NC0038377_J15090237report_20171101

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15090237
Project Name:MAYO STEAM - AB GW ASSESSMENT WATER
Lab Contact:Mary Ann Ogle
Date:9/18/2015
Customer Address:
Customer Name(s):Tim Hunsucker, Jerry Wylie,Brandon Russo, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Page 1 of 72
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015030018 MAYO STEAM 10-Sep-15 9:28 AM Erin Black AMBW-01
2015030019 MAYO STEAM 10-Sep-15 10:20 AM Erin Black ABMW-02
2015030020 MAYO STEAM 10-Sep-15 9:50 AM Erin Black AMBW-02BR
2015030021 MAYO STEAM 10-Sep-15 2:22 PM Erin Black AMBW-03
2015030022 MAYO STEAM 10-Sep-15 2:40 PM Erin Black ABMW-03S
2015030023 MAYO STEAM 10-Sep-15 1:44 PM Erin Black BG-1
2015030024 MAYO STEAM 10-Sep-15 10:27 AM Erin Black MW-12S
2015030025 MAYO STEAM 10-Sep-15 2:15 PM Erin Black MW-12D
2015030026 MAYO STEAM 10-Sep-15 12:45 PM Erin Black Filter Blank
2015030027 MAYO STEAM 10-Sep-15 12:45 PM Erin Black Equipment Blank
10 Total Samples
Page 2 of 72
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:9/18/2015
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030018
Collection Date:10-Sep-15 9:28 AM
Site:AMBW-01
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.020 mg-N/L EPA 353.2 09/14/2015 14:01 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 16 mg/L EPA 300.0 09/11/2015 15:29 BGN9034110
Sulfate 3.6 mg/L EPA 300.0 09/11/2015 15:29 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 15:53 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 13:39 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:40 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.055 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.005 1
Barium (Ba)1.18 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.005 1
Boron (B)3.83 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.05 1
Iron (Fe)3.49 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.01 1
Manganese (Mn)3.06 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.005 1
Strontium (Sr)4.30 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.005 1
Zinc (Zn)0.019 mg/L EPA 200.7 09/15/2015 11:04 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.025 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.005 1
Barium (Ba)1.10 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.005 1
Boron (B)3.81 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.05 1
Iron (Fe)0.010 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.01 1
Manganese (Mn)2.89 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.005 1
Strontium (Sr)4.19 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 14:50 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)132 mg/L EPA 200.7 09/16/2015 09:08M4 FCJORDA0.1 10
Magnesium (Mg)49.8 mg/L EPA 200.7 09/16/2015 09:08 FCJORDA0.005 1
Potassium (K)23.9 mg/L EPA 200.7 09/16/2015 09:08 FCJORDA0.1 1
Sodium (Na)19.7 mg/L EPA 200.7 09/16/2015 09:08 FCJORDA0.05 1
Page 4 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030018
Collection Date:10-Sep-15 9:28 AM
Site:AMBW-01
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.043 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.005 1
Barium (Ba)1.28 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.005 1
Boron (B)3.85 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.05 1
Iron (Fe)4.99 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.01 1
Manganese (Mn)3.43 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.005 1
Strontium (Sr)4.64 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:41 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)17.2 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Arsenic (As)222 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Cobalt (Co)14.0 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Molybdenum (Mo)161 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Nickel (Ni)11.1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA11
Thallium (Tl) Low Level 2.62 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA0.2 1
Vanadium (V) Low Level 64.9 ug/L EPA 200.8 09/15/2015 23:17 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)16.5 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Arsenic (As)123 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Cobalt (Co)12.6 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Molybdenum (Mo)159 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Nickel (Ni)10.4 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:25 MHALL311
Thallium (Tl) Low Level 2.20 ug/L EPA 200.8 09/15/2015 15:25 MHALL30.2 1
Vanadium (V) Low Level 19.0 ug/L EPA 200.8 09/15/2015 15:25 MHALL30.3 1
Page 5 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030018
Collection Date:10-Sep-15 9:28 AM
Site:AMBW-01
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)14.3 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Arsenic (As)269 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Cobalt (Co)16.4 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Molybdenum (Mo)145 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Nickel (Ni)15.7 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:38 MHALL311
Thallium (Tl) Low Level 2.36 ug/L EPA 200.8 09/15/2015 18:38 MHALL30.2 1
Vanadium (V) Low Level 65.8 ug/L EPA 200.8 09/15/2015 18:38 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 650 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 2.6 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 17 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 6 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030019
Collection Date:10-Sep-15 10:20 AM
Site:ABMW-02
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 14:02 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 13 mg/L EPA 300.0 09/11/2015 14:22 BGN9034110
