NC0021253_Renewal (Application)_20180103

NOATHC.i1?0
'ACORPORATED 15�
CITY OF HAVELOCK
Post Office Box 368
1 Governmental Ave.
Havelock, NC 28532
December 15, 2017
Water Quality Permitting Section — NPDES
Division of Water Resources
North Carolina Department of Environmental Quality
1617 Mail Service Center Raleigh, NC, 27699-1617
Re: NPDES Permit Renewal Application (NC0021253)
City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
To whom it may concern:
REDEIVEDIDeNRIDWR
DEC 3 12017
Water Resources
Permitting Section
The City of Havelock Public Services Department is permitted to discharge 2.25 million gallons per day (mgd) of
treated effluent from the City of Havelock Wastewater Treatment Plant (WWTP) to the Neuse River under North
Carolina NPDES Permit NC0021253. This NPDES permit is scheduled to expire on June 30, 2018. The enclosed
application is for the renewal of this permit In accordance with the requirements of federal (40 CFR 122) and state
(15A NCAC 2H .0105(3)) regulations, we are submitting three signed copies of the completed application package
and associated attachments and figures. The application package includes the following information:
• NPDES Permit Application — EPA Form 2A
• EPA Form 2A Additional Information (Process Narrative, Topographic Map, and Process Flow Diagrams)
• City of Havelock WWTP Sludge Management Plan
• First Species Effluent Toxicity Testing, 2015-2017
• Annual Priority Pollutant Analysis Results, 2014-2017
• Technical Memorandum in support of the Reduction of Monitoring Frequency for Exceptionally Performing
Facilities
At the time of this application submittal, the required second species toxicity testing events have not yet been
completed. The four second species effluent toxicity tests are currently scheduled to be completed in December 2017,
January 2018, March 2018, and May 2018. When the toxicity test results become available, they will be forwarded to
the Division of Water Resources (DWR) along with revisions to Part E of EPA Form 2A to include these results. All
second species toxicity tests will be submitted prior to the current permit expiration date of June 30, 2018.
A sample for the annual priority pollutant analysis was not taken in 2016. In it's place, a second sample was taken in
early December 2017. The annual priority pollutant analysis section is currently based on data collected in 2014, 2015,
and 2017. Part D of form 2A as well as Tab E will be updated to replace the 2014 data with the additional 2017 data
when that data becomes available.
Phone [phone] www.havelocknc us Fax [phone]

In accordance with 15A NCAC 2B 0508(b)(1) and the October 2012 DWR Guidance Docuinent for the Reduction of
Monitoring Frequency for Exceptionally Performing Facilities, the City of Havelock respectfully requests a reduction
in frequency monitoring for total suspended solids (TSS), ammonia (NH3-N), and fecal coliform. Effluent sampling
results from the past three years deinonstrate that all state and regulatory and guidance requirements have been met in
support of this request A complete summary of the sampling data and analysis for the reduction of monitoring
frequency is attached in Tab G of this application
If you have any questions regarding any of the NPDES permit renewal application materials, please contact me at (252)
444-6409 or msavaerOhavelocknc us
Sincerely,
4-0��
Mark Sayger
Public Services Director
Attachments
cc
Raymond Burgos, City of Havelock
Mary Sadler, Hazen and Sawyer
Todd Davis, Hazen and Sawyer
Ted Elshof, Hazen and Sawyer
Phone [phone] www havelocknc us Fax [phone]

NPDES Permit Application
City of Havelock, North Carolina
City of Havelock Wastewater Treatment Plant
Table of Contents
Tab A. EPA Form 2A
Tab B. EPA Form 2A Additional Information
a. Measures to Reduce Infiltration and Inflow
b. Process Description
c. Topographic Map
d. Site Map
e Process Flow Diagram
Tab C. Sludge Management Plan
Tab D. Summary of First Species Effluent Toxicity Testing, 2015-2017
Tab E. Annual Priority Pollutant Analysis Results, 2014-2017
Tab F. Second Species Toxicity Testing Results
Tab G. Exceptionally Performing Facilities, Reduction in Frequency Monitoring Analysis

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
EPA Form 2A, NPDES Renewal Application December 2017

FAGILITY NAME, AND PERMIT NUMBER,,
PERMITACTION RE,QU15STED.,
RIVER BASIN
City of Havelock VWVTP, NCO021253
Renewal
Neuse River
FORM
2A NPDES FORM 2A APPLICATION OVERVIEW
NPDES
APPLICATION OVERVIEW
Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet
and a "Supplemental Application Information" packet. The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and C Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet. The following items explain which parts of Form 2A you must complete.
BASIC APPLICATION INFORMATION:
A Basic Application Information for all Applicants All applicants must complete questions A 1 through A 8o A treatment works
Chat discharges effluent to su'rf'ace waters of the United -States must also answer questions A 9 througti A 12.
B Additional Application Information for Applicants with a Design Flow z 0 1 mgd All treatment works that have design flows
greater than or equal to 0 1 million gallons per day most complete questions B 1 through 8.6
C„ Certification. All applicants must complete Part C (Certification)„
SUPPLEMENTAL APPLICATION INFORMATION.
D Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets
one or more of the following crilera must complete Part D (Expanded Effluent Testing Data)'
1 Has a design flow rate greater than or equal to 1mgd,
2, Is required to have a pretreatment program (or has one In place), or
3 Is otherwise required by the permitting authority to provide the Information
E. 'Toxicity Testing Data A treatment works that meets one or more of the following criteria must complete Part l= (Toxicity Testing
Data)`
I Has a design flow rate greater than or equal to 'I mgd,
2 Is required to have a pretreatment program (or has one in place), or
I
3. Is otherwise, required by the permitting authority to submit results of tonicity testing.
F Industrial User Discharges and RCRA%CERCLA Wastes- A treatment works that accepts process wastewater from any
significant industrial users (SIUs) or receives RCRA or CERCLA wastes musf complete Part P (Industrial User Discharges
and RCRAICE'RCLA Wastes) SIUs are defined as'
1 All Pndustrlal users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403 6 and 40
CFR Chapter I, Subchapter N (see instructions), and
'2a Any other industrial user that.
a Discharges an average of 25,OOQ gallons ,per day or more of process wastewater to the treatment works (vuith oertam
exclusions), or
I
b Contributes a process wastestream that makes, up 5 peroent or more of the, average dry weather hydraulic or organic
capacity of the treatment plant, or
c 'Is designated as an SIU by the, control authority
G Combined Sewer,Systems A treatment works that ,has a combined sewer system must complete Part G (Combined Sewer
Systems)
ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION)
ERA, Form 3510-2A (Rev 1-99), Replaces EPA forms 7550-6 & 7,550-2Z Page 1 of 17'

FACILITY NAME AND PERMIT NUMBER-
PERMIT ACTION REQUESTED
RIVER BASIN•
City of Havelock WWTP, NCO021253
Renewal
Neuse River
BASIC APPLICATION INFORMATION
PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS:
All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet
Al Facility Information
Facility Name City of Havelock Wastewater Treatment Plant
Mailing Address P O Box 368, Havelock NC 28532
Contact Person Raymond Burgos
Title Wastewater Treatment Plant B-ORC
Telephone Number [phone]
Facility Address 304 North Jackson Dr
(not P O Box) Havelock, NC 28532
A.2 Applicant Information If the applicant is different from the above, provide the following
Applicant Name City of Havelock
Mailing Address P O Box 368
Havelock, NC 28532
Contact Person Mark Sayger
Title Public Services Director
Telephone Number [phone]
Is the applicant the owner or operator (or both) of the treatment works?
® owner ® operator
Indicate whether correspondence regarding this permit should be directed to the facility or the applicant
❑ facility ® applicant
A.3 Existing Environmental Permits Provide the permit number of any existing environmental permits that have been issued to the treatment works
(include state -issued permits)
NPDES NCO021253 PSD 091101301 (General Air Permit)
UIC Other WQ0000702 (Land Application Permit)
_RCRA Other WQCS00104 (Collection System Permit)
A.4 Collection System Information Provide information on municipalities and areas served by the facility Provide the name and population of each
entity and, if known, provide information on the type of collection system (combined vs separate) and its ownership (municipal, private, etc)
Name Population Served Type of Collection System Ownership
Havelock, NC 12,500 Separate Municipal
Total population served 12.500
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 2 of 17

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED- RIVER BASIN:
City of Havelock WWTP, NCO021253 Renewal Neuse River
A.5 Indian Country
a Is the treatment works located in Indian Country?
❑ Yes ® No
b Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through)
Indian Country?
❑ Yes ® No
A.6 Flow Indicate the design flow rate of the treatment plant (i e , the wastewater flow rate that the plant was built to handle) Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years Each year's data must be based on a 12 -month time period
with the 12th month of "this year' occurring no more than three months prior to this application submittal
a Design flow rate 2 25 mgd
Two Years Apo Last Year This Year
(10/1/2014 - 9/30/2015) (10/1/2015 - 9/30/2016) (10/1/2016 - 9/30/2017)
b Annual average daily flow rate 1.377 1 356 1 304
c Maximum daily flow rate 2 810 3 161 3 233
A.7 Collection System Indicate the type(s) of collection system(s) used by the treatment plant Check all that apply Also estimate the percent
contribution (by miles) of each
® Separate sanitary sewer 100 %
❑ Combined storm and sanitary sewer N/A %
A.8 Discharges and Other Disposal Methods.
a Does the treatment works discharge effluent to waters of the U S ? ® Yes ❑ No
If yes, list how many of each of the following types of discharge points the treatment works uses
I Discharges of treated effluent
II Discharges of untreated or partially treated effluent 0
ui Combined sewer overflow points
IV Constructed emergency overflows (prior to the headworks)
V Other N/A
b Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U S ? ❑ Yes ® No
If yes, provide the following for each surface impoundment
Location
Annual average daily volume discharge to surface impoundment(s)
Is discharge ❑ continuous or ❑ intermittent?
c Does the treatment works land -apply treated wastewater?
If yes, provide the following for each land application site
Location
Number of acres
❑ Yes ® No
Annual average daily volume applied to site
Is land application ❑ continuous or ❑ intermittent?
d Does the treatment works discharge or transport treated or untreated wastewater to another
treatment works? ❑ Yes
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22
® No
mgd
mgd
Page 3 of 17

FACILITY NAME AND PERMIT NUMBER PERMIT ACTION REQUESTED RIVER BASIN -
City of Havelock WWTP, NCO021253 Renewal Neuse River
If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e g , tank truck, pipe)
N/A
If transport is by a party other than the applicant, provide
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number ( )
For each treatment works that receives this discharge, provide the following
Name
Mailing Address
Contact Person
Title
Telephone Number ( )
If known, provide the NPDES permit number of the treatment works that receives this discharge
Provide the average daily flow rate from the treatment works into the receiving facility
e Does the treatment works discharge or dispose of its wastewater in a manner not included
in A 8 through A 8 d above (e g , underground percolation, well injection)
If yes, provide the following for each disposal method
Description of method (including location and size of site(s) if applicable)
Annual daily volume disposed by this method
Is disposal through this method ❑ continuous
or ❑ intermittent?
mgd
❑ Yes ® No
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 4 of 17

FACILITY NAME AND PERMIT NUMBER- PERMIT ACTION REQUESTED RIVER BASIN'
City of Havelock WWTP, NCO021253 Renewal Neuse River
WASTEWATER DISCHARGES:
If you answered "Yes" to question Ag a, complete questions A.9 through A.12 once for each outfall (including bypass points) through
which effluent is discharged Do not include information on combined sewer overflows in this section If you answered "No" to question
A.B.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd."
A.9 Description of Outfall
a Outfall number 002
b Location City of Havelock 28532
(City ortown, if applicable) (Zip Code)
Craven NC
(County) (State)
34°57'11" 76°52'37"
(Latitude) (Longitude)
c Distance from shore (if applicable) 2.040 ft
d Depth below surface (if applicable) 10 ft
e Average daily flow rate 14 mgd
f Does this outfall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A 9 g )
If yes, provide the following information
Number f times per year discharge occurs
Average duration of each discharge
Average flow per discharge
Months in which discharge occurs
g Is outfall equipped with a diffuser?
A.10. Description of Receiving Waters.
® Yes ❑ No
mgd
a Name of receiving water Neuse River
b Name of watershed (if known) Neuse River
United States Soil Conservation Service 14 -digit watershed code (if known) 03020204050020
c Name of State Management/River Basin (if known) Neuse River
United States Geological Survey 8 -digit hydrologic cataloging unit code (if known) 03020204
d Critical low flow of receiving stream (if applicable)
acute Unknown cfs chronic Unknown cfs
e Total hardness of receiving stream at critical low flow (if applicable) Unknown mg/I of CaCO3
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 $ 7550-22 Page 5 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED-
RIVER BASIN:
City of Havelock WWTP, NCO021253
Renewal
Neuse River
A.11. Description of Treatment
a What level of treatment are provided? Check all that apply
❑ Primary ® Secondary
® Advanced ® Other Describe Denitrification filters
b Indicate the following removal rates (as applicable)
Design BOD5 removal or Design CBOD5 removal 96 %
Design SS removal 84 %
Design P removal 78 %
Design N removal 91% at current design flow of 2 25 mgd
Other N/A %
c What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe
Ultraviolet Disinfection
If disinfection is by chlorination is dechlonnation used for this outfalls ❑ Yes ❑ No
Does the treatment plant have post aerations ® Yes ❑ No
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharged Do not include information an combined sewer overflows in this section. All information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods In addition, this data must comply with QAIQC requirements of
40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136 Ate
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
Outfall number 002
MAXIMUM DAILY VALUE
AVERAGE DAILY VALUE
PARAMETER
Value
Units
Value
Units
Number of Samples
pH (Minimum)
6.10
s u
pH (Maximum)
8.30
s u
Flow Rate
3.16
mgd
1.46
mgd
1,093
Temperature (Winter)
23.90
°C
17.16
°C
227
Temperature (Summer)
28.60
°C
23.79
°C
446
' For pH please report a minimum and a mawmum daily value
MAXIMUM DAILY
AVERAGE DAILY DISCHARGE
DISCHARGE
ANALYTICAL
POLLUTANT
METHOD
ML/MDL
Conc.
Units
Conc.
Units
Number of
Samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BIOCHEMICAL OXYGEN
BOD5
63.00
m /L
2.74
m /L
728
SM 5210B
ML
DEMAND (Report one)
CBOD5
N/A
N/A
N/A
N/A
N/A
N/A
N/A
FECAL COLIFORM
1210
No./
10.088
No./
718
SM 9222D
ML
100mL
100mL
TOTAL SUSPENDED SOLIDS (TSS)
22
m /L
2.64
1 m /L
734
SM 2540D
ML
END OF PART A -
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 6 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED-
RIVER BASIN
City of Havelock WWTP, NCO021253
Renewal
Neuse River
BASIC APPLICATION INFORMATION
PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100,000 gallons per day).
All applicants with a design flow rate 2 0 1 mgd must answer questions B 1 through B 6 All others go to Part C (Certification).
B 1 Inflow and Infiltration Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration
230,000 gpd
Briefly explain any steps underway or planned to minimize inflow and infiltration
The City of Havelock Is maintaining ongoing efforts to Identify and rehabilitate sources of 1/1 In their collection system
B 2 Topographic Map Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries This
map must show the outline of the facility and the following information (You may submit more than one map if one map does not show the entire
area )
Please reference Figure 1 for topographic map and Figure 2 for plant site map
a The area surrounding the treatment plant, including all unit processes
b The mayor pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant Include outfalls from bypass piping, if applicable
c Each well where wastewater from the treatment plant is infected underground
d Wells, springs, other surface water bodies, and drinking water wells that are 1) within'/ mile of the property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant
e Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed
f If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where It is treated, stored, and/or disposed
B 3 Process Flow Diagram or Schematic Provide a diagram showing the processes of the treatment plant, including all bypass piping and all
backup power sources or redunancy in the system Also provide a water balance showing all treatment units, including disinfection (e g ,
chlorination and dechlorination) The water balance must show dally average flow rates at influent and discharge points and approximate daily flow
rates between treatment units Include a brief narrative description of the diagram
Please reference Figure 3 through Figure 5 for process flow diagram and the "Additional Information" sheets for process description
B 4 Operation/Maintenance Performed by Contractor(s)
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? ® Yes ❑ No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional
pages if necessary)
Name Svnagro
Mailing Address 284 Boger Road
Mocksville. NC 27028
Telephone Number [phone]
Responsibilities of Contractor Remove and land apply biosolids to permitted sites
B 5 Scheduled improvements and Schedules of Implementation Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B 5
for each (If none, go to question B 6 )
a List the outfall number (assigned in question A 9) for each outfall that is covered by this Implementation schedule
N/A
b Indicate whether the planned improvements or Implementation schedule are required by local, State, or Federal agencies
❑ Yes ❑ No
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 7 of 17

FACILITY NAME AND PERMIT NUMBER-
PERMIT ACTION REQUESTED-
RIVER BASIN -
City of Havelock WWTP, NCO021253
Renewal
Neuse River
c If the answer to B 5 b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable)
N/A
d Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable
For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable
Indicate dates as accurately as possible
Schedule Actual Completion
Implementation Stage MM/DD/YYYY MM/DD/YYYY
- Begin Construction N/A N/A Plant expansion to 2.25 mgd has been completed since
- End Construction N/A N/A the 2014 NPDES Permit Renewal. Expansion to 2.8
mgd or 3.5 mgd are not planned for this permit cycle.
- Begin Discharge N/A N/A
- Attain Operational Level N/A N/A
e Have appropriate permits/clearances concerning other Federal/State requirements been obtained? ❑ Yes ® No
Describe briefly
B.6. EFFLUENT TESTING DATA (GREATER THAN 01 MGD ONLY)
Applicants that discharge to waters of the US must provide effluent testing data for the following parameters Provide the indicated
effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information
on combine sewer overflows in this section All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate
QAIQC requirements for standard methods for analytes not addressed by 40 CFR Part 136 At a minimum effluent testing data must be
based on at least three pollutant scans and must be no more than four and on -half years old
Outfall Number 002
MAXIMUM DAILY
AVERAGE DAILY DISCHARGE
DISCHARGE
ANALYTICAL
POLLUTANT
METHOD
MLIMDL
Conc.
Units
Conc.
Units
Number of
Samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
AMMONIA (as N)
1140
mg/L
0118
mg/L
735
EPA 350 1
ML 0 5/10
CHLORINE (TOTAL
N/A
NIA
N/A
N/A
N/A
NIA
N/A
RESIDUAL, TRC)
DISSOLVED OXYGEN
480
mg/L
758
mg/L
661
SM 4500-H+B
MDL>5.0
TOTAL KJELDAHL
3500
mg/L
1 287
mg/L
153
EPA 3512
AL 21,400 lbs
NITROGEN (TKN)
TN
NITRATE PLUS NITRITE
9.1
mg/L
297
mg/L
152
EPA 353.2
AL 21,400 lbs
NITROGEN
TN
OIL and GREASE
N/A
NIA
NIA
N/A
N/A
N/A
N/A
PHOSPHORUS (Total)
2.97
mg/L
070
mg/L
151
EPA 365 4
QL 0 7110
TOTAL DISSOLVED SOLIDS
N/A
NIA
NIA
N/A
N/A
N/A
N/A
(TDS)
OTHER
N/A
NIA
N/A
NIA
N/A
NIA
N/A
END OF PART B.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 8 of 17

FACILITY NAME AND PERMIT NUMBER
City of Havelock WWTP, NCO021253
BASIC APPLICATION INFORMATION
PART C. CERTIFICATION
PERMIT ACTION REQUESTED- I RIVER BASIN.
Renewal Neuse River
All applicants must complete the Certification Section Refer to instructions to determine who is an officer for the purposes of this
certification All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview Indicate below which
parts of Form 2A you have completed and are submitting By signing this certification statement, applicants confirm that they have reviewed
Form 2A and have completed all sections that apply to the facility for which this application is submitted
Indicate which parts of Form 2A you have completed and are submitting:
® Basic Application Information packet Supplemental Application Information packet
® Part D (Expanded Effluent Testing Data)
® Part E (To)acity Testing Siomonitonng Data)
❑ Part F (Industrial User Discharges and RCRA/CERCLA Wastes)
❑ Part G (Combined Sewer Systems)
ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who
manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true,
accurate, and complete I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment
for knowing violations
Name and official title
Signature
Telephone number
Date signed
l$ mac- 2p�
Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment
works or identify appropnate permitting requirements
SEND COMPLETED FORMS TO:
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina
27699-1617
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 9 of 17

FACILITY NAME AND PERMIT NUMBER
City of Havelock WWTP, NCO021253
PERMIT ACTION REQUESTED
Renewal
RIVER BASIN
Neuse River
SUPPLEMENTAL APPLICATION INFORMATION
PART D. EXPANDED EFFLUENT TESTING DATA
Refer to the directions on the cover page to determine whether this section applies to the treatment works
Effluent Testing, 1 0 mgd and Pretreatment Works If the treatment works has a design flow greater than or equal to 1 0 mgd or it has (or is required
to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following
pollutants Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which
effluent is discharged Do not include information on combined sewer overflows in this section All information reported must be based on data collected
through analyses conducted using 40 CFR Part 136 methods In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and
other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136 Indicate in the blank rows provided below
any data you may have on pollutants not specifically listed in this form At a minimum, effluent testing data must be based on at least three pollutant
scans and must be no more than four and one-halfyears old
See attached analytical results in Tab E
Outfall number 002 (Complete once for each outfall discharging effluent to waters of the United States )
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLIMDL
Conc.
Units
Mass
Units
Conc
Units
Mass
Units
Number
of
Samples
METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS
ANTIMONY
< 3 0
pg/L
< 0 056
Ib/d
< 3 0
pg/L
< 0 056
Ib/d
3
2008
3
ARSENIC
< 5 0
pg/L
< 0 094
Ib/d
< 5 0
pg/L
< 0 094
Ib/d
3
311313-04
5
BERYLLIUM
20
pg/L
00375
Ib/d
< 1 33
Ng/L
< 0 025
Ib/d
3
2007
1
CADMIUM
< 1 0
pg/L
<0019
Ib/d
< 10
pg/L
< 0 019
Ib/d
3
311313-04
1
CHROMIUM
< 5 0
pg/L
< 0 094
Ib/d
< 5 0
pg/L
< 0 094
Ib/d
3
2007
5
COPPER
< 10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
2007
10
LEAD
< 5 0
pg/L
< 0 094
Ib/d
< 5 0
pg/L
< 0 094
Ib/d
3
311313-04
5
MERCURY
<10
pg/L
<0019
Ib/d
<10
pg/L
< 0 019
Ib/d
7
1631E
1
NICKEL
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
2007
10
SELENIUM
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
311313-04
10
SILVER
<50
pg/L
< 0 094
Ib/d
<50
pg/L
< 0 094
Ib/d
3
2007
5
THALLIUM
<10
pg/L
< 0 019
Ib/d
<10
pg/L
< 0 019
Ib/d
3
2008
1
ZINC
70
pg/L
1 316
Ib/d
4759
pg/L
0 894
Ib/d
3
3111B-99
10
CYANIDE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
450OCNE-99
5
TOTAL PHENOLIC
COMPOUNDS
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
4201-78
5
HARDNESS (as CaCO3)
119
mg/L
22330
Ib/d
111 3
mg/L
20892
Ib/d
3
2340C
1
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 10 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED'
RIVER BASIN
City of Havelock WWTP, NCO021253
Renewal
Neuse River
Outfall number 001 (Complete once for each outfall discharging effluent to waters of the United States )
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
ML/MDL
Number
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
of
METHOD
Samples
VOLATILE ORGANIC COMPOUNDS
ACROLEIN
< 100
pg/L
< 1 88
Ib/d
< 100
pg/L
< 1 88
Ib/d
3
EPA 624
100
ACRYLONITRILE
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 624
50
BENZENE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
BROMOFORM
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
CARBON
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
TETRACHLORIDE
CHLOROBENZENE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
ROMO-
< 5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
METHANE
METHANE
CHLOROETHANE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 624
10
2-CHLOROETHYLVINYL
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
ETHER
CHLOROFORM
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
HLOROBROMO-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
METHANE
ME
1,1-DICHLOROETHANE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
1,2-DICHLOROETHANE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
TRANS-1,2-DICHLORO-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
ETHYLENE
-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
ETHYLENE
ETHYLENE
1,2-DICHLOROPROPANE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
1, LORO-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
PROPYLOPYLENE
ETHYLBENZENE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
METHYL BROMIDE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 624
10
METHYL CHLORIDE
< 10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 624
10
METHYLENE CHLORIDE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 624
10
1,1,2,2-TETRA-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
CHLOROETHANE
TETRACHLORO-
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
ETHYLENE
TOLUENE
<5
pg/L I
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 11 of 17

FACILITY NAME AND PERMIT NUMBER
City of Havelock WWTP, NCO021253
PERMIT ACTION REQUESTED'
Renewal
RIVER BASIN
Neuse River
Outfall number 001 (Complete once for each outfall discharging effluent to waters of the United States )
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
1,1,1
TRICHLOROETHANE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
LPA 624
5
1'1'2
TRICHLOROETHANE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
TRICHLOROETHYLENE
<5
pg/L
< 0 094
Ib/d
<5
pg/L
< 0 094
Ib/d
3
EPA 624
5
VINYL CHLORIDE
<10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
EPA 624
10
Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer
TRICHLOROFLUORO
METHANE
<5
pg/L
< 0 094
Ib/d
<4
pg/L
< 0 094
Ib/d
3
EPA 624
5
ACID -EXTRACTABLE COMPOUNDS
P -CHLORO -M -CRESOL
< 20
pg/L
< 0 375
Ib/d
< 20
pg/L
< 0 375
Ib/d
3
EPA 625
20
2 -CHLOROPHENOL
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
2,4-DICHLOROPHENOL
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
2,4 -DIMETHYLPHENOL
< 10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
4,6-DINITRO-0-CRESOL
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
2,4-DINITROPHENOL
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
2-NITROPHENOL
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
4-NITROPHENOL
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
PENTACHLOROPHENOL
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
PHENOL
<10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
EPA 625
10
2'4'6
TRICHLOROPHENOL
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
BASE -NEUTRAL COMPOUNDS
ACENAPHTHENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
ACENAPHTHYLENE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
ANTHRACENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
BENZIDINE
< 100
pg/L
< 1 88
Ib/d
< 100
pg/L
< 1 88
Ib/d
3
EPA 625
100
BENZO(A)ANTHRACENE
<10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0 188
Ib/d
3
EPA 625
10
BENZO(A)PYRENE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 12 of 17

FACILITY NAME AND PERMIT NUMBER-
PERMIT ACTION REQUESTED
RIVER BASIN'
City of Havelock WWTP, NC0021253
Renewal
Neuse River
Outfall number 001 (Complete once for each outfall discharging effluent to waters of the United States )
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
MLIMDL
Number
Conc
Units
Mass
Units
Conc.
Units
Mass
Units
of
METHOD
Samples
3,4 BENZO-
< 10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
EPA 625
10
FLUORANTHENE
BENZO(GHI)PERYLENE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
BENZO(K)
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
FLUORANTHENE
BIS (2-CHLOROETHOXY)
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
METHANE
BIS (2-CHLOROETHYL)-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
ETHER
BIS (2-CHLOROISO-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
PROPYL)ETHER
BIS (2-ETHYLHEXYL)
< 20
pg/L
< 0 375
Ib/d
< 20
pg/L
< 0 375
Ib/d
3
EPA 625
20
PHTHALATE
HE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
PHENYLETHERR
PHENYE
BUTYL BENZYL
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
PHTHALATE
2-CHLORO-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
NAPHTHALENE
4-CHLORPHENYL
< 10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
EPA 625
10
PHENYLETHER
CHRYSENE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
DI-N-BUTYL PHTHALATE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
DI-N-OCTYL PHTHALATE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
DIBENZO(A,H)
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
ANTHRACENE
1,2-DICHLOROBENZENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
1,3-DICHLOROBENZENE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
1,4-DICHLOROBENZENE
<10
pg/L
< 0 188
Ib/d
< 10
pg/L
< 0 188
Ib/d
3
EPA 625
10
3,3-DICHLORO-
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
BENZIDINE
DIETHYL PHTHALATE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
DIMETHYL PHTHALATE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
2,4-DINITROTOLUENE
<10
pg/L
< 0 188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
2,6-DINITROTOLUENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
1,2-DIPHENYL-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
HYDRAZINE
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 13 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED'
RIVER BASIN
City of Havelock WWTP, NCO021253
Renewal
Neuse River
Outfall number 001 (Complete once for each outfall discharging effluent to waters of the United States )
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
MLIMDL
Number
Conc
Units
Mass
Units
Conc.
Units
Mass
Units
of
METHOD
Samples
FLUORANTHENE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
FLUORENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
HEXACHLOROBENZENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
HEXACHLORO-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
BUTADIENE
HEXACHLOROCYCLO-
< 50
pg/L
< 0 939
Ib/d
< 50
pg/L
< 0 939
Ib/d
3
EPA 625
50
PENTADIENE
HEXACHLOROETHANE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
INDENO(1,2,3-CD)
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
PYRENE
ISOPHORONE
< 10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
NAPHTHALENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
NITROBENZENE
<10
pg/L
< 0188
Ib/d
< 10
pg/L
< 0188
Ib/d
3
EPA 625
10
N-NITROSODI-N-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
PROPYLAMINE
N-NITROSODI-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
METHYLAMINE
N-NITROSODI-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0 188
Ib/d
3
EPA 625
10
PHENYLAMINE
PHENANTHRENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
PYRENE
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
1,2,4-
<10
pg/L
< 0188
Ib/d
<10
pg/L
< 0188
Ib/d
3
EPA 625
10
TRICHLOROBENZENE
END OF PART D.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 14 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED'
RIVER BASIN•
City of Havelock WWTP, NCO021253
Renewal
Neuse River
SUPPLEMENTAL APPLICATION INFORMATION
PART E. TOXICITY TESTING DATA
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the
facility's discharge points 1) POTWs with a design flow rate greater than or equal to 1 0 mgd, 2) POTWs with a pretreatment program (or those that are
required to have one under 40 CFR Part 403), or 3) POTWs required by the permitting authority to submit data for these parameters
• At a minimum, these results must include quarterly testing for a 12 -month period within the past 1 year using multiple species (minimum of two
species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution Do not include
information on combined sewer overflows in this section All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC
requirements for standard methods for analytes not addressed by 40 CFR Part 136
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years If a whole effluent toxicity test
conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a
toxicity reduction evaluation, if one was conducted
• If you have already submitted any of the information requested in Part E, you need not submit it again Rather, provide the information
requested in question E 4 for previously submitted information If EPA methods were not used, report the reasons for using alternate methods
If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E
If no biomonitonng data is required, do not complete Part E Refer to the Application Overview for directions on which other sections of the form to
complete
E 1 Required Tests apa_abw QVKhDV Q d3 pondln0 poo E �O bo- U@FA . a. o d CLQ Pcc.)ad @Roc C3 FQ-@URO�3 �
M@0�0, A ZDl gDd dc,@ 8@Sd@w uc@MQ �-tll W embb@aWcd pffca Qo Lftc rq-,A k,'@ @R QW,15 pC-Fi7mB3 gra JUFRD �& 203 1Go
Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years
❑ chronic ❑ acute
E 2 individual Test Data Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years Allow one
column per test (where each species constitutes a test) Copy this page if more than three tests are being reported
Test number Test number Test number
a Test information
Test Species & test method number
Age at initiation of test
Outfall number
Dates sample collected
Date test started
Duration
b Give toxicity test methods followed
Manual title
Edition number and year of publication
Page number(s)
c Give the sample collection method(s) used For multiple grab samples, indicate the number of grab samples used
24 -Hour composite
Grab
d Indicate where the sample was taken in relation to disinfection (Check all that apply for each
Before disinfection
After disinfection
After dechlonnation
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 15 of 17

FACILITY NAME AND PERMIT NUMBER'
City of Havelock WWTP, NCO021253
PERMIT ACTION REQUESTED
Renewal
RIVER BASIN•
Neuse River
Test number Test number Test number,
e Describe the point in the treatment process at which the sample was collected
Sample was collected
f For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both
Chronic toxicity
Acute toxicity
g Provide the type of test performed
Static
Static -renewal
Flow-through
h Source of dilution water If laboratory water, specify type, if receiving water, specify source
Laboratory water
Receiving water
I Type of dilution water If saltwater, specify "natural' or type of artificial sea salts or brine used
Fresh water
Salt water
Give the percentage effluent used for all concentrations in the test series
k Parameters measured during the test (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I Test Results
Acute
Percent survival in 100%
effluent
LC50
95% C I
%
%
%
Control percent survival
%
%
%
Other (describe)
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 16 of 17

FACILITY NAME AND PERMIT NUMBER
PERMIT ACTION REQUESTED
RIVER BASIN
City of Havelock WWTP, NCO021253
Renewal
Neuse River
Chronic
NOEC
%
%
%
C25
%
%
%
Control percent survival
%
%
%
Other (describe)
m Quality Control/Quality Assurance
Is reference toxicant data available?
Was reference toxicant test within
acceptable bounds?
What date was reference toxicant test
run (MM/DD/YYYY)?
Other (describe)
E 3 Toxicity Reduction Evaluation Is the treatment works involved in a Toxicity Reduction Evaluation?
❑ Yes ❑ No Ifyes, describe
E 4 Summary of Submitted Biomonitormg Test Information If you have submitted biomorntonng test information, or information regarding the
cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary
of the results
Date submitted / / (MM/DD/YYYY)
Summary of results (see instructions)
END OF PART E.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
EPA Form 3510-2A (Rev 1-99) Replaces EPA forms 7550-6 & 7550-22 Page 17 of 17

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
EPA Form 2A Additional Information

City of Havelock WWTP
Permit No. NCO021253
Outfall 002
Additional Information
B.2 Topographic Map
See Figure 1 for topographic map and Figure 2 for plant site map.
B.3.1 Process Flow Description — Permitted Capacity of 2.25 mgd
The Havelock WWTP provides advanced wastewater treatment, including
nitrogen removal, to meet effluent limits for discharge to the Neuse River.
The major processes at the WWTP include screening, grit removal, a single -
stage nitrification activated sludge process, denitrification filters, ultraviolet
disinfection, re -aeration, gravity belt thickening, and stabilized solids storage.
As part of the Phase 1 WWTP expansion, completed in May 2015, an effluent
pump station, an outfall pipeline, a cascade aerator, and a diffuser in the
Neuse River were constructed.
Screening
Influent wastewater is conveyed to the Havelock WWTP by a combination of
gravity interceptors and force mains. The influent flow is combined into a 24 -
inch pipeline at the screening facility that passes through a bar screen
designed to remove large solids and debris from the influent wastewater to
prevent clogging and interference with operation of downstream pumps and
other process equipment.
Grit Removal
After passing through the bar screen, the influent wastewater flows to a vortex
(Pista) grit collector through a 24 -inch pipe. After the grit is removed, the grit
collector effluent flows to the influent pump stations.
Influent Pump Stations
The Havelock WWTP is equipped with two influent pump stations. Effluent
from the grit removal facility flows through an 18 -inch pipe to a tee with a 20 -
inch pipe. The 20 -inch pipe interconnects two wet wells, which are used in
combination with pumps to convey the influent wastewater to the aeration
basins. Each influent pump station is comprised of a wet well and three
influent pumps. One influent pump station contains three submersible pumps.
The second influent pump station is a dry pit/ wet pit configuration with three
pumps. All pumps are controlled via float switches in the wet well to keep
0 \30906\006\ENG\Task 040-WWTP NPDES Permit Renewal\Tab B\Form 2A -Additional Information 2017 doc

City of Havelock WWTP
Permit No. NCO021253
Outfall 002
pace with the plant influent flow rate. In addition to raw wastewater, return
activated sludge (RAS) from the secondary treatment stage is returned to the
influent pump station for conveyance to the aeration basin distribution box.
Flow from the influent pump stations are conveyed through 10 -inch and 12 -
inch pipes to the aeration basin distribution box.
Activated Sludge System
The purpose of the activated sludge system is to achieve the BOD removal,
phosphorus removal, and nitrification necessary to comply with the stringent
effluent requirements in the permit. The activated sludge system includes fine
and coarse bubble aeration basins, intermediate pumping, final clarifier
distribution box, final clarifiers, and RAS and waste activated sludge (WAS)
conveyance.
Fine Bubble Aeration
Wastewater enters the fine bubble aeration basins mixed with RAS through a
distribution box. Two sharp -crested weirs split the flow equally between two
aeration basins. The two circular tanks are equipped with a fine bubble
aeration system with ceramic disc diffusers. The diffusers provide the
dissolved oxygen and mixing necessary for operation of the activated sludge
process.
Coarse Bubble Aeration
The mixed liquor from each of the fine bubble aeration basins flows through
16 -inch pipes to the coarse bubble aeration basins for additional BOD
removal and/or nitrification. The three coarse bubble aeration basins are
operated in series in normal operation and are equipped with a coarse bubble
aeration system.
Final Clarifier Pump Station
Effluent from the second -stage aeration basin flows by gravity to the final
clarifier pump station wet well via 16 -inch piping. The Final Clarifier Pump
Station lifts the mixed liquor to a high enough elevation that the wastewater
can flow by gravity through the rest of the treatment plant. A 20 -inch pipe
conveys the pumped flow from the final clarifier pump station to the final
clarifier distribution box. A polyaluminum chloride (PACT) storage and feed
system is provided to feed PACI to the Final Clarifier Pump Station discharge
to enhance suspended solids removal and provide phosphorus removal in the
final clarifiers via precipitation.
0 13090610061ENGUask 040-WWTP NPDES Permit Renewal%Tab B%Form 2A -Additional Information 2017 doc 2

City of Havelock WWTP
Permit No. NCO021253
Outfall 002
Final Clarifiers
Two 65 -foot diameter clarifiers are provided to settle out solids from the mixed
liquor. The final clarifiers provide quiescent flow conditions to allow the mixed
liquor solids to settle to the bottom of the clarifiers. The settled solids are
either returned to the first -stage aeration basins as RAS or wasted to the
Waste Solids Holding Tank as WAS. The clarified effluent flows over the final
clarifier effluent V -notch weirs to the denitrification filters, where the
wastewater undergoes further treatment.
RAS and WAS Conveyance
The RAS and WAS Control Stations control the flow rate of settled activated
sludge from the final clarifiers to the influent pump stations and the Waste
Solids Holding Tank, respectively. WAS flows to the Waste Solids Holding
Tank, and from there is periodically pumped to the gravity belt thickeners for
thickening prior to stabilization and ultimate disposal. The RAS and WAS
flows are measured by four strap -on ultrasonic flow meters, with one RAS flow
meter and one WAS flow meter for each clarifier. RAS and WAS are conveyed
by gravity and manually -operated pinch valves downstream of the flow meters
are used to control the flow rates.
Denitrification Filters
The denitrification filters remove additional suspended solids from the final
clarifier effluent and remove nitrogen through denitrification to comply with the
total nitrogen limit. Final clarifier effluent flows by gravity to three denitrification
filters. An underdrain system collects the filtered wastewater and directs it to a
20 -inch pipe that flows by gravity to the disinfection facilities. The Havelock
WWTP uses methanol as its carbon source, and typically adds between 40
and 80 gallons per day to the filters. Backwash water is drained to the Filter
Backwash Waste Detention Basin, and from there is returned to the influent
pump stations.
Ultraviolet Disinfection
Disinfection is accomplished using ultraviolet (UV) disinfection technology.
Filtered wastewater effluent enters the UV disinfection facilities through a 16 -
inch and 20 -inch parallel pipeline. The old chlorine contact tank was
retrofitted to accommodate the UV modules and now serves as the
disinfection channel.
0 \30906\006\ENG\Task 040-WWTP NPDES Permit Renewal\Tab Worm 2A -Additional Information 2017 doc 3

City of Havelock WWTP
Permit No. NCO021253
Outfall 002
Re -aeration
The re -aeration facilities are located at the Re -aeration Basin and can be
used to provide additional dissolved oxygen in the UV disinfection effluent.
Two platform -mounted mechanical surface aerators are provided in the Re-
aeration Basin. The backwash supply pumps for the denitrification filters are
also located in the Re -aeration Basin.
Effluent Pump Station
The effluent pump station conveys flow through approximately 30,000 linear
feet of 24 -inch piping to the Neuse River.
Cascade Aerator
Prior to discharging into the Neuse River, the effluent passes through a
cascade aerator. The cascade aerator is located near the bank of the Neuse
River and increases the effluent's dissolved oxygen levels to meet permit
requirements.
Diffuser in the Neuse River
After passing through the cascade aerator, the effluent discharges into the
Neuse River through a multi port diffuser located approximately 2,040 feet
from the shoreline.
Please reference Figure 3 for the process flow diagram at a permitted
capacity of 2.25 mgd.
B.3.2 Process Flow Description — Future Permitted Flow Capacity of 2.8 mgd
The process flow at a permitted capacity of 2.8 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 3 -Stage BNR basin to meet nutrient limits.
Please reference Figure 4 for the process flow diagram at a permitted
capacity of 2.8 mgd.
0 \30906\DO6\ENG\Task 040-W W TP NPDES Permit Renewal\Tab B\Fonn 2A- Additional Information 2017 doc 4

City of Havelock WWTP
Permit No. NCO021253
Outfall 002
B.3.3 Process Flow Description — Future Permitted Flow Capacity of 3.5 mgd
The process flow at a permitted capacity of 3.5 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 5 -Stage BNR basin to meet nutrient limits.
Please reference Figure 5 for the process flow diagram at a permitted
capacity of 3.5 mgd.
0 \309061006\ENG\Task 040-WWTP NPDES Permit Renewal\Tab Worm 2A -Additional Information 2017 doc 5

Effluent Discharge Location 002
Constructed as Part of Phase 1 of WWTP Expansion
Lat 34° 57' 11" ,uv
Long 76° 52'37"
'1Y. Cascade Aerator
7t \ *,.+
{
t T 10 NVA:; , r
-� X l � �' "• - ,rte" / � / � __. ,..
Its
r
I li`4 4 I RESt.6VATl �.
i v IT ! w
l!t.RRY INT --�
V Ir
$'
Effluent Outfall Pi eline !' / Z
- —r--
G t 4
�U S Marine Ct>•'ps At,
Cherry Pouu .
City of Havelock WWTP Site>,
Influent Force Main I.+
r t Parallel Interceptors
kw
Copyright:© 2013"National, Geographic Society. cubed,
Influent Force Mains N
Figure 1
—Grev'tylnterceptos r v ` ` ' fWWTP Location Map
24-inch Effluent Pipe w� E
VV � � City of Havelock, NC
USATopoMaps s NCO021253
0 U OA 0.8B.2 of Form 2A
Miles �Pnrcin�''..`
0:\30906\006\ENG\Task 040-WWTP NPDES Permit Renewal\WWTP Location map -Figure t.mxd
rroay, Novemoer z4, w

