NC0038377_J15100326reportrevised110415_20171101

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number: J15100326
Project Name:MAYO STEAM - AB GW ASSESSMENT SURFACE
Lab Contact:Mary Ann Ogle
Date:11/4/2015
Customer Address:
Customer Name(s): Tim Hunsucker, Jerry Wylie,Brandon Russo, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Analytical Lab Revised 11/04/2015
Page 1 of 95
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015033514 MAYO STEAM 13-Oct-15 1:10 PM illegible S-04
2015033515 MAYO STEAM 13-Oct-15 12:50 PM illegible S-01
2015033516 MAYO STEAM 13-Oct-15 2:00 PM illegible S-02B
2015033517 MAYO STEAM 13-Oct-15 1:35 PM illegible S-02
2015033518 MAYO STEAM 13-Oct-15 10:55 AM illegible S-06
2015033519 MAYO STEAM 13-Oct-15 11:30 AM illegible SW-REF1
2015033520 MAYO STEAM 13-Oct-15 12:20 PM illegible S-05
2015033521 MAYO STEAM 13-Oct-15 12:20 PM illegible S-05 Dup
2015033522 MAYO STEAM 13-Oct-15 3:10 PM illegible SW-CB1
2015033523 MAYO STEAM 13-Oct-15 2:55 PM illegible S-03
2015033524 MAYO STEAM 13-Oct-15 2:17 PM illegible S-08
2015033525 MAYO STEAM 13-Oct-15 3:55 PM illegible SW-CB2
2015033526 MAYO STEAM 13-Oct-15 5:58 PM illegible Filter Blank
2015033527 MAYO STEAM 13-Oct-15 5:55 PM illegible FIELD BLANK
2015033528 MAYO STEAM 13-Oct-15 6:00 PM Trip Blank
15 Total Samples
Analytical Lab Revised 11/04/2015
Page 2 of 95
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:10/26/2015
Electronic Data Deliverable (EDD) Sent Separately
Analytical Lab Revised 11/04/2015
Page 3 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033514
Collection Date: 13-Oct-15 1:10 PM
Site: S-04
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.107 mg-N/L EPA 353.2 10/20/2015 13:27 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 17 mg/L EPA 300.0 10/15/2015 17:34 BGN9034110
Sulfate 9.9 mg/L EPA 300.0 10/15/2015 17:34 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.008 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.005 1
Barium (Ba)0.007 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.005 1
Boron (B)0.187 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.05 1
Iron (Fe)0.013 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.01 1
Manganese (Mn)0.180 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.005 1
Strontium (Sr)0.160 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 10/19/2015 09:51 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)17.1 mg/L EPA 200.7 10/19/2015 13:40 FCJORDA0.01 1
Magnesium (Mg)6.27 mg/L EPA 200.7 10/19/2015 13:40 FCJORDA0.005 1
Potassium (K)4.64 mg/L EPA 200.7 10/19/2015 13:40 FCJORDA0.1 1
Sodium (Na)14.3 mg/L EPA 200.7 10/19/2015 13:40 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)1.76 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.005 1
Barium (Ba)0.060 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.005 1
Boron (B)0.190 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.05 1
Iron (Fe)4.09 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.01 1
Manganese (Mn)2.27 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.005 1
Strontium (Sr)0.175 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 10/16/2015 10:41 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 4 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033514
Collection Date: 13-Oct-15 1:10 PM
Site: S-04
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Copper (Cu)2.95 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:26 MHALL311
Thallium (Tl) Low Level 0.599 ug/L EPA 200.8 10/20/2015 17:26 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 17:26 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Chromium (Cr)2.27 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Cobalt (Co)3.09 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Copper (Cu)9.45 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Nickel (Ni)2.02 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA11
Thallium (Tl) Low Level 0.245 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA0.2 1
Vanadium (V) Low Level 3.69 ug/L EPA 200.8 10/21/2015 17:38 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 130 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 6.1 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI110
TOTAL SUSPENDED SOLIDS
TSS 75 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 5 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033515
Collection Date: 13-Oct-15 12:50 PM
Site: S-01
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:30 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 62 mg/L EPA 300.0 10/15/2015 17:52 BGN9034110
Sulfate 43 mg/L EPA 300.0 10/15/2015 17:52 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.020 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.005 1
Barium (Ba)0.140 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.005 1
Boron (B)1.63 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.05 1
Iron (Fe)12.5 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.01 1
Manganese (Mn)2.62 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.005 1
Strontium (Sr)0.351 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 10/19/2015 10:02 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)25.0 mg/L EPA 200.7 10/19/2015 13:52 FCJORDA0.01 1
Magnesium (Mg)8.69 mg/L EPA 200.7 10/19/2015 13:52 FCJORDA0.005 1
Potassium (K)1.86 mg/L EPA 200.7 10/19/2015 13:52 FCJORDA0.1 1
Sodium (Na)36.8 mg/L EPA 200.7 10/19/2015 13:52 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.023 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.005 1
Barium (Ba)0.144 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.005 1
Boron (B)1.64 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.05 1
Iron (Fe)12.8 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.01 1
Manganese (Mn)2.68 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.005 1
Strontium (Sr)0.365 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.005 1
Zinc (Zn)0.014 mg/L EPA 200.7 10/16/2015 10:44 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 6 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033515
Collection Date: 13-Oct-15 12:50 PM
Site: S-01
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Arsenic (As)2.62 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Cobalt (Co)7.83 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:31 MHALL311