Sulfate 19 mg/L EPA 300.0 09/11/2015 14:22 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 15:55 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 13:41 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:43 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.030 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.005 1
Barium (Ba)0.167 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.005 1
Boron (B)8.10 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.05 1
Iron (Fe)0.674 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.01 1
Manganese (Mn)1.17 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.005 1
Strontium (Sr)1.54 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 11:16 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.026 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.005 1
Barium (Ba)0.163 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.005 1
Boron (B)7.94 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.05 1
Iron (Fe)0.182 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.01 1
Manganese (Mn)1.14 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.005 1
Strontium (Sr)1.54 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 15:01 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)74.3 mg/L EPA 200.7 09/16/2015 09:19 FCJORDA0.01 1
Magnesium (Mg)22.9 mg/L EPA 200.7 09/16/2015 09:19 FCJORDA0.005 1
Potassium (K)16.2 mg/L EPA 200.7 09/16/2015 09:19 FCJORDA0.1 1
Sodium (Na)24.2 mg/L EPA 200.7 09/16/2015 09:19 FCJORDA0.05 1
Page 7 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030019
Collection Date:10-Sep-15 10:20 AM
Site:ABMW-02
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.144 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.005 1
Barium (Ba)0.166 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.005 1
Boron (B)8.36 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.05 1
Iron (Fe)0.731 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.01 1
Manganese (Mn)1.23 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.005 1
Strontium (Sr)1.55 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:53 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Arsenic (As)570 ug/L EPA 200.8 09/15/2015 22:58M4 JAHERMA110
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Molybdenum (Mo)1150 ug/L EPA 200.8 09/15/2015 22:58M4 JAHERMA110
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA0.2 1
Vanadium (V) Low Level 2.79 ug/L EPA 200.8 09/15/2015 22:58 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Arsenic (As)529 ug/L EPA 200.8 09/15/2015 15:40 MHALL31010
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Molybdenum (Mo)1100 ug/L EPA 200.8 09/15/2015 15:40 MHALL31010
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:40 MHALL311
Thallium (Tl) Low Level 0.845 ug/L EPA 200.8 09/15/2015 15:40 MHALL30.2 1
Vanadium (V) Low Level 2.10 ug/L EPA 200.8 09/15/2015 15:40 MHALL30.3 1
Page 8 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030019
Collection Date:10-Sep-15 10:20 AM
Site:ABMW-02
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Arsenic (As)600 ug/L EPA 200.8 09/15/2015 18:43 MHALL31010
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Molybdenum (Mo)1880 ug/L EPA 200.8 09/15/2015 18:43 MHALL31010
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:43 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 18:43 MHALL30.2 1
Vanadium (V) Low Level 2.60 ug/L EPA 200.8 09/15/2015 18:43 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 420 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 10 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.5 5
TOTAL SUSPENDED SOLIDS
TSS 6.0 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 9 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030020
Collection Date:10-Sep-15 9:50 AM
Site:AMBW-02BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 14:03 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 25 mg/L EPA 300.0 09/14/2015 08:22 BGN9034110
Sulfate 7.8 mg/L EPA 300.0 09/14/2015 08:22 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 15:58 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 13:44 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:45 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.006 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.005 1
Barium (Ba)0.126 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.05 1
Iron (Fe)0.639 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.01 1
Manganese (Mn)0.183 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.005 1
Strontium (Sr)1.06 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 11:20 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.005 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.005 1
Barium (Ba)0.125 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.05 1
Iron (Fe)0.060 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.01 1
Manganese (Mn)0.181 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.005 1
Strontium (Sr)1.05 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 15:05 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)75.5 mg/L EPA 200.7 09/16/2015 09:23 FCJORDA0.01 1
Magnesium (Mg)13.0 mg/L EPA 200.7 09/16/2015 09:23 FCJORDA0.005 1
Potassium (K)5.49 mg/L EPA 200.7 09/16/2015 09:23 FCJORDA0.1 1
Sodium (Na)31.7 mg/L EPA 200.7 09/16/2015 09:23 FCJORDA0.05 1
Page 10 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030020
Collection Date:10-Sep-15 9:50 AM
Site:AMBW-02BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.081 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.005 1
Barium (Ba)0.129 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.05 1
Iron (Fe)0.804 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.01 1
Manganese (Mn)0.189 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.005 1
Strontium (Sr)1.03 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:57 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Arsenic (As)1.32 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Molybdenum (Mo)6.52 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA0.2 1