FINAL CLARIFIER
NOA
30906-012 Figure 2. cdr
CONTROL BUILDING
❑ ❑
ENGINE
GENERATOR
TRANSFORMER BUILDING
BAR SCREEN
AND GRIT
REMOVAL
(BYPASS UNIT)
AERATION BASIN
DISTRIBUTION BOX
C
STABILIZED SOLIDS
HOLDING BASIN
C
FINE BUBBLE
AERATION BASIN NO. 2
FINE BUBBLE
AERATION BASIN NO. 1
`) � C0 O
111��� ��� INFLUENT
PUMPING STATIONS
0
j� GRIT REMOVAL
BAR 1 1
SCREEN
SOLIDS
HANDLING
BUILDING
O O
SLUDGE
UV PUMPING
DISINFECTION STATION
BASIN �
REAERATION
BASIN
OEFFLUENT
PUMPING STATION
Figure 2
WWTP Site Map
City of Havelock, NC
NCO021253
13.2 of Form 2A
a
BLOWER
BUILDING
N0.2
ICAL STORAGE
EED FACILITY
FINAL CLARIFIER
PUMPING STATION
HIANDMI
COARSE BUBBLE
_ _-
COARSE BUBBLE AERATION BASINS
AERATION BASIN NO. 1 & 2
NO, 3
O
FILTER BACKWASH
WASTE DETENTION BASIN
DENITRIFICATION
FILTERS
FINAL CLARIFIER
WASTE SOLIDS HOLDING TANK
NO.2
FINAL CLARIFIER
WAS CONTROL STATION
FLOW DISTRIBUTION
STRUCTURE RAS CONTROL
mInzIm,_
STATION
FINAL CLARIFIER
NOA
30906-012 Figure 2. cdr
CONTROL BUILDING
❑ ❑
ENGINE
GENERATOR
TRANSFORMER BUILDING
BAR SCREEN
AND GRIT
REMOVAL
(BYPASS UNIT)
AERATION BASIN
DISTRIBUTION BOX
C
STABILIZED SOLIDS
HOLDING BASIN
C
FINE BUBBLE
AERATION BASIN NO. 2
FINE BUBBLE
AERATION BASIN NO. 1
`) � C0 O
111��� ��� INFLUENT
PUMPING STATIONS
0
j� GRIT REMOVAL
BAR 1 1
SCREEN
SOLIDS
HANDLING
BUILDING
O O
SLUDGE
UV PUMPING
DISINFECTION STATION
BASIN �
REAERATION
BASIN
OEFFLUENT
PUMPING STATION
Figure 2
WWTP Site Map
City of Havelock, NC
NCO021253
13.2 of Form 2A

Grit
Removal
Plant Influent
Q=2.25 mgd Bar ScreensZZ
Q=2.25 mgd Q=2.25 mgd
o --e:=>
Cascade
Aerator
Ll:�
Diffuser in
Neuse River
30906-012 Figure 3. cdr
Grit
Q=2.25 mgd Q=3.55 mgd
Legend
FBW
= Filter Backwash
FBWR
= Filter Backwash Return
RAS
= Return Activated Sludge
WAS
= Waste Activated Sludge
TWAS
= Thickened Waste Activated
RAS Q=1.13 mgd
Sludge
EM
=Flow Meter
Aeration Basin
i Distribution -�
Box
►
Fine Bubble
Coarse Bubble
Influent Pump Aeration Basins
Aeration Basins Final Clarifier
Stations
Pump Station
RAS Q=1.13 mgd
FBWR
Q=0.15 mgd
FBW Waste
Reaeration Detention Basin
Tank
Methanol
Q=2.4 mgd
� EU CU cur,
UV Disinfection
Effluent Pump Denitrification
Station FBW Q=0.15 mgd Filters
Q=0.02 mgd Polymer
Polyaluminum
Chloride
Q=3.55 mgd
Final f'-- Distribution
Clarifiers Box
Q=1.15 mgd
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control RAS Control
Solids Holding Thickener Holding Tank Station Station
Basin Q=0.01 mgd Q=0.03 mgd
Q=0.03 mgd Q=1.13 mgd
40 �O�aaaC, Truck Hauling
�I to Land Application

F Q=2.8 mgd
Grit
Removal
Plant Influent
♦ Bar Screens 10
Influent Pump
Stations
Grit FBWR
0-
Cascade
Aerator
Diffuser in
Neuse River
30906-012 Figure 3.cdr
Q=4.4 mgc,
FBW Waste
Reaeration Detention Basin
Tank
CQCQED
Z- A-
C
C c�
3 Stage BNR Basin
RAS Q=1.4 mgd
Methanol
Q=3.0 mgd 1
Effluent Pump UV Disinfection Denitrification
Station FBW Q=0.2 mgd Filters
Q=0.024 mgd Polymer
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control
Solids Holding Thickener Holding Tank Station
Basin Q=0.014 mgd Q=0.038 mgd
47-0.038 mgd
'ilk Truck Hauling
'I IV' to Land Application
Legend
FBW
= Filter Backwash
FBWR
= Filter Backwash Return
RAS
= Return Activated Sludge
WAS
= Waste Activated Sludge
TWAS
= Thickened Waste Activated
Sludge
FM
=Flow Meter
Final Clarifier
Pump Station
Polyaluminum
Chloride
Q=4.4 mgd
Final Distribution
Clarifiers Box
Q=1.4 mgd
RAS Control
Station
Q=1.4 mgd

Plant Influent
Bar Screens
Q=3.5 mgd
o�
Cascade
Aerator
Diffuser in
Neuse River
30906-012
Grit
Removal
F Q=3.5 mgd
Influent Pump
Stations
Q=5.5 mgd
Legend
FBW
= Filter Backwash
FBWR
= Filter Backwash Return
RAS
= Return Activated Sludge
WAS
= Waste Activated Sludge
TWAS
= Thickened Waste Activated
Sludge
=Flow Meter
00 • • °eP• t7-�
°
b°■
• . • fie. +�•
Grit FBWR
_f� Polyaluminum
Methanol Chloride
FBW Waste Q=3.75 mgd Q=5.5 mgd
Reaeration Detention Basin
Tank
M Final Distribution
Clarifiers Box
Effluent Pump UV Disinfection DenitrificaiMM tion
Station FBW Q=0.25 mgd Filters
Q=1.8 mgd
Q=0.03 mgd Polymer
IF � �jgvt M M
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control RAS Control
Solids Holding Thickener Holding Tank Station Station
Basin Q=0.02 mgd Q=0.05 mgd
0=0.05 mgd — LQ=1.75 mgd
Truck Hauling
to Land Application

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Sludge Management Plan
(Including Land Application Permit and Agreement with Synargo)

Solids Treatment
Solids in the form of WAS from the Havelock WWTP currently undergo further treatment
for eventual disposal as a land application product. The existing solids processing
facilities include thickening, WAS holding tank, one 1 -meter gravity belt thickener (GBT),
polymer feed system, GBT feed pumps, thickened WAS (TWAS) feed pumps, and a
stabilized solids holding basin.
The solids thickening process is designed to reduce the volume of WAS from the activated
sludge process. WAS is removed from the final clarifiers and drained by gravity to the
Waste Solids Holding Tank for short-term storage prior to thickening. Each clarifier has
a separate wasting line and pinch valve in the WAS Control Station for controlling WAS
flow to the Waste Solids Holding Tank. Flow meters in the WAS Control Station indicate
WAS flow rate for each final clarifier. Submersible pumps are provided in the Waste
Solids Holding Tank for pumping WAS to the gravity belt thickeners in the Solids Handling
Building. Chemical conditioning of the solids with polymer is provided to separate the
flocculated solids from the free water. The thickened waste activated sludge (TWAS)
from the GBT is collected in a thickened solids hopper, from which it is pumped to the
Solids Stabilization Tank by two TWAS pumps. Free water is drained back to the Influent
Pump Station.
The stabilized solids holding basin is used to store thickened stabilized solids prior to
liquid land application on permitted privately -owned farmland. Piping is provided for
withdrawal of solids from the holding basin and to load the solids into a truck. Decanting
of supernatant to the influent pump stations is also possible using a portable pump.

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
RALEIGH
LAND APPLICATION OF CLASS B WASTEWATER TREATMENT PLANT RESIDUALS
PERMIT (NON -DEDICATED)
In accordance with the piovisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Havelock
Craven County
FOR THE
continued operation of a residuals management program for the City of Havelock and consisting of the
land application of Class B Wastewater Tieatment Plant iesiduals generated by the approved facilities
listed in Attachinent A to the approved sites listed in Attachment B with no discharge of wastes to surface
waters, pursuant to the application received Januaiy 20, 2015, and in conformity with other suppoi ting
data subsequently filed and approved by the Department of Environment and Natural Resources and
considered a part of this permit. The use and disposal of residuals arc iegulated under Title 40 Code of
Federal Regulations Pat 503. This perinnit does not exempt the Permittee from complying with the federal
regulations.
This pennit shall be effective fionn the date of issuance until March 31, 2017, shall void Permit No
WQ0000702 issued April 7, 2008, and shall be subject to the follownng specified conditions and
limitations
I. SCHEDULES
No later than six months prior to the expiration of this permit, the Permittee shall request ienewal of
this pei mit on official Division forms Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will i enew the permit for such period of
time and undei such conditions and limitations as it may deem appropriate Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal
application. [15A NCAC 02T .0108(b)(2), 02T .105(4), 02T .0109]
2. The Permittee shall be in full compliance with the regional office notification requirements
established in Condition III 3. within 90 days of the effective date of this permit. [15A NCAC 02T
.0108(b)(2)]
3 The Permittee shall subnut the Operation and Maintenance (O&M) plan as required in Condition
II14 to the Division within 90 days of the effective date of this permit. [15A NCAC 02T
0108(b)(2)]
WQ0000702 Veision 3 2 Slicll Version 150101 Page 1 of 12

4 The Permittee shall be in firll compliance with the signage requirements established in Condition
111 13 within 180 days of the effective date of this permit [15A NCAC 02T 0108(b)(2)]
ll. PERFORMANCE STANDARDS
The subject residuals management program shall be effectively maintained and operated at all times
so there is no discharge to surface waters, inor any contravention of gnoundwatei or sulfate water
standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance
conditions due to nnploper operation and iliamtenance, the Perinittee shall immediately cease land
applying residuals to the site, contact the Washington regional office supervisor, and take any
immediate coinective actions. [G.S. 143-215.1]
2 Tlus permit shall not relieve the Pernuttee of responsibility for damages to groundwater or suiface
water resulting fiom the operation of this iesiduals management program [15A NCAC 02B .0200,
02L .0100]
3. Only residuals generated by the facilities listed nn Attacluuent A ale approved for laud application in
accordance with this peanut [G S 143-215 1]
4. Only the sites listed in Attachment B are approved for residuals land application. [G.S 143-215.1]
5 Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not
exceed the following Ceiling Concentrations (i e., dry weight basis) or Cumulative Pollutant
Loading Rates (CPLRs):
Parameter
Ceiling Concentration
(nnIligrains per Idlograin)
CPLR
(poiinds per acre)
Ai seine
75
36
Cadmium
85
34
Coppet
4,300
1,338
Lead
840
267
Mei cury
57
15
Molybdenum
75
n/a
Nickel
420
374
Selenium
100
89
Zinc
7,500
2,498
The Permittee shall deternune compliance with the CPLRs using one of the following methods.
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. Foi land where residuals application have not occurred or foi which the required data is
incomplete, by determining background concentrations through representative soil sampling
[I 5A NCAC 02T. 1105]
6 Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC
02T 1106 (a) and (c) Exceptions to this requirement shall be specified in Attaclnnent A. [15A
NCAC 02T 1106]
WQ0000702 Version 3 2 Shell Veision 150101 Page 2 of 12

7. Biological residuals (i.e. residuals genciatcd during the treatment of domestic or anunal piocessing
wastewater, or the biological treatment of industrial wastewater, and as identified in Attachrnent A)
that ale land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T
.1107(a). Exceptions to this requirement shall be specified in Attachrnent A [15A NCAC 02T
.1107]
8 Setbacks for Class B land application sites shall be as follows -
[15A NCAC 02T 1108]
9. Land application areas shall be clearly masked on each site prior to and during any residuals
application event. [15A NCAC 02T .0108(b)(1)]
10. Bulls residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in
exceedance of agronomic rates. Appropuate agronomic rates shall be calculated using expected
nitrogen iequiiements based on the determined Realistic Yield Expectations (RYE) using any of the
following methods -
a Division's pie -approved site specific historical data for specific crop of soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
WQ0000702 Version 3.2 Shell Version 150101 Page 3 of 12
Setback by application type
(feet)
Setback Description
Vehicular
Iuigation
Surface
Surface
Li�ection/
Application
Application
hncorporation
Habitable residence or place of public assembly
under separate ownership of not to be maintained as
400
400
200
art of the project site
Habitable residence or places of public assembly
owned by the Permittee, the owner of the land, of the
lessee/operator of the land to be maintained as part
0
200
0
of the piojcct site
Property lines
50
150
50
Public riglit of way
50
50
50
Pi ivate or public water supply
100
100
100
Sulfate waters (streams — internuttent and peiemnial'
perennial wateibodies, and wetlands
100
100
50
Surface water diveisions (ephemeral streams'
wateiways, ditches)
25
100
25
Groundwater lowering ditches (where the bottom of
the ditch intersects the SHWT)
25
100
25
Subsurface groundwater loweirng system
0
100
0
Wells with exception to monitoring wells
100
100
100
Bedi ock outcrops
25
25
25
Top of slope of embanlanents or cuts of two feet of
more in ver tical height
15
15
15
Building foundations or basements
0
15
0
Watel lilies
0
10
0
Swtnlllllllg pools
100
100
100
Nits ification fields
0
20
0
[15A NCAC 02T 1108]
9. Land application areas shall be clearly masked on each site prior to and during any residuals
application event. [15A NCAC 02T .0108(b)(1)]
10. Bulls residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in
exceedance of agronomic rates. Appropuate agronomic rates shall be calculated using expected
nitrogen iequiiements based on the determined Realistic Yield Expectations (RYE) using any of the
following methods -
a Division's pie -approved site specific historical data for specific crop of soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
WQ0000702 Version 3.2 Shell Version 150101 Page 3 of 12

b Noitli Carolina Historical Data for specific crop and soil types as provided by North Carolina
State University Depa.tnnent of Soil Science(littp://iiutrieiits.soil.ncsti.edu/yields/ilidex.l)lip).
A copy shall be kept on file and reprinted every five yeais in accordance with Condition IV.5.
c. If the RYE cannot be determined using methods (a) of (b) above, the Permittee may use the RYE-
and
YEand appropi rate nutrier_t application rates reported in any of the following documents
I Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Nahual Resource
Conservation Service, or other agronomist
ii Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document. Chapter I
(littp://www.iicagr izov/SWC/teclm/docutmments/9th Guidance Doc 100109 ])df)
in Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (ftp-Hftp-fc sc.egov.usda gov/NHQ/pi-actice-staiidal-ds/staiidards/590.pdf).
d If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T .1109(b) (1) (k)]
11 When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25% um accordance with the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T
0108(b)(1)]
12 If land application sites are to be over -seeded or double -cropped (e g, bermuda grass in the sununer
and rye grass in the winter with both crops to receive residuals), then the second clop can receive an
application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr) This practice may
be allowed as long as the second crop is to be harvested or grazed If the second crop is to be planted
for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A
NCAC 02T 0108(b)(1)]
13. Prior to land application of residuals containing a sodium adsoiptioti intro (SAR) of 10 or lughet, the
Permittee shall obtain and implement recommendations fiorn at least one of the following, the local
Cooperative Extension Office; the Department of Agi iculture and Consumer Ser vices, the Naluial
Resource Conservation Service, a North Carolina Licensed Soil Scientist; of an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e g, gypsum, etc.), of a
mechanism for maintaining ;rte integrity and conditions conducive to crop growth. The Permittee
shall maintain written recores of these reconunnendations and details of their implementation [15A
NCAC 02T .0108(b)(1)]
14 These residuals land application sites were individually permitted on or after December 30, 1983;
therefore, the compliance boundary is established at either 250 feet from the residual land application
area, or 50 feet within the property boundary, whichever is closest to the residual land application
area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to
remediation action according to 15A NCAC 02L .0106(d) (2) as well as enforcement actions in
accordance with North Carolina General Statute 143-215.6A through 143-215.60. Any approved
relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. [15A NCAC 02L
0107(a)]
15. The review boundary shall be established midway between the compliance boundary and the residual
land application area. Any exceedance of groundwater standards at the review boundary shall require
action um accordance with 15A NCAC 02L .0106 [15A NCAC 02L .0108]
WQ0000702 Version 3.2 Shell Version 150101 Page 4 of 12

III. OPERATION AND MAINTENANCE REQUIREMENTS
The residuals management program shall be properly maintained and operated at all times The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water of groundwater standards. [15A NCAC 02T 1110]
2. The Washington Regional Office, telephone number [phone], and the appropriate local
govcinnnent official (i e., county manager, city managei, or health director) shall be notified at least
48 1noLrls pllor to the Initial residuals land application to any new land application site Notification to
the regional supervisoi shall be made from 8:00 a.m. until 5:00 p in on Monday through Friday,
excluding State Holidays. [15A NCAC 02T .0108(b)(1)]
3 The Washington Regional Office shall be notified via email or telephone, [phone], at least 24
hours prioi to conducting any land application activity. Such notification shall indicate, at a
minimum, the anticipated application times, field IDs, and location of land application activities If it
becomes necessaiy to apply to additional fields due to unforeseen events, the Regional Office shall be
notified pi ioi to commencing the application to those fields [I 5A NCAC 02T .0108(b)(1)]
The Pcrnuttee shall maintain an approved Opeiation and Maintenance Plan (O&M Plan)
Modifications to the O&M Plan shall be approved by the Division prioi to utilization of the new plan
The O&M Plan, at the minimum, shall include.
a. Operational functions,
b. Maintenance schedules;
c Safety measures;
d Spill response plan,
e. Inspection plan including the following i nfonnation
i. Names and/or titles of personnel responsible for conducting the inspections,
n Frequency and location of inspections, Including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
ur. Detailed description of inspection procedures including record keeping and actions to be
taken by the inspector in the event that noncompliance is observed pursuant to tine
noncompliance notification requirements under the monitoring and reporting section of the
permit;
Sampling and monitoring plan including the following information.
I Names and/or titles of personnel responsible for conducting the sampling and monitoring,
it Detailed desci iption of monitoring procedures including parameters to be monitored;
in Sampling frequency and procedures to assure that representative samples are being collected
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for
any foreseen fluctuations in residuals quality and indicate the most lrnniting times for
residuals to meet pathogen and vector attraction reduction requirements (e g. facilities that
land apply multiple times per year but have an annual sampling frequency, may need to
sample during winter months when pathogen reduction is most likely to be negatively
affected by cold temperatures)
[15A NCAC 02T. I 1001
WQ0000702 Version 3.2 Slicll Version 150101 Page 5 of 12

5 Upon the Watei 13ollutron Control System Opeiators Certification Collulusslon's (WPCSOCC)
classification of the facility, the Peinuttee shall designate and employ a certified operator in
responsible charge (ORC) and one of more certified operators as back-up ORCs in accordance with
15A NCAC 08G .0201. The ORC of his back-up shall visit the facilities in accordance with 15A
NCAC 08G 0204, or as specified in the most recently approved O&M plan (i.e., see Condition
I1I 4 ), and shall comply with all other conditions of 15A NCAC 08G. 0204. Fol mole information
regarding classification and designation requirements, please contact the Division of Water
Resources' Protection and LCnforcenlent Branch at [phone]. [ 15A NCAC 02T .01 17]
6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall
be maintained at the land application sites during land application activities. [15A NCAC 02T
0108(b)(1)]
7 When the Permittee transports of laud applies bulk residuals, the spill control Provisions shall be
maintained mail residuals transport and application vehicles [15A NCAC 02T 1 1 10]
8 Residuals shall not be stored at any land application site, unless written approval has been requested
and received fionn the Division. [G.S. 143-215 1]
9 When the Peinuttee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff fiom conveying residuals from the land application sites onto adjacent
Properties or into surface waters. [G.S 143-215.1]
10 When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on
land application sites onto which residuals are applied, or application shall be in accordance with the
crop management plan outlined by the local Cooperative Extension Office, the Department of
Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agiononust
and as approved by the Division. [15A NCAC 02T .l 109(b)(1)]
11. Bulk residuals shall not be laud applied under the following conditions
a. If the residuals are likely to adversely affect a threatened or endangered species listed Under
section 4 of the Endangered Species Act or its designated critical habitat;
b If the application causes �iolonged nuisance conditions;
c If the land fails to assimilate the bulk residuals or the application causes the contravention of
surface water of gi oundwater standards;
d. If the land is flooded, fioi en or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur
e Within the 100 -year flood elevation, unless the bulk residuals are infected or incorporated within
a 24-hour period following a residuals land application event;
f. During a measurable precipitation event (Le, greater than 0.01 inch per hour), of witlurn 24 hours
following a i ainfall event f 0.5 inches or gi eater m a 24 -!lour period,
g. If tine slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or mcorprated bulk liquid iesiduals;
h If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of least 6.0, or if an agrononnist provides information indicating that the
pH of the soil, residuals land lune mixture is suitable for the specified crop. Any approved
variations to the acceptable soil pH (6 0) will be noted in this permit;
r If the land does not have aril established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in
a USDA no -till program shall be exempted from meeting this vegetative cover requirement;
WQ0000702 Veision 3 2 Shell Veision 150101 Page 6 of 12

If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot,
If the vertical separation of bedrock and the depth of residuals application is less than one foot,
Application exceeds agronomic rates
[ i SA NCAC 02T 1 109]
12 The following public access restrictions apply to residual land application sites.
a Public access to public contact sites (e,g., golf couises, panes, ball fields, etc.) shall be restiicted
for 365 days after a leslduals land application event,
b Public access to 11011 -public contact sites shall be iestricted for 30 days after a residuals land
application event.
[15A NCAC 02T. I 109(b) (2)]
13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g.,
1,5' x 2') Each sign shall indicate the activities conducted at each site, pernut number, and name and
contact information, including the Permittee of applicator's telephone number. Signs shall be posted
in a clearly visible and conspicuous manner at tine entrance to each land application site during a land
application event, and for as long as the public access iestiretions requued under Condition III 12.
apply. [15A NCAC 02T .0108(b)(1)]
14. The following harvesting and grazing restrictions apply to residual land application sites after each
land application event,
Harvesting and Grazing Description
Restricted
Duration
Animals shall not be allowed to graze during land application activities and
iestiicted period Sites that are to be used for grazing shall have fencing to
30 days
pi event access after each land application event.
Food crops, feed clops and fiber crops shall not be harvested for:
30 days
Turf grown on land where residuals have been applied shall not be harvested for
12 months
Food crops with harvested parts that touch the residual/soil mixture and are
totally above the laud sur face (e g., tobacco, melons, cucumbers, squash, etc)
14 months
shall not be harvested for -
When the residuals remain oil the land surface for four months of longer prior to
incorporation into the soil, f00d Uol)b With halVurtcd pacts below the land
surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be
20 months
harvested for
When the residuals remain on the land surface for less than four months prior to
incorporation into the soil, food crops with harvested parts below the land
38 months
surface shall not be hai vested for
[15A NCAC 02T.1 109(b) (3)]
15. The Peinuttec shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i e., manufactured fertilizers, manures, of other animal waste products) that
have been applied to the site, and a copy of the most recent Nutiicnt Management Plan (NMP) for
those operations where a NMP is required by the US Department of Agncultui e — National Resoui ccs
Conservation Seivice (MRCS) or other State Agencies. The Permittee shall calculate allowable
nutrient loading rates based on the provided information and use appropriate reductions,
WQ0000702 Version 3,2 Shell Veision 150101 Page 7 of 12

Foi the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) on Certified Nut-ient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan. [15A NCAC 02T 0108(b) (1), 02T 1104(c) (4)]
16. No residuals shall be land applied unless the submitted Land Owner Agreement Attaclunent (LOAA)
between the Permittee and landowners or lessees/operators of the land application site is in fiill force
and effect. These agreements shall be considered expmed concuriemt with the permit expiration date,
anct shall be renewed duluig tlnc peiiiul renewal process. [15A NCAC 02T .1104(c)(4)]
IV. MONITORING AND REPORTING REQUIREMENTS
1 Any Division required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensr.re groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 021' 0108(c)]
Residuals shall be analyzed to demonstrate they are non-hazaidous under the Resource Conservation
and Recovery Act (RCRA) Residuals that tests or is classified as a hazardous or toxic waste
under 40 CFR Part 261 shall not be used or disposed under this pern-lit. The analyses
[corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall
be performed at the frequency specified in Attachment A, and the Peinuttee shall maintain these
results for a minimum of five years Any exceptions from the requirements in tills condition shall be
specified in Attachment A
The TCLP analysis shall include the following parameters (the regulatory level in nulligiams per liter
is in parentheses):
Arsenic (5.0)
1,4 -Dichlorobenzene (7.5)
Nitiobenzene (2.0)
Bai win (100 0)
1,2-Dielnloroethane (0 5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1 0)
2,4 -Di nitrotolueme (0 13)
Selenium (1 0)
Caibon teti achloi ide (0.5)
Endiin (0 02)
Silver (5 0)
Chlordane (0 03)
Hexachlorobenzene (0.13)
Teti achloroethylene (0.7)
Chloiobenzene100 0
( )
Heptachlor (and its hydioxide)
(0 008)
Toxaphene (0.5)
Chloroform (6 0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chlomllum (5 0)
I- Iexachloroethane (3,0)
2,4,5 -Trichlorophenol (400.0)
m-Ciesol (200.0)
Lead (5 0)
2,4,6 -Trichlorophenol (2 0)
o -Cresol (200.0)
Lindane (0.4)
2,4,5 -TP (Silvex) (1.0)
p -Cresol (200.0)
Meicury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the iesicluals have been monitored for two years at the fiequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement M no case shall the monitomig fiequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .l 105]
WQ0000702 Version 3 2 Shell Version 150101 Page 8 of 12

3. An analysis shall be conducted on residuals from each source generating facility at the frequency
specified in Attachrrient A, and the Permittee shall maintain the results for a minimum of five years
The analysis shall include the following paiameteis.
Aluminum
Mercury
Potassium
Anmrnonia-Nitrogen
Molybdenum
Selenium
Ai senic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Coppei
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T 1101]
4 Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the time indicated in the sampling
and nmonitoring sections of the approved O&M plan. The rcquued data shall be specific to the
stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen
reduction iequirements in 15A NCAC 02T 1106 (a) and (c), and one vector attraction reduction
requirement in 15A NCAC 02T .1107 (a) shall be met Any exceptions fiom the iequiienments in this
condition shall be specified in Attachment A [15A NCAC 02T .1106, 02T 1107, 02T .1111(c)]
5. An annual representative soils analysis (i.e, Standaid Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B on which a residuals land application event will
occur in the respective calendar year. This analysis shall be m accordance with the "Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture &
Consumer Seivices' website(lmttp•//www.ncaggov/a/arrononmr/imubs htimm) The Permittee shall
maintain these results and a description of the sampling methodologies used to dctcrnmine soil fertility
for a period of no less than five years, and shall be made available to the Division upon request At a
minimum, the Standard Soil Fertility Analysis shall include the following pararrictcrs-
Acidity parameters-
Acidity
[ 15A NCAC 02T 111 l ((I)]
6. Laboratory parameter analyses shall be peifoinmed on the residuals as they are land applied, and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B
.0505]
WQ0000702 Version 3 2 Shell Version 150101 Page 9 of 12
Exchangeable Sodium Percentage
Phosphorus
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Percent Huinic Matter
Zinc
Copper
pH
[ 15A NCAC 02T 111 l ((I)]
6. Laboratory parameter analyses shall be peifoinmed on the residuals as they are land applied, and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B
.0505]
WQ0000702 Version 3 2 Shell Version 150101 Page 9 of 12

7 The Pernnittee shall nnai -am records tracking all residual land application events. At a nunimum,
these records shall include the following
a. Source of residuals,
b. Date of land application;
e. Location of land application (i e , site, field, or zone number as listed in Attachment B);
cl Approximate areas applied to (acres),
e Method of land application,
f Weather conditions (e.g., sunny, cloudy, raining, etc.),
g Piedonnrnant Soil Mapping Unit (e.g., CbB2),
h Soil conditions (e.g., d -,-y, wet, frozen, etc.);
t. Type of crop or crops to be giown on field,
i Nitrogen Application Rate based on RYlrs (if using data obtained from the North Carolina State
University Department of Soil Science Website, the printout page shall be kept on file and
reptinted every five years),
k Volume of residuals land applied in gallons per acre, cubic yard pet acre, dry tons per acre, of wet
ton per acre;
I Volume of animal waste or other rnutuent source applied in gallons per acre, diy ton pei acre, or
wet tons per acre,
Ill. Volume of soil amendtments (e.g, Rinne, gypsum, etc.) applied in gallons per acre, diy ton per
aci e, or wet tons pet acre; and
n Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other
sources of nutrients (e g , if applicable), annual and cumulative pounds per acre of each heavy
metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury,
molybdenum, nickel, selenium, and zinc), annual pounds pet acre of PAN, and annual pounds per
acre of phosphorus applied to each field
[ 15A NCAC 02T .0109(a)]
8. Three copies of an annual report shall be submitted on or before March I" The atulual repolt shall
meet the requirements described in the Instructions for Residuals Application Annual Repotting
Forms, Instructions fo_ reporting and annual report forms arc available at
lnttu•//aortal ncdenr oig/web/wq/aps/lair/reporting, or can be obtained by contactuig the Land
Application Unit directly The annual rcpott shall be submitted to the following address -
Division of Water Resouices
Information Processing Unit
1617 Marl Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T.1 I 1](a)]
9. Noncompliance Notification
The Permittee shall report by telephone to the Washington Regional Office, telephone number (252)
946-6481, as soon as possible, but in no case more than 24 hours or on the next working clay
following the occurrence or fust knowledge of the occuuence of any of the following:
a. Laird application of residuals abnol7nnal in quantity or ehaiacteristic.
b Any failure of the land applicat toil program resulting rrn a release of material to surface waters.
WQ0000702 Vetston 3.2 Shell Vetston 150101 Page 10 of 12

C. Any time self-monitoring indicates the facility has gone out of compliance with its permit
limitations
d. Any piocess unit failure, due to known or unknown reasons, iendering the facility incapable of
adequate iesidual treatment.
c. Any spill of discharge from a vehicle or piping system cluiing residuals transportation.
Airy emergency requiring innrnediate reporting (e.g , discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Peisons
reporting such occurrences by telephone shall also file a written report in letter form within five clays
following first knowledge of the occuuence This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur [15A NCAC 02T .0105(1), 02T .0108(b) (1)]
V. INSPECTIONS
1. The Permrltec shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T
.0108(b)]
Priot to each bulls residuals land application event, the Pernuttee of his designee shall inspect the
iesiduals transport and application facilities to prevent malfunctions, facility detciioiatiorr and
operator errors iesultiing in discharges, which may cause the release of wastes to the environment, a
tlueat to human health or a public nuisance. The Permittee shall maintain an inspection log that
includes, at a munimum, the elate and time of inspection, observations made, and any maintenance,
iepairs, or corrective actions taken. The Pernuttee shall maintain this inspection log for a period of
five years from the date of inspection, and this log shall be made available to the Division upon
request [ 15A NCAC 02T 0l 08(b)]
3 Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities peimitted herein
at any reasonable time for the purpose of determining compliance with this pei mit, may inspect or
copy any records required to be maintained under the terms and conditions of this permit, and may
collect groundwater, surface water or leachate samples. [G.S. 143-215.3(x)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to
an enforcement action by the Division in accordance with North Catoliina General Statutes 143-
215 6A to 143-215 6C [G S. 143-215 6A to 143-215 6C]
This permit shall become voidable if the iesiduals land application events aie not carried out in
accordance with the conditions of this permit. [15A NCAC 02T .0110]
This permit is effective only with respect to the natui e and volume of residuals desci ibcd in the
permit application and other supporting documentation [GS 143-215.1]
WQ0000702 Version 3 2 Shell Veision 150101 Page 11 of 12

4 The issuance of this pein-in does not exempt the Permittee fiom complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional goverimient agencies
(e.g., local, state, and fedeial) Of particular concern to the Division are applicable rivet buffet rules
in 15A NCAC 02B 0200, erosion and sedimentation control requirements in 15A NCAC Chaptei 4
and Under the Division's General Permit NCG010000; any requirements pertaining to wetlands utndei
15A NCAC 02B .0200 and 02H 0500, and documentation of compliance with Article 21 Part 6 of
Chapter 143 of the General Statutes [15A NCAC 02T 0105(c)(6)]
5. In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division foinns, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Peinnittee of record shall remain fully responsible for
maintaining and operating the residuals piogiann peimitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This peinut is subject to revocation or unilateral modification upon 60 clays notice from the Division
Director, in whole or pall fir the requirements listed in 15A NCAC 02T .0110 [15A NCAC 02T
01 10]
Unless the Division Director giants a variance, expansion of tine permitted residuals program
contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC
02T 0120(b) [15A NCAC 02T .0120]
8 The Permittee shall pay the annual fee witlun 30 days after being billed by the Division Failure to
Pay the annual fee accordingly shall because for the Division to revoke this pernnit [15A NCAC 02T
0105(e)(3)]
Perimmit issued this the 24th day of March 2015
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
o Jay iumei man, Director
ivisioi of Water Resources
By Authoi ity of the Environmental Management Conunission
Permit Number WQ0000702
WQ0000702 Version 3 2 Shell Version 150101 Page 12 of 12

ATTACHMENT A - Approved Residual Sources
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
I Maximum Dry Tons per Year is the amount of i esidual, approved fur land apphc.auon from each permitted facility
2 AnalysLs to demonstrate that residuals are non-ha/ardOUS (i c, TCLP, igmtability, reactivity, and corrosivity) as stipulated under penntt Condition IV 2
3 Testing of metals and nutrients as stipulated under permit Condition IV 3
4 Analyses of pathogen and N ector attraction reductions us stipulated under permit Condition IV 4
5 Monitoring frequencies are based on the actual dry tons applied pci yeas using the table below, unles% specitied above
Dry Tons Generated
short tons per year)
Monitor ing Frequency
(Establisiied in 40 CFR iO3 and 15A NCAC 02T.1110
<319
1 /Year
=>319 - <1,650
I/ Quarter (4 times per car)
=>1,650 - <16,500
1/60 Days (6 times per ear)
Approved
1 /month ( i 2 times per ear)
Maximum
Monitoring
Monitoring
Monitoring
Frequency for
Mineralization
Owner
Facility Name County
Permit
Biological
Dry Tons
Frequency for
Frequency for
Pathosen &
Rate
Number
Residuals
Per Year I
Non-haiardous�
Metals and
[Raw=04
Characteristics -
Nutrients 3's
Vector Attraction
Aerobic = 0 3,
Reductions''
Anaerobe. =03,
Compost= 0 I
City of Havelock
Havelock W WTP Craven
NCO021253
Ycs
415
Annually
See Table Below
See Table Below'*
03
Total
413
I Maximum Dry Tons per Year is the amount of i esidual, approved fur land apphc.auon from each permitted facility
2 AnalysLs to demonstrate that residuals are non-ha/ardOUS (i c, TCLP, igmtability, reactivity, and corrosivity) as stipulated under penntt Condition IV 2
3 Testing of metals and nutrients as stipulated under permit Condition IV 3
4 Analyses of pathogen and N ector attraction reductions us stipulated under permit Condition IV 4
5 Monitoring frequencies are based on the actual dry tons applied pci yeas using the table below, unles% specitied above
Dry Tons Generated
short tons per year)
Monitor ing Frequency
(Establisiied in 40 CFR iO3 and 15A NCAC 02T.1110
<319
1 /Year
=>319 - <1,650
I/ Quarter (4 times per car)
=>1,650 - <16,500
1/60 Days (6 times per ear)
=> 16.500
1 /month ( i 2 times per ear)
If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no
sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual
report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0000702 Version 3 2 Attachment A Page 1 of I

THIS PAGE BLANK

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
Field/ Site
O,.tiner
I essee
County
Latitude
Longitude
Net
Acreage
Dominant Soil Series
Footnotes
NC -CV -I -I A'
Campbell, Robert G
McCoy, Charles Myron
Craven
35012'39"
77°25'06'
S 90
Pa- Pantego tine sandy loam
NC -CV -I-1 B
Campbell, Robert G.
McCoy, Charles Myron
Craven
35"12'38"
77"25'06'
700
Pa - Pantego line sandy loam
NC -CV -I -I C'
Campbell. Robert G
McCoy, C harle, Myion
Craven
35°12'31"
77025'09'
1290
Pa - Pantego tine bandy loam
NC -CV -1-11)
Campbell. Robert G
McCoy, Charles Myron
Craven
35012'32"
77025'15"
3120
Pa - Pantego fine sandy loam
NC -CV -I -I E
Campbell, Robert G
McCoy, C harles Myron
Craven
35012'32'
772518"
1640
Pa - Pantego fine sandy loam
NC -CV -I -I G
Campbell. Robert G
McCoy, Charles Myron
Ciaven
35"12'20-
77025'02"
940
Pa - Pante-o fine sandy loam
NC -CV -I -I H
Campbell. Robert G
McCoy, Charles Myron
Craven
35012'12'"
77°25'07'
2600
Pa - Pantcgo tine bandy loam
NC -CV -I -2A
Campbell, Robert G
McCoy, C harles Myron
Craven
35012'20"
77"25'39'
13.50
Pa - Pantego fine sandy loam
NC -CV -I -2A
Campbell Robert G
McCoy, Charles Myron
Craven
35012'10"
77025'23"
550
Pa- Pante,o tine sandy loam
Total for Cowry
130.8
NC -PA -2-1 A
Spencer Farms, Inc
Pamlico
35"09'56'
76"49'32"
10 is
Yo - Yonges loamy fine sand
NC -PA -2-1 B
Spencer Fauns, Inc
Pamlico
35"09'55"'
76049'23"
9 71
Yo - YongLs loamy fine sand
NC -PA -2 -IC
Spencer Farms, Inc
Pamlico
35009'55"
76049'26"
1024
Yo - Yonges loamy tine sand
NC -PA -2-1 D
Spencer Famis, Inc
Pamlico
35009'55'
76"49'23"
1025
Yo - Yon -e% loamy fine sand
NC -PA -2 -IE
Spencer Farms, Inc
Pamlico
35"09'55"
76°49'20"
1012
Yo- Yonges loamy fine sand
NC -PA -2- I F
Spencer Farms, Inc
Pamlico
35009'55"
76 49' 17"
1005
Yo - Yonges loamy tine sand
NC -PA -2 -IG
Spencer Farms, Inc
Pamlico
35°09'55"
76"49'15"
952
Yo - Yonges loamy fine sand
NC -PA -2-2A
Spencer Farms, Inc
Pamlico
35009'17"
76049'20"
2 94
Ar - Argent loam
NC -PA -2-213
Spencer Farms, Inc
Pamlico
35°09'16'
76049' 15"
626
Ar - Argent loam
NC -PA -2-2C
Spencer Farms, Inc
Pamlico
35009'16"
76049'11-
6 48
Yo- Yongcs loamy tine band
NC -PA -2-2D
Spencer Farms, Inc
Pamlico
35009'16'
7V49'07'
7 04
Yo — Yonges loamy tine sand
NC -PA -2-2E
Spencer Farms, Inc.
Pamlico
35"09'17"
76"49'03"
628
Yo — Yonges loamy fine sand
NC -PA -2-3A
Spencer Farms, Inc
Pamlico
35009'19"
76"49'00"
542
Yo — Yonges loamy fine sand
WQ0000702 Version 3 2 Attachment B Pale I of 3

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
NC -PA -2-3B
Spencer Farms, Inc
Pamlico
35009'l 9'
76048'57"
404
Yo - Yonges loamy tine sand
NC -PA -2-3C
Spencer Farms, Inc.
Pamlico
35009' 19'
76048'55"
564
Yo - Yonge�, loamy tine sand
NC -PA -2-31)
Spencer Farms, Inc
Pamlico
35'09' 19'
76°43'51'
804
Sk- Stockade loamy tine sand
NC -PA -2-3E
Spencer Farms, Inc.
Pamlico
35009 20'
76048'=18"
742
Sk- Stockade loamy fine sand
NC -PA -2-317
Spencer Farms, Inc
Pamlico
35009'20"
76"4S'45'
7.42
Sk- Stockade loamy tine sand
NC -PA -2-3G
Spencer Farms, Inc
Pamlico
35009'20"
76048'42"
6 65
Sk- Stockade loamy fine sand
NC -PA -2-4A
Spencer Farms, Inc.
Pamlico
35009'27"
76049'02"
2 43
Yo - Yongcs loamy tint sand
NC -PA -2=113
Spencer Farms, Inc
Pamlico
35009'34"
76'=18'54'
4.34
Sk- Stockade loamy fine sand
NC -PA -24C
Spencer Farms, Inc
Pamlico
35"09 32'
76048'54"
4.51
Sk- Stockade loamy tine sand
NC -PA -241)
Spencer Farms, Inc
Pamlico
35°09'31"
76048'53'
3.62
Sk- Stockade loamv tine sand
NC -PA -2-4E
Spencer Farms, Inc
Pamlico
35°09'29"
76"48'52'
3 55
Sk- Stockade loamy fine sand
NC -PA -24F
Spencer Farms, Inc.
Pamlico
35"09'28"
76"48'52"
3 60
Sk- Stockade loamy tine sand
NC -PA -2-4G
Spencer Farms, Inc
Pamlico
35°09'26"
76"48'51"
3.55
Sk- Stockade loamy tine sand
NC -PA -2-5A
Spencer Farms, Inc
Pamlico
35009'39"
76"49'04'
5.21
Sk- Stockade loamy tine sand
NC -PA -2-513
Spencer Farms. Inc
Pamlico
35"09'40"
76"49'02'
648
Sk- Stockade loamy tine sand
NC -PA -2-5C
Spencer Farris, Inc
Pamlico
35009'40"
76043'58"
6 16
Sk- Stockade loamy fine sand
NC -PA -2-51)
Spencer Farms, Inc
Pamlico
35"09'41"
76048'85"
626
Sk- Stockade loamy tine sand
NC -PA -2-5E
Spencer Farms, Inc
Pamlico
35"09'41"
76048'52"
3 90
Sk- Stockade loamy fine sand
NC -PA -2-5F
Spencer Farms, Inc
Pamlico
35"09'42'
76"48'49 '
359
Sk- Stockade loamy fine sand
NC -PA -2-6A
Spencer Farms. Inc
Pamlico
35"09'51"
76050'21"
521
Sk- Stockade loamy tine sand
NC -PA -2-6B
Spencer Farms, Inc
Pamlico
35"09'52"
76050'] T'
648
Sk- Stockade loamy tine sand
NC -PA -2-6C
Spencer Farms, Inc.
Pamlico
35"09"53"
76"50'13"
6 l6
Sk- Stockade loamy fine sand
NC -PA -2-61)
Spencer Farms. Inc
Pamlico
35"09"54"
76050'10"
626
Yo - Yonaes loamy tine sand
NC -PA -2-6E
Spencer Farms. [nL
Pamlico
35"09'55"
76°50'06"
3 90
Yo- Yonges loamy fine sand
NC -PA -2-6F
Spencer Farms, Inc.
Pamlico
35009'55"
76"50'04"
3 59
Yo - Yonges loamy fine sand
NC -PA -2-6G
Spencer Farms, Inc
Pamlico
35"09'56'
76"50'01"
3 S4
Ar- Argent loam
WQ0000702 Version 3.2 Attachment B Pave 2 of 3

ATTACHMENT B - Approved Land Application Sites
CITY OF HAVELOCK
Certification Date: March 24, 2015
Permit Number: WQ0000702 Version: 3.2
NC -PA -2-7A
Spencer Farms, Inc
Pamlico
35°09'56-
76°49'59"
2 18
Ar- Argent loam
NC -PA -2-7B
Spencer Fanns, Inc
Pamlico
35°09'57'
76°49'57'
257
Ar- Argent loam
NC -PA -2-7C
Spencer Fann,, Inc
Pamlico
35009'57"
76049'55"
332
Ar - Argent loans
NC -PA -2-713
Spencer Farin,, Inc
Pamlico
35009'58'
76049'53"
3 32
Ai -Argent loam
NC -PA -2-7E
Spencer Farms, Inc
Pamlico
35009'59"
76°49'50"
326
Ar- Ar-ent loam
NC -PA -2-7F
Spencer Farms, Inc
Pamlico
35°09'59"
76049'48'
3 03
Ar- Argent loam
NC -PA -2-7G
Spencer Farm,. [nc
Pamlico
35°10 00'
76°49'46'
353
Ar- Argent loam
NC -PA -2-7H
Spencer Farms, Inc.
Pamhco
35°10'00"
76°49'43 '
328
Yo - Yonges loamy tine sand
NC -PA -2-71
Spencer Farm,, Inc
Pamlico
35010'01"
76°49'41"
325
Yo - Yongesloamyfinesand
NC -PA -2-7J
Spcnccr Farms, Inc
Pamlico
35°10'01"
76049'39"
325
Yo - Yonges loamy tine sand
NC -PA -2-7K
Spencer Farm,, Inc
Pamlico
35"10'02"
76049'37"
247
Yo - Yonges loamy fine sand
Tota/for County
269.80
Total
400.60
L. A re-uetmea compiiance uounuary na, uec:n approved for this iand application tine. ibis re -defined compliance boundary is between fielde NC -CV -1-1 A and NC -CV -1-1 C and shall be
located at 50 feet from the water supply well on Robert G Campbell'~ property Note that the 100 -trot setback between wells and the land application area shall still be met.
WQ0000702 Version 3.2 Attaclunent B
Pale 3 of 3