Thallium (Tl) Low Level 0.244 ug/L EPA 200.8 10/20/2015 17:31 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 17:31 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Arsenic (As)2.65 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Cobalt (Co)7.57 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/21/2015 17:45 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 260 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 1.4 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 7 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033516
Collection Date: 13-Oct-15 2:00 PM
Site: S-02B
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.321 mg-N/L EPA 353.2 10/20/2015 13:31 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 64 mg/L EPA 300.0 10/15/2015 18:10 BGN9034110
Sulfate 28 mg/L EPA 300.0 10/15/2015 18:10 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.013 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.005 1
Barium (Ba)0.036 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.005 1
Boron (B)1.51 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.05 1
Iron (Fe)0.058 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.01 1
Manganese (Mn)3.37 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.005 1
Strontium (Sr)0.544 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 10/19/2015 10:06 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)36.9 mg/L EPA 200.7 10/19/2015 13:56 FCJORDA0.01 1
Magnesium (Mg)12.9 mg/L EPA 200.7 10/19/2015 13:56 FCJORDA0.005 1
Potassium (K)2.38 mg/L EPA 200.7 10/19/2015 13:56 FCJORDA0.1 1
Sodium (Na)17.6 mg/L EPA 200.7 10/19/2015 13:56 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.246 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.005 1
Barium (Ba)0.041 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.005 1
Boron (B)1.51 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.05 1
Iron (Fe)0.906 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.01 1
Manganese (Mn)3.37 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.005 1
Strontium (Sr)0.573 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 10/16/2015 10:48 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 8 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033516
Collection Date: 13-Oct-15 2:00 PM
Site: S-02B
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Cobalt (Co)2.62 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:37 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:37 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 17:37 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Cobalt (Co)2.61 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Copper (Cu)1.76 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA0.2 1
Vanadium (V) Low Level 0.550 ug/L EPA 200.8 10/21/2015 17:52 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 250 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 1.9 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 44 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 9 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033517
Collection Date: 13-Oct-15 1:35 PM
Site: S-02
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.024 mg-N/L EPA 353.2 10/20/2015 13:34 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 87 mg/L EPA 300.0 10/15/2015 18:27 BGN9034110
Sulfate 41 mg/L EPA 300.0 10/15/2015 18:27 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.008 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.005 1
Barium (Ba)0.156 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.005 1
Boron (B)1.77 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.05 1
Iron (Fe)3.98 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.01 1
Manganese (Mn)2.39 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.005 1
Strontium (Sr)0.547 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 10/19/2015 10:10 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)29.9 mg/L EPA 200.7 10/19/2015 14:00 FCJORDA0.01 1
Magnesium (Mg)13.9 mg/L EPA 200.7 10/19/2015 14:00 FCJORDA0.005 1
Potassium (K)2.99 mg/L EPA 200.7 10/19/2015 14:00 FCJORDA0.1 1
Sodium (Na)21.1 mg/L EPA 200.7 10/19/2015 14:00 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.009 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.005 1
Barium (Ba)0.166 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.005 1
Boron (B)1.81 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.05 1
Iron (Fe)4.27 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.01 1
Manganese (Mn)2.51 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.005 1
Strontium (Sr)0.581 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 10/16/2015 10:52 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 10 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033517
Collection Date: 13-Oct-15 1:35 PM
Site: S-02
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Cobalt (Co)12.2 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Nickel (Ni)1.95 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:09 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:09 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 17:09 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Cobalt (Co)12.2 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Nickel (Ni)1.98 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/21/2015 17:59 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 290 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 1.2 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 11 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033518
Collection Date: 13-Oct-15 10:55 AM
Site: S-06
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:35 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 12 mg/L EPA 300.0 10/15/2015 20:15 BGN9034110
Sulfate 5.4 mg/L EPA 300.0 10/15/2015 20:15 BGN90340.1 1
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.016 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.005 1
Barium (Ba)0.025 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.05 1
Iron (Fe)0.338 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.01 1
Manganese (Mn)0.134 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.005 1
Strontium (Sr)0.100 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 10/19/2015 10:14 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)14.9 mg/L EPA 200.7 10/19/2015 14:03 FCJORDA0.01 1