Vanadium (V) Low Level 0.509 ug/L EPA 200.8 09/15/2015 23:24 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Arsenic (As)1.16 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Molybdenum (Mo)5.94 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:45 MHALL311
Thallium (Tl) Low Level 0.291 ug/L EPA 200.8 09/15/2015 15:45 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 15:45 MHALL30.3 1
Page 11 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030020
Collection Date:10-Sep-15 9:50 AM
Site:AMBW-02BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Arsenic (As)1.32 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Molybdenum (Mo)6.00 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:49 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 18:49 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 18:49 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 350 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 1.3 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 8.0 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 12 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030021
Collection Date:10-Sep-15 2:22 PM
Site:AMBW-03
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.025 mg-N/L EPA 353.2 09/14/2015 14:04 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 58 mg/L EPA 300.0 09/14/2015 08:39 BGN9034110
Sulfate 0.43 mg/L EPA 300.0 09/14/2015 08:39 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 16:00 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 13:46 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:47 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.042 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.005 1
Barium (Ba)0.287 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.005 1
Boron (B)1.72 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.05 1
Iron (Fe)26.2 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.01 1
Manganese (Mn)1.23 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.005 1
Strontium (Sr)1.54 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 11:23 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.013 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.005 1
Barium (Ba)0.248 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.005 1
Boron (B)1.70 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.05 1
Iron (Fe)8.88 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.01 1
Manganese (Mn)1.17 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.005 1
Strontium (Sr)1.52 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 15:09 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)61.1 mg/L EPA 200.7 09/16/2015 09:27 FCJORDA0.01 1
Magnesium (Mg)14.2 mg/L EPA 200.7 09/16/2015 09:27 FCJORDA0.005 1
Potassium (K)11.8 mg/L EPA 200.7 09/16/2015 09:27 FCJORDA0.1 1
Sodium (Na)10.8 mg/L EPA 200.7 09/16/2015 09:27 FCJORDA0.05 1
Page 13 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030021
Collection Date:10-Sep-15 2:22 PM
Site:AMBW-03
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.047 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.005 1
Barium (Ba)0.278 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.005 1
Boron (B)1.75 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.05 1
Iron (Fe)23.3 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.01 1
Manganese (Mn)1.19 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.005 1
Strontium (Sr)1.53 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 11:02 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Arsenic (As)64.6 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Molybdenum (Mo)5.42 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA0.2 1
Vanadium (V) Low Level 0.574 ug/L EPA 200.8 09/15/2015 23:31 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Arsenic (As)24.5 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Molybdenum (Mo)4.66 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:50 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 15:50 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 15:50 MHALL30.3 1
Page 14 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030021
Collection Date:10-Sep-15 2:22 PM
Site:AMBW-03
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Arsenic (As)69.3 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Molybdenum (Mo)8.12 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:54 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 18:54 MHALL30.2 1
Vanadium (V) Low Level 0.347 ug/L EPA 200.8 09/15/2015 18:54 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 320 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 3.3 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 41 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 15 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030022
Collection Date:10-Sep-15 2:40 PM
Site:ABMW-03S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.022 mg-N/L EPA 353.2 09/14/2015 14:10M2 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 10 mg/L EPA 300.0 09/14/2015 08:56 BGN9034110
Sulfate 0.19 mg/L EPA 300.0 09/14/2015 08:56 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 16:03 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:12 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:50 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.038 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.005 1
Barium (Ba)0.021 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.005 1
Boron (B)1.12 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.05 1
Iron (Fe)9.43 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.01 1
Manganese (Mn)0.812 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.005 1
Strontium (Sr)0.085 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 09/15/2015 11:27 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.017 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.005 1
