENYNOl�YIENTAL gm- MONS License # C-1269 / #C-245 Geok
,i- DATE: 6-15-17 REVISION N0.0
JOB NO. DSO -80 ATTACHMENT NO. 5B
APARTMENTS
X f
FORMER MCCORKLE'S
/CLEANERS i
eOJ I $ ELIZABETH HC
Mw I 001
5
FLOWERS
,♦
ADAM & EVE`
`CACHET NAIL
BOUTIQU
WWEESTPORT BIG & TALL
BENJAMIN MOORE
(BASEMENT)
.per •\
tissue '•.�\
yGR < A
\ \.<0.001
:l
F
I
OFFICE
VARIOUS RETAIL
0.001 \
RESIDENCE RESIDENCE
RESIDENCE
RESIDENCE
RESIDENCE
MW.6
0.150
RESIDENCE
RESIDENCE
RESIDENCE
1
N
LEGEND
SOURCE PROPERTY BOUNDARY
PROPERTY BOUNDARY
SOURCE PROPERTY BUILDING
BUILDING
-01 TYPE II MONITORING WELL
0.385 CIS-1,2-DCE CONCENTRATION IN
mg/L
-0.07 CIS-1,2-DCE ISOCONTOUR LINE IN
mg/L (DASHED WHERE INFERRED)
NOTES:
1. MONITORING WELLS SAMPLED ON 4124/17-
2 MW -2D NOT USED IN CONTOURING
9
APPROXIMATE
0 80 160
SCALE IN FEET
GROUNDWATER CIS-1,2-DCE
ISOCONCENTRATION MAP
--T McCORKLE'S CLEANERS
DSCA SITE: DC600077
1437 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY
: 2923 South Tryon Street -Suite 1(0
hart
hickman Chadotte,North Carolina28203
704586-0007(p) 704586-0373(1)
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geolc
DATE: 6-15-17 REVISION NO. 0
JOB NO. DSO -80 ATTACHMENT NO. 5C
ATTACHMENT 6
GROUNDWATER CONCENTRATION TREND GRAPHS
0.7
M.
0.5
J
b,0
0.4
0.2
0.1
0
05/06/13
PCE Concentrations vs Time
Monitoring Wells MW -2S and MW -3
McCorkle's Cleaners (DC6OOO77)
11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
03/06/17
09/22/17
—#E-- MW -2S
MW -3
0.045
0.04
0.035
0.03
J
ao
E
r 0.025
0
c 0.02
CU
c
0
U
0.015
0.01
0.005
0
05/06/13
PCE Concentrations vs Time
Monitoring Wells MW -21), MW -5, MW -6, MW -7, and MW -8
McCorkle's Cleaners (DC600077)
11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
09/22/17
MW -2D
--*— M W-5
—A MW -6
—f— M W-8
0.0012
0.001
J
dD
E
C
O
0.0006
L
V
v
0.0004
0.0002
PCE Concentrations vs Time
Monitoring Wells MWA and MW -4
McCorkle's Cleaners (DC600077)
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
--4 MW -1
BMW -4
09/22/17
®.
0.7
Ma
z, 0.5
0o
E
c
0
:_• 0.4
ED
L
c
v
c
0 0.3
0.2
0.1
0
05/06/13
TCE Concentrations vs Time
Monitoring Wells MW -2S and MW -3
McCorkle's Cleaners (DC600077)
11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
--f— MW -2S
09/22/17
I►Il�i��
0.02
0.018
0.016
0.014
J
0.012
c
0
+'r 0.01
L
f+
C
c 0.008
0
v
0.006
0.004
0.002
0
05/06/13
TCE Concentrations vs Time
Monitoring Wells MW -213, MW -4, MW -5, MW -6, MW -7, and MW -8
McCorkle's Cleaners (DC600077)
11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
03/06/17 09/22/17
—MW -2D
—0-- MW -4
—4—MW-5
f MW -6
—0 MW -7
—*— M W -8
cis-1,2-DCE Concentrations vs Time
Monitoring Wells MW -2S
McCorkle's Cleaners (DC6OOO77)
14
12
10
J
bb
E
p
8 ...
C
O
v
C
v
6
v
C
O
U
4
2
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17 09/22/17
Date
1.4
1.2
1
J
ba
0.8
c
0
L
C
Cu 0.6
c
0
u
0.4
0.2
cis-1,2-DCE Concentrations vs Time
Monitoring Wells MW -213 and MW -3
McCorkle's Cleaners (DC600077)
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17 09/22/17
Date
MW -2D
MW -3
0.16
0.14
0.1
an
E
c
0
'Z; 0.08
M
.r
c
v
v
C
0 0.06
0.04
cis-1,2-DCE Concentrations vs Time
Monitoring Wells MW -4, MW -5, MW -6, and MW -8
McCorkle's Cleaners (DC600077)
0.02 ♦''�.1
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
09/22/17
-*-MW-4
—* MW -5
—& MW -6
--41— M W-8
0.4
0.35
0.3
0.25
na
E
C
0
+� 0.2
to
L
c
v
U
C
UO 0.15
0.1
0.05
trans-1,2-13CE Concentrations vs Time
Monitoring Well MW -2S
McCorkle's Cleaners (DC600077)
0 _
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17 09/22/17
Date
MW -2S
0.012
i
0.01
J
C�
C
C
4Z 0.006
c
v
U
0.004
0.002
0
05/06/13
trans-1,2-DCE Concentrations vs Time
Monitoring Wells MW -21), MW -3, and MW -6
McCorkle's Cleaners (DC600077)
11/22/13 06/10/14 12/27/14
07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
MW -3
— A MW -6
09/22/17
0.12
0.1
0.04
0.02
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17 09/22/17
Date
Vinyl Chloride Concentrations vs Time
Monitoring Well MW -2S
McCorkle's Cleaners (DC6OOO77)
Note: Non -detect values are graphed as half the laboratory reporting limit.
- N MW -2S
Vinyl Chloride Concentrations vs Time
Monitoring Wells MW -21) and MW -3
McCorkle's Cleaners (DC600077)
0.005
,1X1 / '.
J
Op
E
c
0
0.003
L
C
V
C
0
U
0.002
0.001
0
05/06/13 11/22/13 06/10/14 12/27/14 07/15/15 01/31/16 08/18/16 03/06/17
Date
Note: Non -detect values are graphed as half the laboratory reporting limit.
09/22/17
MW -2D
MW -3
ATTACHMENT 7
LABORATORY ANALYTICAL REPORT
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: (615)726-0177
TestAmerica Job ID: 490-127126-1
TestAmerica Sample Delivery Group: DSO -80
Client Project/Site: McCorkles Cleaners
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Shane Sisco
Authorized for release by. -
413012017
y.4/30/2017 8:32:24 AM
Ken Hayes, Project Manager II
(615)301-5035
ken. hayes@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
Table of Contents
TestAmenca Job ID 490-127126-1
SDG DSO -80
Cover Page .............................................
1
Table of Contents .................................. ......
2
Sample Summary .......................... .... ........
3
Case Narrative ............... ...... ...................
4
Definitions ...............................................
5
Client Sample Results ........... .......... ....... ......
6
QC Sample Results .......................................
24
QC Association ..... ...................................
39
Chronicle ................................................
40
Method Summary ....................... ....... .. ....
42
Certification Summary .................. ...................
43
Chain of Custody .........................................
44
Receipt Checklists .........................................
46
TestAmenca Nashville
Page 2 of 46 4/30/2017
Sample Summary
Client Hart & Hickman, PC
TestAmerica Job ID 490-127126-1
Project/Site
McCorkles Cleaners
SDG DSO -80
Lab Sample ID
Client Sample ID
Matrix
Collected Received
490-127126-1
MW -1
Water
04/24/17 08 55 04/26/17 09 20
490-127126-2
MW -2S
Water
04/24/17 11 00 04/26/17 09 20
490-127126-3
MW -21D
Water
04/24/17 10 25 04/26/17 09 20
490-127126-4
MW -3
Water
04/24/17 09 45 04/26/17 09 20
490-127126-5
MW -4
Water
04/24/17 12 25 04/26/17 09 20
490-127126-6
MW -5
Water
04/24/17 14 45 04/26/17 09 20
490-127126-7
MW -6
Water
04/24/17 15 30 04/26/17 09 20
490-127126-8
MW -7
Water
04/24/17 16 30 04/26/17 09 20
490-127126-9
MW -8
Water
04/24/17 17 20 04/26/17 09 20
TestAmerica Nashville
Page 3 of 46 4/30/2017
Case Narrative
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Job ID: 490-127126-1
Laboratory: TestAmerica Nashville
Narrative
f 4
Job Narrative
L --:—j
490-127126-1
Comments
No additional comments
Receipt
The samples were received on 4/26/2017 9 20 AM, the samples arrived in good condition, properly preserved and, where required, on ice
The temperature of the cooler at receipt was 1 3° C
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
TestAmenca Nashville
Page 4 of 46 4/30/2017
Definitions/Glossary
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
Qualifiers
TestAmenca Job ID 490-127126-1
SDG DSO -80
GC/MS VOA
Qualifier Qualifier Description
4 MS, MSD The analyte present in the original sample is greater than 4 times the matrix spike concentration, therefore, control limits are not
applicable
F2 MS/MSD RPD exceeds control limits
Glossa
Abbreviation
a
%R
CFL
CNF
DER
Dil Fac
DL, RA, RE, IN
DLC
MDA
EDL
MDC
MDL
ML
NC
ND
PQL
QC
RER
RL
RPD
TEF
TEQ
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains no Free Liquid
Duplicate error ratio (normalized absolute difference)
Dilution Factor
Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
Decision level concentration
Minimum detectable activity
Estimated Detection Limit
Minimum detectable concentration
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
Relative error ratio
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
TestAmenca Nashville
Page 5 of 46 4/30/2017
TestAmenca Nashville
Page 6 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
TestAmenca Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG
DSO -80
Client Sample ID: MW -1
Lab Sample ID: 490-127126-1
Date Collected: 04/24/17 08:55
Matrix: Water
Date Received: 04/26/17 09:20
Method: 82608 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
DII Fac
Acetone
ND
250
ug/L
04/28/17 14 14
1
Benzene
ND
100
ug/L
04/28/17 14 14
1 •
Bromobenzene
ND
100
ug/L
04/28/17 14 14
1
Bromochloromethane
ND
100
ug/L
04/28/17 14 14
1
Bromodichloromethane
ND
100
ug/L
04/28/17 14 14
1
Bromoform
ND
100
ug/L
04/28/171414
1
Bromomethane
ND
100
ug/L
04/28/17 14 14
1
2-Butanone (MEK)
ND
500
ug/L
04/28/17 14 14
1
Carbon disulfide
ND
1 00
ug/L
04/28/17 14 14
1
Carbon tetrachloride
ND
1 00
ug/L
04/28/17 14 14
1
Chlorobenzene
ND
100
ug/L
04/28/17 14 14
1
Chlorodibromomethane
ND
100
ug/L
04/28/17 14 14
1
Chloroethane
ND
100
ug/L
04/28/171414
1
Chloroform
ND
100
ug/L
04/28/17 14 14
1
Chloromethane
ND
100
ug/L
04/28/17 14 14
1
2-Chlorotoluene
ND
100
ug/L
04/28/17 14 14
1
4-Chlorotoluene
ND
100
ug/L
04/28/17 14 14
1
as-1,2-Dichloroethene
ND
100
ug/L
04/28/17 14 14
1
as-1,3-Dlchloropropene
ND
100
ug/L
04/28/17 14 14
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/28/17 14 14
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/28/17 14 14
1
Dibromomethane
ND
100
ug/L
04/28/171414
1
1,2 -Dichlorobenzene
ND
100
ug/L
04/28/17 14 14
1
1,3 -Dichlorobenzene
ND
100
ug/L
04/28/17 14 14
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/28/17 14 14
1
Dichlorodifluoromethane
ND
100
ug/L
04/28/17 14 14
1
1,1-Dichloroethane
ND
100
ug/L
04/28/17 14 14
1
1,2-Dichloroethane
ND
100
ug/L
04/28/17 14 14
1
1,1-Dichloroethene
ND
100
ug/L
04/28/17 14 14
1
1,2-Dichloroethene, Total
ND
1 00
ug/L
04/28/17 14 14
1
1,2-Dichloropropane
ND
100
ug/L
04/28/17 14 14
1
1,3-Dichloropropane
ND
100
ug/L
04/28/17 14 14
1
2,2-Dichloropropane
ND
100
ug/L
04/28/17 14 14
1
1,1-Dichloropropene
ND
100
ug/L
04/28/17 14 14
1
Dnsopropyl ether
ND
200
ug/L
04/28/17 14 14
1
Ethylbenzene
ND
100
ug/L
04/28/17 14 14
1
Hexachlorobutadiene
ND
200
ug/L
04/28/17 14 14
1
2-Hexanone
ND
100
ug/L
04/28/17 14 14
1
Isopropylbenzene
ND
100
ug/L
04/28/17 14 14
1
Methylene Chloride
ND
500
ug/L
04/28/17 14 14
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/28/17 14 14
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/28/17 14 14
1
Naphthalene
ND
500
ug/L
04/28/17 14 14
1
n-Butylbenzene
ND
100
ug/L
04/28/17 14 14
1
N-Propylbenzene
ND
100
ug/L
04/28/17 14 14
1
p-Isopropyltoluene
ND
100
ug/L
04/28/17 14 14
1
sec-Butylbenzene
ND
100
ug/L
04/28/17 14 14
1
Styrene
ND
100
ug/L
04/28/17 14 14
1
tert-Butyl benzene
ND
100
ug/L
04/28/17 14 14
1
TestAmenca Nashville
Page 6 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -1
Lab Sample ID: 490-127126-1
Date Collected: 04/24/17 08:55
Matrix: Water
Date Received: 04/26/17 09:20
Method: 82606 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dd Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
100
100
ug/L
ug/L
04/28/171414
04/28/17 14 14
1
1
Tetrachloroethene
ND
100
ug/L
04/28/17 14 14
1
Toluene
ND
100
ug/L
04/28/17 14 14
1
trans-1,2-Dichloroethene
ND
100
ug/L
04/28/17 14 14
1
trans-1,3-Dichloropropene
ND
100
ug/L
04/28/17 14 14
1
1,2,3-Tnchlorobenzene
ND
100
ug/L
04/28/17 14 14
1
1,2,4-Tnchlorobenzene
ND
100
ug/L
04/28/17 14 14
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/28/17 14 14
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/28/17 14 14
1
1,4 -Dioxane
ND
200
ug/L
04/28/17 14 14
1
Trichloroethene
ND
100
ug/L