THIS PAGE BLANK

1--- -1
Fields GA - GG L,
Fields 2A - 2E ( -
Alliance
Grantsboro
Fickis JA IG
Fields 5A - 5F,
J Fields 4A - 4G�
L-- ,_. - --- - -- -
Bayboro
Stonewall
D
E
C
5
k
LL.
n
REFERENCE:
GIS DATA LAYERS WERE OBTAINED FROM ESRI, INC. PLEASE NOT[ THIS MAP IS FOR INFORMATIONAL
PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN, LEGAL, OR ANY OTHER USES THERE AHE NO
GUARANTEES ABOUT ITS ACCURACY, SSME, INC. ASSUMES NO RESPONSIBILITY FOR ANY DECISION
MADE OR ANYACTIONS TAKEN BY THE USER BASED UPON THIS INFORMATION. i Field Boundary I n
SCALE. z : 1 �� = 1 miles FIGURE 1
SPE
-- -s S&ME
('
SPENCER FAR
DATE: 11-06-14 SITE NC -('CITY OF HAVELOCK
Di A; BY MEM VICINITY It 503 LAND APPLICATION PROGRAM
"WWW.SMEINC.COM
'ROJECTNO CITY OF HAVELOCK - LAND Af CRAVEN COUNTY
1588-09-059 ENGINEERING LICENSE NO F -W76 PAMLICO COUNTY, NO
-- ---- WQ0000702
SITE LOCATION MAP
u,

SII vF1I9.1)
101 AI_ACRlti 81 MRI)A(RB
NEI-A(!RIS
SII F./MIA)
TOTAL A('R1\ 111TI-1, F)A(RFS
NEI'ACRES
N(' -PA -2 -IA
15.08
4.90
10.18
NC -PA -2 -SA
6.85
2.66
5.11
NC -PA -2-I11
13.61
3.98
9.71
N(' -PA -2 -SR
6.51
1.56
6A8
NC -PA -24C
13.72
JAI
10.24
NC4PA-2-5('
6.53
156
6.16
NC -PA -2 -ID
13.71
3.46
1025
NC-PM2S1)
6.52
1.10
636
NC -PA -2 -IE
13AS
3A8
11.12
NC -PA -2-5E
6.53
1.47
3.90
NC -PA -2-1 F
13.53
.1.48
10.05
NC -PA -2-5F
5.54
1.85
3.59
NC -PA -LIG
14.95
4.43
9.52
503 LAND APPLICATION PROGRAM
NC -PA -2 -SA THROUGH 5F

"ICI -2
•^ l 1Ili. FIF211 TUTALAI IIFN IIIc FJRFO At'RFN NF:[ At IN ADt., Fill 7JITALA(RIN Ut"'FAIDA(R1ti NIT AI RFN
°I ;i Fleltl SF' NI -PA -3-2A 5.50 2.56 2.94 W -PA -2-71 9,71
2.11 713
Field 5E
NC'-PA-2-28 IIJ! 5.47 6.I6 NC-PA•24C 9.99 liJ 6.65 �t`pJ 'm
�• FI4Id'SD •. T1 N('-YA-2-2C 10.11 .7.70 A.JB VC -PA -7 -IA 7.19 I.K I.17 p yy LU o LU
r FIeId SC { NC -PA -7 -ID 10.77 1 `l 7.04 N(' -PA -248 4.12 1A0 1.74 d 3 y LU W
Field'5B NC-PA3-1F. 9.9) 7.6.5 614 NCrA-24C 1,42 1.91 1.51
I'; ',A N(' -PA -2.3A 7.30 2.16 5.43 NC -PA -240 3.19 IJ7 3.62
N('4'A-7-311 6.90 2.43 J.O+ NCJA"Ir 5.11 116 3-95 Ol
s' VC-PA-7•JC 8.13 I.J9 S.AI N(' -PA -24F 3.16 I.tb l.10 - O
W -PA -I -3O I2.TR J.,J A.04 NI'AA-34(: 5.41 I.K 3.55
IC -PA -2-0.9.7! 231 7.47 O
It , W
REFERENCE' - = N
Field 48 _ OISUATA IAYFR9 WENF OBTAYiFII FROMESW,4K P(EASF NOTE INW MAP 16 fOR �NFURWTIONN PUNROSES WAY IT IS NOI MFAN7 TfMt DESIGN. uuji cif
IOM.(II ANY OTHER USES THERE ARE NO 0IMAAN1EEt ABOUT ITS ACCURACY SAME. INC ASSUMFS W RFIDONSWt111 ANY OFCISIUN y` S:
Uf Y
s UI I7R ANY At T!' -.PIS IAKEN BY TIS USER BASFO UPON T195 NSOI0AATIRN IJi GQ
• FIBIA iC >t=h+� COMPLIANCE BOUNDARY:
^.• iN[C01APlIAN(:F BWN(- FORrATUIIAM)AMP TION SITE IS FSTABIISNED AT F.ITNER 250 FFF7
_ � ' ' • iR(M IIIE RFSIOUAIS IARO AM'34: IONAWAOe t -ECT NTTMNIIS PNOI•ER7 Y MNMnARY
F'nld 4D•'f REVIEW BOUNDARY' 0
0 �.+�'- • Y^��.^ " ^ INF REVIEW BWMMRY SINIL BE E6TAB(ISIEO AROUIB EAIOIIAND APPIK.ATi(Hl iIIC MIDWAY U
.�� r - '�.-^` •1 BETWEEN TIS CO6iLUNCE ROU110MYAMD TIE PENITF.R OF TNF. RESMAIAl3 UtU APPIICATIW+
Fi„id 1C Z
..+�`• �sl �. W
lr\•"' _ - • • Irrigation Well �
■ Dwelling
°.a GW Lowering Ditch
Buffer
T'+s Field Boundary
,I
F Property Boundary
o
Vi az
Fie C f' A20 III Id E rield,3A Fitld,3B io1d�3C F.i4 d,3D Field JE
Field 3F F ei:l y'.,•.4l Z U
Field. B
I...2AZ
1 r
1• •`` o LL Z W �
'01
+M Lu yyy
Z� W UF-� x0
i iF i-- 6 ',R�•
UJI
00
{4 r1 LL. Q)
1JIFIGURE 3 • �e
♦ - M►. CITY OF HAVELOCK
503 LAND APPLICATION PROGRAM
.1 I► I We 1 CRAVEN COUNTY
'. �■ N WQ0000702
1`
- ,� ,�\ p■,. I 1. DETAIL MAP FOR SITES
FsN. DINi1alGlety+ l;r�tY^ I-nrbed, I11hMIr 6-glRph- GNI-SIAITbui 05. USDA. 11SG5. ACK 6efi-plee NC -PA -2-2A THROUGH 2E,
1 Nlpo, M the Use C O 111)"1100
•• NC -PA -2-3A THROUGH 3G AND
NC -PA -2-4A THROUGH 4G

COMPLIANCE BOUNDARY
IDF CI Mr I:UWlIDANY I DN I ALIl l A 1 ICAIKM SIT -F'.1 BI ItiIIDATI I711ER W FI I T F NOM 111E RFS IAMI S --IK AIIONNI
It'I IILIV11.TRC 111111 S-
'I
1N UUUV w1 .A' L/L 0 IW NI•. DINTS IANDAfl-AI IONARtA I
N
RF VIEW BOUNDARYi - y
TIORFVIFV--DARYSIMI BF -81 IS11FDMCURO F. It -AND 1-111-A111)RI'll V-11 IFN:FrIlTlr trMPIMNCC OOIMDMYANIITIIC . 1
M RIMTfSf)I :It RLSKA- LS LAM) AIV•- ICA] NM ARCA - / t �`
AINt�
m
2 ��
Lu LU
Lu e� LU
n
iRId7BFilld.7C
- - - __-.-- ,
Field 7A - - L
_ 0
..IdBG - - - - U
-T ield 6E .. W
Field 6D ly _ uj
Field 6C h
-� Fie Id 6B Field to field 1B .ield 1C leld 1D FWD- FIeId 1F
f i?Id (•.A I
4, � µvNN��gfPRM
_ Y �
Z
K
a?
V zo
Z oQ
UV
�d no
Z Lu
aU� pz
W F LL ?19�
zym UV
W °° r
U)
SFR:/FA7D TOTAI.ACR/S BILAIW IFDACIM NATACR9R SrM/FWD 717FAL AFFIti HI }}kH171.4t Itl:\ Vl l' 41 Nt� I n
SIC -PA -24A 7.55 2.N 5-21 NC-PM2-7C IRn 1.54 3_12
FIGURE 4
W--PA-24B e u L"6AS NGFA-2-7B I.6A 1.51 »2 * • I
Nt-1-A-26C 7.99 IJ3 6.16 NC -PA -2-7E 4.90 Iso 3.26 . CITY OF HAVELOCK
\t -PA-3-60 8.13 u7 6.26 NC -PA -2.7F 45, 1.51 3.0. t� ' 503 LAND APPLICATION PROGRAM
'('PA -24E 5.52 IA2 3.9e W -PA -2-7C 5.10 1.57 3.53 CRAVEN COUNTY
11PA-2.6F 5.16 1.57 3.59 NC -PA -24H 49I 1.54 3.29 I
nC-YA-24(: 5.1e I.7L JJI IVC -PA -2-7I 1.79 I.51 3,25 REFERENCE:
O WQODW702
NC4'A-2-7A 3.OF e.e2 IIF NC -PA -2-71 6.79 1.5/ 325 �S MTAIAYEN3 rLFRk CMr OFROMESRI.INL' PlhA'f U1Fr16SWPISFORI C,RMAT10 PUM NOWY RSNLtWAwTFORDF-. DE FAIL MAP FOR SITES
Iil.AI OR ANV OTIIFR IRCS 1NFRF ARC MIFHNRAMTCCS ABDUf )TS ACCURAGv SFMi. MO ASLMFS ND RFSDON5iBl1 RY iDR ANY eCt'J:HwI
,5 W' -PA -2-7B 6.03 1.46 2.57 NC -PA -2-7K Lal 1.94 2.47 MAoe 1R+Awr ACTwm rAwcw er 7RE usER eASLD ImoN nnsIM ORMAnoR 1 NC -PA -2-6A THROUGH 6G AND
NC -PA -2-7A THROUGH 7N

BIOSOLIDS MANAGEMENT SERVICE AGREEMENT
This SERVICE AGREEMENT (hereinafter called the AGREEMENT) made and entered into
this Ist day of November 2006 (the EFFECTIVE DATE) by and between City of Havelock, NC
(hereinafter called CUSTOMER), and Synagro Central, LLC, (hereinafter called CONTRACTOR
which term shall include its successors and assigns).
WITNESSETH:
In consideration of the following covenants and AGREEMENTS, the CUSTOMER and the
CONTRACTOR hereby mutually agree as follows:
SCOPE
1.1. The CONTRACTOR shall provide b>osolids management services that include
removal, transportation, and land application or other beneficial reuse in accordance with the
terms of this AGREEMENT (hereinafter called SERVICES) of the CUSTOMER'S biosolids
which constitute primarily (liquid semi-solids) residue generated during the treatment of
wastewater (hereinafter called BIOSOLIDS) at the city's wastewater treatment plant located
in Havelock, North Carolina (the PLANT).
2. CONTRACTOR OBLIGATIONS
The CONTRACTOR shall:
2.1. Within four (4) weeks after receipt of notice from CUSTOMER, cause the removal,
transportation, and land application of CUSTOMER'S BIOSOLIDS and, in connection
with such activities, maintain AUTHORIZATIONS and landowner AGREEMENTS
required of CONTRACTOR for agricultural land application and/or disturbed land
reclamation in accordance with all applicable LEGAL REQUIREMENTS which are
currently in effect, or which take effect during the term of this AGREEMENT.
2.2. At the written request of CUSTOMER, and as applicable, provide any
AUTHORIZATIONS which are issued by applicable GOVERNMENTAL
AUTHORITIES for all land approved for BIOSOLIDS land application.
2.3. Notify the CUSTOMER of any notice of violation, action, suit, claim, or legal
proceeding against CONTRACTOR relating to any aspect of the CUSTOMER'S
BIOSOLIDS managed pursuant to this AGREEMENT.
2.4. For BIOSOLIDS which are land applied, employ land application methods approved
or allowed by applicable GOVERNMENTAL AUTHORITIES.
-1-
Havelock Agreement -Final 1107 06 doc

2.5. Develop and implement monitoring, record keeping, and reporting programs as
required by applicable LEGAL REQUIREMENTS, and as set forth in Section 6 of
this AGREEMENT.
2 6. Provide proof of liability and workers' compensation insurance, as set forth in
Section 4 of this AGREEMENT.
2.7. Indemnify CUSTOMER, and hold harmless CUSTOMER, its subsidiaries, affiliates,
successors and assigns and their respective directors, officers, employees,
shareholders, representatives and agents (hereinafter referred to collectively in this
section as CUSTOMER INDEMNITEES) from and against any and all claims,
liabilities, lawsuits, and causes of action, together with reasonable costs, expenses, and
attorneys' fees associated therewith and all amounts paid in defense or settlement of
the foregoing, which may be imposed upon or incurred by CUSTOMER
INDEMNITEES or asserted against CUSTOMER INDEMNITEES by any other
person or persons (including GOVERNMENTAL AUTHORITIES), to the extent
caused by CONTRACTOR'S breach of its obligations under this AGREEMENT or
violation of applicable LEGAL REQUIREMENTS.
2.8. Comply in all material respects with all LEGAL REQUIREMENTS applicable to
CONTRACTOR'S provision of the SERVICES.
2.9. CONTRACTOR'S obligations to take, receive or beneficially reuse BIOSOLIDS shall
be suspended during a Force Majeure.
3. CUSTOMER
The CUSTOMER shall:
3.1. Provide to CONTRACTOR for off-site beneficial reuse 100% of all liquid
BIOSOLIDS generated at the PLANT.
3.2. Provide CONTRACTOR with reasonable access to the CUSTOMER'S BIOSOLID' S
delivery system, except as reasonably required for safety or emergency considerations,
or planned shutdown of the PLANT. It is agreed that when safety, emergency or
shutdown conditions prevent access, that both parties will attempt to resolve such
conditions as expeditiously as possible.
-2-
Havelock Agreement -Final 11 07 06 doc

3.3. Provide CONTRACTOR written notice of the concentration of total nitrogen (as N on
a dry weight basis) in the BIOSOLIDS which CUSTOMER provides, plus all other
information which CONTRACTOR may request to facilitate its compliance with
applicable LEGAL REQUIREMENTS, including without limitation the requirements
of 40 C.F.R. Part 503. Information wluch CONTRACTOR may obtain shall include,
without limitation, the monthly average concentrations (in milligrains per kilogram) of
arsenic, cadmium, copper, lead, mercury, nickel, selenium, and zinc or other
potentially Hazardous Materials present in the BIOSOLIDS, the level of pathogen
reduction which CUSTOMER has achieved. The methods and procedures by which
CUSTOMER samples and analyzes concentrations of potentially HAZARDOUS
MATERIALS, pathogen reduction, shall comply with methods and procedures
prescribed by applicable LEGAL REQUIREMENTS, including without limitation
40 C.F R. Part 503. CUSTOMER shall provide CONTRACTOR with a certification
regarding concentrations of HAZARDOUS MATERIALS, pathogen reduction, as
well as certification that all methods and procedures used by customer for the
sampling and analysis of BIOSOLIDS comply with requirements of 40 C F.R. Part
503, and any other applicable LEGAL REQUIREMENTS. The form of certification,
and the type of information which the CONTRACTOR may request from
CUSTOMER may include the form of certification or the type of information which
CUSTOMER must maintain under 40 C.F.R. § 503 17. CONTRACTOR shall have
the undisputed right to rely upon any information or certification provided by
CUSTOMER, and shall not have any independent duty to investigate or inquire
regarding the subject matter of the CUSTOMER'S certification or of the information
which CUSTOMER provides to CONTRACTOR.
3.4. Not provide to CONTRACTOR any BIOSOLIDS which contain HAZARDOUS
MATERIAL or are hazardous in accordance with 40 C.F.R. Part 261, other federal
law, state law, or which contains a concentration of polychlorinated biphenyls equal to
or greater than 50 milligrams per kilogram of total solids (on a dry weight basis).
3.5. Provide CONTRACTOR with at least [four (4) weeks] advance notice of when
CUSTOMER desires for CONTRACTOR to remove BIOSOLIDS from the PLANT.
3.6. Indemnify, defend, and protect CONTRACTOR from and against all claims, damages,
losses, costs, suits, settlements, causes of action, liabilities, fines, penalties, costs, and
expenses (including but not limited to, investigation and legal expenses, and costs and
expenses associated with Remedial Work) (collectively, CLAIMS) arising out of or in
connection with any acts or omissions of CUSTOMER, or its employees, officers,
directors, representatives, contractors, subcontractors, agents, or affiliates, or any
licensee or mvitee of the PLANT (other than CONTRACTOR), or CUSTOMER'S
breach of any of its obligations under this AGREEMENT, or any violation of any
applicable LEGAL REQUIREMENT by CUSTOMER or any of its employees,
officers, directors, representatives, agents, contractors, subcontractors, or affiliates, or
-3-
Havelock Agreement -Final 11 07 06 doc

its licensees or invitees (other than CONTRACTOR) or any discrepancy in the
character or composition of the BIOSOLIDS from the PLANT compared to analytical
results, certifications or other information provided by CUSTOMER to
CONTRACTOR.
3.7. From time to time, as requested by CONTRACTOR, review a list of proposed land
application sites at which BIOSOLIDS from the PLANT maybe applied, and select
from such sites those sites to which CUSTOMER desires for its BIOSOLIDS to be
applied, and such sites to which it does not desire its BIOSOLIDS to be applied. In
the absence of specific designations by CUSTOMER, CUSTOMER agrees that it shall
have been deemed to select any and/or all of such application as satisfactory locations
for its BIOSOLIDS.
3.8. Notify the CONTRACTOR of operating changes or any other conditions that would
reasonably be expected to affect the BIOSOLIDS handled by CONTRACTOR under
this AGREEMENT.
4. INSURANCE
The CONTRACTOR shall maintain and provide the CUSTOMER evidence of insurance as
follows:
4.1. Worker's Compensation meeting at least the mi iimum requirements of the laws of the
State of North Carolina, and Employer's Liability with a minimum single limit of
$1,000,000.
4.2. Commercial General Liability and Automobile Liability Insurance to include premises
operations and subcontractors. Completed Operations and Contractual Liability are to
be included under the Commercial General Liability coverage. The insurance policies
will have limits of no less than $1,000,000.00 per occurrence and $ 2,000,000.00
aggregate. CUSTOMER shall be named as an additional insured.
5. PAYMENT
The CONTRACTOR shall provide the CUSTOMER with an accounting of the gallons of
BIOSOLIDS removed from the CUSTOMER'S PLANT, and such other information as shall
be reasonably requested. CONTRACTOR will utilize a measurement method based on the
number of tanker loads of BIOSOLIDS removed from the CUSTOMERS'S PLANT and the
capacity, in gallons, of the tankers. The CUSTOMER will be provided with manifests for all
loads removed by the CONTRACTOR.
5.1. The CONTRACTOR shall submit invoices once each month for SERVICES provided
by CONTRACTOR, using the rates and the amounts agreed in Section 10 of this
-4-
Havelock Ao eement-Final 1107 06 doc

AGREEMENT. The CUSTOMER shall pay all invoices within 30 days after receipt
of the invoice.
5.2. It is agreed that in the event of any dispute concerning invoice amount, CUSTOMER
will pay undisputed invoice amounts within 30 days after receipt of the invoice.
6. RECORD KEEPING
The CONTRACTOR shall maintain records and submit sum mary reports to the
CUSTOMER after each hauling event (as requested by CUSTOMER) and on an annual,
cumulative basis. Reports shall include information regarding, but not be limited to:
6.1. Number of loads transported and applied with identification of utilization site(s)
6.2. Such other information as will reasonably allow CUSTOMER to fulfill its
recordkeeping, and reporting requirements under applicable LEGAL
REQUIREMENTS and such other information reasonably deemed by the
CUSTOMER as necessary for this AGREEMENT and which is kept by
CONTRACTOR in the normal course of its business.
7. NOTICES
Except as otherwise provided herein, any notice, demand or other contract disputes or shall
be in writing and shall be personally served, sent by commercial courier service or prepaid
registered or certified mail, or sent by telephonic facsimile delivery with confirmation
thereof. Any such notice shall be deemed communicated upon receipt.
7.1. The following address is hereby designated as the legal address of the
CONTRACTOR. Such address may be changed at any time by notice in writing
delivered to CUSTOMER.
Synagro Central, LLC
7014 E. Baltimore Street
Baltimore, MD 21224
[phone]
Fax: [phone]
Attention: [Stephen Toft]
With a copy to:
Alvin L. Thomas II
General Counsel
Synagro Technologies, Inc.
-5-
Havelock Agreement -Final 11 07 06 doc

1800 Bering Drive, Suite 1000
Houston, Texas 77057
[phone]
[phone] (Fax)
7 2. The following address is hereby designated as the legal address of the CUSTOMER
Such address may be changed at any time by notice in writing delivered to
CONTRACTOR.
Name:
Street Address:
Mailing Address:
Phone Number:
Contact Person:
Fax:
FORCE MAJEURE
City of Havelock
PO Drawer 368
Havelock, NC [28532]
[phone]
Dave Harvell
[phone]
Wherever the word "Force Ma]eure" is used, it should be understood to mean:
8.1. acts of God, landslides, lightning, earthquakes, hurricanes, tornadoes, blizzards and
other adverse and inclement weather, fires, explosions, floods, acts of apublic enemy,
wars, blockades, insurrections, riots or civil disturbances;
8.2. labor disputes, strikes, Work slowdowns, or Work stoppages;
8.3. orders or judgements of any Federal, State or local court, administrative agency or
governmental body, if not the result of willful or negligent action of the party relying
thereon;
8.4. power failure and outages affecting the Premises; and
8.5. any other similar cause or event, including a change in law, regulation, ordinance or
permit, provided that the foregoing is beyond the reasonable control of the party
claiming Force Majeure.
If, because of Force Majeure any party's cost is increased by more than 15% or any party
hereto is rendered unable, wholly or in part, to carry out its obligations under this Contract,
then such party shall give to the other party prompt written notice of the Force Majeure with
reasonable full details concerning it; thereupon the obligation of the party giving the notice, so
far as they are affected by the Force Majeure, shall be suspended during, but no longer than,
the continuance of the Force Majeure. The affected party shall use all possible diligence to
remove the Force Majeure as quickly as possible, but his obligation shall not be deemed to
-6-
Havelock Agreement -Final 1107 06 do,

require the settlement of any strike, lockout, or other labor difficulty contrary to the wishes of
the party involved.
9. TERM
9.1. This AGREEMENT shall be effective from the EFFECTIVE DATE until the 30th day
of September 2011 (the INITIAL TERM). At the end of this term, this
AGREEMENT may be extended on a yearly basis for five (5) additional one year
terms at the option of CUSTOMER and at the mutual agreement in writing of both
parties. The non -defaulting party may terminate this AGREEMENT and shall have no
further obligations to the other party under this AGREEMENT if (i) the other party
fails to observe or perform any material covenant or agreement contained in this
agreement for ten (10) business days after written notice thereof has been given to
such other party by the non-default>ng party or (ii) at any time upon the insolvency of
the other party, or the institution by or against the other party of any proceeding in
bankruptcy or insolvency or for the appointment of a receiver or trustee or for an
assignment for the benefit of creditors.
9.2. CONTRACTOR may terminate this AGREEMENT at any time upon written notice to
CUSTOMER and have no further obligation to CUSTOMER if:
9.2.1. The CONTRACTOR is unable to utilize the BIOSOLIDS due to a change in
any LEGAL REQUIREMENTS that renders the SERVICES illegal, or place
such restrictions or requirements thereon so as to make the provision of the
SERVICES cost prohibitive or to otherwise frustrate the commercial intent of
this AGREEMENT.
9.2.2. The BIOSOLIDS become unsuitable for land application by the
CONTRACTOR by reason of (i) the act or omission of any third party or
CUSTOMER, and through no fault of CONTRACTOR, or (>i) the condition
of the BIOSOLIDS is materially inconsistent with the description and
analysis, certifications or other inforination the CUSTOMER has provided to
the CONTRACTOR regarding the BIOSOLIDS, or (u>) CUSTOMER
breaches its obligations hereunder regarding the quality of the BIOSOLIDS.
9.3. In the event of any change in federal, state or local law or regulation, or any change in
any one of CONTRACTOR'S permits, which is implemented during the Term of this
AGREEMENT and which results in a significant increase or decrease in the cost of
performing the SERVICES, the CUSTOMER and CONTRACTOR agree to attempt
to negotiate a mutually agreeable adjustment to that payment tern -is specified in this
AGREEMENT. Should agreement not be reached, either party may terminate this
AGREEMENT as specified in Article 9.
-7-
Havelock Agreement -Final 11 07 06 doc

10. PRICE
10.1. Except as otherwise provided in this AGREEMENT, CUSTOMER will pay the
following fixed prices for CONTRACTOR'S SERVICES hereunder for the duration
of the INITIAL TERM of this Agreement
Liquid Land Application = $0.057 per gallon
Mobilization = Included at no charge
503 Compliance Sampling (if needed) = Cost plus 15%
Ag -lime (if needed) = Included at no charge
Land Permitting (min 100 acres) = $25.00 per acre
10.2. Upon increases in CONTRACTOR'S costs due to changes in LEGAL
REQUIREMENTS, CONTRACTOR may no more than once each an iiversary year,
request an increase in the fixed prices set forth hereunder. The parties shall in good
faith attempt to negotiate such increase and if successful such shall be effective as of
the beginning of the then most current anniversary of the EFFECTIVE DATE. In
addition, there will be an annual adjustment for price paid for SERVICES provided
by the CONTRACTOR on the anniversary date of the EFFECIVE DATE. The first
adjustment shall be on October 1, 2007, and shall be repeated at the end of each
twelve months thereafter. The adjustment will be the percent increase or decrease in
the Consumer price Index for All Urban Consumers (CPI -U) as published by the U.S.
Department of Labor. The adjustment will be made by multiplying the percent
increase or decrease in the CPI -U over the most recent twelve months reported tames
the current unit price and adding or subtracting the adjustment to the price used
during the previous twelve months.
11. MISCELLANEOUS PROVISIONS.
11 1. Assignment. The CUSTOMER and/or CONTRACTOR shall have the right to assign
this AGREEMENT an writing to any successor in interest, subject to the written
approval of the other party, which approval shall not be unreasonably withheld.
11.2. Governing Law. THIS AGREEMENT AND ALL THE RIGHTS AND DUTIES
OF THE PARTIES ARISING FROM OR RELATING IN ANY WAY TO THE
SUBJECT MATTER OF THIS AGREEMENT OR THE TRANSACTIONS
CONTEMPLATED BY IT, SHALL BE GOVERNED BY, CONSTRUED, AND
ENFORCED IN ACCORDANCE WITH THE LAWS OF THE STATE OF
NORTH CAROLINA.
11.3. Costs and Fees. The prevailing party in any legal proceeding brought by or against
the other party to enforce any provision or term of this AGREEMENT shall be entitled
-s-
Havelock Agreement -Final 11 07 06 doc

to recover against the non -prevailing party the reasonable attorneys' fees, court costs
and other expenses incurred by the prevailing party.
11.4. Consent to Breach Not Waiver. No term or provision hereof shall be deemed
waived and no breach excused, unless such waiver or consent be in writing and signed
by the party claimed to have waived or consented. No consent by any party to, or
waiver of, a breach by the other party shall constitute a consent to, waiver of, or
excuse of any other different or subsequent breach.
11.5. Severability. If any term or provision of this AGREEMENT should be declared
invalid by a court of competent jurisdiction, (i) the remaining terms and provisions of
this AGREEMENT shall be unimpaired, and (ii) the invalid tenn or provision shall be
replaced by such valid tern or provision as comes closest to the intention underlying
the invalid term or provision.
11.6. ENTIRE AGREEMENT. THIS AGREEMENT INCLUDES AND
INCORPORATES BY REFERENCE AS IF FULLY SET FORTH HEREIN,
ALL OF THE TERMS, CONDITIONS AND OBLIGATIONS CONTAINED IN
THIS AGREEMENT, THE INFORMATION FOR PROPOSERS, SPECIFIC
PROVISIONS, AND DRAFT SERVICE AGREEMENT (AS AMENDED).
THIS AGREEMENT, TAKEN WITH THE INFORMATION FOR
PROPOSERS, SPECIFIC PROVISIONS, AND DRAFT SERVICE
AGREEMENT (AS AMENDED) HERETO CONSTITUTES THE COMPLETE
AND EXCLUSIVE STATEMENT OF THE AGREEMENT BETWEEN THE
PARTIES WITH REGARD TO THE MATTERS SET FORTH HEREIN, AND
ALL OTHER AGREEMENTS, PROPOSALS, AND REPRESENTATIONS,
ORAL OR WRITTEN, EXPRESS OR IMPLIED, WITH REGARD THERETO
ARE SUPERSEDED..
11.7. Amendments. This AGREEMENT may be amended from time to time only by an
instrument in writing signed by the parties to this AGREEMENT
11.8. Counterparts. This AGREEMENT maybe executed in counterparts, which together
shall constitute one and the same contract. The parties may execute more than one
copy of this AGREEMENT, each of which shall constitute an original.
11.9 Preaudit Certification. This instrument has been preaudited in the manner required
by the Local Government Budget and Fiscal Control Act.
41teeTillman, Director of Finance
-9-
Havelock Agreement -Final 11 07 06 doc

12. DEFINITIONS
12.1. "AUTHORIZATIONS" means all authorizations, permits, applications, notices of
intent, registrations, variances, and exemptions, required for the removal,
transportation and land application of BIOSOLIDS in compliance with all applicable
LEGAL REQUIREMENTS.
12.2. `BIOSOLIDS" means sludge meeting Class B pathogen requirements, vector
attraction reduction requirements and pollutant concentrations (as defined by 40 CFR
Part 503 and State of North Carolina requirements for land application). Blosolhds
do not include any hazardous materials or substance and must be suitable for land
application under the applicable law.
123. "ENVIRONMENTAL LAWS" means any AUTHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect relating to HAZARDOUS MATERIALS, BIOSOLIDS, or
the protection of the environment, health and safety, or a community's right to know,
including without limitation, the Comprehensive Environmental Response,
Compensation, and Liability Act, the Resource Conservation and Recovery Act, the
Safe Drinking Water Act, the Clean Water Act, the Clean Air Act, the Emergency
Planning and Community Right to Know Act, the Hazardous Materials Transportation
Act, the Occupational Safety and Health Act, and any analogous state or local law.
12.4. "GOVERNMENTAL AUTHORITY" means any foreign governinental authority, the
United States of America, any State of the United States of America, any local
authority, and any political subdivision of any of the foregoing, and any agency,
department, commission, board, bureau, court, tribunal or any other governmental
authority having jurisdiction over this AGREEMENT, 13IOS OLIDS, or COMPANY,
HAULER, or any of their respective assets, properties, sites, facilities or operations.
12.5. "HAZARDOUS MATERIALS" means any "petroleum," "oil," "hazardous waste,"
"hazardous substance," "toxic substance," and "extremely hazardous substance" as
such terms are defined, listed, or regulated under ENVIRONMENTAL LAWS, or as
they become defined, listed, or regulated under ENVIRONMENTAL LAWS.
12.6. "LEGAL REQUIREMENT" means any AUTHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect, including without limitation, ENVIRONMENTAL LAWS
-10-
Havelock Agreement -Final 1107 06 doc

12.7. "REMEDIAL WORK" means investigation, monitoring, clean-up, containment,
removal, storage, remedial or restoration work associated with HAZARDOUS
MATERIALS or BIOSOLIDS.
IN WITNESS WHEREOF, the parties of flus AGREEMENT have hereunto set their hands and seals,
dated as of the day and year first herein written.
C. ("CUSTO R")
ATTEST: 14
aa JJ Q YQS W.
me &Title: RQ, Name &Title: Q2\f\6,, MN Go,,-,
Synagro Central, LLC. ("CONTRACTOR")
FATTEST:
Naive & Title: Alvin L. Thomas, Vice President Name & Title: Dovsha G. Roscoe, Asst. Secretary
Havelock Agreement -Final 1107 06 doe

Amended
Appendix A - Draft Service Agreement
1. General
1. No residuals management operations shall occur on Sundays or legal holidays without
the approval of the Wastewater Treatment Supervisor.
U. All operators shall be well versed with regulations and requirements stipulated in the
EPA 40 C.F.R. Part 503 regulations and the Generator's land application permit
WQ0000702 with the State of North Carolina Department of Environment and Natural
Resources (NCDENR).
III. The total percent solids of the residuals produced by the Generator's facilities shall vary
from 3% #0 6%.A ATeS ons' , or musep ctionj Vgiupii enT
rt is $l' fflion properly in
this range.
1V. The Contractor shall remove all unused materials, tools, equipment and machinery,
waste materials, refuse and other debris from loading area and land application sites.
The Contractor shall see that these sites are at all times left in a neat and orderly
condition.
V. Liquid residuals shall be transported in sealed tank bodies. The capacity of all tankers
and/or any other containers used to calculate the volume of residuals hauled for
payment should be certified by an independent agency capable of performing such
certification. This certification infonnation shall be supplied in writing to the
Wastewater Treatment Supervisor before residuals are hauled for payment.
Vi. All application and transportation, vehicles shall be cleaned no less than once per
month. If residuals are spilled onto vehicles, contractor shall see that the vehicles are
cleaned by the next working day.
VII. The Contractor shall be responsible for repair/replacement of all pavement, driveways,
fences, shrubs, lawns, trees and other public or private property damaged as result of
work performed under agreement with the Generator.
30

VIII. The Contractor shall at all times have a competent project mana11
ger or other
representative on the work site who shall have full authority to act for the Contractor
and who shall see that the work under the Contract is executed in accordance with the
agreement documents. All communications with the project manager shall be binding
as if given to the Contractorbut must be confirmed In writing within 24 hours.
2. Permitting
1. The Contractor shall be responsible for the procurement of additional sites suitable for
land application and shall be responsible for obtaining and compiling the information
^ I accordance with f sch dule
necessary for generation of permit applications/renewals. At a ma,tumum, sukien
acreage must be permitted to annually compensate for the number of acres lost during
the prior year and any increase in biosoiids productions. which approval shall not be unreasonably
withheld n
H. All sites shall meet the approval of the Generator prior to permitting by the State. The
Generator also reserves the right to prohibit the permitting of any site, but such prohibition is subtect to the
reasonableness standard
.III. A copy of the Land Application Permit WQ0000702 and all site maps shall be
maintained on each application vehicle at all times when residuals are being applied.
give Generator reasonable notice
IV. The Contractor shall prior to any correspondence with regulatory
agencies regarding regulatory issues concerning the Generator. All correspondences
shall be copied to the Generator.
V. On a yearly basis, every permitting event, or in the event that development or other
issues require changes in buffers/maps, the Contractor shall be responsible for
providing updated maps for the Land Application Site Books. The project manager
shall evaluate each site during application event for possible adjustments to
buffers/maps.
3. Emergency ResponselSpills
1. The Contractor shall submit to the Generator for approval a Spill Control Plan.
II. A copy of the Spill Control Plan shall be maintained in each transport and application
velucle used by the Contractor.
31

III. Any spills involved with the loading, transportation and/or application of the said
residuals shall be deemed the responsibility of the Contractor and shall be cleaned up
inunediately to the satiaspactibon of the Generator, NCDENR, Division of Water Quality
and/or any landowner that may be involved. Any occurrences shall be inumdiately
reported to the Wastewater Treatment Supervisor.
4. Beneficial Reuse
I. The Contractor shall utilize equipment capable of both surface application and
,,ubsurface uijection/incorporation ind shall provide such capability at the request of the
enerator
1dfi4& as is required to meet vector attraction reduction requirements. at a negotiated price)
II. No residuals generated by the Generator shall be stored at facilities or land -applied on
land not permitted/approved in the Generator's land application permit for NC DENR.
III. All buffer zones shall be marked#x prior to land application.
IV. Any interruption (other than inclement weather) of the beneficial reuse activities for any
period of time longer than (2) days shall be reported to the Generator immediately,
when such interruption is determined.
V. The Contractor shall provide adequate supervision of its employees to mgr proper
application tech-niques are being utilized at all times.
VI. The Contractor shall provide individuals who are capable of and can maintain good
relations with the program participants. Failure to do so shall be grounds for the
immediate suspension of work and the possibility of the revocation of agreement,
VII. The Contractor shall make every effort to provide residuals application to all program
participants.
VIII. The Contractor shall provide the landowner with a copy of the analysis of residuals land
applied to his/her field.(farm report)
IX. Transporters of the Contractor should be aware that they present an image of the
Generator, therefore they should properly and professionally respond to any complaints
by citizens and/or the Generator. This includes but is not limited to obeying all traffic
laws.
32

5. Monitoring/Recordkeeping
I. The Contractor shall be responsible for all monitoring at the land application sites as
required by the Generator's Land Application permit nWQ0000702 and the EPA 40
C.F.R. Part. All residuals sampling shall be the responsibility of the Generator's
V►WTP Personnel.
H. All infonnation shall be kept on file with the Contractor and the Generator. The
Generator requires that the Contractor have a database management system for the
storage of data for residuals management activities performed for the Generator. Um
III. The Contractor shall keep daily logs indicating tanker loading, transportation, and
application volumes, These logs shall be totaled daily and a copy submitted to the
Generator's Residuals Supervisor no later than 4:00 p.m. on the first working day of the
following week.
IV. A report, after each land application event, shall be provided to the Generator indicating
volume of residuals, application rate per acre, land applied, and land application site
information. This information shall include all information as required by the land
application permit and 40 C.F.R. Part 503 regulations. These records shall be
submitted to the Generator by the 15'h day of the following month after the application
event
6. Public Education/Acceptance
cooperate with Generator
I. The Contractor shall h&inodywiin a Public Education Campaign for the Generator.
H. The Contractor shall assist the Generator with the handling of complaints and/or
questions regarding all residual management activities.
III. The Contractor shall maintain good relations with program participants and shall
provide documented notification of biosolids issues that could impact
program/particip ants.
N. The Contractor shall assist the Generator with any other public notification that maybe
required by the regulatory agencies.
33

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
First Species Effluent Toxicity Testing Data
2015-2017

iceAnajt4ica' Plce Analytical
Pa � 1
Laboratory Report
Nit An Hough
City of Havelock
RCCOff tele
03. �� ,
Drawer 358
Date Rc c -;ped
304 N Jackson Dr
Havelock, NC 28532
P-ole:.t BIOASSAY C2118115
Pate Protect No G2237S53
Sampla PIPE 007
Lab ID
92237953001 Collcc
Pa amoters Rasuits
C duh�a Ful--ange Chonlc
Units Repert L mr AI ,'y r d
nu l tiers
Rei -..ed by--
S:a�y Tark-
SiaCy t, "loot f)awlaos (o11)
Raleigh Certification 1ps
3%'l Ccrrcion ; Di e r ., �i,l NC 27,50,
No,it: (arehna l4'astc :ate1 Cc ficaUon r
Nn't, iot n Bio;" ay C- „fi--a , un
r 57
N0111 CargL'7a -)I ':'n.7 Mmol i erjifli
P 'U ! 177,1

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility Havelock VWVTP NPDES# NC 0021253 Pipe# 001 County Craven
Laboratory Performing Test -Face Analytical Sernces Inc, Raleigh Comments INCO 92237953
x G n JG,I I� X
Signature of O R C J :'Signature of Lab Supervisor
SampEe Information
Collection Start Date
Grab
Composite
(DUralion)
Hardness(mg1
Spec Cono (prnhos/cn
Chlonne(mgf
Sample temp at receip
Sample 1
Sample 2
Control
02/16115
02/18/15
Er*1 Time
9 41
5far
----------
Start Reruw' penew,
24
24
24
"
824
786 822
48
678
672
210
<0 1
<0 1
782 783 790
630
05 "c
;
Test
Information`
Treatment
pH Initial
pH Final
D O Initial
DO Final
Temp Initial
Temp Final
Start Date
02118/
15
End Date
02/25/15
,wt Trnte
12 40
Er*1 Time
9 41
5far
Renewl Re'rev,2
Start Reruw' penew,
r
10o
-
100 100 "
Lonnul c-ontrol Conlrcl
824
786 822
780 7 70 792
866
862 856
784 796 780
8 19
874 f 769
782 783 790
630
830 344
7 00 8 11 859
24 1
253 244
24 2 243 24 5
251
253 253
254 259 24 1
Organism# Chronic Test Results
1 2 3 4 5 6 7 8 9 10 1' 12 Final Control Mortality 9 0
Control
',U Contiol 3rd 6roo. 100
Control Repro C4
48 Hour tulortaiity
Control ivVC
1 23 4 5 G 7 8 9 10 11 12 ^��
Sign,ficant?� ® EAdult
Effluent%
# Young
23
25
25
24
1
24
18
26
25
25
# Young
21
26
25
28
22
24
25
25
20
31
L
L
247
Adult
(L)ive (D)ead
L
L
L
L
L
L
L
L
L
L
26
26
23
',U Contiol 3rd 6roo. 100
Control Repro C4
48 Hour tulortaiity
Control ivVC
1 23 4 5 G 7 8 9 10 11 12 ^��
Sign,ficant?� ® EAdult
Effluent%
# Young
23
25
25
24
1
24
18
26
25
25
26
31
za 4
12
(L)ive (D)ead
L29
L
L
L
L
L
L
L
L
L
L
L
°°°Final
Mortality St ni icant
°/u or N4 CGlit,
— —
14—
Effluent%
# Young
L36
2926
26
26
23
2921
2425
�cr
Rep oJuctior lyAnasts
RPprn t OEC=`110", NOEC= 100Adult
Melt od Dunnelta(1-ave
Normal Dslnn� �= atetnod KJIR76GO(OJ
tic 0,30638 Crrcal 1 i,35
(D)ead
L
L
L
L
L
IL
IL
L
L
�.j
,
Effluent%
90
Effluent%
95
Lqual Vdnances?_ "it's Method 3aritetts
Statstic 41E4f6 Cmical 150863
Non_Patanietnc, "^ riaiysis h appitcabie)
Method _
Effluent N�- nh Sum Cr tical Sura
1 2 3 4 5 6 7 8 9 10 tl,,
Effluent% # Young 20 23 1 28 27 32 21 26 26 23 23 249 Overall Analysis
Rosull = Pass or
100 adult L L L L L L L L L L Test LOEC= 100 %. NOEC= 100 °rn
(L)ive (D)ead es, Chronic Value= X100 °!
Shou.d use highest test concenlration or
ATT Environmental Sciences Branch highest concr,ntratio 1 with D 0 = f o mgn
MAIL Div of Water Quality
N C DENR
TO: 1621 Mall Service Center
Raleigh N C 27699-1621 DWQ form AT -3 (8/9') Rev 11195
# Young
26
26
31
19
12
24
25
27
1 21
24
23 5
Adult
L
L
L
L
L
L
L
L
IL
L
4 '`
(L)ive (D)ead
Lqual Vdnances?_ "it's Method 3aritetts
Statstic 41E4f6 Cmical 150863
Non_Patanietnc, "^ riaiysis h appitcabie)
Method _
Effluent N�- nh Sum Cr tical Sura
1 2 3 4 5 6 7 8 9 10 tl,,
Effluent% # Young 20 23 1 28 27 32 21 26 26 23 23 249 Overall Analysis
Rosull = Pass or
100 adult L L L L L L L L L L Test LOEC= 100 %. NOEC= 100 °rn
(L)ive (D)ead es, Chronic Value= X100 °!
Shou.d use highest test concenlration or
ATT Environmental Sciences Branch highest concr,ntratio 1 with D 0 = f o mgn
MAIL Div of Water Quality
N C DENR
TO: 1621 Mall Service Center
Raleigh N C 27699-1621 DWQ form AT -3 (8/9') Rev 11195
Young
27
23
33
24
29
31 1
23
23
27
2726
7
Adult
(L)Ive (D)ead
L
L
L
L
L
L
L
L
L
L
t, tt
Lqual Vdnances?_ "it's Method 3aritetts
Statstic 41E4f6 Cmical 150863
Non_Patanietnc, "^ riaiysis h appitcabie)
Method _
Effluent N�- nh Sum Cr tical Sura
1 2 3 4 5 6 7 8 9 10 tl,,
Effluent% # Young 20 23 1 28 27 32 21 26 26 23 23 249 Overall Analysis
Rosull = Pass or
100 adult L L L L L L L L L L Test LOEC= 100 %. NOEC= 100 °rn
(L)ive (D)ead es, Chronic Value= X100 °!
Shou.d use highest test concenlration or
ATT Environmental Sciences Branch highest concr,ntratio 1 with D 0 = f o mgn
MAIL Div of Water Quality
N C DENR
TO: 1621 Mall Service Center
Raleigh N C 27699-1621 DWQ form AT -3 (8/9') Rev 11195

control
Ceriodaphnia Survival and Reproduction Test -Reproduction
Start Date 2/1$;2015
Test ID
havelock
Sample !D
End Date 2125/2015
Lab ID
FACE -Pace - Raleigh -016
Sample type
Sample Date
Protocol
EPAF 91 -ERA Freshwater
Test Saocies CD Cenodaphnia dubia
Comments
25 000
2,1000
2.1 OOC
Conc-% 1 2
3
4 5 6
7 8 9 10
control
21 UUU
26 000
25 000
28 000
22 000
2-1000
25 000
25 000
20 000
31 000
45
29 000
23 000
25 000
25 000
2,1000
2.1 OOC
18 000
26.000
25 000
25 000
675
36 000
29 000
2.6 000
26 000
26 000
94 000
29 ON
21 000
24 000
25 000
90
26 000
26 000
31 000
19 000
12 000
24 OUO
25 Off
27 000
21 000
2-1000
95
27000
23 000
33 000
24 000
29 000
31 000
23 OOC
23 000
?1000
270,)o
100
20 000
23 000
28 nOO
27000
32 000
21 000
?6,000
20 OOO
23 000
23 OOu
Cone %
Mean
N -Mean
Mean
Transform- Untransformed
Min Max CV°o
N
t -Stat
1 -Tailed
Critical
MSD
control
2,1700
1 0000
24 700
20,000
31 000
13 230
10
MSB
MSE F-Prob
df
45
24 400
09879
24 400
18 000
29 000
11 298
10
0 175
2 287
3 9' 3
675
26 500
1 0729
26 500
21 000
36 000
15 635
10
-1 052
2 287
3 9':)
90
23 500
09514
23 50C
12 000
31 000
2208-D
10
0 701
2 287
3 913
95
26 700
1 0810
26 700
23 000
33 000
13 ? 18
10
-1 169
2 267
3 013
100
24 900
1 0081
24900
20 000
32 000
1447-1
10
-0 117
2287
3 913
Auxiliary Tests
Statistic
Critical
Skew
Kurt
Kolmn9orov D Test indicates normal distnoution (p > 0 01)
066608
1 035
-C 0517
1 157.=8
Bartlett's Test indicates equal variances (p = 0 53)
4 16405
150863
Hypothesis Test (1 -tail, 0.05) NOEC LOEC ChV
TU MSDu MSDp
MSB
MSE F-Prob
df
Dunnett's Tcst 100 >100
1 391266 0158,11
15 5367
14 6389 039193
5,54
40
35
30
225
=O 20
0
Q
cc 15
10
F
Dose -Response Piot
T . . . . . . . y .. . . . . . .. . . . . . . y . . . . . . . . . . . . . . . �
04-
1 -tail 0 05 level
at significance
Page 1 ToxCalc, v5 0 23 Reviewed by T-) )

- t'oeacentration—
Control 7 � I
Total
G
L
i L'
Y � I
Total c < �
2
-
7 - - --—
•' ota l �A
2 � l
7
Total
— Replicates - - - --- - — ---------�
Lt:-- •'� I �! 1 1 �- 1
ite
E7�
r
Pace lnaly tical
3•'es11sr
l'nne
C erlo(%fZf hifia dribia Chronic Fest
_
2
LLL'
5-
I
NPDhS ft
•--�� �
I�`l�
'� !r �
t lilt lit, [ratl,i�ilnAtCIltticl tf�'_. _-���`'-- Oro,tm,mHornIDat�'7llnli <_I_j'.��_, ��� -�
��. l!Z I „nc f r�i r( ulturi 1 �j�5_ Orvalli'm '-walt-r
r'
j` '�z'I �-`I 'r �'`-
�
Da"
1 ._)�
„�• 1 t C)r .lnt`m �S—
01 U110 )ti 1 � _�
1tll Il l) 1t1t1U11 ��a`cI 1C1111, roolell lll"ll
J 7
-
DaN 4DLUL-
_
I Illy
--
�c r
lnal ,I Ranuorm/cel V"' Incubator
��
DaN _
c <
1 lrin,irr Dat, t5'— I lm�
—�
�nahst
I ra t,trr DatC Tlmc
--- -
`-Yi "
1--nditn€ Date 111C
alN `t Rc\
- t'oeacentration—
Control 7 � I
Total
G
L
i L'
Y � I
Total c < �
2
-
7 - - --—
•' ota l �A
2 � l
7
Total
— Replicates - - - --- - — ---------�
Lt:-- •'� I �! 1 1 �- 1
ite
E7�
r
I otal
I
t « til l�
_
2
LLL'
5-
I otal
I
LLL'
I
I.

