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Home My WebLink AboutNC0038377_J16040212report_2017110113339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 Order Summary Report Analytical Laboratory Order Number: J16040212 Project Name:MAYO STEAM - NPDES - AOW Lab Contact:Mary Ann Ogle Date:4/23/2016 Customer Address:Mayo Steam Plant Customer Name(s):Ross Hartfield, Jerry Wylie, Tim Hunsucker, Kathy Webb, Brandon Russo 10660 Boston Road Roxboro,North Carolina 27574 Phone:980-875-5274 Report Authorized By: (Signature) Program Comments: Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report. Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have been qualified by Duke Energy to perform these analyses except where noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows: Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods. Mary Ann Ogle Analytical Lab Page 1 of 11 Sample ID's & Descriptions: Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2016010000 MAYO STEAM 08-Apr-16 4:20 PM illegible S-09 2016010001 MAYO STEAM 08-Apr-16 4:35 PM illegible S-06 2016010002 MAYO STEAM 08-Apr-16 3:05 PM illegible S-01 2016010003 MAYO STEAM 08-Apr-16 3:33 PM illegible S-08 2016010004 MAYO STEAM 08-Apr-16 2:45 PM illegible S-02 2016010005 MAYO STEAM 08-Apr-16 2:35 PM illegible S-03 6 Total Samples Analytical Lab Page 2 of 11 COC and .pdf report are in agreement with sample totals and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. Yes No Technical Validation Review Checklist: Yes No Yes No Report Sections Included: Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Analytical Laboratory QC Report Chain of Custody Reviewed By:Mary Ann Ogle Date:4/23/2016 Electronic Data Deliverable (EDD) Sent Separatel Analytical Lab Page 3 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010000 Collection Date:08-Apr-16 4:20 PM Site:S-09 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 6.40 SI Units Field WorkF1 Temperature 16.0 °C Field WorkF1 Specific Conductance 326 uS/cm Field WorkF1 Turbidity 4.40 NTU Field WorkF1 Flow 0.1310 cfs Field WorkF1 Analytical Lab Page 4 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010001 Collection Date:08-Apr-16 4:35 PM Site:S-06 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 7.10 SI Units Field WorkF1 Temperature 15.0 °C Field WorkF1 Specific Conductance 132 uS/cm Field WorkF1 Turbidity 5.27 NTU Field WorkF1 Flow 0.3970 cfs Field WorkF1 Analytical Lab Page 5 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010002 Collection Date:08-Apr-16 3:05 PM Site:S-01 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 6.20 SI Units Field WorkF1 Temperature 14.0 °C Field WorkF1 Specific Conductance 427 uS/cm Field WorkF1 Turbidity 3.85 NTU Field WorkF1 Flow No Flow cfs Field WorkF1 Analytical Lab Page 6 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010003 Collection Date:08-Apr-16 3:33 PM Site:S-08 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 5.70 SI Units Field WorkF1 Temperature 12.0 °C Field WorkF1 Specific Conductance 416 uS/cm Field WorkF1 Turbidity 4.40 NTU Field WorkF1 Flow No Flow cfs Field WorkF1 Analytical Lab Page 7 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010004 Collection Date:08-Apr-16 2:45 PM Site:S-02 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 6.00 SI Units Field WorkF1 Temperature 13.0 °C Field WorkF1 Specific Conductance 418 uS/cm Field WorkF1 Turbidity 1.69 NTU Field WorkF1 Flow 0.0250 cfs Field WorkF1 Analytical Lab Page 8 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 2016010005 Collection Date:08-Apr-16 2:35 PM Site:S-03 Matrix:NPDES Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Oil and Grease < 5 mg/L EPA 1664B 04/15/2016 07:00 GHUTCHI51 Field Parameters (certification not covered under DPAL certification) pH 6.70 SI Units Field WorkF1 Temperature 15.0 °C Field WorkF1 Specific Conductance 370 uS/cm Field WorkF1 Turbidity 5.14 NTU Field WorkF1 Flow 0.3630 cfs Field WorkF1 Qualifiers: F Field Parameters are not covered under the DPAL certification. If certification is required for these parameters please request field certificates from the samplers. This data is provided at the request of the client. Analytical Lab Page 9 of 11 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J16040212 Q16040297 1664_SPE OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION Level II QC Summary Final QualifierDilMeasuredUnits:Parameter Blank # 1 RDL Relative Concentration Oil and Grease mg/L -1#Error 5 #Error Final QualifierDilMeasuredUnits:Parameter LCS # 1 % Recovery LCL UCLSpike Oil and Grease 37 91.9mg/L -11480134 Final QualifierDilMeasuredUnits:Parameter MS # 1 % Recovery LCL UCLSpike Parent Sample: J16030311 -- 2016007115 Oil and Grease 33.2 87.2mg/L -11480129.5 Analytical Lab Page 10 of 11 Analytical Lab Page 11 of 11