04/28/17 14 14
1
Trichlorofluoromethane
ND
100
ug/L
04/28/17 14 14
1
1,2,3-Tnchloropropane
ND
100
ug/L
04/28/17 14 14
1
1,2,4 -Tri methyl benzene
ND
100
ug/L
04/28/17 14 14
1
1,3,5 -Tri methyl benzene
ND
100
ug/L
04/28/17 14 14
1
Vinyl chloride
ND
1 00
ug/L
04/28/17 14 14
1
Xylenes, Total
ND
300
ug/L
04/28/17 14 14
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
95
70-130
04/28/17 14 14
1
Dibromofluoromethane (Surr)
94
70-130
04/28/17 14 14
1
1,2-Dichloroethane-d4 (Surr)
98
70-130
04/28/17 14 14
1
Toluene -d8 (Surr)
103
70-130
04/28/17 14 14
1
TestAmenca Nashville
Page 7 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -2S
Lab Sample ID: 490-127126-2
Date Collected: 04/24/17 11:00
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dd Fac
Acetone
ND
250
ug/L
04/27/17 14 40
1
Benzene
ND
1 00
ug/L
04/27/17 14 40
1 •
Bromobenzene
ND
1 00
ug/L
04/27/17 14 40
1
Bromochloromethane
ND
1 00
ug/L
04/27/17 14 40
1
Bromodichloromethane
ND
1 00
ug/L
04/27/17 14 40
1
Bromoform
ND
1 00
ug/L
04/27/17 14 40
1
Bromomethane
ND
1 00
ug/L
04/27/17 14 40
1
2-Butanone (MEK)
1350
500
ug/L
04/27/17 14 40
1
Carbon disulfide
ND
1 00
ug/L
04/27/17 14 40
1
Carbon tetrachloride
ND
1 00
ug/L
04/27/17 14 40
1
Chlorobenzene
ND
1 00
ug/L
04/27/17 14 40
1
Chlorodibromomethane
ND
1 00
ug/L
04/27/17 14 40
1
Chloroethane
ND
1 00
ug/L
04/27/17 14 40
1
Chloroform
ND
1 00
ug/L
04/27/17 14 40
1
Chloromethane
ND
1 00
ug/L
04/27/17 14 40
1
2-Chlorotoluene
ND
1 00
ug/L
04/27/17 14 40
1
4-Chlorotoluene
ND
1 00
ug/L
04/27/17 14 40
1
cis-1,2-Dichloroethene
10300
500
ug/L
04/28/17 18 43
50
cis-1,3-Dichloropropene
ND
100
ug/L
04/27/17 14 40
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/27/17 14 40
1
1,2-Dibromoethane(EDB)
ND
100
ug/L
04/27/17 14 40
1
Dibromomethane
ND
1 00
ug/L
04/27/17 14 40
1
1,2 -Dichlorobenzene
ND
100
ug/L
04/27/17 14 40
1
1,3 -Dichlorobenzene
ND
100
ug/L
04/27/17 14 40
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/27/17 14 40
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/27/17 14 40
1
1,1-Dichloroethane
264
1 00
ug/L
04/27/17 14 40
1
1,2-Dichloroethane
ND
100
ug/L
04/27/17 14 40
1
1,1-Dichloroethene
209
1 00
ug/L
04/27/17 14 40
1
1,2-Dichloroethene, Total
2240
1 00
ug/L
04/27/17 14 40
1
1,2-Dichloropropane
ND
100
ug/L
04/27/17 14 40
1
1,3-Dichloropropane
ND
100
ug/L
04/27/17 14 40
1
2,2-Dichloropropane
ND
1 00
ug/L
04/27/17 14 40
1
1,1-Dichloropropene
ND
100
ug/L
04/27/17 14 40
1
Diisopropyl ether
ND
2 00
ug/L
04/27/17 14 40
1
Ethylbenzene
ND
1 00
ug/L
04/27/17 14 40
1
Hexachlorobutadiene
ND
2 00
ug/L
04/27/17 14 40
1
2-Hexanone
ND
100
ug/L
04/27/17 14 40
1
Isopropylbenzene
149
1 00
ug/L
04/27/17 14 40
1
Methylene Chloride
ND
500
ug/L
04/27/17 14 40
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/27/17 14 40
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/27/17 14 40
1
Naphthalene
ND
500
ug/L
04/27/17 14 40
1
n-Butylbenzene
595
1 00
ug/L
04/27/17 14 40
1
N-Propylbenzene
195
1 00
ug/L
04/27/17 14 40
1
p-Isopropyltoluene
ND
1 00
ug/L
04/27/17 14 40
1
sec-Butylbenzene
177
1 00
ug/L
04/27/17 14 40
1
Styrene
ND
1 00
ug/L
04/27/17 14 40
1
tert-Butylbenzene
433
1 00
ug/L
04/27/17 14 40
1
TestAmerica Nashville
Page 8 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -2S
Lab Sample ID: 490-127126-2
Date Collected: 04/24/17 11:00
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
100
100
ug/L
ug/L
04/27/17 14 40
04/27/17 14 40
1
1
Tetrachloroethene
ND
1 00
ug/L
04/27/17 14 40
1
Toluene
ND
1 00
ug/L
04/27/17 14 40
1
trans-1,2-Dichloroethene
200
1 00
ug/L
04/27/17 14 40
1
trans-1,3-Dichloropropene
ND
100
ug/L
04/27/17 14 40
1
1,2,3-Tnchlorobenzene
ND
100
ug/L
04/27/17 14 40
1
1,2,4-Tnchlorobenzene
ND
1 00
ug/L
04/27/17 14 40
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/27/17 14 40
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/27/17 14 40
1
1,4 -Dioxane
ND
200
ug/L
04/27/17 14 40
1
Trichloroethene
ND
1 00
ug/L
04/27/17 14 40
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 14 40
1
1,2,3-Trichloropropane
ND
100
ug/L
04/27/17 14 40
1
1,2,4-Tnmethylbenzene
313
100
ug/L
04/27/17 14 40
1
1,3,5-Tnmethylbenzene
ND
100
ug/L
04/27/17 14 40
1
Vinyl chloride
152
1 00
ug/L
04/27/17 14 40
1
Xylenes, Total
333
300
ug/L
04/27/17 14 40
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
110
70-130
04/27/17 14 40
1
4-Bromofluorobenzene (Surf)
97
70-130
04/28/17 18 43
50
Dlbromofluoromethane (Surr)
105
70-130
04/27/17 14 40
1
Dibromofluoromethane (Surr)
92
70-130
04128/17 18 43
50
1,2-Dichloroethane-d4 (Surr)
106
70-130
04/27/17 14 40
1
1,2-Dichloroethane-d4 (Surr)
100
70-130
0428/17 18 43
50
Toluene -d8 (Surr)
97
70-130
0427/17 14 40
1
Toluene -d8 (Surr)
107
70-130
0428/17 18 43
50
TestAmenca Nashville
Page 9 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -2131
Lab Sample ID: 490-127126-3
Date Collected: 04/24/17 10:25
Matrix:
Water
Date Received: 04/26/17 09:20
Method. 82608 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/28/17 14 38
1
Benzene
ND
1 00
ug/L
04/28/17 14 38
1 •
Bromobenzene
ND
1 00
ug/L
04/28/17 14 38
1
Bromochloromethane
ND
1 00
ug/L
04/28/17 14 38
1
Bromodichloromethane
ND
1 00
ug/L
04/28/17 14 38
1
Bromoform
ND
1 00
ug/L
04/28/17 14 38
1
Bromomethane
ND
1 00
ug/L
04/28/17 14 38
1
2-Butanone (MEK)
ND
500
ug/L
04/28/17 14 38
1
Carbon disulfide
ND
1 00
ug/L
04/28/17 14 38
1
Carbon tetrachloride
ND
1 00
ug/L
04/28/17 14 38
1
Chlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
Chlorodibromomethane
ND
1 00
ug/L
04/28/17 14 38
1
Chloroethane
ND
1 00
ug/L
04/28/17 14 38
1
Chloroform
244
1 00
ug/L
04/28/17 14 38
1
Chloromethane
ND
1 00
ug/L
04/28/17 14 38
1
2-Chlorotoluene
ND
1 00
ug/L
04/28/17 14 38
1
4-Chlorotoluene
ND
1 00
ug/L
04/28/17 14 38
1
cis-1,2-Dichloroethene
193
1 00
ug/L
04/28/17 14 38
1
cis- 1,3-Dichloropropene
ND
1 00
ug/L
04/28/17 14 38
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/28/17 14 38
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/28/17 14 38
1
Dibromomethane
ND
1 00
ug/L
04/28/17 14 38
1
1,2 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
1,4 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/28/17 14 38
1
1,1-Dichloroethane
ND
100
ug/L
04/28/17 14 38
1
1,2-Dichloroethane
ND
100
ug/L
04/28/17 14 38
1
1,1-Dichloroethene
ND
100
ug/L
04/28/17 14 38
1
1,2-Dichloroethene, Total
196
1 00
ug/L
04/28/17 14 38
1
1,2-Dichloropropane
ND
100
ug/L
04/28/17 14 38
1
1,3-Dichloropropane
ND
100
ug/L
04/28/17 14 38
1
2,2-Dichloropropane
ND
1 00
ug/L
04/28/17 14 38
1
1,1-Dichloropropene
ND
1 00
ug/L
04/28/17 14 38
1
Diisopropyl ether
ND
2 00
ug/L
04/28/17 14 38
1
Ethylbenzene
ND
1 00
ug/L
04/28/17 14 38
1
Hexachlorobutadiene
ND
200
ug/L
04/28/17 14 38
1
2-Hexanone
ND
100
ug/L
04/28/17 14 38
1
Isopropyl benzene
ND
1 00
ug/L
04/28/17 14 38
1
Methylene Chloride
ND
500
ug/L
04/28/17 14 38
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/28/17 14 38
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/28/17 14 38
1
Naphthalene
ND
500
ug/L
04/28/17 14 38
1
n-Butylbenzene
ND
1 00
ug/L
04/28/17 14 38
1
N-Propylbenzene
ND
1 00
ug/L
04/28/17 14 38
1
p-Isopropyltoluene
ND
1 00
ug/L
04/28/17 14 38
1
sec-Butylbenzene
ND
1 00
ug/L
04/28/17 14 38
1
Styrene
ND
1 00
ug/L
04/28/17 14 38
1
tert-Butylbenzene
ND
1 00
ug/L
04/28/17 14 38
1
TestAmenca Nashville
Page 10 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerlca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -2D
Lab Sample ID: 490-127126-3
Date Collected: 04/24/17 10:25
Matrix: Water
Date Received: 04/26/17 09:20
Method: 82606 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dd Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
100
100
ug/L
ug/L
04/28/17 14 38
04/28/17 14 38
1
1
Tetrachloroethene
785
1 00
ug/L
04/28/17 14 38
1
Toluene
ND
1 00
ug/L
04/28/17 14 38
1
trans-1,2-Dichloroethene
292
1 00
ug/L
04/28/17 14 38
1
trans-1,3-Dichloropropene
ND
100
ug/L
04/28/17 14 38
1
1,2,3-Trichlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
1,2,4-Tnchlorobenzene
ND
1 00
ug/L
04/28/17 14 38
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/28/17 14 38
1
1,1,2-Tnchloroethane
ND
100
ug/L
04/28/171438
1
1,4 -Dioxane
ND
200
ug/L
04/28/17 14 38
1
Trichloroethene
2 08
1 00
ug/L
04/28/17 14 38
1
Trichlorofluoromethane
ND
1 00
ug/L
04/28/17 14 38
1
1,2,3-Trichloropropane
ND
100
ug/L
04/28/17 14 38
1
1,2,4 -Tri methyl benzene
ND
1 00
ug/L
04/28/17 14 38
1
1,3,5 -Tri methyl benzene
ND
1 00
ug/L
04/28/17 14 38
1
Vinyl chloride
ND
1 00
ug/L
04/28/17 14 38
1
Xylenes, Total
ND
300
ug/L
04/28/17 14 38
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Suri)
95
70-130
04/28/17 14 38
1
Dlbromofluoromethane (Surr)
93
70-130
04/28/17 14 38
1
1,2-Dichloroethane-d4 (Surr)
98
70-130
04/28/17 14 38
1
Toluene -d8 (Surr)
105
70-130
0428/17 14 38
1
TestAmerlca Nashville
Page 11 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -3
Lab Sample ID: 490-127126-4
Date Collected: 04/24/17 09:45
Matrix: plater
Date Received: 04/26/17 09:20
Method: 82608 - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dd Fac
Acetone
ND
250
ug/L
04/27/17 15 06
1
Benzene
ND
1 00
ug/L
04/27/17 15 06
1 •
Bromobenzene
ND
1 00
ug/L
04/27/17 15 06
1
Bromochloromethane
ND
1 00
ug/L
04/27/17 15 06
1
Bromodichloromethane
ND
1 00
ug/L
04/27/17 15 06
1
Bromoform
ND
1 00
ug/L
04/27/17 15 06
1
Bromomethane
ND
1 00
ug/L
04/27/17 15 06
1
2-Butanone (MEK)
ND
500
ug/L
04/27/17 15 06
1
Carbon disulfide
ND
1 00
ug/L
04/27/17 15 06
1
Carbon tetrachlonde
ND
1 00
ug/L
04/27/17 15 06
1
Chlorobenzene
ND
1 00
ug/L
04/27/17 15 06
1
Chlorodibromomethane
ND
1 00
ug/L
04/27/17 15 06
1
Chloroethane
ND
1 00
ug/L
04/27/17 15 06
1
Chloroform
ND
1 00
ug/L
04/27/17 15 06
1
Chloromethane
ND
1 00
ug/L
04/27/17 15 06
1
2-Chlorotoluene
ND
1 00
ug/L
04/27/17 15 06
1
4-Chlorotoluene
ND
1 00
ug/L
04/27/17 15 06
1
cis-1,2-Dichloroethene
385
1 00
ug/L
04/28/17 15 03
1
cis-1,3-Dichloropropene
ND
100
ug/L
04/27/17 15 06
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/27/17 15 06
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/27/17 15 06
1
Dibromomethane
ND
1 00
ug/L
04/27/17 15 06
1
1,2 -Dichlorobenzene
ND
100
ug/L
04/27/17 15 06
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 15 06
1
1,4 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 15 06
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/27/17 15 06
1
1,1-Dichloroethane
270
1 00
ug/L
04/27/17 15 06
1
1,2-Dichloroethane
ND
1 00
ug/L
04/27/17 15 06
1
1,1-Dichloroethene
1 97
1 00
ug/L
04/27/17 15 06
1
1,2-Dichloroethene, Total
326
1 00
ug/L
04/27/17 15 06
1
1,2-Dichloropropane
ND
1 00
ug/L
04/27/17 15 06
1
1,3-Dichloropropane
ND
1 00
ug/L
04/27/17 15 06
1
2,2-Dichloropropane
ND
1 00
ug/L
04/27/17 15 06
1
1,1-Dichloropropene
ND
1 00
ug/L
04/27/17 15 06
1
Dusopropyl ether
ND
200
ug/L
04/27/17 15 06
1
Ethylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
Hexachlorobutadiene
ND
2 00
ug/L
04/27/17 15 06
1
2-Hexanone
ND
100
ug/L
04/27/17 15 06
1
Isopropylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
Methylene Chloride
ND
500
ug/L
04/27/17 15 06
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/27/17 15 06
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/27/17 15 06
1
Naphthalene
ND
500
ug/L
04/27/17 15 06
1
n-Butylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
N-Propylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
p-Isopropyltoluene
ND
1 00
ug/L
04/27/17 15 06
1
sec-Butylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
Styrene
ND
1 00
ug/L
04/27/17 15 06
1
tert-Butylbenzene
ND
1 00
ug/L
04/27/17 15 06
1
TestAmenca Nashville