Barium (Ba)0.020 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.005 1
Boron (B)1.09 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.05 1
Iron (Fe)9.24 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.01 1
Manganese (Mn)0.808 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.005 1
Strontium (Sr)0.083 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.005 1
Zinc (Zn)0.017 mg/L EPA 200.7 09/15/2015 15:13 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)6.15 mg/L EPA 200.7 09/16/2015 09:31 FCJORDA0.01 1
Magnesium (Mg)1.07 mg/L EPA 200.7 09/16/2015 09:31 FCJORDA0.005 1
Potassium (K)1.26 mg/L EPA 200.7 09/16/2015 09:31 FCJORDA0.1 1
Sodium (Na)18.7 mg/L EPA 200.7 09/16/2015 09:31 FCJORDA0.05 1
Page 16 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030022
Collection Date:10-Sep-15 2:40 PM
Site:ABMW-03S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.158 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.005 1
Barium (Ba)0.025 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.005 1
Boron (B)1.13 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.05 1
Iron (Fe)10.4 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.01 1
Manganese (Mn)0.918 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.005 1
Strontium (Sr)0.092 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 09/15/2015 11:06 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Arsenic (As)2.24 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Cobalt (Co)5.09 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Nickel (Ni)1.78 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA0.2 1
Vanadium (V) Low Level 0.473 ug/L EPA 200.8 09/15/2015 23:37 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Arsenic (As)2.07 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Cobalt (Co)5.03 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:56 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 15:56 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 15:56 MHALL30.3 1
Page 17 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030022
Collection Date:10-Sep-15 2:40 PM
Site:ABMW-03S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Arsenic (As)2.44 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Cobalt (Co)5.33 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:59 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 18:59 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 18:59 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 120 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 1.5 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 5.0 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 18 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030023
Collection Date:10-Sep-15 1:44 PM
Site:BG-1
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.645 mg-N/L EPA 353.2 09/14/2015 14:15 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 11 mg/L EPA 300.0 09/11/2015 16:37 BGN9034110
Sulfate 0.37 mg/L EPA 300.0 09/11/2015 16:37 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 16:05 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:14 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.005 1
Barium (Ba)0.087 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.01 1
Manganese (Mn)0.015 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.005 1
Strontium (Sr)0.165 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.005 1
Zinc (Zn)0.022 mg/L EPA 200.7 09/15/2015 11:31 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)12.8 mg/L EPA 200.7 09/16/2015 09:35 FCJORDA0.01 1
Magnesium (Mg)3.41 mg/L EPA 200.7 09/16/2015 09:35 FCJORDA0.005 1
Potassium (K)1.38 mg/L EPA 200.7 09/16/2015 09:35 FCJORDA0.1 1
Sodium (Na)11.6 mg/L EPA 200.7 09/16/2015 09:35 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.276 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.005 1
Barium (Ba)0.091 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.05 1
Iron (Fe)0.300 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.01 1
Manganese (Mn)0.026 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.005 1
Strontium (Sr)0.172 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.005 1
Zinc (Zn)0.017 mg/L EPA 200.7 09/15/2015 11:10 MHH71310.005 1
Page 19 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030023
Collection Date:10-Sep-15 1:44 PM
Site:BG-1
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Nickel (Ni)1.46 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA0.2 1
Vanadium (V) Low Level 3.16 ug/L EPA 200.8 09/15/2015 23:44 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Nickel (Ni)1.78 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 19:04 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 19:04 MHALL30.2 1
Vanadium (V) Low Level 3.93 ug/L EPA 200.8 09/15/2015 19:04 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 120 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 0.913 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 8.0 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 20 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030024
Collection Date:10-Sep-15 10:27 AM
Site:MW-12S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.700 mg-N/L EPA 353.2 09/14/2015 14:16 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 3.1 mg/L EPA 300.0 09/11/2015 16:03 BGN90340.1 1
Sulfate 1.4 mg/L EPA 300.0 09/11/2015 16:03 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/15/2015 11:23 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:17 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:52 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.005 1
Barium (Ba)0.016 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.05 1
Iron (Fe)0.084 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.01 1
Manganese (Mn)0.242 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.005 1