Magnesium (Mg)5.25 mg/L EPA 200.7 10/19/2015 14:03 FCJORDA0.005 1
Potassium (K)2.05 mg/L EPA 200.7 10/19/2015 14:03 FCJORDA0.1 1
Sodium (Na)13.6 mg/L EPA 200.7 10/19/2015 14:03 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.075 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.005 1
Barium (Ba)0.029 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.05 1
Iron (Fe)0.747 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.01 1
Manganese (Mn)0.193 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.005 1
Strontium (Sr)0.104 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 10/15/2015 15:51 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 12 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033518
Collection Date: 13-Oct-15 10:55 AM
Site: S-06
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:42 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:42 MHALL30.2 1
Vanadium (V) Low Level 0.345 ug/L EPA 200.8 10/20/2015 17:42 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA0.2 1
Vanadium (V) Low Level 0.649 ug/L EPA 200.8 10/21/2015 14:50 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 130 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 4.1 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 13 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033519
Collection Date: 13-Oct-15 11:30 AM
Site: SW-REF1
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:36 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 6.6 mg/L EPA 300.0 10/15/2015 19:03 BGN90340.1 1
Sulfate 4.0 mg/L EPA 300.0 10/15/2015 19:03 BGN90340.1 1
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.016 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.005 1
Barium (Ba)0.035 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.05 1
Iron (Fe)0.525 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.01 1
Manganese (Mn)0.212 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.005 1
Strontium (Sr)0.071 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 10/19/2015 10:18 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)8.57 mg/L EPA 200.7 10/19/2015 14:07 FCJORDA0.01 1
Magnesium (Mg)3.51 mg/L EPA 200.7 10/19/2015 14:07 FCJORDA0.005 1
Potassium (K)2.07 mg/L EPA 200.7 10/19/2015 14:07 FCJORDA0.1 1
Sodium (Na)8.58 mg/L EPA 200.7 10/19/2015 14:07 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.754 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.005 1
Barium (Ba)0.051 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.05 1
Iron (Fe)3.88 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.01 1
Manganese (Mn)1.18 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.005 1
Strontium (Sr)0.070 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 10/16/2015 10:56 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 14 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033519
Collection Date: 13-Oct-15 11:30 AM
Site: SW-REF1
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:48 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:48 MHALL30.2 1
Vanadium (V) Low Level 0.360 ug/L EPA 200.8 10/20/2015 17:48 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Chromium (Cr)1.42 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Cobalt (Co)4.72 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Copper (Cu)1.21 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Nickel (Ni)1.20 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA0.2 1
Vanadium (V) Low Level 2.37 ug/L EPA 200.8 10/21/2015 18:06 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 94 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 7.6 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI110
TOTAL SUSPENDED SOLIDS
TSS 66 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 15 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033520
Collection Date: 13-Oct-15 12:20 PM
Site: S-05
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:37 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 64 mg/L EPA 300.0 10/15/2015 19:21 BGN9034110
Sulfate 63 mg/L EPA 300.0 10/15/2015 19:21 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.026 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.005 1
Barium (Ba)0.062 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.005 1
Boron (B)1.56 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.05 1
Iron (Fe)0.010 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.005 1
Strontium (Sr)0.250 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 10/19/2015 10:21 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)38.8 mg/L EPA 200.7 10/19/2015 14:11 FCJORDA0.01 1
Magnesium (Mg)12.9 mg/L EPA 200.7 10/19/2015 14:11 FCJORDA0.005 1
Potassium (K)5.08 mg/L EPA 200.7 10/19/2015 14:11 FCJORDA0.1 1
Sodium (Na)10.9 mg/L EPA 200.7 10/19/2015 14:11 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.064 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.005 1
Barium (Ba)0.065 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.005 1
Boron (B)1.53 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.05 1
Iron (Fe)0.134 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.01 1
Manganese (Mn)0.094 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.005 1
Strontium (Sr)0.255 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.005 1
Zinc (Zn)0.011 mg/L EPA 200.7 10/16/2015 11:00 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 16 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033520
Collection Date: 13-Oct-15 12:20 PM
Site: S-05
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Arsenic (As)1.80 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Copper (Cu)1.58 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Molybdenum (Mo)15.4 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Nickel (Ni)1.86 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:53 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:53 MHALL30.2 1
Vanadium (V) Low Level 0.605 ug/L EPA 200.8 10/20/2015 17:53 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Arsenic (As)2.28 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Copper (Cu)1.41 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Molybdenum (Mo)15.7 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Nickel (Ni)1.90 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA0.2 1