Page 12 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -3
Lab Sample ID: 490-127126-4
Date Collected: 04/24/17 09:45
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dd Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
1 00
1 00
ug/L
ug/L
04/27/17 15 06
04/27/17 15 06
1
1 •
Tetrachloroethene
113
1 00
ug/L
04/27/17 15 06
1
Toluene
ND
1 00
ug/L
04/27/17 15 06
1
trans-1,2-Dichloroethene
474
1 00
ug/L
04/27/17 15 06
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 15 06
1
1,2,3 -Tri ch lorobenzene
ND
1 00
ug/L
04/27/17 15 06
1
1,2,4-Trichlorobenzene
ND
1 00
ug/L
04/27/17 15 06
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/27/17 15 06
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/27/17 15 06
1
1,4 -Dioxane
ND
200
ug/L
04/27/17 15 06
1
Trichloroethene
50 7
1 00
ug/L
04/27/17 15 06
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 15 06
1
1,2,3-Tnchloropropane
ND
1 00
ug/L
04/27/17 15 06
1
1,2,4-Tnmethylbenzene
ND
100
ug/L
04/27117 15 06
1
1,3,5 -Tri methyl benzene
ND
100
ug/L
04/27/17 15 06
1
Vinyl chloride
ND
1 00
ug/L
04/27/17 15 06
1
Xylenes, Total
ND
300
ug/L
04/27/17 15 06
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Sun)
99
70-130
04/27/17 15 06
1
4-Bromofluorobenzene (Sun)
95
70-130
04/28/17 15 03
1
Dibromofluoromethane (Sun)
99
70-130
04127/17 15 06
1
Dibromofluoromethane (Sun)
94
70-130
04128/17 15 03
1
1,2-Dichloroethane-d4 (Surr)
101
70-130
04127/17 15 06
1
1,2-Dichloroethane-d4 (Surr)
95
70-130
04128/17 15 03
1
Toluene -d8 (Surr)
101
70-130
04127/17 15 06
1
Toluene -d8 (Surr)
105
70-130
04128/17 15 03
1
TestAmerica Nashville
Page 13 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -4
Lab Sample ID: 490-127126-5
Date Collected: 04/24/17 12:25
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dd Fac
Acetone
ND
250
ug/L
04/28/17 15 27
1
Benzene
ND
1 00
ug/L
04/28/17 15 27
1
Bromobenzene
ND
1 00
ug/L
04/28/17 15 27
1
Bromochloromethane
ND
1 00
ug/L
04/28/17 15 27
1
Bromodichloromethane
ND
1 00
ug/L
04/28/17 15 27
1
Bromoform
ND
1 00
ug/L
04/28/17 15 27
1
Bromomethane
ND
1 00
ug/L
04/28/17 15 27
1
2-Butanone (MEK)
ND
500
ug/L
04/28/17 15 27
1
Carbon disulfide
ND
1 00
ug/L
04/28/17 15 27
1
Carbon tetrachloride
ND
1 00
ug/L
04/28/17 15 27
1
Chlorobenzene
ND
1 00
ug/L
04/28/17 15 27
1
Chlorodibromomethane
ND
1 00
ug/L
04/28/17 15 27
1
Chloroethane
ND
1 00
ug/L
04/28/17 15 27
1
Chloroform
ND
1 00
ug/L
04/28/17 15 27
1
Chloromethane
ND
1 00
ug/L
04/28/17 15 27
1
2-Chlorotoluene
ND
1 00
ug/L
04/28/17 15 27
1
4-Chlorotoluene
ND
1 00
ug/L
04/28/17 15 27
1
cis-1,2-Dichloroethene
ND
100
ug/L
04/28/17 15 27
1
as-1,3-Dichloropropene
ND
100
ug/L
04/28/17 15 27
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/28/17 15 27
1
1,2-Dibromoethane(EDB)
ND
100
ug/L
04/28/17 15 27
1
Dibromomethane
ND
1 00
ug/L
04/28/17 15 27
1
1,2 -Dichlorobenzene
ND
100
ug/L
04/28/17 15 27
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 15 27
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/28/17 15 27
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/28/17 15 27
1
1,1-Dichloroethane
ND
100
ug/L
04/28/17 15 27
1
1,2-Dichloroethane
ND
1 00
ug/L
04/28/17 15 27
1
1,1-Dichloroethene
ND
100
ug/L
04/28/17 15 27
1
1,2-Dichloroethene, Total
ND
1 00
ug/L
04/28/17 15 27
1
1,2-Dichloropropane
ND
100
ug/L
04/28/17 15 27
1
1,3-Dichloropropane
ND
100
ug/L
04/28/17 15 27
1
2,2-Dichloropropane
ND
1 00
ug/L
04/28/17 15 27
1
1,1-Dichloropropene
ND
1 00
ug/L
04/28/17 15 27
1
Diisopropyl ether
ND
200
ug/L
04/28/17 15 27
1
Ethylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
Hexachlorobutadiene
ND
2 00
ug/L
04/28/17 15 27
1
2-Hexanone
ND
100
ug/L
04/28/17 15 27
1
Isopropylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
Methylene Chloride
ND
500
ug/L
04/28/17 15 27
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/28/17 15 27
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/28/17 15 27
1
Naphthalene
ND
500
ug/L
04/28/17 15 27
1
n-Butylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
N-Propylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
p-Isopropyltoluene
ND
1 00
ug/L
04/28/17 15 27
1
sec-Butylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
Styrene
ND
1 00
ug/L
04/28/17 15 27
1
tert-Butyl benzene
ND
1 00
ug/L
04/28/17 15 27
1
TestAmenca Nashville
Page 14 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -4
Lab Sample ID: 490-127126-5
Date Collected: 04/24/17 12:25
Matrix: Water
Date Received: 04/26/17 09:20
Method: 82606 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dd Fac
1,1,1,2 -Tetrachloroethane
ND
1 00
ug/L
04/28/17 15 27
1
1,1,2,2 -Tetrachloroethane
ND
1 00
ug/L
04/28/17 15 27
1
Tetrachloroethene
ND
1 00
ug/L
04/28/17 15 27
1
Toluene
ND
1 00
ug/L
04/28/17 15 27
1
trans-1,2-Dichloroethene
ND
100
ug/L
04/28/17 15 27
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/28/17 15 27
1
1,2,3-Trichlorobenzene
ND
1 00
ug/L
04/28/17 15 27
1
1,2,4-Trichlorobenzene
ND
100
ug/L
04/28/17 15 27
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/28/17 15 27
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/28/17 15 27
1
1,4 -Dioxane
ND
200
ug/L
04/28/17 15 27
1
Trichloroethene
ND
1 00
ug/L
04/28/17 15 27
1
Trichlorofluoromethane
ND
1 00
ug/L
04/28/17 15 27
1
1,2,3-Trichloropropane
ND
1 00
ug/L
04/28/17 15 27
1
1,2,4-Tnmethylbenzene
ND
100
ug/L
04/28/17 15 27
1
1,3,5-Tnmethylbenzene
ND
1 00
ug/L
04/28/17 15 27
1
Vinyl chloride
ND
1 00
ug/L
04/28/17 15 27
1
Xylenes, Total
ND
300
ug/L
04/28/17 15 27
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dd Fac
4-Bromofluorobenzene (Surr)
96
70-130
04/28/17 15 27
1
Dibromofluoromethane (Surr)
91
70-130
04128/17 15 27
1
1,2-Dichloroethane-d4 (Surr)
98
70-130
04128/17 15 27
1
Toluene -d8 (Surr)
104
70-130
0428/17 15 27
1
TestAmenca Nashville
Page 15 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -5
Lab Sample ID: 490-127126-6
Date Collected: 04/24/17 14:45
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/27/17 15 32
1
Benzene
ND
1 00
ug/L
04/27/17 15 32
1
Bromobenzene
ND
1 00
ug/L
04/27/17 15 32
1
Bromochloromethane
ND
1 00
ug/L
04/27/17 15 32
1
Bromodichloromethane
ND
1 00
ug/L
04/27/17 15 32
1
Bromoform
ND
1 00
ug/L
04/27/17 15 32
1
Bromomethane
ND
1 00
ug/L
04/27/17 15 32
1
2-Butanone (MEK)
ND
500
ug/L
04/27/17 15 32
1
Carbon disulfide
ND
1 00
ug/L
04/27/17 15 32
1
Carbon tetrachloride
ND
1 00
ug/L
04/27/17 15 32
1
Chlorobenzene
ND
1 00
ug/L
04/27/17 15 32
1
Chlorodibromomethane
ND
1 00
ug/L
04/27/17 15 32
1
Chloroethane
ND
1 00
ug/L
04/27/17 15 32
1
Chloroform
ND
1 00
ug/L
04/27/17 15 32
1
Chloromethane
ND
1 00
ug/L
04/27/17 15 32
1
2-Chlorotoluene
ND
1 00
ug/L
04/27/17 15 32
1
4-Chlorotoluene
ND
1 00
ug/L
04/27/17 15 32
1
cis-1,2-Dichloroethene
ND
1 00
ug/L
04/28/17 15 52
1
cis-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 15 32
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/27/17 15 32
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/27/17 15 32
1
Dibromomethane
ND
1 00
ug/L
04/27/17 15 32
1
1,2 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 15 32
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 15 32
1
1,4 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 15 32
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/27/17 15 32
1
1,1-Dichloroethane
ND
1 00
ug/L
04/27/17 15 32
1
1,2-Dichloroethane
ND
1 00
ug/L
04/27/17 15 32
1
1,1-Dichloroethene
ND
1 00
ug/L
04/27/17 15 32
1
1,2-Dichloroethene, Total
1 91
1 00
ug/L
04/27/17 15 32
1
1,2-Dichloropropane
ND
1 00
ug/L
04/27/17 15 32
1
1,3-Dichloropropane
ND
1 00
ug/L
04/27/17 15 32
1
2,2-Dichloropropane
ND
1 00
ug/L
04/27/17 15 32
1
1,1-Dichloropropene
ND
1 00
ug/L
04/27/17 15 32
1
Dnsopropyl ether
ND
2 00
ug/L
04/27/17 15 32
1
Ethylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
Hexachlorobutadiene
ND
2 00
ug/L
04/27/17 15 32
1
2-Hexanone
ND
100
ug/L
04/27/17 15 32
1
Isopropylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
Methylene Chloride
ND
500
ug/L
04/27/17 15 32
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/27/17 15 32
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/27/17 15 32
1
Naphthalene
ND
500
ug/L
04/27/17 15 32
1
n-Butylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
N-Propylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
p-Isopropyltoluene
ND
1 00
ug/L
04/27/17 15 32
1
sec-Butylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
Styrene
ND
1 00
ug/L
04/27/17 15 32
1
tert-Butylbenzene
ND
1 00
ug/L
04/27/17 15 32
1
TestAmenca Nashville
Page 16 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -5
Lab Sample ID: 490-127126-6
Date Collected: 04/24/17 14:45
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
1 00
100
ug/L
ug/L
04/27/17 15 32
04/27/17 15 32
1
1
Tetra chloroethene
ND
1 00
ug/L
04/27/17 15 32
1
Toluene
ND
1 00
ug/L
04/27/17 15 32
1
trans-1,2-Dichloroethene
ND
1 00
ug/L
04/27/17 15 32
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 15 32
1
1,2,3-Tnchlorobenzene
ND
100
ug/L
04/27/17 15 32
1
1,2,4-Trichlorobenzene
ND
100
ug/L
04/27/17 15 32
1
1,1,1 -Trichloroethane
ND
1 00
ug/L
04/27/17 15 32
1
1,1,2 -Trichloroethane
ND
1 00
ug/L
04/27/17 15 32
1
1,4 -Dioxane
ND
200
ug/L
04/27/17 15 32
1
Trichloroethene
ND
1 00
ug/L
04/27/17 15 32
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 15 32
1
1,2,3-Trichloropropane
ND
100
ug/L
04/27/17 15 32
1
1,2,4-Trimethylbenzene
ND
100
ug/L
04/27/17 15 32
1
1,3,5-Tnmethylbenzene
ND
100
ug/L
04/27/17 15 32
1
Vinyl chloride
ND
1 00
ug/L
04/27/17 15 32
1
Xylenes, Total
ND
300
ug/L
04/27/17 15 32
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
102
70-130
04/27/17 15 32
1
4-Bromofluorobenzene (Surr)
95
70-130
04/28/17 15 52
1
Dibromofluoromethane (Suri)
97
70-130
04/27/17 15 32
1
Dibromofluoromethane (Surr)
94
70-130
04128/17 15 52
1
1,2-Dichloroethane-d4 (Surr)
105
70-130
04/27/17 15 32
1
1,2-Dichloroethane-d4 (Surr)
101
70-130
04/28/17 15 52
1
Toluene -d8 (Surr)
100
70-130
04/27/17 15 32
1
Toluene -d8 (Surr)
104
70-130
0428/17 15 52
1
TestAmenca Nashville
Page 17 of 46 4/30/2017
TestAmenca Nashville
Page 18 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
TestAmenca Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG
DSO -80
Client Sample ID: MW -6
Lab Sample ID: 490-127126-7
Date Collected: 04/24/17 15:30
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/28/17 16 16
1
Benzene
ND
100
ug/L
04/28/17 16 16
1 •
Bromobenzene
ND
100
ug/L
04/28/17 16 16
1
Bromochloromethane
ND
100
ug/L
04/28/17 16 16
1
Bromodichloromethane
ND
100
ug/L
04/28/17 16 16
1
Bromoform
ND
100
ug/L
04/28/17 16 16
1
Bromomethane
ND
100
ug/L
04/28/17 16 16
1
2-Butanone (MEK)
ND
500
ug/L
04/28/17 16 16
1
Carbon disulfide
ND
1 00
ug/L
04/28/17 16 16
1
Carbon tetrachloride
ND
1 00
ug/L
04/28/17 16 16
1
Chlorobenzene
ND
100
ug/L
04/28/17 16 16
1
Chlorodibromomethane
ND
100
ug/L
04/28/17 16 16
1
Chloroethane
ND
100
ug/L
04/28/17 16 16
1
Chloroform
ND
100
ug/L
04/28/17 16 16
1
Chloromethane
ND
100
ug/L
04/28/17 16 16
1
2-Chlorotoluene
ND
100
ug/L
04/28/17 16 16
1
4-Chlorotoluene
ND
100
ug/L
04/28/17 16 16
1
cis-1,2-Dichloroethene
150
100
ug/L
04/28/17 16 16
1
cis-1,3-Dichloropropene
ND
100
ug/L
04/28/17 16 16
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/28/17 16 16
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/28/17 16 16
1
Dibromomethane
ND
100
ug/L
04/28/17 16 16
1
1,2 -Dichlorobenzene
ND
100
ug/L
04/28/17 16 16
1
1,3 -Dichlorobenzene
ND
100
ug/L
04/28/17 16 16
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/28/17 16 16
1
Dichlorodifluoromethane
ND
100
ug/L
04/28/17 16 16
1
1,1-Dichloroethane
ND
100
