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Home My WebLink AboutNC0038377_J16040718report_2017110113339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 Order Summary Report Analytical Laboratory Order Number: J16040718 Project Name:MAYO STEAM - NPDES - AOW Lab Contact:Mary Ann Ogle Date:5/11/2016 Customer Address:Mayo Steam Plant Customer Name(s):Ross Hartfield, Jerry Wylie, Tim Hunsucker, Kathy Webb, Brandon Russo 10660 Boston Road Roxboro,North Carolina 27574 Phone:980-875-5274 Report Authorized By: (Signature) Program Comments: Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report. Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have been qualified by Duke Energy to perform these analyses except where noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows: Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods. Mary Ann Ogle Analytical lab Page 1 of 24 Sample ID's & Descriptions: Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2016011887 MAYO STEAM 27-Apr-16 8:10 AM Synterra S-10 2016012039 MAYO STEAM 27-Apr-16 8:10 AM Synterra FIELD BLANK 2 Total Samples Analytical lab Page 2 of 24 COC and .pdf report are in agreement with sample totals and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. Yes No Technical Validation Review Checklist: Yes No Yes No Report Sections Included: Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Analytical Laboratory QC Report Chain of Custody Reviewed By:Mary Ann Ogle Date:5/11/2016 Electronic Data Deliverable (EDD) Sent Separatel Analytical lab Page 3 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 2016011887 Collection Date:27-Apr-16 8:10 AM Site:S-10 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF MERCURY IN WATER - (Analysis Performed by Shealy Labs) Vendor Parameter Complete Vendor Method V_SHEALY TOTAL RECOVERABLE METALS BY ICP Aluminum (Al)0.117 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.005 1 Barium (Ba)0.114 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.005 1 Boron (B)0.729 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.05 1 Calcium (Ca)15.4 mg/L EPA 200.7 05/04/2016 13:53M2 MHH71310.01 1 Iron (Fe)0.068 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.01 1 Magnesium (Mg)7.90 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.005 1 Manganese (Mn)0.918 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.005 1 Potassium (K)1.89 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.1 1 Sodium (Na)14.7 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.05 1 Total Hardness (Ca and Mg)70.9 mg/L (CaCO3) EPA 200.7 05/04/2016 13:53 MHH71310.19 1 Zinc (Zn)0.006 mg/L EPA 200.7 05/04/2016 13:53 MHH71310.005 1 TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Arsenic (As)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Cadmium (Cd)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Chromium (Cr)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Copper (Cu)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Lead (Pb)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Molybdenum (Mo)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Nickel (Ni)1.44 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Selenium (Se)< 1 ug/L EPA 200.8 05/09/2016 23:51 MHALL311 Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 05/09/2016 23:51 MHALL30.2 1 Field Parameters (certification not covered under DPAL certification) pH 5.30 SI Units Field WorkF1 Temperature 14.6 °C Field WorkF1 Specific Conductance 250 uS/cm Field WorkF1 Turbidity 8.63 NTU Field WorkF1 Flow 0.0001 cfs Field WorkF1 Analytical lab Page 4 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 2016012039 Collection Date:27-Apr-16 8:10 AM Site:FIELD BLANK Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF MERCURY IN WATER - (Analysis Performed by Shealy Labs) Vendor Parameter Complete Vendor Method V_SHEALY Qualifiers: F Field Parameters are not covered under the DPAL certification. If certification is required for these parameters please request field certificates from the samplers. This data is provided at the request of the client. M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable. Analytical lab Page 5 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 Q16050061 ICP_TRM TOTAL RECOVERABLE METALS BY ICP Level II QC Summary Final QualifierDilMeasuredUnits:Parameter Blank # 1 RDL Relative Concentration Aluminum (Al) 0.000919 mg/L -10.000919 0.005 < 1/2 RDL Barium (Ba) 0.0002 mg/L -10.0002 0.005 < 1/2 RDL Boron (B) 0.000229 mg/L -10.000229 0.05 < 1/2 RDL Calcium (Ca) 