Vanadium (V) Low Level 0.930 ug/L EPA 200.8 10/21/2015 18:13 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 270 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 4.8 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 17 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033521
Collection Date: 13-Oct-15 12:20 PM
Site: S-05 Dup
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.016 mg-N/L EPA 353.2 10/20/2015 13:38 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 63 mg/L EPA 300.0 10/15/2015 19:39 BGN9034110
Sulfate 63 mg/L EPA 300.0 10/15/2015 19:39 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.025 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.005 1
Barium (Ba)0.061 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.005 1
Boron (B)1.55 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.05 1
Iron (Fe)0.012 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.005 1
Strontium (Sr)0.247 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 10/19/2015 10:25 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)39.3 mg/L EPA 200.7 10/19/2015 14:15 FCJORDA0.01 1
Magnesium (Mg)13.1 mg/L EPA 200.7 10/19/2015 14:15 FCJORDA0.005 1
Potassium (K)5.17 mg/L EPA 200.7 10/19/2015 14:15 FCJORDA0.1 1
Sodium (Na)11.0 mg/L EPA 200.7 10/19/2015 14:15 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.044 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.005 1
Barium (Ba)0.064 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.005 1
Boron (B)1.54 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.05 1
Iron (Fe)0.081 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.01 1
Manganese (Mn)0.062 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.005 1
Strontium (Sr)0.256 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 10/15/2015 15:55 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 18 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033521
Collection Date: 13-Oct-15 12:20 PM
Site: S-05 Dup
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Arsenic (As)1.72 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Copper (Cu)1.49 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Molybdenum (Mo)15.3 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Nickel (Ni)1.71 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 17:59 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 17:59 MHALL30.2 1
Vanadium (V) Low Level 0.612 ug/L EPA 200.8 10/20/2015 17:59 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Arsenic (As)2.12 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Copper (Cu)1.38 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Molybdenum (Mo)16.0 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Nickel (Ni)1.55 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA0.2 1
Vanadium (V) Low Level 0.919 ug/L EPA 200.8 10/21/2015 15:39 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 280 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 4.7 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 19 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033522
Collection Date: 13-Oct-15 3:10 PM
Site: SW-CB1
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.038 mg-N/L EPA 353.2 10/20/2015 13:40 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 66 mg/L EPA 300.0 10/15/2015 19:57 BGN9034110
Sulfate 33 mg/L EPA 300.0 10/15/2015 19:57 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.005 1
Barium (Ba)0.071 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.005 1
Boron (B)1.30 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.05 1
Iron (Fe)0.410 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.01 1
Manganese (Mn)1.29 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.005 1
Strontium (Sr)0.435 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.005 1
Zinc (Zn)0.038 mg/L EPA 200.7 10/19/2015 10:37 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)29.4 mg/L EPA 200.7 10/19/2015 14:19 FCJORDA0.01 1
Magnesium (Mg)11.1 mg/L EPA 200.7 10/19/2015 14:19 FCJORDA0.005 1
Potassium (K)2.54 mg/L EPA 200.7 10/19/2015 14:19 FCJORDA0.1 1
Sodium (Na)24.4 mg/L EPA 200.7 10/19/2015 14:19 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.056 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.005 1
Barium (Ba)0.075 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.005 1
Boron (B)1.31 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.05 1
Iron (Fe)0.776 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.01 1
Manganese (Mn)1.35 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.005 1
Strontium (Sr)0.454 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 10/16/2015 11:03 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 20 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033522
Collection Date: 13-Oct-15 3:10 PM
Site: SW-CB1
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Cobalt (Co)1.78 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 18:04 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 18:04 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 18:04 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Cobalt (Co)1.68 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/21/2015 18:20 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 270 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 2.3 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 7.0 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 21 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033523
Collection Date: 13-Oct-15 2:55 PM
Site: S-03
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.043 mg-N/L EPA 353.2 10/20/2015 13:41 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 70 mg/L EPA 300.0 10/15/2015 22:20 BGN9034110
Sulfate 34 mg/L EPA 300.0 10/15/2015 22:20 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.007 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.005 1
Barium (Ba)0.071 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.005 1
Boron (B)1.47 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.05 1
Iron (Fe)0.151 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.01 1
Manganese (Mn)2.10 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.005 1
Strontium (Sr)0.504 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.005 1
Zinc (Zn)0.022 mg/L EPA 200.7 10/19/2015 10:40 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)32.4 mg/L EPA 200.7 10/19/2015 14:23 FCJORDA0.01 1