ug/L
04/28/17 16 16
1
1,2-Dichloroethane
ND
100
ug/L
04/28/171616
1
1,1-Dichloroethene
ND
100
ug/L
04/28/17 16 16
1
1,2-Dichloroethene, Total
151
1 00
ug/L
04/28/17 16 16
1
1,2-Dichloropropane
ND
100
ug/L
04/28/17 16 16
1
1,3-Dichloro propane
ND
100
ug/L
04/28/17 16 16
1
2,2-Dichloropropane
ND
100
ug/L
04/28/171616
1
1,1-Dichloropropene
ND
100
ug/L
04/28/17 16 16
1
Dusopropyl ether
ND
200
ug/L
04/28/17 16 16
1
Ethylbenzene
ND
100
ug/L
04/28/17 16 16
1
Hexachlorobutadiene
ND
200
ug/L
04/28/17 16 16
1
2-Hexanone
ND
100
ug/L
04/28/17 16 16
1
Isopropylbenzene
ND
100
ug/L
04/28/17 16 16
1
Methylene Chloride
ND
500
ug/L
04/28/17 16 16
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/28/17 16 16
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/28/17 16 16
1
Naphthalene
ND
500
ug/L
04/28/17 16 16
1
n-Butylbenzene
ND
100
ug/L
04/28/17 16 16
1
N-Propylbenzene
ND
100
ug/L
04/28/17 16 16
1
p-Isopropyltoluene
ND
100
ug/L
04/28/17 16 16
1
sec-Butylbenzene
ND
100
ug/L
04/28/17 16 16
1
Styrene
ND
100
ug/L
04/28/17 16 16
1
tert-Butyl benzene
ND
100
ug/L
04/28/17 16 16
1
TestAmenca Nashville
Page 18 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -6
Lab Sample ID: 490-127126-7
Date Collected: 04/24/17 15:30
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2 -Tetrachloroethane
ND
100
ug/L
04/28/17 16 16
1
1,1,2,2 -Tetrachloroethane
ND
100
ug/L
04/28/17 16 16
1
Tetrachloroethene
409
1 00
ug/L
04/28/17 16 16
1
Toluene
ND
100
ug/L
04/28/17 16 16
1
trans-1,2-Dichloroethene
117
100
ug/L
04/28/17 16 16
1
trans-1,3-Dichloropropene
ND
100
ug/L
04/28/17 16 16
1
1,2,3-Trichlorobenzene
ND
100
ug/L
04/28/17 16 16
1
1,2,4-Trichlorobenzene
ND
100
ug/L
04/28/17 16 16
1
1,1,1-Tnchloroethane
ND
100
ug/L
04/28/17 16 16
1
1,1,2-Tnchloroethane
ND
100
ug/L
04/28/17 16 16
1
1,4 -Dioxane
ND
200
ug/L
04/28/17 16 16
1
Trichloroethene
173
1 00
ug/L
04/28/17 16 16
1
Trichlorofluoromethane
ND
100
ug/L
04/28/17 16 16
1
1,2,3-Trichloropropane
ND
100
ug/L
04/28/17 16 16
1
1,2,4-Trimethylbenzene
ND
100
ug/L
04/28/17 16 16
1
1,3,5-Tnmethylbenzene
ND
100
ug/L
04/28/17 16 16
1
Vinyl chloride
ND
1 00
ug/L
04/28/17 16 16
1
Xylenes, Total
ND
300
ug/L
04/28/17 16 16
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Suri)
94
70-130
04/28/17 16 16
1
Dibromotluoromethane (Surr)
93
70-130
04128/17 16 16
1
1,2-Dichloroethane-d4 (Surr)
99
70-130
04/28/17 16 16
1
Toluene -d8 (Surr)
105
70-130
04128/17 16 16
1
TestAmenca Nashville
Page 19 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -7 Lab Sample ID: 490-127126-8
Date Collected: 04/24/17 16:30 Matrix: Water
Date Received: 04/26/17 09:20
F Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromobenzene
ND
Bromochloromethane
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone (MEK)
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chlorodibromomethane
ND
Chloroethane
ND
Chloroform
1 97
Chloromethane
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
cis-1,2-Dichloroethene
ND
as-1,3-Dichloropropene
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane (EDB)
ND
Dibromomethane
ND
1,2 -Dichlorobenzene
ND
1,3 -Dichlorobenzene
ND
1,4 -Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
1,1-Dichloroethene
ND
1,2-Dichloroethene, Total
1 13
1,2-Dichloropropane
ND
1,3-Dichloropropane
ND
2,2-Dichloropropane
ND
1,1-Dichloropropene
ND
Dusopropyl ether
ND
Ethylbenzene
ND
Hexachlorobutadiene
ND
2-Hexanone
ND
Isopropyl benzene
ND
Methylene Chloride
ND
4-Methyl-2-pentanone (MIBK)
ND
Methyl tert-butyl ether
ND
Naphthalene
ND
n-Butylbenzene
ND
N-Propylbenzene
ND
p-Isopropyltoluene
ND
sec -Butyl benzene
ND
Styrene
ND
tert-Butylbenzene
ND
RL
MDL Unit
D Prepared Analyzed
Dd Fac
250
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
500
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/28/17 16 41
1
1 00
ug/L
04/27/17 15 58
1
100
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
200
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
2 00
ug/L
04/27/17 15 58
1
100
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
500
ug/L
04/27/17 15 58
1
100
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
5 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
1 00
ug/L
04/27/17 15 58
1
TestAmenca Nashville
Page 20 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -7
Lab Sample ID: 490-127126-8
Date Collected: 04/24/17 16:30
Matrix: Water
Date Received: 04/26/17 09:20
Method: 82606 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dd Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
100
100
ug/L
ug/L
04/27/17 15 58
04/27/17 15 58
1
1
Tetrachloroethene
211
1 00
ug/L
04/27/17 15 58
1
Toluene
ND
1 00
ug/L
04/27/17 15 58
1
trans-1,2-Dichloroethene
ND
100
ug/L
04/27/17 15 58
1
trans-1,3-Dichloropropene
ND
100
ug/L
04/27/17 15 58
1
1,2,3-Trnchlorobenzene
ND
1 00
ug/L
04/27/17 15 58
1
1,2,4-Trichlorobenzene
ND
1 00
ug/L
04/27/17 15 58
1
1,1,1 -Trichloroethane
ND
1 00
ug/L
04/27/17 15 58
1
1,1,2 -Trichloroethane
ND
1 00
ug/L
04/27/17 15 58
1
1,4 -Dioxane
ND
200
ug/L
04/27/171558
1
Trichloroethene
ND
1 00
ug/L
04/27/17 15 58
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 15 58
1
1,2,3-Trichloropropane
ND
1 00
ug/L
04/27/17 15 58
1
1,2,4 -Tri methyl benzene
ND
100
ug/L
04/27/17 15 58
1
1,3,5-Trimethylbenzene
ND
1 00
ug/L
04/27/17 15 58
1
Vinyl chloride
ND
1 00
ug/L
04/27/17 15 58
1
Xylenes, Total
ND
300
ug/L
04/27/17 15 58
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
D►I Fac
4-Bromofluorobenzene (Surf)
100
70-130
04/27/17 15 58
1
4-Bromofluorobenzene (Surf)
93
70-130
04128/17 16 41
1
Dibromofluoromethane (Surf)
99
70-130
04/27/17 15 58
1
Dibromofluoromethane (Surr)
92
70-130
04/28/17 16 41
1
1,2-Dichloroethane-d4 (Surr)
110
70-130
04/27/17 15 58
1
1,2-Dichloroethane-d4 (Surr)
98
70-130
04/28/17 16 41
1
Toluene -d8 (Surr)
98
70-130
04127/17 15 58
1
Toluene -d8 (Surr)
106
70-130
04/28/17 16 41
1
TestAmenca Nashville
Page 21 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -8
Lab Sample ID: 490-127126-9
Date Collected: 04/24/17 17:20
Matrix: Water
Date Received: 04/26/17 09:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/27/17 16 24
1
Benzene
ND
1 00
ug/L
04/27/17 16 24
1 m
Bromobenzene
ND
1 00
ug/L
04/27/17 16 24
1
Bromochloromethane
ND
1 00
ug/L
04/27/17 16 24
1
Bromodichloromethane
ND
1 00
ug/L
04/27/17 16 24
1
Bromoform
ND
1 00
ug/L
04/27/17 16 24
1
Bromomethane
ND
1 00
ug/L
04/27/17 16 24
1
2-Butanone (MEK)
ND
500
ug/L
04/27/17 16 24
1
Carbon disulfide
ND
1 00
ug/L
04/27/17 16 24
1
Carbon tetrachloride
ND
1 00
ug/L
04/27/17 16 24
1
Chlorobenzene
ND
1 00
ug/L
04/27/17 16 24
1
Chlorodibromomethane
ND
1 00
ug/L
04/27/17 16 24
1
Chloroethane
ND
1 00
ug/L
04/27/17 16 24
1
Chloroform
ND
1 00
ug/L
04/27/17 16 24
1
Chloromethane
ND
1 00
ug/L
04/27/17 16 24
1
2-Chlorotoluene
ND
1 00
ug/L
04/27/17 16 24
1
4-Chlorotoluene
ND
1 00
ug/L
04/27/17 16 24
1
cis-1,2-Dichloroethene
ND
1 00
ug/L
04/27/17 16 24
1
cis-1,3-Dichloropropene
ND
100
ug/L
04/27/17 16 24
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/27/17 16 24
1
1,2-Dibromoethane(EDB)
ND
100
ug/L
04/27/17 16 24
1
Dibromomethane
ND
1 00
ug/L
04/27/17 16 24
1
1,2 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 16 24
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 16 24
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/27/17 16 24
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/27/17 16 24
1
1,1-Dichloroethane
ND
1 00
ug/L
04/27/17 16 24
1
1,2-Dichloroethane
ND
1 00
ug/L
04/27/17 16 24
1
1,1-Dichloroethene
ND
100
ug/L
04/27/17 16 24
1
1,2-Dichloroethene, Total
ND
1 00
ug/L
04/27/17 16 24
1
1,2-Dichloropropane
ND
100
ug/L
04/27/17 16 24
1
1,3-Dichloro propane
ND
100
ug/L
04/27/17 16 24
1
2,2-Dichloropropane
ND
1 00
ug/L
04/27/17 16 24
1
1,1-Dichloropropene
ND
100
ug/L
04/27/17 16 24
1
Dnsopropyl ether
ND
200
ug/L
04/27/17 16 24
1
Ethylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
Hexachlorobutadiene
ND
200
ug/L
04/27/17 16 24
1
2-Hexanone
ND
100
ug/L
04/27/17 16 24
1
Isopropylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
Methylene Chloride
ND
500
ug/L
04/27/17 16 24
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/27/17 16 24
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/27/17 16 24
1
Naphthalene
ND
500
ug/L
04/27/17 16 24
1
n-Butylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
N-Propylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
p-Isopropyltoluene
ND
1 00
ug/L
04/27/17 16 24
1
sec-Butylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
Styrene
ND
1 00
ug/L
04/27/17 16 24
1
tert-Butylbenzene
ND
1 00
ug/L
04/27/17 16 24
1
TestAmenca Nashville
Page 22 of 46 4/30/2017
Client Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerlca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -8
Lab Sample ID: 490-127126-9
Date Collected: 04/24/17 17:20
Matrix: /mater
Date Received: 04/26/17 09:20
Method: 82606 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
ND
ND
1 00
100
ug/L
ug/L
04/27/17 16 24
04/27/17 16 24
1
1
Tetrachloroethene
ND
1 00
ug/L
04/27/17 16 24
1
Toluene
ND
1 00
ug/L
04/27/17 16 24
1
trans-1,2-Dichloroethene
ND
100
ug/L
04/27/17 16 24
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 16 24
1
1,2,3-Tnchlorobenzene
ND
100
ug/L
04/27/17 16 24
1
1,2,4 -Tri chloro benzene
ND
100
ug/L
04/27/17 16 24
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/27/17 16 24
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/27/17 16 24
1
1,4 -Dioxane
ND
200
ug/L
04/27/17 16 24
1
Trichloroethene
ND
1 00
ug/L
04/27/17 16 24
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 16 24
1
1,2,3-Trichloropropane
ND
100
ug/L
04/27/17 16 24
1
1,2,4-Tnmethylbenzene
ND
100
ug/L
04/27/17 16 24
1
1,3,5-Tnmethylbenzene
ND
100
ug/L
04/27/17 16 24
1
Vinyl chloride
ND
1 00
ug/L
04/27/17 16 24
1
Xylenes, Total
ND
300
ug/L
04/27/17 16 24
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
109
70-130
04/27/17 16 24
1
Dibromofluoromethane (Surr)
98
70-130
04/27/17 16 24
1
1,2-Dichloroethane-d4 (Surr)
105
70-130
04/27/17 16 24
1
Toluene -d8 (Surr)
99
70-130
04/27/17 16 24
1
TestAmenca Nashville
Page 23 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 490-425499/7
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425499
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/27/17 12 56
1
Benzene
ND
1 00
ug/L
04/27/17 12 56
1
Bromobenzene
ND
1 00
ug/L
04/27/17 12 56
1
Bromochloromethane
ND
1 00
ug/L
04/27/17 12 56
1
Bromodichloromethane
ND
1 00
ug/L
04/27/17 12 56
1
Bromoform
ND
1 00
ug/L
04/27/17 12 56
1
Bromomethane
ND
1 00
ug/L
04/27/17 12 56
1
2-Butanone (MEK)
ND
500
ug/L
04/27/17 12 56
1
Carbon disulfide
ND
1 00
ug/L
04/27/17 12 56
1
Carbon tetrachloride
ND
1 00
ug/L
04/27/17 12 56
1
Chlorobenzene
ND
1 00
ug/L
04/27/17 12 56
1
Chlorodibromomethane
ND
1 00
ug/L
04/27/17 12 56
1
Chloroethane
ND
1 00
ug/L
04/27/17 12 56
1
Chloroform
ND
1 00
ug/L
04/27/17 12 56
1
Chloromethane
ND
1 00
ug/L
04/27/17 12 56
1
2-Chlorotoluene
ND
1 00
ug/L
04/27/17 12 56
1
4-Chlorotoluene
ND
1 00
ug/L
04/27/17 12 56
1
cis- 1,2-Dichloroethene
ND
1 00
ug/L
04/27/17 12 56
1
cis-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 12 56
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/27/17 12 56
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/27/17 12 56
1
Dibromomethane
ND
1 00
ug/L
04/27/17 12 56
1
1,2 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,3 -Dichlorobenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,4 -Dichlorobenzene
ND
100
ug/L
04/27/17 12 56
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/27/17 12 56
1
1,1-Dichloroethane
ND
1 00
ug/L