Pace Ana a tica i
Incnhatot # 1I)A 1)alr
m'])1 5 it: Raltdmmvecl �f --- 1't d 1) 11c ? 1 tlnc
2'��
D1lutlan 1l�atcr Batch- ��'�"�� Cul;utc !Valet '1'ct-,'
1 _�.-, •-___
: •
Tc,t1---
;lmctcl — Cmnirml
Collection DatC � ��a ����.Qt;
Sample 1"emp CC• ► , ,: i
pII 100% ------ `:
_ p
Chlorine (ttl('/l_,l-
'-
CondlictICit) (pslent)
I Tardncss (nr�!L) ---�
��._—�—...�N
___e�__w..
�
IOO`i�cillilcnl) �
(l�tl)`��':ilill�tll) _�
Illi
Start
End
St_��rt
�
hrttt
Start
t;tl[I__
Control
� �r�•y xi �
"lYcalment 2
„ L' � �
c �• �.Ct ��
-h '���
� � � t'-t�` �
� ��'� r .:t ��
I � j�„
mo.
Start
End
st.11A
I;rtd
� ;start
I I;atti
( nig/ l
Cmntlol
{ c
III
-4 C)c,--
tri r
GJ
r 5\f-
-
`(
TI e,ament 2
a _x Y-= - •--
J •' `�
-`►t<iCt � u
,
Temp_{rattire
End
stat't
� i' Itil
� �tttf"t
1
i I'nd
Colitiol
Treatment ^
;lmctcl — Cmnirml
Collection DatC � ��a ����.Qt;
Sample 1"emp CC• ► , ,: i
pII 100% ------ `:
_ p
Chlorine (ttl('/l_,l-
'-
CondlictICit) (pslent)
I Tardncss (nr�!L) ---�
��._—�—...�N
IOO`i�cillilcnl) �
(l�tl)`��':ilill�tll) _�
kC�
� �r�•y xi �
4r xA�ls
`r 2 1 =l5'

F Y,
n irm El. -r
L
Dc.—sav Cham
JL
-;.Djn�v 1-9n lit
Urlue,,-, DALItIO-1 IJVVC:). (!(Jc
Pla-it Flo4�
8ariPle, Collector PlInt
------- --- --
Composite
)aa Time
,)-A3 Ended q
jj; Pi
Sarnnlc"; P.'I' Hr H.s
Grab
Date Titre !L&.' or IDM
, ajqp,e_ I lol I 11IR'd d Li HI I�Q
1&7 f It
tMethod of to tne Lab
,.tlqlrl () (,,I:; Oc IV Ci 8£8
71
r7R,t,I:nquIbh(-�d B -v
Time
F.'-ue
comments
For Pace IrIc. US,1201-liy
W o r k 0 i . Ie. r N U I - I b 0 r.
Recumg ',empeiatura By tie
Fac_ A-Illyt- -'11 Seg cAms, Inc Mdress 0701 3011"Mrc- 1"; , F'Ach 'Ac '7607 (91

Ali, 1,
Ch-Rirl OI GU3t0dV FO011
cl
D lutioc, (INC)
0 c
C�h
Qici6l,,)
(A'Aector
Print
uuro
ocamolc rwo
composhe
Date Stal tad
Date, E-7,ided
Sarl"plf:-, per H,
G nab
Date
SarrlPl) VQ,Lfn,(-,
'?, d, i5 T-11 1"c"
JN In') Ll
iod (if I rinspoi tation to tne
Time All or U,
chilled uun)g
CIT2 1-11 OTC; L I F
G or
Gornments:
r! 1.jr7
For Pace Analytieal, m-. Use -�)
PaC 0 Woo,Ordol %lllb-:,r .1y
Rcx,emng Tornponaturc- 5-T R.eccx'd By, �j,"
PaceAnalytiu-al SenJC�S, Inc P%ddMl�s Gonfron, r Fir rpip:g!,ri, 276o,, F,,,cfj-
[rile
zr, n
-cj by
Gornments:
r! 1.jr7
For Pace Analytieal, m-. Use -�)
PaC 0 Woo,Ordol %lllb-:,r .1y
Rcx,emng Tornponaturc- 5-T R.eccx'd By, �j,"
PaceAnalytiu-al SenJC�S, Inc P%ddMl�s Gonfron, r Fir rpip:g!,ri, 276o,, F,,,cfj-

Face Analytical
")-A",.1s"wi
Mr Art Hough
City of Havelock
Drawer 368
304 N Jackson Dr
Havelock, NC 28532
Project Metals 1%29
Pace Project No 92238951
Sample. HAVELOCK BIOASSAY METALS
Laboratory Report
Pace Analyttrai Servines, Inc
1225
AShcv �NC tcttl:
Page 1 of i
Report Date 03103/2015
Date Recelvea 02126/201 5
Lab ID 92238951001 Collected 01-29;15 08 00 Matrix mater
Parameters
Results
Units
Report L nut
Analyzed 4loahfiors
Aluminum
ND
-g'L
100
03/02/15 21 15
Antimony
ND
ugrL
50
33/02/15 21 15
Arsenic
ND
ugrL
10 0
0°•,02115 21 15
Barium
ND
ugrL
50
0 102' 15 1.1 15
Beryllium
Nn
ugrL
1 0
03/02/15 21 15
Boron
122
ugiL
500
03/03/15 15 2C
Cadmium
ND
ugiL
1 0
03/02'15 21 15
Calc um
39000
ugrL
100
031C2 15 2' 15
Chromium
ND
UU/l-
50
03102,15 2. 15
Cobalt
ND
ug/L
5 0
031C2,15 2 15
Cooper
ND
ugrL
5 C
03/02.15 21 15
Iron
ND
a 11-
9
50 C
03102,15 � I 5
Lead
ND
uc;4-
5C
03107,1521'5
Maanesrum
2120
ug,'L
100
03'0211511 15
Manganese
6-0
ug/L
50
03,'02;15-1115
Molybcenum
ND
ug/L
5 0
03'02,15 21 15
Nickel
ND
uy/L
50
C3 02115 21 15
Potassium
6110
ug/L
530C
63,02_;1521 15
Selenium
ND
119/1
10 0
03102 115 21 15
S.licon
6240
ugrL
100
0+'02/15 21 15
Silver
ND
ug/l-
5 0
03/02/15 71 15
SOCiLr11
80000
ugrL
5060
03,'02,15 21 I r
Strontium
145
ug/L
i 0
03102;15 2 115
Thallium
ND
,1911-
100
03,'02,'15 2 1 15
Tin
ND
tg/L
5 0
03/02/15 21 15
Ti.anium
ND
u0/1
5 0
03102/15 2, 15
Vanadium
ND
ug/L
50
03i32115 2 1 1 r -i
Zinc
370
ug; L
10 0
03/02 5 21 15
Revievied by
Stacv Taile
stacy tarle,c pacalabs com
Asheville Certification IDs
2225 Riverside Drive Asheville, NC 28804 North CdroDna UVas'ewaler Certification # 40
Florida/NELAP Certification n E8l648 South Carolina Cer, ficatror # 99030001
Massachusetts Certification # M-NCO30 West Virginia Certification A 356
North Carolina Dnnki-ig Water Certification # 37712 Virgmia'VELAP Certlf cation a 46022"

Cleaning lab wait .or WET testing
Steps
Initials/ date
Clean pickle jar with 1/10 oz liquinox and tap water
Rinse with cold tap water twice.
Mix up 10% nirtic acid solution in fume hood wear appropriate PPE.
Rinse pickle far with 10% nitric acid solution with lid on far
Rinse jar with deionized water twice
Rinse jar with pesticide grade acetone Use fume hood and wear PPE as required
r'
Rinse jar with deionized water three times.
Take jar to sampling point effluent sampler.
Replace sampler tubing with new food grade silicone tubing
Rinse tubing and far 3 time with sample water. Ensure jar is filled with sample water.
Empty jar and put in sampler and begin sampling.
Repeat steps every sampling event

effluent Toxicity Report Form - Chronic Pass/Fa3.1 and Acuti.- LCI-, Date: 04/21/15
Fa:ility: CITY C,F HAVELOCK WWTP NPDES# NCO021253 Fipeg, 001 County, CRAVEN
Laboratory Performing Test: PACE ANALYTICAL
Comment~.
X �
.�,-.nn
X
gna
Work Order: 92244399
isor * PA2SED: 8.27% deduction
Environmer,,al Sciences Branch
MAIL ORIGINAL TO. Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Iorth Carolina Ceriodapnnia
Chronic Pass/Fall Reproduction Toxicity Test
.ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
4 Young Produced 1135133136128132134126133127129133129
Adult (L)ive (D)ead JAL IL IL IL IL IL IL IL IL IL IL IL
effluent 6: 906
'REATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV
10.580%
# Young Produced 33133125130 24 31129128 27 29 27 28 6 control orgs
producing 3rd
brood
Adult (L) ive (D) ead TLL L JL_ L L L L L L IL
L 11 1001-.
Chronic Test Results
Calculated t = 2.063
Tabular t = 2 508
Reduction = 8.27
6 Mortality
Avg.Reprod.
0 00
31.25
Control
Control
0.00
28.67
Treatment 2
Treatment 2
PASS FAIL
F] El
Check One
1st sample 1st sample 2nd sample Complete This For Either Test
pH Test Start Date: 04/08/15
Control 7 71 7.20 7.38 7.69 7.58 7 68 Collection (Start) Date
Sample 1: 04/06/15 Sample 2. 04/08/15
Treatment 2 8 30 7.95 8.26 8.59 8.40 8 45 Sample Type/Duration 2nd
1st P/F
s s s Grab Comp Duration D
t e t e t e - I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24 hrs T P P
lst sample 1st sample 2nd sample
D.O. Hardness(mg/1) 50 ........ .........
Control 7.13 8.10 6 39 4 85 7.78 6.99
Spec. Cond.(µmhos) 241 779 762
Treatment 2 8 07 7.85 7.73 6.05 6.25 5.98
Chlorine(mg/1) ,,,,,.,. <0.1 <0.1
LC50/Acute Toxicity Test Sample temp_ at receipt(OC) ,,,,.,., 0 9 0.5
(Mortality expressed as 6, combining replicates)
Note: Please
% % % 6 % Concentration Complete This
° a ° o ° o o s °
Section Also
o Mortality
start/end start/end
LC50 = - Method of Determination Control
95% Confidenceimits Moving Average Probit _
Spearman Karber — Other High
Conc.
pH D 0.
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4 41)

e
t
Effluent Toxicity Statistical Results
- Chronic
Pass/Fail Date: 04/21/15
Facility: CITY OF HAVELOCK WWTP
NPDES#:
N00021253 Pipe#• 001 County.CRAVEN
Laboratory Performing Test: PACE ANALYTICAL
0 3333
Reduction: 8.27%
CONTROL
90a Effluent
# Replicates
12
12
Female Live
12
12
Adult Male
0
0
Adult Dead
0
30
1 3333
4
0
Adult Mortality
0.001
0.0096
# Neonates
375
344
Mean # Neonates
31.250
28.667
Standard Deviation
3.306
2.807
Coefficient of Variation
10.580%
6
Fisher's Exact Test
A = 12 B = 12 a = 12 b = 12
a/A = 1.00 b/B = 1.00
Success is survival
Critical b value = 8
12 > 8
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
I Group Neonates Centered i Group Neonates Centered
1
C
26
-5.2500
13
E
29
0 3333
2
E
24
-4.6667
14
C
32
0.7500
3
C
27
-4.2500
15
E
30
1 3333
4
E
25
-3.6667
16
C
33
1.7500
5
C
28
-3.2500
17
C
33
1 7500
6
C
29
-2.2500
18
C
33
1 7500
7
C
29
-2.2500
19
E
31
2.3333
8
E
27
-1.6667
20
C
34
2 7500
9
E
27
-1.6667
21
C
35
3.7500
10
E
28
-0.6667
22
E
33
4 3333
11
E
28
-0.6667
23
E
33
4.3333
12
E
29
0.3333
24
C
36
4.7500

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont )
COEFFICIENTS AND DIFFERENCES
1 x(n-i-1) x(I) a(i) x(n-i-1) - x(i)
1
2
4.7500
4.3333
-5.2500
0.4493
10.0000
3
4.3333
-4.6667
-4.2500
0 3098
9 0000
4
3.7500
-3.6667
0.2554
0.2145
8.5833
5
6
2.7500
-3.2500
0.1807
7 4167
6
6 0000
0000
7
2.3333
1.7500
-2.2500
0.1512
5833
8
1.7500
-2.2500
-1.6667
0.1245
4.0000
9
1.7500
-1.6667
0.0997
0.0764
3.4167
10
11
1.3333
-0.6667
0.0539
3 4167
2.0000
12
0.7500
0.3333
-0.6667
0.0321
1.4167
0.3333
0.0107
0.0000
1
W =
206.9167
Calculated W = 0.960
X 198.6524
Critical W = 0.884
0.960 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
Test Passes!
F test for Homogeneity of Variance
Control variance 10.9318
F = - = 1.39
Effluent variance 7.8788
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.39 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
31.3 - 28.7
t = = 2.063
1.252
Degrees of freedom = 22
Critical t = 2 508
2.063 < 2.508
Test passed. There is not a significant difference in reproduction
between the Control and the effluent evaluated at a 990 confidence interval
Chronic Test PASSES
0

e
'q"rdmdaFhnia dubia tCh onk Pass/Faf. T
Client: NPDES #. NC
Culture l:ansfer (Da1te,�/Ti,� e : -
Age of Orga333zm { " i� Organism Born (Date/Time)-
Ddution Water Batch: Time Ped (Culture)
Start Date: Z44— Temp Dilution Water:
I" Transfer Date -Time- y
Analyst � ` Randomi
2 1�ansfer Date Tune:
Ending Date - Analyst•
_ --- Time, Analyst:
C©�atr®1-------------------------- -----------------------------------------
-
Day 1 2 3 4 5 6 7 8 ---.
# Youngproduced �(C1 9 1 a
Adult Live, Dead r i
+-
Day 5 1
4# Young Producedf i �3 4r _ 5 h �. g 9 10
U tet) P
# Total produced
Test
�sj— — �-
_ _`
Days Fed ]By Time
l� / -- 1��C�
Organism source: -.�L�,
Temp .Cock
Day p
Day I
solution �
ed: V Incubator: �A,Z
Day 2
2-D
Day 3 1 Z- uS
;wed by:S i
Day 4
Day 51 2
----------------;
Day 6
11 12
Collection (Start) Date
D.O.
Start
1S` Sample. r
2nd Sample
L—
SaYmPle TylseMuua-tion
Control
11 12
/ .
Grab
is' sample-
ample12
Cornposite Duratior_
12i
i
COntT01
1S` Sample 2n Sample
Hardness
(mg/L)
Ll 12
Conductivity
(ILS1cm)I
2-14
`]
--u
3 '
Chlorme
Sample Temp
(°C)
c�>
5
11
12
pH 100%
3�
PH
Start
Enol!
Start
End
-Eand.
Control
2-D
I.6Z
,1• CC -1
Treatment
D.O.
Start
End
Start
End � Start
End
Control
I yJ
10
'
25
11 1212 _ Temp` Start F,rnd Start End St:. n¢, i w'nti
Control
------------------ Tzeaiznezlt;

a-�-wuicni ivGlOe Uare ROVI3ed June 22, 2011
lCa/ Bioassay Chain of Custody Page 1 of 1
° ( , Document Numbei
RAL-CS-007-iev 01 issuing Authority
— Pace Carolinas Quahiy r m n
B10cqssay Chain ®f CUsfady Fora
Facility Name �(�
Address.�4 k -------- - -
�h-a P.0 Box
County l Ta\jen
% Effluent Dilution (iWC)• 160110
__��
Plant Flow Is
Sample Collector, Print
Signat
Samp— le- Type
composite
Date Started
Date Ended
Samples per Hr
Grab
Date
Sample Volume.
Contact _ �r-}- -�-I�•} �q� ---
NPDES permit# ��I--a�'-- pipe -
Test Method C.e�rll���I
Ll _� Time.Q_ I &r PM
:15 Tune; pyC; 6 -or PM
Hrs
jMethod of Transportation fio the Lab_
Time ___-_•________AM or PM
Chilled during Collect%9Wes r No
®r PrValInc, Use Only
Pace Work Order Dumber. ���t,
Receiving Temperature. 0 y r� Ret;eued By:
Pace Analytical Services, Inc Address* 67n1 Conference Dr, Raleigh NC 27607 Phone [phone]

wbufnenl NaMO
Bioassay Chain of Cush
Document Number
-MLL S -007 -rev 05
JB6Oa-ssay Chain ®f Cusi®dy Form
Facility Name d r 40, V(-) 1
Address:
uato Revised. June 22, 2012
Page 1 of 1
Issuing Authority
Pace Carolinas Quality Office
56 r PO E3ox _
Va Gm lo/7
Contact P
County: ���/en NPDES permit#.ISL°OSI �;SVo pipe: 6 4
Effluent Dilution (IWC): l— Test Method. r 0 6 J
Plant Flow: J, r M (r k^j
ff
Sample Collector: Print
Signa
Sample Type:
composite
Date Started
Date Ended
Samples per Nr
Grab
Date:
Sample Volume.
! Time -,
PM
a S Time: D M r PM
# I irs:
Time: Alti9 or PM
Chilled during Collectun?
Yes or No
Tiatn o us o v e ease _ __
r■I��11M/i{!�/1I�/'1���,.'�!`l/,II/�.C�ill�,i.'I�
��
I
_..
i
111VIA 11"UMS:
For Pace Analytical, Inc. Use only
Pace Work Order Number.
Receiving Temperature: I ' Receved gy: '
Pace Analytical Services, Inc Address 6701 Conference Dr., Raleigh, N 27607 Phone (9`19)834-4 84

environments , Inc.
FU Box 15414, Greenville, SC 29606
[phone] FAX [phone]
Craftsman Court, Greer, SC 29650
TOXICITY IDENTIFICATION EVALUATION
USING EDTA CHELATION
TO INVESTIGATE THE POTENTIAL ROLE
OF COPPER AND ZINC IN EFFLUENT TOXICITY
Facility: City of Havelock, NC
Sample ID: WWTP Effluent
April 2015
Page 1 of 22

1.0 INTRODUCTION
In March 2015 a chronic pass/fail toxicity test of effluent from the City of Havelock wastewater
treatment plant (WWTP) indicated a failure Under the Division of Water Resources ATB Action Level
Document for Copper and Zinc (10/25/2000), a toxicity test failure must be followed either by
acceptance of copper and zinc limits or by testing options to confirm that these metals were not the cause
of toxicity. In response to the March 2015 toxicity failure, the City of Havelock has opted to use Option
3, which involves the EDTA treatment under a Toxicity Identification Evaluation to investigate the role
of copper and zinc Specifically, a sample of effluent was tested for chronic toxicity with and without
addition of the metal chelator EDTA EDTA is effective for removal of toxicity caused by cationic
metals such as copper and zinc This report presents the results of the investigation.
Page 2 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

2.0 SAMPLE COLLECTION
A sample of effluent was collected on March 20, 2015 It was assigned ETT ID#44986
3.0 TREATMENT METHODOLOGY
A stock solution of 500 mg/L of disodium EDTA was prepared by adding 0.5 g of solid to 1000
mL of deiomzed water.
10 mL of the 500 ing/L stock solution were added to 1000 mL of Havelock effluent. This
provided an aliquot of effluent with 5 mg/L of EDTA
The 5.0 mg/L EDTA spiked effluent was diluted with surface water to prepare test concentrations
of 45, 60, 75, 90 and 100%. These samples were used to initiate the test and to renew the test
solutions on Day 2 and Day 5 of the test, as per NCDENR protocols.
An aliquot of surface water also was spiked with 5.0 mg/L of EDTA to function as an EDTA
control
Page 3 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

4.0 TOXICITY TESTING METHODS
Toxicity testing was conducted using the Short-term Methods for Measia-117g the Chronic Toxicity of
Effluents and Receiving Waters to Freshwater Organisms Method 2002 EPA -821-R-02-013 and modified
per NCDENR protocols. The test organism was Cei iodaphnia dubia and the dilution water was Hardness
Adjusted (45-50 mg/L) Surface Water. Test organisms were fed 2-5 hours prior to test initiation with
Pseudokirchneriella subcapitata and YAT. Each test dilution was comprised of ten replicates of 1 test
organism
Page 4 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015
Ceriodaphnia dubia
I Temperature:
25°C f 1
2.Light-
100 ft -cd; 16 hr It/8 hr dk
3 Test Chamber Size:
30 mL plastic cup
4.Test Solution Volume-
15 mL
5.Renewal•
Day 2 and day 5
6 Age of Test Organisms.
<24 hours
7.No of Neonates / Test Chamber
1
8.No. Replicates /Dilution
10
9 Feeding:
Daily
10 Cleaning of Test Chambers:
None
11.Aeration.
None
12 -Dilution Water
Hardness adjusted (45-50 mg/L) surface water
13 Effluent Concentrations:
0, 45, 60, 75, 90, 100%
14.Dilution Factor-
NA
15.Test Duration-
7 days
Page 4 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

5.0 RESULTS AND DISCUSSION
5.1 Review of Results
Measured Copper in untreated effluent <5 0 ug/L
Measured Zinc in untreated effluent. 51 0 ug/L
Toxicity test results for treated samples are summarized by treatment, as follows,
Mean Reproduction By Test Concentration
0% 45% 60% 75% 90% 100% IC25 Results
Untreated Effluent 21 8 169 19 1 194 21 8 226 >100% Sample not toxic
(Baseline Test)
5 mg/L EDTA 21 8 203 198 22 1 209 187 >100% Sample not toxic
Spiked Effluent
5.2 Baseline Test
There was no chronic toxicity found in the untreated effluent In as much as the sample was identified as
being chronically toxic in the March 2015 pass/fail chronic test, it seems likely that whatever toxicity
may have been present had degraded or volatilized Toxicity due to cationic metals, such as copper and
zinc, is persistent and would be expected to continue to be present in the sample after the holding period.
Thus, this is evidence that toxicity in the original test was not a result of elevated aqueous copper or zinc
5.3 diked 5 mg/L EDTA Test
No toxicity was present in the untreated sample, therefore the effect of EDTA could not be determined
5.4 Measured Metal Concentrations
Measured concentrations of copper and zinc were too low to be a potential cause of toxicity It would be
expected that copper concentrations would need to exceed 30 ug/L and zinc concentrations exceed 200
ug/L to result in chronic toxicity
Page 5 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

6.0 SUMMARY
• No toxicity was present in the untreated sample
• Test results indicate that toxicity did not result from copper and zinc There are two lines of
evidence for this conclusion;
1). Toxicity was not persistent Toxicity due to copper and/or zinc would be expected to be
persistent in as much as these metals do not degrade or volatilize
2) Measured concentrations of copper and zinc were too low to result in chronic toxicity to the
test organism Ceriodaphnia dubia
• The effectiveness of EDTA treatment for chelation of copper and zinc could not be determined
due to the absence of toxicity in the untreated sample.
Page 6 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility CITY OF HAVELOCK NPDES #
NC 0021253 PI e� 001 County Craven
Equal Var? yes Method
Laboratory Performing Test
ETT Environmental, Inc
Comments
4 5 6 7
8
# Youn
29
18
18
20
16
19
Baseline for EDTA Treatment
20
21
Signature of 0 R C
Signature of Lab Supervisor
Adult
Test e End Date Time
Info 0 04/22/15 12 50
Sample Information
Sampler Sample
Control
ewall Renewal2 tart Renewal
Renewal2
Collection Start Date
320/15
Treatment100% 100% Control Control
ffR
Control
Grab
(D)ead
L
pH Init83 82 81 81
80
L
Composite (Duration)
X
L
L
L
L
124%
L
L
pH Final85 86 82 81
80
L
Hardness(mg/L)
L
500
DOlnil 98 93 85 82 80
81
Spec Cond (umhos cm)
712
215
DO Final 76 79 76 80
Chlorine (mg/L)
<0 05
7a7q
Temp Init 243 247 245 243 247
24 7
Sample temp at Receipt
06
Temp Final 253 255 252 253 255
1 252
1 2 3
tonic Test
Results
9
10 Mean
Final Cont Mort %
0%
Effluent %
Organism #
% Cont 3rd Brood
80%
1
2 3 4 5 6 7 8
9 10 11 12 Mean Control Repro CV
26%
Control
# Younq
31
27
1325
% Red
26
14
18 1
22
1 21
1 21
1 none
none
21 8
48 Hour Mortality
00%1
(D)ead L L L
(L)ive
L
L
L 00%
1000% 10850
7500
(D)ead
L
L
L
L
L
L
L
L
L
L
none I
none
Effluent %
Control
IWC
21
24
0of10
0of10
1
2 3 4 5 6 7 8
9 10 11 12 Mean Significant?
No
h Red
(L)ive
100 0%
(D)ead L L L
Effluent %
# Youn
27
22
0
22
0
24
25
14
20
15
none none 16 9
Final Mortality Sign @
Environmental Sciences Branch
Adult
(L)ive
'Should use highest test concentration or
Division of Water Quality
IL
highest concentration with D O >5 0 mg/I
%Red
TO:
N C DENR
°
45 0 /o
L
L
L
L
L
L
L
L
L
none none 22 5%
% or
DWQ form AT -3 (8/91) Rev 11/95
Page 8
of 22
no concl.
Re roductlon Anal ses
1
2 3 4 5 6 7 8
9 10 Mean Repro LOEC=>100 00°/
Effluent %
60 0%
p o NOEL= 1000%
Method Steel's Test
Normal Dist? no Method Kolmogorov
Statistic 1141 Critical 1035
Equal Var? yes Method
Bartletts
1 2 3
4 5 6 7
8
# Youn
29
18
18
20
16
19
23
20
21
7
191
Adult
/Red
(L)rve
Method Steel's Test
(L)Ive
(D)ead
L
L
L
L
L
L
L
L
L
L
124%
p o NOEL= 1000%
Method Steel's Test
Normal Dist? no Method Kolmogorov
Statistic 1141 Critical 1035
Equal Var? yes Method
Bartletts
1 2 3
4 5 6 7
8
9AM�anStatistic
1406 Critical
1510
Effluent %
# Youn 25 20 0
22 16 22 25
24
22Non-Parametric
Anal sis If a licableAdult
Method Steel's Test
(L)Ive
5 0%
D ead
L
L
L
L
L
L
L
L
L
Effuent % Rank Sum
Critical
450% 9350
7500
1 2 3
4 5 6 7
8
9
10 Mean
600% 9000
7500
Effluent %
#Youn 24 21 19
23 281 22 26
17
211
17 21 8
750% 9800
7500
Adult
% Red
900% 10400
7500
(L)Ive
I
IL
00%1
(D)ead L L L
L L L
L
L
L 00%
1000% 10850
7500
verall Analysis IC25=
>100%
1 2 3
4 5 6 7
8
9
10 Mean
Result = PASS/FAIL or
Effluent %
#Youn 25 21 24
23 25 21 27
21
24
15 22 6
est LOEC >100 00% NOEL=
1000%
Adult
h Red
(L)ive
100 0%
(D)ead L L L
L L L L
L
L
L -37% lChronic Value=
>100%
MAIL
Environmental Sciences Branch
'Should use highest test concentration or
Division of Water Quality
highest concentration with D O >5 0 mg/I
TO:
N C DENR
t% Reduction from Control Reproduction Mean
1621 Mail Service Center
Raleigh, NC 27699-1621
DWQ form AT -3 (8/91) Rev 11/95
Page 8
of 22

Test Day
I'Source D 1 2 3 d S a
'
44986
Client]EFFLUENT
ITY OF HAVELOC
Sample ID
M3 4-9
----�-�_
County
M6 4-9
Start & fed Date
15 -Apr -15
Start & fed Time
08 4-3
Started & fed By
AM
Test Organism
Cenodaphnia dubia
Neo born date
14 -Apr -15
Neo born time
1700-2150
Test Type
NCCD
Dilution Water
NC H20 4-8-15
Units for Conc
44950 E
Test vessels
30 ml
Test volume
14950 F449501
©--�-�-�-®
1
Light
1 IU dk
Initial Temp °C
5
Selenastrum
F205ml
AT
1
,44950
PA 621 R 02 013 1002
W1f
Page 9 of 22
Lauif
44986
Client]EFFLUENT
ITY OF HAVELOC
Sample ID
NPDES#C
County
onth
Start & fed Date
15 -Apr -15
Start & fed Time
1150
Started & fed By
AM
Test Organism
Cenodaphnia dubia
Neo born date
14 -Apr -15
Neo born time
1700-2150
Test Type
NCCD
Dilution Water
NC H20 4-8-15
Units for Conc
%3rd BROOD
Test vessels
30 ml
Test volume
15 ml
Incubator #
1
Light
1 IU dk
Initial Temp °C
5
Selenastrum
F205ml
AT
1
0 05 ml
Test method
PA 621 R 02 013 1002
ommen s
44950 CON E,F,I J
CON TEMP
INITIAL- 243
DAY 2- 247
DAY 5- 24 7
DAY 2, NCH2O 4-15-15

APPENDIX B
EDTA Treated Effluent
AT -3 form and Bench Sheet
Page 10 of 22
Havelock: TIEIEDTA Investigation ETT; April 2015

Facility
Laboratory
Sampl
Collec
Comp(
Hart
Spec C
Chi
Sample
Control
Effluent %
45 0%
Effluent %
60 0%
Effluent %
75 0%
Effluent %
90 0%
Effluent %
100 0%
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
�-i l T yr mAVtLUUK Eu rA TREATED
NPDES # NC 0021253
Pt e# 001 County Craven
Performing Test
ETT Environmental,
Inc
Comments
41'
Treated w/ 5 mg/L of EDTA
)f O R C
Signature of Lab Supervisor
Test
-Tate Time ---[End Date Tlme
Info
04/15/15 1150 04/22/15 1213
e Information
Sample 1
Sample 2
Control
Start
Renewal 1 Renewal 2 tartVReRenewal2
tion Start Date
320/15
Treatment
100% 100% 100% CoControl
Control
Grab
pHlnit
81 83 82
78
)site (Duration)
X
pH Final
8s 8s 86
81
Iness (mg/L)
500
DO Init
86 81 81 85 83
81
)nd (umhoscm)
712
215
DO Final
78 80 73 80 77
Anne (mg/L)
<0 05
Temp Inst
00 247 246. 00 00
73
00
temp at Receipt
06
Temp Final
253 255 25 2 25 3 25 s
25 2
ronic Test
Results
Final Cont Mort %
0%
Organism #
% Cont 3rd Brood
80%
1
2 3
4
5
6 7
B
9 10
11
12 ..an Control Repro CV
26%
# Youn 31
27 13
25
26
14 18
22
21 21
none
none 21 8 48 Hour Mortality
(LEa
Dd L
L L
L
L
L L
L
L L
none
none Control
IWC
0Of10
10of10
1
2 3
4
5
6 7
8
9 10
11
12 Mean Significant?
No
# Young
23
20
17
23
24
21
ne
none 203
Final Mortality Sign
@
Adult
(L)ive
IL
%Red
L
L
L
L
L
L
L
L
L
none
none 6 9/
% or
no conc
Reproduction Anal ses
1
2 3
4
5
6 7
8
9jMean
Repro LOEC=>100 00% NOEL=
1000%
#Youn
24
19
22
27
5
23
25
20
15
Method Dunnetts t Test
Normal Dist? yes Method
Kotm °gorov
Adult
(L)ive
(D)ead
L
L
L
L
L
L
L
L
L
Statistic 0 939 Critical
1 035
Equal Var7 yes Method
Bartietts
1
2 3
4
5
6 7
8
9Statistic
080 Critical
1510
# You n
28
14
16
25
24
28
29
?6
16Non-Parametric
Anal sis if a IlcableAdultMethod
(L)iveD
Dunnetts t Test
ead
L
L
L
L
L
L
L
L
L
Effuent % Calc t
Critical
450% 057
228
1
2 3
4
5
6 7
8
9 10
Mean60
0% 076
750% -011
900% 034
228
228
228
# Young
24
22
14
22
11
25
261
241
211
20
209
Adult
(L)ive
IL
IL
IL
% Red
(D)ead
L
L
L
L
L
L
L
4 1%
100 o% 1 18
228
Overall Analysis IC25=
>100%
1
2 3
4
5
6 7
8
9 10
Mean
Result = PASS/FAIL or
# Young
27
17
5
13
25
17
23
19
20
2,r1871TestLOEC
>100 00% NOEL=
1000%
Adult
/o Red
(L)ive
IL
JChronic
(D)ead
L
L
L
L
L
L
L
L
L
142%
Value=
>100%
Environmental Sciences Branch
MAIL Division of Water Quality
NC DENR
TO: 1621 Mail Service Center
Raleigh, NC 27699-1621
*Should use highest test concentration or
highest concentration with D O >5 0 mg/I
t% Reduction from Control Reproduction Mean
Page 11 of 22 DWQ form AT -3 (8/91) Rev 11/95

Test Day
rc r n 1 1
Page 12 of 22
a
44986 EDTA
Client
ITY OF HAVELOC
Sample ID
FFLUENT
NPDES#
NC
County
onth
----©-�-
tart &fed Date
5 -Apr -15
Start 8 fed Time
D8 4-3
Started & fed By
M
est Organism
erlodaphnia dubia
F6 4
14 -Apr -15
Neo born time
1700.2150
est Type
CCD
"! n Water
C H20 4-6-1
Units for .one
4950 E
----©-�-
est vessels
0 ml
est volume
.. r F©----�-�-
ncubator#
1
Light
1611/8dk
... r 1144950
----�-�'
-
05 ml
AT
1
est method
2f
Ba 02a,3 coax
Emu
Page 12 of 22
a
44986 EDTA
Client
ITY OF HAVELOC
Sample ID
FFLUENT
NPDES#
NC
County
onth
tart &fed Date
5 -Apr -15
Start 8 fed Time
1150
Started & fed By
M
est Organism
erlodaphnia dubia
Neo born date
14 -Apr -15
Neo born time
1700.2150
est Type
CCD
"! n Water
C H20 4-6-1
Units for .one
/o3rd BROOD
est vessels
0 ml
est volume
15 mI
ncubator#
1
Light
1611/8dk
nitlal Temp °C
25
elenastrum
05 ml
AT
OS ml
est method
2f
Ba 02a,3 coax
44950 CON E,F,I,J
MPLE TREATED WITH EDTA
E SPEC PROJ BOOK
R DETAILS
Y 2, NCH2O 4-15-15

APPENDIX C
Chain of Custody
Page 13 of 22
Havelock: TIE/EDTA Investigation ETT; April 2015

ET'f
V 5,
PO Box 1,6414, Greenville, SC 29 6 06-741 4
[phone], (B00) 891-2325 Fax,[phone]
Shipping Address 4 Craftsman Ct, Greer, SC 29650
WWW MT CNYIFCNMENTAL.CCM
CILAIIN OF CUSTODY RECORD
Pate
Client:o // 6 �/'�
/C_
/
Program
Containers
Preservntive
Parameter
Facility:
/ �j^�
W
( . - 1j -
<
o
M hole LmucrcT=x
—
v
`,�a
State: J C , tiPb> S r: 1°S �'J ♦ 9 7 J
Acute
Ch -omit
Test Or�nntsms
U(Composite
only)
(Gran or Commslt_)
=
U
—
Sign, and Pi in t below
the dotted line
c
�
U
JW=
IDTime
COIlLctedby
Uv1:n
z
—
U
>
—
=Z
4
<
v
__SADrIPLE
U
^—
-
y
^
—
v
=
I c
Cnemr-e! nalysls �Otner
Yv)
. r171 � ( I'<%- "'
\�1r�
�
r
II
-------------
'
o
i7C "1; JP
rNv
---------
I
1
-------------
-------------------------
--- — — — — — — — — — — -
Special Instructions
Sample Custody Transfer Record
+SeCL:e
( Recelpt
SamDIC
Date Time Relinquished By /Organization, Received B) /Organization
kr�-a
Temp =C
Presen ear
330 i4nn'j [.z,' 1/ PP Awrl-r,"& OYL
x111/3 r a zl,4' l r o
ap
_
COd.IPOSITE S4AfPLING PROCEDURES TEMPER-1TURE jWONITORIArG PROCEDURES HOLD TfWE PRO C-EDUPj'S
Composite samples must be collected over a 2A bout pencd Sample tempetatire during collection and transport must be bet%%cel For to%icin rustipa the samole must n _i be wed u, 'fun 36 hours
Time Proportional. 1 sample each hour For 24 hours Equal volul 0 0 anc 6 0'C Sampleb -nust not be frozen Use %j ater Ice in sealed bas of samlilc collection (comalez,on of composite samore)
or at minimum 1 sample every 4 hours over 24 hours Sample may not be urea a ,er 72 hou—s from sa_-nole collection
Plow Proportional As per instructions In tiPDES permit

Rogers & Callcott
ENVIRONMENTAL
Client ETT Environmental
Bob Kelley
PO Boc 16414
Greenviile, SC 29606-7414
Dear Client
pPCCR60
Laboratory Report
PI o ject. Wastewater
Work Order. 5040627
Received- 04/15/2015 10 00
Rogers and Callcott appreciates the opportunity to be of service to you The attached laboratory services report includes analytical results and chain of
custody for samples that were received on April 15, 2015 Rogers and Callcott maintains a formal QA/QC program Unless otherwise noted, all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QAIQC confidence interval
for each test method unless otherwise qualified Estimated uncertainty is available upon request
Privileged/ Confidential information maybe contained in this report and is intended only for the use of the addressee If you are not the addressee, or the
person responsible for delivering to the person addressed you may not copy or deliver this message to anyone else If you receive this message by
mistake, please notify Rogers and Callcott immediately
We strive to prov tde a zeellent service to our clients Please contact Kara Hrkach, your Protect Manager, at kaia hrkach(a)rogersandeallcott com or
(864)-335-4956 if you have any questions about this report
Report Approved By
Kara Hrkach
Project Manager
PO Bok 5655 &ccnAle t( 19606 42.6 fanforctit viav "-,,—, vii),- SC ?96U7 nu ib' t3'r I .r, i w -i 1S- umu rogersandcall cott.com
7his report may not be reproduced except infill, irdhout ivntten pernnssion frons Ragers & Callcott, bic
Page 16 of 22
Page 1 of 7