Magnesium (Mg)12.1 mg/L EPA 200.7 10/19/2015 14:23 FCJORDA0.005 1
Potassium (K)2.62 mg/L EPA 200.7 10/19/2015 14:23 FCJORDA0.1 1
Sodium (Na)23.5 mg/L EPA 200.7 10/19/2015 14:23 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.383 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.005 1
Barium (Ba)0.108 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.005 1
Boron (B)1.49 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.05 1
Iron (Fe)2.67 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.01 1
Manganese (Mn)4.37 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.005 1
Strontium (Sr)0.538 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 10/15/2015 15:58 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 22 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033523
Collection Date: 13-Oct-15 2:55 PM
Site: S-03
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Cobalt (Co)1.94 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 18:10 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 18:10 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 18:10 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Cobalt (Co)6.29 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Nickel (Ni)1.21 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA0.2 1
Vanadium (V) Low Level 0.934 ug/L EPA 200.8 10/21/2015 15:46 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 240 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 3.6 mg/L SM5310C/EPA9060A 10/19/2015 14:40 GHUTCHI110
TOTAL SUSPENDED SOLIDS
TSS 45 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 23 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033524
Collection Date: 13-Oct-15 2:17 PM
Site: S-08
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:47M2 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 98 mg/L EPA 300.0 10/16/2015 01:01 BGN9034220
Sulfate 61 mg/L EPA 300.0 10/16/2015 01:01 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.018 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.005 1
Barium (Ba)0.089 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.005 1
Boron (B)1.82 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.05 1
Iron (Fe)0.150 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.01 1
Manganese (Mn)1.69 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.005 1
Strontium (Sr)0.524 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 10/19/2015 10:44 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)32.8 mg/L EPA 200.7 10/19/2015 15:08 FCJORDA0.01 1
Magnesium (Mg)19.0 mg/L EPA 200.7 10/19/2015 15:08 FCJORDA0.005 1
Potassium (K)4.16 mg/L EPA 200.7 10/19/2015 15:08 FCJORDA0.1 1
Sodium (Na)20.8 mg/L EPA 200.7 10/19/2015 15:08 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)16.3 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.05 10
Barium (Ba)0.643 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.05 10
Boron (B)1.87 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.5 10
Iron (Fe)72.6 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.1 10
Manganese (Mn)19.1 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.05 10
Strontium (Sr)0.647 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.05 10
Zinc (Zn)0.086 mg/L EPA 200.7 10/16/2015 09:57 FCJORDA0.05 10
Analytical Lab Revised 11/04/2015
Page 24 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033524
Collection Date: 13-Oct-15 2:17 PM
Site: S-08
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Cobalt (Co)4.32 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Nickel (Ni)1.32 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 18:59 MHALL311
Thallium (Tl) Low Level 0.206 ug/L EPA 200.8 10/20/2015 18:59 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 18:59 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Arsenic (As)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Beryllium (Be)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Cadmium (Cd)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Chromium (Cr)18.6 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Cobalt (Co)158 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Copper (Cu)12.7 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Lead (Pb)20.6 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Molybdenum (Mo)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Nickel (Ni)19.0 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Selenium (Se)< 10 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA1010
Thallium (Tl) Low Level < 2 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA210
Vanadium (V) Low Level 24.4 ug/L EPA 200.8 10/21/2015 15:53 JAHERMA310
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 520 mg/L SM2540C 10/14/2015 15:37 CJELLIO501
Total Carbon
TOC 6.2 mg/L SM5310C/EPA9060A 10/20/2015 13:36 GHUTCHI110
TOTAL SUSPENDED SOLIDS
TSS 11000 mg/L SM2540D 10/14/2015 10:16 CJELLIO2501
Analytical Lab Revised 11/04/2015
Page 25 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033525
Collection Date: 13-Oct-15 3:55 PM
Site: SW-CB2
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 10/20/2015 13:51M2 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 28 mg/L EPA 300.0 10/15/2015 21:27 BGN9034110
Sulfate 12 mg/L EPA 300.0 10/15/2015 21:27 BGN9034110
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
DISSOLVED METALS BY ICP
Aluminum (Al)0.015 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.005 1
Barium (Ba)0.061 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.005 1
Boron (B)0.414 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.05 1
Iron (Fe)0.743 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.01 1
Manganese (Mn)3.58 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.005 1
Strontium (Sr)0.202 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.005 1
Zinc (Zn)0.015 mg/L EPA 200.7 10/19/2015 11:00 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)16.8 mg/L EPA 200.7 10/19/2015 15:12 FCJORDA0.01 1
Magnesium (Mg)6.24 mg/L EPA 200.7 10/19/2015 15:12 FCJORDA0.005 1
Potassium (K)3.07 mg/L EPA 200.7 10/19/2015 15:12 FCJORDA0.1 1
Sodium (Na)11.6 mg/L EPA 200.7 10/19/2015 15:12 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.147 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.005 1
Barium (Ba)0.069 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.005 1