04/27/17 12 56
1
1,2-Dichloroethane
ND
1 00
ug/L
04/27/17 12 56
1
1,1-Dichloroethene
ND
1 00
ug/L
04/27/17 12 56
1
1,2-Dichloroethene, Total
ND
1 00
ug/L
04/27/17 12 56
1
1,2-Dichloropropane
ND
1 00
ug/L
04/27/17 12 56
1
1,3-Dichloropropane
ND
1 00
ug/L
04/27/17 12 56
1
2,2-Dichloropropane
ND
1 00
ug/L
04/27/17 12 56
1
1,1-Dichloropropene
ND
1 00
ug/L
04/27/17 12 56
1
Dnsopropyl ether
ND
2 00
ug/L
04/27/17 12 56
1
Ethylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
Hexachlorobutadiene
ND
2 00
ug/L
04/27/17 12 56
1
° 2-Hexanone
ND
100
ug/L
04/27/17 12 56
1
Isop ropylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
Methylene Chloride
ND
500
ug/L
04/27/17 12 56
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/27/17 12 56
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/27/17 12 56
1
Naphthalene
ND
500
ug/L
04/27/17 12 56
1
n-Butylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
N-Propylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
p-Isopropyltoluene
ND
1 00
ug/L
04/27/17 12 56
1
sec-Butylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
Styrene
ND
1 00
ug/L
04/27/17 12 56
1
TestAmenca Nashville
Page 24 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
TestAmerica Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG
DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-425499/7
Client Sample
ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch 425499
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dd Fac
tert-Butylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,1,1,2 -Tetrachloroethane
ND
1 00
ug/L
04/27/17 12 56
1
1,1,2,2 -Tetrachloroethane
ND
1 00
ug/L
04/27/17 12 56
1
Tetra ch loroethene
ND
1 00
ug/L
04/27/17 12 56
1
Toluene
ND
1 00
ug/L
04/27/17 12 56
1
trans-1,2-Dichloroethene
ND
1 00
ug/L
04/27/17 12 56
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/27/17 12 56
1
1,2,3-Trichlorobenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,2,4-Trichlorobenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,1,1 -Trichloroethane
ND
1 00
ug/L
04/27/17 12 56
1
1,1,2 -Trichloroethane
ND
1 00
ug/L
04/27/17 12 56
1
1,4 -Dioxane
ND
200
ug/L
04/27/17 12 56
1
Trichloroethene
ND
1 00
ug/L
04/27/17 12 56
1
Trichlorofluoromethane
ND
1 00
ug/L
04/27/17 12 56
1
1,2,3-Tnchloropropane
ND
1 00
ug/L
04/27/17 12 56
1
1,2,4-Tnmethylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
1,3,5-Tnmethylbenzene
ND
1 00
ug/L
04/27/17 12 56
1
Vinyl chloride
ND
1 00
ug/L
04/27/17 12 56
1
Xylenes, Total
ND
300
ug/L
04/27/17 12 56
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
D►1 Fac
4-Bromofluorobenzene (Suri)
105
70-130
04/27/17 12 56
1
Dibromofluoromethane (Surr)
100
70-130
04/27/17 12 56
1
1,2-Dichloroethane-d4 (Surr)
103
70-130
04/27/17 12 56
1
Toluene -d8 (Surr)
98
70-130
04/27/17 12 56
1
Lab Sample ID: LCS 490-425499/3
Client
Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425499
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
100
98 89
ug/L
99
39-150
Benzene
200
2062
ug/L
103
70-130
Bromobenzene
200
21 96
ug/L
110
70-130
Bromochloromethane
200
2053
ug/L
103
70-130
Bromodichloromethane
200
21 63
ug/L
108
70-130
Bromoform
200
21 66
ug/L
108
70-137
Bromomethane
200
2556
ug/L
128
53-150
2-Butanone (MEK)
100
8740
ug/L
87
55-143
Carbon disulfide
200
2023
ug/L
101
64-135
Carbon tetrachloride
200
2378
ug/L
119
70-147
Chlorobenzene
200
21 34
ug/L
107
70-130
Chlorodibromomethane
200
2145
ug/L
107
70-133
Chloroethane
200
1854
ug/L
93
60-138
Chloroform
200
22 08
ug/L
110
70-130
Chloromethane
200
21 73
ug/L
109
33-150
2-Chlorotoluene
200
2211
ug/L
111
70-130
4-Chlorotoluene
200
21 83
ug/L
109
70-130
TestAmerica Nashville
Page 25 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-425499/3 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 425499
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec
Limits
cis-1,2-Dichloroethene
200
2091
ug/L
105
70-130
cis-1,3-Dichloropropene
200
21 07
ug/L
105
70-133
1,2-Dibromo-3-Chloropropane
200
1961
ug/L
98
45-138
1,2-Dibromoethane (EDB)
200
2063
ug/L
103
70-130
Dibromomethane
200
21 02
ug/L
105
70-130
1,2 -Dichlorobenzene
200
2235
ug/L
112
70-130
1,3 -Dichlorobenzene
200
21 98
ug/L
110
70-130
1,4 -Dichlorobenzene
200
2190
ug/L
109
70-130
Dichlorodifluoromethane
200
2409
ug/L
120
48-150
1,1-Dichloroethane
200
1964
ug/L
98
70-130
1,2-Dichloroethane
200
21 51
ug/L
108
70-130
1,1-Dichloroethene
200
2096
ug/L
105
70-132
1,2-Dichloroethene, Total
400
4055
ug/L
101
70-130
1,2-Dichloropropane
200
1867
ug/L
93
70-130
1,3-Dichloropropane
200
1984
ug/L
99
70-130
2,2-Dichloropropane
200
2237
ug/L
112
60-143
1,1-Dichloropropene
200
2080
ug/L
104
70-130
Dusopropyl ether
200
1736
ug/L
87
66-142
Ethylbenzene
200
2163
ug/L
108
70-130
Hexachlorobutadiene
200
21 16
ug/L
106
70-138
2-Hexanone
100
8477
ug/L
85
54-142
Isopropyl benzene
200
2320
ug/L
116
70-131
Methylene Chloride
200
2065
ug/L
103
70-130
4-Methyl-2-pentanone (MIBK)
100
8583
ug/L
86
60-137
Methyl tert-butyl ether
200
1990
ug/L
100
70-130
Naphthalene
200
1898
ug/L
95
54-150
n-Butylbenzene
200
2222
ug/L
111
68-137
N-Propylbenzene
200
21 60
ug/L
108
70-134
p-Isopropyltoluene
200
2143
ug/L
107
66-130
sec-Butylbenzene
200
21 54
ug/L
108
70-135
Styrene
200
2270
ug/L
113
70-130
tert-Butyl benzene
200
2096
ug/L
105
70-130
1,1,1,2 -Tetrachloroethane
200
2190
ug/L
109
70-130
1,1,2,2 -Tetrachloroethane
200
2023
ug/L
101
69-131
Tetrachloroethene
200
2240
ug/L
112
70-130
Toluene
200
21 23
ug/L
106
70-130
trans-1,2-Dichloroethene
200
1964
ug/L
98
70-130
trans-1,3-Dichloropropene
200
2066
ug/L
103
63-142
1,2,3-Tnchlorobenzene
200
1897
ug/L
95
46-150
1,2,4-Tnchlorobenzene
200
1859
ug/L
93
58-147
1,1,1-Tnchloroethane
200
2333
ug/L
117
70-135
1,1,2 -Trichloroethane
200
2044
ug/L
102
70-130
1,4 -Dioxane
400
3564
ug/L
89
18-150
Trichloroethene
200
21 55
ug/L
108
70-130
Trichlorofluoromethane
200
2451
ug/L
123
59-150
1,2,3-Trichloropropane
200
1950
ug/L
98
70-131
1,2,4-Trimethylbenzene
200
2212
ug/L
111
70-130
1,3,5-Tnmethylbenzene
200
2248
ug/L
112
70-130
TestAmenca Nashville
Page 26 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-425499/3
Matrix: Water
Analysis Batch: 425499
Analyte
Vinyl chloride
Xylenes, Total
LCS LCS
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surf) 98
Dibromofluoromethane (Surr) 99
1,2-Dichloroethane-d4 (Surr) 106
Toluene -d8 (Surr) 99
Lab Sample ID: LCSD 490-425499/4
Matrix: Water
Analysis Batch: 425499
Analyte
Acetone
i
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
as-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2 -Dichlorobenzene
1,3 -Dichlorobenzene
1,4 -Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethene, Total
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
TestAmerica Job ID 490-127126-1
SDG DSO -80
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
D %Rec Limits
Added
Result Qualifier
Unit
200
19 57
ug/L
400
4465
ug/L
Limits
70-130
70-130
70-130
70-130
%Rec
LCSD LCSD
Result Qualifier
D %Rec Limits
D %Rec
98 57-137
RPD
112 70-132
100
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
LCSD LCSD
Result Qualifier
Unit
D %Rec
%Rec
Limits
RPD
RPD
Limit
100
9697
6g/L
97
3-9-- 150
2
23
200
2081
ug/L
104
70-130
1
12
200
21 24
ug/L
106
70-130
3
16
200
2057
ug/L
103
70-130
0
16
200
21 39
ug/L
107
70-130
1
14
200
21 15
ug/L
106
70-137
2
14
200
2502
ug/L
125
53-150
2
19
100
9409
ug/L
94
55-143
7
19
200
2070
ug/L
104
64-135
2
16
200
2332
ug/L
117
70-147
2
16
200
2146
ug/L
107
70-130
1
12
200
2086
ug/L
104
70-133
3
13
200
1854
ug/L
93
60-138
0
15
200
21 56
ug/L
108
70-130
2
14
200
21 34
ug/L
107
33-150
2
20
200
2234
ug/L
112
70-130
1
15
200
2229
ug/L
111
70-130
2
15
200
2072
ug/L
104
70-130
1
15
200
21 24
ug/L
106
70-133
1
15
200
2001
ug/L
100
45-138
2
19
200
2066
ug/L
103
70-130
0
13
200
2076
ug/L
104
70-130
1
14
200
2250
ug/L
113
70-130
1
12
200
2270
ug/L
114
70-130
3
13
200
2252
ug/L
113
70-130
3
12
200
2402
ug/L
120
48-150
0
16
200
1972
ug/L
99
70-130
0
17
200
21 35
ug/L
107
70-130
1
13
200
2070
ug/L
103
70-132
1
20
400
41 10
ug/L
103
70-130
1
14
200
1870
ug/L
94
70-130
0
15
200
1967
ug/L
98
70-130
1
12
200
2228
ug/L
111
60-143
0
20
200
21 00
ug/L
105
70-130
1
16
TestAmerica Nashville
Page 27 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
Method: 82608 -Volatile Organic Compounds (GC/MS) (Continued)
TestAmerica Job ID 490-127126-1
SDG DSO -80
" Lab Sample ID: LCSD 490-425499/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Matrix: Water
Prep Type: Total/NA
Prep Type: Total/NA
Analysis Batch: 425499
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Spike
LCSD LCSD
D %Rec Limits
Acetone ND
%Rec
4062
RPD
Analyte
Benzene ND
Added
Result Qualifier Unit
D %Rec
Limits
RPD
Limit
Dusopropyl ether
ug/L
200
1753
ug/L
88
66-142
1
14
I Ethylbenzene
200
2203
ug/L
110
70-130
2
12
Hexachlorobutadiene
200
2253
ug/L
113
70-138
6
16
2-Hexanone
100
8728
ug/L
87
54-142
3
17
Isopropylbenzene
200
2273
ug/L
114
70-131
2
13
Methylene Chloride
200
2049
ug/L
102
70-130
1
15
4-Methyl-2-pentanone (MIBK)
100
8897
ug/L
89
60-137
4
21
Methyl tert-butyl ether
200
2045
ug/L
102
70-130
3
16
Naphthalene
200
2047
ug/L
102
54-150
8
15
n-Butylbenzene
200
22 87
ug/L
114
68-137
3
14
N-Propylbenzene
200
2214
ug/L
111
70-134
2
14
p-Isopropyltoluene
200
22 09
ug/L
110
66-130
3
13
sec-Butylbenzene
200
2205
ug/L
110
70-135
2
14
Styrene
200
2301
ug/L
115
70-130
1
12
tert-Butyl benzene
200
21 56
ug/L
108
70-130
3
14
1,1,1,2 -Tetrachloroethane
200
2186
ug/L
109
70-130
0
13
1,1,2,2 -Tetrachloroethane
200
2071
ug/L
104
69-131
2
15
Tetrachloroethene
200
2212
ug/L
111
70-130
1
17
„ Toluene
200
21 18
ug/L
106
70-130
0
13
trans-1,2-Dichloroethene
200
2038
ug/L
102
70-130
4
15
trans-1,3-Dichloropropene
200
2050
ug/L
103
63-142
1
13
1,2,3-Trichlorobenzene
200
1985
ug/L
99
46-150
5
16
1,2,4-Trichlorobenzene
200
1944
ug/L
97
58-147
4
15
1,1,1 -Trichloroethane
200
2382
ug/L
119
70-135
2
15
1,1,2 -Trichloroethane
200
2040
ug/L
102
70-130
0
13
1,4 -Dioxane
400
3877
ug/L
97
18-150
8
34
Trichloroethene
200
21 33
ug/L
107
70-130
1
14
Trichlorofluoromethane
200
2472
ug/L
124
59-160
1
22
1,2,3-Trichloropropane
200
2002
ug/L
100
70-131
3
14
1,2,4-Trimethylbenzene
200
2239
ug/L
112
70-130
1
13
1,3,5-Tnmethylbenzene
200
2244
ug/L
112
70-130
0
14
Vinyl chloride
200
2037
ug/L
102
57-137
4
15
Xylenes, Total
400
4496
ug/L
112
70-132
1
11
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
4-Bromotluorobenzene (Surr)
92
70-130
Dibromofluoromethane (Surf)
98
70-130
I 1,2-Dichloroethane-d4 (Surr)
103
70-130
Toluene -d8 (Surr)
98
70-130
Lab Sample ID: 490-127126-1 MS
Client Sample ID: MW -1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425499
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits
Acetone ND
500
4062
ug/L
81 39-150
Benzene ND
100
1031
ug/L
103 55-147
Bromobenzene ND
100
1088
ug/L
109 60-133
TestAmerlca Nashville
Page 28 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-127126-1 MS Client Sample ID: MW -1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 425499
Analyte
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
as-1,2-Dichloroethene
as-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2 -Dichlorobenzene
1,3 -Dichlorobenzene
1,4 -Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethene, Total
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Dusopropyl ether
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
Sample Sample
Result Qualifier
Spike
Added
MS BAS
Result Qualifier
ND
100
9805
ND
100
1038
ND
100
1037
ND
100
1197
ND
500
4351
ND
100
9446
ND
100
1221
ND
100
1061
ND
100
101 2
ND
100
8803
ND
100
1104
ND
100
9655
ND