. Rogers & Callcott
ENVIRONMENTAL
Certificate of Analysis
Client ETT Environmental
Bob Kelley
PO Box 16414
Greenville, SC 29606-7414
Sample Number Sample Description
5040627-01 44986
2L~'Q PCCpp���
r,
`1Q.01
South Cat ohna Gi eenwile Labor atony Identification 23105
South Cat olnm Columbia Labor atoi y Idenfcation 40572
NoitliCatohnaLabotatotyCeitificatioiiNumben 27
Not th Can ohna Di inking [FaterLab Number 45710
NEL4P Utah Cei trficate Number SC000042014-1
Georgia Di inking A%atet Lab ID 880
Project- Wastewater
Work Order: 5040627
Received: 04/15/2015 10 00
Matrix Sampled
Wastewater 03/20/15 10 30
T� pe
PO Bo. 5655 G eanvil,e SC 2QbC,(, 426 F,; i•„ est V iv G, cc,-.nllc ,C 2Q601 ?(h .3. I , .b Rt,•i ? ? i .,1 #0 roger-sandeallcott.eom
04!_t3Q015 13 36 77ns report mm• not be repioducer4 esceot tri, 49L;1ttlt7ipjfiggen pemtissron ftomRogeis & Callcott, lilt
Page 2 of 7

Rogers & Callcott
ENVIRONMENTAL
ETT Environmental
PO Box 16.114
Greenville, SC 29606-7414
Sample Data
Sample Number 5040627-01
Sample Description 44986 collected on 03/20/15 10 30
Project Wastewater
Work Order 5040627
Reported- 04/23/15 13 36
Parameter
Reporting
Result Limit Units
DF Analysed Method Flag Analyst Batch
Total Metals
Copper
ND 0 005 mg/l,
100 04/21/15 14 32 EPA 200 7 A4LR 135D0574
Zinc
0.051 0 010 mg/L
1 00 04/21/15 14 32 EPA 200 7 1`4LR B5D0574
PO Bo, 5655 G,eennll. U- 291,06 112E Fan`oi _5L W.,. Gie,_i wllc SC ?9607 ipr, 1164 2 i !_',n F364 "i 1,10 roger-sandeallcott eom
04/_r3!_r013 13 36 77us report may not be reproduced evicept in ANge'*8 m fvPgen pemussron G om Rogers & Callcott, Inc
Page 3 of 7

Rogers & Callcott
ENVIRONMENTAL
ETT Environmental Project Wastewater
PO Box 16414 Work Order 5040627
Greenville, SC 29606-7414 Repotted 04/23/15 13 36
Sample Preparation Data
Parameter Batch Sample ID
P Prepared Analyst
EPA 200.7 Metal Digestion
EPA 200 7 B5D0574 5040627-01 04/16/2015 08 08 MLR
a
PO Box 5655 Ot^ennlhs 5C 296C6 426 F7 I tOl; sc VVIV Ciecr�dlc SC 29D07 rogersandcalleott,eom
04123!-015 13 36 Tins repo! mm,not be reproduced accpl niPdgErgiglibfiggen permission from Rogers & Callcon, inc
Page 4 of 7

Rogers & Callcott
ENVIRONMENTAL
ETT Environmental Project Wastewater
PO Box 16414 Work Order 5040627
Greenville, SC 29606-7414 Reported 04/23/15 13 36
Data Qualifiers and Definitions
ND Analyte NO I DETECTED at or above the reporting limit
NR Not reported
PO go), 56$5 G•eonvdle SC 29666 426 Ft if,� _<_t W-i� G,eci ville SC X1)607 „ 46 � i IS'• t36r1 ?32 �I.10 rogersandcallcott.eom
air nIr,i✓•�
04232015 13 36 77rrs report mai not be reproducec( except mP4(gaift btrggen permssron from Rogers & Callcott, brc
Page 5 of 7

ETTCTTAIN OF CUSTODY RECORD
- ex�ironrrl�ent
PO Box 18414, GreenVitle, bC 29806.7414 Parc 1_ p f —L
[phone] [phone] Fax [phone]
Shrpping Address 4 Craftsman Ct, Greer, SC 29850
WWW CTTCNV'Q0NNCNTAL.00N
Ciient: 9 -7 -7 --
Facilit):
Program Containers
Prescnatn'c
Nranicters
State-. )\PDES 4:
Whole Crnacm iovcnt
Acute
Citron, Tcst Organisms
i
ICampos to ooh) tC--lb nr Cnmpesac}
O J
Sign, and Pi nit ocloxx
1250.
2- HCl.
=
cte coiled line
c
'a_ '-
SAMPLE ID p,rtTime Couectedu
VD °-
utermasnmpkemva,unn.re
e,
=
=7,qc
< <s=
Chemrca Anat/srsBCther
-------------
�L/
!
1930
zh
-------------
CD------------1
j
N
It
—
:tial Instructions
mple Custody Transfei Record
Date Time Relinquished By
N
111POS1TES4,11PLPJG PROCEDURES TE-11PERATURE d1O)WORING PROCEDURES
to nposite samples trust be collected oxer a 24 hour period S unplc temperature durinc collection and trampor, must be between
to e Proportional 1 sample each hour for : 4 hours Equal volm 0 0 and G 0 nC Samples must not be frezcn Use xxater ice in sealed bays
ot mmimurn I sample ever, <I hours over 24 hours
-4 x' Proportional As per Instructions in NPDES nmol
WIT
4ecirr Reccip I Samole
Orsanleattone
a Area Tcmn C Preserved,
FI,'OLD TI 111 PROC 5D _ RES --
or in".", testing the sample must first be used tx rhvn 36 hours
of sample collection (complei on of cnmpos,'e sample)
Sample may not be used after 72 1101175 from samp)e collectton

Rogers & Callcott
ENVIRONMENTAL
Sample Receipt Verification
Date i Work
Client: Received: - r I Order: L� I I✓ C� 1
CarnerName:Chent FedEx UPS
Tracking Number
US Mail Courier Field Services Other
Receipt Criteria
Y
e
HSP04
�
Comments
— — - - - -----
s,
o
A
Shipping container/ cooler intact?
Damaged I eaktng Other.
Custody seals intact9
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact9
Damaged Leaking Other -
Sample ID on COC agree with label on bottle(s)?
Date / time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottlesreceived'?
Samples received within holding time?
Sample volume sufficient for analysisO
VOA vials tree of headspace (<6mm bubble)'
Samples cooled' Temp at receipt recorded on COC
Tcmp measured with 1R thermometer • SN 97050067
Ice Cold Packs Dry lce None
Samples requiring pH preservation at proper pH'
Note Samples for metals analysts may be prescr�ed upon receipt in the lab
Samples dechlonmaled for parameterb requiring chlorine removal at
—
the time of sample collection?
If to -house preservation used — record Lot #
HCL
HSP04
H,,SO4
-
— — - - - -----
NaOH
HNO3
Other
Comments:
Were non-conformance issues noted at sample recei
Non -Conformance issue other than noted above.
Revned July 2014
Yes or I[No
Page 22 of 22
i
Completed by --_-_-
Page7 of 7

ETe,,,nnnT-b,r.1r
P.O, BOX It414. Greeny lie, SC 25606
[phone] FAX [phone]
4 Craftsman Cant, Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Plant
NPDES #: NCO021253
Test Date:
Laboratory ID#: T45892
Test Reviewed and Approved By:
A& 414
Robert W Kelley, PhD
QA/QC Officer
Certification #E87819
Test results presented to tits report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. ofHealth Included results pertain only to provided samples
Pat=e 1 of 6
13 -Oct -15
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Toxil
Facility City of Havelock
Lab ming
Signature of Operator In f
X
Signature of Laboratory S
rvlsor
Form - Chronic Mys
NPDES # N
Pipe# 01
: v nvtronmental Sciences Bran
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
Surviving C
5
5
4
3
4
4
4Q00
70
Original#
5
5
4
3
4
5Weight(per
58
41
Original)
Fecundity (gmvidltotal females)
0 00097
0 00115
0 00075
0 00057
254
0 00077
0 00121
256
011
12
012
010
1H
0/2
1r1
art
Treatment 2 Replicates
1
2
3
4
5
6
7
0
Survlwng #
3
5
5
5
5
Original #
4
5
5
5
5Weight
�-0014
(per Original)
Fecundity (gravidn.tal females)
000079
12
0 001100
1/3
00114
02
0 00110
113
00010
010
1A
112
0 00113
Oro
I Water Quality Data
Day
Control 0 1 2 3 4 5
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity initial
85
83
81
82
82
83
6
83
7
694
80
76
79
77
79
79
80
65
70
64
66
67
71
68
58
41
47
43
47
50
53
254
253
255
256
254
255
253
2581
2591
260
260
259
25 7
25 9
2491
251 1
2531
25.2
255 1
25.91
2511
Treatment 0 1 2 3 4 5 6
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
87
83
83
83
82
82
83
7
694
81
79
79
78
75
80
81
65
69
61
64
69
71
69
51
49
38
48
49
51
55
256
255
4
254
254
�025
26 0
250
25
25 7
25 9
26 5
251
251
25 1
Sampls 1 2 3
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/i.)
Sample Temp at Receipt
DWQ Form AT -4 (6199)
10/11/15 10/13/15 10/15115
24 hours
24 hours
24 hours
689
694
722
<0 05
006
<0 05
00
00
28
not frozen not frozen
23 -Oct -15
%Survival
Avg Weight (mg) 0 226 Avg Fecundity 35 7%
%Survival
Avg Weight (mg) 0222 Avg Fecundity 443%
Test Results
Significant Mortality?
Yes No
X
Check One
Growth
Col. t 0 159
Tabular 1 gq
Fecundity
Calc t NA'
Tabular 177
control fecundity less than 50%
PASS FAIL
X
Check Ono
Effluent Test Concentration 15%
5 replicates were set for each control lest replicate, where <5 are shown the organisms were lost during renewal
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during renewal
Page 2 of 6
Paee 2 of 6

V'M LoW'IT InM
In M In In Lo In In
m
N N N N N N N
m
o
C �
m
E c
E m
U e d (L
LuC
o
N
o U Z 0 0 0 0 0 0
m
H
L
m
O
a
H
Y
U
a
E
=
H
W
v1
J
m
w
F
o>
x
a y
E E
in
O co
N
a
E❑
in
U 2'o
O
a
Z U
o
Q
N
r
w
w
T
m
c=
o 'm'
E
E
0
a
n
o
�•
v a
?. .'.
w
E
m E
E
n 3
V
z
m E
?
9
p
r
o
J
m
41
Z
U
S[
N N
Orl
F Z
V'M LoW'IT InM
In M In In Lo In In
m
N N N N N N N
m
o
C �
m
E c
E m
U e d (L
LuC
o
N
o U Z 0 0 0 0 0 0
11111111111111
111111
111111111
I
oil
11
1111111
ollsommis
loss
possomis
0o00o00o
iMINE
ii
iiiiiiBRIOU
ii
loommom
1111111
111111
eee�eeee�eee�eeeeseee�eeeeeeeeeeee
eeeeeeell�ll�
�eeeeeeee

ETI-
M-��
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fa:c(854) 877 6938
Shipping Address 4 Craftsman Ct, Greer, SC 29650
W W W.riTTEN VIRONMENTAL.CCM
CHAIN Or- CUSTODY RECORD
Pace —j of-_
Client:
✓e OG
Program
Containers
Presen•ative
Parameters
Facility y
WeLllf Gia fe c - / rectf�e� f FQ
�
Whole L•filucntToxiciry
Q
State: a NPDES R: e
"?&a
acute
Chronic
I Test Organisms
M
o
U(Composite
only
(Grab or Composite)
<
—
5
o
L)
_.
Z
U
Sign, and Print below
r
>
y
o
_
-
cA
0
=
0
IgFL504
2=HCL
A
z
�
v
r^_
lite dotted line
.O
s'13-1-11,103-
—'
�_
_f
-
SAMPLE ID
V
Composite Start Date Thne
Sample Collection Dale Time
Collected by
U
cry
r�J
rn
O
Z
,
C
a
'
C7
O
>
rj
J=ZI.AC
6- other
J
<
<
U
U
CJ
Q
L
rn
=10
_
3
L
Chemical Analysis 8 Outer
^
y�G+ae:� I>GerYlc�eZ
HA
�}
1 . �a. d
rr�
�
'Iq
9.7
-------------
-------------------------Special
-------------
-------------
-------------
SpecialInstructions:
Sample Custody Transfer Record
Secure
Receipt I
Sample
Date Time Relinquished By/ Organization Received By / Organization
Area
Term) 'C
Preser% ed?
0: o.
1-f-00
/ iGIle- loe-d"
S
I
I
co -1 5
6,831,
UPs
Fn"
I
I o
I
I
I
COMPOSITE SAMPLIArG PROCEDURES I TEMPERATURE A10NITORING PROCEDURES HOLD TME PP,OCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing dhe sample must first be used within 36 hours
Time Proportional. I sample each hour for 24 hours Equal volui 0.0 and 6 0 'C Samples most not be frozen Use water ice in sealed bas of sample collection (completion of composite sample).
or at minimum I sample every 4 hours over 24 hours Sample may not be used after 72 hours from sample collection

ET jL I
h•�'+ax,�5t�r:�'=i'-"i-4'+J-17�JJ�_4��-C�ll�l'1h�'Li�
PO Bax 16414, Greenville, SC 29606-7414
(864) B77-6942, [phone] Fatc(864) 877 6938
Shipping Address- 4 Craftsman Ct, Greer, SC 29550
W W W.CTTEN V IRO NMENTAL COM
CHAIN Vre CUSTODY RECORD
CORD
Pa --e —I— of
c:ttent: -
Program
Containers
Preservative
Parameters
Facility: �� �� �' n w a
Whole [fttnentToriciq
State NPDES R: D
Acute
Chronic
Test Organisms
rn
i
"
a(Composite
only
(Grab or Composite)
u
=
c
_
o
U
0
Sign, and Print below
the dotted line
j
'
__
_
-0
U
'
1= HCL
3 Hno;
=
S------
Composite Start Date Time
Sample Collection Date Timer2
_
rn
Z
�
C
y
v
>
—
5-Zro1c
53
<
o�,?T=
UUChemicalAnal}51580
_SAMPLEID
6=Odor
ler
10-15115
WDoi�t�la
------------
IIIc
-------------
II
I
-------------
II
Ilii
V
II
IIII
Special Instructions
Sample Custody Transfer Record
Secure
Receipt
I
Sample
Date Time Relin uislied By/ Organization Received By / Organization
Area
Temp eC
Preserved9
d
t0 -IS
g3DtAfI5
LTi
D
COMPOSITE SAAIPLING PROCEDURES
TEMPERATURE AdONITORIArG PROCEDURES
HOLD TI.41E PP.00EDURES
Composite samples must be collected over a 24 hour period.
Sample temperature during collection and transport must be between
For toxicity testing the sample must firsi be used iilthin 36 hours
Time Proporhonal• 1 sample each hour for 24 hours. Equal voluu
0 0 and 6.0 eC Samples must not be frozen. Use nater ice in sealed bas.
of sample collection (completion of composite sample)
or at minimum 1 sample every 4 hours over 24 !tours
Sample may not be used after 72 hours from sample collection.
Flow Proportional- As per instructions In NPDES permit

ET".t"
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax[phone]
Shipping Address 4 Craftsman Ct, Greer, SC 29650
W W W.6TTENV 1 RONM ENTAL.COM
CHAIN OF CUSTODY RECORD
Pa --e e
Client:
'/ G
Program
Containers
Preservative
Parameters
Facility: We fete ,B t ��� f
3
U
y
_
;_
cn
L
�
z
y
o
U
o
a
U
_
>
—
1-1-1204
z=HCL
'-HN,03
4=idaoH
5= ZTLA
e=0d,cr
lithof°CmucntTaxieicp
Q
=
>
Chemical Analysis E Other
r•,
t
c
Z
s
_
State C NPDTS
Acute
Chronic
7°st Organisms
SAMPLE ID
u
U
v
(Composite only)
Composft° swrt Date Time
(Grab or Composite)
Sample Cali �,ao Date Time
Sian, and Print below
the dotted line
Collected by
a
<
U
—
U
J
r
—
U
_
U
;o
t]
'o
_
=
_
_
U
•.,
{�ivc.�r�-
1 • l , t
10. • 15tVA711,1
A��v
G
'
-------------
--------------------------------------Special
-------------
--------------
-------------
SpecialInstructions:
Sample Custody Transfer Record
Date Time Relinquished B / Organization Received By / Oreamzation
Secure
Area
Receipt
TemD °C
Sample
Presened')
I
2
I
COMPOSITE SAMPLING PROCEDURES TEMPER-ITURE HOAUTORIArG PROCEDURES HOLD TME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be betmcen For toxicit-, testing the sample must first be used vnthin 36 hour
Time Proportional: i sample each hour for 24 hours. Equal volui 0.0 and 6 0 °C Samples must not be frozen. Use water ice in sealed bas of sample collection (completion of composite sample)
or at minimum I sample even 4 hours over 24 hours Sample may not be used after 72 hours from sample collection_
Flow Pro ottiona er instructions in NPDES permit

ET--,,-n-Tent-,,c
P O. Box 1 E-414 Greenv Ile, SG Z3606
(664) B77-6942 FAX [phone]
4 Craftsman Court, Greta, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Plant
NPDES # NCO021253
Test Date:
Laboratory ID#: T46334
Test Reviewed and Approved By:
wok 4/4
Robert W Kelley, Ph D
QA/QC Officer
16'309'`!"`'M Certification #E87819
Test results presented to this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health Included results pertain only to provided samples
Page 1 of 6
12 -Jan -16
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certiftcahon # 022

Effluent Toxici
Facility City of Havelock
X -A -
Xlgnatu�e of Operator io,Rf1
� p
Signature of Laboratory SuDerviso
Form -Chronic Mysidopsis Pass/Fail
�y NPDES # NCO021253 Pi e#
yQOtinental Inc Comments
Date 21 -Jan -16
County Craven
: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
Surviving #
4
4
5
5
5
5
4
4
Onginal #
5
4
5
5
5
5
5
4
Weight (per Original)
000097
000115
1 000075
000057
000104
000077
000121
000115
Fecundity (gravid/total females
1/2
0/0
1/3
0/1
1/3
0/1
0/0
0/1
Treatment 2 Replicates
1
2
3
4
5
6
7
8
Surviving #
4
4
4
4
4
5
5
3
Onginal #
5
5
5
5
4
5
5
5
Weight (per Original)
000111
000089
000083
000075
000090
0.00093
000128
000073
Fecundity (gravid/total females
0/1
1/1
0/0
1/3
012
0/4
0/2
0/1
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
84
83
83
82
83
83
82
24 hours
24 hours
79
80
78
79
80
80
83
70
61
71
62
66
65
64
52
61
50
50
50
54
57
254
256
252.
253.
250.
254.
25 6
[E 2E24
257
261 1
2581
2,571
2581
261
259
25 3
257
2551
2491
2501
24 6
25 3
Treatment 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity initial
84
83
83
82
83
83
82
24 hours
24 hours
80
81
78
80
82
80
83
72
67
71
62
66
63
65
51
54
47
44
50
47
54
253
256
253,
250
252
256
[E 2E24
261
2581
2571
258
261
259
246
2,921
2671
263
257
Sample 1 2 3
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Temp at Receipt
1-10-16
1-12-16
1-14-16
24 hours
24 hours
24 hours
781
766
795
<0 05
1 <0 05
<0 05
1
1 00
24
partially
frozen
%Survival
Avg Weight (mg) 0 205 Avg Fecundity 27 3%
%Survival 84 6
Avg Weight (mg) 0 191 Avg Fecundity 14 3%
Test Results
Significant Mortality?
Yes No
X
Check One
Growth
Calc t 051
Tabular 1 1 94
Fecundity
Rank Sum
Crit Value
PASS FAIL
X
Check One
Test Date 01/12/16
Effluent TestConrznfration 15% 'Control fecundity <50%, not used as endpoint
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during renewal
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during renewal
Page 2 of 6

W
0
W
00 '0
DDDDDD
M T-r,w N-•D�3 _
M.
a
O 'u
O Q
O m
m
N N N N N N
CA CA N Cr CA C11 (A
CA.[a CAw NCAA
i-
saloons1111
m
C;
a
m
3
>
O
O O
cn
0
cu
0a
3=
p
N
z
C)
m=
T D
a
C
3 3
z
O
D
o
<
c m
O
a
T
D{
O
b
O
=
3
Z
-I x
D
in
z
rn
�
m
i����������n��ee�eeeeeseeeeeeee�
�
..
NiiNE�
��n����e�e-eeeeee�eeeee�
_e1eeeeeeeeeeeee
11111111
11111111111111111111
���A���1
�����A�A�
I�III
III
III
III
.IIII�IIIIIIIIIIII
=III'
�llllll
1:
1111111111
1
INS-sssss
-1111111
ssss�sl�
a
�sissssssss'��snsssn�sssss�sn�"�"sss's'sssss��
00 '0
DDDDDD
M T-r,w N-•D�3 _
M.
a
O 'u
O Q
O m
m
N N N N N N
CA CA N Cr CA C11 (A
CA.[a CAw NCAA
i-
m
C;
a
m
3
>
O
O O
cn
0
cu
0a
3=
p
N
z
C)
m=
T D
a
C
3 3
z
O
D
o
<
c m
O
a
T
D{
O
b
O
=
3
Z
-I x
D
in
z
rn
�
m

ET'jL'
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address* 4 Craftsman Ct, Greer, SC 29650
WWW.CTTENVIRDNMENTAL COM
CHAIN uF CUSTODY RECORD
Pace _L 0,
Client:
�C k
Program
Containers
Preservative
Parameters
Facility: /. le L
�l/ 7 l re- 76i.,eYJTe,,/-Whole
7
c
Un
v
_
�Tme
c
o
-
M-0^
Z
J
E2
�;'
U
`—'
c>
ti
=
1-H2SO4
2-14CL
3-1-NO3
6 p c
MountTocieit3
c
n
'
L
c
ChemOther
'
Z
_
/
State: C NPD );S r": 1 00,242-5-3
Acute
Chronic
Test Organisms
ID
U
U
(Composite only)
Composite Start Date Time
(Grab or Composite)
Sample Collection Date
Sign, and Print below
the dotted line
Collected by
=
-.52
<
<
U
v
o
a
_
Ln
_
U
Tom=
al
M14cO//ein—A
I
,fit T, A :, e o F
------------
---------------------------------------------
-----------
-------------
-------------
Special
Special Instructions:
Sample Custody Transfer Record
Time me Relin uished By/ Organization Received By / Organization
Securz
Area
I Recenpt
Tzmo'C
Sample
Preser ed7
geNs
a--. T� � oc
., 4
I -o2-16
093J
1. Z
611
COMPOSITE SAMPLING PROCEDURES TEA?PERdTURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 (tour perSample temperature during collection and transport must be between For toxicnt) testing the sample must first be used v iihin 36 hours
Time Proportional I sample each hour for 24 hours Equal volun 0.0 and 6 0 °C Samples must not be frozen Use water ice in sealed bas of sample collection (completion of composite sample)
or at minimum 1 sample every 4 (tours over 24 (tours. Sample may not be used after 72 hours from sample collection

.Elm"IL'
jj:::::::::111 ;; 71
1T2 1 't �
PO Boxn10414, Greenville, SC 29506-7414
[phone], [phone] Faic(864) 877 6938
Shipping Address 4 Craftsman Ct, Greer, SC 29650
W W W.ETTENVIAl7NMENTAL.00M
CHAIN k,-, CUSTODY RECORD
Page —1— of
k.tient: C %
Facility: 1 l�'
G
=
G
U
Program
v
o
cit
cq
=
•-
z
�in
Containers
GL
=
(j
c
j
Preservative
u
1-H2S0J
�- HCL
1=\SOH
s=ZnAc
6= Odicr
Parameters
Whole Cmuent Toxicity
,�
2
21s
o
2
Chemical Analvsis ✓i Other
'-
Ci
n
<
_
State: NPDES R:
Acute
Chronic
Test Organisms
SAMPLE ID
=
a
U
s
U
O
(Composite only)
Composite Stain Date Time
(Crab or Composite)
sample Collection Date TimeCorrected
Sion' and Print below
Ute dotted line
by _
m
v
'+
U
-a
v
<
`y—^
U
-
U
ca
a
=
?
I L�-
L
>
✓i
oH
=
m
U
`
_
1I2
II
-------------
-------------------------Special
-------------
SpecialInstructions -
Sample Custody Transfer Record
Date TlmeRelin uished 1300reanization Received Bvl Organization
Secure
Area
Receipt
TemD 'C
Sample
Preserved?
t t'D
Y
t- iy-1
D
11
bGp
>✓-rr
Pa
Hi 0j
COMPOSITE SAMPLING PROCEDURES TEMPER<1TURE A10MITORING PROCEDURES HOLD TIME PROCEDURE'S
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional. 1 sample each ]tour for 24 hours Equal volui 0 0 and 6 0 'C Samples must not be frozen Use water ice in sealed bas of sample collection (completion of composite sample)
or at minimum 1 sample every 4 (tours over 24 hours. Sample may not be used after i2 (tours from sample collection
Plow Proportional As per instructions in NPDES Demtit

CILMN U- F CUSTODY RECORD
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax -[phone]
Shipping Address- 4 CraRsman Ct, Greer, SC 29550
W WW.I=rMN V IRONMWi,MA4Co M
Pave of
l:ltent:
A!/
Facility:( 1��600 / q fef s.�er7f ��-�t
3
c_
U
Program
rq
B
cn
o
a
o
z
o
U
o
�
Containers
s
^_
y
iJ
E
o
>
Presen-amble
—
I= HCL
--tn.o�
4=Na014
6- Od,Q
Parameters
iq
Whole timuentToOrg
N
o
Chemical Analysis a Other
�
i
J
State C NPD)rs #: c �a�as3
Acutc
Chhronic
Test Organisms
SAMPLE ID
U(Composite
U
only)
Camposrtc $tart Datc Time
(Grab or Composite)<
Sampic Collmmn Dntc Time
Sten, and Print below
rite dotted line
Collected by
^
¢
¢
y
U
=
U
_
U
U
y'
n
`
fF%est
/� /�
//Q0.
/(
�-
- -- r ---
j
✓
S t�-�G
`�ie33 �E C
1
- - - - - - - - - - - - -
l
-------------
-------------
Special Instructions.
Sample Custody Transfer Record
Date Time Relinquished B / Omanization Received By / Organization
Secure
:area
Receipt
TemiD 'C
Sample
Presermd?
1, 4
Ft>uQ G3 vet b (7�,,
11L rC,
C1��1
_;r
i
y .
CUA4PUS7iC SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES
Composite samples must be collected over a 24 hour period. during temperature dung collection and transport must be between
Time Proportional: I sample each hour for 24 hottrs Equal volut 0.0 and 6 0 'C. Samples must not be frozen rise.water tee in sealed bas
or at minimum I sample every 4 hours over 24 hours
,er
HOLD 713 PROCEDURES
For toxicity testing the sample must first be used writhin 36 hours
of sample collection (completion of composite sample)
Sample may not be used after 72 hours from sample collection

emlmrlm�li , Inc
P 0, Sfax I E414, GreeflV Ile, SC 29606
[phone] FAX [phone]
4 Craftman Court, Grier, SC 29550
Americamysis lbahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CI'T'Y OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES # NCO021253
Test Date:
Laboratory ID#: T46884
Test Reviewed and Approved By.
Robert W Kelley, PhD
QA/QC Officer
Certification #E87819
Test results presented to this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health Included results pertain only to provided samples
Page 1 of 6
19 -Apr -16
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Toxicity Report Form - Chronic R
Facility City of Havelock WWTP NPDES #
X /fid y G��e
r—
Slgnature of Opera
X
Signature of Laboratory S
s Pass/Fail
Date 29 -Aar -16
County Craven
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
Surviving #
5
5
4
4
5
4
4
5
Original #
5
5
4
5
5
4
5
5
Weight (per Original)
000156
000179
000135
000149
0 00202
0 00151
000172
000183
Fecundity (gravid/total females
1/1
0/2
0/1
2/2
1/2
1/3
0/0
2/2
Treatment 2 Replicates
1
2
3
4
5
6
7
8
Surviving #
5
5
4
5
5
5
5
5
Original #
5
5
--T
j
5
5
5
5
5
5
Weight (per Original)
0 00219
CO215
0 00181
000225
000228
000182
000162
000205
Fecundity (gravid/total females;
3/3
1/2
1/1
1/1
1/1
0/0
1/3
2/2
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Inifial
81
80
83
80
81
80
83
x
x
78
77
76
76
77
78
77
75
67
64
66
74
73
67
57
45
53
50
52
50
54
252
253,
254,
251 1
253.
253,
253
2581
2601
2-5-7
25 6
260
260,
260
24 5
247
2491
2491
251 1
2501
2461
Treatment 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity initial
Sample
Collection Start Dale
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Temp at Receipt
DWO Form ATA (6/99)
82
80
83
80
81
82
83
x
x
79
79
79
79
76
79
79
74
66
64
67
75
71
65
54
41
55
49
53
40
47
250
253,
255.
252.
253
254
256.
25 B
26 0
25 7
25 8
26 0
26 0
26 0
24 4
2451
2501
2501
2461
2481
247
17 -Apr -16
19 -Apr -16
21 -Apr -16
x
x
x
738
758
777
006
<0 05
<0 05
01
02
09
%Survival 94 7
Avg Weight (mg) 1 66 Avg Fecundity 53 8%
%Surnval
Avg Weight (mg) 2 02 Avg Fecundity 76 9%
Test Results
Significant Mortality?
Yes No
X
Check One
Growth
Calc t -2601
Tabular 1 1 94
Fecundity
Rank Sum
Cnt Value
PASS FAIL
X
Check One
Test Date 02/09/16
Effluent Test Concentration 3%
5 replicates were set for each control lest replicate, where <5 are shown the organisms were lost during renewal
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during renewal
Page 2 of 6

III
IIS
1i-11ITI
I�
�
iIi
fli
Hill
L�
i'
Ll
hili

ET"x"
a 2
PO Box 16414, Greenville, SC 29506-7414
[phone], [phone] Fax[phone]
Shipping Address- 4 Craftsman Ct, Greer, SC 29650
WW W.=EN V n70NMENTAL.COM
CHAIN u- F CUSTODY RECORD
Page —4-- of 4—
Client:
Program
Containers
Preservative
Parameters
Facility: / I� l �� ler � L/111,
e 17
WholeEmucntToxicity
n
State: NPDES 2
Acute
Chronic I
Test Organisms
U
(Composite only)
(Grab or Composite)
Z5
<
o
12
U o
—
Stan, and Print below
.UJ
3
-
•3-HNO3
x
o
I=H?SO4
2mHCt
=
=
_
=
N'
<
die dotted line
__
^c
U
N
y
a=NaoH
SAMPLE ID
6—
Composite Start Date Time
Sample Collection Date Time
Collected by
U
J5
V'3Z
—_
c-
c7
>
—
a= other
<
<
v
U
U
❑
t=
Z I
r;5
=101"P:*121
Chemical Analysis 8 Other
1
11,
a'
OfI
I I
I
I
Iq o
q $3 'q A
-------------
-------------
-------------
-------------
Special Instructions
Sample Custody Transfer Record
Secure
Receipt
I
I Sample
o
Date Time Relinquished By/ Organization Received By / Or_amzation
Area
Temp eC
Preserved
/�16
/00-5
- IzIalr�
I
I
I
I
COMPOSITE SAMPLING PROCEDURES
TEt1,fPER_,1TURE IWOMTORING PROCEDURES
FOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period
Sample temperature during collection and transport must be bemeen
For toxicity testing die sample must first be used iNithin 36 hours
Time Proportional 1 sample each hour for 24 hours Equal volui
0.0 and 6 0 °C Samples must not be frozen Use hater ice In sealed bas
of sample collection (completion of composite sample)
or at minimum 1 sample every 4 hours over 24 hours
Sample may not be used after 72 hours from sample collection
Flow Proportiom ler instructions in NPDES permit.

M; `
PO Box 16414, Greenville, SC 29606-7414
(B64) 877-6942, [phone] Fa:c(864) 877 6938
Shipping Address. 4 Craftsman Ct, Greer, SC 29650
W W W.CTTENV1GCNMENTAL.00M
CHAIN VF CUSTODY RECORD
Page of 7E7-1
Client:
Program
Containers
Preservative
Parameters
Facility:e� -77e
me,-'1
11'holaCmucatToxicity
State: 1\`PDl $ ri'r:
Acura
Chronic
Test Organisms
ts
—
0
^
(Composite only)
(Grab or Composite)
<
�_
_
=
i
o
—
z
U
Sign, and Print below
Ej
>
aES
ca
oo
a- HCL
_
N
21
V
tOCompositesmn
the dotted line
E
o
3-HNO3
4-NaOH
U
uU
_—
ID
Date Time
Collection Dale Time
Collected by
,
>
i= Z:�c
¢Smple
^
jo
_
CSAMPLE hemical Analysis & Other
—
a/e��o,7
la8l�'g
-
-------------
c
-foil
r----------
0
D-----------
-------------
Special Instructions
Sample Custody Transfer Record
Secure
I.Axea
I Receipt
( Sample
Date Time Relinquished B1 y / Organization Received By / Organization
Temp 'C
Preserved9
CTT"
I
I
I
I
COAfPOSITE SAMPLING PROCEDURES TEMPERATURE iWONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For toxicity testing die sample must fist be used «ithtn 36 hours
Time Proportional 1 sample each hour for 24 hours Equal volui 0.0 and 6 0 eC Samples must not be frozen Use water ice in sealed bas of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection
Flow proportional- As per instructions in NPDES permit

ET r o
MINOR
PO Box 16414, Greemnlle, SC 29605-7414
[phone], [phone] Far(864) 877 6938
Shipping Address- 4 Craftsman Ct, Greer, SC 29650
WWW-(C7TENVtRONMEN AL.COM
CHCA.E�I U- f CUSTODY RECORD
Page _Zof—j
Client:
Program
Containers
Presemntire
Parameters
Facility: // 1 1,�
Te (It 16P-1 7f �mC>� �iil
Whole LmucntTaxicth
State: C NPDES m: Q" �2
Acute
Chronic
Test Organis ns
o
U
(Composite only)
(Grab or Composite)
c
U
H
y
_o
—
Z
r
Sign, and Pont below
_
=
ca
=
2 -HCL
L
>
s
the dotted line
❑
_
o
ti
=
aOH
—
SAMPLE ID
tj
Composite Start Date Time
Sample Collecooa Date Time
Collected by
U
o
rn
✓]
o
Z
a
CL
U
o
—
SsZaAe
6=Oilier
ii
^
U
U
U
p
=
[-
2
vi
5,
—
s
U
U
—
>
Chemical Analysts o Other
—
cif CG//�c�t��l
-------------
----
-------------
-------------
-------------t
-------------
-------------
I
Li
II
Special Instructions
Sample Custody Transfer Record
Secure
Receipt
Sample
Date Time Reh ished By I Oraamzatton Received By I Organization
Area
Temp eC
Presen ed9
ra- -v
r g0—bq'
It 2 .
Ogg)
P5
617-
I o.
CO>VIPOSITE SAMPLING PROCEDURES TEAl, PERaTURE il<IONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be bemcen For toaiciq testing die sample must first be used ivithin 36 hour
Time Proportional. I sample each Hour for 24 hours Equal volui 0 0 and 6 0 eC Samples must not be frozen Use water ice in sealed bas of sample collection (completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection

ETen,,-,etital, IRC
P.O. Box 10414, Greenville. SC 29605
(964) B77-6042 FAX [phone]
4 Craftsman Court, Greer, 5C 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES # NCO021253
Test Date:
Laboratory ID#: T47373
Test Reviewed and Approved By.
Robert W Kelley, PhD
QA/QC Officer
•rr==►" Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health Included results pertain only to provided samples
Page 1 of 6
19 -Jul -16
Farhad Rostampour
Laboratory Director
SCDHEC Certification 423104
NCDENR Certification # 022

trnuent ( oxicity Report Form - Chronic M sido sis Pass/Fail Date 28 -Jul -16
Facility City of Havelock WWTP NPDES # PI e# County Craven
Laborato 31,Comments
x d f�
le
Signature of Operator in Re pons) Cbe
x ,-,
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Rrarlch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
Surviving #
5
4
3
5
5
3
5
3
%Survival 97 1
Original #
5
4
3
5
5
3
5
4
52
Weight (per Original)
—0342
0 473
1 0 393
0 442
0 398
0 373
0 222
0 148
Avg Weight (mg) 0 349 Avg Fecundity 75 0%
Fecundity (gravid/total females
12
22
1/1
2/2
1/2
1/1
12
1/2
Treatment 2 Replicates
1
2
3
4
5
6
7
8
Surviving #
4
4
3
4
4
5
3
1
%Survival
Original #
4
5
4
5
5
5
4
2
52
Weight (per Original)
0 255
0 272
1 0 238
0 370
0 334
OA48
0 318
0 230
Avg Weight (mg) 0 308 Avg Fecundity 90 6%
Fecundity (gravid/total females
1/1
1/1
2/3
1/1
2/3
22
0/0
1/1
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Inibal
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
80
81
8Z
82
82
83
a3
x
x
79
83
78
81
79
79
82
74
68
66
65
66
73
77
53
54
47
52
51
57
55
254
256
253
257
254
255
257
2611
25 9 1
25 9
2601
261 1
2591
25 9
2551
2571
2601
2651
2641
2661
2701
0 1 2 3 4 5 6 7
80
82
82
82
82
82
83
x
x
80
79
79
80
81
81
82
75
67
67
67
66
73
77
56
44
47
52
52
57
62
250
257
253
257
264
265
255
261
2691
2591
2601
261 1
59
259j-
259
2571
2,561
2631
2631
2461
255
211
Sample 1 2 3
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mgti-)
Sample Temp at Receipt
DWO Form ATA (6/99)
17 -Jul -16
19 -Jul -16
21 -Jul -16
x
x
x
723
733
660
4005
<0 05
<0 05
02
1 02
03
Test Results
Significant Mortality?
Yes No
x
Check One
Growth
Calc t 0 86
Tabulart 194
Fecundity
Rank Sum 66
Cnt Value 51
PASS FAIL
x
Check One
Test Date 07/19/16
Effluent Test Corcentration 15%
5 replicates were set for each control lest replicate, where <5 are shown the organisms were lost during renewal
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during renewal
Page 2 of 6

I
Mffl
I
11TH
V
I
llllll
I
1
H
i
T
-T
I I
I
I
I
ill
i

E r.
T �t
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax[phone]
Shipping Address 4 Craftsman Ct, Greer, SC 29550
-W -I rC—IRCNMCN Al CO.
CHAIN OF CUSTODY RECORD
Page of
Client:
OCit
Program
Contnmers
Presen-etive
Parameters
Facility: ^CC'Z' �
rvnele cmaent Toxictq
�
—
i
State: IYPDLS m: �0 ��
Acute
Chronic
Tett Orgnnisms
U
(Composite only)
(G2b or Composite)
< p
v
c
Lj
i
o
M.
i?
Sian, and Print below
a
3
y
-
_
o
?m HCL
=
z
file dotted Iine
=
E
c
U
o
H
E
-Hi.oa
--
—_
r
_
ce
SAMPLE ID
ComPM'testan Date Time
sampleCa1l.O=Date Time
Collected bi
U
ti
rn
Z
-
U
>
—
6.Od-
4
4
U
J
U
z
n
—
U
c
2
Chemical Analysis & Other
6/7373,1
-------------
-------------
LiLl
Special Instructions:
Sample Custody Transfer Record
Secure
I Receipt
I Sample
Date Time lin uished By/ Or;amzation Received BY / Organization
.Area
Temp eC
Presen ed'
l
03 3 S
D.
COMPOSITE SAMPLING PROCEDURES TEMPERATURE 411ONITORIA'G PROCEDURES HOLD TWE PROCEDURES
Composite samples must be collected over a 24 hour period_ Sample temperature during collection and transport must be bemcen For to-,icity testing the sample must first be used c%ithin 36 hour.
Time Proportional 1 sample each hour for 24 hours Equal volu 0 0 and 6 0 aC Samples must not be frozen Use hater ice in sealed bas of sample collection (completion of composite sample)
or at minimum 1 sample every 4 (tours over 24 Hour Sample ma) not be used after 72 hours from sample collection
Flow Proportional. As per instructions in NPDES permit

ET c W
.1
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address, 4 Craftsman Ct, Greer, SC 29650
WWW CTTCNVIRn NH 6NTAl.COM
CHAIN vF CUSTODY IAC®RD
Page 7- of
Client:
Program
Containers
Preservative
Parameters
Facility:/,g
Whole Muentroxidn
2
�
State: 6 NPDES n: Cly©O /0-53
Acute
Chronic I
Test Organisms
p
e
(Composite only)
(Grab or Composite)
G
o
V
Sign, and Print below
j
yCIDo
a -HCI
-
v
the dotted line
=
F
U
°
y
B
a- ox
°
tj
—
*,m
SAMPLE ID
U
compositasiart Ome Time
Samplc Calleo— Dale
Time
Collected b1
d
U
o
rn
o
Z
o
13
U
o
>
—
5=ZaAc
6= 0�
o
<
o
<
U
U
U
L
2
r
_
U
i
L
Chemical Analysis 8 Other
—
•� U e��
7/9jJ�
1
0
JCS
o
i
,r`UA
✓
I-------------
I
------------
I
n-------------
-------------
-------------
-------------
Special Instructions
Sample Custody Transfer Record
(Secure
I Receipt
I Sample
Date Time Relinquished By I Organization
Received By I Organization
Area
Temo'C
Preser\ed2
CN a i JL -
010
S
Ir
(o.
COMPOSITE SAMPLING PROCEDURES
TEMPERATURE MONITORING PROCEDURES
HOLD TIME PROCEDURES
Composite samples must be collected over a 24 (tour period
Sample temperature during collection and transport must be beth+gen
For toxicity testing the sample must first be used within 36 hour.
Time Proportional 1 sample each hour for 24 hours Equal volui
0 0 and 6 0 aC Samples must not be frozen Use water ice in sealed
bas
of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours
Sample may not be used after 72 hours from sample collection
Flow Proportional- As per instructions in NIPDES permit

CD
0
ETT
PO Box 16414, Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address 4 Craftsman Ct, Greer, SC 29650
WWW-CTMNVIRCNMENTA QOM
CHAIN OF CUSTODY RECORD
Client:
�"
Program
Containers
Preservative
Parameters
Facility: �Jh5 &- 6e r l eoih ���1
Cf,zf
Whole Cmaent roximn•
n
State: /Pr, NPDES
Acute
Chronic
Test Organisms
o
Ra
U(Composite
only)
(Grab or Composite)
U
<
o
12
L
C
U
-
a
—
n
—_
J
and Pi int below
9i
o
I=i -Sod
CLSign,
_
=n2m
r-
n
ID
t?
the dotted line
g
cSAMPLE
--HNO3
aaNaoH
5s Znac
�
Uc
°
�N
-
composite Start Date lime
smple Cotlecuon Date Time
Collected by
U
i
rn
z
6 -other
<
<u
J
_
U
r
2
Chemical Analysis 8 Other
-------------
-------------
-------------
J
-------- ----
IL
LE
I I
Special Instructions
Sample Custody Transfer Record
Secure
I Receipt I
Sample
a
Time me_ -Relinquished By 1 Organization Received By 1 Oraanization
?sea
Tem 'C
Preserved'
1105 1 J
Z� f.
o i s
I
0, 3
COMPOSITE.S14AIPLING PROCEDURES TVIPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For tomcm testing the sample must firsbe used nithin 36 hour.
Time Proportional l sample each hour for 24 )tours Equal volui 0.0 and 6 0'C Samples must not be frozen Use water ice in scaled bags of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours Sample ma}• not be used after 72 hour from sample collection
Flow Proportional As per instructions in NPDES permit.