Boron (B)0.422 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.05 1
Iron (Fe)4.36 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.01 1
Manganese (Mn)3.80 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.005 1
Strontium (Sr)0.218 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 10/15/2015 16:06 FCJORDA0.005 1
Analytical Lab Revised 11/04/2015
Page 26 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033525
Collection Date: 13-Oct-15 3:55 PM
Site: SW-CB2
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Cobalt (Co)2.73 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 19:05 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 19:05 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 19:05 MHALL30.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Cobalt (Co)2.77 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA0.2 1
Vanadium (V) Low Level 0.805 ug/L EPA 200.8 10/21/2015 16:00 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 160 mg/L SM2540C 10/14/2015 15:37 CJELLIO251
Total Carbon
TOC 8.7 mg/L SM5310C/EPA9060A 10/20/2015 13:36 GHUTCHI110
TOTAL SUSPENDED SOLIDS
TSS 14 mg/L SM2540D 10/14/2015 10:16 CJELLIO51
Analytical Lab Revised 11/04/2015
Page 27 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033526
Collection Date: 13-Oct-15 5:58 PM
Site: Filter Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 10/19/2015 11:04 FCJORDA0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 10/20/2015 19:10 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 10/20/2015 19:10 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 10/20/2015 19:10 MHALL30.3 1
Analytical Lab Revised 11/04/2015
Page 28 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033527
Collection Date: 13-Oct-15 5:55 PM
Site: FIELD BLANK
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Analytical Lab Revised 11/04/2015
Page 29 of 95
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15100326
2015033528
Collection Date: 13-Oct-15 6:00 PM
Site: Trip Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.
Analytical Lab Revised 11/04/2015
Page 30 of 95
Analytical Lab Revised 11/04/2015
Page 31 of 95
Analytical Lab Revised 11/04/2015
Page 32 of 95
Analytical Lab Revised 11/04/2015
Page 33 of 95
Analytical Lab Revised 11/04/2015
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Page 35 of 95
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Page 36 of 95
Analytical Lab Revised 11/04/2015
Page 37 of 95
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QJ14052Lot Number:
AB GW Assessment Water -Project Name:
10/19/2015Date Completed:
Grant Wilton
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 42
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QJ14052
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: AB GW Assessment Water -
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 42
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QJ14052

Project Name: AB GW Assessment Water -
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 10/13/2015 13102015033514Aqueous 10/14/2015
002 10/13/2015 12502015033515Aqueous 10/14/2015
003 10/13/2015 14002015033516Aqueous 10/14/2015
004 10/13/2015 13352015033517Aqueous 10/14/2015
005 10/13/2015 10552015033518Aqueous 10/14/2015
006 10/13/2015 11302015033519Aqueous 10/14/2015
007 10/13/2015 12202015033520Aqueous 10/14/2015
008 10/13/2015 12202015033521Aqueous 10/14/2015
009 10/13/2015 15102015033522Aqueous 10/14/2015
010 10/13/2015 14552015033523Aqueous 10/14/2015
011 10/13/2015 14172015033524Aqueous 10/14/2015
012 10/13/2015 15552015033525Aqueous 10/14/2015
013 10/13/2015 17552015033527Aqueous 10/14/2015
014 10/13/2015 18002015033528Aqueous 10/14/2015
(14 samples)
Page: 3 of 42
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QJ14052

Project Name: AB GW Assessment Water -
Project Number:
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 2015033514 Aqueous Alkalinity SM 2320B-60 mg/L 5
001 2015033514 Aqueous Bicarbonate Alkalinity SM 2320B-60 mg/L 5
001 2015033514 Aqueous Mercury (CVAFS)1631E 4.25 ng/L 7
002 2015033515 Aqueous Alkalinity SM 2320B-64 mg/L 8
002 2015033515 Aqueous Bicarbonate Alkalinity SM 2320B-64 mg/L 8
002 2015033515 Aqueous Methane RSK - 175 34 ug/L 9
003 2015033516 Aqueous Alkalinity SM 2320B-67 mg/L 11
003 2015033516 Aqueous Bicarbonate Alkalinity SM 2320B-67 mg/L 11
003 2015033516 Aqueous Mercury (CVAFS)1631E 3.34 ng/L 13
004 2015033517 Aqueous Alkalinity SM 2320B-28 mg/L 14
004 2015033517 Aqueous Bicarbonate Alkalinity SM 2320B-28 mg/L 14
005 2015033518 Aqueous Alkalinity SM 2320B-61 mg/L 17
005 2015033518 Aqueous Bicarbonate Alkalinity SM 2320B-61 mg/L 17
005 2015033518 Aqueous Methane RSK - 175 26 ug/L 18
005 2015033518 Aqueous Mercury (CVAFS)1631E 1.25 ng/L 19
006 2015033519 Aqueous Alkalinity SM 2320B-39 mg/L 20
006 2015033519 Aqueous Bicarbonate Alkalinity SM 2320B-39 mg/L 20
006 2015033519 Aqueous Methane RSK - 175 26 ug/L 21
006 2015033519 Aqueous Mercury (CVAFS)1631E 5.32 ng/L 22
007 2015033520 Aqueous Alkalinity SM 2320B-27 mg/L 23
007 2015033520 Aqueous Bicarbonate Alkalinity SM 2320B-27 mg/L 23
008 2015033521 Aqueous Alkalinity SM 2320B-27 mg/L 26
008 2015033521 Aqueous Bicarbonate Alkalinity SM 2320B-27 mg/L 26
009 2015033522 Aqueous Alkalinity SM 2320B-46 mg/L 29
009 2015033522 Aqueous Bicarbonate Alkalinity SM 2320B-46 mg/L 29
009 2015033522 Aqueous Methane RSK - 175 52 ug/L 30
009 2015033522 Aqueous Mercury (CVAFS)1631E 3.95 ng/L 31
010 2015033523 Aqueous Alkalinity SM 2320B-49 mg/L 32
010 2015033523 Aqueous Bicarbonate Alkalinity SM 2320B-49 mg/L 32
010 2015033523 Aqueous Methane RSK - 175 20 ug/L 33
010 2015033523 Aqueous Mercury (CVAFS)1631E 8.67 ng/L 34
011 2015033524 Aqueous Alkalinity SM 2320B-16 mg/L 35
011 2015033524 Aqueous Bicarbonate Alkalinity SM 2320B-16 mg/L 35
011 2015033524 Aqueous Methane RSK - 175 10 ug/L 36
011 2015033524 Aqueous Mercury (CVAFS)1631E 8.98 ng/L 37
012 2015033525 Aqueous Alkalinity SM 2320B-45 mg/L 38
012 2015033525 Aqueous Bicarbonate Alkalinity SM 2320B-45 mg/L 38
012 2015033525 Aqueous Methane RSK - 175 86 ug/L 39
012 2015033525 Aqueous Mercury (CVAFS)1631E 3.32 ng/L 40
(39 detections)
Page: 4 of 42
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033514
QJ14052-001
10/13/2015 1310