100
1105
ND
100
1089
Nb
100
1040
ND
100
101 0
ND
100
9049
ND
100
9557
ND
100
9976
ND
100
1092
ND
100
111 1
ND
100
1085
ND
100
1095
ND
100
9902
ND
100
1026
ND
100
9783
ND
200
2034
ND
100
91 91
ND
100
9348
ND
100
1080
ND
100
1024
ND
100
8606
ND
100
1087
ND
100
1053
ND
500
3753
ND
100
1175
ND
100
1022
ND
500
3996
ND
100
9405
ND
100
8989
ND
100
1138
ND
100
1096
ND
100
1086
ND
100
1106
ND
100
1196
ND
100
1086
ND
100
1072
ND
100
9812
TestAmenca Nashville
Page 29 of 46 4/30/2017
%Rec
Unit
D %Rec
Limits
ug/L
98
59-132
ug/L
104
70-140
ug/L
104
53-150
ug/L
120
30-150
ug/L
87
50-143
ug/L
94
35-150
ug/L
122
56-150
ug/L
106
70-130
ug/L
101
66-140
ug/L
88
58-141
ug/L
110
66-138
ug/L
97
10-150
ug/L
111
67-138
ug/L
109
69-138
ug/L
104
68-131
ug/L
101
70-133
ug/L
90
38-138
ug/L
96
65-137
ug/L
100
70-130
ug/L
109
70-130
ug/L
111
68-131
ug/L
108
70-130
ug/L
109
10-150
ug/L
99
61-139
ug/L
103
64.136
ug/L
98
54-150
ug/L
102
60-134
ug/L
92
67-130
ug/L
93
70-130
ug/L
108
50-146
ug/L
102
54-150
ug/L
86
56-142
ug/L
109
65-139
ug/L
105
61-141
ug/L
75
44-150
ug/L
118
70-137
ug/L
102
64-130
ug/L
80
50-140
ug/L
94
55-141
ug/L
78
32-150
ug/L
114
61-141
ug/L
107
53-150
ug/L
109
66-137
ug/L
111
55-136
ug/L
120
70-130
ug/L
109
70-138
ug/L
107
70-131
ug/L
98
56-145
TestAmenca Nashville
Page 29 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-127126-1 MS
Matrix: Water
Analysis Batch: 425499
Spike
Sample Sample
Analyte
Result Qualifier
Tetrachloroethene
ND
Toluene
ND
trans-1,2-Dichloroethene
ND
trans-1,3-Dichloropropene
ND
1,2,3-Trichlorobenzene
ND
1,2,4-Trichlorobenzene
ND
1,1,1 -Trichloroethane
ND
1,1,2 -Trichloroethane
ND
1,4 -Dioxane
ND
Trichloroethene
ND
Trichlorofluoromethane
ND
1,2,3-Trichloropropane
ND
1,2,4-Trimethylbenzene
797
1,3,5-Trimethylbenzene
ND
Vinyl chloride
ND
Xylenes, Total
ND
Spike
MS MS
Added
Result Qualifier
100
111 1
100
1043
100
9944
100
9732
100
8748
100
8988
100
121 3
100
9922
2000
1883
100
1067
100
1222
100
9578
100
1107
100
1090
100
8999
200
2283
MS MS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 97 70-130
Dibromofluoromethane (Surr) 99 70-130
1,2-Dichloroethane-d4 (Surr) 104 70-130
Toluene -d8 (Surr) 98 70-130
Lab Sample ID: 490-127126-1 MSD
Matrix: Water
Analysis Batch: 425499
Analyte
Sample Sample
Result Qualifier
Acetone
ND
Benzene
ND
Bromobenzene
ND
Bromochloromethane
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone (MEK)
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chlorodibromomethane
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
as-1,2-Dichloroethene
ND
cis- 1,3-Dichloropropene
ND
1,2-Dibromo-3-Chloropropane
ND
Spike
MSD MSD
Added
Result Qualifier
500
471 1
100
1051
100
1159
100
1004
100
1080
100
1108
100
1204
500
4425
100
9884
100
1238
100
1129
100
1082
100
8878
100
1080
100
101 4
100
1157
100
1127
100
1059
100
1074
100
9728
Page 30 of 46
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MWA
Prep Type: Total/NA
Client Sample ID: MW -1
Prep Type: Total/NA
%Rec
Unit
D %Rec
Limits
ug/L
111
57-138
ug/L
104
64-136
ug/L
99
59-143
ug/L
97
63-142
ug/L
87
36-150
ug/L
90
47-147
ug/L
121
68-144
ug/L
99
70-130
ug/L
94
11-150
ug/L
107
63-135
ug/L
122
44-150
ug/L
96
65-131
ug/L
103
64-136
ug/L
107
69-139
ug/L
90
57-150
ug/L
114
69-132
Client Sample ID: MW -1
Prep Type: Total/NA
TestAmerlca Nashville
4/30/2017
%Rec
RPD
Unit
D %Rec
Limits
RPD
Limit
ug/L
94
39-150
15
28
ug/L
105
55-147
2
22
ug/L
116
60-133
6
18
ug/L
100
59-132
2
21
ug/L
108
70-140
4
196
ug/L
111
53-150
7
20
ug/L
120
30-150
1
44
ug/L
89
50-143
2
28
ug/L
99
35-150
5
34
ug/L
124
56-150
1
18
ug/L
113
70-130
6
15
ug/L
108
66-140
7
19
ug/L
89
58-141
1
31
ug/L
108
66-138
2
21
ug/L
101
10-150
5
43
ug/L
116
67-138
5
17
ug/L
113
69-138
3
15
ug/L
106
68-131
2
21
ug/L
107
70-133
6
19
ug/L
97
38-138
7
26
TestAmerlca Nashville
4/30/2017
CSC Sample Results
Client Hart & Hickman, PC
TestAmenca Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/AOS) (Continued)
Lab Sample ID: 490-127126-1 MSD
Client
Sample ID: MW -1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425499
Sample Sample
Spike
MSD MSD
%Rec
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
1,2-Dibromoethane(EDB)
ND
100
1052
ug/L
105
65-137
10
21
Dibromomethane
ND
100
1032
ug/L
103
70-130
3
19
1,2 -Dichlorobenzene
ND
100
1161
ug/L
116
70-130
6
15
1,3 -Dichlorobenzene
ND
100
1171
ug/L
117
68-131
5
14
1,4 -Dichlorobenzene
ND
100
1130
ug/L
113
70-130
4
14
Dichlorodifluoromethane
ND
100
1101
ug/L
110
10-150
1
50
1,1-Dichloroethane
ND
100
9915
ug/L
99
61-139
0
23
1,2-Dichloroethane
ND
100
1082
ug/L
108
64-136
5
22
1,1-Dichloroethene
ND
100
9912
ug/L
99
54-150
1
24
1,2-Dichloroethene, Total
ND
200
2046
ug/L
102
60-134
1
22
1,2-Dichloropro pane
ND
100
9297
ug/L
93
67-130
1
19
1,3-Dichloropropane
ND
100
1002
ug/L
100
70-130
7
17
2,2-Dichloropropane
ND
100
1085
ug/L
108
50-146
0
20
1,1-Dichloropropene
ND
100
1059
ug/L
106
54-150
3
24
Dnsopropyl ether
ND
100
8721
ug/L
87
56-142
1
22
Ethylbenzene
ND
100
1147
ug/L
115
65-139
5
18
Hexachlorobutadiene
ND
100
1167
ug/L
117
61-141
10
26
2-Hexanone
ND
500
4237
ug/L
85
44-150
12
21
Isopropylbenzene
ND
100
1259
ug/L
126
70-137
7
17
Methylene Chloride
ND
100
1037
ug/L
104
64-130
1
22
4-Methyl-2-pentanone (MIBK)
ND
500
4378
ug/L
88
50-140
9
24
Methyl tert-butyl ether
ND
100
1006
ug/L
101
55-141
7
24
Naphthalene
ND
100
1005
ug/L
89
32-150
11
40
n-Butylbenzene
ND
100
1200
ug/L
120
61-141
5
17
N-Propylbenzene
ND
100
1137
ug/L
111
53-150
4
18
p-Isopropyltoluene
ND
100
1157
ug/L
116
66-137
6
16
sec -Butyl benzene
ND
100
1161
ug/L
116
55-136
5
50
Styrene
ND
100
1180
ug/L
118
70-130
1
16
tert-Butylbenzene
ND
100
1141
ug/L
114
70-138
5
17
1,1,1,2 -Tetrachloroethane
ND
100
1128
ug/L
113
70-131
5
16
1,1,2,2 -Tetrachloroethane
ND
100
1021
ug/L
102
56-145
4
19
Tetra chloroethene
ND
100
1179
ug/L
118
57-138
6
17
Toluene
ND
100
1100
ug/L
110
64-136
5
18
trans-1,2-Dichloroethene
ND
100
9867
ug/L
99
59-143
1
25
trans-1,3-Dichloropropene
ND
100
1048
ug/L
105
63-142
7
18
1,2,3-Tnchlorobenzene
ND
100
9704
ug/L
97
36-150
10
43
1,2,4-Tnchlorobenzene
ND
100
9765
ug/L
98
47-147
8
24
1,1,1 -Trichloroethane
ND
100
1250
ug/L
125
68-144
3
17
1,1,2 -Trichloroethane
ND
100
1038
ug/L
104
70-130
5
18
1,4 -Dioxane
ND
2000
2001
ug/L
100
11-150
6
50
Trichloroethene
ND
100
1092
ug/L
109
63-135
2
17
Tnchlorofluoromethane
ND
100
1287
ug/L
129
44-150
5
32
1,2,3-Trichloropropane
ND
100
1061
ug/L
106
65-131
10
19
1,2,4-Tnmethylbenzene
797
100
1161
ug/L
108
64-136
5
18
1,3,5-Tnmethylbenzene
ND
100
1163
ug/L
115
69-139
6
17
Vinyl chloride
ND
100
9602
ug/L
96
57-150
6
37
Xylenes, Total
ND
200
2325
ug/L
116
69-132
2
17
TestAmerlca Nashville
Page 31 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
TestAmenca Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG
DSO -80
Method: 6260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-127126-1 MSD
Client Sample ID: MW -1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425499
MSD MSD
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surf)
98
70-130
Dibromofluoromethane (Surr)
97
70-130
10
1,2-Dichloroethane-d4 (Surr)
101
70-130
Toluene -d8 (Surr)
101
70-130
Lab Sample ID: MB 490-425892/7
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch 425892
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
250
ug/L
04/28/17 13 50
1
Benzene
ND
1 00
ug/L
04/28/17 13 50
1
Bromobenzene
ND
1 00
ug/L
04/28/17 13 50
1
Bromochloromethane
ND
1 00
ug/L
04/28/17 13 50
1
Bromodichloromethane
ND
1 00
ug/L
04/28/17 13 50
1
Bromoform
ND
1 00
ug/L
04/28/17 13 50
1
Bromomethane
ND
1 00
ug/L
04/28/17 13 50
1
2-Butanone (MEK)
ND
500
ug/L
04/28/17 13 50
1
Carbon disulfide
ND
1 00
ug/L
04/28/17 13 50
1
Carbon tetrachloride
ND
1 00
ug/L
04/28/17 13 50
1
Chlorobenzene
ND
1 00
ug/L
04/28/17 13 50
1
Chlorodibromomethane
ND
1 00
ug/L
04/28/17 13 50
1
Chloroethane
ND
1 00
ug/L
04/28/17 13 50
1
Chloroform
ND
1 00
ug/L
04/28/17 13 50
1
Chloromethane
ND
1 00
ug/L
04/28/17 13 50
1
2-Chlorotoluene
ND
1 00
ug/L
04/28/17 13 50
1
4-Chlorotoluene
ND
1 00
ug/L
04/28/17 13 50
1
cis-1,2-Dichloroethene
ND
100
ug/L
04/28/17 13 50
1
as-1,3-Dichloropropene
ND
1 00
ug/L
04/28/17 13 50
1
1,2-Dibromo-3-Chloropropane
ND
100
ug/L
04/28/17 13 50
1
1,2-Dibromoethane (EDB)
ND
1 00
ug/L
04/28/17 13 50
1
Dibromomethane
ND
1 00
ug/L
04/28/17 13 50
1
1,2 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 13 50
1
1,3 -Dichlorobenzene
ND
100
ug/L
04/28/17 13 50
1
1,4 -Dichlorobenzene
ND
1 00
ug/L
04/28/17 13 50
1
Dichlorodifluoromethane
ND
1 00
ug/L
04/28/17 13 50
1
1,1-Dichloroethane
ND
1 00
ug/L
04/28/17 13 50
1
1,2-Dichloroethane
ND
1 00
ug/L
04/28/17 13 50
1
1,1-Dichloroethene
ND
1 00
ug/L
04/28/17 13 50
1
1,2-Dichloroethene, Total
ND
1 00
ug/L
04/28/17 13 50
1
1,2-Dichloropropane
ND
1 00
ug/L
04/28/17 13 50
1
1,3-Dichloropropane
ND
100
ug/L
04/28/17 13 50
1
2,2-Dichloropropane
ND
1 00
ug/L
04/28/17 13 50
1
1,1-Dichloropropene
ND
1 00
ug/L
04/28/17 13 50
1
Diisopropyl ether
ND
200
ug/L
04/28/17 13 50
1
Ethylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
Hexachlorobutadiene
ND
200
ug/L
04/28/17 13 50
1
2-Hexanone
ND
100
ug/L
04/28/17 13 50
1
TestAmenca Nashville
Page 32 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
LCS LCS
Result Qualifier
100
7302
TestAmenca Job ID 490-127126-1
Project/Site McCorkles Cleaners
200
2121
200
SDG
DSO -80
1835
200
1709
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
2260
Lab Sample ID: MB 490-425892/7
70-130
ug/L
85
Client Sample ID: Method Blank
Matrix: Water
113
53-150
Prep Type: Total/NA
Analysis Batch: 425892
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dd Fac
Isopropylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
Methylene Chloride
ND
500
ug/L
04/28/17 13 50
1
4-Methyl-2-pentanone (MIBK)
ND
100
ug/L
04/28/17 13 50
1
Methyl tert-butyl ether
ND
1 00
ug/L
04/28/17 13 50
1
Naphthalene
ND
500
ug/L
04/28/17 13 50
1
n-Butylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
N-Propylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
p-Isopropyltoluene
ND
1 00
ug/L
04/28/17 13 50
1
sec-Butylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
Styrene
ND
1 00
ug/L
04/28/17 13 50
1
tert-Butylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
1,1,1,2 -Tetrachloroethane
ND
100
ug/L
04/28/17 13 50
1
1,1,2,2 -Tetrachloroethane
ND
1 00
ug/L
04/28/17 13 50
1
Tetrachloroethene
ND
1 00
ug/L
04/28/17 13 50
1
Toluene
ND
1 00
ug/L
04/28/17 13 50
1
trans-1,2-Dichloroethene
ND
1 00
ug/L
04/28/17 13 50
1
trans-1,3-Dichloropropene
ND
1 00
ug/L
04/28/17 13 50
1
1,2,3-Trichlorobenzene
ND
100
ug/L
04/28/17 13 50
1
1,2,4-Trichlorobenzene
ND
100
ug/L
04/28/17 13 50
1
1,1,1 -Trichloroethane
ND
100
ug/L
04/28/17 13 50
1
1,1,2 -Trichloroethane
ND
100
ug/L
04/28/17 13 50
1
1,4 -Dioxane
ND
200
ug/L
04/28/17 13 50
1
Trichloroethene
ND
1 00
ug/L
04/28/17 13 50
1
Trichlorofluoromethane
ND
1 00
ug/L
04/28/17 13 50
1
1,2,3-Trichloropropane
ND
1 00
ug/L
04/28/17 13 50
1
1,2,4-Tnmethylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
1,3,5-Tnmethylbenzene
ND
1 00
ug/L
04/28/17 13 50
1
Vinyl chloride
ND
1 00
ug/L
04/28/17 13 50
1
Xylenes, Total
ND
300
ug/L
04/28/17 13 50
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed
Dd Fac
4-Bromofluorobenzene (Surr)
96
70-130
04/28/17 13 50
1
Dibromofluoromethane (Surr)
95
70-130
04/28/17 13 50
1
1,2-Dichloroethane-d4 (Surr)
97
70-130
04/28/17 13 50
1
Toluene -d8 (Surr)
103
70-130
04/28/17 13 50
1
Lab Sample ID- LCS 490-425892/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425892
Analyte
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Spike
Added
LCS LCS
Result Qualifier