Strontium (Sr)0.022 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.005 1
Zinc (Zn)0.059 mg/L EPA 200.7 09/15/2015 11:35 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.005 1
Barium (Ba)0.016 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.01 1
Manganese (Mn)0.240 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.005 1
Strontium (Sr)0.022 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.005 1
Zinc (Zn)0.073 mg/L EPA 200.7 09/15/2015 15:17 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)1.77 mg/L EPA 200.7 09/16/2015 09:38 FCJORDA0.01 1
Magnesium (Mg)0.723 mg/L EPA 200.7 09/16/2015 09:38 FCJORDA0.005 1
Potassium (K)1.53 mg/L EPA 200.7 09/16/2015 09:38 FCJORDA0.1 1
Sodium (Na)5.43 mg/L EPA 200.7 09/16/2015 09:38 FCJORDA0.05 1
Page 21 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030024
Collection Date:10-Sep-15 10:27 AM
Site:MW-12S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.098 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.005 1
Barium (Ba)0.019 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.05 1
Iron (Fe)0.108 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.01 1
Manganese (Mn)0.253 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.005 1
Strontium (Sr)0.023 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.005 1
Zinc (Zn)0.064 mg/L EPA 200.7 09/15/2015 11:14 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Cobalt (Co)1.11 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Nickel (Ni)1.82 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 23:50 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Cobalt (Co)1.15 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Nickel (Ni)1.52 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:01 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:01 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 16:01 MHALL30.3 1
Page 22 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030024
Collection Date:10-Sep-15 10:27 AM
Site:MW-12S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Chromium (Cr)3.23 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Cobalt (Co)1.02 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Nickel (Ni)2.98 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 19:09 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 19:09 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 19:09 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 55 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 0.633 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 23 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030025
Collection Date:10-Sep-15 2:15 PM
Site:MW-12D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.664 mg-N/L EPA 353.2 09/14/2015 14:17 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 4.1 mg/L EPA 300.0 09/11/2015 16:20 BGN90340.1 1
Sulfate 0.99 mg/L EPA 300.0 09/11/2015 16:20 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/15/2015 11:30 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:19 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:55 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.010 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.005 1
Barium (Ba)0.018 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.05 1
Iron (Fe)0.048 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.01 1
Manganese (Mn)0.207 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.005 1
Strontium (Sr)0.086 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 09/15/2015 11:39 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.005 1
Barium (Ba)0.017 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.05 1
Iron (Fe)0.029 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.01 1
Manganese (Mn)0.196 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.005 1
Strontium (Sr)0.084 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 09/15/2015 15:20 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)11.7 mg/L EPA 200.7 09/16/2015 09:42 FCJORDA0.01 1
Magnesium (Mg)3.04 mg/L EPA 200.7 09/16/2015 09:42 FCJORDA0.005 1
Potassium (K)1.41 mg/L EPA 200.7 09/16/2015 09:42 FCJORDA0.1 1
Sodium (Na)9.03 mg/L EPA 200.7 09/16/2015 09:42 FCJORDA0.05 1
Page 24 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030025
Collection Date:10-Sep-15 2:15 PM
Site:MW-12D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.220 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.005 1
Barium (Ba)0.020 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.05 1
Iron (Fe)0.277 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.01 1
Manganese (Mn)0.218 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.005 1
Strontium (Sr)0.085 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.005 1
Zinc (Zn)0.009 mg/L EPA 200.7 09/15/2015 11:18 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Nickel (Ni)1.38 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA0.2 1
Vanadium (V) Low Level 0.436 ug/L EPA 200.8 09/15/2015 23:57 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Nickel (Ni)1.32 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:06 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:06 MHALL30.2 1
Vanadium (V) Low Level 0.470 ug/L EPA 200.8 09/15/2015 16:06 MHALL30.3 1
Page 25 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030025
Collection Date:10-Sep-15 2:15 PM
Site:MW-12D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Chromium (Cr)1.10 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Nickel (Ni)1.35 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 18:23 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 18:23 MHALL30.2 1
Vanadium (V) Low Level 0.637 ug/L EPA 200.8 09/15/2015 18:23 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 100 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 1.7 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 7.0 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Page 26 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030026