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2224 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2224 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2224 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 60 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 60 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 42
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033514
QJ14052-001
10/13/2015 1310
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1709 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 42
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Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033514
QJ14052-001
10/13/2015 1310
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1426 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 4.25 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 42
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033515
QJ14052-002
10/13/2015 1250
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2241 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2241 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2241 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 64 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 64 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 42
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033515
QJ14052-002
10/13/2015 1250
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1726 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 34 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 42
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Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033515
QJ14052-002
10/13/2015 1250
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1442 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 42
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033516
QJ14052-003
10/13/2015 1400
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2247 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2247 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2247 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 67 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 67 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 42
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033516
QJ14052-003
10/13/2015 1400
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1743 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 42
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Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033516
QJ14052-003
10/13/2015 1400
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1447 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 3.34 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 42
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033517
QJ14052-004
10/13/2015 1335
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2252 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2252 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2252 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 28 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 28 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 42
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033517
QJ14052-004
10/13/2015 1335
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1759 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 42
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Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033517
QJ14052-004
10/13/2015 1335
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1452 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 42
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033518
QJ14052-005
10/13/2015 1055
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2258 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2258 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2258 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 61 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 61 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033518
QJ14052-005
10/13/2015 1055
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1816 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 26 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033518
QJ14052-005
10/13/2015 1055
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1458 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 1.25 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033519
QJ14052-006
10/13/2015 1130
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2304 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2304 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2304 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 39 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 39 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033519
QJ14052-006
10/13/2015 1130
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1833 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 26 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033519
QJ14052-006
10/13/2015 1130
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1513 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 5.32 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033520
QJ14052-007
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2310 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2310 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2310 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 27 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 27 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033520
QJ14052-007
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1850 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033520
QJ14052-007
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1518 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033521
QJ14052-008
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2329 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2329 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2329 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 27 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 27 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033521
QJ14052-008
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1906 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033521
QJ14052-008
10/13/2015 1220