100
7302
200
2144
200
2121
200
2071
200
1835
200
1709
200
2260
Unit
D %Rec
%Rec
Limits
ug/L
73
39-150
ug/L
107
70-130
ug/L
106
70-130
ug/L
104
70-130
ug/L
92
70-130
ug/L
85
70-137
ug/L
113
53-150
TestAmenca Nashville
Page 33 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC TestAmerica Job ID 490-127126-1
Project/Site McCorkles Cleaners SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-425892/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425892
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2-Butanone (MEK)
100
1076
ug/L
108
55-143
Carbon disulfide
200
1920
ug/L
96
64-135
Carbon tetrachloride
200
1897
ug/L
95
70-147
Chlorobenzene
200
2225
ug/L
111
70-130
Chlorodibromomethane
200
1947
ug/L
97
70-133
Chloroethane
200
2320
ug/L
116
60-138
Chloroform
200
2024
ug/L
101
70-130
Chloromethane
200
2379
ug/L
119
33-150
2-Chlorotoluene
200
2151
ug/L
108
70-130
4-Chlorotoluene
200
21 06
ug/L
105
70-130
cis-1,2-Dichloroethene
200
2071
ug/L
104
70-130
cis-1,3-Dichloropropene
200
2089
ug/L
104
70-133
1,2-Dibromo-3-Chloropropane
200
2047
ug/L
102
45-138
1,2-Dibromoethane (EDB)
200
21 68
ug/L
108
70-130
Dibromomethane
200
2061
ug/L
103
70-130
1,2 -Dichlorobenzene
200
2205
ug/L
110
70-130
1,3 -Dichlorobenzene
200
2180
ug/L
109
70-130
1,4 -Dichlorobenzene
200
2149
ug/L
107
70-130
Dichlorodifluoromethane
200
1959
ug/L
98
48-150
1,1-Dichloroethane
200
2049
ug/L
102
70-130
1,2-Dichloroethane
200
2065
ug/L
103
70-130
1,1-Dichloroethene
200
2209
ug/L
110
70-132
1,2-Dichloroethene, Total
400
41 73
ug/L
104
70-130
1,2-Dichloropropane
200
21 11
ug/L
106
70-130
1,3-Dichloropropane
200
2242
ug/L
112
70-130
2,2-Dichloropropane
200
2048
ug/L
102
60-143
1,1-Dichloropropene
200
2045
ug/L
102
70-130
Dnsopropyl ether
200
2006
ug/L
100
66-142
Ethylbenzene
200
21 82
ug/L
109
70-130
Hexachlorobutadiene
200
1766
ug/L
88
70-138
2-Hexanone
100
1183
ug/L
118
54-142
Isopropylbenzene
200
21 01
ug/L
105
70-131
Methylene Chloride
200
2236
ug/L
112
70-130
4-Methyl-2-pentanone(MIBK)
100
1147
ug/L
115
60-137
Methyl tent -butyl ether
200
2014
ug/L
101
70-130
Naphthalene
200
1998
ug/L
100
54-150
n-Butylbenzene
200
2010
ug/L
101
68-137
N-Propylbenzene
200
21 73
ug/L
109
70-134
p-Isopropyltoluene
200
2014
ug/L
101
66-130
sec-Butylbenzene
200
2006
ug/L
100
70-135
Styrene
200
21 61
ug/L
108
70-130
tert-Butylbenzene
200
1924
ug/L
96
70-130
1,1,1,2 -Tetrachloroethane
200
2070
ug/L
103
70-130
1,1,2,2 -Tetrachloroethane
200
2215
ug/L
111
69-131
Tetrachloroethene
200
2246
ug/L
112
70-130
Toluene
200
21 65
ug/L
108
70-130
trans-1,2-Dichloroethene
200
21 02
ug/L
105
70-130
trans-1,3-Dichloropropene
200
1949
ug/L
97
63-142
TestAmenca Nashville
Page 34 of 46 4/30/2017
CSC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-425892/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 425892
Analyte
Sample Sample
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec
Limits
1,2,3-Tnchlorobenzene
Result Qualifier
200
2033
ug/L
102
46-150
1,2,4-Trichlorobenzene
ND F2
200
2017
ug/L
101
58-147
1,1,1 -Trichloroethane
ND
200
2037
ug/L
102
70-135
1,1,2 -Trichloroethane
ND
200
2241
ug/L
112
70-130
1,4 -Dioxane
ND
400
4256
ug/L
106
18-150
Trichloroethene
ND
200
2144
ug/L
107
70-130
Tnchlorofluoromethane
ND
200
21 93
ug/L
110
59-150
1,2,3-Trichloropropane
ND
200
2234
ug/L
112
70-131
1,2,4-Trimethylbenzene
ND
200
2062
ug/L
103
70-130
1,3,5-Tnmethylbenzene
ND
200
2071
ug/L
104
70-130
Vinyl chloride
ND
200
21 96
ug/L
110
57-137
Xylenes, Total
ND
400
4257
ug/L
106
70-132
Chlorodibromomethane
LCS LCS
1000
1000
ug/L
100
66-140
Surrogate
%Recovery Qualifier
Limits
1074
ug/L
107
58.141
4-Bromofluorobenzene (Surr)
99
70-130
1004
ug/L
100
66-138
Dibromofluoromethane (Surr)
94
70-130
1058
ug/L
106
10-150
1,2-Dichloroethane-d4 (Surr)
94
70-130
1118
ug/L
112
67-138
Toluene -dB (Surr)
100
70-130
1092
ug/L
109
69-138
Lab Sample ID: 490-127126-2 MS
Matrix: Water
Analysis Batch: 425892
Client Sample ID: MW -2S
Prep Type: Total/NA
TestAmerica Nashville
Page 35 of 46 4/30/2017
Sample Sample
Spike
MS MS
%Rec
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
ND F2
5000
3668
ug/!-
73
39-150
Benzene
ND
1000
1069
ug/L
107
55-147
Bromobenzene
ND
1000
1077
ug/L
108
60-133
Bromochloromethane
ND
1000
1013
ug/L
101
59-132
Bromodichloromethane
ND
1000
9339
ug/L
93
70-140
Bromoform
ND
1000
8632
ug/L
86
53-150
Bromomethane
ND
1000
1045
ug/L
104
30-150
2-Butanone (MEK)
ND
5000
6146
ug/L
123
50-143
Carbon disulfide
ND
1000
8156
ug/L
82
35-150
Carbon tetrachloride
ND
1000
9664
ug/L
97
56-150
Chlorobenzene
ND
1000
1140
ug/L
114
70-130
Chlorodibromomethane
ND
1000
1000
ug/L
100
66-140
Chloroethane
ND
1000
1074
ug/L
107
58.141
Chloroform
ND
1000
1004
ug/L
100
66-138
Chloromethane
ND
1000
1058
ug/L
106
10-150
2-Chlorotoluene
ND
1000
1118
ug/L
112
67-138
4-Chlorotoluene
ND
1000
1092
ug/L
109
69-138
cis-1,2-Dichloroethene
10300
1000
12240 4
ug/L
191
68-131
cis- 1,3-Dichloropropene
ND
1000
1057
ug/L
106
70-133
1,2-Dibromo-3-Chloropropane
ND
1000
1033
ug/L
103
38-138
1,2-Dibromoethane(EDB)
ND
1000
1072
ug/L
107
65-137
Dibromomethane
ND
1000
1023
ug/L
102
70-130
1,2 -Dichlorobenzene
ND
1000
1117
ug/L
112
70-130
1,3 -Dichlorobenzene
ND
1000
1139
ug/L
114
68-131
TestAmerica Nashville
Page 35 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerlca Job ID 490-127126-1
SDG DSO -80
Method: 82608 - Volatile Organic Compounds (GC/IVIS)
(Continued)
Lab Sample ID: 490-127126-2 MS
Client Sample ID: MW -2S
Matrix: Water
Prep Type: Total/NA
Analysis Batch- 425892
Sample Sample
Spike
MS MS
%Rec
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,4 -Dichlorobenzene
ND
1000
1109
ug/L
111
70-130
Dichlorodifluoromethane
ND
1000
9127
ug/L
91
10-150
1,1-Dichloroethane
ND
1000
9822
ug/L
98
61-139
1,2-Dichloroethane
ND
1000
1026
ug/L
103
64-136
1,1-Dichloroethene
ND
1000
1034
ug/L
103
54-150
1,2-Dichloroethene,Total
10400
2000
13340 4
ug/L
146
60-134
1,2-Dichloropropane
ND
1000
1077
ug/L
108
67-130
1,3-Dichloropropane
ND
1000
1178
ug/L
118
70-130
2,2-Dichloropropane
ND
1000
1051
ug/L
105
50-146
1,1-Dichloropropene
ND
1000
1028
ug/L
103
54-150
Dusopropyl ether
ND
1000
9576
ug/L
96
56-142
Ethylbenzene
ND
1000
1130
ug/L
113
65-139
Hexachlorobutadiene
ND
1000
9475
ug/L
95
61-141
2-Hexanone
ND
5000
5913
ug/L
118
44-150
Isopropylbenzene
ND
1000
1128
ug/L
113
70-137
Methylene Chloride
ND
1000
1042
ug/L
104
64-130
4-Methyl-2-pentanone(MIBK)
ND
5000
5789
ug/L
116
50-140
Methyl tert-butyl ether
ND
1000
9388
ug/L
94
55-141
Naphthalene
ND
1000
9928
ug/L
99
32-150
n-Butylbenzene
ND
1000
1049
ug/L
105
61-141
N-Propylbenzene
ND
1000
1180
ug/L
118
53-150
p-Isopropyltoluene
ND
1000
1057
ug/L
106
66-137
sec -Butyl benzene
ND
1000
1091
ug/L
109
55-136
Styrene
ND
1000
1120
ug/L
112
70-130
tert-Butylbenzene
ND
1000
1085
ug/L
107
70-138
1,1,1,2 -Tetrachloroethane
ND
1000
1077
ug/L
108
70-131
1,1,2,2 -Tetrachloroethane
ND
1000
1127
ug/L
113
56-145
Tetrachloroethene
ND
1000
1146
ug/L
115
57-138
Toluene
ND
1000
1146
ug/L
115
64-136
trans-1,2-Dichloroethene
131
1000
1102
ug/L
97
59-143
trans-1,3-Dichloropropene
ND
1000
9979
ug/L
100
63-142
1,2,3-Tnchlorobenzene
ND
1000
1022
ug/L
102
36-150
1,2,4-Tnchlorobenzene
ND
1000
1015
ug/L
102
47-147
1,1,1 -Trichloroethane
ND
1000
9960
ug/L
100
68-144
1,1,2 -Trichloroethane
ND
1000
1179
ug/L
118
70-130
1,4 -Dioxane
ND
20000
18870
ug/L
94
11-150
Trichloroethene
ND
1000
1065
ug/L
106
63-135
Trichlorofluoromethane
ND
1000
1097
ug/L
110
44-150
1,2,3-Trichloropropane
ND
1000
1124
ug/L
112
65-131
1,2,4-Tnmethylbenzene
ND
1000
1083
ug/L
108
64-136
1,3,5-Trimethylbenzene
ND
1000
1076
ug/L
108
69-139
Vinyl chloride
ND
1000
1008
ug/L
101
57-150
Xylenes, Total
ND
2000
2216
ug/L
111
69-132
MS MS
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
98
70-130
Dibromofluoromethane (Surr)
92
70-130
1,2-Dichloroethane-d4 (Surr)
94
70-130
TestAmenca Nashville
Page 36 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmerica Job ID 490-127126-1
SDG DSO -80
Method: 8260B - Volatile
Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-127126-2
MS
Client Sample ID: MW
-2S
Matrix. Water
Prep Type: Total/NA
Analysis Batch: 425892
MS MS
Surrogate
%Recovery Qualifier
Limits
Toluene -d8 (Surr)
102
70-130
Lab Sample ID: 490-127126-2
MSD
Client Sample ID: MW
-2S
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425892
Sample Sample
Spike
MSD MSD
%Rec
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
ND F2
5000
5274 F2
ug/L
105
39-150
36
28
Benzene
ND
1000
1105
ug/L
110
55-147
3
22
Bromobenzene
ND
1000
1087
ug/L
109
60-133
1
18
Bromochloromethane
ND
1000
1064
ug/L
106
59-132
5
21
Bromodichloromethane
ND
1000
9680
ug/L
97
70-140
4
196
Bromoform
ND
1000
8534
ug/L
85
53-150
1
20
Bromomethane
ND
1000
1108
ug/L
111
30-150
6
44
2-Butanone (MEK)
ND
5000
6084
ug/L
122
50-143
1
28
Carbon disulfide
ND
1000
9532
ug/L
95
35-150
16
34
Carbon tetrachloride
ND
1000
9977
ug/L
100
56-150
3
18
Chlorobenzene
ND
1000
1145
ug/L
115
70-130
0
15
Chlorodibromomethane
ND
1000
9923
ug/L
99
66-140
1
19
Chloroethane
ND
1000
1190
ug/L
119
58-141
10
31
Chloroform
ND
1000
1081
ug/L
108
66-138
7
21
Chloromethane
ND
1000
1137
ug/L
114
10-150
7
43
2-Chlorotoluene
ND
1000
1128
ug/L
113
67-138
1
17
4-Chlorotoluene
ND
1000
1091
ug/L
109
69-138
0
15
cis-1,2-Dichloroethene
10300
1000
12480 4
ug/L
215
68-131
2
21
cis- 1,3-Dichloropropene
ND
1000
1059
ug/L
106
70-133
0
19
1,2-Dibromo-3-Chloropropane
ND
1000
1052
ug/L
105
38-138
2
26
1,2-Dibromoethane (EDB)
ND
1000
1109
ug/L
111
65-137
3
21
Dibromomethane
ND
1000
1066
ug/L
107
70-130
4
19
1,2 -Dichlorobenzene
ND
1000
1146
ug/L
115
70-130
3
15
1,3 -Dichlorobenzene
ND
1000
1135
ug/L
113
68-131
0
14
1,4 -Dichlorobenzene
ND
1000
1121
ug/L
112
70-130
1
14
Dichlorodifluoromethane
ND
1000
1012
ug/L
101
10-150
10
50
1,1-Dichloroethane
ND
1000
1109
ug/L
111
61-139
12
23
1,2-Dichloroethane
ND
1000
1039
ug/L
104
64-136
1
22
1,1-Dichloroethene
ND
1000
1124
ug/L
112
54-150
8
24
1,2-Dichloroethene, Total
10400
2000
13720 4
ug/L
164
60-134
3
22
1,2-Dichloropropane
ND
1000
1108
ug/L
111
67-130
3
19
1,3-Dichloropropane
ND
1000
1110
ug/L
111
70-130
6
17
2,2 -Di chloro propane
ND
1000
1117
ug/L
112
50-146
6
20
1,1-Dichloropropene
ND
1000
1049
ug/L
105
54-150
2
24
Dusopropyl ether
ND
1000
1048
ug/L
105
56-142
9
22
Ethylbenzene
ND
1000
1124
ug/L
112
65-139
1
18
Hexachlorobutadiene
ND
1000
9991
ug/L
100
61-141
5
26
2-Hexanone
ND
5000
5700
ug/L
114
44-150
4
21
Isop ropylbenzene
ND
1000
1132
ug/L
113
70-137
0
17
Methylene Chloride
ND
1000
1126
ug/L
113
64-130
8
22
4-Methyl-2-pentanone (MIBK)
ND
5000
5782
ug/L
116
50-140
0
24
TestAmerlca Nashville
Page 37 of 46 4/30/2017
QC Sample Results
Client Hart & Hickman, PC
TestAmerica Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG DSO -80
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-127126-2
MSD
Client Sample ID: MW -2S
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 425892
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Methyl tert-butyl ether
ND
1000
1025
ug/L
103
55-141
9
24
Naphthalene
ND
1000
1054
ug/L
105
32-150
6
40
n-Butylbenzene
ND
1000
1073
ug/L
107
61-141
2
17
N-Propylbenzene
ND
1000
1178
ug/L
118
53-150
0
18
p-Isopropyltoluene
ND
1000
1086
ug/L
109
66-137
3
16
sec -Butyl benzene
ND
1000
1121
ug/L
112
55-136
3
50
Styrene
ND
1000
1099
ug/L
110
70-130
2
16
tert-Butyl benzene
ND
1000
1106
ug/L
109
70-138
2
17
1,1,1,2 -Tetrachloroethane
ND
1000
1069
ug/L
107
70-131
1
16
1,1,2,2 -Tetrachloroethane
ND
1000
1163
ug/L
116
56-145
3
19
Tetrachloroethene
ND
1000
1119
ug/L
112
57-138
2
17
Toluene
ND
1000
1118
ug/L
112
64-136
2
18
trans-1,2-Dichloroethene