ET,-..,,Tm,b,=
P.O. Box 1 E414, Gfeenv ile, SC 29606
[phone] FAX [phone]
4 Craftsman Carrs, Greer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES # NCO021253
Test Date:
Laboratory ID#: T47853
Test Reviewed and Approved By
4/4
Robert W Kelley, Ph D
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Flonda Dept of Health Included results pertain only to provided samples
Page 1 of 6
11 -Oct -16
Farhad Rostampour
Laboratory Director
SCDHEC Certtfrcatron #23104
NCDENR Certification # 022

Ffflunnt Tnvirifir 0---.4 C......
. ca—'. au Date 11 -Oct -16
Facility CITY OF HAVELOCK NPDES # NCO021253 PI e# 001 County—
ount Craven
Laboratory Pe . Comments
X
Signature of Operator In Respo>�le,arge
Xls — �' "
Signature of LaboratorySupervisor
MATT nDTL'WA1i grd-1
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
7.7
Surviving #
4
4
5
5
5
5
4
5
%Survival 100 0%
Original #
4
4
5
5
5
�; 5
4
5
69
Weight (per Original)
05200
04775
0 3880
04940
0 3980
0 3820
0 5550
04420
Avg Weight (mg) 0 457 Avg Fecundity 865%
Fecundity(gravid/total females)
1/2
212
1/1
2/2
3/4
2/3
2/2
3/3
256
Treatment 2 Replicates
1
2
3
4
5
6
7
8
7.7
Surviving#
4
5
5
5
3
5
4
4
%Survival
Original #
4
5
5
5
4
5
5
4
69
Weight (per Original)
04325
03740
03500
03580
05350
05520
03320
04725
Avg Weight (mg) 0 426 Avg Fecundity 750%
Fecundity (graAdllotal females)
1/ 1
2/2
1/2
1/ 1
2/2
2/2
0/1
1/2
256
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initiai
83
80
82
82
82
81
83
24 hr
24 hr
7.7
79
79
78
77
78
82
74
66
67
63
65
70
67
54
61
50
53
69
45
60
252
25 3
256
1 254
252
251
1 249
263
260
261
259
26 3
260
263
251
256
247
249
25 6
247
248
Treatment 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Tamp Inlhal
Temp Final
Salinity Initial
Semple
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg1L)
Sample Temp at Receipt
DWQ Form AT -4 (6199)
83
81
82
83
82
83
83
24 hr
24 hr
78
79
79
80
82
80
82
75
75
62
61
62
65
62
55
50
46
51
67
49
61
250
1 254
256
1 257
256
1 253
1 257
26 3
260
261
259
26 3
26 0
263
248
1 26 3
255
257
248
249
1 250
09 -Oct -16
11 -Oct -16
13 -OG -16
082
Tabular t
1 76
24 hr
24 hr
24 hr
405
445
445
<0 05
<0 05
<0 05
02 1
02
22
Test Da e
Effluent Test Concentration
I Test Results I
Significant Mortality?
Yes No
x
Check One
PLASS FAIL
I -
Check One
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during re
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during
Page 2 of 6
Growth
Calc t
082
Tabular t
1 76
Fecundity
Calc t
0 36
Tabular t
1 76
PLASS FAIL
I -
Check One
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during re
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during
Page 2 of 6

ET"jL'
PO Box 16414, Greenville, SC 29505-7414
[phone], [phone] Fax[phone]
Slupping Address- 4 Craftsman Ct, Greer, SC 29650
W�-Vit rrMVIg0NMC YAL.COM
CHAIN OF CUSTODY RECORD
Page --`of 77
Client: C i I
Facility: ' )
<
v
s
^
U
Program
v
�c
O
rn
n
=
w
C
O
z
o
-55
=
0
O
a
Containers
O
a
a
U
52
=
O
>
Preservative
I -lis 04
2 -HCL
3=ZnAc
b. p
Parameters
Whole Lmocntroxlan•
3
^
_
o
Z
Chemical Analysis & Other
C�
_
State: L NPDLS�:
Acute
Chronic
Test Organisms
SAMPLE ID
oU
U
e
U
(Composite only)
CompntlleStnn pato Time
(Grab or Compose)
Sample Coucct on pme Tima
Sign, and Print below
file dotted line
Collected by
=_
c
4
iJ_=
2
¢
0
_
U
J
_
U
-
=
U
CI
_
t
✓;
—
2
_
s
—
--
p
=—
U
C
-
dlacoo6.'wio
o'yr
l
a
J
"�
1/
Iv,
I
I
l�Caiiec `c
-------------
-------------
-------------
IT
-------------
-1
I
L
HT
Special Instructions -- I .
Sample Custody Transfer Record
Date Time Relinquished -By /Organization Received By/ Organization
Secure
Area
Receipt
Temp'C I
Sample
Preserved?
IN
10-A ga2 Yl u)OT-p
D I
PS
err-
O
0 U
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period
Time Proportional I sample each (tour for 24 hours Equal volui
or at minimum I sample every 4 hours over 24 hours
I'low Proportional As per instructions in NPDES permit
TEWERATURE AI0A7TORING PROCEDURES
Sample temperature during collection and transport must be between
0 0 and 6 0'C Samples must not be frozen Use water ice in sealed bas
HOLD TIDE PR0CED CtRES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample)
Sample may not be used after 72 hour from sample collection

PO Box 16414, Greenville. SC 29608-7414
[phone], [phone] Fa:c(864) 877 6938
Shipping Address 4 Craftsman Ct. Greer, SC 29850
W W W.ETTCN V IGONH CNTAL.COM
CHAIN uF CUSTODY RECORD
Page Or
Client: '"�
j `
Program
Containers
Preservative
Parameters
Facility: Ips �� j,Z y i !�G
a
c
1 T
\1'huleLmucntrnxicih
State: Cw`i NPDL$R: � i3`r�
Acute
Chronic
Test Organisms
s
c
p
(Composite only)
(Grab orCompos.te)
o
o
_
J
U
=
U
y
_
Z
Sign, and Print below
>
-
;
o
2 -HCI
Z-
on
?
�_
•_,
r
the dotted line
e
�
U
y
U
=
?-ta 03
y
-
_
SAMPLE ID
U
Camposneslart Daic Time
Somplc Catimion Dote Time
Co eted b
U
C.
ti
rn
o
1 Z
o
c
V-101
m
o
>
'j
—
3=Zaic
6-od,cr
¢
Q
U
U
U
ci
*=
z
n
U
_
3
L
Chemical Analysis 8: Other
-------------
-------------
II
II
Special Instructions
Sample Custody Transfer Record
Secure
Receipt
Sample
Date Time Relinquished By/ Organization Received By / Organization
Area
Tem =C
Preseri ed9
•� ��
Cl
I
10 l3 �a
gas
I
I p '0Z
COMPOSITE SAMPLING PROCEDURES
TEAfPERATURE 190NlTORIArG PROCEDURES
HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period
Sample temperature during collection and transport must be between
For toxicity testing the sample must first be used within 36 houu3
Time Proportional l sample each hour for 24 hours Equal volui
0 0 and 6.0 aC Samples must not be frozen Use water ice in sealed bass
of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours.
Sample may not be used after 72 hours from sample collection
Flow Proportional As per instructions in NPDESpen-nit

ET's'
PO Box 16414, Greenville, SC 296D6-7414
[phone], [phone] Fax[phone]
Shipping Address 4 Craftsman Ct, Greer, SC 29650
WW X-"CNVIRONMiE—AL.CDM
CION G -e CUSTODY RECORD
Pale �_ of�
t hent: ,
1�G`
AV
Program
Containers
Preservative
Parameters
WholermucntTocicity
Facility:
, ep 60
State: NPDES / #:
Acute
Citronfc
TestOrgantsms
—
�
o
n
n
U(Composite
only)
(Grab or Composite)G
o
12
—
o
G
V
c
=
Sign, and Print below
ea
3
a
on
^
2- HCL
L
a
2
`^
•_,
=
s
the dotted hoe
3-HNO3
_"
g
=
?
"
'
=
<
SAMPLE ID
V
Composte Stan Daca rima
Sample Collection Dale Time
Collected b3
U
en
ri4
Z
C
U
j
u
4=UGH
i= ZnAc
u
<
V=
<
U
U
U
-
ri
=
3
-776.OdLr
rn
U
_
Chemical Analysis 8 Other
WV7?53C
I
-------
III
I
-------------
i
-------------IT
I
i
TI
-------------
I
I
I
IT
-F
---fl-I
Special Instructions:
Sample Custody Transfer Record
Secure
[krea
Receipt
I
Sample
Date Time Relinquished B / Orgaamzation Received By I Organization
Tamp °C
Presen•edv
V i 1 CD
l
4�-- l� .� I d Oj ✓C /Q;� Wk) / 7)
`—
16IM-)161
ei3r
Ur
I
I a �-
�o r• � sY�
av-l.
C/
I I
l '
COMPOSITE SA,IdPLING PROCEDURES
TEMPERATURE ,VOAUTORING PROCEDURES
HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period
Sample temperature during collection and transport must be between
For toxicity testing die sample must first be used within 36 hours
Time Proportional I sample each (tour for 24 hours Equal volui
0 0 and 6 0 eC Samples must not be frozen Use water ice In sealed bans
of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours
Sample may not be used after 72 hour from sample collection
Flow Proportional As per instructions In NPDES permit

ETE-.---T-,-,-c
(EGA) B77-6942 PAX [phone]
P 0. 0vx IE414. Greeny tie. SC 23606 4 Craftsman Calm, Graer, SC 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: Wastewater Treatment Plant
NPDES # NCO021253
Test Date: 10 -Jan -17
Laboratory ID #: T48371
Test Reviewed and Approved By.
4/4
Robert W Kelley, Ph D
QA/QC Officer
Certification #E87819
Test results presented in taus report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Flonda Dcpt of Health Included results pertam only to provided samples
Page 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Toxicity Report Form - Chronic Mvstdoosts Pass/Fat
ate an
a ty Have ock NP E# NC 2 peg ty a e
La a ry P rf m rag es ment
-� —
- & -- i, _ _ _
S g at e e t r Resp `n �e Charg
x I oo - - -
S g re ab t ry p ry
.I It9vttIL, 1MN�%I- t,v %rronmcnt c s
`tl v ion \1° re, u t
IN I rl,VIR
t�\ Ca I 's"I v z (n t
Ftal tgh \ `) (;
Wg Q
a
F'
9
i
�
� F
l
I
I s e s I
hS
4

O
rl
m
a
m
m
t
n
m
E
0 °c
E
m
U
m
o z
m
a
f7
z
¢
w
m
- E
C
a
¢ c
m
m
�
c O
m
=
U
4
m
U
O
EF
IL
0
U F-
_
E
E
a
R m
F- x
U
3 z
m
L)
O N
o¢¢¢
E
K
U Z
O
N
(p N
N
E
E
m
0 d
9 0
n
d o
m i>
a
F
E E
i
E o
1
H
0
H -
J U
m z
U a
m m
Ul
z z
O
O
rl
m
a
m
m
0
0
J
S
c
5
m
E
0 °c
E
m
U
m
o z
c
E
m
- E
C
a
¢ c
m
m
�
c O
U O
O
rl
SOON
10
'0000000000�o�o-���iin
11iiiii
1iiiiiu�0����
foo
0000000000�o
iiiiiiiiiiiiii�
�000�oo
0000000iiiiiiiiiiiiiiiiniiiiii
�000�oo�00001H�oiiiiii�
�00000�oo�000�o
MUM
11111111111111111111111!
sasses
�.ee�
e�ee�ee
eee�eeee
ee�eee
eeeeee�Illll�
O
rl

ET r A
Y�7 �tygq
q 7HW114.
��.'�t 6 ° '�.4��+�i.L�lREENVILLE, 9C 29fiOfi-7414
[phone], 1013131 091-2325 FAX [phone]
SNIPPING ADDRESS 4 CRAFTSMAN CT, GREER, $C 29650
WWW-ETTGNVIRONMENTAL DOM
CHAIN Of CUSTODY RECORD
Page
Client:�
/ ° Qt
Program
Containers
Preservative
Parameters
/• g4I l
Facility: Pr /� T/�!E'1I7 �.��
¢
3:q?
tIC'...
C"�
r,
Zn'
ME
C
O
m
❑
O
D
O
O
1-HZSO4
-
33-HN0
4 -NOON
e -osier
Whole Effluent Toxicity
W
.0..
�
aea(Composite
P
Chemical Analysis & Other
7t 3 Colk4(on
p
¢
.]
W
0
vHCL
¢
U32A
dState: NPDES #. � /3
Acute
Chronic
I Test Organisms
ID
=�,�tJen
Y
U
f0.i
only)
i
(Grab or Composite)
y
—-0.E1
A
¢
12.U
v
✓
U
tip
y
_
`L
v
nm
v
p
�;
�c
m��
a
3a)
vE�F
ZSAMPLE
iL
Special Instructions
Sample Custody Transfer Record
Time Relinquished B / Or a/nization/� Received By / Organization
Secure
Area
Receipt Sample
Tem °C Preserved?
/D�atte-7
//C///
//C/' /
VO�
/ s� 71 n
a
u Ps
6;T7—
.0
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 (tour period Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional 1 sample each hour for 24 hours Equal volui 0 0 and 6 0 eC Samples must not be frozen Use water ice in sealed bags of sample collection (completion of composite sample)
or at minimum 1 sample every 4 hours over 24 hours Sample may not be used after 72 hours from sample colleenon
Flow Proportional As per instructions in NPDES permit

.00
ET'i
PO 60x 16414, GREENVILLE. SC 29606-7414
11364)1377-6942, [phone] Fn -[phone]
SMIPPINO ADDRESS 4 CRAFTSMAN CT. GREER. SC 29650
t4V/W LTTENVIRO .MENTAL COM
CHAIN vF CUSTODY RECORD
Page of_7
Client: l.,�/
/ oir {�T/c
Program
Containers
Preservative
Parameters
Facility: ;lie Cry
A �T
n� /lf ��
3
..
�p
U
v
a
O
_Cn
iu
�
.-
O
z
I
❑
M
o
U
r,-,
O
at
PV1
2
y
m
a
rn
m
A
V
E
_
O
>
L5q,71
U
V✓
I-H2SO4
2• HCL
3-HNO3
4-NaOH
S-ZMc
e- oU cr
whole Effluent T
IP
1
?:
>
O
1 Chemical Analysts & Other
�:/vr Co% >1
_
a
0o
z
U
¢
LIJ
+�83'r 1
State' G NPDES th r
Acuto
Chronic
Test Organisms
SAMPLE ID
U
V
(Composite only)
Composite Start Date Time
(Grab or Composite)0
Sample Coaeuwn Date Time
/
Collected by
-�=V1
—
cs
�
y
¢
U
�
y
¢
r.
C
o
U
^
M
0
C.3
m_
-O
o
U
cD
f
❑
c
^
u
a
,?
9vVi
c`a
v,
;U
E
o
0
E11111
Special Instructions
Sample Custody Transfer Record
Dale Time Relinquished B I / Or arimbon
//- /71 15X
Received By / Organization
Secure
Area
Receipt
Tem °C
Sample
Preserved9
1 -II- 17
095r.UPS
rich
v
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period
Time Proportional I sample each hour for 24 hours Equal voltu
or at minimum l sample every 4 hours over 24 hours
Flow Proportional: As per instructions in NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0 0 and 6 0 °C Samples must not be frozen Use water ice in sealed bags
HOLD TIME PROCEDURES
For toxicity testing the sample must fust be used within 36 hours
of sample collection (completion of composite sample)
Sample may not be used after 72 hours from sample collection
N.

FTI�
PO BOX 1 641 4. BRCENVILLE. 9C 299505-741 4
(8641 877-6942. 180131 B91-2325 FAX [phone]
SHIPPING ADDRESS 4 OPAF 5MAN CT, GREER, SC 29650
WWW-CTYEN V IRONMENTAL.COM
CHAIN t_,F CUSTODY RECORD -
Page of
- - - - . ,v rcrvi 1 unc mvrwI UrUIVU YRUC;EUURES FFortoxicity
TIME PROCEDURES
Composite samples must be collected over a 24 hour pcnod Sample temperature during collection and transport must be between
Time Proportional 1 sample each hour for 24 hours Equal vola 0 0 and 6 0 °C Samples must not be frozen Use slater ice in sealed ba testing the sample must first be used within 36 hours
or at minimum 1 sample every 4 hours over 24 hoursle collection (complenon ofcomposite sample)
Flow Pro ortional As r mstruehons m NPDES permitmay not be used after 72 hours from sample collection

ETe,,,,t,tniai, Inc
P 0. Box 16414 Greenvile SG 28606
(S64) 877,6842 FAA [phone]
4 Craftman Courl, Greer, SG 29650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-12-02-014 Method 1007
Client: CITE' OF HAVELOCK
Facility: WWTP
NPDES # NCO021253
Test Date: 18 -Apr -17
Laboratory ID #: T49110
Test Reviewed and Approved By:
Robert W Kelley, PhD
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Flonda Dept of Hedlth Included results pertain only to provided samples
Page 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Tnxirity Rannrt Fnrm (hrnnlr Mvclrinncic D -1r: 1
Fa ty Have o
N•
NP # JC 02 5 P pe# 0 ounty C ave
ab at ry Pe nrm
x� r�
ng,Te t /I sell mme ,t
'!%
r I e pe r
esp Pte tha n
S at e of ab a ry
Su ery r
Y t R R cat
•••- o. •••�+•_ _tea. yap e_••• I l ll l l l l IV 111 a l ov lell uv" Dva 11411
D
vi on f `NN ater Qua rtN
1) V R
62J Nla I Set% cc(:enter
Ra cogh N(m27699-I0'21,
a n R t a s
�J
Wa ty
Da
4
nt 65
a
T,re rn
aS
� e
q
s t

ET
yr
ao eDx 1 ea 14, r3Reenva�E sc z98ots-741 a
11384) 077-6942, [phone] FAX [phone] r938
SHIPPING ADDRESS 4 CRAFTtaMAN CT ORECR, SC 29690
WWW ETTENVIRONMENTAL COM
CHAIN Of CUSTODY RECORD
Page —L_ of
Client: ,
[,��j--
Program
Containers
Preservative
Parameters
i ��"����n� Q� 2-1
We, Facility: 1e �P� (,
¢
a
3
U
`y
S
rn
c
u
to
C
o
MOO
o
z
�_
m
O
U
0�
4t
v
a
5
o
>
1
~
1=H2504
2- HCL
3mHNO3
4-NaOH
S=ZnAc
w0he[
Whole Emuen[Tortnq
`
=
3
y
_
Ro
2
Chemical Analysis & Other
Q
<
-- )
C7
[iii
if9nofl
State: NC NPDES #: /5?
Acute
Chronic
Test Organisms
SAMPLE ID
K
U
fj
V
c
(Composite only)
Compos,teStart Date Time
-"1116117
(Grab or Composite)
SsmpleCoaclilanData Time
11117117
Collected by
�,'.
w
y
0.
U
¢
.V-
U
y
=
to)
¢
�_
C
^D^,
o
`^
v
U_
p
S
o
v
9
U
ea
ea
-o
c
`�
c)
a
h
c
`'
y=
A
O
d—
rin
T
z
U
Ill
--11TT
Special instructions
Sample Custody Transfer Record
Date Time Relinquished B / Or anization Received B / Organization
Secure
Area
Receipt
Tem °C
Sample
Preserved9
f636
=
r8
8�Ei
dEx
p v
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional 1 sample each hour for 24 hours Equal vols 0 0 and 6 0 °C Samples must not be frozen Use water ice in sealed bags of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours Sample may not be used after 72 hours from sample collection
Flow Proportional As per uistruchons in NPDES Permit

ET'jL",-
PC]
13OX 1 641 4. SACENVILLE. SC 29 606-74 1 4
(864)877-15942. 18001 a91 -2325 F".18641 877 6938
SNIPPING AOOPESS 4 CPA1 SMAN Or. GRCEA, 8O 29650
W W W.ETTEN VniCNMCNTAL.COM
CHAM OF CUSTODY RECORD
Page of
Client: r ,
(_,. � f � /
Program
Containers
Preservative
Parameters
Facility:
a`sa
in
o
_
o
>
=s=oaM
1=H2504
2- HCL
=[03
i- ZnAc
Effluent Toxicity
L�Lt]7
R
Q
ci
h>
e
Q
im
W
z
UQ
E
v�
State: AIC NPDES #: 00,? offWhole
Acute
lChronic
I Test Organtslns
SAMPLE ID
pu
o
U
U
aC7
(Composite only)
Composne Start Date Time
(Grab or Composite)
®pleCollectionDnte Time
Collected by
'c
�=
U
_
t)
U
...
y
2
?'
o
U
c.0ee
� o
a
m
T>tQ
43N
o
Special Instructions- [Apn oye, YaQ I al-. b -P- kA5 t,i-nCj -4p�ryt +t I�U1+k '� k C D L `rky- cff�weds
d t, I;Ls na-� sealed t -50 "t" li _ exL Y�v� eAk��Q i +Kk COO ( . _ 6-D3 d
Sample Custody Transfer Record
Date Time Relinquished By/ Organization Received By / Or anlzanon
Secure
Area
Receipt
Temp °C
Sample
Preserved9
1-2
UP5
i
PLVAt-
io
It
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must fust be used within 36 hours
Time Proportional I sample each hour for 24 hours Equal voluj 0 0 and 6 0 PC Samples must not be frozen Use water Ice in sealed bags of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours Sample may not be used after 72 hours from sample collection
Flow Proportional: As per instructions in NPDES permit

ET
PO 13OX 1 641 4. GPEENVILLE. SC 29606-7414
(1964) 877-6942. [phone] FAX [phone]
SHIPPING ADDRESS 4 rRAF S..N Cr. GREER Sc 2965❑
WWW ET CNVIRONMENTAL.COM
CHAIN OF CUSTODY RECORD
Page of
Client: ci tq U`$_ f
' pav�.. t�LJ
Facility:utV� 7�j�
¢
a
U
Program
C
W
in
0
.-
Z
0
L.,
a
Containers
vi
iL
t7
.•
�
Preservative
1=It2SO4to
4=NaOHLQ
$= oche
c=oaar
Parameters
Whole Effluent Toxicity
P
fir
3
[]
R
:2 Chemical Analysis & Other
zm
C]
<
r
Pit
State: NPDES th C, 0a 91;
Acute
Chronic
Test Organisms
SAMPLE ID
E(
lJ
V
Composite
(Composite only)
Composae Start Date Time
(Grab or Composite)
Sample Collection Date Time
Collected b Y
U
d
U
d
G
�.
U
^
U
,1
U
ci
e
[�
3
o
i9 T
rs.
v,
_
-
U
i
Special Instructions
Sample Custody Transfer Record
Date Time Relinquished By/ Organization Received By / Organization
Secure
Area
Receipt
Tem aC
Sample
Preserved?
,'311 li'
'OSS1
j 1 p
&Litv1rC. Cat 1�c�1(21�C, �}�U� T
U 2217
1 U5,6
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional 1 sample each hour for 24 hours Equal volui 0 0 and 6 0 °C Samples must not be frozen Use water ice in sealed bags of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours Sample may not be used after 72 hours from sample collection
Flow Proportional As per instructions in NPDES permit

ET-.,,Mb1,nc
P.O. BOX l W4. Greenvale. SC 23606
SEG4y 877-6942 FAX[phone]
4 C!"Asman Coup, Grier, SC 29550
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES #• NCO021253
Test Date: 18 -Jul -17
Laboratory ID #: T49644
Test Reviewed and Approved By
4411 t1l
Robert W Kelley, PhD
QA/QC Officer
J Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health Included results pertain only to provided samples
Page 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR certification # 022

Facility Havelock
- - - -.... _............. �...., �.� v aaarrall Date 18 -Jul -17
NPDES # NCO021253 PI e# 001 County Craven
Lab
na St now• - Comments
X
5
Signature of Opera
Jinespoq l e
X
�s
SI nature of Laboratory Supervisor
4
MATT nDT!'iATAT grrN. r�__.e_______�_. .,-•
v■uu■dua■ Ul,■carLc3 Ul A11CH
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates
1
2
3
4
5
6
7
8
78
Surviving #
4
3_
_ 4
5
4
5
5
5
%Surnval
Original #
4
4
5
5
4
5
5
5
49
Weight (per Original)
0 390
0 213
0 262 _
0 360
0 440
0 362
0 324
0 354
Avg Weight (mg) 0 338 Avg Fecundity 783%
Fecundity (gravid/total females)
1/2
1 /1
2/3
1/2
1 /1
3/3
3/5
2/2
255
Treatment 2 Replicates
1
2
3
4
5
6
7
8
78
Surviving #
3
3
1 5
4
4
1 4
5
5
%Survival
Original #
5
5
1 5
4
4
4
1 55
49
49
Weight (per Original)
0 212
0188
1 0 322
0 368
0 283
0 338
1 0 336
0 308
Avg Weight (mg) 0 294 Avg Fecundity 1000%
Fecundity (gravid/total females)
2/2
2/2
0/0
2/2
2/2
2/2
2/2
3/3
255
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Treatment
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Temp at Receipt
80
80
82
80
82
82
83
24 hr
24 hr
78
78
73
77
77
7.9
80
70
66
64
63
68
72
62
51
53
5C
49
49
38
52
264
255
254
25L 1
254
1 252
252
267
26.7
269
265
267
267
265
247
255
260
21-0 1
262
262
171
n I o
81
80
83
V9
82
81
83
24 hr
24 hr
79
80
_ti6
79
78
80
80
68
68
67
52
68
67
64
52
50
44
47
48
45
59
50
257
256
'25 9
262
25,4
256
267
267
269
265
267
26,7
266
243
24,3
256
256
238
240
256
16 -Jul -17
18 -Jul -17
20 -Jul -17
24 hr
24 hr
24 hr
730
698
646
<0 05
007
<0 05
07
i 08
1 22
Results
Significant Mortality?
Yes No
X
Check One
Growth
Calc t 1 30
Tabular t 176
Fecundity
Rank Sum 70
Crit value 49
PASS FAIL
X
Check One
Test Date
Effluent Test Concentration
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during rei
5 replicates were set for each treatment lest replicate, where <5 are shown the organisms were lost during
DWQ Form AT -4 (6/99)
Page 2 of 6

W
0
0 > 0
0 5�
r�
� y
N
O m
a
m
.o
3 z
N N
Z m c a
2 N
n �
0 3
o
m N
n
0
3
�
o
c
n
s
m
m
0-
D
f
e
Z Z
3
O
n
0 0
3 3
—-
_En
1 Ci
D -0
-n
C
0�
�c
z
--I
O
w
m
IM
Z
m
m
111111mmmmill
ME
1111111MR111111
�
illmilmols
����0���
11111111111111111111111111111111���9��5�
0 > 0
0 5�
r�
� y
N
O m
a
m
.o
3 z
N N
Z m c a
2 N
n �
0 3
o
m N
n
0
3
�
o
c
n
s
m
m
G
Y�
r�
-� �
a• �
O m
2 2
0 N
N N
3 m
2 N
n �
�
0-
D
f
e
Z Z
3
O
n
0 0
3 3
—-
_En
1 Ci
D -0
-n
C
0�
�c
z
--I
O
w
m
IM
Z
m
m

Ery
3.4i" a�"" �
SPC BOX 16414, GREENVILLE. SC 29606-7414
[phone]• I8001 891.2325 FAX [phone]
SHIPPING AODRE00 4 CRAFTSMAN CT. GREER. SC 29550
WWW LTTCNVIRONMENTAL.COM
CHAIN Of CUSTODY RECORD
Page ( of
Client: ._r
P—i Cat- \IeA jGv—)
Program
Containers
Preservative
Parameters
Facility
\re{'t'
¢
ai-
3
Urn
e
=
e9j
to
o
m
O
Z
v
c
O
a
to
4
i
y
R
O
c
O
>
u
1-HIS04
2m HCL
4-NaOH
S-ZnAc
6=Other
Whole Effluent Toxicity
E-
t✓
3
Chemical Analysis & Other
p
<
2
CID
<
State: IVPDES #:
Aeute
Chronic
Tat Organisms
SAMPLE ID
—°
1
(Composite only)
Composite Start Date TimE
(Grab or Composite)
S=p)eCoaecuanDate nine
Collided by
F1
i
e"a
V
<
V
=
U
¢
n
a.
o
D
U
-
o
c
co
c
o
[a
o
c
c
�.
�-
E
US
m
T
a
T=i—
z
m
ive, �'
�" . ►
i tl
ib
�L, �+t
c?
✓
�. 9 @ CC VL -Hon
`I A
Special Instmctions
Sample Custody Transfer Record
Date Time Relinquished B / Organization Received By/ Organization
Secure
Area
Receipt
Tem aC
Sample
Preserved)
'c4.
Vbr i �t i'1�`�°L�iXTl
1
Old
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TBfE PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be beMeen For toxicity testing the sample must first be used withm 36 hours
Time Proportional 1 sample each hour for 24 hours Equal volu 0 0 and 6 0 'C. Samples must not be frozen Use water ice to sealed bags of sample collection (completion of composite sample)
or at minimum 1 sample every 4 boars over 24 hours Sample may not be used after 72 hours from sample collection.

PO Box 16414, GREENVILLE, SC 29606.7414
[phone], (BOO) 991 -2325 FAX [phone]
SHIPPING ADDRCSS 4 CRAFTSMAN Cr. GREER. SC 29650
WWW.LT ENVIRDNMKWAL.CCM
CHAIN of CUSTODY RECORD
Page of
Client: py �
"� � W �
Program
Pg
Containers
Preservative
Parameters
Facility: W Wdk t
"�
U
$
in
y
rn
p
tz
o
z
`m
U
o
. Y
;
E
y
a
C7
"
E
o
>
y
U
1-HSO4
3 -HCL
NO3
4-NaOH
5s ZnAo
�O�M
whole Effluent ioxielty
W
F
�.
�]
3�
a
c
Chemical Analysis &Other
(�
Q
�
Q
u
_
State: NPDES ai:
'y �j
Acute
Chrome
I Test Organisms
SAMPLE ID
e(Composite
C7
only)
Composite Start Date Time
(Grab or Composite)
SempkCollecuonDala Time
Collected by
r
y
�
3
U
Q
U
�
=
U
Q
O
U
V
U
�
o
U
�
U
�
�.
Q
�
4
�
.y
T—
�
G
?
n
�
c
T
x
52
O
U
5 $'
►i
.i�ll�-
No
Vau (bufws,
��
11.1°�- C611ler-1'
47wh
ILI
Special Instructions
Sample Custody Transfer Record
Date Time Relinquished B /Organization Received B ! Organization
Secure
Area
Receipt
Tem DC
Sample
Preserved9
tcq,
mq
'7
093
PE)
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional 1 sample each hour for 24 hours Equal voluj 0.0 and 6 0 DC Samples must not he frozen. Use water ice in sealed bags of sample collection (completion of composite sample)
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection
Flow Proportional As per instructions in NPDES permit

ET"jL'
PO 8D% 16414, GREENVILLE. SC 29BO6-7414
[phone], (80171 891-2325 F—:(1364) 977 6930
SHIPPIN13 ADDRESS 4 CRAFTSMAN CT, GREEK, SC 29650
WWW ET MNVIRDNMENTAL COM
CHAIN OF CUSTODY RECORD
Page Of�_
Client:
I \1
Program
Containers
Preservative
Parameters
whole Effluent Toaetty
Facility: qn y
tC �1
State: NPDES 9: LL Coal W,52j
Acule Chronic
Test Organisms
2
c
d D
=
n
Q
o
U
(Composite only)
(Grab or Composite)
__
¢
2'
$
"
_ o ;'
e+ U
D
U 3 a
? c
.0
3eo
m
I-NSO4
2=HCL
-� a
w 7 d
r.
_ >
z
_
Coll
A
�,
y
y
_
3-HNO3
4=Na0)i
0 o
o E d o C
Q
SAMPLE ID
Campos ac Start Date Time
Sample Collection Date Time
Collected by
y
U
V1
rn
pr
(�
��
5=ZnAc
=other
v v
¢ ¢ U
r a
ct U o i �, E~ 3 Chemical Analysis & Other
w
0
)
)
n
)
I
IT
Special Instruct3ons
Sample Custody Transfer Record
Secure Receipt
Sample
P
Date Time Relinquished B / Organization
Received By / Organization
Area Tem nC
7<
Preserved9
Dry 9�
- G✓%'�
Z l
P5
A . i! ah
2.Z
COMPOSITE SAMPLING PROCEDURES
TEMPERATURE MONITORING PROCEDURES
HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period.
Sample
temperature during collection and transport must be between
For toxicity testing the sample must first be used within 36 hours
Time Proportional 1 sample each hour for 24 hours. Equal volul
0 0 and
6 0 °C Samples must not be frozen Use water ice in scaled bags
of sample collection (completion of composite sample)
or at minimum 1 sample every 4 hours over 24 hours.
Sample may not be used after 72 hours from sample collection
Flow Proportional- As per instructions in NPDES permit.

envirunmtatta .Inc
P.O, Box 10414, Gfeei Ale, SC 29605
(E84) B77.G942 FAX (864) 877-G938
4 CraRsrnan Ccud, Glaer, 5C 20650
Americamysis bahia Survival, Growth and Fecundity Test
EPA -821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES #• NCO021253
Test Date: 10 -Oct -17
Laboratory Sample ID #: T50175
Test Reviewed and Approved By:
4411 411�
Robert W Kelley, PhD
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health Included results pertain only to provided samples
Page 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Tnxicitv Rennrt Fnrm - Chrnnic Mvcirinnwic Pa-.c/Fail
naso 1 n -n, f-1 7
Facility Havelock NPDES # NCO021253 PI e# 001 County Craven
Laboratory Performing Test Comments
x
Signature of Operator In Responsible Charge
x
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
Surviving # 5 4 5 3 / 4 4 5 5
Original # 5 4 5 3 4 4 5 5
Weight (per Original) 0 346 0 350 0 404 1 0 517 0 355 0 465 0 436 0 342
Fecundity (gravid/total females)
3/4
3/3
2/3
2/2
2/3
213
2/3
1/2
Treatment 2 Replicates
1
2
3
4
5
6
7
8
Surviving # 4 5 5 5 5 4 4 4
Original # 4 5 5 5 5 5 4 5
Weight (per Original) 0 395 0 362 0 380 1 0 402 0 404 0 216 0 288 0 300
Fecundity (gravid/total females) 2/3 1/2 2/2 1/ 1 1/2 0/0 1/ 1 313
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Indial
79
80
80
79
80
80
81
24 hr
24 hr
78
75
75
75
77
76
81
74
74
73
66
68
69
74
50
37
47
35
39
46
59
258
254
245
252
251
250
251
268
264
268
267
265
266
267
250
264
266
268
247
248
248
Treatment 0 1 2 3 4 5 6 7
pH Initial
pH Final
DO Initial
DO Final
Temp Initial
Temp Final
Salinity Initial
BO
80
80
79
80
80
81
24 hr
24 hr
79
79
75
76
77
77
81
77
77
79
66
68
69
76
62
49
39
41
40
41
62
258
252
256
255
257
256
254
268
264
268
267
265
266
267
258
260
240
230
235
236
237
Sample Test Date
Collection Start Date
Grab
Composite (Duration)
Conductivity (pmhos/cm)
Chlorine (mg/L)
Sample Temp at Receipt
08 -Oct -17
10 -Oct -17
12 -Oct -17
24 hr
24 hr
24 hr
790
784
780
<0 05
<0 05
<0 C5
07
10
1'
%Survival 100 0%
Avg Weight (mg) 0 412 Avg Fecundity 740%
%Survival
Avg Weight (mg) 0 344 Avg Fecundity 810%
Test Results
Significant Mortality?
Yes No
x
Check One
Growth
Calc t 1 75
Tabular t 1 1 76
Fecundity
Rank Sum 61
Cnt Value 51
PASS FAIL
x
Check One
Effluent Test Concentration
5 replicates were set for each control test replicate, where <5 are shown the organisms were lost during renewa
5 replicates were set for each treatment test replicate, where <5 are shown the organisms were lost during rene
DWQ Form AT -4 (6/99)
Page 2 of 6

w
O
ch
d
O)
c0
d
-
^
O
m
N
a
O
Z ¢ C
(/)
¢ If o
Q
m
m
It U N
E
in o
O m
U)
W
d
a
Q toil ❑ Z
c
d
E
:
= Cl)
�E O
E
a
E
E
Z } a
¢N
O
`o
o
Q ^ 11
m
W O all
�
O
^
�C
H
N
o>
o o
a¢
Z
�c
m
3
o>
O o
W
O
U
U
E
E
m
o
m
uoi
F-
m y
2?
U"
Z U
o
.-
d
O¢
U i
g
O O
U
Z
Z
e
o
V
voi
N
.-
in
04
voi a
^l w
°
T
0-°
a
n
o
>>
J
V N
2 V
w
O
ch
d
O)
c0
d
-
^
O
N
a
O
Z ¢ C
0
¢ If o
m
m
It U N
E
in o
O m
C
U
d
a
Q toil ❑ Z
c
d
E
:
= Cl)
�E O
E
a
E
E
Z } a
¢N
O
`o
o
Q ^ 11
U
W O all
w
O
ch
d
O)
c0
d
�I�I�YN��I����In11111w1111�A1111A1����'
�
■�����
1�����■I����Y��oO�ooO
Y����
I�O�OOO
00000O�IN�����■�����
1�����■1����■��oO�ooO
fo�o��i��iiii
■�iiii�iiiii�iiiii�u00000000������
�ii�i��o�o��00����
ERRO�i�idini
iiii�
ii�ii���ii-�-o-00�0�����
111111
111111
MORRIS
�ee�e
eee�e
�ee�eee
�eee�
seeeee�see�eell
w
O
ch
d
O)
c0
d

I" W"Woftl 19
-enwronih-enial-
PO Bax 1641 4 GREENVILLE Sr 29606.745 4
(864) 677"6942 (BOOM 391»2325 FAX�YB64) 877 6922
SHIPPING Ap ORE55 4 CRGrT9t1A(,v CT GFEER- SC 29650
WWW ETTEyNVIRONMENTAL COM
CHAIN uF CUSTODY RIECQRD
l"a oF—
Client: /
,r/�/ GC,"�/C
Program
Containi.rc�
Presenatile
PatametetS
Facility. r �
,.'••7 �-;nI✓4 /�Cyl�
'•
cri
Etc(
o
\1 fialG Efnuent Toilctn
—
Chemical Analyses & Other
--
/'Il
State, �)�,✓ APD);S it �r/�Ld� �C/J-h �'
icutc
Chronic Iest binum<
SAI 1�.PLE 1D
(Com osltc only
p )
(Grab yr Gdmba>(,e}
5nnrt
>
u
>
a\/~
-2%'
"t7
'
I
�
I
i
FIL
1
1
1
1
1
1
Special Instractions
Sample Custody Tratisfei Record
T_Ime ,— _Relinquished By s Oramzation P.ecehed B% Oreanazatinn 1
Secur
area
i ReCelpt
I'emp'C
Sample
d,'
,,Date
fop
10 0
-
f
C
COMPOSITE S4 WFL1 i G PROCEDURES
Composite samples must be collected ovCr a,24 hour period
Time'ProportionaL 1 sample each hour for 24 hours Equal
or at minimum I sample every 4 hours over 24 hours.
Flow Proportiona �r instructions In NPDES permit
TE,WPER4TURG A101'II'ORIAG PROCEDURES
Sample temperature during collection and transport, must be bem eels
0 0 and 6 0 °C Samples must not be frozen Use Nater ice in sealed bags
HOLD TPIIE'PROC,iDf RES
For testing the SainoIo must first he LKCu %uth"p 36 hours
of sample collection (,comolctlon o1 composite semplc)
Sample maN, not be used atter i2 hpur5 from samnk; collection,

0
6
CHAIN Of CUSTODY RECORD
y'O a'c r — —
PO Baa 1 661 4 GPEENVILLE„ SC 29606 7414
(364) B77 6942 5900) 891 2325 F—,(863) 877 ,693E
GylvrsiNG ADD' ESS 4 C—SMAN CT GREEK SC 29650
WWW ETTE�NVIRCNMENTAL DOM
Client ick . r , K I , 1_ -, / ('i 1'• a't
Program (o[rtuncr� I Preser'sahle F tame rS
Facility I , —y— j
i 1
�
v(� � C' i r I �9�1 � d! CK ')�
R hoTc Ff(luent I ct�ICI[s
�
i
State: A/ INPD s M A � t ^
�-tL
Chronic
res[ OrL',1r3—Pr
!
11(t
JiNo
J
SAMPLE ID �
C),oppm��poppsltGSto D,te Time�,S—T,`!gCMI,1..n
D,tL Time
(7011eLt4d to
-7
z
�
3
�
—
or
�
�
9 �, -,
wry;
C
=
Chemical Anafysts & Other
i
)pcclal Instructions
Sample Custody Transfer Record secure h 2cceIFl I -Sampl-
Date -line Relinquished By OroanizatiotI Fcccived>3v Organization .yep -t.mp C �Presorvcd'
zz
i ( I
i0 1� LI
0,11POSITE S 111PLING PROC'EDL',RES TEMPER--ITURE A10WTORING PROGMIRLS NOI D TI�11E PROGCEL (2rS
'omposite samples must be collected oyer a 24 hour per!Qd Sample temperature during. colbction and transport must be bemcen For IQvicin te,tTna,hu sample mpt t firt be used «lthali I)�) hours
-ime Proportional 1 sample each hour for 24 hours Equal V`olut 0 0 and 6 0 °O Samples must not be lrozen C Se Mater ice III sealed baL,� of 'sample Collection ((AmpICU0I1 or cQntposite, satiiple
it at minimum I sample ever} 4 hours over 24 hours Samnle ma} not be, us --o atter —2 hours From sample calfcaaon
Io a Proportional, As per mstructiQns in NPDES permit

CHAIN Of CUSTODY RECORD
- environmental
PO BOX 1 641 4, GPEEI-IL IE SC 29606 741 4
69641677-6942 'BOO) 891-2°3,25 F—,(E36�) 677 6933
SHTPFING AOORESS-� 4 CRArTSMAr, CT CREEP Sr 29650
WWW OTYGfNVfFjONMEfNTAI —
Client: � % �/ �'�
1 % �� (� f f✓ �
Piorram
Containers
Presenarne
Pat ant eters
Facility.
iJ//..} / C �l�i'�/�'tr / J�'�C,'/•ti L�,� t"->
�
s
s
z
R•holc
i(nuent 'I o—tl
Chemical Analysis 8 Other
State, NPD1:S i- `� ���r' �� % ✓�,�,�
leuti
C,ttronic
'fest 9r��nicttic
_
_
SAMPLE ID v
(COmI)OSIte OrIINJ
Compostt� Start Dmf Time
Grab z5r Compo�l.aj
S� plyCuuection DI'L Time
cottertea ��
<
j
!
N
f
IIJ
111
I��
Special Instructions
I
i
Sample Custody Transfer Record
Date Time Relin uislte Fad/Ora. izaiiQn ReCU1ed 13%'Organization
Secure.
La
RCOCI t
1 Iernp �C
Sample
�Prc5erncd'-'
COdIPOSITCSAMPLING PROCEDURES TEA IPERATLRE VONIITORIV,G PROCEDCRF.S HOLD 71,1-L PR00CD2�RES
Composite samples must be collected over a 24 hour period Sample temperature during collection and transport, must be betsseen, for (o\iclt} testing the sample must Ctrsf oe u;ed within 36 hour,
Time Proportional 1 sample each hour for 24 hours Equal Volui 0.0 and 6 0'C Samples must not be frozen. Usc tater ice in sealed baps, of sample collection fcompletlon of compoirt, sample
or at minimum 1 sample ever} 4 hours o> er 24 hours ,Sample maga not be used a lfrom m
er �2 hour, om ,ample collectloa
Cioxi Pronortiona er instructions in NPDES nermit

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Annual Priority Pollutant Analysis Data
2014-2017