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1523 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033522
QJ14052-009
10/13/2015 1510
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2335 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2335 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2335 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 46 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 46 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033522
QJ14052-009
10/13/2015 1510
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1923 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 52 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033522
QJ14052-009
10/13/2015 1510
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1528 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 3.95 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033523
QJ14052-010
10/13/2015 1455
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2340 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2340 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2340 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 49 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 49 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033523
QJ14052-010
10/13/2015 1455
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 1940 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 20 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033523
QJ14052-010
10/13/2015 1455
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1549 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 8.67 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 34 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033524
QJ14052-011
10/13/2015 1417
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2346 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2346 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2346 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 16 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 16 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 35 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033524
QJ14052-011
10/13/2015 1417
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 2010 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 10 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 36 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033524
QJ14052-011
10/13/2015 1417
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1554 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 8.98 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 37 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033525
QJ14052-012
10/13/2015 1555
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 10/15/2015 2352 HMA 87374
1 (Bicarbonate ) SM 2320B-2011 1 10/15/2015 2352 BWS
1 (Carbonate Al) SM 2320B-2011 1 10/15/2015 2352 BWS
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 45 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 45 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 38 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033525
QJ14052-012
10/13/2015 1555
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/16/2015 2027 JJG 87454
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 86 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 39 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033525
QJ14052-012
10/13/2015 1555
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1559 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E 3.32 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 40 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033527
QJ14052-013
10/13/2015 1755
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1401 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 41 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015033528
QJ14052-014
10/13/2015 1800
10/14/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 10/15/2015 1406 BNW 10/14/2015 1815 87300
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 42 of 42
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

QC Summary
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:QQ87374-001
87374
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 10/15/2015 221210mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:QQ87374-002
87374
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 91 10/15/2015 22189110090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:QJ14052-001MS
87374
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 150 10/15/2015 22308710070-130601
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:QJ14052-001MD
87374
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 150 10/15/2015 22368510070-1301.3 20601
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ87454-001
87454
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 10/16/2015 140310ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ87454-002
87454
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 350 10/16/2015 124411930070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ87454-003
87454
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 360 10/16/2015 125912130070-1302.3 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS) - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ87300-001
87300 1631E
10/14/2015 1815Analytical Method:1631E
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Mercury (CVAFS)ND 10/15/2015 16090.500 ng/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ87300-002
87300 1631E
10/14/2015 1815Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ng/L)(ng/L)
Mercury (CVAFS)5.24 10/15/2015 16151055.00 75-1251
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS) - MS
Batch:Prep Method:
Prep Date:
Sample ID:QJ14052-005MS
87300 1631E
10/14/2015 1815Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ng/L)(ng/L)(ng/L)
Mercury (CVAFS)6.36 10/15/2015 15031025.00 71-1251.25 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Mercury (CVAFS) - MSD
Batch:Prep Method:
Prep Date:
Sample ID:QJ14052-005MD
87300 1631E
10/14/2015 1815Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ng/L)(ng/L)(ng/L)
Mercury (CVAFS)6.7 10/15/2015 15081095.00 71-1255.2 241.25 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QJ14052
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Analytical Lab Revised 11/04/2015
Page 95 of 95