131
1000
1236
ug/L
111
59-143
11
25
trans-1,3-Dichloropropene
ND
1000
9677
ug/L
97
63-142
3
18
1,2,3-Tnchlorobenzene
ND
1000
1079
ug/L
108
36-150
5
43
1,2,4-Tnchlorobenzene
ND
1000
1046
ug/L
105
47-147
3
24
1,1,1 -Trichloroethane
ND
1000
1090
ug/L
109
68-144
9
17
1,1,2 -Trichloroethane
ND
1000
1131
ug/L
113
70-130
4
18
1,4 -Dioxane
ND
20000
19290
ug/L
96
11-150
2
50
Trichloroethene
ND
1000
1096
ug/L
110
63-135
3
17
Trichlorofluoromethane
ND
1000
1139
ug/L
114
44-150
4
32
1,2,3-Trichloropropane
ND
1000
1148
ug/L
115
65-131
2
19
1,2,4-Trimethylbenzene
ND
1000
1095
ug/L
109
64-136
1
18
1,3,5-Tnmethylbenzene
ND
1000
1080
ug/L
108
69-139
0
17
Vinyl chloride
ND
1000
1086
ug/L
109
57-150
7
37
Xylenes, Total
ND
2000
2179
ug/L
109
69-132
2
17
MSD MSD
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surf)
101
70-130
Dibromofluoromethane (Surf)
95
70-130
1,2-Dichloroethane-d4 (Surr)
97
70-130
Toluene -d8 (Surr)
101
70-130
TestAmerica Nashville
Page 38 of 46 4/30/2017
QC Association Summary
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
GC/MS VOA
Analysis Batch: 425499
TestAmenca Job ID 490-127126-1
SDG DSO -80
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-127126-2
MW -2S
Total/NA
Water
8260B
490-127126-4
MW -3
Total/NA
Water
8260B
490-127126-6
MW -5
Total/NA
Water
8260B
490-127126-8
MW -7
Total/NA
Water
8260B
490-127126-9
MW -8
Total/NA
Water
8260B
MB 490-425499/7
Method Blank
Total/NA
Water
8260B
LCS 490-425499/3
Lab Control Sample
Total/NA
Water
8260B
LCSD 490-425499/4
Lab Control Sample Dup
Total/NA
Water
8260B
490-127126-1 MS
MW -1
Total/NA
Water
8260B
490-127126-1 MSD
MW -1
Total/NA
Water
8260B
Analysis Batch: 425892
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-127126-1
MW -1
Total/NA
Water
8260B
490-127126-2
MW -2S
Total/NA
Water
8260B
490-127126-3
MW -2D
Total/NA
Water
8260B
490-127126-4
MW -3
Total/NA
Water
8260B
490-127126-5
MW -4
Total/NA
Water
8260B
490-127126-6
MW -5
Total/NA
Water
8260B
490-127126-7
MW -6
Total/NA
Water
8260B
490-127126-8
MW -7
Total/NA
Water
8260B
MB 490-425892/7
Method Blank
Total/NA
Water
8260B
LCS 490-425892/4
Lab Control Sample
Total/NA
Water
8260B
490-127126-2 MS
MW -2S
Total/NA
Water
8260B
490-127126-2 MSD
MW -2S
Total/NA
Water
8260B
Prep Batch
Prep Batch
TestAmenca Nashville
Page 39 of 46 4/30/2017
Lab Chronicle
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1
SDG DSO -80
Client Sample ID: MW -1
Lab Sample ID: 490-127126-6
Date Collected: 04/24/17 14:45
Lab Sample ID: 490-127126-1
Date Collected: 04/24/17 08:55
Date Received: 04/26/17 09:20
Matrix: Water
Dil Initial
Date Received: 04/26/17 09:20
Batch Prepared
iPrep Type Type Method
Run Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 82606
Batch Batch
10 mL
Dil
Initial
Final
Batch Prepared
425499 04/27/17 15 32 NC TAL NSH
Prep Type Type Method
Run
Factor
Amount
Amount
Number or Analyzed Analyst Lab
I- -
LTotal/NA Analysis 8260B
1
10 mL
10 mL
425892 04/28/17 14 14 BBR TAL NSH
Client Sample ID: MW -2S
Lab Sample ID: 490-127126-2
Date Collected: 04/24/17 11:00
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
l;
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 82606
50
10 mL
10 mL
425892 04/28/17 18 43 BBR TAL NSH
L Total/NA Analysis 82608
1
10 mL
10 mL
425499 04/27/17 14 40 NC TAL NSH
Client Sample ID: MW -2D
Lab Sample ID: 490-127126-3
Date Collected: 04/24/17 10:25
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run
Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 82606
1
10 mL
10 mL
425892 04/28/17 14 38 BBR TAL NSH
Client Sample ID: MW -3
Lab Sample ID: 490-127126-4
Date Collected: 04/24/17 09:45
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
Dil
Initial
Final
Batch Prepared
Ii Prep Type Type Method
Run
Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 8260B
1
10 mL
10 mL
425892 04/28/17 15 03 BBR TAL NSH
Total/NA Analysis 8260B
1
10 mL
10 mL
425499 04/27/17 15 06 NC TAL NSH
Client Sample ID: MW -4 Lab Sample ID: 490-127126-5
Date Collected: 04/24/17 12:25 Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
I—Total/NA Analysis 82608 1 10 mL 10 mL 425892 04/28/17 15 27 BBR TAL NSH
Client Sample ID: MW -5
Lab Sample ID: 490-127126-6
Date Collected: 04/24/17 14:45
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
Dil Initial
Final
Batch Prepared
iPrep Type Type Method
Run Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 82606
1 10 mL
10 mL
425892 04/28/17 15 52 BBR TAL NSH
Total/NA Analysis 82608
1 10 mL
10 mL
425499 04/27/17 15 32 NC TAL NSH
TestAmerica Nashville
Page 40 of 46 4/30/2017
Lab Chronicle
Client Hart & Hickman, PC
TestAmerica Job ID 490-127126-1
Project/Site McCorkles Cleaners
SDG DSO -80
Client Sample ID: MW -6
Lab Sample ID: 490-127126-7
Date Collected: 04/24/17 15:30
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
Dil
Initial
Final
Batch Prepared
[Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
1 Total/NA Analysis 8260B
1
10 mL
10 mL
425892 04/28/17 16 16 BBR TAL NSH
Client Sample ID: MW -7
Lab Sample ID: 490-127126-8
Date Collected: 04/24/17 16:30
Matrix: Water
Date Received: 04/26/17 09:20
Batch Batch
Dd
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab 13
Total/NA Analysis 8260B
1
10 mL
10 mL
425892 04/28/17 16 41 BBR TAL NSH
Total/NA Analysis 82606
1
10 mL
10 mL
425499 04/27/17 15 58 NC TAL NSH
Client Sample ID: MW -8
Lab Sample ID: 490-127126-9
Date Collected: 04/24/17 17:20
Matrix: Water
Date Received: 04/26/17 09:20
F Batch Batch
Dd
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
I Total/NA Analysis 82608
1
10 mL
10 mL
425499 04/27/17 16 24 NC TAL NSH
Laboratory References:
TAL NSH = TestAmenca Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmenca Nashville
Page 41 of 46 4/30/2017
Method Summary
Client Hart & Hickman, PC
Project/Site McCorkles Cleaners
TestAmenca Job ID 490-127126-1 Y
SDG DSO -80
Method Method Description Protocol Laboratory
82606 Volatile Organic Compounds (GC/MS) SW846 TAL NSH
Protocol References:
SW846 = 'Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates
Laboratory References•
TAL NSH = TestAmenca Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmenca Nashville
Page 42 of 46 4/30/2017
Accreditation/Certification Summary
Client Hart & Hickman, PC TestAmerlca Job ID 490-127126-1 -
Project/Site McCorkles Cleaners SDG DSO -80
Laboratory: TestAmerica Nashville
The accreditations/certifications listed below are applicable to this report
F1 Authority Program
North Carolina (WW/SV11) State Program
EPA Region Identification Number Expiration Date
4 387 12-31-17
Page 43 of 46
TestAmerica Nashville
4/30/2017
€a°
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORM ' 90-1271" Chai9111111111111 "'
490-127126 Chain of Custody
Cooler Received/Opened On 4/26/2017 Ca) 0920
Time Samples Removed From Cooler Time Samples Placed In Storage"(2 Hour Window)
1 Tracking # 663,0 (last 4dig�its, FedEx) Courier: FedEx
IR Gun ID/�
_160656843 pH Strip Lot � 11V Chlorine Strip Lo4Ei
2. Temperature of rep. sample or temp blank when opened: L. 3 Degrees Celsius
3. if Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO.. V�A
4. Were custody seals on outside of cooler? Y - NO.AA
If yes, how many and where: "r%'7 /l 4-
5. Were the seals intact, signed, and dated correctly? YE ...NO ... NA
6. Were custody papers inside cooler?, I _ Y�E ...NO. NA
I certify that 1 opened the cooler and answered questions 1-6 (Intial) t��( �•
7. Were custody seals on containers: YES( and Intact YES. .NO... A
Were these signed and dated correctly? YES ... NO..4�A
8. Packing mat'I used? BubblewraG' P�asticPeanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: (�/ ce Ice -pack Ice (direct contact) Dry ice /O"�ther None
10. Did all containers arrive in good condition (unbroken)? rlmt...NO.. NA
11. Were all container labels complete (#, date, signed, pres., etc)? ..NO ... NA
12. Did all container labels and tags agree with custody papers? _NO ... NA
!L
13a. Were VOA vials received? e� ,ln0.&-<A
b. Was there any observable headspace present in any VOA vial? YES ... NO..&,
14. Was there a Trip Blank in this cooler? YES .. O.. A If multiple coolers, sequence #
I certify that 1 unloaded the cooler and answered ques ions 7-14 (Intial)
15a. On pres'd bottles, �i H test strips suggest preservation reached the correct pH level? YESA ..NA
b. Did the bottle labels indicate that the correct preservatives were used ES ..NO ... NA
16 Was residual chlorine present? YES ... Nt
I certifythat I checked for chlorine and PH as per SOP and answered questions 15-16 (Intial)
17. Were custody papers properly filled out (ink, signed, etc)? YE NO.. NA
18. Did you sign the custody papers In the appropriate place?
19. Were correct containers used for thianalysis requested?
20. Was sufficient amount of sample sent in each container?
21. Were there Non -Conformance issues at login? YE$ .Was a NCM generated?
S .NO ... NA
S NO ... NA
S.. O.. NA
)
BIS = Broken in shipment
Cooler Receipt Form doc LF -I Revised 12/15/15
End of Form
Page 44 of 46 4/30/2017
Chafttte Service Center
Chan ofTestAmerica
Temperature on Receipt C)
Custody Record
M
DMA-ingWater7 Yes❑ /VoA THE LEADER IN ENVIRONMENTAL TESTING cr
TAI _A1 2a n nnn
client
C,<-*\- 9 4 k& 2 L
F-Jecl Manager
SVNC,"_ S Co
Date
LI)Qq11:7-
Cham of custody Number
287937
Address _
OLIW U Vilv� 6 y S _W_ 166
Telephone Number (Area Code)/Fax Number
40"i — _0604
Lab Number
1
Page __L_ Of 1
City
StRte
Zlp Code
Sde ContactLab Contact
wiC vA 4i4A Yk
t
Analysis (.4ltach /rst d
more space /s needed)
Specia//nstructions/
Conditions of Receipt
Project Name and Location (State)
AC-G cYc
Can7L-r1Waybd/Number
ConlracUPurdtase OMei/Quote No
— C /o
UV
MWIN
Containers &
Preservatives
Sample /.D. No and Descnpbon
(Containers for each sample maybe combined on one line)
Date
Time
ei
3
fV\W-
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Poss/b/e Hazard /denbAcatlon
ElNon-Hazard ❑ Flammable 1:1 slur, /mtant ElPoison B Unknown
Sampla Disposal (A fee may be assessed rfsamp/es are retained
ElReturn To client Dlsposa/By Lab ❑ Archive For Months longerthan 1 month)
rum.arouna rime rrequueo` uG Hegmrements Ppr ecrty)
❑ 24 Hours ❑ 48 Hours ❑ 7Days ❑ MDays ❑ 21 Days A Other H} Ski \LE4i �y
> Re/rngmshed By I y I p'tp 1 ReceeoIL A 1 n 1411 Date Time
DISTRIBUTION. WH/TE- Returned to Client wdh Report, CANARY- Stays with the Sample, PINK- Fie/d Copy
0
m
Login Sample Receipt Checklist
Client Hart & Hickman, PC
Login Number: 127126
List Number: 1
Creator: Vest, Laura E
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter
The cooler's custody seal, if present, is intact
True
Sample custody seals, if present, are intact
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with
Samples were received on ice
True
Cooler Temperature is acceptable
True
Cooler Temperature is recorded
True
COC is present
True
COC is filled out in ink and legible
True
COC is filled out with all pertinent information
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels
True
Containers are not broken or leaking
True
Sample collection date/times are provided
True
Appropriate sample containers are used
True
Sample bottles are completely filled
True
Sample Preservation Verified
N/A
There is sufficient vol for all requested analyses, incl any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4")
Multiphasic samples are not present
True
Samples do not require splitting or compositing
True
Residual Chlorine Checked
N/A
TestAmerica Nashville
Page 46 of 46
Job Number 490-127126-1
SDG Number DSO -80
List Source: TestAmenca Nashville
4/30/2017
F3