-�- ---Min
. 4, �%---
I
-* =f �Dr+inking Wa Vi r.+�IDL. 3�771a5�
� wastewater ID; 10
P O BOX 7085, 114 OAKMONT DRIVE PHONE (252) 75G -G208
GREENVILLE, N.0 27835-7085 FAX [phone]
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
ID#: 204 H
DATE COLLECTED: 05/29/14
DATE REPORTED : 06/25/14
REVIEWED BY: � �
Effluent
Analysis
Method
PARAMETERS
Date Analyst
Code
Ammonia Nitrogen as N, mg/l
0.06
06/03/14 ALB
350.1 R2-93
Total Kjeldahl Nitrogen as N,mg/1
1.54
06/02/14 ANO
351.2 R2-93
Nitrate -Nitrite as N, mg/l
3.66
05/30/14 ANO
353.2 R2-93
Total Phosphorus as P, mg/l
0.93
06/02/14 ALB
365.4-74
Oil & Grease (HEM), mg/l
<5.0
05/30/14 SEJ
1664B
Phenol, ug/l
<5
06/06/14 SEJ
420.1-78
Total Cyanide, mg/l
<0.005
06/05/14 SEJ
450OCNE-99
Total Hardness, mg/l
119
06/04/14 TRB
2340C-97
Total Dissolved Residue, mg/l
461
06/02/14 LW
2540C-97
Antimony, ug/l
<3.0
06/20/14 LFJ
EPA200.8
Arsenic, ug/l
<5.0
06/04/14 MEL
311313-04
Beryllium, ug/l
< 1.0
06/03/14 LFJ
EPA200.7
Cadmium, ug/l
< 1.0
06/06/14 MEL
3113B-04
Copper, ug/I
<10
06/03/14 LFJ
EPA200.7
Total Chromium, ug/l
<5.0
06/03/14 LFJ
EPA200.7
Lead, ug/l
< 5.0
06/09/14 MEL
311313-04
Nickei, ug/l
<10
06/03/14 LFJ
EPA200.7
Selenium, ug/l
<10
06/04/14 MEL
3113B-04
Silver, ug/l
<5.0
06/03/14 LFJ
EPA200.7
Thallium, ug/1
< 1.0
06/20/14 LFJ
EPA200.8
Zinc, ug/1
48
06/05/14 MTM
3111B-99
ID#: 204 H
DATE COLLECTED: 05/29/14
DATE REPORTED : 06/25/14
REVIEWED BY: � �

PO BOX 7085 114 OAKMONT DRIVE
GREENVILLE N C 27835 085
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY:
VOLATILE ORGANICS
RPA MPTUnn C 7 A
CLIENT ID:
ANALYST:
DATE COLLECTED
DATE ANALYZED:
DATE REPORTED:
Wastewater ID: 9n
PHONE [phone]
FAX [phone]
204 H
MAO
06/20/14
06/27/14
07/07/14
PARAMETERS, ug/1
Effluent
-I.
Chloromeihane
<10 00
- 2
Vinyl Chloride
< 10.00
� 3.
Bromomethane
< 10.00
4
Chloroethane
< 10.00
5.
Trichlorcfluorontethane
<5.00
-6
14-Dichloroethane
< 5.00
�7.
Meth) lene Chloride
< 10.00
" 8.
trans-1,;-Dichloroethene
<5.00
"- 9.
1,1-Dichloroethene
<5.00
<1-0
Chloroform
<5.00
--11.
1,1,1 -Trichloroethane
< 5.00
--12
Carbon Tetrachloride,
<5.00
-13
Benzene
<5.00
1.1
1.2-Dicliloroethane
<5.00
-15
Trichloroethene
<5 00
-16
1.2-Dichloropropane
<5 00
-17
Bromodichloromethane
<5 00
-18.
2-Chloroethyl,.tnyl Ether
<5.00
19.
cis-1,3-Dichloropropene
< 5.00
.-20.
Toluene
<5.00
-21 -
trans-1,3-Dichloropropene
<5 00
-22.
1,1,2 -Trichloroethane
<5.00
-.-23
Tetrachloroethene
<5 00
-24.
Dibromochloromethane
<5 00
--25.
Chlorobenzene
<5 00
-26.
EtliNlbencenc
<5 00
--27
Bromoform
<5.00
-28
1 1.2 2-Tetrachlcr"I ma<
<5 00
1'29
1,3 -Dichlorobenzene
<5.00
X30
1,4-Dichlorobeniene
<5 00
=31.
1,2-Dichlorobeniene
<5 00
- 32
Ac -olein
< 100 00
�-- 33
Acrylonitrile
<50 00
Wastewater ID: 9n
PHONE [phone]
FAX [phone]
204 H
MAO
06/20/14
06/27/14
07/07/14

NIMQ00��c��� alp D�c�o
EENVILLE, N C 27835-7085
lod
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 2 532
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
PARAMETERS, ug/l
:1.
f:21:
N-Nitrosodimethylamine
Phenol
13.
Bis(2-Chloroethyl) Ether
+1 4.
2 -Chlorophenol
€� 5.
1,3 -Dichlorobenzene
y 6.
1,4 -Dichlorobenzene
-7.
1,2 -Dichlorobenzene
rs- 8.
Bis(2-Chloroisopropyl) Ether
"" 9.
Hexachloroethane
-w10-
N-Nitrosodi-N-Propylamine
--11.
Nitrobenzene
x.12.
Isophorone
X13.2-Nitrophenol
14.
• 2,4 -Dimethylphenol
15.
Bis(2-Chloroethoxy) Methane
-16.
2,4-Dichlorophenol
,017.
1,2,4-Trichlorobenzene
.s18.
Naphthalene
' 19.
Hexachlorobutadiene
0.20.,
4-Chloro-3-Methylphenol
X21.
Hexachlorocyclopentadiene
22.
2,4,6 -Trichlorophenol
-- 23.
2-Chloronaphthalene
-24.
Acenaphthylene
25.
Dimethylphthalate
--26.
2, 6-Dinitroto ulene
T' 27.
Acenaphthene
- 28.
2,4-Dinitroplienol
29. f.4-Nitrophenol
30. ,
30I'Flu4ore
2,-Du- - -_
.�31.
enitrotoluene
-� 32. -
Diethylphthalate
33.
4-Chlorophenyl Phenyl Ether
-34..
4, 6-Dinitro-2-Methylphenol
-•35.
N-Nitrosodiphenylamine
® 36.
4-Bromophenyl Phenyl Ether
--37.
Hexachlorobenzene
r- 38.
Pentachlorophenol
...-39.
Phenanthrene
-40.
Anthracene
-41.
Di-N-Butylphthalate
- 42.
Fluoranthene
43.
Benzidine
.� 44.
Pyrene
X45.
Butylbenzylphthlate
X46.
Benzo[a]anthracene
47.
3,3-Dichlorobenzadine
•� 48.
Chrysene
CLIENT ID:
1-HUNE [phone]
FAX [phone]
204 H
ANALYST: CHS
DATE COLLECTED: 06/20/14
DATE EXTRACTED: 06/26/14
DATE ANALYZED: 07/01/14
DATE REPORTED: 07/07/14
Effluent
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
<10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
<20.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 50.00
< 50.00
-< 10.00
< 10.00
< 10.00
< 10.00
<50.00
< 10.00
< 10.00
< 10.00
< 50.00
< 10.00
< 10.00
<10.00
< 10.00
< 100.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
Page: 1

�r
(iwuQ�C���
PO BOX 7085 114 OAKMONT DRIVE
GREENViLLE N C 27835-70 5
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 8532
REVIEWED BY:
SEN_IVOLATILE ORGANICS
EPA METHOD 625
PARAMETERS, ug/1
49.
B►s(2-Ethy=hexyl)phthalate
—50.
Di-N-Octylphthalate
— 51.
Benzo[b]fluoranthene
�— 52
Benro[k]fhioranthene
x;53.
Benzo[alpyrene
x.54.
Indeno(1,2,3-C,d)pyrene
li 55
Dibenzo[a,h]anthracene
—56
Benzo[g,h,i]perylene
—57.
1,2-Dipheny1hydrazine
Wastewater ID:
PHONE [phone]
FAX [phone]
CLIENT ID: 204 H
ANALYST: CHS
DATE COLLECTED: 06/20/14 Page: 2
DATE EXTRACTED: 06/26/14
DATE ANALYZED: 07/01/14
DATE REPORTED: 07/07/14
Effluent
<20 00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10.00
< 10 00

Envirorn
P.O Box -70,15 114 Oakmont Dr
Gicenvil l `. nC '7858
environ tz--v c m1 me com
CHAIN OF CUSTODY RECORD
Elio ,c (2 S z)156-6208 • Fax [phone] DISINFLCI'ION
w1
• 20 JCHLORINE
Page of
CHLORINE NEUTRALIZED AT COLLECTION
� L . 4 H Week: 23
L! V Z L L Z LZ (✓� pH CHECK (LAB)
CITY HAVELOCK
AIR, ,!%,RT1H0UGH ❑ NONE P P P P G G P P P P G G G G G G
WASTEH'ATER TREATIMENT PLANT
304 N_ JACKSON DRIVE C C C C C C D C A A A A A E E E
HAVE LOCK NC 28532
�o I
E F_
(252) 4-44-6421
u.r v v
�
o
LU
rr
_
d
N
w
O p 0
Z
U
Uc
CC
Rt
U3
COLLECTION
oo
N
W
Q
gg
zz
SAMPLE LOCATION
DATE TIME
o¢
Q
F
Z
F
v
H
aj
W
A
A
Wcc
Effluent
✓ �O
I
15
�+ --
((
f
j ct�j
RE 7E BY (SIG) DA ME COMMENTS
3 '
RECE
IVED13Y(SIG)f DATEIi1ME
RELINQJISHED BY (SIG) DATE/TIME RECEIVED BY Sif-
�' r 1SE READ Instructions for completing this firm •n the reverse slde
-ORM #5
wll
CONTAINER TYPE, P/G
CHEMICAL PRESERVATION
A -NONE D-NAOH
B-HNO, E -HCL
C - H2SO, F -ZINC ACETATE/NAOi
G - NATHIOSULFATE
CLASSIFICATION
UWASTEWATER(NPDES)
JDRINKINGWATER
DWQ/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING S MENT/DEL[VERY
,Y N
SAMPLES COLLECTED BY
(Please Pnnt) , I ` i I
SAMPLES RECEIVED IN LAB A7__QZ�°C
0
Sampler must place a 'C" for composite sample or a `G" for
Grab ,amnla in tha hlnrkc nhnuo fnr onrh noromn}nr r —� f-4

EK..- Invironn , Inc.
F-- <D �� ___., 1 14 Oakmont Dr
CHAIN OF . _ ,'STODY RECORD
G r'Ceuvlllc, NC 27858
Page 1 1
e Y"A V11011nlent I iac C011l
of
COO (257) 756_6208 . Fax [phone]
DISINFLCTION
77,
1 1
1
1
1
CHLORINE NEUTRALIZED AT COLLECTIOI
X-111 7':
CHL'0121NG
204 H Week: 23
t J
(/7i �/
li�
pH CHECK (LAB)
CITZ' OF HAVELOCK
nls - ART HOUGH
NONE
G
G
IG
IG
G
G
CONTAINER TYPE,PlG
W^, STEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HA VBLOCK NC 28532
A
A
A
E
E
E
CHEMICAL PRESERVATION
cz
o
(252> 444-6421
A -NONE D-NAOH
o
f o
z
Q
m
a
lu
Q
C
B-HNO E -HCL
COLLECTION
_ ~
�¢
w
"�
c�
o
w
Q,
�y
w
SO,
C- H SO F - ZINC ACETATE/NAC
H,
LOCATION
o¢
w
o
o
M
InA A
eq
Q
�
�
w
¢
G NATHIOSULFATE
DATE TIME
I. 0
aQ
Effluent
0�0 «
`
�I
15
1•
CLASSIFICATION
1
WASTEWATER (NPDES)
DRINKING WATER
DWQ/GW
i
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING 4 ' ENT/DELIVERY
Y N
SAMPLES
(Please
COL ECTED BY
Pnnt)
RELINQ HED S R) DATE/TIME
SAMPLES RECEIVED IN LA �� r(
11120M
DATERIME
COMMENTS
RE C BY (SIG)
0-36
511
Ye
D
RELINQUISH Y (SIG) DTE. [ME RECEI -D BY (SI )
DATEMME
BY (SIG) I DATE/TIME I RECEIVED BY (SIG)
PLEASE READ Instructions for completing this form on the reverse side Sampler must place a "C" for composite sample or a °G" for V "
=ORM 05
Grab samnlP In fhP hlnrkc ahrnia fnr cash noromnfnr rnn-fn I

1% hCoo mugW21
GREE ILLS N C 27835-7085
:11kti 11 WETp�
11i' fEWH-TFP TREATMENT ACAP!
f:, �s,� SOIV L�PT'J
Lfiluent
P �K,��lh�l fzRS
Anah sis Method
Date Nnah°st Gode
lnunonia Nitrogen as \, ml;/1
<0.04
0512,1715
R\D
350 1, R2-93
Total Kleldahl Nitrogen is 1,mg/l
't 57
05f27/15
RNI)
351 2 R2-93
uV'/trate-Nnrr(C ati \, n1k/1
5 66
05122/15
KI)B
353 2 R2-93
total Phosphorus as P, ink/I
2 1l
05/28/15
kKI;
365 4-74
()it R (,r(aj�C CHLM), nl�/1
<5 0
0512INS
SLI
1664B
Phenol, In, I
<5
06/06//15
X1'.1
420 ,1-78
Total Glanuicp mg 1
<0 005
(15/29/'15
SLJ
45000NE-99
l otal Hardness, m-, 1
110
0j1261,15
'I RB
2340(-'-97
Total 'Dn,ohCd Re.idue, mK/I
465
0512611,5
KKK
2540('.-97
kntunom, uh I
<3 0
051726/15
1, F.1
EPA200 8
Ar.uuc, u;;/l
<5.0
06/112/15
'\1'111
311:38-04
Bet N 11111111 m, I
<I 0
05129/15
I,F,I
CP4200.7
Gadnuum, ui
< 1 (1
06/01/15
111 11
311313-04
I otal Chromium. m, I
<5 0
05729/15
14.1
LPA200 7
(popper, ul;'I
< 10
()5129/15
1 1',1
LPA200.7
Lead. ❑g 1
<5 0
05/29/15
NI I iNs 1
:311313-04
Nickel, u►; I
< 10
05/29/15
IA
I,PA200 ,7
15CICC111In1 [w I
< 10
06/08/1 --;
M 111
311311-04
Slher', ug:l
<511
05129115
LIJ
LPA200.7
1 halhum, a /I
< 1 0
05126/15
LI..1
EPA200 8
Zinc. ugl
55
06/01/15
JAIN
3111B-99
DNE [phone]
FAX [phone]
ID#: 204 H
DATE COLLECTED: 05/20/15
DATE REPORTED : 07/14/15
REVIEWED BY; �'�/

Fp _ _ n L' it I it
PO BOX 7085 114 OAKMONT DRIVE PHONE (252) 756'6208
GREENVILLE N C 27835-7085 FAX [phone]
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
MR. ART HOUGH
WASTEWATER TREATMENT PLANT ANALYST: MAO
304 N. JACKSON DRIVE DATE COLLECTED: 05/20/15
HAVELOCK, NC 28532 DATE ANALYZED: 05,/;23/15
DATE REPORTED: 07/14/15
REVIEWED BY:'
VOLAT=LE' ORGANICS
EPA METHOD 624
P 1R ��ik 1 FRS, ug 1
�—
� I'(llnent
I
(_Jhloromethane
0 00
2
N mm I Chloride
< i0 00
3
Bromomethanc
i < lo oo
4
Chloroethane
<10 00
5
`I'ri(hlorofluorontrthan(i
-,5 00
6
1,1-1)1(hloroelhane
<5 00
7
11etli lene Ghlornie
< 10 00
8,
trans-1,2-Dichlorixthen6
<5 00
9
1,1-Di(hlorocathenQ
<, 00
10
(ahlorolorm
<5.00
11
1,1,1-Tri(hloroethan(,
<5 00
12
Garbon retrachlonde
<5.00
I3
Beniene
< 5 00
14
1,2-Dichloroethalm
<5 00
15,
'1 ri(hloroethem.
< 5 00 7
16
1,2-Dlchloropl opanc.
<5 00
17
Bromodlchloromethane
<1 00
18
2-ChloroethN h nn 1 Lther
< 5 00
19
cis-1,-Dtchk�ropropcne
<5-0()
20
`toluene
<5-00
21
trans-l,3-Di(hlor)piopcne
<5_00
22
1,1,2-1 nchloroetnane
< 5 00
23
Tetra,hloroethene
<,5,00
24
Dibromo(hloromohanoD
<5.o0
25
Chloroheni1•116
<5 00
26.
1, thv lben/enc
<5 00
27
Rromolorm
<5 00
28
1,1,2,2-Tetracehloroethane
<5.00
29
1,3-Dichlorobeni ene
< 5 110
1 30
1.4 -Di hlorobewene,
<;
3I
7,2-Dlctllol ohenc en"
< 5-oo
32
�(rolem
< 100 00 1
33
k(rvionitrile
<,511 ,00 1

oo��o�oor�� % hcoo T
GREENVILLE N C 27835-7085
moo
CLIENT: CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
REVIEWED BY: ✓�� �o� p�
SEMIVOLATILE ORGANICS
EPA METHOD 625
DNE [phone]
FAX [phone]
CLIENT ID: 204 H
ANALYST: CHS
DATE COLLECTED: 05/20/15 Page: 1
DATE EXTRACTED: 05/22/15
DATE ANALYZED: 06/18/15
DATE REPORTED: 07/14/15
1'AKA\Ih"I'F�RS, ugil
� hftlncnt
I
N-Nitrmochmeth\ lamme
< 10 00
2
Phenol
< 10 00
3
Bn(2-( hloroctln1) `Ether
< 10 00
4
2-(.hlorophenol
< 10 00
5
1,3-Dichlorohenicne
<10 110
1,4-Dichlorobeniene,
< 10 00
7
1,2-Dichlorobeniene
< 10 00
8
13is(2-(.hloroctiopropNU Lthcr
<1000
9
Hexachlorocthane
< 10 00
10
N- sitroso(h-N-Prol)vl.iminc
< 10 Olt
I l
Nitrobenzene
< I0.00
U
I.ophoronct
<1(l o0
1:
2-Nrtrophenol
< 10 00
14
2,4-Dunethylphenol
< IO 00
15
13n(2-Chloroetho\0 \leth.me
< 10 00
16
2,4-Dichlorophenol
< 10 00
17
1,2,4-Trichlorobcnmic
< 10 00
18
N'tphthalenc
< 10 00
19.
Hcxachlorobutadiene
< 10 00
20
4-Chloro-3-11ethN Iphenol
< 30.00
2,1
Hevachloro(Nclopentadtene
< 10 00
22
2,4,6-1 richlorophenol
< 10 00
21
2-( hloronaphth.denc
I < 10 00
24
\cenaphtliN lent
< 10.00
25
Dunetln Iphth.►late
< lo o0
26
2,6-Duntrotoulene
< 1(1.0(1
27
Acenaphthene
< to (10
28
2,4-Duutrophenol
<5O 00
29
4,Nrtrophenol
<5o00
30
2,4-Duutrotoluene
<10 . 00
I I
Rluorene �
< 10 00
32
Uie[hn Iphthalatc 1
< 10 00
33
4-C.hlorophem I Phenvl I"thc,r
< 10 00
34
4,6-Duutro-2-Nicth,.lphenol
<50 00
°t5
N-Nitrosochphemlanune
<1(1011
36
4-13romophent I Phenvi Lther
< 10 00
37
Hexaehlorobenienc
< 10 00
38
Pentachlorophenol
<50 00
39
Phenanthrene.
< 0.00
40
Anthracene
<10 00
41
Di-N-Buh Iphthalatc
< 10 00
42
Fluoranthene
< 10 00
43.
13cnndme.
< 100 00
44
PN rene.
< 10,00
45
13uh Ibenn 1phthlatc
< 10 00
46
Beniola]:cntltraccn4
< 10 00
47
3,3-Dichlorobeniadute
< 10 00
48
i
Glin,,ene
< 10 00

rr v
GREENVILLE N C 27835-7085
CLIENT: CITY OFHAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N., JACKSON DRIVE
HAVELOCK, NC 2,8532,E
REVIEWED B'Y:`°
SEMIVOLATILE ORGANICS
EPA METHOD 625
FAX [phone] ---
CLIENT ID: 204 H
ANALYST: CHS
DATE COLLECTED: 05/20/15
DATE EXTRACTED: 05/22/15
DATE ANALYZED: 06/18/15
DATE REPORTED:, 07/14/15
Page: 2
PARS'NIF rL,RS. Lig, J
l;fllucnt
49
liis(2-Eth�illexNl,)phthalate.
<20 00
50
Di-A-Oct)lphthalate
< 10 00
51
Beniolbjfluoranthene
< 10, 00
52
Benrolk1fluoranthene
< 10 00
53
Ben/ola]piienm
< 10,00
54
Indeno(1,2,3-(A)p- rene
< 10 00
55,
Dibenrol'a,hlantliracene
< 10 00
Ben/olg,h,i]perN lene
< 10 00
57-
1,2-Diphem Itivdrazin"
< 10 00
Page: 2

Environment 1, line.
PO Box 7037, 114 Oak1nollr T)r
Giccuvil1e. NC 27858
CRAIN OF CUSTODY RECORD
Page I of _ I
�u.u� uliouuiu I_iniY
Ul)LNI1A_ I R)N
Phone il252) 756-620 • Fax (252) 7i6-0633
CHLORINE NEUTRALIZED AT COLLECTION
CLJLC)kNt
,�
pHCHECK (LAB)
CLIENT: 204H Week: 23
f�
p
p
P
P
G
G
P
PP
CONTAINERTYPE P/G
CITY OF HAVELOCK
NONE
MR. ART HOUGH
P
G
G
G
G
G
G
WASTEWATER TREATMENT PLANT
('
304 N. JACKSON DRIVE t
(,fit
C
C
C
C
C
C
D
C
A
A
A
A
A
E
E
E
CHEMICAL PRESERVATION
HAVELOCK NC 28532
E
� A -NONE D -NADH
[phone]
6 HNO E HCL
J
L.
(r d
U
Q
Z
Cr
u
v
v
u
S
w
COLLECTION
y i
1�
`J
w
w
G
o
g
�
y
o
C9
c
0
�
C/)
c
,n
a
A
A
C
�,
A
A
w C H,SO, F -ZINC ACETA fE NP,OH
s G- NA THIOSULFATE
SAMPLE LOCATIONDATE
TIME
ti a
W Q
W
e
Effluent*Mr'i
e
15
w»a
' ;ra
F,
r;
� r�
;�;y
s
'
E
CLASSIFICATION
WASTEWATER (NPDES)
DRINKING WATER
DVVQIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES CO TE BY
(Please nnt)
7T]
SAMPLES RE EIV IN LAB AT�C
flELINOUISHED BY ($16b (5 PLEB)
D4,TETIME
RECEIV D -Y (SIG)
COMMENTS
AEICOUISH
�,DATSTNIMIE
�
Y IG)
OATEIFIME
RECEIVED BY (Si
DATE/TIME
RELINQUISHED BY tSIG)
DATFJTIME
RECEIVED BY (SIG)
DATETIME
PLEASE READ Instl uctlons foi completing this furm on the re7,else sida Sampler must place a 'C" for composite sample or a `G' for �`"�``'"'S Crab sample in the blocks above for each parameter requested N_ ? 845

w o T (� Dp ra— R p (� 0 n" Lol
?O BOX 7085 114 OAKMONT DRIVE
GREENVILLE N C 27835-7085
CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
PHONE [phone]
FAX [phone]
ID#: 204 H
DATE COLLECTED: 0'2/23/17
DATE REPORTED : 04/03/17
REVIEWED BY:
�� 2
Effluent
1nal�sis
Nle(hod
PARA\IL1'ERti
Dale
Anahsl
( o d u
lnnnoma Nitrogen as N, mg/l
0 06
02 24/17
AKS
350 1 R2-93
Total Kjeldahl Ndiogen as N,mg/l
0 91
02127/17
AKS
351 ', R2-93
Nitrate -Nitrite a. N. mg 1
1:7.1
02f2)41117
iN IP
353,.2 R2-93
1 otal Phosphorus as P, mg/I
1.26
02/27417
RA.1
3654-74
(')d R Greatiu (110r). mg/I
<5
02P24117
S,EJ
1664B
Phenol, ug 1
<5
03/01/17
SI -1
420.1-78
l'otal GNanulu, mg I
<0 005
03/02117
SE,1
4500CNE-99
Total Hardn"s, mg I
105
02/27 J7
KK'11
2340(-97
l'otal Diswh ed Residue, mg/I
444
02/28/17
SDB
254OC-97
AntmionN, ug 1
<3, 0
0324/17
,111N
EPA200 8
1rwmc, ug I
<5 0
03/07 17
'\l IM
311313-04
Berrllmm, ug 1
2
03/06/17
IaF.I
EPA200 7
Gadmlllm, ug 1
< 1 0
03/08/,17
'11TH
311311-04
'I oral (chromium, ug 1
<,5 0
03100 17
LFJ
EPA200.7'
(copper, ug I
< 10
03/06/17
LFJ
Ll'/X200.7
['.call, ug I
<5.0
03109/17
NIT11
31136-04
"SICKL1, ug I
<10
03/06/17
1, 'I
FPA200 7
Selennmi ug 1
< 10
03/15 17
N1`1 11
'3113B-0.1
5iher, ug/l
<5.0
03/0617
LFJ
EI'A2OO.7
fhalhum, ug I
< 1 0
03 23/,17
J'11h
EPA200.8
/im- ug I
70
03,106A7
LI I
EPA200 7
PHONE [phone]
FAX [phone]
ID#: 204 H
DATE COLLECTED: 0'2/23/17
DATE REPORTED : 04/03/17
REVIEWED BY:
�� 2

PO BOX 7085 114 OAKMONT DRIVE
GREENVILLE, N C 27835-7085
CLIENT: CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
r
REVIEWED BY:-
. o ,
VOLATILE ORGANICS
EPA METHOD 624
PHONE [phone];,
FAX [phone]
CLIENT I'D• 204 H
ANALYST:, MAO
DATE COLLECTED: 02/23/17
DATE ANALYZED: 03/08/17
DATE REPORTED: 04/03/17
PARANlbTlfliti, i►g/1'
k_filuent
1
Chloromethane
< 10 00
2.
Vinyl Chloride
< 10 00
3
Bromomethane.
< 10.00
�4
C;hloroethane
<,10 00
5
"1'n(.hlorofluorom�lhane;
<5 00
6
1,1-Dichloroethane
< 5,.00
7
llethNlene Chlonde
<10,00
8
tram-l.2-Dichlort)etheiie
<5 00
9
1,1-Dachloroethene
<5 00
10.
Chloroform
<5.00
11
1„1,1 -Trichloroethane
<5.00
12
Carbon letrachlorado
<5 00
13.
Ben/em;
<5 00
14
1,24* hloroethane
<5.00
15.
1 riddoroethene
<5 00
16
lag-Dichloropropane
<5 00
17.
Bromodichlorometh.ane
<5.00
18
2-ChloroethN 1N ini I Esther
<5'.00
19,
us-I3-Dichloropropene
<5.00
20,
Toluene
<5.00
21
tr.an-,-1,3-DichloropropEtic
<5 00
22,
1,1,2-1 richlorwthane
< 5.00
23
1 etra(hlorocthene
< 5 00
24
Dibromochloronwthane
<5 00
25
C hlorobeniene
<5.00
26
Eth%lben^rc "
<5 00
27-
Bromoform
<5 00
28'.1
1,1,2,2=Tetrachloro0hane
�<5 00
29.,
1,3-Dichlorobenfene
<5.00
30
1,4 -Dichlorobenzene
< 5.00
;1,
1.2 -Dichlorobenzene
<5 00
12
Acrole'm
<100.00
33
Acrvlon'Itr11G
<50.00

T 00 n»(�)ci 2 c 00 TF0(-io- �
u O BOX 7085 114 OAKMONT DRIVE
GREENVILLE N C 27835-7085
CLIENT: CITY OF HAVELOCK
MR. TIM WEBB
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK, NC 28532
1
REVIEWED BY:
SEMIVOLATILE ORGANICS
EPA METHOD 625
CLIENT ID:
PHONE [phone]
FAX [phone]
204 H
ANALYST: JAP
DATE COLLECTED: 02/23/17
DATE EXTRACTED: 02/27/17
DATE ANALYZED: 03/02/17
DATE REPORTED: 04/03/17
Page: 1
Effluent
PARA11L'1'FR5, uk/l
1
N-NUroso(luuethZ lan►me
< 10.00
2
Phenol
< 10-00
3
il►,42-Cohloroctlivi) Ether
< 10 00
4.
2 -Chlorophenol
< 10 00
5
,1,3-D►ehloroben/cm.
< ]0-0(1
6
1,4-D'►(hlot oben/cne
< 10.00
7
1,2-Duhlorobeniene
< 10.00
3.
i3�5(2-Chloro-i-methN lcthrl) Esther,
< 10 00
9
Hexachloroethane
< 10 00
IO
\ ;lrtrosod►-A-Prop%Immi to
< 10 00
11
N►trobeniene
<JO 00
12
lsophoromt
< 10 00
l3
2-A►trophenol
< 10 00
14
2,4-DunctliN 1phenol
< JO 00
15
Bis(2-ChloroethoxN) lletimne
< 10.00
16-
2,4-D►chlorophcnol
< 10, 00
17,
1,2,4-Tr►chlorobeniene
< 10 00
18.
FlN.iphthalene.
< 10 00
19
Hexachlorobutad►enc
< 10 00
20
4-CMoro-3-Meth 1phenol
<2000
21
ilexachlorocNclopentadicne
< 10 00
22
2,4,6-11►chlorophenol
<J0.00
'23.
2-Chloronaphthalene
< IO -00
24
A(enaphthvlenc
< 10.00
25
DlmethN Iphthalate
< 10 00
26
2,6-Dmrtrotoulen<
< 10 00
27
%cenaphthene
< 10 00
28
2;4-D►n►trophenol
< 50.00
29
.4-N►trophenol
<50 00
30
234-Dm►trotoluene
< 10 00
31,
Eluorene
< 10 00
32
D►ethn Iphthala(c
< 10 00
33
4-Ghlorophen} I Pl►eni 1 Cthet
< 10 00
34
4,6-Dinnro-2-Nlethviphenol
<50,00
35
lanune
< 10 00
36
4-BromophenN I PhenN I Esther
< 10-00
37.
Hexachlorobeniene
< 10.00
38.
Pentachlorophenol
< 50.00
39.
Phenanthrene
< 10 00
40
Anthracene
< 10.00
41
Di-N-But%Iphthalate
< 10 00
42
Eluoranthene
< 10.00
43
Bene►dme
< 100.00
44
I'v rene
< 10 00
45-
Butvibeimlphthlat"
<l0()(I
46
Beniolalanthra(ene
< 10.00
47
3.3-D►chlo►obeniadu►c
< 10 00
48
(,hr%tcne
< 10.110
Page: 1

c
U'WoRUM hooTpown�o
PO BOX 7085, 114 OAKMONT DRIVE
GREENVILLE, N C 27835-7085
PHONE [phone],
FAX [phone]
CLIENT: CITY OF HAVELOCK CLIENT TDs 204 H
MR. TIM WEBB
WASTEWATER TREATMENT PLANT ANALYST: JAP
304 N. JACKSON DRIVE DATE COLLECTED: 02/23/17 Page: 2
HAVELOCK, NC 28532 DATE EXTRACTED: 02/27/17
DATE ANALYZED: 03/02/17
REVIEWED BY,: ,=fir DATE REPORTED: 04/03/17
SEMIVOLATILE ORGANICS
EPA METHOD 625
PARA1l' -1 h,FZ ltg/l
Effluent
498�5�-E�th�lhe��'_�phthalatc:
<20.00
50
Di-N"L0ch Iphthslate
< 10.00
5'1
Ben^rQIbJtluoranthene
< 1000
52
flenioIkIfluoranthen4
< 10-00
51
Beniolall)N row
< 10.00
54
Indeno(l,2,-C,d)pN rent
< 10.00
-55
Dibeniola,hlanthra(ene
<< 10.00
56
lien/olg,h,ijpe,-N lene
< t0 00
57
1,p2-Diphcn%11ivdraiune
< 10M

I n%f1unnlcni I ('I-IAIN OF( -T4 IUl Idl',C'Okl)
(,i,t:n,ilk- A(,'7SSti
CA IIIdIIIkIItI IIIk. l,OII1
I)I�I\I I (,I I(=)\
Ph(,n, 25') 56 020,8 • I ' tO U(,
CHLORINE NEUTRALIZED AT COLLECTION
(.III t)I:I\I
�)
pHCHE K LAB
C1,1ENI: 20-1 H Week 12
F I
P
P
P
P
(`
WAINER TYPE P
CITY OF 111%,V1:1-0ch
'I
NIR UNI WE13a
HEMICAL PRESERVATION
WASTE N%'ATER 'FREA'1 NIE11 1'1,AN1'
304 N JACKSO'1 DRIVE
C
C
C
C
C
C
1)
C
A
A
k
A
A
E
E
E
HAVELOCK NC 28532
A NONE D NADH
[phone]
z-
w z
w
L.
„
r
N
"'
N
cn
w B HNO E HCL
2 Q
Z
z
L
O
_
!_
G
:7
4
I
7
'�
cc
Q LL
z
G
J
v
y
c
c
W
Lu
w C H SO F Z N A El ATE NA H
COLLE TION
w
LIJ `-
0
LL
0
`o
E
°
�
y
y
G
�
a
�
�
^
"
n
=
�,
�
=
N
N
,,
C
Q G NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
%
lO� U
3
4-
�--
Effluent
,r'�j
14
LASS FICATION
WASTEWATER NPDES
❑ DR NK NG WATER
DWQ,GW
SOLID WASTE SECTION
HAIN OF USFODY SEAL MIAIN(A NED
DUR NG SHIPMENT DE IVFRY
N
SAMPLES COLLECTED BY
Please Print
SAMPLES RECEIVED IN LAB AT �� C
RE N UISHED BY SIG SAMPLER
DATETIME
RECEIV SIG
ATE'TIME
COMMENTS
/�V2A
�?Sti
REUT�QUISHED BY SIG
DATETIME
RECE VED B" SIG
DATETIME
REL NQUISHED BY SIG
DATETIME
RECE VED BY IG
DATETIME
PLEASE READ lFStl Luctions fol comp eting thI o mo n the reve15e Side Sampler must place a C for composite sample or a G for
FORM Grab sample In the blocks above for each parameter requester: N ° 23 1 8 3

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Second Species Toxicity Testing Results 2017-2018
(Results will be submitted prior to the expiration of the existing NPDES Permit on 6/30/2018)

City of Havelock Wastewater Treatment Plant
City of Havelock, North Carolina
Exceptionally Performing Facilities, Reduction of Monitoring Frequency Analysis

Attachment A
Calculations for the City of Havelock WWTP Effluent Data for Monitoring Frequency Reduction Analysis
Date BOD, (Summer) BOD, (Winter) TSS NH3-NNH3-N (Winter) Fecal Coliform
(Summer)
Units me/L me/L me/L me/L me/L #/100 mL
3 -year average
258
341
260
012
008
192
No. data points
44600
28900
73400
44600
28900
71700
Monthly
Average Permit
5
10
30
05
1
35
Limit
Avg % of Permit
52%
34%
9%
24%
8%
5%
Limit
Sampling Results
11
9
0
4
0
2
> 200% of PL
Weekly Average
75
15
45
15
3
276
Permit Limit
Weekly Average
0
3
0
0
0
0
Violations in Past
Year

Attachment B
City of Havelock WWTP NPDES Permit Renewal Discharge Monitoring Report Data
10/1/2014 to 9/30/2017
Date
BODS (Summer)
BODS (Winter)
TSS
NH3-N
(Summer)
NHO (Winter)
Fecal Coliform
Units
mg/L
mg/L
mg/L
mg/L
mg/L
#/100 mL
10/1/2014
<2.0
<2.5
0.08
2
10/2/2014
<2.0
<2.5
011
<1
10/3/2014
<2.0
<2.5
<0 04
<1
10/4/2014
10/5/2014
10/6/2014
<2.0
<2.5
<0.04
<1
10/7/2014
Q.0
<2.5
<0 04
1
10/8/2014
<2 0
2.7
0.06
<1
10/9/2014
<2 0
<2 5
007
1
10/10/2014
2.9
Q.5
<0 04
1
10/11/2014
10/12/2014
10/13/2014
<2.0
3.8
<0.04
<1
10/14/2014
<2 0
<2 5
<0 04
<1
10/15/2014
<2 0
<2 5
008
<1
10/16/2014
<2 0
<2.5
<0 04
<1
10/17/2014
<2 0
<2 5
<0.04
1
10/18/2014
10/19/2014
10/20/2014
<2.0
<2 5
0.27
<1
10/21/2014
<2 0
<2 5
<0 04
3
10/22/2014
<2.0
<2 5
0.27
1
10/23/2014
<2 0
<2 5
0.07
1
10/24/2014
<2 0
<2.5
0.07
2
10/25/2014
10/26/2014
10/27/2014
<2 0
<2.5
0.05
<1
10/28/2014
<2 0
<2 5
0.05
3
10/29/2014
<2 0
<2 5
006
2
10/30/2014
<2 0
<2 5
007
3
10/31/2014
<2 0
<2 5
004
5
11/1/2014
11/2/2014
11/3/2014
3.2
<2 5
<0 04
1
11/4/2014
2.8
<2 5
0.06
5
11/5/2014
<2 0
<2 5
0.05
5
11/6/2014
<2 0
<2 5
0.07
1
11/7/2014
<2 0
<2 5
012
1
11/8/2014
11/9/2014
11/10/2014
2.5
<2.5
0.06
1
11/11/2014
11/12/2014
<2 0
<2 5
0.04
<1
11/13/2014
<2 0
<2 5
0.04
1
11/14/2014
3.6
<2 5
0.06
35
11/15/2014
11/16/2014
11/17/2014
11/18/2014
11/19/2014

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
NH3-N (Winter)
(Summer)
Fecal Coliform
11/20/2014
11/21/2014
11/22/2014
11/23/2014
11/24/2014
11/25/2014
11/26/2014
11/27/2014
11/28/2014
11/29/2014
11/30/2014
12/1/2014
29
6.0
006
<1
12/2/2014
<2.0
<2 5
007
<1
12/3/2014
<2 0
<2 5
0.04
2
12/4/2014
63
<2.5
<0 04
520
12/5/2014
<2.0
<2 5
0.06
11
12/6/2014
12/7/2014
12/8/2014
<2.0
<2.5
176
1
12/9/2014
<2 0
<2 5
033
<1
12/10/2014
3.0
<2 5
005
<1
12/11/2014
<2 0
<2 5
013
2
12/12/2014
<2 0
<2 5
Oil
14
12/13/2014
12/14/2014
12/15/2014
<2 0
<2 5
013
2
12/16/2014
<2.0
<2.5
014
<1
12/17/2014
<2.0
<2.5
0.11
<1
12/18/2014
<2 0
<2.5
<0 04
1
12/19/2014
<2 0
<2.5
<0 04
<1
12/20/2014
12/21/2014
12/22/2014
<2 0
<2.5
<0 04
<1
12/23/2014
25
<2 5
<0 04
7
12/24/2014
Q.0
<2 5
0.08
1
12/25/2014
12/26/2014
12/27/2014
12/28/2014
12/29/2014
<2 0
<2 5
0.07
1
12/30/2014
<2 0
<2.5
<0 04
2
12/31/2014
1/1/2015
1/2/2015
<2 0
<2.5
<0.04
<1
1/3/2015
1/4/2015
1/5/2015
<2.0
<2 5
0.04
1
1/6/2015
<2 0
<2 5
<0.04
3
1/7/2015
<2 0
<2 5
<0.04
3
1/8/2015
26
<2 5
<0 04
1
1/9/2015
<2.0
<2.5
0.04
1
1/10/2015
1/11/2015
1/12/2015
<2 0
<2 5
0.07
<1

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
NH37N (Winter)
(Summer)
Fecal Coliform
1/13/2015
<2.0
<2 5
0.06
<1
1/14/2015
<2 0
<2.5
0.09
2
1/15/2015
<2 0
<2 5
<0 04
1
1/16/2015
<2 0
<2 5
<0 04
<1
1/17/2015
1/18/2015
1/19/2015
1/20/2015
<2 0
<2.5
0.11
<1
1/21/2015
<2.0
<2.5
0.23
<1
1/22/2015
<2.0
<2 5
<0 04
<1
1/23/2015
<2.0
<2 5
<0 04
<1
1/24/2015
1/25/2015
1/26/2015
<2 0
<2 5
<0.04
1
1/27/2015
<2 0
<2.5
007
<1
1/28/2015
3.2
<2 5
010
8
1/29/2015
<2 0
<2.5
0.27
1
1/30/2015
<2 0
<2.5
<0 04
<1
1/31/2015
2/1/2015
2/2/2015
2/3/2015
<2.0
<2.5
<0.04
<1
2/4/2015
<2.0
<2 5
030
<1
2/5/2015
Q.0
110
Oil
1
2/6/2015
<2.0
<2 5
009
<1
2/7/2015
2/8/2015
2/9/2015
<2 0
<2 5
007
<1
2/10/2015
<2 0
<2.5
0.09
<1
2/11/2015
<2 0
Q.5
<0.04
<1
2/12/2015
<2.0
<2.5
009
1
2/13/2015
<2 0
<2.5
<0.04
5
2/14/2015
2/15/2015
2/16/2015
<2 0
<2.5
0.07
<1
2/17/2015
2.9
3.4
<0.04
5
2/18/2015
<2.0
<2.5
<0 04
<1
2/19/2015
<2.0
Q.5
<0 04
<1
2/20/2015
2/21/2015
2/22/2015
2/23/2015
2/24/2015
2/25/2015
2/26/2015
<2 0
<2.5
<0 04
1
2/27/2015
<2 0
<2 5
0.10
<1
2/28/2015
3/1/2015
3/2/2015
<2 0
<2 5
<0.04
<1
3/3/2015
<2 0
<2.5
005
<1
3/4/2015
<2 0
<2 5
0.05
<1
3/5/2015
<2 0
<2.5
0.08
1
3/6/2015
<2.0
<2.5
019
1
3/7/2015

Date
BODS (Summer)
BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter)
Fecal Coliform
3/8/2015
3/9/2015
<2 0
<2.5
0.20
<1
3/10/2015
<2 0
<2 5
<0.04
<1
3/11/2015
2.9
Q.5
010
<1
3/12/2015
<2 0
<2.5
<0.04
1
3/13/2015
Q.0
<2.5
006
<1
3/14/2015
3/15/2015
3/16/2015
<2.0
<2.5
013
<1
3/17/2015
<2.0
Q.5
011
<1
3/18/2015
<2.0
<2.5
0.63
<1
3/19/2015
<2.0
<2 5
0.63
<1
3/20/2015
<2.0
<2.5
0.20
2
3/21/2015
3/22/2015
3/23/2015
<2.0
<2 5
0.10
<1
3/24/2015
72
<2 5
Oil
<1
3/25/2015
<2.0
<2.5
013
<1
3/26/2015
<2.0
Q.5
007
<1
3/27/2015
<2.0
<2 5
007
<1
3/28/2015
3/29/2015
3/30/2015
<2 0
<2 5
<0 04
<1
3/31/2015
<2 0
<2.5
<0 04
<1
4/1/2015
Q.0
<2.5
0.07
<1
4/2/2015
<2.0
<2.5
010
4
4/3/2015
4/4/2015
4/5/2015
4/6/2015
<2 0
<2.5
037
<1
4/7/2015
<2 0
<2 5
Oil
<1
4/8/2015
<2 0
<2.5
007
<1
4/9/2015
<2.0
<2.5
011
3
4/10/2015
<2.0
<2 5
008
3
4/11/2015
4/12/2015
4/13/2015
<2 0
<2 5
014
0
4/14/2015
<2.0
<2.5
0.20
3
4/15/2015
2.2
<2.5
0.13
<1
4/16/2015
<2 0
<2.5
0.06
<1
4/17/2015
Q.0
<2.5
0.06
<1
4/18/2015
4/19/2015
4/20/2015
11.0
<2 5
0.08
1
4/21/2015
12.0
<2 5
<0 04
<1
4/22/2015
>15*
<2 5
<0.04
3
4/23/2015
>11*
<2 5
0.10
6
4/24/2015
4/25/2015
4/26/2015
4/27/2015
<2 0
<2.5
012
<1
4/28/2015
5.5
<2.5
014
<1
4/29/2015
<2 0
<2.5
0.09
<1
4/30/2015
<2 0
<2.5
0.08
12