Collection Date:10-Sep-15 12:45 PM
Site:Filter Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/16/2015 14:57 ACPAYNE0.05 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 15:24 FCJORDA0.005 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:11 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:11 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 16:11 MHALL30.3 1
Page 27 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030027
Collection Date:10-Sep-15 12:45 PM
Site:Equipment Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 14:18 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 09/11/2015 13:14 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 09/11/2015 13:14 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/15/2015 11:32 ACPAYNE0.05 1
UNDIGESTED METALS BY ICP
Calcium (Ca)2.17 mg/L EPA 200.7 09/16/2015 09:46 FCJORDA0.01 1
Magnesium (Mg)0.074 mg/L EPA 200.7 09/16/2015 09:46 FCJORDA0.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 09/16/2015 09:46 FCJORDA0.1 1
Sodium (Na)< 0.05 mg/L EPA 200.7 09/16/2015 09:46 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.118 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.005 1
Barium (Ba)0.006 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.05 1
Iron (Fe)0.237 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.01 1
Manganese (Mn)0.020 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.005 1
Strontium (Sr)0.014 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 11:22 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 19:14 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 19:14 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 19:14 MHALL30.3 1
Page 28 of 72
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090237
2015030027
Collection Date:10-Sep-15 12:45 PM
Site:Equipment Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L SM2540C 09/14/2015 13:45 CJELLIO251
Total Carbon
TOC 0.303 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 16 mg/L SM2540D 09/11/2015 10:29 CJELLIO51
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.
M4 The spike recovery value was unusable since the analyte concentration in the sample was disproportionate
to the spike level. The associated Laboratory Control Spike recovery was acceptable.
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Page 37 of 72
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QI11072Lot Number:
J15090237Project Number:
AB GW Assessment Water - MayoProject Name:
09/16/2015Date Completed:
Grant Wilton
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QI11072
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: AB GW Assessment Water - Mayo
Project Number: J15090237
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 22
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QI11072

Project Name: AB GW Assessment Water - Mayo
Project Number: J15090237
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/10/2015 09282015030018Aqueous 09/11/2015
002 09/10/2015 10202015030019Aqueous 09/11/2015
003 09/10/2015 09502015030020Aqueous 09/11/2015
004 09/10/2015 14222015030021Aqueous 09/11/2015
005 09/10/2015 14402015030022Aqueous 09/11/2015
006 09/10/2015 13442015030023Aqueous 09/11/2015
007 09/10/2015 10272015030024Aqueous 09/11/2015
008 09/10/2015 14152015030025Aqueous 09/11/2015
009 09/10/2015 12452015030027Aqueous 09/11/2015
(9 samples)
Page: 3 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QI11072

Project Name: AB GW Assessment Water - Mayo
Project Number: J15090237
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 2015030018 Aqueous Alkalinity SM 2320B-590 mg/L 5
001 2015030018 Aqueous Bicarbonate Alkalinity SM 2320B-590 mg/L 5
001 2015030018 Aqueous Methane RSK - 175 8200 ug/L 6
002 2015030019 Aqueous Alkalinity SM 2320B-320 mg/L 7
002 2015030019 Aqueous Bicarbonate Alkalinity SM 2320B-320 mg/L 7
002 2015030019 Aqueous Methane RSK - 175 9300 ug/L 8
003 2015030020 Aqueous Alkalinity SM 2320B-270 mg/L 9
003 2015030020 Aqueous Bicarbonate Alkalinity SM 2320B-270 mg/L 9
003 2015030020 Aqueous Methane RSK - 175 10 ug/L 10
004 2015030021 Aqueous Alkalinity SM 2320B-180 mg/L 11
004 2015030021 Aqueous Bicarbonate Alkalinity SM 2320B-180 mg/L 11
004 2015030021 Aqueous Methane RSK - 175 8600 ug/L 12
005 2015030022 Aqueous Alkalinity SM 2320B-64 mg/L 13
005 2015030022 Aqueous Bicarbonate Alkalinity SM 2320B-64 mg/L 13
005 2015030022 Aqueous Methane RSK - 175 110 ug/L 14
006 2015030023 Aqueous Alkalinity SM 2320B-54 mg/L 15
006 2015030023 Aqueous Bicarbonate Alkalinity SM 2320B-54 mg/L 15
006 2015030023 Aqueous Methane RSK - 175 16 ug/L 16
007 2015030024 Aqueous Alkalinity SM 2320B-13 mg/L 17
007 2015030024 Aqueous Bicarbonate Alkalinity SM 2320B-13 mg/L 17
007 2015030024 Aqueous Methane RSK - 175 12 ug/L 18
008 2015030025 Aqueous Alkalinity SM 2320B-57 mg/L 19
008 2015030025 Aqueous Bicarbonate Alkalinity SM 2320B-57 mg/L 19
(23 detections)
Page: 4 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030018
QI11072-001
09/10/2015 0928
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0002 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0002 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0002 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 590 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 590 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030018
QI11072-001
09/10/2015 0928
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 50 09/16/2015 1559 DCS 85084
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 8200 2ug/L500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030019
QI11072-002
09/10/2015 1020