0.00376 mg/L -10.00376 0.01 < 1/2 RDL Iron (Fe) 0.000425 mg/L -10.000425 0.01 < 1/2 RDL Magnesium (Mg) 0.000516 mg/L -10.000516 0.005 < 1/2 RDL Manganese (Mn) 0.000031 mg/L -10.000031 0.005 < 1/2 RDL Potassium (K) 0.00374 mg/L -10.00374 0.1 < 1/2 RDL Sodium (Na) -0.0171 mg/L -1-0.0171 0.05 < 1/2 RDL Zinc (Zn) -0.000115 mg/L -1-0.000115 0.005 < 1/2 RDL Final QualifierDilMeasuredUnits:Parameter LCS # 1 % Recovery LCL UCLSpike Aluminum (Al) 4.94 5 98.9mg/L -1158514.94 Barium (Ba) 5.07 5 101mg/L -1158515.07 Boron (B) 5.13 5 103mg/L -1158515.13 Calcium (Ca) 5.07 5 101mg/L -1158515.07 Iron (Fe) 5.11 5 102mg/L -1158515.11 Magnesium (Mg) 5.03 5 101mg/L -1158515.03 Manganese (Mn) 5.04 5 101mg/L -1158515.04 Potassium (K) 4.95 5 99mg/L -1158514.95 Sodium (Na) 4.94 5 98.7mg/L -1158514.94 Zinc (Zn) 5.06 5 101mg/L -1158515.06 Final QualifierDilMeasuredUnits:Parameter MS # 1 % Recovery LCL UCLSpike Parent Sample: J16040764 -- 2016012100 Aluminum (Al) 5.86 5 96.3mg/L -1307015.86 Barium (Ba) 5.18 5 100mg/L -1307015.18 Boron (B) 5.25 5 102mg/L -1307015.25 Calcium (Ca) 85.1 5 36.1mg/L -13070185.1 Iron (Fe) 5.63 5 97.8mg/L -1307015.63 Magnesium (Mg) 17.8 5 88.4mg/L -13070117.8 Manganese (Mn) 4.92 5 98.1mg/L -1307014.92 Potassium (K) 16.3 5 88.3mg/L -13070116.3 Sodium (Na) 16.8 5 88.1mg/L -13070116.8 Zinc (Zn) 4.84 5 96.3mg/L -1307014.84 Final QualifierDilMeasuredUnits:Parameter MSD # 1 RPD% Recovery LCL UCLSpike Parent Sample: J16040764 -- 2016012100 Aluminum (Al) 5.87 5 96.6 0.332mg/L -1307015.87 Analytical lab Page 6 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 Q16050061 ICP_TRM TOTAL RECOVERABLE METALS BY ICP Level II QC Summary Final QualifierDilMeasuredUnits:Parameter MSD # 1 RPD% Recovery LCL UCLSpike Parent Sample: J16040764 -- 2016012100 Barium (Ba) 5.2 5 100 0.319mg/L -1307015.2 Boron (B) 5.22 5 101 0.492mg/L -1307015.22 Calcium (Ca) 85.3 5 39.6 9.4mg/L -13070185.3 Iron (Fe) 5.65 5 98 0.245mg/L -1307015.65 Magnesium (Mg) 17.8 5 88.8 0.451mg/L -13070117.8 Manganese (Mn) 4.94 5 98.4 0.305mg/L -1307014.94 Potassium (K) 16.4 5 89.3 1.15mg/L -13070116.4 Sodium (Na) 16.8 5 88.3 0.295mg/L -13070116.8 Zinc (Zn) 4.84 5 96.2 0.0208mg/L -1307014.84 Analytical lab Page 7 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 Q16050066 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS Level II QC Summary Final QualifierDilMeasuredUnits:Parameter Blank # 1 RDL Relative Concentration Antimony (Sb) -0.0079 ug/L -1-0.0079 1 < 1/2 RDL Arsenic (As) -0.2 ug/L -1-0.2 1 < 1/2 RDL Cadmium (Cd) -0.0003 ug/L -1-0.0003 1 < 1/2 RDL Chromium (Cr) 0.0011 ug/L -10.0011 1 < 1/2 RDL Copper (Cu) -0.123 ug/L -1-0.123 1 < 1/2 RDL Lead (Pb) 0.0021 ug/L -10.0021 1 < 1/2 RDL Molybdenum (Mo) 0.0035 ug/L -10.0035 1 < 1/2 RDL Nickel (Ni) -0.0024 ug/L -1-0.0024 1 < 1/2 RDL Selenium (Se) -0.0075 ug/L -1-0.0075 1 < 1/2 RDL Thallium (Tl) Low Level -0.0573 ug/L -1-0.0573 0.2 < 1/2 RDL Final QualifierDilMeasuredUnits:Parameter LCS # 1 % Recovery LCL UCLSpike Antimony (Sb) 54.1 50 108ug/L -11585154.1 Arsenic (As) 52.3 50 105ug/L -11585152.3 Cadmium (Cd) 51 50 102ug/L -11585151 Chromium (Cr) 48.9 50 97.7ug/L -11585148.9 Copper (Cu) 49.4 50 98.8ug/L -11585149.4 Lead (Pb) 49.2 50 98.4ug/L -11585149.2 Molybdenum (Mo) 50.1 50 100ug/L -11585150.1 Nickel (Ni) 50.7 50 101ug/L -11585150.7 Selenium (Se) 49.4 50 98.8ug/L -11585149.4 Thallium (Tl) Low Level 48.5 50 97.1ug/L -11585148.5 Final QualifierDilMeasuredUnits:Parameter MS # 1 % Recovery LCL UCLSpike Parent Sample: J16040718 -- 2016011887 Antimony (Sb) 54.4 50 109ug/L -13070154.4 Arsenic (As) 52.4 50 105ug/L -13070152.4 Cadmium (Cd) 50.5 50 101ug/L -13070150.5 Chromium (Cr) 48 50 95.8ug/L -13070148 Copper (Cu) 48.3 50 96.3ug/L -13070148.3 Lead (Pb) 48.6 50 97.1ug/L -13070148.6 Molybdenum (Mo) 51.3 50 103ug/L -13070151.3 Nickel (Ni) 50 50 97ug/L -13070150 Selenium (Se) 48.8 50 97.5ug/L -13070148.8 Thallium (Tl) Low Level 46.2 50 92.4ug/L -13070146.2 Final QualifierDilMeasuredUnits:Parameter MSD # 1 RPD% Recovery LCL UCLSpike Parent Sample: J16040718 -- 2016011887 Antimony (Sb) 53.6 50 107 1.41ug/L -13070153.6 Analytical lab Page 8 of 24 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040718 Q16050066 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS Level II QC Summary Final QualifierDilMeasuredUnits:Parameter MSD # 1 RPD% Recovery LCL UCLSpike Parent Sample: J16040718 -- 2016011887 Arsenic (As) 52 50 104 0.766ug/L -13070152 Cadmium (Cd) 49.8 50 99.4 1.38ug/L -13070149.8 Chromium (Cr) 48.2 50 96.2 0.458ug/L -13070148.2 Copper (Cu) 48.6 50 96.9 0.58ug/L -13070148.6 Lead (Pb) 49.2 50 98.2 1.13ug/L -13070149.2 Molybdenum (Mo) 49.8 50 99.5 3.09ug/L -13070149.8 Nickel (Ni) 48.8 50 94.6 2.53ug/L -13070148.8 Selenium (Se) 49.6 50 99.3 1.77ug/L -13070149.6 Thallium (Tl) Low Level 47.5 50 95 2.84ug/L -13070147.5 Analytical lab Page 9 of 24 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Duke Energy 13339 Hagers Ferry Rd Bldg 7405 Huntersville, NC 28078 Attention: Mary Ann Ogle RD29027Lot Number: J16040718Project Number: Mayo NPDES AOW - Low Level HgProject Name: 05/05/2016Date Completed: Grant Wilton Project Manager This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Page: 1 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. SHEALY ENVIRONMENTAL SERVICES, INC. Case Narrative Duke Energy Lot Number: RD29027 SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329 Project Name: Mayo NPDES AOW - Low Level Hg Project Number: J16040718 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Page: 2 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Duke Energy Lot Number: RD29027 Project Name: Mayo NPDES AOW - Low Level Hg Project Number: J16040718 Sample Number Sample ID Matrix Date Sampled Date Received 001 04/27/2016 08102016011887Aqueous 04/29/2016 002 04/27/2016 08102016012039Aqueous 04/29/2016 (2 samples) Page: 3 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary Duke Energy Lot Number: RD29027 Project Name: Mayo NPDES AOW - Low Level Hg Project Number: J16040718 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 2016011887 Aqueous Mercury (CVAFS)1631E 1.12 ng/L 5 (1 detection) Page: 4 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Duke Energy 2016011887 RD29027-001 04/27/2016 0810 04/29/2016 Aqueous Project Name: Mayo NPDES AOW - Low Level Project Number: J16040718 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631E 1 05/04/2016 1234 COH 04/29/2016 1720 12157 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Mercury (CVAFS)7439-97-6 1631E 1.12 1ng/L0.500 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page: 5 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Duke Energy 2016012039 RD29027-002 04/27/2016 0810 04/29/2016 Aqueous Project Name: Mayo NPDES AOW - Low Level Project Number: J16040718 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 1631E 1 05/04/2016 1249 COH 04/29/2016 1720 12157 AnalyticalCAS Parameter Number Method Result Q PQL Units Run Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500 J = Estimated result < PQL and > MDL PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria_ H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page: 6 of 6 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. QC Summary QC Data for Lot Number: RD29027 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) - MB Batch:Prep Method: Prep Date: Sample ID:RQ12157-001 12157 1631E 04/29/2016 1720Analytical Method:1631E Matrix:Aqueous Parameter Result Q PQL Units Analysis DateDil Mercury (CVAFS)ND 05/04/2016 11270.500 ng/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_ QC Data for Lot Number: RD29027 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) - LCS Batch:Prep Method: Prep Date: Sample ID:RQ12157-002 12157 1631E 04/29/2016 1720Analytical Method:1631E Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ng/L)(ng/L) Mercury (CVAFS)5.03 05/04/2016 11321015.00 75-1251 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_ QC Data for Lot Number: RD29027 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) - MS Batch:Prep Method: Prep Date: Sample ID:RD29027-001MS 12157 1631E 04/29/2016 1720Analytical Method:1631E Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec Limit Sample Amount Dil(ng/L)(ng/L)(ng/L) Mercury (CVAFS)5.39 05/04/2016 1239855.00 71-1251.12 1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_ QC Data for Lot Number: RD29027 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Mercury (CVAFS) - MSD Batch:Prep Method: Prep Date: Sample ID:RD29027-001MD 12157 1631E 04/29/2016 1720Analytical Method:1631E Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD Limit Sample Amount Dil(ng/L)(ng/L)(ng/L) Mercury (CVAFS)5.24 05/04/2016 1244825.00 71-1252.8 241.12 1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results PQL = Practical quantitation limit ND = Not detected at or above the PQL Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" J = Estimated result < PQL and > MDL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_ QC Data for Lot Number: RD29027 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Analytical lab Page 24 of 24