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter) Fecal Coliform
5/1/2015
<2
<2.5
006
2
5/2/2015
5/3/2015
5/4/2015
< 2
< 2.5
0.06
<1
5/5/2015
< 2
< 2.5
0.09
<1
5/6/2015
< 2
< 2.5
008
8
5/7/2015
2.5
< 2.5
Oil
1
5/8/2015
< 2
< 2.5
0.2
4
5/9/2015
5/10/2015
5/11/2015
< 2
< 2 5
0.11
17
5/12/2015
< 2
< 2.5
018
5/13/2015
< 2
< 2.5
017
1
5/14/2015
< 2
< 2 5
< 0 04
< 1
5/15/2015
27
< 2 5
018
< 1
5/16/2015
5/17/2015
5/18/2015
21
< 2.5
0.05
< 1
5/19/2015
< 2
< 2 5
< 0.04
< 1
5/20/2015
3.5
8.3
< 0 07
2
5/21/2015
< 2
< 2 5
< 0.04
3
5/22/2015
< 2
< 2.5
006
< 1
5/23/2015
5/24/2015
5/25/2015
5/26/2015
3.4
< 2 5
< 0.04
5
5/27/2015
< 2
<25
0.91
4
5/28/2015
< 2
< 2 5
007
2
5/29/2015
<2
<2.5
0.08
< 1
5/30/2015
5/31/2015
6/1/2015
> 26
3.5
008
1
6/2/2015
> 13
<25
0 07
1
6/3/2015
> 13
< 2.5
01
2
6/4/2015
> 13
< 2.5
009
3
6/5/2015
> 13
<2.5
0.07
6/6/2015
6/7/2015
6/8/2015
2.5
<2.5
011
3
6/9/2015
<2
<2 5
005
< 1
6/10/2015
< 2
< 2.5
005
3
6/11/2015
< 2
< 2.5
< 0 04
6
6/12/2015
<2
<2 5
01
1
6/13/2015
6/14/2015
6/15/2015
< 2
< 2 5
0.09
5
6/16/2015
<2
<2 5
0.13
3
6/17/2015
<2
<2 5
0.12
23
6/18/2015
<2
<2 5
007
5
6/19/2015
<2
<2.5
006
< 1
6/20/2015
6/21/2015
6/22/2015
< 2
< 2 5
< 0 04
9
6/23/2015
<2
<2.5
019
6

00
\
00
\
00
\
OD
\
00
\
00
\
00
\
OO
OO
OO
OD
OO
OO
OO
OO
OO
V
\
V
\
V
\
V
\
J
\
J
\
V
\
V
\
J
\
V
\
J
\
V
\
J
\
V
\
V
\
V
\
J
\
J
\
V
\
V
\
V
\
V
\
J
V
V
V
V
J
J
V
V
07
\
01
\
O1
\
Q7
\
01
\
0l
\
Q1
\
I-+-
M
N
Ln
N
A
N
W
F-•
N
N
N
N\\\\\\\\\
O
UJ
00
V
Cl
Ul
A
W
N
N
W
F�
W
O
N
W
N
W
N
J
N
M
N
W
N
A
N
W
N
N
N
N
N
O
N
W
I--�
00
F-•
V
F-�
M
F-•
V7
N
A
I--'
W
F-�
N
N
N
N\\\\\\\\\
O
l0
00
V
01
U7
A
W
N
F+
W
O
N
l0
N
00
N
V
N
Cl)
N
Ln
N
A
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
Ol
0
0
0
0
0
0
0
O
O
O
O
O
O
O
N
O
O
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
O
F,
O
F-�
O
N
O
N
O
F,
O
F,
O
O
O
N
0
0
0
0
0
0
0
4�
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
N
W
F,
U'I
F,
Ul
lJl
Ul
lJl
w
W
W
Ul
Ul
N
U1
W
Ut
111
Ul
N
111
N
Ul
U7
l71
Ul
V7
Ul
Ul
Ul
Ul
Ut
Ul
Ul
In
V7
Ul
U7
U'1
Ul
U1
U7
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
O
v
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Ul
A
A
A
A
A
A
A
N
A
A
A
A
A
A
A
A
A
A
A
A
A
H
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
W
N
N
N
N
N
N
N
W
N
N
N
N
N
N
N
N
N
N
N
N
N
3
3
00
O
v
NS
1
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
W
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
n7
N
N
N
to
Ul
Ul
Ul
In
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
1n
Ul
w
Ul
Ul
U1
Ul
Ul
Ul
U1
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ln
Ul
Ul
Ul
(n
H
H
O
O
AO
O
O
F+
O
A
o
O
O
O
O
O
N
O
O
O
O
O
O
O
O
A
O
A
o
A
0
O
O
O
A
0
A
0
O
O
O
A
0
O
O
O
C Z
3 s
00
000
JN
000
0���.
-+
wN
~'
"C)
oN
0000
?
000
J
01
l77
00ui
Cl
lJl
U7
3 w
A
Ln
V
J
J
F-�
A
Ol
Ul
W
N
W
N
Ql
N
N
Cl)
J
O?
00
01
V
A
fD Z
Z
w
CZ
G
7
fD
T
n
n
m
W
w
m
w
Ln
N
F'
N
W
V
N
w
O
N
A
N
O
UlJ
F-�
00
Ul
V
w
01
l--•
J
A
O
m
00
m
w
m
n
O
N
J
N
l0
E-+
J
O
3

F�
"
�-
�,
�--
�--
�,
"
�
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
w
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
--
0
0
0
0
0
0
0
0
0
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
\
N
\
N
\
N
\
N
N
\\\\\\\\
--
W
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
F�
N
N
\
\
\
\
\
\
\
\
\
W
W
N
N
N
N
N
Ul
N
A
N
W
N
I--'
O
l0
00
V
v
l0
00
V
Ol
l!1
A
W
N
F-�
O
l0
\
00
\
V
\
01
\
W
\
A
\
W
\
N
\
F+
\
O
l0
\
00
00
\
V
\
Cl)
\
W
\
A
\
W
\
N
\
F-�
\
O
\
�'
\
O
\
W
\
00
\
V
\
Cl
\
\
\
\
\
\
\
\
\
\
03
\
N
\
N
\
N
\
NN
\
\
N
\
N
\
N
\
N
\
N
N
N
N
N
N
N
N
N
N
\
N
N
N
N
N
N
N
N
N
N
N
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
N
NN
N
N
N
N
NN)
N
N
N
N
N
"
m
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
o
O
O
O
O
O
O
O
O
O
F-'
N
N
N
N
N
N
O
O
o
O
O
O
O
O
O
O
O
O
O
O
O
N
N
N
N
N
N
N
N
H
H
N
N
N
N
N
N
N
N
Ul
Ul
W
W
NLrl
W
LPA ,
Ul
N
N
N
N
N
N
N
N
W
w
w
W
U1
Ln
W
Ul
w
Ul
w
Ul
w
Ul
w
U7
Ul
Ul
Ul
w
U7
w
l/'I
{A
Ul
U7
Ul
Ul
U7
Ul
V7
Ul
w
Ul
w
U7
Ul
W
Ul
U1
w
Ul
Uf
Ln
Ul
Ln
11l
Ul
Ln
Ui
Ul
Ul
Ul
Ul
ll1
l!1
Ul
w
Ul
Vl
W
Ul
O
v
N
A
A
A
A
A
A
A
A
KJA
A
A
N
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
V1
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
C
3
3
�o
0
v
rr
fD
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
N
N
N
N
N
N
N
N
W
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
LA
Ul
Ul
Ul
Ul
Ul
In
Ul
Ln
Ul
Ln
Ln
N
Ut
Ln
Ul
M
Ul
In
l!7
Ln
N
U7
In
Ul
Ul
Ul
l!l
Ul
l!1
Ul
In
Ul
111
111
Ul
In
Ul
V7
H
N
A
0
A
0
OA
A
0
A
0
A
0
A
0
A
o
OA
A
o
A
o
A
o
A
0
A
00
OOA
OAA
O
0
W
O
O
O
O
O
O
O
O
O
O
O
A
0
O
O
O
=
C
O
W
0
O
O
O
O
A
O
O
O
N
0,
V
O
O
O
00
W
N
O
00
O
00
O
l0
O
00
O
V
O
00
O
V
O
V
O
V
00
O
O
0
O
0
O0
0
wZ
A
A
A
A
A
l0
A
A
A
A
mZ
Z
2
W
sZ
r
rt
fD
n
d
A
A
V-�
A
m
W
Ul
W
A
N
N
M
A~
W
N
F-`
N
N
N
~
N
N
N
N
W
W
A
Ul
N
n
O
N
N
f-+
O
O
3

Date
BODS (Summer)
BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter)
Fecal Coliform
10/10/2015
10/11/2015
10/12/2015
< 2
< 2.5
< 0.04
< 1
10/13/2015
< 2
< 2.5
017
< 1
10/14/2015
< 2
< 2.5
0.04
< 1
10/15/2015
< 2
< 2.5
006
2
10/16/2015
< 2
< 2.5
006
< 1
10/17/2015
10/18/2015
10/19/2015
< 2
< 2.5
0.07
8
10/20/2015
< 2
< 2.5
0.07
4
10/21/2015
< 2
< 2.5
0.10
< 1
10/22/2015
< 2
< 2 5
< 0 04
< 1
10/23/2015
< 2
< 2 5
005
2
10/24/2015
10/25/2015
10/26/2015
< 2
< 2.5
005
< 1
10/27/2015
< 2
< 2 5
006
1
10/28/2015
< 2
< 2.5
0.05
1
10/29/2015
< 2
< 2.5
005
< 1
10/30/2015
< 2
< 2 5
0.09
<1
10/31/2015
11/1/2015
11/2/2015
<2
< 2 5
0.04
4
11/3/2015
<2
<2 5
0.14
3
11/4/2015
< 2
< 2 5
0.05
2
11/5/2015
< 2
< 2 5
< 0.04
1
11/6/2015
< 2
< 2 5
0.04
< 1
11/7/2015
11/8/2015
11/9/2015
<2
<2.5
<0 04
11/10/2015
< 2
< 2.5
< 0 04
2
11/11/2015
11/12/2015
< 2
< 2.5
< 0.04
11/13/2015
< 2
< 2 5
< 0.04
< 1
11/14/2015
11/15/2015
11/16/2015
< 2
< 2.5
< 0.04
< 1
11/17/2015
<2
<2.5
<0.04
< 1
11/18/2015
2.4
< 2.5
0.4
< 1
11/19/2015
< 2
< 2.5
005
0
11/20/2015
< 2
< 2.5
0.04
2
11/21/2015
11/22/2015
11/23/2015
< 2
< 2.5
007
< 1
11/24/2015
< 2
< 2 5
< 0 04
11/25/2015
< 2
< 2 5
< 0 04
1
11/26/2015
14
11/27/2015
11/28/2015
11/29/2015
11/30/2015
<2
<2 5
0.07
< 1
12/1/2015
<2
< 2 5
< 0.04
< 1
12/2/2015
<2
<2 5
0.04
4

Date
BODS (Summer) BODS (Winter)
TSS
NH3-NNH3-N (Winter)
(Summer)
Fecal Coliform
12/3/2015
<2
<2 5
<0.04
2
12/4/2015
<2
< 2.5
<0.04
3
12/5/2015
12/6/2015
12/7/2015
3.2
<2.5
0.04
2
12/8/2015
< 2
< 2.5
0.05
< 1
12/9/2015
< 2
< 2.5
< 0 04
< 1
12/10/2015
< 2
< 2.5
< 0 04
< 1
12/11/2015
< 2
< 2.5
< 0.04
< 1
12/12/2015
12/13/2015
12/14/2015
<2
<2 5
<0 04
1
12/15/2015
< 2
< 2.5
< 0 04
1
12/16/2015
<2
<2.5
<0 04
< 1
12/17/2015
< 2
< 2.5
< 0 04
1
12/18/2015
< 2
< 2.5
< 0.04
< 1
12/19/2015
12/20/2015
12/21/2015
< 2
< 2.5
< 0 04
< 1
12/22/2015
< 2
< 2.5
< 0 04
< 1
12/23/2015
< 2
< 2.5
< 0.04
< 1
12/24/2015
12/25/2015
12/26/2015
12/27/2015
12/28/2015
25
< 2 5
< 0 04
1
12/29/2015
< 2
< 2 5
< 0 04
< 1
12/30/2015
< 2
< 2 5
< 0 04
1
12/31/2015
< 2
< 2 5
< 0.04
< 1
1/1/2016
1/2/2016
1/3/2016
1/4/2016
< 2
< 2.5
< 0.04
< 1
1/5/2016
4
< 2 5
< 0.04
1
1/6/2016
< 2
< 2 5
< 0.04
< 1
1/7/2016
< 2
< 2 5
< 0.04
1
1/8/2016
< 2
< 2 5
< 0 04
1
1/9/2016
1/10/2016
1/11/2016
< 2
< 2 5
< 0 04
< 1
1/12/2016
< 2
< 2.5
0.05
< 1
1/13/2016
< 2
< 2.5
0.07
< 1
1/14/2016
< 2
< 2.5
< 0.04
1
1/15/2016
< 2
< 2.5
< 0.04
< 1
1/16/2016
1/17/2016
1/18/2016
1/19/2016
< 2
< 2.5
< 0.04
< 1
1/20/2016
< 2
< 2.5
< 0 04
2
1/21/2016
< 2
< 2 5
< 0.04
< 1
1/22/2016
< 2
< 2.5
< 0.04
< 1
1/23/2016
1/24/2016
1/25/2016
< 2
< 2 5
< 0.04
11

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N NH3-N (Winter)
(Summer)
Fecal Coliform
1/26/2016
< 2
< 2.5
< 0.04
2
1/27/2016
< 2
< 2.5
< 0.64
4
1/28/2016
83
0.0811
5
1/29/2016
26
< 2.5
006
20
1/30/2016
1/31/2016
2/1/2016
< 2
<25
0 09
649
2/2/2016
67
10
0.18
6
2/3/2016
< 2
< 2 5
006
1
2/4/2016
4
6.5
0.18
10
2/5/2016
<2
2.7
0.12
9
2/6/2016
2/7/2016
2/8/2016
< 2
< 2.5
< 0 04
1
2/9/2016
< 2
10
0.04
< 1
2/10/2016
< 2
< 2.5
< 0 04
1
2/11/2016
< 2
< 2.5
< 0 04
1
2/12/2016
< 2
< 2.5
< 0 04
1
2/13/2016
2/14/2016
2/15/2016
<2
< 2 5
0.11
< 1
2/16/2016
< 2
< 2 5
0.05
2
2/17/2016
<2
< 2 5
<0 04
< 1
2/18/2016
< 2
< 2 5
0.07
1
2/19/2016
< 2
< 2 5
0.05
1
2/20/2016
2/21/2016
2/22/2016
<2
< 2 5
0.05
< 1
2/23/2016
<2
< 2.5
005
< 1
2/24/2016
< 2
< 2.5
007
2
2/25/2016
< 2
< 2.5
006
1
2/26/2016
< 2
< 2.5
009
1
2/27/2016
2/28/2016
2/29/2016
4
< 2 5
005
1
3/1/2016
< 2
< 2.5
0.07
1
3/2/2016
3.5
< 2 5
006
1
3/3/2016
< 2
< 2 5
0.06
< 1
3/4/2016
< 2
< 2.5
0.04
< 1
3/5/2016
3/6/2016
3/7/2016
< 2
< 2.5
< 0 04
1
3/8/2016
< 2
< 2 5
005
< 1
3/9/2016
< 2
< 2.5
007
24
3/10/2016
< 2
< 2 5
005
< 1
3/11/2016
< 2
3.7
006
< 1
3/12/2016
3/13/2016
3/14/2016
< 2
< 2.5
005
< 1
3/15/2016
< 2
< 2 5
0.08
1
3/16/2016
37
< 2.5
0.09
1
3/17/2016
< 2
< 2 5
0.04
< 1
3/18/2016
< 2
< 2.5
0.07
2
3/19/2016

to
to
U1
W
W
U'1
A
A
A
A
A
\
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
w
w
w
w
w
W
w
w
w
w
w
w
\
N
\
N
\
N\\\\\\\\\
\
W
\
N
\
N
\
N
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
I--'
\
N
\
N
\
F-+
\
N
\
I--�
\
N
\
F-�
\
F-+
\\\\\\\\\
\
W
\
W
\
N
\
N
\
N
\
\
\
N
\
N
\
N
\
N
\
N
N
N
O
lO
00
J
Ol
U'1
A
W
N
I-�
O
W
M
J
M
111
A
W
N
N
O
W
M
J
M
U7
A
W
N
I--�
O
l
00
V
Ol
l/'1
A
W
N
N
N
O
w
w
V
N
m
N
w
A
W
N
N
O
v
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
N
N
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
0
N
N
N
N
N
N
N
N
N
N
N
N
M
O
O
O
N
N
N
N
F+
N
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
N
N
N
N
F-)
N
O
O
O
O
O
O
O
O
O
O
O
O
�p
N
N
N
Ql
m
Ol
a)
O1
Ol
m
Ol
Ol
01
01
Ol
N
N
N
N
N
N
N
Ql
Ol
0)
01
Ol
M
01
M
01
01
Cl)
01
N
N
N
hm
Ol
Ol
Ol
Ql
Ol
Ol
Ol
m
Ql
m
Ol
01
01
Ql
01
Ql
C)
Ol
0)
Ol
Ql
m
Ol
Ol
m
Ol
G)
Ql
Ql
0)
Ol
Ol
D1
cn
Ql
m
cn
Ol
Ol
cn
Ol
cn
Ol
Ol
cn
Ql
Ol
m
Ql
Ol
Ol
m
O
v
A
A
A
w
A
A
n
A
n
n
n
A
n
N
A
n
n
A
N
A
A
A
A
A
N
n
A
A
A
A
y
N
N
N
V
N
N
N
N
N
N
N
N
N
C
N
N
N
N
C
N
N
N
N
N
N
N
N
N
N
C
3
3
ro
O
v
A
A
N
A
n
A
A
A
N
N
Cl)
N
N
N
N
Ni
7
.M
m
A
n
n
A
A
A
n
A
n
A
A
n
n
A
n
A
n
A
n
A
A
A
A
A
A
A
A
A
A
A
A
n
A
A
A
A
n
A
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
W
N
N
N
N
y
w
w
w
w
w
w
w
w
w
w
W
In
w
w
U'1
Ul
Ul
Ul
Ul
In
W
Ul
W
w
N
w
w
w
Ul
U'1
Ul
Ul
Ln
Ul
W
U7
Ul
y
y
O
O
C
O
O
O
O
O
O
O
O
O
O
O
O
O
O
0
0
0
0
0
0
0
0
0
O
C Z
0
0
0
0
0
0
O
1-A
0
C
ON
o
o
o
o
00000
CDOOM
O
3 =
U'1
Ul
A
A
V
V
Ol
w
00
00
0
N
V
LO
Ol
In
V
A
V
Ol
0)
A
U'1
U9
l0
m
00
fD Z
Z
2
w
O
O
O
O
O
O
O
O
OJ
~'
~'
W
A
cZ
LOO
wOn
G
7
M
fD
T
n
m
n
A
nn
N~+
~+~+
n
I--'
n
A
n
n
A
A
n
N
n
n
n
N
n
N
�'
n
n
n
ni
n
A
n
n
n
n
F+
F,
N
CD
—
O
3

Cl)
M
m
m
m
m
M
m
m
m
Q1
0
0
0
0
Ol
m
m
m
m
m
m
M
m
M
Ol
01
M
01
01
Ul
w
Ul
W
U7
Ul
W
Ul
W
W
Ul
w
Ul
Ul
Ul
N
Ul
Ul
Ul
V
Ul\
V
V
\\\
V
V
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\\\\
\
\
W
\
W
\
\
\
\
\
\
\
N
\
N
\
N
\
N
\
F -A
\
N
\
I -A
\
F--
\
\
\
Ul
\
A
\
W
\
N
\
F-'
\
W
O
N
l0
N
00
N
V
N
01
N
Ul
N
A
N
W
N
N
N
F+
N
O
N
l0
N
00
F-�
V
N
QI
N
Ul
N
A
I-�
W
N
N
F-'
N
H\\\\
O
l0
\
DD
\
V
\
Q1
\
Ul
\
A
\
W
\
N
\
N
\
F-+
O
N
l0
N
00
Si
V
N
O1
N
V7
N
A
W
N
\
F'
\
O
\
l0
\
00
\
V
\
Qt
\
Ul
\
A
W
G
Ol
N
N
N
N
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
N
N
N
N
N
N
N
N
\
N
\
N
A
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
OO
OO
N
0)m
N
01
N
cn
NNm
N
N
N
F -A
F-'
1--'
N
N
N
F-'
N
M
M
M
M
m
M
0)
M
m
N
N
N
F-`
N
F'
"
Ol
0
0
0
0
M
01
01
M
m
M
M
m
m
m
m
m
m
m
mO
M01
M
m
m
M
m
0)
M
M
01
Ol
m
01
m
M
0
0
0
N
V
A
W
A
A
N
A
A
A
A
A
N
A
A
N
A
W
W
A
W
W
N
N
A
N
A
A
A
N
A
A
A
N
A
(/f
A
N
Ln
N
N
M
N
N
N
N
F'
N
Ul
N
N
W
N
N
W
LO
A
N
00
N
m
N
N
N
N
N
N
N
U7
N
3
�o
O
0
�o
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
A
N
W
Ul
Ul
Ul
Ul
Ul
Ul
U7
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
Ul
W
U1
Ul
Ul
Ul
Ul
Ul
Ul
in
Ul
Ul
Ul
H
O
O
O
O
O
O
O
O
O
O
O
A
O
A
A
A
0
A
0
O
O
O
A
0
O
O
O
O
O
O
O
O
O
A
0
A
0
O
O
O
C Z
3=
N
o
0
0
0
o
i-•
i--�
o
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
o
0
3
M
W
w
M
V
00
M
N
00
V
01
A
m
A
.OP
C
A
00
A
U7
U7
00
V
M
Ul
V
m
V
A
A
A
W
Ul
Z
M
S
w
Cz
G
7
e*
fD
T
fD
n
d
V
W
N
A
N
N
N
N
Ul
W
N
N
N
A
V
N
N
N
A
W
l0
A
A
A
F-+
N
N
A
F+
A
F-'
W
A
W
N
A
r1
O
3

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter) Fecal Coliform
7/6/2016
< 2
< 2.5
Oil
8
7/7/2016
22
< 2 5
< 0 04
4
7/8/2016
< 2
< 2 5
0.09
3
7/9/2016
7/10/2016
7/11/2016
< 2
< 2.5
0.26
4
7/12/2016
< 2
<25
0.07
3
7/13/2016
< 2
< 2 5
0.08
2
7/14/2016
< 2
< 2 5
008
3
7/15/2016
< 2
< 2 5
0.11
4
7/16/2016
7/17/2016
7/18/2016
< 2
< 2.5
0.06
63
7/19/2016
< 2
< 2 5
0.08
231
7/20/2016
< 2
< 2.5
< 0 04
6
7/21/2016
< 2
< 2 5
0.05
9
7/22/2016
24
< 2.5
< 0 04
3
7/23/2016
7/24/2016
7/25/2016
2.4
< 2.5
004
42
7/26/2016
< 2
< 2.5
< 0.04
35
7/27/2016
< 2
< 2.5
< 0 04
< 1
7/28/2016
2.3
< 2.5
004
1
7/29/2016
28
< 2.5
005
4
7/30/2016
7/31/2016
8/1/2016
2.7
< 2.5
007
2
8/2/2016
2.8
< 2.5
008
1
8/3/2016
3.7
< 2.5
Oil
1
8/4/2016
3
< 2.5
012
1
8/5/2016
4.6
< 2.5
009
1
8/6/2016
8/7/2016
8/8/2016
3.9
< 2.5
012
< 1
8/9/2016
3.2
< 2.5
008
2
8/10/2016
2.8
< 2.5
0.08
3
8/11/2016
<2
< 2.5
0
2
8/12/2016
< 2
< 2.5
0.12
< 1
8/13/2016
8/14/2016
8/15/2016
27
<2.5
0.05
1
8/16/2016
<2
<2.5
0.05
1
8/17/2016
< 2
< 2.5
< 0.04
4
8/18/2016
<2
< 2 5
< 0 04
7
8/19/2016
2.5
< 2 5
007
8/20/2016
8/21/2016
8/22/2016
96
3.6
0.07
58
8/23/2016
4.4
2.9
012
d
8/24/2016
2.7
5.8
017
18
8/25/2016
4.2
< 2 5
013
4
8/26/2016
2.8
<25
0.1
2
8/27/2016
8/28/2016

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter) Fecal Coliform
8/29/2016
3.7
<2 5
006
6
8/30/2016
2.5
<25
< 0 04
2
8/31/2016
28
<2 5
<0.04
7
9/1/2016
26
< 2 5
006
6
9/2/2016
26
< 2 5
004
11
9/3/2016
9/4/2016
9/5/2016
9/6/2016
2.3
<25
0 07
154
9/7/2016
< 2
<25
0.06
9
9/8/2016
< 2
<25
< 0 04
7
9/9/2016
< 2
< 2.5
005
2
9/10/2016
9/11/2016
9/12/2016
< 2
28
0.06
25
9/13/2016
< 2
< 2.5 -
0.06
16
9/14/2016
<2
<2.5
007
13
9/15/2016
< 2
< 2.5
0.08
6
9/16/2016
< 2
< 2 5
0.09
5
9/17/2016
9/18/2016
9/19/2016
53
< 2.5
012
1
9/20/2016
<2
<2 5
0.06
14
9/21/2016
3.2
< 2 5
008
2
9/22/2016
< 2
< 2.5
Oil
1
9/23/2016
< 2
< 2 5
004
< 1
9/24/2016
9/25/2016
9/26/2016
< 2
< 2 5
< 0 04
1
9/27/2016
3.8
<2.5
004
< 1
9/28/2016
< 2
< 2 5
< 0 04
< 1
9/29/2016
< 2
< 2.5
< 0 04
1
9/30/2016
<2
<2.5
<0 04
1
10/1/2016
10/2/2016
10/3/2016
2.5
28
< 0.04
< 1
10/4/2016
<2
<2.5
0 060
1
10/5/2016
< 2
< 2.5
< 0.04
< 1
10/6/2016
3.2
<2,5
<0 04
< 1
10/7/2016
43
<2.5
<0 04
< 1
10/8/2016
10/9/2016
10/10/2016
<2
<2 5
<0.04
1
10/11/2016
< 2
< 2 5
< 0 04
< 1
10/12/2016
< 2
<25
< 0.04
3
10/13/2016
<2
< 2 5
< 0 04
< 1
10/14/2016
<2
< 2,5
< 0 04
< 1
10/15/2016
10/16/2016
10/17/2016
<2
<2.5
004
1
10/18/2016
<2
<25
0 04
1
10/19/2016
< 2
< 2 5
006
< 1
10/20/2016
< 2
< 2 5
0.05
< 1
10/21/2016
2 4
< 2 5
007
1

Date
BODS (Summer)
BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter)
Fecal Coliform
10/22/2016
10/23/2016
10/24/2016
2.1
<25
0.07
< 1
10/25/2016
2.2
<25
0.05
4
10/26/2016
<2
<2 5
0
< 1
10/27/2016
< 2
< 2.5
< 0 04
< 1
10/28/2016
<2
<2.5
006
1
10/29/2016
10/30/2016
10/31/2016
< 2
2.7
0.05
< 1
11/1/2016
<2
< 2.5
< 0 04
1
11/2/2016
9
< 2.5
006
< 1
11/3/2016
8.7
< 2 5
005
24
11/4/2016
96
<25
0 14
1
11/5/2016
11/6/2016
11/7/2016
< 2
< 2.5
0
5
11/8/2016
81
< 2.5
0.07
< 1
11/9/2016
46
<2.5
0.05
1
11/10/2016
6.5
Q.5
0
< 1
11/11/2016
11/12/2016
11/13/2016
11/14/2016
<2
<2.5
<0 04
< 1
11/15/2016
12
<2.5
<0.04
< 1
11/16/2016
12
< 2.5
005
< 1
11/17/2016
68
< 2.5
0.06
< 1
11/18/2016
26
< 2 5
<0.04
< 1
11/19/2016
11/20/2016
11/21/2016
<2
<2 5
0.09
< 1
11/22/2016
< 2
<2.5
0.09
< 1
11/23/2016
25
< 2 5
0.05
< 1
11/24/2016
11/25/2016
11/26/2016
11/27/2016
11/28/2016
24
< 2 5
<0 04
< 1
11/29/2016
26
<2 5
<0.04
< 1
11/30/2016
13
< 2 5
<0.04
< 1
12/1/2016
24
<2 5
0.05
< 1
12/2/2016
24
9.9
0.04
1
12/3/2016
12/4/2016
12/5/2016
12
2.6
004
< 1
12/6/2016
63
<2 5
< 0.04
< 1
12/7/2016
13
<2 5
0.060
< 1
12/8/2016
23
<2 5
0.08
< 1
12/9/2016
< 2
<2.5
014
< 1
12/10/2016
12/11/2016
12/12/2016
2
<2.5
012
1
12/13/2016
< 2
Q.5
0
< 1
12/14/2016
2
<2.5
< 0 04
< 1

N
N
N
N
N
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
\
0)
\
Ln
\
\
\
\
W
W
N
N
N
N
N
N
N
N
N
N
0
l!7
NN
W
\D
\0
\
\C
\l!
\
\W
\
\
\WN
\
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\N
\\NO
0�p
\lN!
\N
\WN
\NN
\N\
0
00
Cl)
lJ
W
NNO
0
00
\
O
0
00
V
O1
l!
W
NJ
LD
00
U
IUN
0
N
0
N
0
N
0
N
0
0
N
NNN
N
N
N
N
O
N
O
O
N
O
O
O
O
O
O
O
O
O
NO
O
O
NNN
O
OO
N
N
N\\
N
NO
N
N
OOOOO
N
N
N
O
NN
O
NV
N
N
N
N
O
O
O
O
O
O
O
O
O
O
O
O
O
0
V
VVN
V
V
V
V
VV
VVV
14
V
V
V
N
N
NNN
N
N
N
N
N
N
N
N
N
N
N
NV
0)
01
T
O)
M
On
O1
0)
0n
On
cn
M
m
M
M
M
01
0
0
N
C
3
3
A
ao
O
0
N
AA
A
V
A
A
N
N
A
A
A
A
N
W
A
(n
A
A
A
A
W
A
A
A
A
A
A
A
A
A
N
A
W
l!1
N
N
N
00
N
N
N
N
N
N
N
N
o
N
N
W
N
N
N
N
N
N
N
N
N
N
N
N
N
Nen
N
M
Ln
7
fp
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
.�
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
W
N
N
N
N
N
in
V7
Ln
Ul
U7
Ln
Ln
Ul
Ln
Ln
Ln
U1
Ln
Ln
U1
U1
U7
V7
U1
V7
in
Ln
U7
Ln
W
N
W
Ln
Ln
lA
(n
Ln
Ln
01
H
c z
3
z
x
O
O
A
O
O
O
O
O
O
AO
0
A
0O
O
o
o
O
O
A
O
O
O
O
O
A
O
O
O
O
O
A
O
A
O
A
O
ZC
0
O
0
0
0
olLl!1
OO
0
0
o
o
o
O
O
o
V
d1
Ao
C
V
.
l!1
A
0
m
0
c
00
V
A
L
U
00m
m
0
0
A
G
7
fD
m
r
n
lu
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
N
A
A
A
A
A
N
A
A
A
A
N
A
A
A
N
C
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
yi
0
1
3

W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
WN
W
W
W
W
W
W
W
W
W
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
F�
F-'
O
l0
00
V
Q1
l77
A
W
N
F�
O
l0
00
V
Q1
U'1
A
W
N
F-'
O
l0
00
V
01
ll1
A
W
N
N
00
J
m
y
A
W
N
F-A
O
w
00
J
m
Ul
A
W
N
N
O
LO
00
V
\
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
\
N
\
N
O
NN
O
O
N
O
N
O
N
O
N
O
N
O
N
O
NN
O
O
NN
O
O
NN
O
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
O
O
O
O
O
O
O
O
O
Nm
O
O
N
O
N
O
NN
O
O
N
O
N
O
N
O
N
O
N
O
N
O
N
N
N
N
N
N
N
O
O
O
rt
m
F�
F-'
ll
H+
N
N
F�
H
F-A
1--'
F-`
"
N
N
F,
N
N
N
N
N
O
N
O
i"
O
"
O
I-•
O
"
O
F--
O
N
N
N
N
V
J
V
V
V
V
V
J
J
V
V
J
V
V
V
J
V
J
J
V
V
V
J
V
J
V
J
J
J
V
V
V
V
V
V
J
J
J
V
J
V
V
V
V
W
0
O
N
N
C
3
3
�o
O
v
N
N
N
W
WW
n
N
N
NA
n
n
n
n
N
W
n
n
n
n
n
W
N
n
n
A
n
n
n
n
n
n
n
n
N
n
n
n
A
Ol
Oo
A
NLD
W
A
N
N
N
N
N
F+
N
N
N
N
N
l77
A
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
7
fD
n
n
n
n
n
N
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
n
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
W
N
N
N
N
N
N
N
N
N
N
N
l0
N
y
In
In
In
In
In
In
V7
U9
In
In
In
In
In
Ln
In
(n
In
N
In
In
Ln
In
Ln
In
F'"
In
In
Ln
In
In
In
Ln
In
in
Ln
Ln
00
In
V1
H
C Z
fD Z
Z
2
W
0
0
0
0
0
0
0
0
0
O
n
p
O
O
O
n
O
O
O
n
O
O
0
0
0
0
0
O
O
O
O
O
O
O
O
O
O
0
0
0
0
0
O0
O
O
1.0
V
l0
l0
O
J
0
00
0
M
0
Ln
O
0)
O
0)
O
00
O
V
O
0)
O
00
O
J
F—
Ln
F--
N
"
O
O
O
~'
O
O
O
O
O
00
O"
O
"
O
O
O
A
0
A
F-'
00
w
m
V
J
00
M
M
W
00
W
00
N
y
00
M
7
rf
f0
fD
A
d
A
n
n
n
n
n
F,
n
n
n
n
O
n
n
n
N
nn
F�
F
A
n
N
N
00
N
n
n
n
n
N~
r
O
3

In
\
l!7
\
(Jl
\
l!7
\
lJl
\
lJl
\
lA
\
lJl
\
111
\
Ul
\
lJl
\
lJl
\
Ul
\
l!7
\
lA
\
lJl
\
y
y
y
N
y
w
W
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
\
A
A
A
A
A
A
A
A
N
Vl
N
A
N
W
N
N
N
r
N
O
r
l0
r
00
r
V
r
Ol
r
In
r
A
r
W
r
N
r
r
r
O
\\\\\\\\\
�O
0o
V
O1
l
A
w
N
r
W
O
N
LO
N
w
N
V
N
Ol
N
w
N
A
N
W
N
N
N
r
N
O
r
l0
r
00
r
V
r
01
r
In
r
A
r
W
r
N
r
r
r
O
\\\\\\\\
t0
0o
V
M
vl
A
w
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
N
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
N
\
N
\
\
N
\
N
\
\
\
OJ
N
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
Or
Or
Or
Or
Or
Or
O
Or
Or
N
N
N
N
N
N
N
N
N
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
N
O
Or
Or
N
Or
Or
Or
N
O
N
O
N
O
m
pO
r
r
V
r
V
r
V
r
V
r
r
r
r
r
r
r
r
r
r
r
VV
r
r
r
rrr
r
r
rrrrr
r
V
V
r
VVVV
r
r
V
V
V
V
VV
v
N
N
A
N
N
W
N
N
A
N
W
W
W
Pb
W
A
N
N
N
w
A
N
A
A
N
N
W
N
"''
W
N
NN
A
N
N
A
A
w
in
V
N
A
r
N
l0
r
lO
00
lO
U7
N
N
Ln
r
Ln
Ln
V
l0
N
N
LO
A
V
Ut
r
r
A
Ul
N
Ul
Ol
N
CO
c
3
�o
1
v
r+
�o
W
N
A
N
A
A
N
A
A
N
A
N
A
N
A
A
A
A
N
A
N
A
A
N
A
N
A
N
A
A
A
N
N
N
N
A
A
N
A
A
A
A
N
A
N
A
A
A
A
A
A
N
A
N
111
L l
N
w
y
N
Ul
y
y
y
N
y
N
y
N
y
W
Ul
N
Ul
Lrl
Ul
Ul
N
w
N
In
Ol
V
l0
N
lrl
to
N
vl
N
ul
N
ul
W
W
N
Vl
N
Ul
N
Ln
N
M
N
In
w
N
l!1
y
y
y
O
O
O
O
O
A
O
O
O
O
O
O
A
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
A
O
O
O
O
C Z
3 =
r
Ul
O
00
r
A
r
Ul
r
N
O
w
r
A
N
00
O
Ol
r
WAO
O
Ul
r
N
r
(n
r
V
r
O)
r
W
O
W
O
l0
r
r
~'
r
N
r
NW
O
r
M
r
V
r
W
O
%a
O
M00
O
O
Ol
O
V
O
00
O
00
O
00
A
fD Z
1
Z
cZ
G
7
f0
7
T
m
d
A
A
W
N
r
l0
A
~'
0
A
r
�'
W
A
A
N
r
r
A
A
r
N
l!7
A
r
V
A
A
r
r
A
A
In
A
A
W
N
Ol
A
A
m
O
r
r
W
w
w
r
r
r
r
r
r
r
A
r
O
3

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter) Fecal Coliform
5/26/2017
29
Q.5
Oil
< 1
5/27/2017
5/28/2017
5/29/2017
5/30/2017
2.5
<2.5
012
< 1
5/31/2017
3.3
<2 5
009
< 1
6/1/2017
2.9
<25
0 1
2
6/2/2017
2.1
< 2 5
008
1
6/3/2017
6/4/2017
6/5/2017
28
< 2.5
016
4
6/6/2017
21
< 2 5
0.34
< 1
6/7/2017
< 2
< 2.5
< 0.04
1
6/8/2017
< 2
< 2.5
0.11
2
6/9/2017
< 2
< 2 5
0.06
< 1
6/10/2017
6/11/2017
6/12/2017
24
< 2.5
009
1
6/13/2017
< 2
< 2.5
01
< 1
6/14/2017
< 2
< 2.5
018
< 1
6/15/2017
< 2
< 2.5
021
< 1
6/16/2017
< 2
< 2.5
014
< 1
6/17/2017
6/18/2017
6/19/2017
< 2
< 2.5
0.09
4
6/20/2017
< 2
< 2 5
0.04
2
6/21/2017
< 2
< 2 5
0.08
2
6/22/2017
< 2
27
0.13
1
6/23/2017
3.5
< 2 5
0.17
< 1
6/24/2017
6/25/2017
6/26/2017
< 2
< 2.5
0.11
< 1
6/27/2017
< 2
< 2.5
0.06
< 1
6/28/2017
< 2
< 2.5
0.06
4
6/29/2017
< 2
< 2.5
0.07
< 1
6/30/2017
< 2
< 2.5
0.07
< 1
7/1/2017
7/2/2017
7/3/2017
< 2
< 2 5
0.09
1
7/4/2017
7/5/2017
< 2
< 2 5
007
3
7/6/2017
< 2
< 2 5
006
1
7/7/2017
< 2
< 2 5
01
< 1
7/8/2017
7/9/2017
7/10/2017
< 2
< 2.5
01
1
7/11/2017
< 2
< 2 5
006
< 1
7/12/2017
< 2
< 2 5
008
< 1
7/13/2017
< 2
< 2.5
007
1
7/14/2017
< 2
< 2 5
02
< 1
7/15/2017
7/16/2017
7/17/2017
< 2
< 2.5
0.13
< 1
7/18/2017
< 2
< 2 5
009
1

Date
BODS (Summer) BODS (Winter)
TSS
NH3-N
(Summer)
NH3-N (Winter) Fecal Coliform
7/19/2017
< 2
<25
0 16
< 1
7/20/2017
< 2
< 2 5
007
< 1
7/21/2017
< 2
< 2 5
0.1
< 1
7/22/2017
7/23/2017
7/24/2017
< 2
< 2 5
01
6
7/25/2017
< 2
< 2 5
01
< 1
7/26/2017
< 2
< 2 5
009
< 1
7/27/2017
< 2
< 2 5
007
1
7/28/2017
< 2
< 2 5
007
< 1
7/29/2017
7/30/2017
7/31/2017
< 2
< 2.5
007
< 1
8/1/2017
< 2
< 2 5
007
< 1
8/2/2017
< 2
< 2 5
01
2
8/3/2017
< 2
< 2 5
008
1
8/4/2017
< 2
< 2.5
008
< 1
8/5/2017
8/6/2017
8/7/2017
37
< 2.5
014
2
8/8/2017
< 2
< 2.5
Oil
3
8/9/2017
< 2
< 2 5
0.07
1
8/10/2017
< 2
< 2 5
0.06
< 1
8/11/2017
< 2
< 2 5
< 0.04
1
8/12/2017
8/13/2017
8/14/2017
< 2
< 2 5
016
< 1
8/15/2017
< 2
28
0.06
< 1
8/16/2017
< 2
< 2 5
006
1
8/17/2017
< 2
< 2 5
008
1
8/18/2017
22
< 2 5
Oil
5
8/19/2017
8/20/2017

Date
BODS (Summer) BODS (Winter)
TSS
NH3-NNH3-N
(Summer)
(Winter) Fecal Coliform
8/21/2017
< 2
< 2.5
0.08
8
8/22/2017
< 2
< 2 5
0.1
4
8/23/2017
< 2
< 2.5
008
34
8/24/2017
< 2
< 2.5
0.05
12
8/25/2017
< 2
< 2.5
0.05
6
8/26/2017
8/27/2017
8/28/2017
< 2
< 2.5
006
10
8/29/2017
< 2
< 2.5
< 0.04
15
8/30/2017
< 2
< 2 5
005
11
8/31/2017
< 2
< 2.5
0.05
4
9/1/2017
<2
<2.5
005
< 1
9/2/2017
9/3/2017
9/4/2017
9/5/2017
< 2
< 2 5
< 0 04
98
9/6/2017
< 2
< 2.5
< 0.04
40
9/7/2017
< 2
< 2.5
< 0.04
147
9/8/2017
<2
<2 5
005
80
9/9/2017
9/10/2017
9/11/2017
<2
<2 5
006
14
9/12/2017
< 2
< 2.5
0.08
12
9/13/2017
< 2
< 2 5
008
2
9/14/2017
<2
Q.5
009
2
9/15/2017
< 2
< 2 5
004
10
9/16/2017
9/17/2017
9/18/2017
<2
<2.5
0.05
9
9/19/2017
13
< 2 5
006
35
9/20/2017
49
Q.5
<0 04
20
9/21/2017
<2
<2 5
<0 04
6
9/22/2017
< 2
< 2 5
0.27
10
9/23/2017
9/24/2017
9/25/2017
<2
<2 5
014
3
9/26/2017
2.5
<2.5
009
9/27/2017
< 2
< 2 5
0.18
< 1
9/28/2017
<2
<2 5
0.06
< 1
9/29/2017
<2
<2 5
0.05
1
9/30/2017

Water Resources
EN YIRONNEWAI. OUACITY
January 03, 2018
Frank Bottorff
City of Havelock
PO Box 368
Havelock, NC 28532
Subject: Permit Renewal
Application No. NCO021253
Havelock WWTP
Craven County
Dear Applicant:
ROY COOPER
CTMWMT
MICHAEL S- REGAN
swratmy
LnMA CULPEPPER
Aterhn Direcfw
The Water Quality Permitting Section acknowledges the December 21, 2017 receipt of your permit renewal application
and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 15OB-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit.
The permit writer will contact you if additional information is required to complete your permit renewal. Please respond
in a timely manner to requests for additional information necessary to allow a complete review of the application and
renewal of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq. nc.gov/permits-regulations/permit-g uidancelenvironmenta I -application -tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
_3c w
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
cc: Central Files w/application
ec: WQPS Laserfiche File w/application
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919-R07-6300