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0010 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0010 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0010 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 320 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 320 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030019
QI11072-002
09/10/2015 1020
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 20 09/15/2015 1803 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 9300 2ug/L200
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030020
QI11072-003
09/10/2015 0950
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0017 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0017 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0017 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 270 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 270 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030020
QI11072-003
09/10/2015 0950
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1550 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 10 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030021
QI11072-004
09/10/2015 1422
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0024 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0024 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0024 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 180 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 180 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030021
QI11072-004
09/10/2015 1422
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 50 09/16/2015 1609 DCS 85084
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 8600 2ug/L500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030022
QI11072-005
09/10/2015 1440
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0029 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0029 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0029 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 64 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 64 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030022
QI11072-005
09/10/2015 1440
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1617 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 110 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030023
QI11072-006
09/10/2015 1344
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0034 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0034 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0034 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 54 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 54 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030023
QI11072-006
09/10/2015 1344
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1628 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 16 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030024
QI11072-007
09/10/2015 1027
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0039 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0039 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0039 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 13 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 13 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030024
QI11072-007
09/10/2015 1027
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1641 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 12 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030025
QI11072-008
09/10/2015 1415
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0045 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0045 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0045 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 57 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 57 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030025
QI11072-008
09/10/2015 1415
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1820 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 22
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Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030027
QI11072-009
09/10/2015 1245
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/13/2015 0050 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 0050 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 0050 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 22
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Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015030027
QI11072-009
09/10/2015 1245
09/11/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090237
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/15/2015 1831 JJG 85000
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

QC Summary
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:QQ84762-001
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 09/12/2015 220810mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:QQ84762-002
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 110 09/12/2015 221410610090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ85000-001
85000
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 09/15/2015 143810ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ85000-002
85000
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 150 09/15/2015 14049815070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ85000-003
85000
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 140 09/15/2015 14159115070-1307.5 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ85084-001
85084
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 09/16/2015 152910ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ85084-002
85084
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 130 09/16/2015 15058815070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ85084-003
85084
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 130 09/16/2015 15188715070-1300.98 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI11072
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 72 of 72